DEQ-CFW_00060325

JAN 21 2015 -r
�Gyvi�C;;io;21 C3n1.3 EFFLUENT JAN UNTH 20i5NPDES PERMIT NO. NC0003673 DISCHARGE NO. 001 November YEAR 2014
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY
mm,
DENR JAN 9 2
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
(SIGNATt1RE OF OPERATOR IN RESPONSIBLE CHARGE)
BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
..-)%-
DATE
Oa
o
a=oN
I
C
c
d
O
V
p
FLOW
y
'
U
~
aL
N
G
m
c
z
MW
K
O
a
0:
°6
O
XIx
w
WaWJ
W
=
W
W
XW
W
=
F
O
IL
IL
Q
~O
~
zYP
Q
~
z
Nv,
la-
O
EFF X
jWW
Q~
C R
HRS
HRS
YIN
MGD
*C
UNITS
Lb/Day
Lb/Day
mg/L
ug/L
Lb/Day
Lb/Day
Lb/Day
Lb/Day
LbMay
1,
osoo
_
-,24
1.203
_
.,, .
..
.3,E
...
2
osoo
24
1.232
3,;
osoo
7,24
YN
1 115
; x23 �,
e7:3
,. 381 3,
<387 8
,
x;
4
osoo
24
Y
0.996
22
7.4
127.1
108.0
5:'
osoo
241
!Y:`
.0:497
21
7;3:
39 81
A57.5
6
osoo
24
Y
0.912
TD.A:M
7
osoo
y 24
yY :0.730t
.
:t
m 3K
1 .
-
.�
8
osoo
24
1.037
9
0800
` 24
40 820.
}0.769
r
. ,
_
x
_
10
0800
24
BG
20
8.0
<12.8
36.9
11
0800
24
$ ,
` o0 966 _
219.-
12
osoo
24
Y
1.113
20
8.0
<18.6
<46.4
13.
osoo
Za,
-ii,.
Y
1.021
._r} ... szn
ne-. ��3
e,.e..Q
a..:.BeM$'.
}�.. ,'Lf��-
14
0800
24
Y
1.012
15'
osoo
24
0.778:z_
�w
r�F
aan
s }
"r
r
%.�'
16
0800
24
0.898
17
osoo,'24
.
208
18
0800
24
Y
0.962
19
7.6
<16.0
28.9
19
osoo
, 24
Y _
_0 857
,.17 {
7 5.,
y20 7 �
,�25 7�
�:<4 5, e
;;x
�z
e
h
20
0800
24
Y
0.879
2119800
u24<
Y=:x
22
08001
24
0.999
23
.0800
_ `24
: {
1007 ,
_. _.
`344 3,
60.5
t
24
0800
24
Y
1.069 1
21
7.6
222.9
61.7
osoo
c_.
"24
,
21,
751Q1
925 9,
26
0800
24 1
Y
1.397
21
7.6
27
osoo
#241194fi.
3
28
0800
24
*
0.782
29
0800
:$ 24
30
0800
24
1.232
31 osoo
AVERAGE
r 24
0.980
{
16.
48.0
0
MAXIMUM
ii,MINIMUM
7
2
s
.4 7
17
7.3
<T 2.
72 -
<4.5
Comp.'(C);Grab '(G);'
_'
:`:G_
G,
. C .'
, C
G.
' G
_'.G
G
G. _
_G'.
G',
Monthly Limit
2.0
182.6
303.1
0.113
8.36
10.91
12.72
7.90
6-9
484.7
'981.5
0.5
20.85
'25.44'
29.96
19.65
DEM Form MR4 (12/93)
* Holiday
DEQ-CFW 00060325

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements L-J
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
i.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plan
Permittee (Please print or
I�
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
00010 Temperature
00076 Turbidity
00080 Color (Pt -Co)
00082 Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00556
00600
00610
00625
00630
PARAMETER CODES
Oil & Grease 00951 Total Fluoride
Total Nitrogen 01002 Total Arsenic
Ammonia Nitrogen
Total Kjeldhal
Nitrogen
Nitrates/Nitrites
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060326

EFFLUENT
NPDES PERMIT NO. NC0003673 DISCHARGE NO. 002 MONTH November YEAR 2014
FACILITY NAME DuPont - Fayetteville Works CLASS 3 COUNTY Bladen
OPERATOR IN RESPONSIBLE CHARGE (ORC) Jamie R. Lewis GRADE 4 PHONE [phone]
CERTIFIED LABORATORIES (1) TBL Laboratory (Lumberton) (2)
CHECK BOX IF ORC HAS CHANGED I� PERSON(S) COLLECTING SAMPLES Jamie R. Lewis / Arnold Ray Beard
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES
DIV. OF WATER QUALITY mow, X
DENR O (SIGNAT RE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER JAN 9 2015 BY THIS SIGNATURE, I CERTIFY THAT THE REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE
d
r=
d
to
FLOW
W
c
w
EFF X
W>
i=Y
o
o
d
d
�y
�
o
O
w
O0
6Q
0
'o
40
w
a
zi
Q
L
O
.ao
xo
X
«daN
E
w�W
U
U.Q
LLI
RE
=
F0
z
x 0�
co
~
c
O
a
o`
o
R
0
HRS
HRS
YIN
MGD
'C
UNITS
M91L
mglL
mglL
uglL
mglL
mg/L
P!F
1:
osoo
' 24
42Al2 .;
2
0800
24
1.124
3:
osoo
a24 ,
.` Yi
,1s385,
20
A6
4
o800
24
Y
1.166
20
6.6
5:
osoo
424,,
,vim.,
..
r � •r
6
0800
24
Y
1.279
20
6.8
7
osoo
`2a {.
'Y`
;101220
k
8
0800
24
1.112
9
080024
10
0800
24
B
2.088
18
7.6
11w
Osoo
24 x
B;
;2.862
12
0800
24
Y
3.015
19
7.8
13
osoo
'$24
Y _
2.978,
$19, g
V
14
0800
24
Y
3.414
18
6.9
15
1 osoo
;24,:4:
t00a
w
t s°-
16
0800
24
4.049
17
osoo
' 24r
Y ;
: 4.228
18
" 6.7
P.
18
0800
24
Y
3.876
1 16
6.6
<2.0
18.7
22.2
1.14
1.65
'
:Y1
;880..
.4._
}6:5
;:s
0031
20
0800
24
Y
4.698
14
6.6
21
osoo
24
Y
4 461
13
`--6.6
22
osoo
24 1
4.296
23
0600
':�24
:9.966
24
osoo
24
Y
10.435
17
6.9
25
osoo
.. 24>
; .Y _
; :8:596, .
. 17..;,
' 6.8 ..
"" : . _
N
26
osoo
24
Y
2.971
17
6.7
27:
0800
-'24,
* '
�2.501
2810800
24
*
3.350
29
'osoo.
24.,_
30
osoo
24 1
2.866
31 osoo
AVERAGE
.24
3.467
8
.7
2.
0.03
. 4
1.65
MAXIMUM
a ..
._ .:.
.4 T 5
8
<
7
2
4
5
YP
MINIMUM1.012
1
6.6
<2
18.7
22.2
0.03
.65
Comp. °(C)'Grab (6)G
=..
> G '
C
C
'G
;C
,C
C
Monthly Limit
'Daily Limit
6-9'
DEM Form MR -I (12193) *Holiday
DEQ-CFW 00060327

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements rX
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plant Majfjlager
Per ittee (Please print or typ
r '
z�
Signature of ermittee** C Date
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
00010
Temperature
00076
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00556
00600
00610
00625
00630
PARAMETER CODES
Oil & Grease 00951 Total Fluoride
Total Nitrogen 01002 Total Arsenic
Ammonia Nitrogen
Total Kjeldhal
Nitrogen
Nitrates/Nitrites
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance may be obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060328

A
Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 11/26/14
Facility: DUPONT FAYETTEVILLE WORKS NPDES#: NC0003573 Pipe#: 002 County: BLADEN
Laboratory Perf ming Test: MERITECH LABS, INC.
Comments:
X
signature o Opeuator in Response e Charge
S gnat re or Laboratory Supervisor * PASSED:-10.62% Reduction
Work Order: Environmental Sciences Branch
MAIL ORIGINAL TO: Div. of Water Quality
N.C. DENR
1621 Mail Service Center
Raleigh, North Carolina 27699-1621
forth Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
:ONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12
# Young Produced I,22I29`25`25I26I29I21I15I23,10I27I21
Adult (L)ive (D)ead IIL IL IL IL IL IL IL IL IL IL IL IL
9ffluent %: 3.3%
'REATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV
24.661%
# Young Produced 26 27 29 25126127 27 26 11 27 26 25 % control orgs
producing 3rd
brood
Adult (L) ive (D) ead L L L L L L L L L L L L 100
Chronic Test Results
Calculated t =
Tabular t =
% Reduction = -10.62
Mortality
Avg.Reprod.
0.00
22.75
Control
Control
0.00
25.17
Treatment 2
Treatment 2
PASS FAIL
X
Check One
1st sample 1st sample 2nd sample Complete This For Either Test
pH Test Start Date: 11/19/14
Control 8.14 8.03 8.09 8.05 8.16 8.15 Collection (Start) Date
Sample 1: 11/17/14 Sample 2: 11/19/14
Treatment 2 8.19 7.97 8.08 8.07 8.16 6.35 Sample Type/Duration 2nd
1st P/F
s s s Grab Comp. Duration D
t e t e t e I S S
a n a n a n Sample 1 X 24.0 hrs L A A
r d r d r d U M M
t t t Sample 2 X 24.0 hrs T P P
1st sample 1st sample 2nd sample
D.O. Hardness (mg/1) 48 ........ .........
Control 7.59 7.55 7.74 7.55 7.26 7.55
Spec. Cond.(umhos) 168 427 257
Treatment 2 7.48 7.56 7.94 7.55 7.54 7.58
Chlorine (mg/1) ........ < 0 . 1 <0 . 1
LC50/Acute Toxicity Test Sample temp. at receipt (°C) ,,...... 0.2 0.4
(Mortality expressed as %, combining replicates)
%
%
o
%
%
o
%
a
%
o
%
0
%
0
%
0
% 0
% 0
%
0
Note: Please
Concentration Coplete This
rSemction Also
Mortality
start/end start/end
JC50 = % Method of Determination
950-. Con i ence Limits Moving Average _ Probit
o -- o Spearman Karber _ Other
Control
High
f'nn r
PH
Organism Tested: Ceriodaphnia dubia Duration(hrs):
Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41)
li •
DEQ-CFW 00060329

NPDES NO: NC0003573 DISCHARGE NO: 002 MONTH: November YEAR: 2014
FACILITY: DuPont - Fayetteville Works COUNTY: Bladen
STREAM: Cape Fear River STREAM: Cape Fear River
LOCATION: DuPont River Pump Station LOCATION: Boat Ramp - 4500 ft belowProspectHall Landing
UPSTREAM DOWNSTREAM
•
DWCL Form MR-3 (Revised 7/2000)
00010
00400
00310
00610
00530
00094
0
(D
2
0
0)
CD
(D
0)
E (a
0
CD
0)
a)
V
a
CD
a)
2
- E
C)
C14
A
c\1
>1
0
'D
0 L)
()
a)
0-
ca
a)
E
C
0
CL
LO
0
a) 0
LL
0
E
a)
0
HIRS
*C
units
mg/L
mg/L
#/100MI
pmho/cm
2
4
6
7
8
10
11
A
12
13
14
16
T
18
�19
20
21,--
22
24
26
27'
28
30
31
Average
Makimu* m
Minimum
DEQ-CFW-00060330

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements �X
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements
Noncompliant
If the facility is noncompliant, please comment on corrective actions being taken in respect to equipment, operation,
maintenance, etc., and a time table for improvements to be made.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or
supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate
the information submitted. Based on my inquiry of the person or persons who manage the system, or those
persons directly responsible for gathering the information, the information is, to the best of my knowledge and belief,
true, accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Ellis H. McGaughy - Plant
Per ittee (Please print or 1
Aa 'M rm r
ature of
1 Z I: -10H
22828 NC Hwy 87 W, Fayetteville, NC, 28306-7332 [phone] October 31, 2016
Permittee Address Phone Number Permit Exp. Date
00010
Temperature
00076
Turbidity
00080
Color (Pt -Co)
00082
Color (ADMI)
00095 Conductivity
00300 Dissolved Oxygen
00310 BOD5
00340 COD
00400 pH
00530 Total Suspended
Residue
00545 Settleable Matter
00556
00600
00610
00625
00630
PARAMETER CODES
Oil & Grease 00951 Total Fluoride
Total Nitrogen 01002 Total Arsenic
Ammonia Nitrogen
Total Kjeldhal
Nitrogen
Nitrates/Nitrites
00665
Total Phosphorous
00720
Cyanide
00745
Total Sulfide
00927
Total Magnesium
00929
Total Sodium
00940
Total Chloride
01027 Cadmium
01032 Hexavalent Chromium
01034 Chromium
01037 Total Cobalt
01042 Copper
01045 Iron
01051 Lead
01067 Nickel
01077 Silver
01092 Zinc
01105 Aluminum
01147 Total Selenium
31616 Fecal Coliform
32730 Total Phenolics
34235 Benzene
34481 Toluene
38260 MBAS
39516 PCB's
50050 Flow
50060 Total
Residual
Chlorine
71880 Formaldehyde
71900 Mercury
81551 Xylene
Parameter Code assitance maybe obtained by calling the Water Quality Compliance Group at [phone], extension 581 or 534
The monthly average for fecal coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting
facility's permit for reporting data
* ORC must visit facility and document visitation of facility as required per 15A NCAC 8A .0202 (b) (5) (B).
** If signed by other than the premittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B .0506
(b) (2) (D)
DEQ-CFW 00060331