DEQ-CFW_00060442

CEI V ED
OCT 2 5 2013
khan u MCESSING UNIT
N.C. Division of Water Quality
Attn: Central Files
1617 Mail Service Center
Raleigh, NC 27699-1617
DuPont Fluoroproducts
22828 NC 87 Highway West
Fayetteville, NC 28306-7332
October 22, 2013
/F
OC l 2 8 2013
DISCHARGE MONITORING REPORT — September 2013
OA
Attached is E. I. DuPont de Nemours & Company, Inc., Fayetteville Works Discharge
Monitoring Report for the month of September 2013.
If you have any questions, please contact Jamie R. Lewis at [phone].
JRL: bao
Attachment DENR—FRO
UV 13 2013
cc: Ken Cook - ENGR, Old Hickory Y
J. R. Lewis - FW M V
M. E. Johnson - FW
File: F-1-3-4
E.I. du Pont do Nemours and Company
DEQ-CFW 00060442

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 001 MONTH September YEAR 2013
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED L� PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
DENR 140V 4 - 2013
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
(SIGNATUft OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
as-(
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HRS
HRS
Y/N
MGD
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UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
Lb/Day
1.
6800
24
0.920, ?
2
o800
24
0.824
25.4
109.3
3
0800
24`
Y
0.625
30
8.00
22;4
53.2
4
o800
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0.576
30
7.96
18.7
83.1
<5.0
5
0800
' 24
Y
0.613 `
30` :
795:.
6
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0.744
7
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.24._s
:1.028
8
0800
24
0.989
9,
0800
24
Y
1.075`
30
7.70
101:3
104 0
10
0800
24
Y
0.858
30
7.74
42.9
314.9
11
'0800
�24 _
: Yt,
' 0.866 '
30
717
41`9
157 4
12
0800
24
Y
0.989
13
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_ 0.943.
14
0800
24
0.987
15
0800
.24'
:
"0.974 .,
16
0800
24
Y
1.000
29
7.47
<16.7
108.4
17
0`800
24
Y
0999
29 ""
740
20:8
100:8
18
0800
24
Y
0.939
27
7.32
21.9
122.2
20
0800
24
Y
0.852
21
0800.
24
'0.905 ;
22
0800
24
0.817
23
0800
;.14 `
Y
0.855
27
7.55,E
17.1>
75.6
24
0800
24
Y
0.896
26
7.40
16.4
47.8
25
0800
24
Y
0.897
25
7.41 `'
24:7-'
26
0800
24
Y
0.821
27
oaoo..
24
Y..
'.0 857 `
-
28
0800
24
0.882
29
0800
24
0.933
30
o800
24
Y
0.953
25
7.24
25.4
<26.2
31
osoo.
-24
AVERAGE
0.884
28
29.2
101.81
0
MAXIMUM
1:075
30 '
8.00.
101.3
314 9
<5.0
MINIMUM
0.576
25
7.24
16.4
<26.2
<5.0
Comp. (C) Grab (G)
":
G
G
C
C
G
G
G
G
G
G
G
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
Daily Limit
17
6-9 1
484.7
'981.5
0.5
1.2G.85
25.44
29.98
19.65
DEM Form MR-1 (12/93) * Holiday
DEQ-CFW 00060443

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements C�
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements L�
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
r:5
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
00082
Color (ADMI)
00625
Total Kjeldhal
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
00300
Dissolved Oxygen
00310
BOD5
00665
Total Phosphorous
00340
COD
00720
Cyanide
00400
pH
00745
Total Sulfide
00530
Total Suspended
00927
Total Magnesium
Residue
00929
Total Sodium
00545
Settleable Matter
00940
Total Chloride
01092 Zinc
01027
Cadmium
01105 Aluminum
01032
Hexavalent Chromium
01147 Total Selenium
01034
Chromium
31616 Fecal Coliform
32730 Total Phenolics
01037
Total Cobalt
34235 Benzene
01042
Copper
34481 Toluene
38260 MBAS
01045
Iron
39516 PCB's
01051
Lead
50050 Flow
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by.other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060444

EFFLUENT
NPDES PERMIT NO. NC0003573 DISCHARGE NO. 002
FACILITY NAME DuPont - Fayetteville Works CLASS
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
MONTH September YEAR 2013
3 COUNTY Bladen
GRADE 4 PHONE [phone]
CHECK BOX IF ORC HAS CHANGED L-J
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
DENR
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
X
(SIGNAT RE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
;;
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HRS
HRS
Y/N
MGD
-0
UNITS
mg/L
mg/L
mg/L
ug/L
mg/L
mg/L
P/F
1
0800
24..
` _ 18.004 "
2
0800
24
16.334
3
osoo
24.
Y
15.976
32:
7.89'
0.50
.3.34
4
0800
24
Y
13.695
32
7.85
5
0800
.24
Y
` 13.630:
32 :-`
7;87.
6
10800
24
Y
15.415
32
7.91
. 7
10800
24,
=18.461
8
10800
24
18.700
9
10800
24 ".
Y
18.321
31 ..
7.85
-
1010800
111
0s00
24
_ 24.
Y
' Y :
14.419
.14.492
31
31
7.81
7.76"-
12
0800
24
Y
1 14.647
31
7.71
13106601
24
Y"
._14.573
31'
7:70:
14
0800
24
14,689
15
0800
..24`
�`13.957
16
0800
24
Y
13.045
30
7.70
17
o660
24
Y
A 2.358 `
30,
7.63'"
18
080o
24
Y
11.429
28
7.65
0.016
19
0800
24
:, Y ,
18.793 -
281.
.7.69
20
0800
24
Y
8.526
28
7.71
21
0806
24 `,
9.847<
22
08001
24
7.952
23
0860 1
24`
Y
` 7.784 `
26
722
24
08001
24
Y
8.017
25
7.19
25
6860
24...Y.
7.810`
25.-'.-
7.17;`:
_
26
0800
24
Y
7.335
25
7.15
27
osoo
24-
Y
7.6,42 -.`
' . 25 ,
7 20;"
2810800
24
8.358
29
000
.24.
;:11786
30
osoo
24
Y
8.861
25
7.22
31
0600
'24`.,
_.:.
AVERAGE
12.495
29
0.016
0.50
3.34
MAXIMUM'.
18.70T
32 `
7.91
0.01.6
"0.50
MINIMUM
7.335
25
7.15
0.016
0.50
3.34
Comp: (C) Grab"(G)`
G'
G
C
C
G
G
C
C
C
,
Monthly Limit
Daily Limit
6-9
DEM Form MR-1 (12/93) * Holiday
DEQ-CFW 00060445

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGauahv -
type)
Signature of Pe mi ee
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 (9 0) 678-1315
Permittee Address Phone Number
Date
October 3 1, 2016
Permit 3 Date
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride
01067 Nickel
50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic
01077 Silver
Residual
00080 Color (Pt -Co) 00610 Ammonia Nitrogen
01092 Zinc
Chlorine
00082 Color (ADMI) 00625 Total Kjeldhal 01027 Cadmium
01105 Aluminum
Nitrogen
00095 Conductivity 00630 Nitrates/Nitrites 01032 Hexavalent Chromium
00300 Dissolved Oxygen
01147 Total Selenium
71880 Formaldehyde
01034 Chromium
00310 BOD5 00665 Total Phosphorous
31616 Fecal Coliform
71900 Mercury
00340 COD 00720 Cyanide 01037 Total Cobalt
32730 Total Phenolics
34235 Benzene
81551 Xylene
00400 pH 00745 Total Sulfide 01042 Copper
34481 Toluene
00530 Total Suspended 00927 Total Magnesium
38260 MBAS
Residue 00929 Total Sodium 01045 Iron
39516 PCB's
00545 Settleable Matter 00940 Total Chloride 01051 Lead
50050 Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581
The monthly average for fecal coliform is to be reported as a GEOMETRIC
or 534
mean.
facility's permit for reporting data
Use only units designated
in the reporting
ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
* If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A
NCAC 2B
(b) (2) (D)
.0506
DEQ-CFW 00060446

'+ , r
NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: September YEAR: 2013
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft below Prospect Hall Landing
UPSTREAM DOWNSTREAM
•
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®mm
MMMMMM®®
MMEM
DWQ Form MR-3 (Revised 7/2000)
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00310
00610 1
00530
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HRS
°C
units
mg/L
mg/L
#/100ml
µmho/cm
_1
2
3
4,
5..
6
• 7..
8
,9
10
11
12
14
15
16
17-.
18
19
-
20
21
22
23
24
26
27
28
29'
30
31
.;_.
Average
Maximum
Minimum
DEQ-CFW 00060447

I , R
Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements 0
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
22828 NC Hwy 87 W
Permittee Address
Ellis H. McGaughy - P
PeAittee (Please print
28306-7332 [phone]
Number
Date
October 31, 2016
Permit
PARAMETER CODES
00010 Temperature 00556 Oil & Grease 00951 Total Fluoride 01067 Nickel 50060 Total
00076 Turbidity 00600 Total Nitrogen 01002 Total Arsenic 01077 Silver Residual
00080
Color (Pt -Co)
00610
Ammonia Nitrogen
01092 Zinc
Chlorine
00082
Color (ADMI)
00625
Total Kjeldhal
01027
Cadmium
01105 Aluminum
Nitrogen
00095
Conductivity
00630
Nitrates/Nitrites
01032
Hexavalent Chromium
01147 Total Selenium
71880 Formaldehyde
00300
Dissolved Oxygen
01034
Chromium
31616 Fecal Coliform
71900 Mercury
00310
BOD5
00665
Total Phosphorous
32730 Total Phenolics
81551 Xylene
00340
COD
00720
Cyanide
01037
Total Cobalt
34235 Benzene
00400
pH
00745
Total Sulfide
01042
Copper
34481 Toluene
00530
Total Suspended
00927
Total Magnesium
38260 MBAS
Residue
00929
Total Sodium
01045
Iron
39516 PCB's
00545
Settleable Matter
00940
Total Chloride
01051
Lead
50050 Flow
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506
(b) (2) (D)
DEQ-CFW 00060448