DEQ-CFW_00059889

E1rar%er, Jim
From: Michael E Johnson [[e-mail]]
Sent: Friday, July 16, 2010 12:38 PM
To: Barber, Jim
Cc: Hardee, Ed
Subject: Re: Residuals land application forms
Attachments: DuPont Fayetteville Sediments Results.pdf
Jim
Thank you for calling me today and discussing DuPont's options to remove the river water sediment
from our basin and placing it in our on -site Borrow Area.
Per your request, attached are the analytical results for the required seven samples of the
sediment. All analyses were done by the Compuchem lab in Cary. The one outstanding analyte is the
PFOA result that NC-DWM is especially interested in, as this analysis is performed at another lab.
I will work to get that result ASAP, but it will no doubt be at less than 1 ppb levels.
You will see that Sample 01 was run as a duplicate, and Samples 02 through
07 were all run as single analyses.
I also color coded the table for my own use. The cells that are not colored were "non -detectable"
or "less than MDL". The cells colored blue had positive measurable concentrations of the analyte.
The cells colored yellow had laboratory qualifiers on them, for which "J" means the result was
estimated due to a data quality issue and the result was less than the PQL, and a "B" qualifier
means that contamination was seen in either the trip blank, equipment blank or method blank.
Mike
Michael E. Johnson
Environmental Manager
DuPont Company
Fayetteville Works
[phone]
(See attached file: DuPont Fayetteville Sediments Results.pdf)
This communication is for use by the intended recipient and contains information that may be
Privileged, confidential or copyrighted under applicable law. If you are not the intended
recipient, you are hereby formally notified that any use, copying or distribution of this e-mail,
in whole or in part, is strictly prohibited. Please notify the sender by return e-mail and delete
this e-mail from your system. Unless explicitly and conspicuously designated as "E-Contract
Intended", this e-mail does not constitute a contract offer, a contract amendment, or an acceptance
of a contract offer. This e-mail does not constitute a consent to the use of sender's contact
information for direct marketing purposes or for transfers of data to third parties.
Francais Deutsch Italiano Espanol Portugues Japanese Chinese Korean
http://www.DuPont.com/corp/email disclaimer.html
DEQ-CFW 00059889

Table _. Summary of Analytical Results
Location
NRW B-01I NRW B-01
NRW B-02
NRWSB-03
NRW B-04
NRW S-05
NRW -06
N WSB-07
Date
3/25/101
3/25/10
3/25/10
3/25/10
3/25/10
3/25/10
3/25/10
3/25/10
Top
(ft)
01
0
0
0
0
0
0
0
LabName
Method
Group
CAS No.
Analyte
TCLP Analytes
Units
Bottom (ft)
Duplicate
01
DUP
0
FS
0
FS
0
FS
0
FS
0
FS
0
FS
0
FS
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM8260E
82608
82606
82606
8260E
82606
8260B
8260B
82609
A.VOC
A.VOC
A.VOC
A.VOC
A.VOC
A.VOC
A.VOC
A.VOC
A.VOC
75354
107062
71432
56235
1089 77
67663
78933
127184
79016
1,1-DICHLOROETHENE
1,2-DICHLOROETHANE
BENZENE
CARBON TETRACHL RIDE
CHLOROBENZENE
CHLOROFORM
METHYL ETHYL KETONE
TETRACHLOROETHYLENE
TRICHLOROETHENE
MG/L
M /L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
<0.025
<0.025
<0.025
<0.025
<0.025
<0.02
<0.063
<0.025
0.0064J
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.025
<0.05
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.063
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0. 663
<0.025
cD.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.063
_ <0.025
<O.025
70.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.063
_ <0.025
<6.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<06363
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.063
<0.025
0.083
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.063
<0.025
<OA25
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
GOMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
COMPUCHEM
8260E
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
8270C
82700
8270C
8270C
A.VOC
A.VOC
B.SVOC
B.SVOC
B.SVOC
B.SVOC
B.SVOC
B.SVOC
BSVOC
B.SVOC
B.SV C
B.SVOC
B.SVOC
B.SVOC
75014
1064 77
95954
88062
121142
95487
108394
106445
118741
87683
67721
98953
87865
110861
VINYL CHLORIDE
1,4-DICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
2,4-DINITROTOLUENE
2-METHYLPHENOL (O-CRESOL)
3-METHYLPHENOL (M-CRESOL)
4-METHYLPHENOL (P-CRESOL)
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE
HEXACHLOROETHANE
NITROBENZENE
PENTACHLOROPHENOL
PYRIDINE
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
MG/L
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.025
<0.05
<0.025
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.025
<0.05
<0.025
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.025
<0.05
<0.025
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.025
<0.65
<0.025
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.025
<0.05
<0.025
_
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.025
<0.05
<0.025
<0.025
<0.025
<0.05
<0.05
<0.025
<0.05
<0.05
<0.05
<0.025
<0.025
<0.025
<0.0 -
<0.05
<0.025
COMPUCHEM
COMPUCHEM
COMPUCHEM
8151A
6151A
8081
D.HERB
D.HERB
E.PEST
94757
93721
57749
2,4-DICHLOR_OPHENOXYACETIC ACID
SILVEX
CHLORDANE
MG/L
MG/L
MG/L
<0.025
<0.005
<6.0086
<0.025
<0.005
<0.008.
6
<0.025
<0.005
<0 086
<0.025
<0.005
<0.025
<0.005
<0.025
<0.005
<0.0086
<0.025
<0.005
<0.025
<o.DD5
<0.0086
<0.0086
<0.0086
<0.0086
COMPUCHEM
8081
E.PE$T
72208
ENDRIN
MG/L
<0.001
<0.001
<0.001
<0.001
<0.001
<0.001
<0.001
<0.001
COMPUCHEM
8081
E.PEST
76448
HEPTACHLOR
MG/L
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
COMPUCHEM
8081
E.PEST
1024 773
HEPTACHLOR EPDX DE
MG/L
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
COMPUCHEM
8081
E.PEST
58899
LINDANE
M /L
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005
<0.0005P<�O
0005
COMPUCHEM
8081
E.PEST
72435
METHOXYCHLOR
MG/L
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005
<0.005.005
COMPUCHEM
8081
E.PEST
8001 552
TOXAPHENE
MG/L
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025
<0.025.025
Total Analytes
0.0176 B 0.0174 B 0.0179 B 0.0178 B 0.0182 B 0.0144 B 0.0158 B 0.0156 J
0.117 J 0.112 J 0.139 J 0.107 J 0.141 J 0.106 J 0.0898 J 0.116.1
<0.5 <0.5 <0.5 <0.5 0.00068 J <0.5 <0.5 I <0.5
0.0056 J 0.0041 J 0.0048 J 0.0068 J 0.0081 J 0.0076 J 0.0085 J 0.0066 J
0.0088 B 0.0135 J 0.0075 B 0.0095 B 0.02 J 0.0073 B 0.0057 B 0.0042 J
<0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1 <0.1
0.0169 B 0.0172 B 0.0197 B 0.0186 B 0.0178 B 0.0187 B 0.019 B 0.0182 J
<0.5 <0.5 1 <0.5 1 <0.5 1 <0.5 1 <0.5 I <0.5 1 <0.5
1911 123 J 74.2 J 508 J 213 J 77.7 J 540 J 196 J
18500 J 19500 J 16800 J 119000 J 69400 J 16000 J 118000 J 41800 J
198 J 182 J 177 J 1120 J 520 J 153 J 11901 413 J
0.84 J 1.2 J 0.46 J 4.1 J 4.1 J 0.85 J 5.7 J 2.5 J
196 J 146 J 147 J 620 J 293 J 92.3 J 631 J 210 J
70.1 B 88.2 B 60.7 B 215 B 198 B 57.3 B 247 B 122 B
3 J 1.8 J 1.5 J 7.9 J 5.1 J 2.5 J 10.3 J 3 J
0.18 J 0.17 J 0.15 J 0.41 J 0.28 J 0.1 J 0.48 J 0.19 J
8;2 J 10.4 J 5.4 J 49.2 J 28.7 J 6.9 J 58.7 J 18.1 J
8.3 J 7.4 J 7.3 J 25.7 J 16.4 J 5.6 J 30 J 10.7 J
3.9 J 3.4 J 3.8 J 14.2 J 7.8 J 2.9 J 15.5 J 6.9 J
0.36 J 0.51 J 0.36 J 2.4 J 1.7 J 0.37 J 2.8 J 1 J
10.6 J 16.4 J 9.6 J 105 55 12.7 J 121 38.4
0.04 J <0.06 0.02 J 0.1 J 0.08 J <0.04 0.11 0.04 J
<0.2 <0.2 4.2 <0.2 <0.2 <0.2 <0.2 <0.2
COMPUCHEM
6610B
G.MET
7440382
ARSENIC
MG
COMPUCHEM
6010B
G.MET
7440393
BARIUM
M /L
COMPUCHEM
601013
G.MET
7440439
CADMIUM
MG/L
COMPUCHEM
6010B
G.MET
7440473
CHROMIUM
MG/L
COMPUCHEM
601 OB
G.MET
7439921
LEAD
MG/L
COMPUCHEM
7470A
IG.MET
7439976
MERCURY
MG/L
COMPUCHEM
6010B
G.MET
7782492
SELENIUM
MG/L
COMPUCHEM
6010E
G.MET
7440224
SILVER
MG/L
COMPUCHEM
COMPUCHEM
6010B
6010E
G.MET
G.MET
7440702
7429905
CALCIUM
ALUMINUM
MG/KG
MG/KG
COMPUCHEM
6010E
G.MET
7439954
MAGNESIUM
MG/KG
COMPUCHEM
60106
G.MET
7439987
MOLYBDENUM
MG/KG
COMPUCHEMI6010B
G.MET
7440097
POTASSIUM
MG/KG
COMPUCHEM
6010B
G.MET
7440235
SODIUM
MG/KG
COMPUCHEM
6020
G.MET
7440382
ARSENIC
MG/KG
COMPUCHEM
6020
G.MET
7440439
CADMIUM
MG/KG
COMPUCHEM
6020
G.MET
7440508
COPPER
MG/KG
COMPUCHEM
6020
G.MET
7439 221
LEA
MG/KG
COMPUCHEM
6020
G.MET
7440 220
NICKEL
MG/KG
COMPUCHEM
6020
G.MET
-ET
7782492
SELENIUM
MG/KG
COMPUCHEM
6020
6. M
7440666
ZINC
M /KG
COMPUCHEM
7471 A
G.MET
74399
MERCURY
MG/KG
COMPUCHEM
300
H.MISC
147976 7558
NITRATE
MG/KG
COMPUCHEM
300
H.MISC
14797650
NITRITE
MG/KG
<t
<1
<1
<1
<t
<1
<1
<1
Basin Sediments 3-10 crosstabs.xls:Sheeti
< and ND = Non detect at stated reporting limit Page 1 of 2 7/16/2010: 12:04 PM

Table _. Summary of Analytical Results
Location
NH W B-01
RW -01
NRW B-02
NRW B-03
NRW B-04
NRW B-05
NRWSB-06
NRW -07
Date
3/25/10
3/25/10
3/25/10
3125/10
3/25/10
3/25/10
3/25/10
3/25110
Top (ft)
0
0
0
0
0
0
0
0
a
COMPU
COMPUCHEM
Method
350.1
Group
H.MISC
CAS No.
7664417
Analyte
AMMONIA
Units
MG/KG
Bottom (ft)
Duplicate
0
DUP
<0.1
1.61 J
<5
<250
<250
5.31
>140
0.63
96
45.7
0
FS
<0.1
4.16 J
<5
<250
<250
5.11
>140
0.63
96
45.7
0 0 0
FS FS FS
1.17 1.16 0.62s
5.53 J 5.72 J 4.19 J
<5 <5 __ <5
<250 _ <250 <250
<250 <250 <250
5.24 5.51 5
>140 >740 >140
0.37 0.97 0.5
33 440 60
78.3 29.8 57.9
0
FS
c0.1
4.52 J
<5
<250
<250
5.06
>740
0.52
65
55
0
FS
<0.1
2.04 J
<5
<250
<250
525
>t40
1.2
330
24.6
0
FS
1.3
3.45 J
<5
<250
<250
5.09
>140
1.5
110
42.7
COMPUCHEM
COMPUCHEM
CO -MP UCHEM
COMPUCHEM
COMPUCHEM
351.2
H.MISC
CO21
TOTAL KJELDAHL NITROGEN
MG/KG
365.4
9014
9034
9040B
H.MISC
H.MISC
H.MISC
7723140
EVS0029
EVS0030
PHOSPHORUS
REACTIVE CYANIDE
REACTIVE SULFIDE
MG/KG
MG/L
MG/L
H.MISC
C0066
PH-CORROSIVITY
PH UNITS
COMPUCHEM1010
UNK
EVS0009
FLASHPOINT
DEGREESF
MICROBAC
MICROBAC
1682
9221E
2540 G
UNK
H MISC
TMISC
EVS0879
EVS0238
SALMONELLA
FECAL COLIFORM _
PERCENT SCLIDS _
MPN/4G
MPN/G
-
y
MICROBAC 'SM
MS0544
Basin Sediments 3-10 crosstabs.xls:Sheetl
< and ND = Non detect at stated reporting limit Page 2 of 2 7/16/2010: 12:04 PM

barber, Jim
From:
Michael E Johnson [[e-mail]]
Sent:
Wednesday, July 14, 2010 2:41 PM
To:
Barber, Jim
Cc:
Hardee, Ed
Subject:
Re: Residuals land application forms
Tim:
At long last we have the needed analytical results for us to complete and submit the application
form for the permit to allow DuPont to remove the Cape Fear River sediment from our in -ground basin
and take it to our on -site Borrow Area.
It has been long enough since you and Ed visited here, that I am fuzzy on the exact program that we
need to be applying under.
I think the correct program is the "Dedicated Residuals Land Application Program", but please
confirm that I am correct.
Thank you for your help.
Mike
Michael E. Johnson
Environmental Manager
DuPont Company
Fayetteville Works
[phone]
This communication is for use by the intended recipient and contains information that may be
Privileged, confidential or copyrighted under applicable law. If you are not the intended
recipient, you are hereby formally notified that any use, copying or distribution of this e-mail,
in whole or in part, is strictly prohibited. Please notify the sender by return e-mail and delete
this e-mail from your system. Unless explicitly and conspicuously designated as "E-Contract
Intended", this e-mail does not constitute a contract offer, a contract amendment, or an acceptance
of a contract offer. This e-mail does not constitute a consent to the use of sender's contact
information for direct marketing purposes or for transfers of data to third parties.
Francais Deutsch Italiano Espanol Portugues Japanese Chinese Korean
http://www.DuPont.com/corp/email disclaimer.html
1
DEQ-CFW 00059892