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HomeMy WebLinkAboutDEQ-CFW_00059889E1rar%er, Jim From: Michael E Johnson [Michael.E.Johnson@USA.dupont.com] Sent: Friday, July 16, 2010 12:38 PM To: Barber, Jim Cc: Hardee, Ed Subject: Re: Residuals land application forms Attachments: DuPont Fayetteville Sediments Results.pdf Jim Thank you for calling me today and discussing DuPont's options to remove the river water sediment from our basin and placing it in our on -site Borrow Area. Per your request, attached are the analytical results for the required seven samples of the sediment. All analyses were done by the Compuchem lab in Cary. The one outstanding analyte is the PFOA result that NC-DWM is especially interested in, as this analysis is performed at another lab. I will work to get that result ASAP, but it will no doubt be at less than 1 ppb levels. You will see that Sample 01 was run as a duplicate, and Samples 02 through 07 were all run as single analyses. I also color coded the table for my own use. The cells that are not colored were "non -detectable" or "less than MDL". The cells colored blue had positive measurable concentrations of the analyte. The cells colored yellow had laboratory qualifiers on them, for which "J" means the result was estimated due to a data quality issue and the result was less than the PQL, and a "B" qualifier means that contamination was seen in either the trip blank, equipment blank or method blank. Mike Michael E. Johnson Environmental Manager DuPont Company Fayetteville Works (910) 678-1155 (See attached file: DuPont Fayetteville Sediments Results.pdf) This communication is for use by the intended recipient and contains information that may be Privileged, confidential or copyrighted under applicable law. If you are not the intended recipient, you are hereby formally notified that any use, copying or distribution of this e-mail, in whole or in part, is strictly prohibited. Please notify the sender by return e-mail and delete this e-mail from your system. Unless explicitly and conspicuously designated as "E-Contract Intended", this e-mail does not constitute a contract offer, a contract amendment, or an acceptance of a contract offer. This e-mail does not constitute a consent to the use of sender's contact information for direct marketing purposes or for transfers of data to third parties. Francais Deutsch Italiano Espanol Portugues Japanese Chinese Korean http://www.DuPont.com/corp/email disclaimer.html DEQ-CFW 00059889 Table _. Summary of Analytical Results Location NRW B-01I NRW B-01 NRW B-02 NRWSB-03 NRW B-04 NRW S-05 NRW -06 N WSB-07 Date 3/25/101 3/25/10 3/25/10 3/25/10 3/25/10 3/25/10 3/25/10 3/25/10 Top (ft) 01 0 0 0 0 0 0 0 LabName Method Group CAS No. Analyte TCLP Analytes Units Bottom (ft) Duplicate 01 DUP 0 FS 0 FS 0 FS 0 FS 0 FS 0 FS 0 FS COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM8260E 82608 82606 82606 8260E 82606 8260B 8260B 82609 A.VOC A.VOC A.VOC A.VOC A.VOC A.VOC A.VOC A.VOC A.VOC 75354 107062 71432 56235 1089 77 67663 78933 127184 79016 1,1-DICHLOROETHENE 1,2-DICHLOROETHANE BENZENE CARBON TETRACHL RIDE CHLOROBENZENE CHLOROFORM METHYL ETHYL KETONE TETRACHLOROETHYLENE TRICHLOROETHENE MG/L M /L MG/L MG/L MG/L MG/L MG/L MG/L MG/L <0.025 <0.025 <0.025 <0.025 <0.025 <0.02 <0.063 <0.025 0.0064J <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.025 <0.05 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.063 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0. 663 <0.025 cD.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.063 _ <0.025 <O.025 70.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.063 _ <0.025 <6.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <06363 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.063 <0.025 0.083 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.063 <0.025 <OA25 COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM GOMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM COMPUCHEM 8260E 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C 82700 8270C 8270C A.VOC A.VOC B.SVOC B.SVOC B.SVOC B.SVOC B.SVOC B.SVOC BSVOC B.SVOC B.SV C B.SVOC B.SVOC B.SVOC 75014 1064 77 95954 88062 121142 95487 108394 106445 118741 87683 67721 98953 87865 110861 VINYL CHLORIDE 1,4-DICHLOROBENZENE 2,4,5-TRICHLOROPHENOL 2,4,6-TRICHLOROPHENOL 2,4-DINITROTOLUENE 2-METHYLPHENOL (O-CRESOL) 3-METHYLPHENOL (M-CRESOL) 4-METHYLPHENOL (P-CRESOL) HEXACHLOROBENZENE HEXACHLOROBUTADIENE HEXACHLOROETHANE NITROBENZENE PENTACHLOROPHENOL PYRIDINE MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L MG/L <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.025 <0.05 <0.025 <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.025 <0.05 <0.025 <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.025 <0.05 <0.025 <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.025 <0.65 <0.025 <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.025 <0.05 <0.025 _ <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.025 <0.05 <0.025 <0.025 <0.025 <0.05 <0.05 <0.025 <0.05 <0.05 <0.05 <0.025 <0.025 <0.025 <0.0 - <0.05 <0.025 COMPUCHEM COMPUCHEM COMPUCHEM 8151A 6151A 8081 D.HERB D.HERB E.PEST 94757 93721 57749 2,4-DICHLOR_OPHENOXYACETIC ACID SILVEX CHLORDANE MG/L MG/L MG/L <0.025 <0.005 <6.0086 <0.025 <0.005 <0.008. 6 <0.025 <0.005 <0 086 <0.025 <0.005 <0.025 <0.005 <0.025 <0.005 <0.0086 <0.025 <0.005 <0.025 <o.DD5 <0.0086 <0.0086 <0.0086 <0.0086 COMPUCHEM 8081 E.PE$T 72208 ENDRIN MG/L <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 <0.001 COMPUCHEM 8081 E.PEST 76448 HEPTACHLOR MG/L <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 COMPUCHEM 8081 E.PEST 1024 773 HEPTACHLOR EPDX DE MG/L <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 COMPUCHEM 8081 E.PEST 58899 LINDANE M /L <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005 <0.0005P<�O 0005 COMPUCHEM 8081 E.PEST 72435 METHOXYCHLOR MG/L <0.005 <0.005 <0.005 <0.005 <0.005 <0.005 <0.005.005 COMPUCHEM 8081 E.PEST 8001 552 TOXAPHENE MG/L <0.025 <0.025 <0.025 <0.025 <0.025 <0.025 <0.025.025 Total Analytes 0.0176 B 0.0174 B 0.0179 B 0.0178 B 0.0182 B 0.0144 B 0.0158 B 0.0156 J 0.117 J 0.112 J 0.139 J 0.107 J 0.141 J 0.106 J 0.0898 J 0.116.1 <0.5 <0.5 <0.5 <0.5 0.00068 J <0.5 <0.5 I <0.5 0.0056 J 0.0041 J 0.0048 J 0.0068 J 0.0081 J 0.0076 J 0.0085 J 0.0066 J 0.0088 B 0.0135 J 0.0075 B 0.0095 B 0.02 J 0.0073 B 0.0057 B 0.0042 J <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 0.0169 B 0.0172 B 0.0197 B 0.0186 B 0.0178 B 0.0187 B 0.019 B 0.0182 J <0.5 <0.5 1 <0.5 1 <0.5 1 <0.5 1 <0.5 I <0.5 1 <0.5 1911 123 J 74.2 J 508 J 213 J 77.7 J 540 J 196 J 18500 J 19500 J 16800 J 119000 J 69400 J 16000 J 118000 J 41800 J 198 J 182 J 177 J 1120 J 520 J 153 J 11901 413 J 0.84 J 1.2 J 0.46 J 4.1 J 4.1 J 0.85 J 5.7 J 2.5 J 196 J 146 J 147 J 620 J 293 J 92.3 J 631 J 210 J 70.1 B 88.2 B 60.7 B 215 B 198 B 57.3 B 247 B 122 B 3 J 1.8 J 1.5 J 7.9 J 5.1 J 2.5 J 10.3 J 3 J 0.18 J 0.17 J 0.15 J 0.41 J 0.28 J 0.1 J 0.48 J 0.19 J 8;2 J 10.4 J 5.4 J 49.2 J 28.7 J 6.9 J 58.7 J 18.1 J 8.3 J 7.4 J 7.3 J 25.7 J 16.4 J 5.6 J 30 J 10.7 J 3.9 J 3.4 J 3.8 J 14.2 J 7.8 J 2.9 J 15.5 J 6.9 J 0.36 J 0.51 J 0.36 J 2.4 J 1.7 J 0.37 J 2.8 J 1 J 10.6 J 16.4 J 9.6 J 105 55 12.7 J 121 38.4 0.04 J <0.06 0.02 J 0.1 J 0.08 J <0.04 0.11 0.04 J <0.2 <0.2 4.2 <0.2 <0.2 <0.2 <0.2 <0.2 COMPUCHEM 6610B G.MET 7440382 ARSENIC MG COMPUCHEM 6010B G.MET 7440393 BARIUM M /L COMPUCHEM 601013 G.MET 7440439 CADMIUM MG/L COMPUCHEM 6010B G.MET 7440473 CHROMIUM MG/L COMPUCHEM 601 OB G.MET 7439921 LEAD MG/L COMPUCHEM 7470A IG.MET 7439976 MERCURY MG/L COMPUCHEM 6010B G.MET 7782492 SELENIUM MG/L COMPUCHEM 6010E G.MET 7440224 SILVER MG/L COMPUCHEM COMPUCHEM 6010B 6010E G.MET G.MET 7440702 7429905 CALCIUM ALUMINUM MG/KG MG/KG COMPUCHEM 6010E G.MET 7439954 MAGNESIUM MG/KG COMPUCHEM 60106 G.MET 7439987 MOLYBDENUM MG/KG COMPUCHEMI6010B G.MET 7440097 POTASSIUM MG/KG COMPUCHEM 6010B G.MET 7440235 SODIUM MG/KG COMPUCHEM 6020 G.MET 7440382 ARSENIC MG/KG COMPUCHEM 6020 G.MET 7440439 CADMIUM MG/KG COMPUCHEM 6020 G.MET 7440508 COPPER MG/KG COMPUCHEM 6020 G.MET 7439 221 LEA MG/KG COMPUCHEM 6020 G.MET 7440 220 NICKEL MG/KG COMPUCHEM 6020 G.MET -ET 7782492 SELENIUM MG/KG COMPUCHEM 6020 6. M 7440666 ZINC M /KG COMPUCHEM 7471 A G.MET 74399 MERCURY MG/KG COMPUCHEM 300 H.MISC 147976 7558 NITRATE MG/KG COMPUCHEM 300 H.MISC 14797650 NITRITE MG/KG <t <1 <1 <1 <t <1 <1 <1 Basin Sediments 3-10 crosstabs.xls:Sheeti < and ND = Non detect at stated reporting limit Page 1 of 2 7/16/2010: 12:04 PM Table _. Summary of Analytical Results Location NH W B-01 RW -01 NRW B-02 NRW B-03 NRW B-04 NRW B-05 NRWSB-06 NRW -07 Date 3/25/10 3/25/10 3/25/10 3125/10 3/25/10 3/25/10 3/25/10 3/25110 Top (ft) 0 0 0 0 0 0 0 0 a COMPU COMPUCHEM Method 350.1 Group H.MISC CAS No. 7664417 Analyte AMMONIA Units MG/KG Bottom (ft) Duplicate 0 DUP <0.1 1.61 J <5 <250 <250 5.31 >140 0.63 96 45.7 0 FS <0.1 4.16 J <5 <250 <250 5.11 >140 0.63 96 45.7 0 0 0 FS FS FS 1.17 1.16 0.62s 5.53 J 5.72 J 4.19 J <5 <5 __ <5 <250 _ <250 <250 <250 <250 <250 5.24 5.51 5 >140 >740 >140 0.37 0.97 0.5 33 440 60 78.3 29.8 57.9 0 FS c0.1 4.52 J <5 <250 <250 5.06 >740 0.52 65 55 0 FS <0.1 2.04 J <5 <250 <250 525 >t40 1.2 330 24.6 0 FS 1.3 3.45 J <5 <250 <250 5.09 >140 1.5 110 42.7 COMPUCHEM COMPUCHEM CO -MP UCHEM COMPUCHEM COMPUCHEM 351.2 H.MISC CO21 TOTAL KJELDAHL NITROGEN MG/KG 365.4 9014 9034 9040B H.MISC H.MISC H.MISC 7723140 EVS0029 EVS0030 PHOSPHORUS REACTIVE CYANIDE REACTIVE SULFIDE MG/KG MG/L MG/L H.MISC C0066 PH-CORROSIVITY PH UNITS COMPUCHEM1010 UNK EVS0009 FLASHPOINT DEGREESF MICROBAC MICROBAC 1682 9221E 2540 G UNK H MISC TMISC EVS0879 EVS0238 SALMONELLA FECAL COLIFORM _ PERCENT SCLIDS _ MPN/4G MPN/G - y MICROBAC 'SM MS0544 Basin Sediments 3-10 crosstabs.xls:Sheetl < and ND = Non detect at stated reporting limit Page 2 of 2 7/16/2010: 12:04 PM barber, Jim From: Michael E Johnson [Michael.E.Johnson@USA.dupont.com] Sent: Wednesday, July 14, 2010 2:41 PM To: Barber, Jim Cc: Hardee, Ed Subject: Re: Residuals land application forms Tim: At long last we have the needed analytical results for us to complete and submit the application form for the permit to allow DuPont to remove the Cape Fear River sediment from our in -ground basin and take it to our on -site Borrow Area. It has been long enough since you and Ed visited here, that I am fuzzy on the exact program that we need to be applying under. I think the correct program is the "Dedicated Residuals Land Application Program", but please confirm that I am correct. Thank you for your help. Mike Michael E. Johnson Environmental Manager DuPont Company Fayetteville Works (919) 679-1155 This communication is for use by the intended recipient and contains information that may be Privileged, confidential or copyrighted under applicable law. If you are not the intended recipient, you are hereby formally notified that any use, copying or distribution of this e-mail, in whole or in part, is strictly prohibited. Please notify the sender by return e-mail and delete this e-mail from your system. Unless explicitly and conspicuously designated as "E-Contract Intended", this e-mail does not constitute a contract offer, a contract amendment, or an acceptance of a contract offer. This e-mail does not constitute a consent to the use of sender's contact information for direct marketing purposes or for transfers of data to third parties. Francais Deutsch Italiano Espanol Portugues Japanese Chinese Korean http://www.DuPont.com/corp/email disclaimer.html 1 DEQ-CFW 00059892