DEQ-CFW_00060708

KNW
EFFL ENT CT 2 20
NPDES PERMIT NO. NC0003573 DISCHARGE'NO. 001 MONTH September YEAR 2010
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4,_, , . PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie Lewis I Ray Beard i Russell Rotan
Mail ORIGINAL and ONE COPY to: NUV 0 8 2010
ATTN: CENTRAL FILES 0 A t
DIV. OF WATER QUALITY q{nj X U .` `" hj� IV
DENR 4o V 2 GU�® (SIGNA URE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
FLOW
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HRS
HRS
Y/N
MGD
-C
UNITS
Lb/Day
Lb/Da1
1
08001
24
Y
0.878
28
7.83
<14:6
65.9
2
0800
24
Y
0.920
3
>osoo
24
Y
0.839
4
0800
24
1.056
5
osoo
24
0.864
6
0800
24
*
0.721
*
<12.01
47.5
7
0800
24
Y
0.850
28
7.87
14.9
36.2
8
o800
24
Y
0.896
28
7.94
<14.9
59.8
9
osoo
24
Y
0.800
28
7.92
10
0800
24
Y
0.824
11
0800
24
0.744 i
12
0800
24
0.745
13
osoo
24
Y
0.935
27
7.81
21.8
39.8
14
0800
24
Y
0.774
27
7.75
20.0
65.8
15
0800
24
- Y
0.841
27
.....................
7.77
19.6
_..._...._ _...
98.2
16
0800
24
Y
0.736
17
0800
24
Y
0.433
18
0800
24
0.287
19.
rosoo
24
0.050
20
0800
24
Y
0.000
**
**
**
21
osoo
24
Y
0.000
22
0800
24
Y
0.000
**
**
**
**
23
0800
24
Y
0.000
24
0800
24
Y
0.000
25
osoo
24
0.000
2610800
24
0.000
27
o800
24
" Y
0.000
28
0800
24
Y
0.196
25
6.73
8.7
20.6
29
080o
24
Y
0.140
25
6.78
2.7
8.2
30
osoo 1
24
Y
0.139
24
6.85
4.4
14.1
¢�,
w
F
oz
N
00
U
q2
O
X m
x
-
U
<5.0
MINIMUM 0.000 1 24 1 6.73 <12 1 8.2 <5.0
Comp,,(C) Grab (G) G G C C G C
Monthly Limit 2.0 191.3 317.8 PASS
Daily Limit' 6-9 508.2 1030 0.5
DEM Form MR-1 (12193)
* Holiday
** Shutdown
DEQ-CFW 00060708

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements F7
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be -made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
mnt or type)
A j r14l1
ign&ure of
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp.-Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
Chlorine
00082
Color (ADM])
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147
Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730
Total Phenolics
81551 Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530
Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
" If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
01 81 iJQ
DEQ-CFW 00060709

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH September YEAR 2010
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie Lewis / Ray Beard / Russell Rota
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY X
DENR (SIGN4kURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
50050
00010
00400
1 00951
00665
00600
51521
00310
00340
Y
FLOW
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HRS
HRS
Y/N
MGD
'C
UNITS
Lb/Day
mg/L
mg/L
ug/L
mg/L
mg/L
1
0800
24
Y
18.868
29
7.25
1983
2
0800
24
Y
17.177
28
7.41
3
0800
24 `
Y
17,959
29
7.12
4
0800
24
1 17.185
5
0800
24
17.619
6
0800
24
18.156
7
0800
24
'' Y
17.120
28
7.30
0.38
2.29
8
o800
24
Y
17.504
29
7.60
2029
0.06
9
osoo
24 '
Y
17.552
28
7.51
10
moo
24
Y
17.152
28
7.40
11
080o
24
16.387
`-
12
0800
24
15.715
13
0800
24
Y
16.660
27
7.39
14
0800
24
Y
15.033
27
7.40
15
0800
24
Y
14.817
27
7.41
2076
16
0800
24
Y
14.672
27
7.37
17
'0800
24
Y
14.254
27
7.31
18
0800
24
14.318
19
0800
24
13.182
20
080o
24
Y
0.000'
21
0800
24
Y
0.000
*'
22
0800
24
Y
0.000
23
0800
24
r Y
0.000
**
24
0800
24
Y
0.000
25
o800
24
0.000
26
0800
24
0.000
2710800
24 1
Y
0.000'
28
0800
24
Y
0.196
25
6.70
Note:
09/28-30/10
flow completely
from Outfall
001
29
0800
24
Y
0 140
24
689
119
30
0800
24
Y
0.139
24
6.90
31
0800
24
AVERAGE
10.394
27
1552
0.38
2.29
0.06
MAXIMUM
18.868
29
7.60
2076
0.38
2.29
0.06
MINIMUM
0.000
24
6.70
119
0.38
2.29
0.06
0mp. (G) Grab (G)
G
G
G
C
C
G
C
C
Monthly Limit
Daily Limit
i
I 1
1 6-9
7917
DEM Form MR-1 (12/93)
* Holiday
** Shutdown
DEQ-CFW 00060710

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements '
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
Permittee (Please print or type)
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp..Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
Chlorine
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147
Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730
Total Phenolics
81551 Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530
Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
" ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
01 81 100
DEQ-CFW 00060711

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: September YEAR: 2010
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
C
00010
00400
00310
00610
00530
00094
51521
3
N
OI
S
0
(y
O E
>
:a
o
d
N
p
=
w
7
V
(a
G0
cm
O N
CL m
O,
M
4)
V •+
N
O V
a
>
~
~
QW
LL N
d
o
�'
a
m
HRS
°C
units
mg/L
mg/L
#/100m1
µmho/cm
ug/L
DWQ Form MR-3 (Revised 7/2000)
00010
00400
00310
00610
00530
00094
x
O
U
C.1
a .0
•d6
y
E
.��+
•>
r
O
a3+ y
(aci
=
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G
N
N
C.
M
a
d
>
am
L•
ui
6
R E
F-
f'
O
LL
V
_N
3
m
HRS
°C
units
mg/L
mg/L
#/100ml
',µmho/cm
1
2
3
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
31
Average
Maximum
Minimum
DEQ-CFW 00060712

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements LJ
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Karen B. Wrigley - Plant Manager
Permittee (Please print or type)
l -
0/lLf I is
Signature of
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092
Zinc
Chlorine
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105
Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147
Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616
Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730
Total Phenolics
81551 Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235
Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481
Toluene
00530
Total Suspended
00927
Total Magnesium
38260
MBAS
Residue
00929
Total Sodium
01045
Iron
39516
PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
01 81 K1,101
DEQ-CFW 00060713

am.
N.C. Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
DuPont Fluoroproducts
Fayetteville Works Plant
22828 NC Highway 87 West
Fayetteville, NC 28306
October 14, 2010
DISCHARGE MONITORING REPORT — September 2010
Attached is E. I. DuPont de Nemours & Company, Inc., Fayetteville Works Discharge
Monitoring Report for the month of September 2010.
If you have any questions, please contact Jamie R. Lewis at [phone].
JRL: jlp
Attachment
cc: Ken Cook - ENGR, Old Hickory
J. R. Lewis - FW
J. L. Locklear - FW
File: F-1-3-4
E.I. du Pont de Nemours and Company
DEQ-CFW 00060714

DEQ-CFW 00060715