DEQ-CFW_00060643

OA
EFFLU NT JUN 2 8 2011
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 001 MONTH May YEAR 2011
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHA 6�4 A PERSON(S) COLLECTING SAMPLES Jamie Lewis / Ray Beard / Russell Rotan
Mail ORIGINAL and ONE COPv!\s' D
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
JUN 2 0 2011 x'
DENR (SIGNATLIRE OF OPERATOR IN RESPONSIBLE CHARGE) �t J� ri ;
1617 MAIL SERVICE CENTER CENTRAL FILES BY THIS SIGNATURE, 1. CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 DWQ/BOQ
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Lb/Day
Lb/Day
mg/L
P/F
Ug/L.
1
6800
24
0.831
2
0800
24
Y
0.574
25
7.85
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16.8
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Comp.,,(C) Grab (G) G G C C G. C
Monthiv Limit 1 2.0 191.3 317.8 PASS
DEM Form MR-1 (12/93)
* Holiday
DEQ-CFW 00060643

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plant
Per ittee (Plea print or t�
11
nature
�i
Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01027 Cadmium
01032
Hexavalent Chromium
01034
Chromium
01037
Total Cobalt
01042
Copper
01045
Iron
01051
Lead
01092 Zinc
01105 Aluminum
01147
Total Selenium
31616
Fecal Coliform
32730
Total Phenolics
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCB's
50050
Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060644

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 05/12/11
Facility=t--�PONT FAYETTEVILLE NPDES#: NC0003760 Pipe#: 002 County: BLADEN
Laborator Perfoen Test: MERITECH LABS, INC.
Comments: dilution water batch
Xf2}
Signatu e o t Operaor in Responsible C a ge 877 and 878 used. 878 hard 46mg/1
X and 177umhos
Signature of Laboratory Supervisor * PASSED:-19.28W Reduction
Work Order: Environmental Sciences Branch
MAIL ORIGINAL TO: Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
forth Carolina Cerioclapnnia
Chronic Pass/Fail Reproduction Toxicity Test
�ONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced 1121120126121125126116115116118118127
Adult (L)ive (D)ead JIL (L IL IL IL IL IL IL IL IL IL IL
affluent W: 3.3W
PREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 li 12
# Young Produced 1121127128129126118126126125124126121
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL IL IL IL IL
Chronic Test Results
Calculated t = -2.567
Tabular t = 2.508
Reduction = -19.28
t Mortality
Avg.Reprod.
0.00
20.75
Control
Control
0.00
24.75
Treatment 2
Treatment 2
Control CV
20.868W PASS FAIL
control orgs �K]
producing 3rd
brood Check One
91.7%,
1st sample 1st sample 2nd sample Complete This For Either Test
PH Test Start Date: 05/04/11
Control 8.14 8.10 8.19 8.02 8.12 7.96 Collection (Start) Date
Sample 1: 05/02/11 Sample 2: 05/04/11
Treatment 2 8.13 8.04 8.17 7.94 8.08 8.00 Sample Type/Duration 2nd
1st P/F
s s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d U M M
t t t Sample 2 X 24 hrs T P P
1st sample 1st sample 2nd sample
D.O. Hardness (mg/1) 46
Control 7.39 7.35 7.57 7.24 7.50 7.26
Spec. Cond.(pnhos) 178 295 262
Treatment 2 7.43 7.32 7.52 7.25 7.48 7.18
Chlorine(mg/1) ,,,,.... 0.13 0.11
LC50/Acute Toxicity Test Sample temp. at receipt(°C) ,. 0.1 0.4
(Mortality exuressed as %, combininu replicates)
Note: Please
Concentration Complete This
Section Also
Mortality
start/end start/end
C,C50 = %- Method of Determination
95W Con i ence Limits Moving Average - Probit
9.-- g Spearman Karber _ Other
Control
High
PH
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
m •
DEQ-CFW 00060645

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH May YEAR 2011
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE _(910) 678-1219
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX 1F ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie Lewis I Ray Beard / Russell Rotan
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY X wm-"✓
DENR (SIGNATU OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617
50050
00010
00400
00951
00665 1
00600
51521
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00340
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Y/N
MGD
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UNITS
Lb/Day
mg/L
mg/L
ug/L
mg/L
mg/L
1
108001
24 1
8.763
2
108001
24 1
Y
9.794
25
7.49
3
1-08001
24 1
Y
10.680
25
7.50
4
108001
24 1
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11.553
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1 489
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=Y
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6
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11.722
24
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7
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1 11.918
8
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24
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24
7.52
10
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24
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11.764
24
7.46
71
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24
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1UT6
25
1.55
545
0059
12
0800
24
Y
13.096
25
7.43
13
0800
24
B
11;.293
27
7.44
14
0800
24
13.015
15
0800'
24
12.359
16
0800
24
Y
13.081
25
7.41
17
0800
24
Y
12.640
25
7.37
0.398
2,22
1, <2.0
25.6
18
08001
24 1
Y
12.470
25
7.60
903
19
08001
24 1
Y
12614
25
7.34
20
08001
24 1
Y
12.037
25
7.41
21
08001
24 1
12.312
22
08001
24 1
12.369
23
08001
24 1
Y
12.765
26
747
24
08001
24 1
Y
12.765 1
27
7.52
25
08001
24 1
B
12.636
29
7.13
700
26
08001
24
Y
13.300
28
7.36
27
08001
24
Y
13.061
28
7.32
28
0800
24
12.729
29
0800'
24
13.585
30
0800
24
12.953
31
0800
24 1
Y
13.251
29
7.44
AVERAGE
12.135
26
659
0.398
2.22
0.059
0.00
25.60
MAXIMUM
13.585
29
7.60
903
0.398
2.22
0.059
<2.00
25.60
MINIMUM
8.763
24
7.13
489
0.398
2.22
0.059
<2.00
25.60
MID. (C);Grab (G)
G
G
G
C
G
G
1 C
C
Monthly Limit
Daily Limit
6-9
7917
DEM Form MR-1 (12/93)
Holiday
DEQ-CFW 00060646

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H.
re of
print or
?AI A I
Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01092
01027 Cadmium 01105
01032
Hexavalent Chromium
01147
01034
Chromium
31616
32730
01037
Total Cobalt
34235
01042
Copper
34481
38260
01045
Iron
39516
01051
Lead
50050
Zinc Chlorine
Aluminum
Total Selenium
71880 Formaldehyde
Fecal Coliform
71900 Mercury
Total Phenolics
81551 Xylene
Benzene
Toluene
MBAS
PCB's
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060647

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: May YEAR: 2011
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
00010
00400
00310
00610
00530
00094
51521
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~
Q
N
IL d
:i
d
'06
HRS
°C
units
mg/L
mg/L
#/100mi
Nmlro/cm
ug/L
1 i
DWQ Form MR-3 (Revised 7/2000).
00010
00400
00310
00610
00530
00094
Y
C
W
Q
Ul
C
V
y
G E
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C1
B
m
HRS
°C
units
mg/L
mg/L
#/100m1
pmno/cm
1
2
3
5
6
7
9
10
11
12
13
14
15V
:
Li
16
17
18
'19
20
21
22
23
24
25
26
27
28
29
30
31
Average
Maximum
Minimum
DEQ-CFW 00060648

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
),
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2011
Permittee Address Phone Number Permit Exp. Date
00010
Temperature
00076
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00556
00600
00610
00625
00630
PARAMETER CODES
Oil & Grease 00951 Total Fluoride
Total Nitrogen 01002 Total Arsenic
Ammonia Nitrogen
Total Kjeldhal
Nitrogen
Nitrates/Nitrites
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel 50060 Total
01077 Silver Residual
01092 Zinc Chlorine
01105 Aluminum
01147 Total Selenium
71880 Formaldehyde
31616
Fecal Coliform
71900 Mercury
32730
Total Phenolics
81551 Xylene
34235
Benzene
34481
Toluene
38260
MBAS
39516
PCB's
50050
Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
"' If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060649

DuPont Fluoroproducts
22828 NC Highway 87 W
Fayetteville, NC 28306-7332
amo
DuPont Fluoroproducts
June 16, 2011
N.C. Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
DISCHARGE MONITORING REPORT — May 2011
Attached is E. I. DuPont de Nemours & Company, Inc., Fayetteville Works Discharge
Monitoring Report for the month of May 2011.
If you have any questions, please contact Jamie R. Lewis at [phone].
JRL: jlp
Attachment
cc: Ken Cook - ENGR, Old Hickory
J. R. Lewis - FW
J. L. Locklear - FW
File: F-1-3-4
E. f. du Pont de Nemours and Company
FLA Rev. 312000
DEQ-CFW 00060650