DEQ-CFW_00060488

EFFLUENT .
lJ�
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 001 MONTH February YEAR 2013
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to: p
ATTN: CENTRAL FILES ..MAR 2 p 2013
DIV. OF WATER QUALITY X d0rJ_j_?_ 9UArl,J pr
DENR (SIGNATU E OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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HRS
Y/N
MGD
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UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
1
0800
- 24 -
Y
2
0800
24
0.945
3 `
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24'
..
0.930.
4
0800
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6
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0.927
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7.50
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,
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10800
24
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0.915
9
0800
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0.890
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0600
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0.933
19 _
. 7.55
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68.5
12
0800
24
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0.920
20
7.73
42.2
43.7
13
0800
24
Y
0.959 ,°
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7:70:
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32.0
1410800
24
Y
0.932
15
0860
24
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-0.944
16
0800
24
0.892
17
0800
.24.
0.831
18
0800
24
Y
0.899
18
7.63
18.0
43.5
IaLzi
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19
0800
24
Y
0.949 '
17
7.661
15.8
29.3A
m
20
0800
24
Y
0.864
17
7.70
<14.4
<20.9
a
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21
0600
24
Y
0.910
22
0800
24
Y
1.048"fulVAL
ETTE
23
0806
24
1.005
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24
0800
24
0.843
25
0800
24,1
Y
1 0.922
191,7.61
<15.4
<48.4
26
0800
24 1
Y
1 0.930
19
7.63
<15.5
27.9
27
0800
24.
`-� Y ..
V.882
19
7.65%
..17.7
<20.6
28
o800
24
Y
0.853
29
0860
.24 -
30
0800
24
31
0800
24_.
AVERAGE
0.918
18
31.7
43.4
0
MAXIMUM
"1.048
21 _`
7.73
71.1
109.0
<50
MINIMUM
0.795
15
7.40
<14.4
<20.6
<5.0
Comp; (C) Grab (G)
G:
G
C
C '.
G
G
G"
G`
G
G
G
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
Daily Limit
6-9 1484.7
981.5
0.5
20.85
25.44
.29.96
19.65
DEM Form MR4 (12/93)
DEQ-CFW 00060488

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plant
Peffnittee (Please print or t
-22---2bt3
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01092
01105
01147
31616
32730
34235
34481
38260
39516
50050
Zinc
Aluminum
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Toluene
MBAS
PCB's
Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 26 .0506
(b) (2) (D)
DEQ-CFW 00060489

r
EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002 MONTH February YEAR 2013
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES (�
DIV. OF WATER QUALITY X
DENR (SIGNATURE F OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
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MGD
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UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1
o8o0
24 ::1
Y
20.305
11 '
7.51''
2
0800
24
20.534
3
0800
24 `
20.355
4
0800
24
Y
20.379
11
7.52
5
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Y
20.672
12 ;:
7.04 ;
<20
<30.0
6
0800
24
Y
20.681
11
7.34
1
15.5
0.87
2.65
7,
6800
124
Y
,23.695
11
7.60
8
0800
24
Y
20.775
11
7.51
9.
0860
-'--24
20.379 '
10
0800
24
20.745
11
osoo
24';
Y
21.'030 `
13
7.41
2
12
0800
24
Y
21.051
13
7.46
13
0800
•`24 :'
. :'Y
20.425
13 '
7M _
0.032
14
080o
24
Y
20.255
13
7.50
15
o800
24
Y'
'.20.621'
13
7.61
16,0800
_:
24
20.222
17
0800
24
19.802
18
0800
24
Y
20.294
12
7.51
19
0800
.24:.
Y
20.339"
12
7.70:
20
o800
24
Y
20.132
12
7.64
21
0800
24
Y
20.554
11
7.59'.
22
ono
24
Y
20.681
11
7.55
2310800
24
21.711
2410800
24
20.670
2510800
24 1
Y
20.324
11
7.70
26
0800
24 1
Y
22.769
11
7.62
27
0800
:24.1
Y
: 20.298 °
11
7.53 ,
2810800
24 1
Y
20.313
11
7.59
2916800
24
30
080o
24
3110800
':24.
AVERAGE
20.715
12
0.0
0.0
15.5
0.032
0.87
2.65
P
MAXIMUM .
23.695
13
7.70
<2
<30
15.5
0.032
0 87 .
2.65
P
MINIMUM
19.802
11
77.04
<2
<30
15.5
0.032
0.87
2.65
P
ComP (C) Grab (G)
G
G"
C
C
G
G
C:
G
C
Monthly Limit
Daily Limit
6-9
DEM Form MR-1 (12/93)
DEQ-CFW 00060490

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plant
Permittee (Please print or b
3 -22--Zol,3
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037
Total Cobalt
01042
Copper
01045
Iron
01051
Lead
01092
01105
01147
31616
32730
34235
34481
38260
39516
50050
Zinc
Aluminum
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Toluene
MBAS
PCB's
Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060491

Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 02/22/13
Facility: DUPONT FAYETTEVILLE WORKS NPDES#: NC0003573 Pipe#: 002 County: BLADEN
L�Signa
orat y Pe f ming Test: MERITECH LABS, INC.
Comments: dilution water batch 13
X
ure o Operator in Responsible Charge also used: hard-42, cond-159
X � '!
Signature o L oratory Supervisor * PASSED: -7.24% Reduction
Work Order: Environmental Sciences Branch
MAIL ORIGINAL TO: Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
Vorth Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
�ONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced II27I26I26I26I24I24I19I26I26`22I20I24
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL IL IL IL IL
affluent %: 3.3%
CREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV
10.708%
# Young Produced 29 28 27 23 27 27 27 25 25 23 23 27 % control orgs
producing 3rd
brood
Adult (L) ive (D) ead L L L L L L L L L L L L 100 %
Chronic Test Results
Calculated t = -1.831
Tabular t = 2.508
% Reduction = -7.24
% Mortality
Avg.Reprod.
0.00
24.17
Control
Control
0.00
25.92
Treatment 2
Treatment 2
PASS FAIL
X
Check One
1st sample 1st sample 2nd sample Complete This For Either Test
pH Test Start Date: 02/13/13
Control 8.08 8.00 8.02 8.11 8.08 8.06 Collection (Start) Date
Sample 1: 02/11/13 Sample 2: 02/13/13
Treatment 2 8.08 7.97 8.01 8.10 8.10 7.92 Sample Type/Duration 2nd
1st P/F
s s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24 hrs L A A
r d r d r d U M M
t t t Sample 2 X 24 hrs T P P
1st sample 1st sample 2nd sample
D.O. Hardness (mg/1) 42 ........ .........
Control 7.74 7.59 7.87 7.76 7.79 7.48
Spec. Cond.(pmhos) 160 478 398
Treatment 2 7.70 7.57 7.97 7.75 7.80 7.47
Chlorine (mg/1) ........ 0.44 0.12
LC50/Acute Toxicity Test Sample temp. at receipt(°C) ........ 0.9 0.2
(Mortality expressed as %, combining replicates)
%
%
%
°
I %
%
%
%
%
%
Note: Please
Concentration Complete This
Section Also
Mortality
start/end start/end
C,C50 = % Method of Determination
950-. Con 1 ence Limits Moving Average _ Probit -
-- Spearman Karber Other
Control
High
f'nn r
pH
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
It •
DEQ-CFW 00060492

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: February YEAR: 2013
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
cu
•
rM
DWQ Form MR-3 (Revised 7/2000)
00010
00400
00310
00610
00530
00094
Y
U
y
U
v
cc
4)i
o
-a m
o
x
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f6
N
:3 NCL
T
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N
>
a)m
f0E
o
E
(D
a
,n
O
�_
U
I-
LL
m
H
m
HRS
°c
units
mg/L
mg/L
#1100mi
µmho/cm
'1
3
4
5
6
7
8
9.
10
11.
12
13
14
15 .
16
17
18
19
20
21.
22
23,
24
25
26
27
28
29
30
Average
Maximum
Minimum
DEQ-CFW 00060493

r
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plant
PerVottee (Please print or t
ZZ- 2013
of
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 (910) 6"-1315 October 31, 2016
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01092 Zinc
01027 Cadmium 01105 Aluminum
01032 Hexavalent Chromium 01147
01034
Chromium
31616
32730
01037
Total Cobalt
34235
01042
Copper
34481
38260
01045
Iron
39516
01051
Lead
50050
Total Selenium
Fecal Coliform
Total Phenolics
Benzene
Toluene
MBAS
PCB's
Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060494