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DEQ-CFW_00062313
EFFLILIEK Amended Copy) 2007 NPDES PERMIT NO. NC 0003573 DISCHARG NO. 002 MONTH Dece�r ` YEAR 2006 FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. G ddie GRADE 4 PHONE (910) 678-1219 CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberto (2) CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Ray Beard Mail ORIGINAL and ONE COPY to: ATTN: CENTRAL FILES DIV. OF WATER QUALITY DENR 1617 MAIL SERVICE CENTER RALEIGH, NC 27699-1617 X (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS MAR 3 0 ) 007 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE uj C _ o a o 0 o E 0 N O o 50050 00010 00400 00951 00665 00600 00310 00340 FLOW w a� w W ~ s ° w ° O= M ao ° a a z w 0 Z v N p m In °U EFF X INF 0 w B C o tr HRS HRS Y/N MGD "c UNITS Lb/Day mg/L mg/L mg/L mg/L 1 o800 24 Y 12.063 20 8.0 2 o800 24 12.201 3 o800 24 12.295 4 o800 24 Y 12.192 16 7.5 5 0800 24 Y 12.001 17 7.7 1021 0.41 1.14 6 o800 24 Y 11.950 15 7.9 7 0800 24 Y 12.063 16 7.9 8 o800 24 Y 12.249 15 7.7 9 o800 24 14.353 10 o800 24 17.720 1110800 24 Y 10.063 13 8.2 12 0800 24 Y 10.064 13 7.9 614 13 0800 24 Y 11.536 14 8.0 14 o800 24 Y 11.108 16 7.8 15 0800 24 Y 11.257 15 7.8 16 o800 24 11.606 17 080o 24 11.520 18 o800 24 Y 11.622 18 8.0 19 080o 24 Y 11.245 17 7.9 1304 20 o800 24 Y 11.452 14 8.3 21 0800 24 Y 1 11.240 14 8.1 22 o800 24 Y 1 10.958 16 7.2 23 o800 24 10.848 24 o800 24 11.088 25 0800 24 11.052 26 o800 24 Y 10.927 16 7.8 27 o800 24 Y 10.420 17 8.1 912 28 o800 24 Y 10.207 16 7.9 29 o800 24 Y 10.876 16 8.1 30 o800 24 11.193 31 o800 24 11.462 AVERAGE 11.640 16 963 0.41 1 1.14 MAXIMUM 17.720 20 8.3 1304 0.41 1.14 MINIMUM 10.063 13 7.2 614 0.41 1 1.14 Comp. (C) Grab (G) G G I C C C C C Monthly Limit Daily Limit 1 1 6-9 7917 DEM Form MR-1 (12/93) k Holiday DEQ-CFW 00062313 w f Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements 0 Compliant All monitoring data and sampling frequencies do NOT meet permit requirements ICJ Noncompliant If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc., and a time table for improvements to be made. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 22828 N _Barry Hudson - Site Manager Permittee (Please print or type) Signature 87 W. Favetteville. NC. 283044332 (910) 678-1315 Number Date October 31, 2006 Permit Exp. Date PARAMETER CODES 00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total 00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual 00080 Color (Pt -Co) 00610 Ammonia Nitrogen 00082 Color (ADMI) 00625 Total Kjeldhal Nitrogen 00095 Conductivity 00630 Nitrates/Nitrites 00300 Dissolved Oxygen 00310 BOD5 00665 Total Phosphorous 00340 COD 00720 Cyanide 00400 pH 00745 Total Sulfide 00530 Total Suspended 00927 Total Magnesium Residue 00929 Total Sodium 00545 Settleable Matter 00940 Total Chloride 01027 Cadmium 01032 Hexavalent Chromium 01034 Chromium 01037 Total Cobalt 01042 Copper 01045 Iron 01051 Lead 01092 Zinc 01105 Aluminum 01147 Total Selenium 31616 Fecal Coliform 32730 Total Phenolics 34235 Benzene 34481 Toluene 38260 MBAS 39516 PCB's 50050 Flow Chlorine 71880 Formaldehyde 71900 Mercury 81551 Xylene Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at (919) 733-5083, extension 581 or 534 The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data " ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (6). "" If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b) (2) (D) 4 �4 DEQ-CFW 00062314 QW. NCDENR Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Discharge Monitoring Report — December 2006 NPDES Permit No. NC0003573 Dear Sirs: DuPont Fluoroproducts 22828 NC Highway 87 W Fayetteville, NC 28306-7332 March 8, 2007 Enclosed is the amended DuPont — Fayetteville Works' Discharge Monitoring Report for December 2006. The Outfall 002 daily flow for December 18, 2006, was inadvertently omitted on the original DMR submittal. DuPont apologizes for this omission and any inconvenience this may have caused. If you have any questions regarding this matter, please feel free to call me at (910) 678-1155. Environmental Manager Enclosures cc: Mr. Mark Brantley, NCDENR DWQ, Fayetteville Regional Office E.I. du Pont de Nemours and Company DEQ-CFW 00062315 aU PONTe NCDENR Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 RECEIVED MAR t 2 2007 DENR - FAYETTEVILLE REGIONAL OHICE Subject: Discharge Monitoring Report —December 2006 NPDES Permit No. NC0003573 DuPont Fluoroproducts 22828 NC Highway 87 W Fayetteville, NC 28306-7332 March 8, 2007 Dear Sirs: Enclosed is the amended DuPont — Fayetteville Works' Discharge Monitoring Report for December 2006. The Outfall 002 daily flow for December 18, 2006, was inadvertently omitted on the original DMR submittal. DuPont apologizes for this omission and any inconvenience this may have caused. If you have any questions regarding this matter, please feel free to call me at (910) 678-1155. Environmental Manager Enclosures cc: Mr. Mark Brantley, NCDENR DWQ, Fayetteville Regional Office E.I. du Pont de Nemours and Company DEQ-CFW 00062316 AMCoc CoPj� EFFLUENT (Amended Copy) NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 002 MONTH December YEAR 2006 FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE (910) 678-1219 CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2) CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Ray Beard Mail ORIGINAL and ONE COPY to: ATTN: CENTRAL FILES �- j� A DIV. OF WATER QUALITY X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE 1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE 50050 00010 004( FLOW w a N EFF X o 05 Q INF O a o _E ~ rx O W a o v N o v L V N N Q JLu F 0 0 0� z w G 0 C7 O U J O F = ~ n O IL Z U to O J Q 0 eL m a. a 1 2M7 n► t �Fr10N QFRCF e:ee e:ee umsom • e:ee e:ee 1 1. m e: e e m©���___�_______ MMIMIM e:ee 1 mwmm • o:ee 1' mmmm MIMMEM 1 m e: e e m© EHIMEMMEMMEMMM AVERAGE 11.640 16 MAXIMUM- `17,720: .,20 - 8.3i- 304 :0.41 1:14 " - - MINIMUM 10.063 13 7.2 614 0.41 1.14 Comp: (C) Grab"(G) G G _` C C' C= C C Monthly Limit Daily Limit 6=9 7917 DEM Form MR-1 (12/93) * Holiday DEQ-CFW 00062317 Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements^J Compliant All monitoring data and sampling frequencies do NOT meet permit requirements u Noncompliant If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc., and a time table for improvements to be made. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 22828 NC Hwy 87 Permittee Address Barry Hudson - Site Manager Permittee (Please print or type) (910) 678-1315 Phone Number 3 --s_,O Date ir31, 2006 Exp. Date PARAMETER CODES 00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total 00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual 00080 Color (Pt -Co) 00610 Ammonia Nitrogen 01092 Zinc Chlorine 00082 Color (ADM]) 00625 Total Kjeldhal 01027 Cadmium 01105 Aluminum Nitrogen 00095 Conductivity 00630 Nitrates/Nitrites 01032 Hexavalent Chromium 01147 Total Selenium 71880 Formaldehyde 00300 Dissolved Oxygen 01034 Chromium 31616 Fecal Coliform 71900 Mercury 00310 BOD5 00665 Total Phosphorous 32730 Total Phenolics 81551 Xyiene 00340 COD 00720 Cyanide 01037 Total Cobalt 34235 Benzene 00400 pH 00745 Total Sulfide 01042 Copper 34481 Toluene 00530 Total Suspended 00927 Total Magnesium 38260 MBAS Residue 00929 Total Sodium 01045 Iron 39516 PCB's 00545 Settleable Matter 00940 Total Chloride 01051 Lead 50050 Flow Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at (919) 733-5083, extension 581 or 534 The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data * ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B). ** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b) (2) (D) DEQ-CFW 00062318 NPDE$ PERMIT NO. NC 0003573 FACILITY NAME DuPont - Fayetteville Works OPERATOR IN RESPONSIBLE CHARGE (ORC) R CERTIFIED LABORATORIES (1) TBL Laboratory CHECK 13OX IF ORC HAS CHANGED Mail ORIGINAL and ONE COPY to: ATTN: CENTRAL FILES DIV. OF WATER QUALITY DENR �..nu eco%nr.F CFNTER TMS EF NT DISCHARG NO. 001 MONTH December Y,EAR.� 20 CLASS 3 COUNTY Bladen obert J. G ddie GRADE 4 PHONE (910.) 678-1219 Lumbert ) (2> PERSON(S) COLLECTING SAMPLES Robert J. Geddle / Ray Beard X r Pcf C (SIGNATURE OF OPERAT RESPONSIBLE CHARGE) BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS �.n cneac i-1�- � -7 --- --.. ACCURATE AND CO RALEIGH, NC 27699-1617 50050 00010 00400 00310 00530 00556 TG3P6 39700 r FLOW w EFF X �N °- ;� ww me v x Oz FLin INF 0 vO-i = w t°- c=t z 0 IL W N 2K aa >° o w LU m20 F0 _ Oa 1- U HRS HRS YIN � MGD `C UNITS Lb/Day Lb/Day mg/L p/E ug/L 1 'osoo 24 Y 0.800 2 osoo 24 0.688 3 osoo 24 Y 0.712 0.773 19 7.8 40.0 135.4 <5 4 osoo 24 24 Y 0.619 16 8:0 61.4 149.7 5 oso0 Y 0.802 17 8.0 34.8 216.7 6 0800 24 7 o 24 Y 0.732 8 osoo 24 Y 0.797 9 0soo 24 0.604 10 0800 24 Y 0.764 0.700 17 7.8 127.9 2078 11 0800' 24 24 Y 0.768 15 7.9 112.1 211.4 12 0800 Y 0.596 19 7.9 79.5 193.9 13' osoa 24 14 osoo 24 Y 0.963 15 osoo 24 Y 0.721 16 osoo 24 0.868 17' osoo 24 Y 0.838 0.718 22 7.8 50.9 59.9 18 0800 24 24 Y 0.753 22 7.8 23:9 81.6 19 osoo Y 0.664 22 7.9 31.0 116.3 20 osoo 24 21 0800 24 Y 0.728 22 osoo 24 Y 0.678 23 Osoo 24 0.677 24 osoo 24 0.635 25 osoo 24 * Y 0.780 0.520 21 8.2 49.0 81.5 26 osoo 24 24 Y 0.535 16 8.3 14.7 53.5 27' osoo 28 osoo 24 Y 0.539 14 8.1 22.5 67.4 29 osoo 24 Y 0.613 30 0800 24 0.710 31 osoo 24 0.755 0.711 18 54.0 131.3 0 AVERAGE MAXIMUM 0.963 22 8.3 127.9 216.7 <5 MINIMUM 0.520 14 7.8 14.7 53.5 <5 Comp. (C) Grab (G) G G C C G C PASS Monthly Limit 2.00 191.3 H317.08E] 5Daily EJE Limit508.2 DEM Form MR4 (12/93) * Holiday DEQ-CFW 00062319 Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements �J Compliant All monitoring data and sampling frequencies do NOT meet permit requirements Noncompliant If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc., and a time table for improvements to be made. "1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowin ations." Barry Hudson re bf Pe ittet3 " Date 22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 (910) 678-1315 October 31, 2006 Permittee Address Phone Number Permit Exp. Date 00010 Temperature 00076 Turbidity 00080 Color (Pt -Co) 00082 Color (ADM[) 00095 Conductivity 00300 Dissolved Oxygen 00310 BOD5 00340 COD 00400 pH 00530 Total Suspended Residue 00545 Settleable Matter 00556 00600 00610 00625 00630 PARAMETER CODES Oil & Grease 00951 Total Fluoride Total Nitrogen 01002 Total Arsenic Ammonia Nitrogen Total Kjeldhal Nitrogen Nitrates/Nitrites 00665 Total Phosphorous 00720 Cyanide 00745 Total Sulfide 00927 Total Magnesium 00929 Total Sodium 00940 Total Chloride 01027 Cadmium 01032 Hexavalent Chromium 01034 Chromium 01037 Total Cobalt 01042 Copper 01045 Iron 01051 Lead 01067 Nickel 01077 Silver 01092 Zinc 01105 Aluminum 01147 Total Selenium 31616 Fecal Coliform 32730 Total Phenolics 34235 Benzene 34481 Toluene 38260 MBAS 39516 PCB's 50050 Flow 50060 Total Residual Chlorine 71880 Formaldehyde 71900 Mercury 91551 Xylene Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at (919) 733-5083, extension 581 or 534 The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data " ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B). "" If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b) (2) (D) DEQ-CFW 00062320 EFFLUENT NPDES PERMIT NO. INC 0003573 DISCHARGE NO. 002 MONTH December YEAR 2006 FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE (910) 678-1219 CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2) CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Roberti. Geddie / Ray Beard Mail ORIGINAL and ONE COPY to: ATTN: CENTRAL FILES DIV.OF WATER QUALITY X ��%/�� Je'l /-A� DENR (SIGNATURE OF OPERAT IN RESPONSIBLE CHARGE) DATE 1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE 50050 00010 00400 00951 00665 00600 00310 00340 FLOW c EFF X Lu � p0 0 vr I — a `Y INF O 9 1 ys o 0 a o V) w W a oE O(L iwti c NN N O W U LL = J ~ m "}'� ~ a O C 0 G HRS Y/N MGD C UNITS Lb/Day mg/L mg/L mg/L mg/L soo 24 Y 12063 20 800 24 12.201soo _.soo 24 24 Y 12.192 16 7.5 soo2001 17 7 1021 0.41 114 oo 24 Y 11.950 15 7.9 JHRRS oo 24 Y 12.063 oo 24 Y 12.249 15 7.7 soo '24 14 .53oo 24 17.720 oo 24 Y oo 24 Y 10.064 13 7.9 614 oo2400 24 Y 11.108 16 7.8 16 0800 24 Y 11.257 15 7.8 16 0800 24 11.606 97 osoo 24 41520 18 0800 24 Y 18 8.0 19 osoo 24 _....._._. Y 11345 17 7.9 1,304 20 0800 24 Y 11.452 14 8.3 21` osoo 24 _. Y 11.240 14 8.1 22 osoo 24 Y 10.958 16 7.2 23 osoo 24 10'848 24 osoo 24 11.088 25 6800 24 11052 26 osoo 24 Y 10.927 16 7.8 27 0800 24 Y 10420 17 8.1 912 28 080o 24 Y 10.207 16 7.9 29 osoo 24 Y" 10 876 16 8.1 30 0800 24 11.193 31' 0800 24 11..462 AVERAGE 11.640 16 963 0.41 1.14 MAXIMUM 17.720 20 8.3 ' 1304 0.41 1.14 MINIMUM 10.063 13 7.2 614 0.41 1.14 Comp. (C) Grab (G) G G C C C C C Monthly Limit Daily Limit 6-9 7917 DEM Form MR-1 (12/93) * Holiday DEQ-CFW 00062321 Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements 0 Compliant All monitoring data and sampling frequencies do NOT meet permit requirements I�J Noncompliant If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc., and a time table for improvements to be made. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are si ificant penalties for submitting false information, including the possibility of fines and imprisonment for wing violaf L Date 22828 NC Hwy 87 W, Fayetteville, NC, 2t306-7332 (910) 678-1315 October 31, 2006 Permittee Address Phone Number Permit Exp. Date PARAMETER CODES 00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total 00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual 00080 Color (Pt -Co) 00610 Ammonia Nitrogen 00082 Color (ADMI) 00625 Total.Kjeldhal Nitrogen 00095 Conductivity 00630 Nitrates/Nitrites 00300 Dissolved Oxygen 00310 BOD5 00665 Total Phosphorous 00340 COD 00720 Cyanide 00400 pH 00745 Total Sulfide 00530 Total Suspended 00927 Total Magnesium Residue 00929 Total Sodium 00545 Settleable Matter 00940 Total Chloride 01027 Cadmium 01032 Hexavalent Chromium 01034 Chromium 01037 Total Cobalt 01042 Copper 01045 Iron 01051 Lead 01092 Zinc 01105 Aluminum 01147 Total Selenium 31616 Fecal Coliform 32730 Total Phenolics 34235 Benzene 34481 Toluene -38260 MBAS 39516 PCB's 50050 Flow Chlorine 71880 Formaldehyde 71900 Mercury 81551 Xylene Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at (919) 733-5083, extension 581 or 534 The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data * ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B). ** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b) (2) (D) �v , Iil DEQ-CFW 00062322 EFFLUENT NPDES PERMIT NO. NC 0003573 DISCHARGE NO. 006 MONTH December YEAR 2006 FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen OPERATOR IN RESPONSIBLE CHARGE (ORC) Robert J. Geddie GRADE 4 PHONE (910) 678-1219 CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2) CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Robert J. Geddie / Ray Beard Mail ORIGINAL and ONE COPY to: ' ATTN: CENTRAL FILES DIV. OF WATER QUALITY X I DENR (SIGNATURE OF OPERA OR IN RESPONSIBLE CHARGE) 1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS vni Gir.N N(: 97R9A-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE / -/�(- 0,7 DATE DEM Form MR-1 (12/93) DEQ-CFW 00062323 Facility Status: (Please check one of the following) All monitoring data and sampling frequencies meet permit requirements L� Compliant All monitoring data and sampling frequencies do NOT meet permit requirements 77 Noncompliant If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation, maintenance, etc., and a time table for improvements to be made. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for si, it ' e information, including the possibility of fines and imprisonment for knoyiola ' ns." H v/-Z� Date 22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 (910) 678-1315 October 31, 2006 Permittee Address Phone Number Permit Exp. Date PARAMETER CODES 00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total 00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual 00080 Color (Pt -Co) 00610 Ammonia Nitrogen 00082 Color (ADMI) 00625 Total Kjeldhal Nitrogen 00095 Conductivity 00630 Nitrates/Nitrites 00300 Dissolved Oxygen 00310 BOD5 00665 Total Phosphorous 00340 COD 00720 Cyanide 00400 pH 00745 Total Sulfide 00530 Total Suspended 00927 Total Magnesium Residue 00929 Total Sodium 00545 Settleable Matter 00940 Total Chloride 01027 Cadmium 01032 Hexavalent Chromium 01034 Chromium 01037 Total Cobalt 01042 Copper 01045 Iron 01051 Lead 01092 Zinc 01105 Aluminum 01147 Total Selenium 31616 Fecal Coliform 32730 Total Phenolics 34235 Benzene 34481 Toluene 38260 MBAS 39516 PCB's 50050 Flow Chlorine 71880 Formaldehyde 71900 Mercury 81551 Xylene Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at (919) 733-5083, extension 581 or 534 The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data * ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B). ** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506 (b) (2) (D) i� DEQ-CFW 00062324 4M. N.C. Division of Water Quality Attn: Central Files 1617 Mail Service Center Raleigh, NC 27699-1617 DuPont Fluoroproducts Fayetteville Works Plant 22828 NC Highway 87 West Fayetteville, NC 28306-7332 January 22, 2007 DISCHARGE MONITORING REPORT — December 2006 Attached is E. I. DuPont de Nemours & Company, Inc., Fayetteville Works Discharge Monitoring Report for the month of December 2006. If you have any questions, please contact Robert Geddie at (910) 678-1219. RJG: sns Attachment cc: Ken Cook - ENGR, Old Hickory R. J. Geddie - FW M. E. Johnson - FW G. G. Santiago- FW File: F-1-3-4 E.I. du Pont de Nemours and Company DEQ-CFW 00062325 acC.Or DEQ-CFW 00062326