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HomeMy WebLinkAboutDEQ-CFW_00061366pp- DUPONT - FAYETTEVILLE WORKS RENEWAL APPLICATION 1 _. NPDES PERMIT NC0003573 �J AY - 2 2006 MAY 1, 2006 DEQ-CFW 00061366 FORM U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. Number 9 TEA c 1 GENERAL INFORMATION GENERAL Consolidated Permits Program F NC0003573 D 1 2 3 14 15 Read the "General Instructions" before starting.) LABELITEMS S GENERAL INSTRUCTIONS If a preprinted label has been provided, affix it in the designated space. F NC0003573 Review the information carefully; if any of it is incorrect, cross through it and enter the correct data in the appropriate fill --in area below. Also, if any of the DuPont Fayetteville Works y 828 NC Hwy 87 W Fayetteville, preprinted data is absent (the area to the left of the label space lists the information that should appear), please provide it in the proper fill --in area(s) ER, NC 28306-7332 below. If the label is complete and correct, you need not complete Items, I, III, V, and VI (except VI-B which must be completed regardless). Complete all 22828 NC Hwy 87 W DUart items if no label has been provided. Refer to the instructions for detailed item Township, NC 28306 descriptions and for the legal authorizations under which this data is collected. OLLUTANT CHARACTERISTICS 11N RUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, must submit this form and the supplemental form listed in the parenthesis following the questions. Mark "X" in the box in the third column if the supplemental form is attached. If you answer "no" to each question, you need not submit any of these forms. You may answer "no" if your activity is excluded from permit requirements; see Section C of the instructions. See also, Section D of the instructions for definitions of bold --faced terms. MARK'X' MARK'X' SPECIFIC QUESTIONS YES NO FORM ATTACHED SPECIFIC QUESTIONS YES NO FORM ATTACHED A. Is this facility a publicly owned treatment works B. Does or will this facility (either existing or proposed) include a which results in a discharge to waters of the U.S. ? X concentrated animal feeding operation or aquatic animal pro- X (FORM 2A) duction facility which results in a discharge to waters of the U.S? 16 17 iB t9 21 FORM 26 C. Is this a facility which currently results in discharges X X D. Is this a proposed facility (other than those described in A or B X to waters of the U.S. other than those described in above) which will result in a discharge to water of the U.S. ? 22 23 24 25 26 27 A or B above FORM 2C FORM 2D E. Does or will this facility treat, stare, or dispose of F. Do you or will you inject at this facility industrial or municipal hazardous wastes? (FORM 3) X effluent below the lowermost stratum containing, within one quarter mile of the well bore, underground sources of drinking X 26 29 30 31 33 wateR FORM 4 G. Do you or will you inject at this facility any produced H. Do you or will you inject at this facility fluids for special process, water or other fluids which are brought to the surface such as mining of minerals, in situ combustion of fossil fuel, in connection with conventional oil or natural gas pro- X or recovery of geothermal energy ? X duction, inject fluids used for enhanced recovery of (FORM 4) oil or natural gas, or inject fluids for storage of liquid 34 35 36 37 36 89 hydrocarbons? FORM 4 1. Is this facility a proposed stationary source which is J. Is this facility a proposed stationary source which is NOT one one of the 28 industrial categories listed in the in- X of the 28 industrial categories listed in the instructions and X structions and which will potentially emit 100 tons and which will potentially emit 250 tons per year of any air per year of any air pollutant regulated under the pollutant regulated under the Clean Air Act and may effect Clean Air Act and may affect or be located in an or be located in an attachment area'? (FORM 5) 49 41 42 43 44 45 attainment area ? FORM 5 III. NAME OF FACILITY E.I. du Pont de Nemours & Compan CONTACT 9�; IV. FACILITY A. NAME & TITLE (Last, first, & Title) B. PHONE (area code & no 2 Michael E. Johnson, Environmental Manager (910) 678 1155 75 45 46 - 48 49 - 51 16 1 V. FACILITY MAILING ADDRESS A. STREET OR P.O. BOX iX53 22828 NC Hwy87 W 45 B. CITY OR TOWN C. STATE D. ZIP CODE -" 4 Fayetteville NC 2830677332 15 Vt. 76 40 41- 42 FACILITY LOCATION A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER - 5 22828 NC Hwy 87 W 45 15 B. COUNTY NAME- Bladen 48 70 C. CITY OR TOWN D. STATE E. DP CODE F. COUN'CODE - �1 4 Duart Township NC 1147 28306 a--- J 15 18 40 EPA Form 3510-1 (8-90) *(1) Permitted under Federal and State Laws No Forms 3 or 4 required - see Attachment'1-1 DEQ-CFW 00061367 CONTINUED FROM THE FRONT VII. SIC CODES (4-d1g1L1—darcrpdcdb) A. FIRST B. SECOND 7 2869 (specify) Nafion® Solution, Vinyl Ether and HFPO monomers 7 2821 (specify) Teflon® FEP resin, Polyvinyl flouride resin Polyvinyl butyral Resin, Nafion® Resins C. THIRD D. FOURTH j 3081 (specify) Nafion® Membrane, (specify) Butacite® sheeting, SentryGlas Plus VIII. OPERATOR INFORMATION MM B. Is the name listed in Item VIII-A also the A. NAME owner? c Yes ❑ No 16 E. I. DuPont de Nemours & Co., Inc. 55 66 C. STATUS OF OPERATOR (e�le,rhe aP ro ' I kit msa„swa�b— Y'o d-,, s � .1 D. PHONE NUMBER area code6no.J F= Federal M= Public (ofh—han redeal —W,) o=one (aPaer, P=P&v . �S=S— (specify) njq 302 r48- 774 49 - 51 1000 52 - 55 E. STREET OR P.O. BOX 1007 Market Street 45 C. STATE D. ZIP CODE IX. INDIAN LAND F. CITY OR TOWN Wilmington DE Is the facility located on Indian 19898 s Lands? 15 16 40 1 41 42 47 st 52 Q Yes ® No X. EXISTING ENVIRONMENTAL PERMIT A. NPDES (Discharges to Surface Water - - D. RSSB Air Emissions from PTposed Sources T H19 NC0003573 9 15 16 11 Title V - 03735T28 (Major Source) 5 i6 17 30 B. UIC (Underground Injection of Fluids E. OTHERS (Specify) (specify) T I 9 17 NA 9 NA 15 16 15 1 16 17 30 C. RCRA Hazardous Wastes D. OTHERS (Specify) (specify) 9 NA 15 15 17 30 9 J= NCD 047 368 642 and 90 day storage areas 15 16 XI. MAP 17 Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of XII. NATURE OF BUSINESS (provide a brief description) > Manufacturing of DuPontTm Teflon® FEP resin. > Manufacturing of DuPontTM SentryGlas Plus® . > Manufacture of DuPontTm Nafion® Membrane, Nafion® Resins, Nafion® Solution, FLPR Vinyl Ether and HFPO monomers > Manufacture of Polyvinyl butyral (PVB) Resin and DuPontTM Butacite® Interlayer plastic sheeting > Manufacture of Ammonium perfluorooctanoate (APFO) > Manufacture of Polyvinyl flouride resin (PVF) XIII. CERTIFICATION (see instructions) I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information cont A. NAME & OFFICIAL TITLE (type or print) B. SIGNATUREC. DATE SIGNE Barr L. Hudson, Plant Mgr4 -A COMMENTS FOR OFFICIAL USE ONLY 8 5 16 EPA Form 3510-1 (8-90) DEQ-CFW 00061368 Form Approved. EPA I.D. NUMBER OMB No. 2040-0086 Please print or type in the unshaded areas NCO003573 only. F 7 Approval expires 8-31-98 U.S. ENVIRONMENTAL PROTECTION AGENCY FORM APPLICATION FOR PERMIT TO DISCHARGE WASTEWATER 20 EXISTING MANUFACTURING, COMMERCIAL, MINING AND SILVICULTURAL OPERATIONS NPDES Consolidated Permits Program [,,djT LO CATION , OC N L ATIO For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water. A.OU I I -ALL - NUMBER B. LATITUDE C. LONGITUDE D. RECEIVING WATER (hame), (list), DEG, - 2. MIN. ,& SEC. 1 DEG-. 2. MIN. 3. SEC. 001 34 50 25N 78 50 9W Cape Fear River via Outfall 002 002 34 50 22N 78 50 9W Cape Fear River 006 34 50 20N 78 49 55W Cape Fear River via Outfall 002 II. FLOWS, SOURCES 6F.P6LLUTIONj AND TREATMENT TECHNOLOGIES A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations, treatment units, and outfalls. If a water balance cannot be determined (e.g., for certain mining activities), provide a pictorial description of the nature and amount of any sources of water and any collection or treatment measures. B. For each ouffall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water, and storm water runoff, (2) The average flow contributed by each operation; and (3) The treatment received V the wastewater. Continue on additional sheets if necessary. 1 OUTFACE NO 2 OPERATION N CON b AVERAGE PLOW 4 LIST CODES PROM: &-OPERATION�(ZiOQ DESCRIPTION uni S vist) 002 Outfall 001 965,039 GPD Discharge to Surface Water (Cape Fear River) 4-A Outfall 006 100,000 GPD Non -contact water 15,220,755 GPD Boiler B/D, Stormwater 193,000 GPD TOTAL 16,478,794 GPD 001 NAFION AREA: Biological Wastewater Treatment Plant: - Neutralization 61,429 GPD - WWT Influent Sump 1-0 - Treaters & FPX Process 12,286 GPD - Equalization (equipped with Mixing & Aeration) 1-0; 3-E - MMF Process & Scrubber 12,286 GPD - Emergency Retention Tank 1-0 BUTACITE AREA: - Pre -Digester Tank 3-E - Flake 665,760 GPD -Activated Sludge Tank 3-A - Extrusion 1,329 GPD - Clarification (2 in -ground in parallel) 1_U - Recycle 292,350 GPD SENTRY GLASS AREA - Quench & Wash 10,000 GPD TEFLON AREA - EPS Tape Quench & Wash 10,000 GPD - TRX Cutters & Scrubbers 45,000 GPD Neutralized Regenerate 50,000 GPD Sanitary Sewer 8,000 GPD Contact Stormwater 12,000 GPD TOTAL 1,180,439 GPD 006 PVF PROCESS 100,000 GPD Solids Separation I_U TOTAL 100,000 GPID .......... - ...... . ......... - - ....... ...... ...... ...... .... . ...... . ....... ...... .. . ......... ......... . ......... _ :_. ': --- b-cat 96 ..... ........ ...... . ... ....... EPA Form 3510-2C (8-90) PAGE I of 4 CONTINUE ON PAGE 2 DEQ-CFW-00061369 CONTINUED FROM PAGE 1 Except for storm runoff, leaks or spills, are any of the discharges described in Items II -A or B intermittent or seasonal? YES (complete the following table) X �NO (go to Section /ll) A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility? X YES (complete Item 111-8) IINO (go to Section IV) B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)? I YES (complete Item 111-C) I X �NO (go to Section IV) C. If you answered "Yes" to Item II I-B, list the quantity which represents an actual measurement of your level of production expressed in the terms and units used in the applicable effluent guideline, and indicate the affected outtalls. Not applicable Wo production based applicable effluent guidelines Are you now required by any Federal, State or Local authority to meet any implementation schedule for the construction, upgrading, or operation wastewater treatment equipment or practices or any other environmental programs which may effect the discharges described in this plication? This includes but is not limited to, permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, pulations, court orders, and grant or loan conditions. YES (complete the following Table) J X INO (go to Section /V-8) OPTIONAL: You may attach additional sheets describing any additionat water pouutton control programs torotner environmental projects wnicn may affect your discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned and indicate your actual or planned schedules for construction. I (MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED orm 3510-2C (8-90) PAGE 2 OF 4 CONTINUE ON PAGE 3 DEQ-CFW 00061370 EPA I.D. NUMBER (copy from Item 1 of Form 1) NC0003573 CONTINUED FROM PAGE 2 Form Approved. OMB No. 2040-0086 4pproval expires 8-31-98 V. INTAKE AND EFFLUENT CHARACTERISTICS A, B, & C : See instructions before proceeding -Complete one set of tables for each outfall -Annotate the outfall number in the space provided. Note: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9. D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession. 1 POI:.LUTANT 2. SOURCE i.:POLLUTANT 2. SOURGE None of the pollutants listed in Table 2C-3 of the instructions are believed to be present in the discharge. VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct? YES (list all such pollutants below) C_�NO (go to Section VI-8) Applicable guidelines require testing all V-C compounds identifying any potential discharges EPA Form 3510-2C (8-90) PAGE 3 OF 4 CONTINUE ON PAGE 4 DEQ-CFW 00061371 CONTINUED FROM PAGE 3 VII. BIOLOGICAL TOXICITY TESTING DATA Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in relation to your discharge within the last 3 years? r X YES (identify the test(s) and describe their purposes below) I �NO (go to Section Vlll) North Carolina c. dubia Chronic Pass/Fail Reproduction Toxicity Tests performed each quarter in accordance with NPDES permit conditions. No toxicity effect reported during last 3 years of testing final discharge. NC DENR has copies of test results submitted with DMRs last 3 years. Vill. CONTRACT ANALYSIS INFORMATION Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm? r X YES (list the name, address, and telephone number of, I �NO (go to Section W and pollutants analyzed by, each such laboratory or firm below) A. NAME B ADDRESS . TELEPHONE (area cArle D ROLLUTANT;ANALYM. (ffst) : .....:. _..-. na Pace Analytical 2225 Riverside Drive, 828.254.7176 Aquatic Toxicity Services, Inc. Ashville, NC 28804 TBL 2401 W. 5th Street 910.738.6190 Lumberton, NC BOD5, COD, TSS, Priority Pollutants, Fluoride, Total Phosphorous, Total Nitrogen IX. CERTIFICATION I certify under penalty of law this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations. A. NAME & OFFICIAL TITLE (type of print) B. PHONE NO. (area code & no.) Barry L. Hudson, Plant Mgr (910) 678-1247 C. SIGNATURE % D. DATE SIGNED ;6AAA,i K EPA Form 3510-2C (8-ri PAGE 4OF4 DEQ-CFW 00061372 DuPont Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information Supplemental Information — Permit Renewal Application — May 1, 2006 Current Site Water Management Process wastewater and stormwater from the various manufacturing areas are collected in the respective area sumps and ultimately conveyed via a gravity flow underground process sewer pipe to the site's central wastewater treatment plant (WWTP). Sanitary sewage is conveyed via a separate underground sewer system to the WWTP. The permitted flowrate of the WWTP is 2.0 MGD, with an actual average flowrate of approximately one MGD. This process wastewater is commingled in the WWTP Influent Sump where it is pumped to an 850,000-gallon Equalization Basin. The Equalization Basin is mixed with two floating submerged mixers. Three floating surface aerators in the basin cool and aerate the incoming wastewater. A 175,000-gallon Emergency Retention Tank is available for temporary storage of wastewater which may need additional treatment or acclimation in the WWTP activated sludge process at a controlled rate that allows for proper biological treatment. Wastewater from the Equalization Basin is normally pumped to a 250,000-gallon Predigester Tank in which initial biological activity with the WWTP activated sludge begins. The Predigester Tank is aerated. The partially treated wastewater from the Predigester Tank is pumped to a 1,700,000-gallon Aeration Tank. The Aeration Tank is the site of the majority of the biological activity. The Aeration Tank is aerated primarily by a diffused air system located in the bottom of the tank. The tank can have supplemental aeration via a floating BiomixerO that injects air through submerged rotors. The biologically treated wastewater is then sent to two in -ground clarifiers (119,000 gallons and 168,000 gallons respectively) in parallel. The clarified treated effluent is discharged to and through Outfall 001. The wasted sludge is sent to a Dissolved Air Floatation (DAF) unit, then to a 47,000 gallon Sludge Storage Tank, and finally to a Rotary Filter for thickening. The thickened sludge is dewatered in a Sludge Press, and can be dried in a steam -heated dryer for additional moisture removal. The dewatered and/or dried sludge is transported off -site to a commercial Subtitle D landfill. Non -contact process cooling water and non -process stormwater are conveyed via surface ditches to the site's Woodlined Ditch. In addition, excess riverwater flow and Outfall 001 effluent are discharged directly to the Woodlined Ditch. The combined, total flow of water from the site is discharged and monitored at Outfall 002. The Outfall 002 maximum 30-day average flow was 16.3 MGD during the period from 2005 to 2006. Flow variability at Outfall 002 is from 3.0 to 18.6 MGD, however, flow can consistently be in the 16.3 MGD range. DEQ-CFW 00061373 DuPont Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information Proposed Changes in Operations PVF Manufacturing Facility: The DuPont Company — Fayetteville Works has been selected as the location for the DuPontTM Polyvinyl Fluoride (PVF) manufacturing process. The manufacturing facility is in the process of being designed, and will produce PVF polymer resins. PVF resin to be manufactured at the Fayetteville plant is used in DuPontTM Tedlar® fluoropolymer film business. Tedlar® film is manufactured at other DuPont site location (not the Fayetteville plant). Tedlar® is used in the photovoltaic industry in photovoltaic cells and the aircraft industry for interior cabin surfaces, as well as many other uses. This new facility construction will be completed in August 2007 and begin start up in October 2007. The manufacturing facility will be located near the existing Teflon® FEP resin manufacturing area. This process will produce polyvinyl fluoride (PVF) resin (CAS No. 24981-14-4). As with most fluorochemical processes, the wastewater from the PVF manufacturing process is expected to have very little or no biological oxygen demand (BOD5) value. Treatability tests have been performed on samples from another DuPont site which currently manufactures PVF. These studies have indicated use of non -biological treatment will meet effluent limitation of OCPSF NSPS guidelines of Subpart D—Thermoplastic Resins (40 CFR 414.40). DuPont proposes to discharge the treated wastewaters from this new facility through a currently permitted outfall, designated as Outfall 006. The contact process wastewater and stormwater will be treated with solids separation technology prior to discharging to the outfall. A suggested change to the language of the current permit's narrative for Outfall 006 that would accommodate the new PVF Manufacturing Facility follows: "Beginning on the effective date of this permit and lasting through the expiration date, the Permittee is authorized to discharge from Outfall 006 (Polyvinyl fluoride Manufacturing Facility low -biodegradable process wastewaters). Such discharges shall be limited and monitored by the Permittee as specified below:" The process wastewater is expected to contain unreacted vinyl fluoride (CAS No. 00075-02-5). The anticipated quantity of vinyl fluoride from the PVF Manufacturing Facility is 0.312 pounds per day. This quantity would equate to 0.9 mg/L vinyl fluoride at Outfall 006 and 0.0035 mg/L vinyl fluoride at Outfall 002. Finally, non -contact cooling, condensate, and stormwater from the PVF Manufacturing Facility will be discharged directly to Outfall 002 via the site's Woodlined Ditch. DEQ-CFW 00061374 DuPont Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information Current Operating Conditions Butacite@ Manufacturing: The DuPont Company — Fayetteville Works' Butacite& manufacturing area produces two final products. DuPontTM Butacite& Interlayer plastic sheeting is the final product used in safety glass such as automobile windshields. Polyvinyl butyral (PVB) resin is shipped off -site as a transfer to other DuPont locations for final processing. Wastewater generated from this manufacturing facility is treated in the site's biological wastewater treatment plant (WWTP). Nafion@ Manufacturing: The DuPont Company — Fayetteville Works' Nafion0 manufacturing area produces five final products. DuPontTM Nafion0 Membrane is a plastic film used in the chloroalkali industry and in electrochemical fuel cells. Nafion0 Resins are ultimately extruded into a finished film. The FLPR Vinyl Ether and HFPO monomers are shipped to other DuPont locations to produce various fluorochemical products such as DuPontTM TeflonO. Wastewater generated from this manufacturing facility is neutralized and discharged to the WWTP. Teflon@ Manufacturing: The DuPont Company — Fayetteville Works' PMDF Teflon@ manufacturing area produces DuPontTM TeflonO FEP resin. Teflon@ FEP resin is used in the electronics industry as a coating for wire, as well as many other uses. This facility was constructed in 1999-2000 and was started up in December 2000. Wastewater generated from this manufacturing facility is treated in the WWTP. APFO Manufacturing: The DuPont Company — Fayetteville Works' APFO manufacturing area produces ammonium perfluorooctanoate. The APFO produced in this unit is used to produce fluoropolymers and fluorinated telomers, but none of the produced APFO is used at the Fayetteville Works site. This facility was started up in November 2002. All wastewater generated from this manufacturing facility is collected and shipped off -site for disposal. No process wastewater from this manufacturing facility is discharged to the site's biological WWTP or to the Cape Fear River. SentryGlas@ Plus Manufacturing: The DuPont Company — Fayetteville Works' SentryGlas@ Plus manufacturing area produces DuPontTM SentryGlas@ Plus ionoplast interlayer laminate. SentryGlas& Plus interlayer is used for laminated safety glass in side, rear, and overhead automobile windows. It is also used in architectural applications desiring safety glass. This facility was started up in June 2005. There is no contact process wastewater generated from this manufacturing facility, therefore only sanitary waste from this area is treated in the WWTP. This manufacturing facility does discharge non -contact cooling water to the woodlined ditch and ultimately to Outfall 002. DEQ-CFW 00061375 DuPont Company — Fayetteville Works NPDES Permit No. NC0003573 Supplemental Information Form 2C Permit Application Data Unavailable Priority Pollutants, special conventional and non -conventional analysis required testing results were not available at the time of Permit Application submittal. This data will be submitted when lab reports are received and input into the Form 2C as an appendum. These absent analytical results are indicated with an asterisk (*) on the Form 2C, Pages V-1 through V-9. Data Abnormalities When compiling the Outfall analytical database to perform the statistical analysis required in Form 2C, there were several apparent data abnormalities reported in the DMRs. These abnormalities, whether analytical or sampling event derived, are worth noting and or correcting in the Form 2C as they are misleading of representing the discharge from the site. Data Noted: On 11/08/05 a COD value of 102 mg/L was reported for Outfall 002 at a high flow rate of 13.3 MGD resulting in a calculated mass of 11,292 lb/day. Upon review of Outfall 001 data and site's operating conditions, this value appears in error and the corresponding mass discharge is believed to be incorrect. As with all analytical results when retains are not available for retest, one must apply logic based on available information. This value was still reported in the 2C data, but noted here as to the possible error. Data Revised: Total Phosphorus is monitored at Outfall 002 once a month. On site there is only one potential source of phosphorus. The Butacite® operation uses phosphoric acid in the batch operation. During the months of December and March 2005, the maximum number of batches in a given day was twenty (20) batches. The quantity of phosphoric acid "as Phosphorus" in each batch is 4.7 lb/batch or a maximum of 94.5 lb/day "Total Phosphorus" potentially being discharged. This value is in line with what is normally reported 15 to 50 lbs per day which will vary as biological uptake will occur as well as equalization within the biological treatment system. Any value grossly in excess of 95 lb/day Phosphorus is highly probable in error, either analytical or sampling, and not representative of operations, therefore misleading. In March 2005, a concentration of 307 ppm was reported and a respective 14,092 lb Total P/day in the discharge. In December 2005, a concentration of 10.7 ppm was reported and a respective 1,040 lb Total P/day in the discharge. In both cases these values are orders of magnitude greater than what can physically be used and processed through manufacturing much less through biotreatment and are evidently grossly in error. The likely scenario is either typographic or analytical dilution calculation errors, in which both cases would be decimal place transposing errors. Rather than just not include these two data points, for purposes of the Form 2C reporting we chose to revise the numbers from 307 ppm to 0.307 ppm and 10.7 ppm to 0.107 ppm and respective mass discharge of 14.092 and 10.4 lbs P/day. These are in ranges of normal reported values of the time periods of concern and more in line with likely amounts from the operating unit. DEQ-CFW 00061376 %Sow UNITED STATES DEPARTMENT OF THE INTERIOR GEOLOGICAL SURVEY 7@° 34' 52' 30 -"60" 3f 3E 50 K if 31 47' 30 DUART QUADRANGLE NORTH CAROLINA 7.5 MINUTE SERIES (TOPOGRAPHIC) w SPJ4 SHIM' PAm is, QUADRANGLE 'v STATE OF NORTH CAROLINA DEPARTMENT OF NATURAL RESOUR AND COMMUNITY DEVELOPMENT RALEIGH. N. C. DEQ-CFW 00061377 w t , } K � s t 3R y OUTFALL / Y � f. Form 2C, Part III B: NPDES PERMIT APPLICATION WATER BALANCE (Revised 4115106) DuPont - Fayetteville, NC Flows Unit: GPD Basis: All Production Manufacturing, using Maximum 30 day average of measured flows �� Cape Fear River ,_� Outfall 002 161,420,194 Chlorine NON -CONTACT 16„. Or — — — — — Non -Contact Cooling Water - - - ► 13 Q43 T55 tottram each - - - - - - F------------------------------------------------------------ -- 15r003r755,------------ unEt--——— ———— — —— —— t 1 -:�.. eac AiOn I Filtered Water Supply DEMMERALIZERS ',r vt Neutralized Regenerate Chlorine Potable Water Supply Plant Sanitary I I BOILERS Facilities I Stormwater I Stormwater from Process Area Pads Non -process Stormwater DYMETROL EPS TAPE TRX QUENCH & QUENCH & CUTTERS & WASH WASH SCRUBBERS l j I BUTACITE FLAKE I EXTRUSION RECYCLE 45,000 1 5,000 NAFION CAUSTIC ACID TREATERS & FPX MMF SCRUBBERS I SCRUBBERS PROCESS I PROCESS & SCRUBBERS NEUTRAL- DMSO IZATION STILL 700 ' Biological WWTP [W11losol'J.d's +To nd£II Dis osal............................................[To La i BIOSOLIDS I SOLID WASTE ! 1 Outfall 001 rewi I1111tI.1 PVF Physical Solids Separation Treatment Product Loss & Unit Evaporation I 967,70.0 'l DEQ-CFW 00061379 PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or a6 of this in(ormallon on separate sheets (use the same fomud) Instead of compleft these pages. SEE INSTRUCTIONS E.P. A. I.D. Number (copy from Item 1 of Form 1) NC0003573 -j Fonn Approved OMB No. 2040 0086 Approval ezplres 831-98 V. INTAKE & EFFLUENT CHARACTERISTICS (Continued from page 3 of Form 2-C) f '„• ourFALL No. ons r a ona a s. PART A -YOU mu pro e e resums or at leastone analysis tor every pollutant n this table. Complete one e r eac o n 001 2 EFFLUENT 1. POLLUTANT AND CAS 3. UNITS 4. INTAKE (op6onap NO a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (gavailabla) b. LONG TERM AVRG. VALUE (if ays"s) d. NO. OF ffblank) a LONG TERM AVERAGE VALUE CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS a CONCEN'rRAT1ON b. MASS (1) CoNCENTRAn (2) Mass (ffavaUable) ANALYSES b. NO. OF ANALYSES a. Biochemical Oxygen Demand 3 77.0 2981.2 33.30 265.90 9.70 72.30 169 MG/L PPD NA NA (SOD) NA b. Chemical NA Oxygen Demand * NA NA NA * MG/L PPD NA NA (GOD) c. Total Organic * Carbon (TOC) * NA NA NA * MG/L PPD d. Total Suspended NA NA NA Solids (TSS) 56.0 349.3 26.70 169.80 18.90 133.20 169 MG/L PPD NA NA NA e. Ammonia (as N) * * NA NA NA NA MG/L PPD NA NA NA f. Flow value 1.30 value 1.0 value value 0.9 395 MGD NA NA g. Temperature value value value 23.0 value (winter) 117.2 79 "C8.7 h. Temperature value NA NA value value 30.0 (summer) 23.0 21.0 88 cc value NA NA Minimum Maximum Minimum Maximum i. pH 6.9 8.0 NA NA 167 PART B-Mark "X" in column Za for each pollutant you know or have reason to all Alh- believe is Mark "X" in present column 2b for each pollutant you believe to be absent If you mark column 2a for any pollutant which is limited either directly, or Indirectly but expressly, In an effluent limitations guideline, you must provide the results of at least one analysts for that pollutant For other pollutants for which you mark column 2a, you must data provide quantitative or an explanation of their presence In your discharge. Com late one table for each outfall. See the instructions for additional details and requirements. i MARK)' & EFFLUENT 4. UNITS 5. INTAKE (opllona!) b. MAXIMUM 30 DAY VALUE (if avallable) m LONG TERM AVRG. VALUE (ff b. NO. OF MA1meuM DAILY VALUE avallable) a. LONG TERM AVERAGE VALUE ANALYSES I. POLLUTANT & CAS NO. D. NO. OF pfavatlable) a BELIEVED a BELIEVED (1) CONCENTRAMN (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES (1) (2) MASS (1) CONCENTI7ATION (2) MASS PRESENT ABSENT CONCENTRATION a. Bromide (24959-67-9) X NA NA NA NA* • b. Chlorine NA NA NA Total Residual X * i • • i c. Color X * • NA NA NA NA i i i NA NA NA NA NA NA d. Fecal Colfform X i i NA NA NA NA • • i NA NA NA e. Fluoride (16984-48-8) X i i NA NA NA NA f. Nitrate— NA NA NA Nitrite (as N) X NA NA NA NA • • t FDA C- 2r.4n_9P 10_nn1 NA NA NA nW= lr! 1 ITEM V-B CONTINUED FROM PREVIOUS PAGE I- POLLUTANT AND CASE NO 2. MARK "X' 3. EFFLUENT 4. UNITS 5. INTAKE (optional) MAXWUM DAILY VALUE b. NAMUM 30 DAY VALUE at -affawe) a LONG TERM AVRG. VALUE (9 BELIEVED (ffa-ftWe) d. NO. OF a. LONG TERM AVERAGE VALUE a. PRESENT ABSENT CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS b. NO. OF ANALYSES g. Nitrogen, Total Organic (as N) x NA NA NA NA NA NA NA h. Oil and Grease x 28 223 28 223 NA NA- 14 MG/L PPD NA NA NA I. Phosphorus (as P), Total x NA NA NA NA NA NA NA (7723-14-0) NA NA NA L -4� NA NA NA (1) Alpha, Total x NA NA NA NA NA NA (2) Beta, Total x NA NA NA NA NA (3) Radium, total x NA NA FZK- NA NA NA NA NA (4) Radium 226 Total x NA NA NA NA NA NA k. Sulfate (as SO4) NA NA —NA (14808-79-8) , x NA NA NA NA NA NA NA I. Sulfide (as S) x NA NA NA NA NA NA NA m. Sulfite (as S03) (14266,45-3 x NA NA NA NA NA NA NA n. Surfactants x NA NA NA NA NA NA NA o. Aluminum, Total (7429-90-5) x NA NA NA 1 NA NA NA NA p. Barium, Total 1 (7440-39-3) x NA NA NA NA NA NA NA q. Boron, Total (7440-42-8) x NA NA NA NA NA NA NA r. Cobalt, Total (7440-48-4) x NA NA 1 NA NA NA NA NA s. Iron, Total (7439-89-6) x NA MA 1 NA NA NA NA NA t. Magnesium (7439-95-4) x NA NA NA NA NA NA NA u. Molybdenum, Total (7439-98-7) x NA NA NA NA NA NA NA v. Manganese, (7439-96-5) x NA NA NA NA NA NA NA w. Tin Total (7440-31-5) x NA NA NA NA NA NA NA x. Tltanium,Total (7440-32-6) IMDA C A ^ 1. nm x NA NA NA 1 NA 1 NA 1 NA NA 1 — 1- -1 PAGh V-;,d CONTINUED ON PAGE V-3 Form Approved EPA I.D. NUMBER (eopyfrom Hem 1 ofForm 1) OUTFACE NUMBER OMB No. 2040 0086 CONTINUED FROM PAGE 3 OF FORM 2-C I mt%nnnnn —^--- w Approval expires 831-98 PART C - U you are a primary industry and thks outfall contalms process wastewater, refer to Table 2c 2 in the instructions to determine which of the GC1MS iracgoas you must test for. Mark "X" in column 2 a for all such GCWS fractions that apply to your Industry and for ALL toxic metals, cyanides, and total phenols. if you are not required to mark column 2a (secondary industries, nonprocess wastewater outfails, and nonrequired GC/MS fractions), mark "X" in column 2-b for each pollutant you know or havo reason to believe is present Mark "X" in column 2-c for each pollutant believe is absent If you you mark column 2a for any pollutant, you must provide the results of at least one analysis for that pollutant If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant N you know or have reason to believe it wm be discharged in concentrations of 10 ppb or greater. dyou mark column 2b for aerctsK acrylonWHe 2A dWtrophenot, or 2-methyl-4,6 dbdtrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason that you discharge In concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant Is expected to be discharged. Note that there are 7 pages to this part, please review each carefully. Complete one table (all 7 pages) for each outrall. See Instructions for additional details and requirements. I. POLLUTANT AND CASE NO 7- MARK "X" 3. EFFLUENT 4. UNITS S. INTAKE (opttona l a MAXIMUM DAILY VALUE b. MAXIMUM 3e DAY eva➢eble) VALUE fir a LONG TERM AVRQ. VALUE (if avaDable) a LONG TERM AVERAGE VALUE TESTING (lfevaAehle) tl. NO, OF a b. BELIEVED aBEL�VED REQUIRED (1) '"' PRESENT ABSENT 1)CONCENIRATX) (2)MASS CONCENTRATION (2I MASS (1) CQNCENTRATI (2) MASS ANALYSES CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS b NO. OF ANALYSES _ _ ,� n..r'"'AJ.i.i ��_-•.,M e �?';' .+`,� � 5, . 1 1 M. Antimony S.,I' j4J.' '},. l X * * NA NA �C}� �.1..�,., Total (7440-36-0) NA NA 2M. Arsenic, Total NA NA NA (7440-38-2) X * * NA NA NA NA * NA NA NA 3M. Beryllium, Total (7440-41-7) X * NA NA NA NA * W. mium, NA NA NA Total (7440-43-9) X " NA NA NA NA " SM romium, otal NA NA NA (7440-47-3) X * NA NA NA NA NA NA NA 6M. Copper, Total NA (7440-50-8) X * * NA NA NA NA NA NA 7M. Lead, Total (7439-92-1) X * * NA NA NA NA * NA NA NA 8M. Mercury, Total (7439-97-6) X * * NA NA NA NA * NA NA NA 9M. Nickel, Total (7440-02-0) X * NA NA NA NA * * NA NA NA 10M. Selenium, Total (7782.49-2) X * NA NA NA NA * * NA NA NA 11 M. Silver Total (7440-22-4) X * * NA NA NA NA * * NA NA NA 12M. Thallium Total (7440-28-0) X * NA NA r NA NA * * * NA NA NA 13M. Zinc, Total (7440-66-6) X * * NA NA NA NA * * NA NA NA 14M. Cyanide, Total (57-12-5) X * NA NA NA NA * NA NA NA 15M. Phenols Total X * NA NA NA NA * * NA NA NA ,1 4 .. N� .. '::91; i �.., L .. . ^.,.?: r ✓-': Y $ a. --.i k v., ','t rY,.. fp',i� c4 �l.R� 4 ,'.� G { .2:5� f, k DCr i 2,3,7,8-Tetrachloridibenzo-P Dioxin (1764-01-6) X NA NA NA NA 11=13A 9:—'2A4n_9r- room rr%aac vv CONTINUED ON PAGE V-4 ITEM V-B CONTINUED FROM PREVIOUS PAn;: 1. POLLUTANT AND CASE NO (IfeYB/lebfe) 1V.Acrolein"` (107-02-8) 2V. Acrylonitrile (107-13-1) 3V. Benzene (71-43-2) W. Bis (Chloromethyl) a. TESTING REQUI2ED 11 X X X Z MARK "X" b BELIEVED PRESENT 3. EFFLUENT a MAXIMUM DAILY VALUE cBELIEVED (1) ABSENT CONCENTRATION 4. UNITS 5. INTAKE (OpdonBq b. MAXIMUM 30 DAY eveAebfe) (1) (2) MASS CONCENTRATION VALUE (B (2) MASS NA NA NA a LONG TERM AVRG. evs4ebte) (1) CONCENTRATION NA NA NA VALUE (!T rl) �� •. NA NA NA d. NO. OF ANALYSES NA a LONGTERM AVERAGE VALUE ANALYSES NA (1) CONCENTRATION �',�,til�v� * (2) MASS r CONCENTRATION -,,;"}a�`��F� (2) MASS NA * * * * NA NA NA NA NA NA NA NA NA * NA NA NA NA NA NA NA Ether (542-88-1) 5V. Bromoform ( 75-25-2) 6V. Carbon Tetrachloride X X * * NA NA NA NA NA NA NA NA NA * NA NA NA * * NA NA NA (56-23-5) 7V. Chlorobenzene X * NA NA NA NA NA NA NA NA NA (108-90-7) 8V. Chlorodibromomethane X * NA NA NA NA NA NA * * NA NA NA (124-48-1) 9V. Chloroethane (75-00-3) 10V. 2 Chlorohylvinyl X X * * * * NA NA NA NA NA NA NA NA * * NA NA NA NA NA NA NA Ether (110-75-8) 11V. Chloroform (67-66-3) 12V. Dichlorobromomethane X X * * * NA NA NA NA NA NA NA NA NA NA * * * NA NA * NA NA NA (75-27-4) 13V. Dichlorodifluoromethane X * * NA NA NA NA NA * NA NA NA (75-71- 8) 14V.1,1 Dichloroethane X * NA NA NA NA NA * NA NA NA (75-34-3) 15V.1,2 Dichloroethane X * * NA NA NA NA NA NA NA NA (107-06-2) 16V.1,1 Dichloroethylene X * * NA NA NA NA NA * * NA NA NA (75-354) 17V. 1.2 Dichloropropane X * * NA NA NA NA NA * NA NA NA (78-87-5) 18V.1,3 Dichloropropylene X * NA NA NA NA NA NA NA NA (542-75-6) 19V. Ethylbenzene(100-41-4) 20V. Methyl Bromide X X * * * NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (74-83-9) 21V. Methyl Chloride X * NA NA NA NA NA * (74-87-3) EPA Form 3510-2C 9.901 X NA NA NA 'NA NA * NA NA NA ^" CONTINUED ON PAGE V-5 Form Approved EPA LD. NUMBER (copy from mom I Of Form 1) OUTFALL NUMBER OMB No. 2040 0086 CONTINUED FROM PAGE V-4 I 1j[`_Mfl1A74 1. POLLUTANT AND CASE NO (lfava() M) 2 MARK "X' 3 EFFLUENT 4. UNITS Approval expires 831-98 8.(op na) a MAXW= DAILY VALUE b. MA)MWM so DAY aveftb) VALUE (9 a LONG TERM AVRQ. VALUE (8 everabb) d. NO. OF ANALYSES a-':r�a..,��y.'�'� a LONG TERM AVERAGE VALUE b. NO. OF (2) MASS ANALYSES aTESTWG REQU�iEO b. BELIEVED PRESENT - aMELIEVED ABSENT ON (1) CONCEMRATION � ;'� (2) MASS :u.a, et4 (1) CONCENTRATION ,�';,-'ti` 2 MASS '+'"')<� 0) CONCENTRATION �:,, _.�r_: � (2) MASS .F n•��'.^ CONCENTRATION e✓''-, .may (2) MASS +u�i CONCENTRATION ';�YtRs.'� 22V Methylene Chloride NA NA (75-09-2) x 23V.1,1,2,2 Tetrachloro- * * NA NA NA NA NA * NA ethane (79-34-5) x 24V. Tetrachloroethylene * * NA NA NA NA NA * NA NA NA (127-18-4) x 25V. Toluene (108-88-3) x 26V.1,2-TransDichloro- * * * NA NA NA NA NA NA NA NA NA NA * * * NA NA NA NA NA NA NA NA ethylene (156-60-5) x 27V. 1,1,1 Trichloroethane * * NA NA NA NA NA * NA (71-55-6) x 28V. 1,1,2 Trichloroethane * * NA NA NA NA NA * NA NA NA (79-00-5) x 29V. Trichloroethylene * * NA NA NA NA NA * * NA NA NA (79-01-6) x 30V. Trichlorofluoro- * * NA NA NA NA NA * * NA NA NA methane (75-69-4) x 31V. Vinyl Chloride * * NA NA NA NA NA NA NA NA (75-01-4) x .. .,, .. 1A. 2 Chlorophenol _ 7�`Y,%d. N NA NA NA NA N) A NA NA (95-57-8) x 2A 2A Dichlorohenol NA NA NA NA NA * NA NA NA (120-83-2) x 3A. 2,4 Dimethylphenol * * NA NA NA NA NA * NA NA NA (105-67-9) x 4A 4,6 Dinitro-O-Cresol * *I NA NA NA NA NA * * NA NA NA (534-52-1) x * * NA NA NA NA NA * * NA NA NA 5A. 2,4 Dinitrohenol (51-28-5) x * * NA NA NA NA NA * NA NA NA 6A.2-Nitrophenol(88-75-5) x * * NA NA NA NA NA * NA NA NA 7A4-Ni rophenol(100-02-7) 8A. P-Chloro-M-Cresol x * * NA NA NA NA NA * * NA NA NA 59-50-7 9A. Pentachiorop enol x * NA NA NA NA NA * * NA NA NA (87-86-5) 10A. Phenol (108-95-2) x x * * * NA NA NA NA NA NA NA NA NA NA * * NA NA NA NA NA NA 11A. 2,4,6 Tdchloro- phenol (88-06-2) x * NA NA NA NA NA * * NA NA NA CDA C..w.w 4GAn -2n /o nm —• -- • .-•••• .... •.. W-YYr rwuF= V-6 CONTINUED ON PAGE V-6 CONTINUED FROM PAGE V-6 1. POLLUTANT AND CASE NO 2. MARK W 3. EFFLUENT 4. UNITS 5 INTAKE (Opffimq a MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE (A a LONG TERM AVRG. VALUE (B VALUE aVBfl9lN6) ava9aWe) a LONG TERM AVERAGE VALUE b. BELIEVED PRESENT CJHaJEVED ABSENT (1) CONCENTRATION rl) MASS (i)CONCEN71TA710N (2)MASS (1)CONCEN77iAnON (2)MASS (1)CONCENTRA7lOIJ N..'•r (2) MASS a TESTING (lfeYallablB) REQUIRED d NO. Or ANALYSEShALY NO. E ANALYSES _ r •j .,. . ... -_.,_, ftM . L+yJ+2p�i•°FVf'Cb�f,". i��i!'M �N... ..-*Iq�.. ':. c 1B. Acenaphthene i -.. i :Y, , ram.. s S.'k'F W r'd .:. J S..__. •.:v F (83-32-9) X * * NA NA NA NA NA * NA NA NA 2B. Acenaphtylene (208-96-8) X * * NA NA NA NA NA * NA NA NA 3B. Anthracene (120-12-7) X * NA NA NA NA NA * * NA NA 4B. Benxo (92-87-5) X * * NA NA NA NA NA * * NA 5B. Benxo (a (a) NA NA NA NA Anthracene (56-55-3) X * * NA NA NA NA NA * * NA 6B. Benxo (a) NA NA Pyrene (50-32-8) X * NA NA NA NA NA * * NA NA 7B3,4 Benzofluororanthene NA (205-99-2) X * NA NA NA NA NA NA NA 8B. Benzo(ghi)Perylene (191-24-2) X * NA NA NA NA NA NA NA NA 9B. Benxo (k) Fluoranthene (207-08-9) X * * NA NA I NA NA NA * * NA NA NA 10B. Bis(2-Chloroethoxy) Methane (111-91-1) X * * NA NA NA NA NA * * NA NA NA 11 B. Bis(2-Chloroethyl) Ether (111-44-4) X * * NA NA NA NA NA * * NA NA NA 12B Bis(2Chlorolsopropyl) Ether (102-60-1) X * * NA NA NA NA NA * * NA NA NA 13B. Bis(2-Elthylhexyl) Phthalate (117-81-7) X I NA NA I NA NA NA * * NA NA NA 14B.4BromophenylPhenyl Ether (101-55-3) X * * NA NA NA NA NA * * NA NA NA 15B. Butyl Benzyl Phthalate (85-68-7) X * * NA NA NA NA NA * * NA NA NA 16B. 2-Chloronapthalene (91-58-7) X * * NA NA NA NA NA * NA NA NA 17B.2-Chlorophenyl Phenyl Ether (7005-72-3) X * * NA NA NA NA NA * * NA NA NA 18B.Chrysene(218-01-9) X * * NA NA NA NA NA * * NA NA NA 19B. Dibenzo (a,h) Anthracene (53-70-3) X * * NA NA NA NA NA * * NA NA NA 20B. 1,2 Dichlombenzene (95-50-1) X * NA NA NA NA NA * * NA NA NA 21B. 1,3 Dichiorobenzene (541-73-1) PDA Rn.... Y8:4n_9n )n_nn% X * * NA NA NA NA NA NA NA NA -- - -- �- --i rnaoc v-o CONTINUED. ON PAGE V-7 CONTINUED FROM PAGE V-6 EPA ID. NUMBER (Copy /Iom Hem NCO003673 i' OPForm 1) OUTFALL NUMBER 001 w„ ^rl wrw OMB Na 2040 0086 Approval expires 8.31-98 I. POLLUTANT AND CASE NO (8 avatlabl@ .jm:i �-.. .. �`^(2) a TESTING 2. MARK "X" b, 3. EFFLUENT a MAXULUM pPJLY VALUE 4. UNITS S. INTAKE (optbnaq b. MA7®1UM SO DAY evadabfe) VALUE (9 a LONG TERM AVRQ atellabfe) VALUE (B tl. NO. OF ANALYSES a LONG TERM AVERAGE VALUE b. NO. OF ANALYSES REQUIRED BELIEVED PRESENT aBF1JEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCEMRATION MASS �V (1) CONCEMR4TION .ramr,,�,. (2) MASS it) CONCENTRATION ,r (2)MASS ' �W � (1) CONCENTRATION (2) MASS 22B.1,4 Dichlorobenzene NA * NA (106-46-7) 23B.3,3' Dichlorobenzidine X * * NA NA NA NA NA NA (91-94-1) 24B. Diethyl Phthalate X * NA NA NA NA NA * * NA NA NA * NA NA NA (84-66-2) 25B. Dimethyl Phthalate X * * NA NA I NA NA NA * * NA NA NA (131-11-3) 26B. Di-N-Butyl- X * * NA NA NA NA NA NA Phthalate (84-74-2) 27B. 2,4 Dinitro X * * NA NA NA NA NA * * NA NA toluene (121-14-2) 28B. 2,6 Dinitrotoluene X * * NA NA NA NA NA * * NA NA NA * NA NA NA (606-20-2) 29B. Di-N-Octyl Phthalate X * NA NA NA NA NA * NA NA (117-84-0) 30B.1 2 Diphenylhydrazine X NA NA NA NA NA * * (as Azobenzene) ,(122-66-7) 31 B. Fluoranthene X * * NA NA NA NA NA NA NA NA NA (206-44-0) 32B. Fluorene (86-73-7) 33B. Hexachlorobenzene X X * * * * NA NA NA NA NA NA NA NA NA NA * * NA NA NA NA NA NA NA NA (118-74-1) 34B. Hexachlombutadiene X * * NA NA NA NA NA * * NA NA NA (87-68-3) 35B. Hexachlorocyclo- X * * NA NA NA NA NA pentadiene (77-47-4) 36B. Hexachloroethane X NA NA NA NA NA * * NA NA NA NA NA (67-72-1) 37B.ind no1,2,3 cdPyrene X NA NA NA NA NA * * NA (193-39-5) 38B. Isophorone X * NA NA NA NA NA * * NA NA NA (78-59-1) 39B. Naphthalene (91-20-3) 40B.Nitrobenzene (98-95-3) 41 B. N-Nitrosodime- X X X * * NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA * * * * * NA NA NA NA NA NA NA NA NA thylamine (62-75-9) 42B. N-Nitrosodi-N- X * * NA NA NA NA NA NA NA NA Propylamine (621-64-7) EPA Fnrm AM n.9r !R-onl X * NA NA NA NA NA * * NA NA NA ^"- " CONTINUED ON PAGE V-8 CONTINUED FROM PAGE V-7 - I. POLLUTANT AND CASE NO a TESTING Qravaildbl8) REQUIRED 43BN-Nitrosodiphenylamine Z MARK 9(- IEFFLUENT MAXIMUM 4. UNITS & INTAKE (opff=4 a. DAILY VALUE 6. MAXIMUM 30DAY avOoble) VALUE (If r- LONGTERM AVRG. VALUE (Hevalab/e) d. NO. ANA.�L°YSES a. LONG TERM AVERAGE VALUE 0. N0. OF ANALYSES ,7. 0. BELIEVED PRESENT .' aBI1JEVED ABSENT _. (1) CONCENTRATION (2)MASS (1) CONCENTRATION s (2)MASS (1) CONCENTRATION (2)MA.SS (1) CONCENTRATION " (1) coNI noN (z) MASS NA NA NA (86-30-6) X 44B. Phenanthrene * * NA NA NA NA NA * " (85-01-8) X 45B. Pyrene (129-00-0) x 46B.1,2,4Trihiorobenzene * * * NA NA NA NA NA NA NA NA NA NA * * NA NA NA NA NA NA NA NA r � NA ~ NA ✓~ NA NA (120-82-1) x 1 P. Aiddn (3094)0-2) X 2P. a-BHC (319-84-6) X 3P. 13-BHC (319-85-7) X 4P. y-BHC (5&89-9) X 5P. &-BHC (319-86-8) X 6P. Chlordane (57-74-9) X 7P. 4,4' DDT (50-29-3) x 8P. 4.4' DDE (72-55-9) X 9P. 4,4 DDD (72-54-8) X 1OP. Diedrin (60-57-1) x 11 P. a-Endosulfan * * * * * * * * * * * " * * * * NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NAy NA NA NA NA NA NA NA NA NA NA* NA NA NA NA NA NA NA NA NA NA " * * " * * * * * * * * * NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (115-29-7) X 12P. f�-Endosulfan * NA NA NA NA NA * NA (115-29-7) X 13P. Endosulfan Sulfate * * NA NA NA NA NA NA NA NA NA NA (1031-07-8) x 14P. Endrin (72-20-8) X 15P. Endrin Aldehyde * * * NA NA NA NA NA NA NA NA NA NA * * NA NA NA NA (7421-93-4) x 16P. Heptachlor NA NA NA NA NA * * NA NA NA (76-44-8) x * * NA NA NA NA NA * * NA NA NA FPA Fnr lqG4n-1jrr, rsLnm rruc V-a CONTINUED ON PAGE V-9 EPA I.D. NUMBER (copy from hem 1 oPForm 1) OUTFACE NUMBER Form Approved CONTINUED FROM PAGE V-8 I Nr_nnnasma OMB No. 2040 0086 I WWI Approval expires 8-31-98 1. POLLUTANT AND CASE NO 2. MARK W a MAXIMUM DAILY VALUE 3. EFFLUENT 4. UNITS 5. INTAKE (optional) b. MAXIMUM 30 DAY VALUE (H - wabla) a LONG TERM AVRG. VALUE (ff -uftla) a LONG TERM AVERAGE VALUE (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (IPevallable) a TESTING b. BELIEVED ¢BELIEVED REQUIRED PRESENT ABSENT (1) CONCENTRATION (2) MASS 17P. Heptachlor d. NO. OF ANALYSES b. NO. OF ANALYSES NA Epoxide (1024-57-3) X 18P. PCB-1242 NA NA NA NA * NA NA NA NA NA (53469-21-9) X 19P. PCB-1254 NA NA NA NA * (11097-69-1) X * * 20P. PCB-1221 NA NA NA NA * NA NA NA NA NA NA (11104-28-2) X * 21 P. PCB-1232 NA NA NA NA * * NA NA NA (1114-16-5) X * 22P. PCB-1248 NA NA NA NA * NA NA NA (12672-29-6) X 23P. PCB-1260 NA NA NA NA * * NA NA (11096-82-5) X * 24P. PCB-1016 NA NA NA NA * * NA NA NA (12674-11-2) X * 25P.Toxaphene NA NA NA NA * * NA (8001-35-2) X * * NA NA NA NA NA NA NA EPA Form 351n-2C fR.am * ri1VG V-D PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or allE.P. A. I.D. Number (copy from Item 1 of Forth 1)NC0003573 of this Information on separate sheets (use the same format) Instead of compieft these pages. SEE INSTRUCTIONS Forth Approved OMB No. 2040 0086 Approval expires 8-31-08 V. INTAKE &EFFLUENT CHARACTERISTICS Continued from a e 3 of Form 2 C ( page ) otrrFALLPART A No. -You mustprovide e resu is at east one ana „-'' _ry,. ys s or every po utant n s e. Complete ete one toe r each o See In cUons or a ona etas s 002 2. EFFLUENT 1. POLLUTANT AND CAS 3. UNITS 4. INTAKE (option I NO a MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (If amflable) b. LONG TERM AVRG. VALUE (B'avatfable) d. NO. OF (Specify8blank) a. LONG TERM AVERAGE VALUE CONCENTRATION �) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION �) MASS a CONCENTRATION b. MASS (1) (2) NWSS (Ilavallebl� ANALYSES ANALYSES a. Biochemical coNCENTRAnoN Oxygen Demand 212.0 9775.7 106.00 4887.90 26.50 1222.00 5 MG/L PPD NA (BOD) NA NA b. Chemical NA Oxygen Demand 102.0 11291.9 102.0 11291.9 57.8 4853.2 4 MG/L PPD NA (COD) NA c. Total Organic * Carbon (TOC) * NA NA NA NA * MG/L PPD d. Total Suspended k NA NA NA Solids (TSS) NA NA NA NA MG/L PPD NA NA NA e. Ammonia (as N) * NA NA NA NA MG/L PPD NA f. Flow value NA NA value value 18.60 16.3 value 10.6 396 MGD NA NA g. Temperature value value (winter) 22.0 16 7 value 14.9 128 a value C NA NA h. Temperature value value value (summer) 39.0 32.2 25.8 146 eC value NA NA Minimum Maximum Minimum Maximum3�� , i. pH 6.2 8.6 NA NA s,, 274 PART B -Mark "X" In column 2a for each pollutant you know or have reason to believe is preseaL Mark "X" in column 2b for each pollutant you believe to be absent If you mark column 2a for any pollutant which Is limited either directly, or Indirectly but expressly, In an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide quantttatNe data or an explanation of their presence In your discharge. Complete one table for each outfall. See the Instructions for additional details and requirements. I MARK'W 3. EFFLUENT 4. UNITS !i. INTAKE (optionaq a raawmum DAILY VALUE b. b. MAXIMUM 3o DAY VALUE (Havalable) r- LONGTERM AVRG. VALUE (if available) b. NO. OF LONG TERM AVERAGE VALUE ANALYSES 1. POLLUTANT & CAS NO. D. NO. OF of available) a SWEVED b. BR IEVEO (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES (1) (2) MASS (2) MASS PRESENT ABSENT CONCENTRATION CONCENMTION a. Bromide (24959-67-9) X NA NA NA NA Chlorine NA NA NAb. Total Residual X * * � � � � * y c. Color X NA NA NA NA * NA NA NA NA NA NA d. Fecal Coliforrn X . NA NA NA NA NA NA NA e. Fluoride (16984-48-8) X * * NA NA NA NA Nitrate— NA � NAf. Nitrfte (as N) X Np, NA NA NA CPA C--'7R4A_9' 10 en% NA NA NA ITEM V-B CONTINUED FROM PREVIOUS PAGE 1. POLLUTANT AND CASE NO 2 MARK "X" 3. EFFLUENT 4. UNITS S. INTAKE (opBonffi) a MA%RMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (3 alwable) a LONG TERM AVRG. VALUE (P avauawe) a LONG TERM AVERAGE VALUE BELIEVED (/f 8Y81(eble) d. NO. a bAELIEVED PRESENT ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS b. NO.OF ANALYSES g. Nitrogen, NA Total Organic (as N) X * * NA NA NA NA * * NA NA h. Oil and Grease X * *' NA NA NA NA * * I. Phosphorus NA NA NA NA NA NA NA NA (as P) , Total X 1.3 152.3 1.3 152.3 0.35 36.1 12 MG/L PPD (7723-14-0) NA t w y fi , r s � t,. „��.'.7an��.9v:�..r ..r�", a NA NA NA ' NA (1) Alpha, Total X * * NA NA NA * * * * * NA NA NA (2) Beta, Total X * * NA NA (3) Radium, total X * NA NA NA NA NA * * * NA NA NA (4) Radium 226 Total X * NA NA NA NA * * NA NA NA NA NA k. Sulfate (as SO4) NA NA NA (14808-79-8) X ' * NA NA NA NA * * * NA I. Sulfide (as S) X NA NA NA NA * NA m. Sulfite (as S03) NA NA (14265-45-3 X * * NA NA NA NA * * * NA NA NA n. Surfactants X * * NA NA NA NA NA NA NA o. Aluminum, Total (7429-90-5) X * * NA NA NA NA * NA NA NA p. Barium, Total 9440-39-3) X * * NA NA NA NA * * * NA NA NA q. Boron, Total (7440-42-8) X * * NA NA NA NA * * * NA NA NA r. Cobalt, Total (7440-48-4) X * * NA NA NA NA * NA NA NA s. Iron, Total (7439-89-6) X * * NA NA NA NA * * NA NA NA t. Magnesium (7439-95-4) X * *NA NA NA NA * * NA NA NA u. Molybdenum, Total (7439-98-7) X * * NA NA NA NA * * NA NA NA v. Manganese, (7439-96-5) X * * NA NA NA NA * * NA NA NA w. Tin Total (7440-31-5) X * * NA NA NA NA * * NA NA NA x. Tdanium,Total (7440-32-6) X * * NA NA NA NA * * NA NA NA CAA C...... 4Cdn -2^ /o nm • -- •- ��-��� PAvt V z CONTINUED ON PAGE V-3 EPA J.D. NUMBER (copy from Here 1 orForm 1) OUTFALL NUMBER CONTINUED FROM PAGE 3 OF FORM 2-C I Nt_r1nr1ZG71% I nn� Forth Approved OMB No. 2040 0086 Approval expves 631-98 PART C - It you are a primary industry and this outiall contains process wastewater, refer to Table 2c 2 in the coons to determine which of the GClMS fractions you must testfor. Mark "X' in column 2 a for all such GCIMS fractions that apply to your Industry and for ALL twdc metals, cyanides, and total phenols. If you are not required to mark column 2a (secondary industries, mmProcass wastewater COWS, and nonrequired GCIMS fractions), mark "X' in column 2-b for each pollutant you know or have reason to believe Is present. Mark W in column 2a for each pollutant you believe Is absent. If you mark column 28 for any pollutant, you must provide the results of at least one analysis for that pollutant. Hyou mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant If you know or have reason to believe it will be discharged in concentrations of 10 ppb or greater. if you mark column 2b for acrolein, acrylonitrile 2,4 dinitrophanol, or 2-methyl-4,6 dlnitrophenol, you must provide the results of at least one analysis for each of these pollutants which you know or have reason that you discharge in concantratiwns of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part, please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for additional detaRs ami requirements. I. POLLUTANT AND CASE NO 2. MARK')" 3. EFFLUENT 4. UNITS h. MAXIMUM 30 DAY VALUE (it e. LONG TERM AVRG. VALUE (if S. INTAKE (optionaq a MAXIMUM DALL.Y VALUE avalable) eva/We) a. LONG TERM AVERAGE VALUE (IfarW(able) (1) tL NO. OFREQUIRED (1) (�) CONCENTRATION (2) MASS CONCENTRATION (2) MASS (1) CONCENTRATION(2) MASS ANALYSES CONCFs1TRATION (2) MASS B NO. OF ANALYSES a.TESTING b. BELIEVED CAELMVED PRESENT ASSENT (q) CONCENTRATION (2) MASS [t .f Antimony * Total (7440-36-0) X NA NA NA NA * * NA NA NA 2M. Arsenic, Total (7440-38-2) X * NA NA NA NA * * NA NA NA 3M. Beryllium, Total (7440-41-7) X NA NA NA NA * * * NA NA NA a mium, Total (7440-43-9) X * * NA NA NA NA * * NA NA NA SIT"Crifornium, I otal (7440-47-3) X * NA NA NA NA NA NA NA 6M. Copper, Total (7440-60-8) X NA NA NA NA * * * NA NA NA 7M. Lead, Total (7439-92-1) X * NA NA NA NA * * NA NA NA 8M. Mercury, Total (7439-97-6) X * * NA NA NA NA * * * NA NA NA 9M. Nickel, Total (7440-02-0) X * * NA NA NA NA * * * NA NA NA 10M. Selenium, Total (7782-49-2) X * * NA NA NA NA * * * NA NA NA 11 M. Silver Total (7440-22-4) X * * NA NA NA NA * NA NA NA 12M. Thallium Total (7440-28-0) X * * NA NA I NA NA * * NA NA I NA 13M. Zinc, Total (7440-66-6) X * * NA NA NA NA * * * NA NA NA 14M. Cyanide, Total (57-12-5) X * * NA NA NA NA * * * NA NA NA 15M. Phenols, Total X * * NA NA NA NA NA NA NA WIG r'.y,�� u� :. .. % '✓Xd �Ls �,'�y{t�",w+', C 1 ytJ �{� k.u.._$. ?�c�:..J.Y'x G,...,.l.y� L1 .fd� "Z •" 4.i.. 1� a't: i4:? .r..2� 'i... 2,3,7,8-Tetrachloridibenzo-P Dioxin (1764-01-6) X NA NA NA NA a.r� rvuu .aa 1v Lv to -au) VAUM V-3 CONTINUED ON PAGE V-4 ITEM We CONTINUED FROM PREVIOUS PAGE I. POLLUTANT AND CASE NO (Ifeva118b1e) a. TESTING REQUIRED - ... v �:.... n 1V. Acrolein 2 MARK'X' b. BELIEVED PRESENT -.. 3. EFFLUENT a. MAXIMUM DAILY VALUE C.BELE_VED (1) ABSENT CONCENTRATION (2) MASS 4. UNITS tl. NO. OF ANALYSES (1) CONCENTRATION S. INTAKE (OptlOnal) b. MAXMM 30DAY avaws) (1) CONCENTRATION VALUE (Y (2) MASS c LONG TERM AVRM avesaW (1) CONCENTRATION VALUE (6 (2) MASS a. LONG TERM AVERAGE VALUE b. NO. OF s S (2) MASS (1) CON (2)MASS (2) NA NA NA NA NA NA * * * * NA NA NA NA NA NA NA NA NA (107-02-8) X 2V. Acrylonitrile (107-13-1) X 3V. Benzene (71-43-2) X W. Bis (Chloromethyl) * * * NA NA NA NA NA NA NA NA NA Ether (542-88-1) X 5V. Bromoform ( 75-25-2) X 6V. Carbon Tetrachloride * * * NA NA NA NA NA NA NA NA NA NA * NA NA NA NA NA NA (56-23-5) X 7V. Chlorobenzene NA NA NA NA NA * NA NA NA (108-90-7) X 8V. Chlorodibromomethane * * NA NA NA NA NA * NA NA NA NA NA NA NA NA NA (124-48-1) X 9V. Chloroethane (75-00-3) X 1 OV. 2 Chlorohylvinyl * NA NA NA NA NA NA NA NA NA NA * * * NA NA Ether (110-75-8) X 11 V. Chloroform (67-66-3) X 12V. Dichlorobromomethane * NA NA NA NA NA NA NA NA NA NA * NA NA NA NA NA NA (75.27-4) X 13V. Dichlorodifluoromethane * * NA NA NA NA NA NA NA NA (75-71- 8) X 14V.1,1 Dichloroethane NA NA NA NA NA * NA (75'34-3) X 15V. 1,2 Dichloroethane * * NA NA NA NA NA * * NA NA NA (107-06-2) X 16V.1,1 Dichloroethylene * NA NA NA NA NA I NA NA NA (75-354) - X 17V.1,2 Dichloropropane * * NA NA NA NA NA NA NA NA (78-87-5) X 18V. 1,3 Dichloropropylene NA NA NA NA NA * NA NA NA (542-75-6) X 19V. Ethylbenzene(100-41-4) X 20V. Methyl Bromide * * NA NA NA NA NA NA NA NA NA NA * * * NA NA NA NA NA NA (74-83-9) X 21 V. Methyl Chloride J-X * * NA NA NA NA NA NA NA NA (74-87-3) * * NA NA NA I NA NA * * NA NA NA FPA A_om -- " -- - -"' rK%xc V•4 CONTINUED ON PAGE V-5 CONTINUED FROM PAGE v� I. POLLUTANT3. AND CASE NO (if—gable)aTESTWG EPA I.D. NUMBER 2. MARK "X" (copy from /t al 1 of Form 1) NC0003573 EFFLUENT . — ""11— OUTFALLNUMBER OW No. 2040 002 Approval exp(res 0086 8-31-98 a MAXIMUM DALLY VALUE b. MAXMUM 30 DAY VALUE (ff eva9able) a LONG TERMAVRG. VALUE (f aoaileMe) 4. UNITS 5. INTAKE (OpUonai a LONG TERM AVERAGE VALUE (1) TX) MASS CONCENTRA (2) b. NO. OF ANALYSES REQUIRED .,, b. BELIEVED 66E1lEVED PRESENT ABSENT .. (1) CONCENTRATION (2) MASS � CONCENTRATION (2) MASS i (� C.ONCENTRA �O �� w2 d NO. OF ANALYSES C CON ENTRA (2)MASS }J 22V Methylene Chloride NA NA NA NA ~' NA (75-09-2) 23V.1,1,2,2Tetrachlom- X * * NA NA NA NA NA NA NA ethane (79-34-5) 24V. Tetrachloroethylene X * NA NA NA NA ' * NA NA NA NA (127-18-4) 25V. Toluene (108-88-3) 26V. 1,2-TransDichioro- X X * * * * NA NA NA NA NA NA NA NA NA NA* NA NA NA * NA NA NA ethylene (156-60-5) 27V. 1,1,1 Trichloroethane X * * NA NA NA NA * ' NA NA NA (71-55-6) 28V. 1,1,2 Trichloroethane X ' NA NA NA NA NA * ' NA NA NA (79-00-5) 29V. Tdchioroethylene X * ' NA NA NA NA NA -6) 30V. 30V. Trichlorofluoro- X * ' NA NA NA NA NA * * NA NA NA methane (75-69-4) 31V. Vinyl ChlorideNA X I NA NA NA NA NA * * NA �, i — NA NA NA (75-01-4) _ .. 1A. 2 Chlorophenol X L* q uy r. NA NA NA NA NA (95-57-8) 2A 2,4 Dichlorohenol X ' NA NA NA NA NA * * NA NA NA NA NA NA (120-83-2) 3A. 2,4 Dimethylphenol X ' NA NA NA NA NA ' * NA NA NA (105-67-9) 4A 4,6 Dinitro-O-Cresol X NA NA NA NA NA * NA NA (534-52-1) 5A. 2,4 Dinitrohenol X * * NA NA NA NA NA * ' NA (51-28-5) X ' NA NA NA NA NA * NA NA NA 6A.2-Nitrophenol(88-75-5) 7A4-Nhrophenol(100-02-7) 8A. P-Chloro-M-Cresol X X ` * NA NA NA NA NA NA NA NA NA NA * NA NA NA NA NA NA NA NA 59-50-7 9A. Pentachlomphenol X * NA NA NA NA NA ' * NA (87-86-5) 10A. Phenol (108-95-2) 11A. 2,4,6 Trichloro- X X * * * NA NA NA NA NA NA NA NA NA NA * * NA NA NA NA NA . NA phenol (88-06-2) EPA Form simm, mam X ' * NA I NA NA NA NA * * NA NA NA r11KW= v-a CONTINUED ON PAGE V-6 CONTINUED FROM PAGE V-6 1. POLLUTANT AND CASE NO (ff aVaU3b1@) y - - — { 1 B. Acenaphthene 2 MARK gC" 4. UNITS d NO. OF ANALYSES (1) CONCENTRATION i1- :ems' ',1�' /. '�£� S'7� iL Us' -'Rs. � & INTAKE (optlonao a MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY eve9ab7e) VALUE (u a LONG TERM AVRG. VALUE(® eve able) a LONG TERM AVERAGE VALUE b. N0. OF ANALYSES a TESTING REQUIRED _ b. BELIEVED PRESENT e.BEL1EVED ABSENT ���, (1) CONCENTRATION ✓;' v1 :�1 �. (2) MASS .t. _ r (1) CONCENTRATION ,.. %:;:. �. (2) MASS .Sat. (1) CONCENTRATION ^ �. RnSr.. �i r� 3 :i2 Cl) MASS .}�.'J IT-- •Y. (2) MASS (1) CONCENTRATION h� JYt.f� a'':A�fr �f^.� (2) MASS Y�Gi NA NA (83-32-9) 2B. Acenaphtylene X * * NA NA NA NA NA NA * * NA NA NA NA NA NA NA NA NA (208-96-8) 3B. Anthracene (120-12-7) 4B. Benadine (92-87-5) 5B. Benzo (a) X X X * * * * * NA NA NA NA NA NA NA NA NA NA NA NA NA NA * NA * * NA NA NA Anthracene (56-55-3) 6B. Benzo (a) X * NA NA NA NA NA * * NA NA NA Pyrene (50-32-8) 7B3,4 Benzofluororanthene X. * * NA NA NA NA NA * * NA NA NA (205-99-2) 8B. Benzo(ghi)Perylene X * * NA NA NA NA NA * NA NA NA (191-24-2) 9B. Benxo (k) X NA NA NA NA NA * Fluoranthene (207-08-9) 10B. Bis(2-Chloroethoxy) X * * NA NA NA NA NA * NA NA NA I NA NA NA Methane (111-91-1) 11 B. Bis(2-Chloroethyl) X * * NA NA NA NA NA Ether (111-44-4) 12B Bis{2Chlorolsopropyl) X * * NA NA NA NA NA * * NA Ether (102-60-1) 13B. Bis(2-Elthylhexyl) X * * NA NA NA NA NA * * NA NA NA NA NA NA Phthalate (117-81-7) 14B.4BromophenylPhenyl X * NA I NA NA NA NA * * NA NA Ether (101-55-3) 15B. Butyl Benzyt X * * NA NA NA NA NA * NA Phthalate (85-68-7) 16B. 2-Chloronapthalene X * NA NA NA NA NA * NA NA NA (91-58-7) 17B.2-Chlorophenyl Phenyl X * NA NA NA NA NA * * NA NA NA Ether (7005-72-3) 18B.Chrysene(218-01-9) 19B. Dibenzo (a,h) X X * * * NA NA NA NA NA NA NA NA NA NA * NA NA NA NA NA NA Anthracene (53-70-3) 20B. 1,2 Dichlorobenzene X * NA NA NA NA NA * NA NA NA (95-50-1) 21B. 1,3 Dichlorobenzene X * NA NA NA NA NA * * NA NA NA (541-73-1) EPA Farm 351 a_2c IR.Qm X * *I NA ......- ., „ NA NA NA NA * * NA NA NA CONTINUED ON PAGE V-7 EPA I.D. NUMBER (copy from Item 9 of Form v OUTFACE NUMBER CONTINUED FROM PACE V.s Form Approved OMB Nn 2ndD MAR Approval expires 831-98 3. EFFLUENT I. POLLUTANT AND CASE NO 2 MARK ")r 4. UNITS 5.1N7AKE (optlonaQ a MAXIMUM DAILY b. MAXIMUM 30 DAY VALUE Qr m LONG TERM AVRG. VALUE (fP a LONG TERM AVERAGE VALUE (If dVJ/leble) a TESTING VALUE evaeu.) eveltable) Q NO OF b. BELIEVED c.BEIJEVm • ... ,.., REQUIRED PRESENT ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES ANAL CENTRA (1)0ON TION (2)MASS ( 1) CONCENTRATION �) MASS ANALYSES 22B.1,4 ,. � ( . k >¢ A'i :. `� "zw.; �'"4�.y d �.i,"..+� . ., M17 � �e ✓'d � � _ Dichlorobenzene 6-7) X * 3BA 2 3B.3,3' Dichlorobenzidine NA NA NA NA NA * * NA NA NA (91-94-1) 24B. Diethyl Phthalate X * * NA NA NA NA NA NA NA NA NA NA NA (84-66-2) 25B. Dimethyl Phthalate X * NA NA NA NA NA * * (131-11-3) X * * 26B. Di-N-Butyl- NA NA NA NA NA * NA NA NA Phthalate (84-74-2) X * * NA NA NA I NA NA * * 27B. 2,4 Dinitro NA NA NA toluene (121-14-2) X * * NA NA NA NA NA * 28B, 2,6 Dinitrotoluene NA NA NA (606-20-2) X * NA NA NA NA NA * NA NA NA 29B. Di-N-Octyl Phthalate * NA NA NA (117-84-0) X * NA NA NA NA NA * 30B.1 2 Diphenylhydrazine (as Azobenzene) (122-66-7) X * * NA NA NA NA NA * 31 B. Fluoranthene NA NA NA (206-44-0) X * * NA NA NA NA NA * NA NA NA 326. Fluorene (86-73-7) X * * NA NA NA NA NA * 33B. Hexachicrobenzene NA NA NA (118-74-1) X * NA NA NA NA NA * NA NA NA 34B. Hexachlorobutadiene (87-68-3) X * * NA NA NA NA NA NA NA NA 35B. Hexachlomeycio- pentadlene (77-47-4) X * * NA NA NA NA NA * NA NA NA 36B. Hexachloroethane (67-72-1) X * NA NA NA NA NA * * NA NA NA 37B.Indeno1,2,3 cdPyrene (193-39-5) X * NA NA NA NA NA * * NA NA NA 38B. Isophorone (78-59-1) X * * NA NA NA NA NA NA NA NA 39B. Naphthalene (91-20-3) X * * NA NA NA NA NA NA 40B.Nitrobenzene (98-95-3) X * * NA NA NA NA NA * * NA NA 41 B. N-Nitrosodime- NA NA NA thylamine (62-75-9) X * * NA I NA I NA I NA NA * NA NA NA 42B. N-Nitrosodi-N- Propylamine (621-64-7) X * * NA NA NA NA NA * * NA NA NA EPA Fnrm AM n-9r mckni r'l. = v-r CONTINUED ON PAGE V-8 CONTINUED FROM PAGE V-7 1. POLLUTANT AND CASE NO (Nava1(ab1B) Z MARK W 3. EFFLUENT 4. UNITS S. INTAKE (optfonao a MAXNUM DAILY VALUE b. MAMUM 30 DAY evabwe) VALUE (Q c LONG TERM AVRM VALUE (9aveAeble) E. NO. OF ANALYSES a LONG TERM AVERAGE VALUE (2) MASS b. NO. OF ANALYSES a TESTING REQUIRED b. BELIEVED PRESENT N eBEL1EVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION ItrOSOdih p enylamine * NA NA NA (86-30-6) 44B. Phenanthrene X * NA NA NA NA NA * NA NA NA (85-01-8) 45B. Pyrene (1294)0-0) 46B.1,2,4Trihlorobenzene X X * * NA NA NA NA NA NA NA NA NA NA * * NA NA NA * * * * * * * NA NA (120-82-1) f w� ' �'`'NA 1 P. Aldrin (309-00-2) 2P. a-BHC (319-84-6) 3P. P-BHC (319485-7) 4P. y--BHC (58-89-9) 5P. S BHC (319-86-8) 6P. Chlordane (57-74-9) 7P. 4,4' DDT (50-29-3) SP. 4.4' DDE (72-55-9) 9P. 4,4' DDD (72-54-8) 1OP. Diedrin (60-57-1) 11 P. a-Endosulfan X X X X X X X X X X X * * * * * * * * * NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA * * * * * * * * * * * * * * * NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (115-29-7) 12P. S-Endosulfan X * * NA NA NA NA NA NA NA NA (115-29-7) 13P. Endosulfan Sulfate X * NA NA NA NA NA * * NA NA NA (1031-07-8) 14P. Endrin (72-20-8) 15P. Endrin Aldehyde X X * * * * NA NA NA NA NA NA NA NA NA NA * * * * NA NA NA NA NA NA (7421-93-4) 16P. Heptachlor X * NA NA NA NA NA * NA NA NA (76-44-8) X * * NA NA NA NA NA * NA NA NA FPA Fnr '444n-on m-om «%oc rro CONTINUED ON PAGE V-9 Form Approved EPA I.D. NUMBER (copy from Item I OfFoi7n 1) OUTFALL NUMBER OMB No. 2040 0086 CONTINUED FROM PAGE V-8 I me-nnn-=712 I I -------- - I ... I Approval wores 8-31-98 I. POLLUTANT AND CASE NO 2. MARK tW 3. EFFLUENT 4. UNITS 5. INTAKE (optbnal) b. MA)aMUM 30 DAY VALUE (ff C. LONG TERM AVRG. VALUE (ff MAXIMUM DAILY VALUE avaqa*) avaWe) a. LONG TERM AVERAGE VALUE a TESTING b. BELIEVED c.BWEVED d. NO. OF ANALYSES ffavagable) b. NO. OF REQUIRED PRESENT ABSENT (i) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRA71ON (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES 17P. Heptachlor Epoxide (1024-57-3) x NA NA NA NA 18P. PCB-1242 NA NA NA (53469-21-9) x NA NA NA NA NA NA NA 19P. PCB-1254 (11097-69-1) x NA NA NA NA NA NA NA 20P. PCB-1221 (11104-28-2) x NA NA NA NA NA NA NA 21P. PCB-1232 (1114-16-5) x NA NA NA NA NA NA NA 22P. PCB-1248 (12672-29-6) x NA NA NA NA NA NA NA 23P. PCB-1260 (11096-82-5) x NA NA NA NA NA NA NA 24P. PCB-1016 (12674-11-2) x NA NA. NA NA NA NA NA NA 25P. Taxaphene (8001-35-2) x NA NA NA NA NA NA CDA C- 12=11n 100, to nm %- —, rk%%7= V-%P W E.P. A. I.D. Number (copy from item 1 of Form 1) PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report sans or all NC0003573 Form approved of Ids Information on separate sheets (use the same tomcat) Instead of oompleung these pages. OMB No. 2040 0085 SEE INSTRUCTIONS APPMV81 expires 8-31-88 V. INTAKE & EFFLUENT CHARACTERISTICS (Continued from page 3 of Form 2-C) ouTFAu No. -You must provide e resu is o at east one analysis or every pollutant n s e. Complete one table or ea o a . bee instructions or additional eta s. 006 2 EFFLUENT 1. POLLUTANT AND CAS 3. UNITS 4. INTAKE (option)) NO a. MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE (if evallable) b. LONG TERM AVRG. VALUE (Navapa ttb) d NO. OF (SperJfy Hblank) a. LONG TERM AVERAGE VALUE ( CONCENTRATION (2) MASS11) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS a CONCENTRATION b. MASS plavatlable) ANALYSES (ii (2) MASS . CONCENTRATION ANALYSES a. Biochemical Oxygen Demand WA WA NA NA NA NA WA MG/L PPD NA NA NA (BOD) b. Chemical Oxygen Demand WA WA NA NA NA NA WA MG/L PPD NA NA NA (COD) o Total Organic Carbon (TIC) WA NIA NA NA NA NA NIA MG/L PPD Total Suspended NA NA NA S Solids (fSS) NA NA NA NA WA MG/L PPD NA NA NA e. Ammonia (as N) WA WA NA NA NA NA WA MG/L PPD f. Flow value WA value NA NA value NA WA MGD NA NA value NA g. Temperature (w/nter) value WA value NA NA value Np, WA _ aC NA value NA F. value value value NA NA merature WA NA NA NA NIA a value C(sum NA NA Minimum Maximum Minimum Maximum "` j i:; I. pH WA WA NA NA WA PART B -Mark "X" In column 2a for each pollutant you know or have reason to believe is present Mark "X" In column 2b for each pollutant you believe to be absent If you mark column 2a for any pollutant which Is limited either directly, or indirectly but expressly, In an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant For other pollutants for which you mark column 2a, you must provide quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements. 2. MARK W 3. EFFLUENT 4. UNITS 5. INTAKE (opgonQ a MAxIMuM DAILY VALUE b. MAXIMUM 30 DAY VALUE (favaffewe) c. LONGTERM AVRG. VALUE (IfavaUable) a. LONG TERM AVERAGE VALUE b. NO. OF ANALYSES 1. POLLUTANT &CAS NO. D. NO. Qfava08ble) a BELIEVED b. BELIEVED (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION i2)MAS3 ANALYSES ni CONCENTRATION (2) MASS (i) CONCENTRATION (2) MASS PRESENT ABSENT a. Bromide (24959-67-9) X WA WA NA NA NA NA N/A WA WA NA NA NA b. Chlorine Total Residual X WA WA NA NA NA NA WA WA WA NA NA NA c. Color X WA WA NA NA NA NA WA WA WA NA NA NA d. Fecal Col'tform X WA WA NA NA NA NA WA WA WA NA NA NA e. Fluoride (16984-48-8) X WA WA NA NA NA NA WA WA WA NA NA NAf. Nitrate— Nitrite (as N) X WA WA NA NA NA NA WA WA WA � NA M .. ............. 1-1 1'Al7C V-T ITEM V-B CONTINUED FROM PREVIOUS PAGE I. POLLUTANT AND CASE NO 2 MARK ")r 3. EFFLUENT 1 4. UNITS 6. INTAKE (optional a MAXIMUM DAILY VALUE b. MAXIMUM 30 DAY VALUE ff gygggy/g) a LONG TERM AVRG. VALUE ff ac, ,cvcn g�aMg) a LONGTERM AVERAGE VALUE g, PRESENT bgE�VEp ABSENT (1) CONCEMRATION (2) MASS (!f BVeQa6te) (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1} CONCENTRATION 2 MASS () d NO. OF ANALYSES (1) CONCENiRATIQN (2) MASS b. NO. OFRATI ANALYSES g. Nitrogen, Total Organic (as N) X WA N/A NA NA NA NA WA WA WA NA NA NA h. Oil and Grease X WA WA NA NA NA NA WA N/A WA NA NA NA 1. Phosphorus NA (as P) , Total X WA WA NA NA NA NA WA N/A WA NA NA NA NA (7723-14-0) NA NA NA NA (1) Alpha, Total X N/A WA NA NA „. N/A N/A N/A NA NA NA (2) Beta, Total X N/A N/A NA NA (3) Radium, total X WA WA NA NA NA NA NA WA N/A WA NA NA NA (4) Radium 226 Total X N/A NIA NA NA NA NA WA N/A WA NA NA NA NA k. Sulfate (as SO4) NA NA NA WA N/A WA NA NA (14808-79-8) X WA N/A NA NA NA NA WA N/A WA NA NA NA 1. Sulfide (as S) X N/A WA NA NA NA NA WA N/A N/A NA NA NA m. Sulfite (as S03) (14265-45-3 X WA WA NA NA NA NA WA N/A WA NA NA NA n. Surfactants X WA WA NA NA NA NA WA WA WA NA NA NA o. Aluminum, Total (7429-90-5) x WA WA NA NA NA NA WA N/A WA NA NA NA p. Barium, Total (7440-39-3) X WA WA NA NA NA NA WA WA WA NA NA NA q. Boron, Total (7440-42-8) X WA WA NA NA NA NA WA NA NA NA r. Cobalt, Total N/A WA (7440-48-4) x N/A WA NA NA NA NA WA WA WA NA NA NA s. Iron, Total (7439-89-6) X WA WA NA NA NA NA WA N/A WA NA NA NA t Magnesium (7439-95-4) X WA N/A NA NA NA WA NA NA NA NA N/A WA u. Molybdenum, Total (7439-98-7) X WA WA NA NA NA NA N/A N/A WA NA NA NA v. Manganese, (7439-96-5) X WA WA NA NA NA NA WA WA WA NA NA NA w. Tin Total (7440-31-5) X WA N/A NA NA NA NA WA NA NA NA N/A N/A x. TitaniurnJotal (7440-32-6) X WA N/A NA NA NA NA WA NIA WA NA NA NA �.....,.. —.— to -awl PAGE V-Z CONTINUED ON PAGE V„3 Form Approved EPA I.D. NUMBER (copy from @enr 1 of Form 1) OUTFALL NUMBER OMB No. 2040 0086 CONTINUED FROM PAGE 3 OF FORM 2.0 1 ►rnn PART C - If you YUtl are a primary Industry and this outrafl cm— reins process wastewater, refer to Table 2" in the instrucuons to determine which of the Gr4MS irectihms Approval expires 8-31-96 you must test for. Mark "x' In column 2 a for a0 such GCNMS fractions that apply to your Industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2a (secondary industries, nonprocess wastewater outfallS, and nonrequired GCNMS fractions), mark "r in column 2-b for each pollutant you know or have reason to believe Is present Mark W in column 2c for each pollutant you believe is absent. If you mark colunm 2a for any pollutant, you must provide the results of at least one analysis for that If pollutant you mark column 2b for any pollutant, You must provide the results of at least one analysis for that pollutant If you know or have reason to believe it will be discharged In concentrations of 10 ppb or greater. If you mark column 2b for acrolsin, acrylonitrfle 2,4 dlNtrophanoi, or 2-methyl-4,6 dhdtrophanol, you must provide the results least of at one analysis for each of these Pollutants which you know or have reason that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must ether submit at least one analysis briefly or describe the reasons the pollutant is expected to be discharged Note that there are 7 pages to this part, please review each carefully. Complete one table (all 7 pages) for each outfall. See Instructions for additional detatis and requirements. I. POLLUTANT AND CASE NO 2 MARK "X" 3. EFFLUENT 4. UNITS 6. INTAKE (opffona. I a MA)MK M DAILY VALUE b. MARUyUM SO DAY avaAabb) VALUE (A a LONGTERM AVRG. VALUE (f (lfavailable) &TESTING b.BELIEVED MBELIEVED (1) avellablel dNO. OF a. LONG TERM AVERAGE VALUE (1) CONCENTRATION MASS (1) CONCENTRATION (2) MASS REQUIRED PRESENT ABSENT (1) CONCENT1tATl0 (2)MASS N N CONCENTRATION (2 )MASS )CON (1 CENTRATIO (2) MASS ANAL ANALYSES b.NO.ALY E ANALYSES ,. 1M.Antimony Total (7440-36-0) X N/A N/A NA NA NA N/A 2M. Arsenic, Total NA N/A N/A NA NA NA N/A NA NA NA (7440-38-2) 3M. Beryllium, X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA Total (7440-41-7) W. Cadmium, X N/A N/A NA NA NA NA N/A N/A Total (7440-43-9) romhum, O X N/A N/A NA NA NA NA N/A NIA N/A NA NA NA (7440-47-3) 6M. Copper, Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (7440-50-8) 7M. Lead, Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (7439-92-1) 8M. Mercury, Total X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (7439-97-6) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 9M. Nickel, Total (7440-02-0) 10M. Selenium, X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA NA NA Total (7782-49-2) X N/A N/A NA NA NA NA N/A N/A N/A NA 11 M. Silver Total (740-22-4) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 12M. Thallium NA NA Total (7440-28-0) X N/A N/A NA NA NA NA N/A N/A N/A NA 13M. Zinc, Total (7440-66-6) X N/A N/A NA NA NA NA N/A NIA N/A NA NA NA 14M. Cyanide, Total (57-12-5) X I N/A N/A NA NA NA NA N/A N/A N/A NA NA NA 15M. Phenols Total X N/A NIANA NA NA N/A N/A N/vAyf NA NA '4:, i S1 .- h �,. y bn�� .:� h`ry _ ry9yfi 2 1M nC� "('.4 Q: b r x Leh. `S �2';2.� ��. M�. ���u �� t$P�.w.'� k h h h,C ^"( ..il a#��' ...aQu6'✓'1t ftlr 2,3,7,8-Tetrachloridibenzo-P Dioxin (1764-01-6) X N/A NA NA NA EPA Form 3510.2C [P-On1 CONTINUED ON PAGE V-4 ITEM V-S CONTINUED FROM PREVIOUS PAGE 1. POLLUTANT AND CASE NO 2 MARK'X' 3. EFFLUENT 4. UNITS S. INTAKE (optlonaQ a ElA7IDGUM DAILY b. MAITIMUM 30 DAY VALUE IV a LONG TERM AVRG. VALUE pT ((feV2lWb1B) VALUE avm98ble) aysuaWel d. NO. OF a LONG TERM AVERAGE VALUE a.TESTING LSELEVED c.SELIEVED (1) (1) REQUIRED PRESENT' ABSENT CONCENTRATION (2) CONCENTRATION (2) MASS CONCENTRATION (1) CONCERATiON (2) MASS ANALYSES (1) CONCENTRATIO (2) MASS (1) CONCENTRATION b.NO.OF ANALYSES C 1 V. Acr 1 o eiI N/A NA NA NA (107-02-8) X NIA N/A NA NA NA NA NA N/A 2V. Acrylonlidle (107-13-1) X N/A N/A NA NA NA NA NA NIA N/A NA NA NA 3V. Benzene (71-43-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA W. Bis (Chloromethyl) Ether (5424M-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 5V. Bromoforin (75-25-2) X N/A. N/A NA NA NA NA NA N/A N/A NA NA NA 6V. Carbon Tetrachloride (56-23-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 7V. Chlorobenzene (108-90-7) X N/A N/A NA NA NA NA I NA N/A N/A NA NA NA 8V. Chlorodibromomethane (124-48-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 9V. Chloroethane (75-00-3) X N/A N/A NA NA NA NA NA N/A NIA NA NA 1 OV. 2 Chlorohylvinyl Ether (110-75-8) X N/A NIA NA NA NA NA NA N/A N/A NA NA JNA 11V. Chloroform (67-66-3) X NIA N/A. NA NA NA NA NA N/A NIA NA NA 12V. Dichlorobromomethane (75-27-4) X N/A NIA NA NA NA NA NA NIA NIA NA NA NA 13V. Dichlorodifluoromethane (75-71- 8) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 14V.1,1 Dichloroethane (75-34-3) X N/A N/A NA NA NA I NA NA N/A N/A NA NA NA 15V.1,2 Dichloroethane (107-06-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 16V.1,1 Dichloroethylene (75-35-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 17V.1,2 Dichloropropane (78-87-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 18V.1,3 Dichloropropylene (542-75-6) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 19V. Ethylbenzene(100-41-4) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 20V. Methyl Bromide (74-83-9) X N/A NIA NA NA NA NA NA N/A N/A NA NA NA 21V. Methyl Chloride (74-87-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA V,III YV,V LV V-S/V! VAUt V-4 CONTINUED ON PAGE V-5 EPA LO. NUMBER (copy from Item 1 of Form 1) OUTFALL NUMBER CONTINUED FROM PAGE V-4 I luf1nnn4a74 Form Approved OMB No. 2040 0086 - - - - - - - Approval expires 831-98 I. POLLUTANT AND CASE NO 2 MARK "X" 3. EFFLUENT 4. UNITS S. INTAKE (opffonao a MAMIUM DAILY b. MAXI!%UM 30 DAY VALUE (N a LONG TERMG. A VALUE (d VALUE �, % & LONG TERM AVERAGE VALUE &TESTING REQUIRED b.BELIEVED PRE SENT CSELIEVED ABSENT (1) CONCENTRATION (2)MASS i1) CONCENTRATION (2j MASS CONCENTRATION (2) MASS 1 CONCENNTRATION (2) MASS (1) CONCENTRATION (2) MASS (IfavaUable) I` d.NO. OF ANALYSES b. LYO. E ANALYSES e V. , S 1.. 22V Methylene Chloride (75-09-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 23V.1,1,2,2 Tetrachloro- ethane (79-34-5) X N/A NIA NA NA NA NA NA NIA N/A NA NA NA 24V. Tetrachloroethylene (127-18-4) X I N/A N/A NA NA NA NA NA N/A N/A NA NA NA 25V. Toluene (108-88-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 26V. 1,2-TransDichioro- ethylene (156-60-5) X NIA NIA IVA NA NA NA NA NIA N/A NA NA NA 27V. 1,1,1 Trichloroethane (71-55-6) X N/A N/A NA NA NA NA NA N/A N/A I NA NA I NA 28V. 1,1,2 Trichloroethane (79-00-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 29V. Trichloroethylene (79-01-6) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 30V. Trichicrofluoro- methane (75-69-4) X N/A N/A NA NA NA NA NA NIA N/A NA NA NA 31V. Vinyl Chloride (75-01-4) X N/A N/A NA NA NA NA NA N/ NA NA NA q "fit 14' 1A. 2 Chlorophenol (95-57-8) X N/A N/A NA NA NA NA NA N/A NIA NA NA NA 2A 2,4 Dichlorohenol (120-83-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 3A. 2,4 Dimethylphenol (105-67-9) X N/A NIA NA I NA NA NA NA N/A N/A NA NA NA 4A 4,6 Dinkro-O-Cresol (534-52-1) X N/A N/A NA NA NA NA NA N/A NIA NA NA NA 5A. 2,4 Dinitrohenol (51-28-5) X N/A NIA NA NA NA NA NA N/A N/A NA NA NA 6A.2-Nitrophenol (88-75-5) X NIA N/A NA NA NA NA NA N/A N/A NA NA NA 7A4-Nitrophenol(100-02-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 8A. P-Chloro-M-Cresol 59-50-7 X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 9A. Pentachlorophenol (87-86-5) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 10A. Phenol (108-95-2) X N/A NIA NA NA NA NA NA NIA N/A NA NA NA 11A. 2,4,6 Trichloro- phenol (88-06-2) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA �rr� rvnn as 1 V LV In -awl PAGE V-5 CONTINUED ON PAGE V-6 CONTINUED FROM PAGE V-6 1. POLLUTANT AND CASE NO 2 MARK nr 3. EFFLUENT 4. UNITS S. INTAKE (optbnao a MAXIMUM DAILY b. MA)OMUM 30 DAY VALUE (H t LONG TERM AVRG. VALUE (if VALUE aveflaNe) avatlwa) a LONG TERM AVERAGE VALUE a TESTING RECORED b. BELIEVED PRESENT a9ELIEVED ABSENT CEMRA noN cz) MASS (ffavaila6fe) (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION d NO. OF ANALYSES (2) MASS b. N0. OF ANALYSES (1) coNCENrRanoN (z) Mass ._. _ _ .__ <. .., ,. 1•:'; rA ��>:�R. Y, Aa y 4.y �} '.,?.o- a'Yfi >4,,,' Y.r r.�'s�h J'" 6 t%' �ii� "� a :2.c 55 S L ,.' s 1 B. , �y r,fg,° , .�f :^ 1 �' Acenaphthene (83-32-9) X WA WA NA NA NA NA NA WA WA NA NA NA 2B. Acenaphtyiene (208-96-8) X WA WA NA NA NA NA NA WA WA NA NA NA 3B. Anthracene (120-12-7) X WA WA NA NA NA NA NA WA WA NA NA NA 4B. Benzidine (92-87-5) X WA WA NA NA NA NA NA N/A WA NA NA NA 5B. Benzo (a) Anthracene (56-55-3) X WA WA NA NA NA NA NA WA WA NA NA NA 6B. Benzo (a) Pyrene (50-32-8) X WA WA NA NA NA NA NA WA WA NA NA NA 7B3,4 Benzofluororanthene (205-99-2) X WA WA NA NA NA NA NA WA WA NA NA NA 8B. Benzo(ghi)Perylene (191-24-2) X WA WA NA NA NA NA NA WA WA NA NA NA 9B. Benxo (k) Fluoranthene (207-08-9) X WA WA NA NA NA NA NA WA WA NA NA NA 10B. Bis(2-Chloroethoxy) Methane (111-91-1) X WA WA NA NA NA NA NA N/A N/A NA NA NA 11 B. Bis(2-Chloroethyl) Ether (111-444) X WA WA NA NA NA NA NA WA WA NA NA NA 12B Bis{2Chlorolsopropyl) Ether (102-60-1) X WA I WA NA NA NA NA NA WA WA NA NA NA 13B. Bis(2-Elthylhexyl) Phthalate (117-81-7) X WA WA NA NA NA NA NA WA WA NA NA NA 14B.4BromophenylPhenyl Ether (101-55-3) X WA WA NA NA NA NA NA WA N/A NA NA NA 15B. Butyl Benzyl Phthalate (85-68-7) X WA WA NA NA I NA NA NA WA WA NA NA NA 16B. 2-Chloronapthalene (91-58-7) X WA WA NA NA NA NA NA WA WA NA NA NA 17B.2-Chlorophenyl Phenyl Ether (7005-72-3) X WA WA NA NA NA NA NA WA WA NA NA NA 18B.Chrysene(218-01-9) X WA WA NA NA NA NA NA WA WA NA NA NA 19B. Dibenzo (a,h) Anthracene (53-70-3) X WA WA NA NA NA NA NA WA WA NA NA NA 20B. 1,2 Dichlorobenzene (95-50-1) X WA WA NA NA NA NA NA WA WA NA NA NA 21B. 1,3 Dichlorobenzene (541-73-1) X WA WA NA NA NA NA I NA WA WA NA NA NA -• ^ • �•••• %- i PAGE V-0 CONTINUED ON PAGE V-7 CONTINUED FROM PAGE V-6 EPA I.D.rmm ER (CPYrrom Hem of Farm 1/ OUTFALL NUMBER eWpT0veu OMB No. 2040 0086 NC0003573 008 Approval expires 8-31-88 I. POLLUTANT AND CASE NO 2 MARK "X' 3. EFFLUENT 4. UNITS 5. INTAKE (oP>Yormo a MA)OMUM ONLY 6. MAXIMUM 3p DAY VALUE (// a LONG TERM AM. VALUE (H VALUE (ff evallebin) a TESTWG b. BE N aAEN VN.UE) evaPaWeJ d NO. OF a LONG TERM AVERAGE (1)CONCENTRATION 2 ()MASS (1)CONCENTRATION (2)MASS S. m REQUIRED SEENT PRESENT T ASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS (1) CONCENTRATION (2) MASS ANALYSES b. O OF ANALYSES 226. 1 _ . ;4 Dichlorobenzene NA NA (106-46-7) 23B.3,3' Dichiambenzidine X N/A N/A NA NA NA NA NA N/A NIA NA N/A N/A NA NA NA (91-94-1) 24B. Diethyl Phthalate X NIA N/A NA NA NA NA NA NA N/A N/A NA NA NA (84-66-2) 25B. Dimethyl Phthalate X N/A N/A NA NA NA NA N/A N/A NA NA NA (131-11-3) 26B. Di-N-Butyl- X NIA N/A NA NA NA NA NA Phthalate (84-74-2) X NIA N/A NA NA NA NA NA N/A N/A NA NA NA 27B. 2,4 Dinitro N/A N/A NA NA toluene (121-14-2) X N/A N/A NA NA NA NA NA 28B. 2,6 Dinitrotoluene NA (606-20-2) 29B. Di-N-Octyl Phthalate X N/A NIA NA NA NA NA NA N/A N/A NA NA NA (117-84-0) 30B. 12 Diphenylhydrazine X NIA N/A NA NA NA NA NA N/A N/A NA NA NA N/A NA NA NA (as Azoberizene) (122-66-7) X NIA N/A NA NA NA NA NA N/A 31B. Fluoranthene NA NA NA (206-44-0) X N/A N/A NA NA NA NA NA N/A N/A 32B. Fluorene (86-73-7) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 33B. Hexachlorobenzene (118-74-1) X N/A NIA NA NA NA NA NA N/A N/A NA NA NA 34B. Hexachlorobutadiene NA NA (87-68-3) X N/A N/A NA NA NA NA NA N/A N/A NA 35B. Hexachlorocyclo- pentadiene (77-47-4) X N/A NIA NA NA NA NA NA N/A NIA NA NA NA 36B. Hexachloroethane (67-72-1) X NIA NIA NA NA NA NA NA N/A N/A NA NA NA 37B.Indeno1,2,3 cdPyrene (193-39-5) X NIA N/A NA NA NA I NA NA N/A N/A NA NA NA 38B. Isophorone NA (78-59-1) X N/A N/A NA NA NA NA NA N/A N/A NA NA 39B. Naphthalene (91-20-3) X NIA N/A NA NA NA NA NA N/A NIA NA NA NA 40B.Nitrobenzene (98-95-3) X N/A N/A NA NA NA NA NA N/A N/A NA NA NA 41B. N-Nitrosodime- , thylamine (62-75-9) X N/A N/A NA NA NA NA NA N/A N/A NA NA 42B. N-Nitrosodi-N- NA NA Propylamine (621-64-7) X N/A N/A NA NA NA NA NA NIA N/A NA NA EPA Form 3510-2C lS-901 ^"� V-1 CONTINUED ON PAGE V-8 CONTINUED FROM PACE V.7 1- POLLUTANT AND CASE NO a TESTING (lfavalla6le) REQUIRED 43BN-Nitrosodiphenylamine (86-30-6) X 44B. Phenanthrene (85-01-8) X 45B. Pyrene (129-00-0) X 46B. 1,2,4Tdhlorobenzene (120-82-1) X 1P.Aldrin(309-00-2) X. 2P. a-BHC (319-84-6) X 3P. (i-BHC (319-85-7) X 4P. y-BHC (58-89-9) X 5P. &-BHC (319-86-8) X 6P. Chlordane (57-74-9) X 7P. 4,4' DDT (50-29,3) X 8P. 4A' DDE (72-55-9) X 9P. 4,4' DDD (72-54-8) X 10P. Diedrin (60-57-1) X 11 P. a Endosulfan (115-29-7) X 12P. fl-Endosulfan (115-29-7) X 13P. Endosulfan Sulfate (1031-07-8) X 14P. Enddn (72-20-8) X 15P. Endrin Aldehyde (7421-93-4) X 16P. Heptachlor (76-44-'8) X EPA Form 3510-2C (RAM 2 MARK W 3.EFFLUENT 4. UNITS 5. INTAKE (opBonao a MAXIMUM DAILY VALUE b, MAXIMUM 30 DAY —bbw VALUE ((/ a LONG TERM AVRG. VALUE ff—a11able) NO (>F ANALYSES ,�9r.,::.. a LONG TERM AVERAGE VALUE b, N(L OF ANALYSES b. BEIJF/FD PRESENT c.BEI.IEVED ABSENT (1) CONCENTRATIOQMASS WA WA WA N/A y d Y� .qf�+�li.r", { WA WA N/A N/A :�i. i ��ii l 1 CONC ENTRATIONd () +i N. NA NA NA NA ,� ��w 'dF Lh Ii4,�.1W x (2) MASS ,. NA NA NA NA a9 { "T y 4 NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA (1) CONCENTRATION ' NA NA NA NA Ah 1'. - �2 fit` NA NA NA NA NA NA NA NA NA I NA NA NA NA NA NA NA (2) MASS P h.l.. (1) CONCENTRATION „21r (2) MASS ::u?3--.; 4 i (1) CONCENTRAMOMN �.r.t 7 f „jR,.w"4 _ NA (2) MASS a .te,"R"?'"'q�,(,.l NA <,W , NA NA NA A NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA WA WA NA NA NA NA NA NA WA WA N/A N/A WA WA N/A N/A N/A NA NA NA NA NA NA NA NA NA WA N/A WA WA WA WA WA WA WA WA N/A WA NIA WA NIA WA N/A N/A WA N/A WA WA WA N/A N/A N/A NIA WA WA WA N/A WA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA ....... NA NA NA WA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA WA WA WA WA N/A N/A N/A WA NA NA NA NA NA NA NA NA NA NA NA NA N/A N/A NA NA NA WA WA WA WA , NIA N/A N/A N/A WA N/A N/A WA NA NA NA NA NA NA NA NA NA NIA NA NA NA N/A NIA WA N/A WA NA NA NA NA NA NA NA NA NA NA NA NA NA NA NA •rwc v-a CONTINUED ON PAGE V-9 EPA I.D. NUMBER (copy from Them 1 Of Form 1) OUTFALLNUMBER .—....-11. ..au CONTINUED FROM PAGE V-8 NC0003573 006 OMB No.2l)40 Approval expires 0086 s-31.98 1. POLLUTANT AND CASE NO 3. EFFLUENT 2 MARK °X" b. MAXIMUM 30 DAY VALUE (B a LONG TERM AVRG. VALUE (ff a. MAXIMUM DAILY VALUE 8vaitable) avaHaMe) 4. UNITS 5. INTAKE (Optional) a LONG TERM AVERAGE VALUE a TESTING REQUIRED b. BELIEVED PRESENT GgELIEVED ABSENT (1) CONCENTRATION (2) MASS (1) CONCENTRATION � MASS (1 )CON CONCENTRATION _i :. (2) MASS d. NO. OF ANALYSES (If available) 17P. Heptachlor b. NO. OF ANALYSES (1) CONCENTRATION (2) MASS /e hv. (1) CONCENTRATION (2) MASS NA N/A N/A N/A NA NA NA Epoxide (1024-57-3) 18P. PCB-1242 X N/A N/A NA NA NA N/A NA NA NA (53469-21-9) 19P. PCB-1254 X N/A N/A NA NA NA NA NIA N/A NIA N/A NA NA NA (11097-69-1) 20P. PCB-1221 X N/A N/A NA NA NA NA N/A N/A NA NA NA (11104-28-2) 21 P. PCB-1232 X N/A N/A NA NA NA NA NIA N/A (1114-16-5) 22P. PCB-1248 X N/A N/A NA NA NA NA N/A NIA N/A NA NA NA N/A NA NA NA (12672-29-6) 23P. PCB-1260 X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA (11096-82-5) 24P. PCB-1016 X NIA N/A NA NA NA NA N/A N/A NA NA NA (12674-11-2) 25P.Toxaphene X N/A N/A NA NA NA NA N/A N/A N/A (8001-35-2) X N/A N/A NA NA NA NA N/A N/A N/A NA NA NA EPA Form 35in-2C ist-am