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HomeMy WebLinkAboutDEQ-CFW_00025382Hazardous Waste Section File Room Document Transmittal Sheet Your Name: EPA ID: Facility Name: Document Group: Document Type: Description: Date of Doc: Author of Doc: OVA Darnell Mitchell N C D 0 4 7 3 6 8 6 4 2 E.I.DUPONT FAYETTEVILLE WORKS Groundwater (GW) Other (0) RCRA Phase I Report 8/18/2003 Corp. Remediation Grp. File Room Use Only Date Recieved by File Room: Date Scanned: Month Day Year NCD047368642 Scanner's Initi DEQ-CFW-00025382 RCRA PHASE I REPORT DUPONT FAYETTEVILLE, NORTH Preparedfor • - f � i M CORPORATEREMEDIATION GROUP An Alliance between DuPont• URS Diamond • �•wo*c e • • DEQ-CFW 00025383 0CDRPC:'RATE=- REMEEDIATICIN GRC-UP LOG OF BORING FTA-01 An Afftan - 5atwr— DUPOnt —1 UIRS lDtam®rj e32. Falrvaiw .—d NC 28210 (Page 1 of 1) Date Started 11114/02 "X* Coordinates : 11205.00 GREGG Drilling and Testing Date Completed :11/14/02 "NP"Coordinates :13246.00 106 Butternut Road Hole Diameter 2 inch Driller Anthony Martin Summerville, SC 29483 Location Fayetteville, NC Driller Number NC# 3169 Logged By Bryan Heath Depth in co U DESCRIPTION Feet (D 9 D 0 0— W.I. Gravel cover Medium to fine tan silty SAND SM E 1 CIL 'A. Well: FTA-01 Elev.: 147.20 PID PPM 25 DEQ-CFW-00025384 oplWELL CONSTRUCTION RECORD C North Carolina - Department off:nvironment and Natural Resources - Division of Water Quality - Groundwater Section NVELIXONTRACTOR (INDIVIDUAL) NAME (print)--,5-i�eo ,, 61 e�/�s.. CERTIFICATION#) YY NVEII, CONTRACTOR COMPANY NANIE 7,�6 PHONE # 0,13) LG-J-S-Yo ST,liTENVELL. CONSTRUCTION PERMIT# ASSOCIATED WQ PERMITH 61'applicable) (it'applicable) Wf--'LL USE (Check Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 Monitoring &-11ccovery 0 Heat Pump Water Injection 0 Other 0 If Other, List Use 2. WELL LOCATION: Nearest Town: County 8 leis (Street Name, Numbers, Community, Subdivision, Lot No., Zip Code) 3. OWNER: c'- E Address L-, e-5 71- (Simet or Route No.) /-'�,v e, We U " // r- City or 14own State Zip Code Area code- Phone number 4. DATFDRILLED 5. TOTAL DEPTI-L—La-�--- 6. DOES WELL REPLACE EXISTING WELL? YES 0 NO 7. STATIC WATER LEVEL Below Top of Casing: Zy FT. (Use ­+­ if Above Top of Casing) 8. TOP OF CASING IS FT. Above Land Surface* *Top of casing terminated at/or below land surrace requires a variance in accordance with 15A NCAC 2C.01 18. 9. YIELD (gpm): 3 METHOD OF TESTeo th 10. WATER ZONES (denth): /; fo d- I , 11. DISINFECTION: Type 12. CASING: Depth Diameter From 0 To Ft. k' From To I. t. From To Ft. Topographic/Land setting 0 Ridge 0 Slope 0 Valley &-ftaT-- (check appropriate box) Latitude/longitude of well location (degrees/minutes/seconds) Latitude/longitude source:O GPSO Topographic map (check box) DEPTH DRILLING LOG From To Formation Description 0 r LOCATION SKETC14 Amount Show direction and distance in miles from at least Wall Thickness two State Roads or County Roads. Include the road or Weight/Ft. Material numbers and comm n roa nam7?. 1�1s' , 70 1 - *f Uri e- 13. GROUT: Depth Material Method From To From To Ft. 14. SCREEN: Depth Diameter From_( ;L To_a_,I,,- Ft. 9 0 in. From To Ft. in. 15. SAND/GRAVEL PACK: Depth Size From d.2 To--Lo I. t. From To FL — Slot Size Material 16 in. S.5, in. Material MWIM 821 0 L) ej 4 6 e cLy e v. I DO I I ER F 13Y CERTIFY TI IATTI-1 IS WE Lt. WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C. WELL CON STR f-jun ON STANDARDS. AND °TI IAT A COPY OF THIS IS RECORD I IAS BEEN PROVI D ED TO THE WELL OWNER W STORE OF PERSON CONSTRUCTING TI I E WELL DATE Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, NC 27699-1636 Phone No. (919) 733-3221, within 30 days. GW-I REV. 07/2001 DEQ-CFW-00025385 DEQ-CFW 00025386 U AELL CONSTRUCTION RECORD North Carolina - Department ol'Environment and Natural Resources - Division of Water Quality - Groundwater Section A90ACIIJ CERTIFICATION #�Sl PHONE N (69)6S�2-3KJ3 M ELL CONTRACTOR COMPANYNANIE 6 t esc, .-IX ASSOCIATED WQ PERNIIT# (it'applicable) (if applicable) 111111111111111IM11111 WELL USE (Chell� Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 Monitoring Recovery 0 1 leat Pump Water injection 0 Other 0 1 f0ther. List Use 2. WELL LOCATIONJ5C.,ye V14stiale- Nearest Town: k07EV-1-#r-- County d C u-_d- e. n 87 (Street Name, Numbers, Community, Subdivision, Lot No., Zip Code) . S#eo,-Ile. Address C- 87 47 (Street or Route No.) j=�•ti 10I, CL"t l& &JO/ A's City 41 own Slate Zip Code (76qY-)- ICA - 6 � 3 3 Area code- Phone number 4. DATE DRILLED 5. TOTAL DEPTH: as 6. DOES Wl--'I,I, REPLACE T EXISING WELL? YES 0 NO Fr' 7. STATIC WATER LEVEL Below Top of Casing: / Y FT. (Use -+" if Above Top of Casing) 8. TOP OFCASING IS FT. Above Land Surl'ace* *Top of casing terminated at/or below land surface requires a variance in accordance with 15A NCAC 2C.01 18. 9. YIELD (gpm): 3 METHOD OF TEsTjyy,V,, 10. WATER ZONES (denth): I a itu ;k/ 11. DISINFI:C'I'ION:'I-)-pe____,___.___— Amount 12. CASING: Wall Thickness Depth Diameter or Weight/Ft. From , 1 0 /; I"t. 21, From 1 0— Ft.— From 1 0— Ft.— 13. GROUT- Depth Material From To Ft. Ceyhen-1- From "To Ft. ICI. SCREEN: Depth Diameter From To ;,% From To Ft. in. 15. SAND/GRAVEL PACK: Depth Size From To /0 Ft. W,�L From To Ft. Topographic/Land setting 1 0 Ridge 0 Slope 0 Valley 1--a—t (check appropriate box) Latitude/longitude of well location (degrees/minutes/seconds) Latitude/longitude source:O GPSO Topographic map (check box) DEPTH DRILLING LOG From To Formation Descriptign cod Lsft� J- PU kk Z r_- lemaA 6)144 wwe,' ---- --------- LOCATION SKETCH Show direction and distance in miles from at least two State Roads or County Roads. Include the road Material numbers anHcom n!!Ines. web T Slot Size Material 1 in. in. Material 87 U I DO I IFREBY CERTIFY THATTHIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C. WELL CONSTRUCTION STANDARDS. AND Ti [AT A COPY OF THIS RECORD I IAS BEEN PROVIDED TO THE WELL OWNER SI(XATURF OF PERSON CONSTRUCTINGTI IF WELL 1H Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, NC 27699-1636 Phone No. (919) 733-322 1, within 30 days. GW-1 REV. 07/2001 DEQ-CFW-00025387 011(mix? -qc>- CCDRPCDIRATE REMEDIATIC)N OF?CDUP LOG OF BORING FTA-03 An At b-twa®� DuPont and IJF?S IWrno—f --.1- .—. Ch1111tt- NC 28210 (Page 1 of 1) Date Started :11/13/02 "X" Coordinates : 9948.00 GREGG Drilling and Testing Date Completed :11113/02 "Y" Coordinates :12597.00 106 Butternut Road Hole Diameter 2 inch Driller Anthony Martin Summerville, SC 29483 Location Fayetteville, NC Driller Number NC# 3169 Logged By Bryan Heath Depth in 0 DESCRIPTION Feet co 0—•Gravel caner I Medium grained tan clayey SAND RE R Red slightly clayey, silty SAND "I SM 10 Laminated grey CLAY CL SW Fine grained pinkish SAND Fins grained greyish white SAND - SW 15— Medium grained yellow SAND SW 20— I CL K Z Z J Dary arey/black clay. with lignite fragments 903MM 7�0 Go mo §M DEQ-CFW-00025388 WELL CONSTRUCTION RECORD COIPA North Carolina - Department ol'Environment and Natural Resources - Division ol'Water Quality - Groundwater Section NVE Ll. CONTRACTNOR (IDIVI III JAL) NA NI E (print) Sieult 'A CERTIFICATION ad* Ykrl `®'ELL CONTRACTOR CONIPANYNANIL 6) 11110 N E H (&b 6V STATF WELL CONSTRUCTION PERMIT# --3 ASSOCIATED WQ PERNIIT# 61'applicable) (ifapplicable) WI-11. USE (Check Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 Nloniloring�tecovery 0 11 cat Pump Water Injection 0 Other IfOtherAistUsc WFLI. LOCATION: Nearest Town: E,-'1--1&TPi(,-LLX--CountY (Street Name, Numbers, Community, Subdivision, Lot No., Zip Code) 3. OWNER: k1 Add li� F 2, L�, (Street or Route No.)- -? - City or Town Slate Zip Code Area code- Phone number 4. DATE DRI LI.ED 6 ;L, 5. TOTAL, DEPTH: I % f 6. DOES WEI.I. REI"I,ACF EXISTING WEE? YES 0 W110 7. STATIC WATER I.EVEL Below Top of Casing: ZV' FT. 41 (Use "+" if Above Top of Casing) 8. TOP OF CASING IS 3 FT. Above Land Surface* *Top of casing terminated at/or below land surface requires a variance in accordance with 15A NCAC 2C.01 18. 9. YIEI.D(gpm): J METHOD OF TESTAW, IO.WA,ri,,izZONES(depili):--/d -ILO 11. DISINFECTION: Type 12. CASING: Amount Wall Thickness Depth Diameter orWeight/Ft. Material numbers From I , 0 Ft. I From , I , 0— FL — From TO Ft. 13. GROUT: Depth Material From --B— To 0 Ft. (c 14 e H FromToFt. Method ,A) u r 14. SCREEN: Depth Diameter Slot Size Material From 1 To I Ft.�in. in. S. From To Ft. in. in. 15. SAND/GRAVEL PACK: Depth Size Material From 17t. From To FL — Topographic/Land setting 0 Ridge 0 Slope 0 Valley _qYlat (check appropriate box) Latitude/longitude of well location (degrees/minutes/seconds) Latitude/longitude source:O GPSO Topographic map (check box) DEPTH DRILLING LOG From To Formation Description 8 - - _-mac ZL SDK 4A 1*11-4 Al C/c&",n .3 4)"4 tr t LOCATION SKETCH Show direction and distance in miles from at least two State Roads or County Roads. Include the road I com n rornames. I DO WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C. WELL ('ONSTRI, JUHON STANDARDS. AND T1 IA'r A COPY OF THIS RECORD I IAS BFEN PROVIDED TO THE WELL OWNER SJOATURE01- PERSON CONSTRUCTING TI IF WELL DA' Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC 27699-1636 Phone No. (919) 733-322 1, within 30 days. GW-I REV. 07/2001 DEQ-CFW-00025389 <2 __rfl-9t) -C*>- O-ORPCDRATE= FREMEEDIATIC-N GROUP LOG OF BORING NAF-01 An A111.-- b®t— DuPont UFZS C>'—w:f F.-- R—d NC �210 (Page 1 of 1) Date Started :12/04/02 "X" Coordinates :11050.00 GREGG Drilling and Testing Date Completed :12104/02 "Y" Coordinates :13010.00 106 Butternut Road Hole Diameter 2 Inch Driller Anthony Martin Summerville, SC 29483 Location Fayetteville, NC Driller Number NC# 3169 Logged By Bryan Heath Depth CL In DESCRIPTION Feet 0 - 1 0 w "I Well: NAF-01 Elev.: 146.61 Riser Bentonite Seal Sand Screen DEQ-CFW-00025390 C(01PV WELL CONSTRUCTION RECORD From S To .0 Ft. From To Ft. From To Ft.- 13. GROUT°: Depth Material From To 9, Q FL From To Ft. 14. SCREEN: Depth Diameter Slot Size From To_j_�- FL- P.- in. -Q& in. From To Ft. in. in. 15. SAND/GRAVEL PACK: Depth Size Material From To 1 5. 0 Ft. From To Ft.- 16. REMARKS: North Carolina - Department ol'Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRA(7011 (INDIVIDUALW' CERTIFICATION ) NAME (print) Lf�\r, y�,l "'EI.I.CON,rR..'L(-rORCOMPANY NANIE e,6-4--J\a _PRONE N J STATE WELL CONSTRUCTION PERNIIT# ASSOCIATED WQ PERAIIT# (il"applicable) (ifapplicabie) WI:Ll. lisl: (Check Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 Monitoring IY Recover), 0 Heat Pump Water Injection 0 Other 0 If Other. List Use 2. WELL LOCATION: Nearest Cou nty (Street Name. Numbers, Community Subdivision, Lot No., Zip Code) 3. OWNER: —DIAODA-- C V, CT Address (L)��Jq Lw"i-ow (Street or Rome No.) Cka,-LiLe- lycl- aA91D ity or Town Sr to Zip Code Area =�Pbone number 4. DATE DRILLED 5. TOTAL DEPTH: 6. DOES WELL REPLACE EXISTING WELL? YES 0 NO 7. STATIC WATER LEVEL Below Top of Casing: -7. V5 FT. (Use -+- if Above Top of Casing) 8. TOP OF CASING IS 0 FT. Above Land Surface* *Top of casing terminated at/or below land surface rcquirts a variance in accordance with 15A NCAC 2C.01 I& 9. YIELD (gpm): _ METHOD OF TEST 10. WATER ZONES (depth): 11. DISINFECTION: Type Amount 12. CASING: Wall Thickness , I Depth Diameter or Weight,/Ft. Material Material 5 Topographic/Land setting 0 Ridge 0 Slope 0 Valley 0 Flat (check appropriate box) Latitude/longitude of well location (degrees/minutes/seconds) (check box) DEPTH DRILLING LOG From To Formation Description c)— (7 LOCATION SKETCH Show direction and distance in miles from at least two State Roads or County Roads. Include the road numbers and common road names. I DO 11FREBY C]"RTIFYTHATTnis WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND Tim A COPY OF THIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER. SIGNATUA OF PERSON CONSTRUCTING THE WELL Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC 27699-1636 Phone No. (919) 733-322 1, within 30 days. GW-1 REV. 07/2001 A- DEQ-CFW-00025391 DEQ-CFW 00025392 kiW�� U��k--' � ( `'WELL CONSTRUCTION RECORD ~ °--� u u � North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRACI'OR (INDIVIDUAL) NAME (print �J Al r CERTIFICATION WE'LL USE icub|cBox):Residential O K1unicipuKPub|icO Industrial Agricultural Mon — Recover), 0 Heat pump Water lr�jcction 0 OtherD If'Other.ListUse 2WELL . /" (Sirect Name, Numbers, Community, Subdivision, Lot No_ Zip Code) , County Address Aa2d��� ay or Town State Zip Code Area code- Phone number 4. DATE DRILLED 5. TOTAL DEPTH- / 6. DOES WELL RCPLAC|CXlS11WELL? YES D NO ~ ?. STATIC WATER LEVEL Below Top uyCasing: '1 -[�,VFT. (use-+^iAbove Top ofmung) 8. TOP UFCASING IS |/�_ PT. Above Land Surface" *Top "fcasing terminated at/or below land surface requires u variance maccordance with /5Awcac2c.u/18. 9. YIRL.D(8pm):METHOD UPTEST 11.D|S|NHEC7|(�4:?y Amuuo________� 12.CA8|NG: Wall Thickness Depth Diameter or Weight/Ft. Material From 0 To �_C? I. L4�—� From 1\!_____|l______ Pmm1lL____F/`— ______ _______ }]. GROUT: Depth k4mcriu| [NoUmd From 10Tu_QF/ From ToFt. 14. 8CRCCN: Depth Diameter From n. From To___Ft.—__in. \5.3AND/GR&VELPACK: Depth Size From [La,�. From Pc16. REMARKS. ______ Slot Size Material -- //D.in. 15J__ _______' Material Topographic/Land setting ORidge OSlope OVukJ OFlat (check appropriate box) Latitude/longitude ufwell location Latitude/longitude mourcr:OQPGOTopographic map (check box) DEPTH DRILLING LOG From To Formation Description 'Okir Orin LOCATION SKETCH Show direction and distance inmiles from atleast two State Roads orCounty Roads. Include the mud numbers and common road names. |D0UFR[UYCEKl FYTlkQ'TH|SYY[LiV/^SCON3?KUCT[D|NxCCOKDaNCCVV[rH|5ANCAC2C,WCLL CONSTRUCTION sTANDARDS. AND THATA COPY OFTHIS RECORD HAS BEEN PROVIDED TO THE WELL OWNER SIGNATURE PERSON C0NSTKUCT!N011{EWELL 0-0 IPA Submit the original mthe Division u[Water Quality, Groundwater Section, 1636Mail Service Center - Raleigh, NC DEQ-CFW 00025394 From + 3, 0 To 5. 0 Ft. 4 From To— Ft. From To Ft.- 13. GROUT: Depth Material From D To r9,0 Ft. From To Ft. 14. SCREEN: Depth Diameter Slot Size From 5.o To_L15 :1) Ft. ;), in. .010 in. From To Ft. in. in. 15. SAND/GRAVEL PACK L, Depth Size Material From '0 -1-0-1!5 From To Ft.- 16. REMARKS: �6 WELL CONSTRUCTION' RECORD North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTR;%(-I'OR (INDIVIDUAL) NAME (print)A IrN AQ)aj k6� r h',C� CERTIFICATION WELL CONTRA(-roR COMPANY NAME G re qj -Te- 6-h in —PIIONE # 6113) `632:99/9 J STATE WELL CONSTRII(-FION PERMITN ASSOCIATED WQ PERMIT# (il'applicable) --- (if applicable) wn'l. uSI7 ( 5beck Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 Monitoring k Recovery 0 Heat Pump Water Injection 0 Other IrOther.List Use 2. WELL LOCAT19NZ: . Nearest To®e-- County e/A (Street Name, Numbers, Community, Subdivision, Lot No., Zip Code) 3. OWNER: n p ek +- C AG Address (1515(4 jEarvj:62� izi-,B (Street or Route No.) City, or Town State Zip Code )- — Area code- Phone number 4. DATE DRILLED__L-�- L-1 - 0,;, 5. TOTAL DEPTH: I 6. DOES WELL REPLACE EXISTING WELL? YES 0 NO 13/ 7. STATIC WATER LEVEL Below Top of Casing: 11.97-_- FT. (Use "+" if Above Top of Casing) 8. TOP OF CASING IS FT. Above Land Surface* *Top of casing terminated at/or below land surface requires a variance in accordance with 15A NCAC 2C.01 18. 9. Y I ELD (gpm): _ METHOD OF TEST 10. WATER ZONES (depth): 11. DISINFECTION:Type Amount 12. CASING: Wall Thickness Depth Diameter or Weight/Ft. Material Method Material 55 Topographic/Land setting I Ridge 0 Slope 0 Valley 0 Flat (check appropriate box) Latitude/longitude of well location (degrees/minutes/seconds) Latitude/longitude source:0 GPSO Topographic map (check box) DEPTH DRILLING LOG From To Formation Descr tion . ....... . ....... LOCATION SKETCH Show direction and distance in miles from at least two State Roads or County Roads. Include the road numbers and common road names. I DO 11FREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS RECORD I [AS BEEN PROVIDED TO THE WELL OWNER fm om SIGNATUAEOF PERSON CONSTRUCTING ]'HE WELL DATE Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Raleigh, NC 27699-1636 Phone Nu. (919) 733-322 1, within 30 days. GW- I REV. 07/2001 DEQ-CFW-00025395 WELL CONSTRUCTION RECORD North Carolina - Department ot'Environment and Natural Resources - Division of'Water Quality - Groundwater Section WELL CONTRAC, ['OR (INDIVIDUAL)NAME (print) VJ - Mar-�A_ CERTIFICATION# WELL CONTRACTOR COMPANY NAME G T5� �Ih, LO WELL USE (Check Applicable 8um):Residential O K4unioipuKPub|icO Industrial Agricultural Monitoring V Recovery O feat Pump Water |nJrndonO Othu O Il'Other.ListUse 2. WELL LOC&T (Street Name. Numbers, Community Subdivision, Lot No., Zip Code) l0W#GR (Street or Route No.) City or Town State Zip Code Area code- Phone number 5TOTAL ~� 6. DOES WELL REPLACE EXISTING WELL? YES NO 7.S[xT1CWATER LEVEL Below Top ofCusi Above Top ofCasing) O.TOP 0FCASING |S°L�1�_FT. 6buveLand Surface* *Top ureasing terminated ^murbelow land surface requires ^ variance /naccordance with /axmouCzc.o//m 9. YIELD (&pm):METHOD OFTEST |O. WATER I0NC3(drpth): ||. DISINFECTION: Type Ammunt_________ 12. CASING: Wall Thickness Depth Dimnmz, *,w6ight/R. /Nmuhal From l Ft. — From To- Ft, From To- Ft.______ |]. GROUT: Depth K4umrio| Method From 0lo__�,^0 F/ |� ,omTv_____�/ ' 14. SCREEN: Ucy/h Diameter Slot Size Material From To jti.n Ptin. ])WQ in. From 7o_____Pt._in. in. |j. 8AND/GRAVELP&CK: Depth Size K4m^,iu{ !'mm_�LQ_yo_/5L0_1�t`C_-�,�_ From To Pt. Topographic/Land settio 0 Ridge 0 Slope 0 Valley 0 Flat (check appropriate box) Latitude/longitude of well location Latitude/longitude sourcc:O GPSO Topographic map (check box) DEPTH DRILLING LOG From To Formation Description LOCATION SKETCH Show direction unddistanoeinni|cs from mileast two State Roads mCounty Roads. Include the road numbers and common road names. /D0||[0FBYCE0lFYTHK[TH|SWELL WAS CONSTRUCTED |MACCORDANCE WITH |5A NCACDC,WELL 00NKTKU(-[0NSlAN&4KDS. ANDn IAT 8COPY OPT1U8RECORD | [AS BEEN PROVIDED T0THCVY iL0VVNEK / | J� »\ )^/t�-//1-7 5((;N0nRF,bF IYEKSONCONSTRVc,rlN(Jll|EWELL DA Submit the original tuthe Division uf Water Quality, Groundwater Section, /636Mail Service Cenuwr-Rwleigk NC ]76ov-\636Phone No. (Y1o)7JJ-3%2l,within 3Udays. GVY-|REV. U7/2OO| , DEQ-CFW 00025397 DEQ-CFW 00025398 DEQ-CFW 00025399 04/14/2003 13: 50 GREGG SUMMERVILLE PAGE 02' WELL CONSTRUCTION RECORD2- North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELLCONTRACTOR (INDIVIDUAL) NAME (print CERTIFICATION JI—RU WELL CONTRACTOR COMPANY NAME Gregg Drilling & Testing, Inc. PHONE N (84? 832-491R STATE WELL CONSTRUCTION rERMITW ASSOCIATED WQ PERMITO (ifapplicable) (ifapplicable) WELL USE (Check Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 Monitoring 1K Recovery 13 Heat Pump Water Injection 13 Other if Other, List Use 2. WELL LOCATION: Nearest Town:_ Fayetteville county Bl aden 87 West (Street Name. Numbers, Community, Subdivision, Lot No., Zip Code) 3. OWNER: DuPont--CRG, Address -63-24 Fairview Road - ------------ (street or ittovie NO.) Charlotte, NC "28210 City or Town stow Zip Code (704)- 362-6633 Area code- Phone ukunbcr 4. DATE DRJLLED..---5/j33 6L 5, TOTAL r i 7 6. DOES WELL REPLACE EXISTING WELL? YES 0 NO Re 7. STATIC WATER LEVEL Below Top of Casing. q FT. (Use -+" if Above Top of Casing) 8. TOP OF CASING IS FT- Above Land Surface* *Top oresising lenninaftv! sitlor below lend surface requires a variance in accordance with ISA NCAC 2C.01 I& 9. Y I ELD (gpm): _ METHOD OF TEST 10. WATER ZONES (depth): — -------- It, DISINFECTION: Type_ Amount 12. CASING: Wall Thickness 0 Depth Diameter or Weight/Ft. Material From To 462!-1 &h-40 wc� FromFt— From 13. GROUT: From--0— Depth Material Method TZM— Ftj/, Jlt�/ �' ^UA— From To Ft 14, SCREEN- Dopth Dial"oter Slot Size Material From To 20s' Ft,_jqLin. -010 From To 15. SAND/GRA .X—CK. Depth Size Material From To 20 Ft. From To-- ft. Topographic/Land setting 0 Widge 0 Slope 0 Valley 0 Flat (check appropriate box) Latitude/longitude of well location I - (dcgmcs/ inutes/scc Latitude/longitUde source.'D OPSO Topographic map (cbmk box) DEETH PRILLING. LQG From To Formation Desqriptlon !ILLLA — - --- -------- - --- ---- EICH Show direction and distance in miles from at least two State Roads or County Roads. Include the road numbers and common road names. 2161111311M 11 111191 � . I VIAA)-1-r 'FN,;At-' "' Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC 27699-1636 Phone No. (919) 733-3221, within 30 days. GW- I REV. 07/2001 RX TIME 04/14 '03 12': 49 DEQ-CFW-00025400 DEQ-CFW 00025401 04/14/2003 13:50 843-832-4919 GREGG SUMMERVILLE PAGE 0-3 WELL -CONSTRUCTION RECORD North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTIU%CTOR (INDIVIDUAL) NAME (print) Anthony Martin CERTIFICATION #- 3 16 9 WELL CONTRACTOR COMPANY NAME Gregg Dri I I i ng & Tes ti nq nC PHONE 84? 832-4918 STATE WELL CONSTRUCTION PERMITS ASSOCIATED WQ PERMIT# 1. WELL USE (Chock Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 MonitoringlK Recovery 0 Heat Pump Water injection 0 Other 0 If Other, List Use____. 2. WELL LOCATION: Topogmphic/Land sening NearestTown. Fayetteville county B I aden DRidge USlope OValley GFlat 87 West (check apprupriate box) (Street Nnme. Nwnbcrs, Community, Subdivision, Lot No,, Zip Code) Latitudellongitude of well location 3, OWNER: DuPont -CRG Address 6324-Fair-view Road Latitude/longitude source:O OPSO Topographic map (Street Of Ro . ute No.) Charlotte, NC -28210 (check box) DEPIM DELILLINQ LOG City or Town Stan Zip Code From TO Formation Despriptioik 362-33 (104j- 66 n (2- Area code. Phone number 1. 4 4.DATEDRILLED 0114102- =Mo' 5. TOTAL DEPTH: 2f) -I— , T'J tic 1, 6. DOES WELL REPLACE EXISTING WELL? YES 0 No W 7. STATIC WATER LEVEL Below Top of Casing: FT. (Use "+" ifAbove Top ofCasiag) 8. TOP OF CASING IS FT, Above Land Surface* *Top ofca3ing termloatitt! atior bdow land surrher "uIres a variance in accordance with ISA NCAC 2C.01 I& 9. YIELD (Spm), _ METHOD OF TEST 10. WATER ZON ES (depth): Q LCAT bN-SLETCH If. DISINFECTION' Type_ Amount Show direction and distance in miles from at least 12. CASING: Wall Thickness two State Roads or County Roads. Inc * lude the road Depth Diameter or Weight/R. Material Fromo TFt. Us I ahA) -ac,-- _ _L:y — -- numbers and common road names. From To 1140014 From To-- Ft. 13. GROUT: Depth matcrial mcthw Lib From To- Ft, 14SCRF-EN: Depth QLAMeter Slot Size UpIcirial �ZQ (�Iaa C004T-IkAwl� From To FLN4!' in. Qt in. IrC, t4 C 51. From To- Ft. in, in. dl� 15. SAND/GRAVEL ,,ACK. Depth ize Material From 2 To 20 F L d A From To— 16. REMARKS: I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS. AND THAT A COPY OF THIS RECORD HAS BEEN PROVIDED TO T7HE WELL OWNER 6ur 4- %SIGNATURE OF PERSON CONSTRUCTING THE WELL DATE Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center- Raleigh, NC 27699-1636 Phone No. (919) 733-3221, within 30 days. OW-1 REV. 07/2001 RX TIME 04/14 '03 12:49 DEQ-CFW-00025402 DEQ-CFW 00025403 04/14/2003 13:50 843'D-832-4919 0 .. .......... GREGG SUPS MERVILLE PAGE 04 Submit the original to the Division of Water Quality, Groundwater Section, 1636 (Mall Service Center -Raleigh. NC 27699-1636 Phone No. (919) 733-3221, within 30 days. G W- I REV. 07/2001 RX T111E 04114 '03 12:49 DEQ-CFW-00025404 DEQ-CFW 00025405 WELL CONSTRUCTIO N RECORD North Caro |ino-Department of I -'nvironment and Natura I Resources -D i vision of Water Quality - Groundwater Section %% FI.I. CONTRACTOR (INDIVIDUAL) NAME (print) s te cz d. A ds e /j CERTIFICATION #; yrl i VVELiUS[ Ch |icuh|rBox):Residential O Municipal/Public O Industrial Agricultural 2. WELL LOCATION: (Street Name. Numbers, Community, Subdivision, Lot No., Zip Code) 3. (Street or Route No.) City br Town State Zip Code Area code- Phone number 4. DA]1EDR|LL — TOTAL DEPTH: 6. DOES WELL REPLACE EXISTING WELL? YES ,N8'ff 7. STATIC WATER LEVEL Below Top o[Cudmg:_/V__FT. , (Use `'^i/Above Tupvrcm.ou) x. TO|`0[CAS|NG !9!FT. Above Lund Surface* 'lop v,casing terminated wvwrbelow land surface pn^/ps* variance in accordawith /a«mCACzc o//u 9. Y|2LD(gpm) 10. WATER ZONES (dcpdb): 11.D|S|NFEC7|8N: Type Aommu________� 12. CASING: Wall Thickness Depth Diameter orVeighNl Material }'nwm_lo/ '<i/L NY From [v-8._______ FmmTu_____Fc______ 13. GROUT: Depth &imc6al Method From T'L_ Pt From ToFt. 14. SCRE2X Depth Diameter Slot Size k0utchu1 From To_10Fc__Yy_in. /0' in. [mmTo Ft. in. in. \i SAN|NOR/\YELP&CK: Depth Size Material From |'o_1-0_'|'��_J�'�__ ^ Fmm'roFt.16. ______ . REMARKS: Topographic/Land setting (check appropriate box) Latitude/longitude of well location Topographic map (check box) DEPTH DRILLING LOG From To Formation Description LOCATION SKETCH Show direction and distance inmiles from atleast two State Roads urCounty Roads. Include the road numbers �yucommon road names. |D8||[0EDYC[KOFYTl6A[TH|3WELL. WAS CONSTRUCTED |NACCORDANCE WITH l5ANCAC2C.WELL CONSTRUCTION STANDARDS. AND'mAT A COPY OF THIS RECORD HAS BEEN PROVIDFD'rO THE WELL OWNER rA TRE OF PERSON CONSTRUCTING THE WELL 11 DATE Submit the original mthe Division uyWater Quality, Groundwater Section, 1636Mail S«mi, Center - Raleigh, NC DEQ-CFW 00025407 "No appenju North Carolina - Department ol'l--.nvironment and Natural Resources - Division ofWater Quality - Groundwater Section / fif-applicable) (if applicable) WELL US[(Che/k Applicable Box): Residential O Municipal/Public O Industrial O Agricultural O Z.Topographic/Land mcu,esu / oetthnu ORidge 00opc OVukJ illu tcheck appropriate box) (Street Name, Numbers, Community, Subdivision, Lot wu.Zip Code) Latitude/longitude n[well location '. OWNER:— `_g_----__. Latitude/longitude xouor:DCPSOTopographic map (Street wRoute wo) (check box) e At Odle C40 A DEPTH DRILLING LOG City ArTown State Zip Code From To Formation Description `L^' Area code- Phone number ' DATE DRILLED 5. TOTAL DEPTH: �— 6. DOES YYC|J.REPLACE EXISTING WELL? YES N0e~ 7. B'0lC oVA'/'Ek U7Vl�L8c|uwTopo[Cusin8:_F7. , (Use ''+^.rAbove Top v/oa^nV) 8. TOP OF CASING IS FT. Above Land Surface* *Top "/ca,ioxterminated avn,below land surface requires u variance /" accordance with /sAmoxCzm.u//m V. YIELD (&pm):_&#::_METHOD (]FTES 10. WATER 20N[8(dcpth): / .L LOCATION SKETCH ||. DISINFECTION: Type Amomu least Dhowd�r�xiununddiounocinmi|���um�� 12. CASING: WaUThidmca two State Roads orCounty Roads. Include the road Depth Di�nmc, mWeig`NtMaterial ' numbersd —'-' |'nom0___ [o_J1___|{ PO el" From To|'t.______ From To— yt.______ |lGRUUT: Depth k4ute,iu| Method From CTv|l From ToFt. 14. SCKE,2N: Depth Dimnou, Slot Size Material Fromt iT Ftin. jm in. From TvI'/.'__in. in. !i 8ANDK;KAVEL PACK: Depth Size K4ute,W � From _lllO/6[/._XA�__ � . From To— FL________ |D0U[K[BYr[KDFYTNJTH|SWEU.WAS CONSTRUCTED IN ACCORDANCE WITH|5A NCAC 2C,WELL CONSTRUCTION STANDARDS, ANDTHAT A COPY OF THIS R17COIZD I IAS BEEN PROVIDED TO THE WELL OWNER � S|UNATWPU[PERSON [0N9TKUCT|N0ll{EVV[LL ' Dx Submit the original tothe Division of Water Quality, Cruund*mterSection, l636Mail Service Center- Raleigh, NC DEQ-CFW 00025409 WELL CONSTRUCTION RECORD North Carolina - Department ofEnvironment and Natural Resources - Division of'WaterQuality ' Groundwater Section PHONE WELL USE (Check Applicable Bux): Residential Moni6pmVPublicO Industrial Agricultural Monitoring P�cco%ery 0 1 Icat Pump Water I n.j ection 0 Other 0 1 f Other. 1, ist Use 2. WELL LOCATION: (Street Name. Numbers, Community, Subdivision, Lot No., Zip Code) I0WNBK AuNmo (Street wRoute wu/ City SrTown State Zip Code Area code- Phone number 4. DATE DRILLED 5.TOTAL DCPT>l 6. DOES \VBJ.RC|^LACE[0SllNGWELL? YES NO43—~^ 7. STATIC WATER LCYCLBelow Top o[Cuai (Use '+^nAbove Top u/cas.m) 8. TOPOFCASING IS FT. Above Land Surface* °mvvreauoxterminated at/or below land surface requires ^ rw,u^o,/uaccordance with /5A NcAczc 01/8 B. Y|CLD(gpm): )i D|S|N[CC7|0N:T\pc 12. CASING: Depth Diameter From _— /u_—_—r/ 6mn ]o___H.__`_ From ]oFt. ______ GROUT: Depth Material From 0Tu� Ft. _______ From TvFt.________ SCR[CN: Depth Qium,/:r Frum__�Tu_/\( �� ` �� in �p—f— ' From To— Ft. in. 8/\NDfG|{AY[L9ACK: Depth Size From To— Ft.______ |k REMARKS: Amoum_______� Wall Thickness mWciglaffit. Material Slot Size Material _loin. in. Material Topographic/Land setting O Ridge 0 Slope 0 Valley tat (check appropriate box) Latitude/longitude of well location Latitude/longitude map (check box) DEPTH DRILLING LOG From To Formation Description LOCATION SKETCH Show direction and distance |nmiles from ouleast two State Roads orCounty Roads. Include the road numbers and common wut:Wumom. /00|UFK[BYr[KOP/llk\TTU|SWELL WAS CONSTKUC]lD|NACCORDANCE WITH |l^NCxC2C,WELL CONSI'R L ICTION STANDAR DS, AND'ri IATA COPY OF TI I Is RECORD I IAS BEEN PROVIDED TO TI I E WELL OWN r R [0FP[KSONCONSTRUCTING ll/CWELL Submit the original mothe Division of Water Quality, Groundwater Section, l636Mail Service C,nmr-RandAh, NC OEQ-CFVV_00025410 GREGG Drilling and Testing Date Completed 09/18/02 "Y" Coordinates :13012.00 106 Butternut Road Hole Diameter 2 inch Driller Anthony Martin Summerville, SC 29483 Location Fayetteville, NC Driller Number NC# 3169 Logged By Mandel Harvey Depth in 0- DESCRIPTION Feet 0 4 removed while clearing utilities � � Lo Rm OEQ-CFVV_00025411 04,114/'2003 13: 50 843-832-4919 GREGG SUMMERVILLE PAGE 05 WELL CONSTRUCTION RECORD Pz--03 North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRACTOR (INDIVIDUAL) NAME (print) An ',hony Martin CERTIFICATION.Y-2162 WELL CONTRACTOR COMPANY NAME Gregg Drilling & Testing, _Inc.,*' PHONE N 832-4918 STATE WELL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT00 (irapplicable) (if appjivable) 1. WELL USE (Check Applicable Box): Residential 0 Municipal/Public 13 Industrial 0 Agricultural 0 Monitoring 11X Recovery 0 Heat Pump Water Injection it OtherO IfOthcrListUse 2. WELL LOCATION: Topographic/Land setting NearestTown: Fayetteville County B1 aden 0 Ridge 0 Slope 0 Valley 0 Flat 87 West (Check fi1 pr0pri3tc box) (Street Niune, Numbers, Community. Subdivision. Lo(No., Zip Code) Lhiritude/longitude of well location 3. OWNER: DuPont CRG (dcgrces/minuics/wonds) Address --Zn4 Fairvii;i Road Latitude/longitude sourcc:0 OPSO Topographic map (street or lkokw4e- 0.) (check box) Charlotte, NC "28210 DIM DRILLMCi L0-Q .- City or Town State Zip Code From To Formation escriptiton 362-6633 Area code- Phone ntunber 4. DATE DRILLED 1b I J'g 1) nilIRS 5. TOTAL DEPTH: 6, DOES WELL RE PLACE EXISTING WELL? YES 0 NO VK Arl& 7. STATIC WATER LEVEL Below Top of Casing: (Use -+" if Above t4-wc—wing) 8. TOP OF CASING IS FT. Above Land Surface* *Top of casing terminated Wor below land surftce requim a variance in *ccotslnoce with ISA NCAC 2C 01 IL 9. YIELD (gpm)- _ METHOD OF TEST 10. WATER ZONES (depth): LocA'n 11, DISINFECTION: Type_ Amount Show direction and distance in miles from at least 12. CASING: Wall Thickness two State Roads or County Roads. Include the road Depth piameter or Wcight/Ft. Mwcrial numbers and common road names. To_j:�_ Ft �ftll 2U_40 (Z, From TO Ft. From To— Ft.- 13. GROUT: Depth Material Method From nand- ",�' ap d From Y. Ft. 14. SCREEN, Depth D' ame tcr SA0j[)Llot Size material From 115 To �ZQ Ft. l _y From— To 15. SAND/GRAVEL PACK: Depth From Size Material --LO To� 2-0 Ft, A4-: Z /r.�r,- 4— A 'P From To— FL- 16. REMARKS: I DO HEREBY CERTIFY THAT THIS WELL WAS CONSTRUCTED IN ACCORDANCE WITH 15A NCAC 2C, WELL CONSTRUCTION STANDARDS, AND THAT A COPY OF THIS RFCORD HAS BEEN PROVIDED TO THE WELL OWNER n 4— SIGNATURE OF PERSON CONSTRUCTING THE WELL DATE Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Rjdcigh, NC 27699-1636 Phone No. (919) 733-3221, within 30 days. GW-1 REV. 07/2001 R"," TIME 04/14 '03 12:49 DEQ-CFW-00025412 GREGG Ddlling and Testing Date Completed :09118/02 'Y'Coordinates :12633.00 106 Butternut Road Hole Diameter 2 inch Driller Anthony Martin Summerville, SC 29483 Location Fayetteville, NC Driller Number NC# 3169 Logged By Mandel Harvey Depth in DESCRIPTION Feet U) red orange fine Sand SW SW orange fine Sand SW and yellow fine Sand .��hite SW yellow orange fine Sand SW 15 SW orange and pink medium Sand grey and pale red Clay CL I CL black Clay | K41 9E OEQ-CFVV_00025413 04/14/2003 13:50 843-832-4919 GREGG SUMMERVILLE P"'GE 06 WIPMg—ous North Carolina - Department of Environment and Natural Resources - Division of Water Quality � Groundwater SectioD WELL CONTRACTOR (INDIVIOVAL) NAME(print) Anthony Martin CERTIFICATION N—RU WIMLCONTRACTORCONIPANYNAMF Gregg Drilling & Testing,. Inc. rHONE 0 (84? 832-4918 STATE WELL CONSTRUCTION PERMITN ASSOCIATED wQ r%FLmiT# 6 f aPPLI C at) 10 (if ap(licable) 1. WELL USE (�hcck Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 0 Monitorin&V Recovery 0 Beat Pump Water Injection 0 Other 0 If Other, List Use — I 2. WELL LOCATION, Nearest Town: Fayetteville County BI aden 87 West (Street Name, Nmnibm. Community, Su Z�vislonLot No., Zip Code) 3. OWNER: DuPont Address --6324 Fairview oad .......... (Street or Route No.) Charlott NC "M210— City or Town State Zip Code (,LO4). 362-6633 Area 0 Dcodc- Ph be 1 Fib 't ( 0 4. ATE DR.IL 5. TOTAL DEPTH: 6. DOES WELL RE PLACE EXISTING WELL? YESO NO 7. STATIC WATER LEVEL Below Top of Casing: IF (Use -+" if Above Top of Casing) S. TOP OF CASING IS FT. Above Land Surface* *-Top of casing terminated at/or below �%odwrlkce rctiulm a variance In accordRuce with ISA NCAC 2C.0118. 9. YIELD (Spm),. METHOD OF TEST W. WATER ZONES (depth): 11, DISINFECTION: Type_,Amount 12. CASINO: Wall Thici�-m— Depth Iliametcr or Weightfl, Material From b To_A�_ From To -- Ft._ From To— 13. GROUT: Dcpth Material Meth From 0 To! I From --0AJhL— To Ft. 14. SCREEN., D,;, D, I r Jarne c Slot Size Material From To 15. SANPACK: D/GRAVEL Depth Size Material From 108 --To ' ——Ft.-.+,!;k RD From -- _- 16. REMARKS: Topographic/Land setting 0 Ridge 0 Slope 0 Valley 0 Flat (check appropriate box) Latitude/longitude of well location T 4"R f. wwff wlim— ..... ..... WRAP numbers and common mad names. 7-.%w 11017ME Submit the original to the Division of Water Quality, Groundwater Section, 1636 Mail Service Center - Releigb, NC 27699.1636 Phone No. (919) 733-3221, within 30 days. GW-I REV. 07/2001 0=4 I� r RX TIME 04/14 '03 12:49 DEQ-CFW-00025414 CORPORATE REMEDIATIC3N C--RC.UP LOG OF BORING PZ-10 An A//JncB b-t--n ,Dj'o'r and a.— Cha l.tt- NC 28210 (Page I of 1) Date Started 09/18/02 "X" Coordinates : 9841.00 GREGG Drilling and Testing Date Completed :09/18/02 'Y'Coordinates :1264.00 106 Butternut Road Hole Diameter 2 inch Driller Anthony Martin Summerville, SC 29483 Location Fayetteville, NC Driller Number NC# 3169 Logged By Mandel Harvey Depth in DESCRIPTION Feet co removed while clearing utilities E im orange red fine Sand SW yellow white fine Sand SW reddish brown fine Sand SW CL reddish brown Clay CL black Clay Well: PZ-10 Elev.: 146.98 PID PPM mite Seal )n q9 DEQ-CFW-00025415 04/14/2003 13:50 843-832-4919 GREGG SUMMERVILLE PAGE 07 rA WELL CONSTRUCTION RECORD P North Carolina - Department of Environment and Natural Resources - Division of Water Quality - Groundwater Section WELL CONTRACTOR(11NDIVIDUAL) NAME (po.q Anthony CERTIFICATION O—UL9 WELL CON'fKAC`TOR COMPANY N.AmE Gregg Drilling PRONE a L��832�4918 STATE WFLL CONSTRUCTION PERMIT# ASSOCIATED WQ PERMIT# (ira Ica- le) 1, (ifn licable) WELL USE (Check Applicable Box): Residential 0 Municipal/Public 0 Industrial 0 Agricultural 13 Monitoring OX Recovery 13 Heat Pump Water Injection 0 Other 0 If Other, List Use- 2, WELL LOCATION. Nearest Town: Fayetteville County Bladen 87 West (Sirect Name. Nwnbcm Community, Subdivision, Lot No., Zip Code) 3- OWNER: DuPont CRG- Address 6324 Fairview -Road (Sir=% or Rowe No-) Charlotte, -NC 28210 Cit), or Town State Zip Code (1.�4j. 362-6633 Ara gode- Phone nurnbcr 4, DATE DRILLED q 112 162L 5. TOTAL DEPTH:- lb( 6, DOES WELL, REPLACE EXISTING WELL? YES 0 NO 1d 7. STATIC WATER LE VEL Below Top of (Use ­+" if Above Top ofCAsing) 8. TOP OF CASING IS FT. Above Land Surface* *Top or cusing terniloated at/or below IsmA surface requira a variant* In accordance with ISA NCAC 2C.01 It. 9. YIELD (gpm): _ METHOD OF TEST 10. WATER ZONES (depth): 11. DISINFECTION- Type_ Amount - 12, CASING: Wall Thickness From Depth To 15 D' t 'r 'am" c F t. R —4 or Weiglit/Ft. -Material -th 40 From From- To Ft. 13, GROUT: Depth Material Meth From Q To( From TO Ft. 14. SCREEN: Dcpth DI ctc, Slot Size Material From k 15 To Ft =in.• From TO Ft. -in. in. 15. SAND/GRAVEL PACK: Depth Size Material From To2Q Ft. *Z- From I r4i a 13 • Topogtaphic/Land setting 0 Ridge 0 Slope 0 Valley 11 Flat (check Appnmrim box) Latitude/longitude of well location &T KQIMJ� LQQhTIQN SKEICH Show direction and distance in miles from at least two State Roads or County Roads. Include the road rww kcrs and common road names. r4c S-+ MM Submit the original to the Division of Water Quality, Groundwater Seefloo, 1636 Mail Service Center -Raleigh. NC 27699-1636 Phone No. (919) 733-3221, within 30 days. GW- I REV. 07/2001 RX TIME 04114 '03 12:49 DEQ-CFW-00025416 DuPont EnvironmentalCorporate Database ,• Preliminary Administration Review Project Sheet Verify location/jobname in sample table KAR Project Backstop Disk Deliverable Integrity QC Batch Integrity (Correct problems/Pull backstop as necessary) KAR Completeness Check Samples X 100% Tests X 100% Parameters 100% or X <100% KAR Accuracy Check CED Results vs. Hard Copy Lab Reports KAR Comments/Narrative Review KAR Laboratory Services Coordinator Overview Review Report Cover letter/title page for customer KAR Report Finish Copy and Bind KAR Mail to Client(s) Kelly R.inehimer 1/6/03 Certified by Date DEQ-CFW 00025417 The following process is followed on all projects where data is delivered to the Corporate Environmental Database (CED) and a report is generated from the CED. All projects that bypass the CED (Le., are directly reported by a laboratory) do not receive the rigorous treatment presented below. Preliminary Administration To begin a report, the reporting coordinator checks out the file and updates the reporting schedule. A review of the project sheet is the next step to familiarize the coordinator with specifications and special instructions. Finally, the location and Jobname is either added, corrected, or verified to ensure all samples are properly identified as in the project. UOM First, the backstop is used to check the disk deliverable integrity of all project data. This tool checks the CED readiness of the data. Second, quality control batch integrity is checked by the backstop. It is verified that all samples for each test have appropriate quality control samples attached. Completeness Check Data completeness is checked against project specifications. First, all sample points are identified as 100% complete. Then, all tests for each sample point are checked for 100% completeness. A parameter (or analyte) count is verified for each sample and test. A 100% parameter check and/or reporting threshold check can be done if requested in project specifications. Accuracy Check The results reported by disk and located in the CED are checked against the bard copy laboratory reports for accuracy. This stage is a 100% check of the accuracy of the data. Comments/Narrative Review Three steps are included in the comments/narrative review. First, any comments made by the laboratory are located in the hard copy reports. Second, the quality control section(s) of the laboratory reports are reviewed for obvious quality control deficiencies (matrix spike or replicate outside control limits without appropriate comment). If questionable, the laboratory is contacted for verification. Finally, the appropriate comments are entered into the CED. A person familiar with the project (usually the customer service representative) reviews the completed report and the reviewer produces a cover letter. Report Finis ailing The final step is to copy, bind, and mail the report to the client(s) in the format specified in the project specifications. d:\transfer\fwmakape\2002\cedcklst 1. doc DEQ-CFW-00025418 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: FTA-2002 C of C Sampleid: FAY-G-FTA-01 Sampling Point: FTA-01 Date Sampled: DECEMBER 4, 2002 Lab Sample ID: 3955464-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Analyte Parameter Dilution Result Prep/Method: 3010A/6010B CHROMIUM 1 0.0166 LEAD 1 0.0152 J NICKEL 1 0.0159 Prep/Method: 5030B/8260B Unit MDL PQL January 6, 2003 Page 1 Date Analyzed MG/L 0.0020 0.0050 Dec 12, 2002 MG/L 0.0089 0.0200 Dec 12, 2002 MG/L 0.0019 0.0050 Dec 12, 2002 1,2,4-TRIMETHYLBENZENE 1 NO U UG/L 1. 5. Dec 10, 2002 1,3,5-TRIMETHYLBENZENE 1 NO U UG/L 1. 5. Dec 10, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 10, 2002 ETHYLBENZENE 1 NO U UG/L 0.8 5. Dec 10, 2002 ISOPROPYLBENZENE 1 NO U UG/L 1. 5. Dec 10, 2002 M+P-XYLENE 1 ND U UG/L 0.8 5. Dec 10, 2002 0-XYLENE 1 NO U UG/L 0.8 5. Dec 10, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 10, 2002 Surrogates: 1;'2-DICHLOROETHANE-D4 1 93.0 RPR Dec 10, 2002 4-BROMOFLUOROBENZENE 1 106.0 RPR Dec 10, 2002 DIBROMOFLUOROMETHANE 1 89.0 RPR Dec 10, 2002 TOLUENE-D8 1 105.0 RPR Dec 10, 2002 Prep/Method: 351OC/8270C 1-METHYLNAPHTHALENE 1 NO U UG/L 1. 10. Dec 10, 2002 2-METHYLNAPHTHALENE 1 ND U UG/L 1. 10. Dec 10, 2002 ACENAPHTHENE 1 NO U UG/L 1. 10. Dec 10, 2002 ACENAPHTHYLENE 1 NO U UG/L 1. 10. Dec 10, 2002 ANTHRACENE 1 NO U UG/L 1. 10. Dec 10, 2002 BENZO(A)ANTHRACENE 1 ND U UG/L 1. 10. Dec 10, 2002 BENZO(A)PYRENE 1 NO U UG/L 1. 10. Dec 10, 2002 BENZO(B)FLUORANTHENE 1 ND U UG/L 1. 10. Dec 10, 2002 BENZO(G,H,I)PERYLENE 1 ND U UG/L 1. 10. Dec 10, 2002 BENZO(K)FLUORANTHENE 1 ND U UG/L 1. 10. Dec 10, 2002 CHRYSENE 1 ND U UG/L 1. 10. Dec 10, 2002 DIBENZ(A,H)ANTHRACENE 1 ND U UG/L 1. 10. Dec 10, 2002 FLUORANTHENE 1 NO U UG/L 1. 10. Dec 10, 2002 FLUORENE 1 NO U UG/L 1. 10. Dec 10, 2002 INDENO(1,2,3-CD)PYRENE 1 NO U UG/L 1. 10. Dec 10, 2002 NAPHTHALENE 1 NO U UG/L 1. 10. Dec 10, 2002 PHENANTHRENE 1 ND U UG/L 1. 10. Dec 10, 2002 PYRENE 1 ND U UG/L 1. 10. Dec 10, 2002 Surrogates: 2-FLUOROBIPHENYL 1 83.0 RPR Dec 10, 2002 NITROBENZENE-D5 1 84.0 RPR Dec 10, 2002 TERPHENYL-D14 1 49.0 RPR Dec 10, 2002 Comments: Lab personnel received 2 of the 3 volatile vials broken for sample FAY-G-FTA-01. The tab was able to pull the sample from the last vial. Field personnel did not include the date/time on COCs 65468/65476 upon receipt of the bottles for sample -FTA-01. Qualifiers: U The constituent should be considered not detected. J The result is between MDL and PQL and should be considered an estimate. DEQ-CFW 00025419 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: FTA-2002 C of C SampLeid: FAY-G-FTA-02 Sampling Point: FTA-02 Date Sampled: DECEMBER 4, 2002 Lab Sample ID: 3955465-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLytelParameter Dilution Result Prep/Method: 3010AI6010B CHROMIUM 1 0.0077 LEAD 1 ND U NICKEL 1 0.0211 Prep/Method: 503OB/8260B Unit MDL POL January 6, 2003 Page 2 Date Analyzed MG/L 0.0020 0.0050 Dec 12, 2002 MG/L 0.0089 0.0200 Dec 12, 2002 MG/L 0.0019 0.0050 Dec 12, 2002 1,2,4-TRIMETHYLBENZENE 1 ND U UG/L 1. 5. Dec 10, 2002 1,3,5-TRIMETHYLBENZENE 1 ND U UG/L 1. 5. Dec 10, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 10, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 10, 2002 ISOPROPYLBENZENE 1 ND U UG/L 1. 5. Dec 10, 2002 M+P-XYLENE 1 ND U UG/L 0.8 5. Dec 10, 2002 O-XYLENE I ND U UG/L 0.8 5. Dec 10, 2002 TOLUENE I ND U UG/L 0.7 5. Dec 10, 2002 Surrogates: 1,2-DICHLOROETHANE-D4 1 93.0 RPR Dec 10, 2002 4-BROMOFLUOROBENZENE 1 105.0 RPR Dec 10, 2002 DIBROMOFLUOROMETHANE 1 90.0 RPR Dec 10, 2002 TOLUENE-D8 1 104.0 RPR Dec 10, 2002 Prep/Method: 351OC18270C 1-METHYLNAPHTHALENE 1 NO U UG/L 1. 10. Dec 11, 2002 2-METHYLNAPHTHALENE 1 ND U UG/L 1. 10. Dec 11, 2002 ACENAPHTHENE 1 ND U UG/L 1. 10. Dec 11, 2002 ACENAPHTHYLENE 1 ND U UG/L 1. 10. Dec 11, 2002 ANTHRACENE 1 ND U UG/L 1. 10. Dec 11, 2002 BENZO(A)ANTHRACENE 1 ND U UG/L 1. 10. Dec 11, 2002 BENZO(A)PYRENE 1 ND U UG/L 1. 10. Dec 11, 2002 BENZO(B)FLUORANTHENE 1 ND U UGIL 1. 10. Dec 11, 2002 BENZO(G,H,I)PERYLENE 1 ND U UG/L 1. 10. Dec 11, 2002 BENZO(K)FLUORANTHENE 1 ND U UG/L 1. 10. Dec 11, 2002 CHRYSENE 1 ND U UG/L 1. 10. Dec 11, 2002 DIBENZ(A,H)ANTHRACENE 1 ND U UG/L 1. 10. Dec 11, 2002 FLUORANTHENE 1 ND U UG/L 1. 10. Dec 11, 2002 FLUORENE 1 ND U UG/L 1. 10. Dec 11, 2002 INDENO(1,2,3-CD)PYRENE 1 NO U UG/L 1. 10. Dec 11, 2002 NAPHTHALENE 1 ND U UG/L 1. 10. Dec 11, 2002 PHENANTHRENE 1 NO U UG/L 1. 10. Dec 11, 2002 PYRENE 1 NO U UG/L 1. 10. Dec 11, 2002 Surrogates: 2-FLUOROBIPHENYL 1 92.0 RPR Dec 11, 2002 NITROBENZENE-D5 1 90.0 RPR Dec 11, 2002 TERPHENYL-D14 1 65.0 RPR Dec 11, 2002 Comments: Lab personnel received 2 of the 3 volatile vials broken for sample FAY-G-FTA-02. The Lab was able to pull the sample from the Last vial. Field personnel did not include the date/time upon receipt of the bottles forsample -FTA-02 on CoCs 65469/65477. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025420 Corporate Environmental Database LauAnnLvoia Report Location: nnsTrsvzLLs January 6, 2000 Job Name: pTx-2002 page 3 c of n namp!eid: rAY'a'pT« o3 Sampling Point: rTx'03 Date Sampled: uscammsn 4, ZOUZ Lou Sample /o: 3955466-1 Analysis Lab, LAwcxn Sample Type: anouwo wxTsm oc Lx,ei; uc (moom nu Process) Dilution Result Unit MDL POL Date AnaiyKg� Prep/Method: 301GA/6010B conomIun 1 0'006 wo/L 0'0020 0'0050 Dec 12, 2002 LEAD 1 wo u mo/L 0'00e9 0'0200 Dec 12, 3002 wIcnsL 1 o'nssu mo/L 0'0019 0'0050 Dec 12, 2002 /,c,^-/x/ME/w,LmEmzays 1 wn u uo/L 1' 5' Dec 10, 2002 1 S 5-rnIMEToYmswzsws 1 wo u us/� 1 ' 5 ' Dec 10' �02 o�N�sws 1 wo u oo/L 05 5 Dec 102002 srxYLBewzsuE 1 wo u us/L 0.8 5' Dec 10' 2002 Imopeor,mswZsws I wo u ua/L 1' 5' Dec 10' 2002 w+p-xvLswe 1 wn u us/L 0.8 5' Dec 10' 2002 o'xYLsws 1 wu u oo/L 0.8 5' Dec 10` 2002 7oLuswp 1 wo u us/L o'r 5' Dec 10' 2082 Surrogates: 1,3-ozxoLnnuETxxws'o4 1 93'0 xpm Dec 10, 2002 4-oxomorLuonoosmasms 1 107.0 npn Dec 10' 2003 mIanomoFLuonnmsTxAwe 1 90'0 npx Dec 10, 2002 ToLusw*-nV 1 )oa'o mnn Dec 10, 2002 1-msro,LmxporoxLsws 1 wu u uo/L 1' 10' Dec 12, 2002 2-msroYLw*px7xxLcwe 1 wo u oo/L 1' 10' Dec 12, 2002 AcsmAPmxcws 1 wn u uu/L 1' 10' Dec 12, ZDnZ AcEwxpoT*yLEws 1 wu u ou/L 1' 10' Dec 12, znoZ «wTonA:sws 1 wo u uo/L 1' 10' Dec 12, 2003 aswzo(x)xwTonAuswe 1 wu u ws/L l' 10' Dec ?Z, 2002 mswzo(m)p,nEws 1 wo o oo/L l' 10' Dec 12, 2002 uEwzo(o),LuoxAwrocwc 1 mn u uG/L 1' 10' Dec 12, 2002 aEmZo(u,x I)psnYLswc 1 wu u oc/L 1 ' 1n ' Dec 12' 2002 oswzo(K)r[oonxwrxsms 1 wo u us/� 1 10 Dec 122002 nxm,mEws 1 wu o ws/L 1' 10' Dec 12, 2002 oIoswZ(x o)xwrxmACcwc 1 wo u us/L 1 10 Dec 12 ^ ZnoZ pLuomAw7�cwE 1 xo u oG/L 1' 1U' Dec 12. 2002 FLuonews 1 wo o us/L 1' 10' Dec 12, 2002 Imoswn(1 2 3-nu)pYnsoc 1 wo u uo/L 1 10 Dec 12' 2002 wxpxT**L�w�� 1 wo u uo/L ,' m' Dec 122002 poswxw7xxsws 1 wn u UG/L 1' 10. Dec 12^ 2002 p,Rsws 1 wo u UGvL 1. 10. Dec 12, 3002 Surrogates: 2'auoxunIposNYL 1 91'0 xpn Dec 12, 2002 wITmooswosws-n5 1 91-0 *p* Dec 12, 2002 rsxvxswYL'o14 1 44-0 xPu Dec 12, 2002 Comments: Field personnel did not sign Lancaster coc 65470 upon receipt of the bottles or no\hnqvinh the samples to the Laboratory with m signature. Field personnel did not include the date/time the bottles were received on oanoc (TsxposmrL'o14): Recovery value for surrogate was Low. Sufficient volume was not available to reextroct the sample. Qualifiers: U The constituent should be considered not detected. OEQ-CFVV_00025421 Corporate Environmental Database Lab Analysis Report Location: FaYer/svIus Job Name: Fn«'2002 n of c yampteid: mo-o'ruLm-Fnx Sampling Point: TgLc-pTx Date Sampled: oEconesn 4, 2002 Lab Sample ID: 3955487-1 xnaivuiu Lab: Lxwcxo Sample Type: BLANK uwTsm nc Level: uu (*nom uc Process) AnalytelPara ter Dilution Result 1'2,4'rnzmsrxYLmswzsws 1 wu u 1 3 5-TnzmsTxYmswZsws 1 wn u o�w�swE 1 wo u EToYLBewZcws 1 NO u Imopmop,LgsmzswE 1 NO u m+p'xYLcws 1 wn u o-x,Lcws 1 wo u roLuswc 1 wo u Surrogates: 1,2-oIcxLonosrxewc-o4 1 91'0 wpn 4-nmow0FLuonouswZcwc 1 108'0 Rpx ozonomnrLoonomETxAws 1 e9'0 Rpo roLusws-n8 1 107'0 npn January G,2003 Page 4 Unit MDL PQL Date Analyzed uo/L 1' 5' Dec 10' 2002 uo/L 1. 5' Dec 10, 2002 um/L 0'5 5' Dec /U, 2002 on/L 0-8 5' Dec 10. 2002 uo/L 1- 5' Dec m, 2002 uo/L 0-8 5' Dec 10' 2002 ua/L 0.8 5' Dec m, 2002 ua/L 0'7 5. Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec m' 2002 Dec 10, 2002 Comments: Field personnel did not include the date/time the bottles were received on cou 65475' Lab personnel received all s vials for samples FAY-n snoLo rrn-mn1/'oxYe broken' therefore voiatiieo were not reported for these momn/eu' Qualifiers: Corporate Environmental Database Lab Analysis Report Summery of Positive npnuito Location: FmYsTTcvIus January 6, 2003 Job Name: FT*'2002 page 1 Result Unit MDL PQL Method No. Sampling Point: FTA'01 C of c mm ieid: FxY-a'nx'01 Date Sampled: Dec 4^ 2002 Sample Type: annuwo w^Tsx uc Level: uo (xomn uc Process) cxxomzum 0'0166 ws/L o'oVZU V'Ooso 6010B Lcmo 0'0152 J wa/L 0'0089 0-0200 6010B wzcusL 0'0159 mo/L 0-0019 0'0050 60108 Sampling point: prx-UZ c of o o iwid: ,xr-a-p/x-OZ Date Sampled: Dec 4, 2002 Sample Type: onoumo wm7sn QC Level: oc (AuoM uc Process) nxnowIom 0'0077 wa/L 0'0020 0.0050 60108 NICKEL 0'0211 ms/L 0'0019 0'0050 80108 Sampling point: rrx'us c of u Sa (vid: FAY-G'rrA-09 ' Date Sampled: Dec 4' 2002 Sample Type: mxuuwn :nTsn oc Level: mc (xomw oo Process) ' conomImm 0.0081 ws/L 0.0020 0.0050 6010o wznnsL 0.0356 ws/L 0'0019 0.0050 00108 ouaiifiero: Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: FTA-2002 Batch Identifier Method Number: 6010B Batch Start Date: 11DECO2 Instrument: 005478 Batch Number: 5 The following field samples are included in this batch: January 6, 2003 Page 1 Date QC Sample Name Sampled Lab Sample ID Level FAY-G-FTA-01 04DECO2 3955464-1 LANCAS QC FAY-G-FTA-02 04DECO2 3955465-1 LANCAS QC FAY-G-FTA-03 04DECO2 3955466-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: CHROMIUM 103 LCS-1 LANCAS LEAD 101 LCS-1 LANCAS NICKEL 101 LCS-1 LANCAS Method Blank: CHROMIUM ND MG/L .002 BLANK-1 LANCAS LEAD ND MG/L .0089 BLANK-1 LANCAS NICKEL ND MG/L .0019 BLANK-1 LANCAS Matrix Spike: CHROMIUM 110 3955464-1 LANCAS LEAD 101 3955464-1 LANCAS NICKEL 103 3955464-1 LANCAS Matrix Spike Duplicate: CHROMIUM 105 4 3955464-1 LANCAS LEAD 103 2 3955464-1 LANCAS NICKEL 101 1 3955464-1 LANCAS Replicate: CHROMIUM 0.0186 MG/L 0 3955464-1 LANCAS LEAD 0.0105 MG/L 0 3955464-1 LANCAS NICKEL 0.0164 MG/L 0 3955464-1 LANCAS Batch Identifier Method Number: 8260B Prep Method: 5030B Pre -prep: Batch Start Date: 10DECO2 Instrument: 083630 Batch Number: 1 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-FTA-01 04DECO2 3955464-1 LANCAS QC FAY-G-FTA-02 04DECO2 3955465-1 LANCAS QC FAY-G-FTA-03 04DECO2 3955466-1 LANCAS QC FAY-K-TBLK-FTA 04DECO2 3955467-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1,2,4-TRIMETHYLBENZENE 102 LCS-1 LANCAS 1,3,5-TRIMETHYLBENZENE 102 LCS-1 LANCAS BENZENE 96 LCS-1 LANCAS ETHYLBENZENE 107 LCS-1 LANCAS ISOPROPYLBENZENE 110 LCS-1 LANCAS M+P-XYLENE 110 LCS-1 LANCAS 0-XYLENE 108 LCS-1 LANCAS TOLUENE 104 LCS-1 LANCAS Method Blank: 1,2,4-TRIMETHYLBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,3,5-TRIMETHYLBENZENE ND UG/L 1 BLANKA-1 LANCAS BENZENE ND UG/L .5 BLANKA-1 LANCAS ETHYLBENZENE ND UG/L .8 BLANKA-1 LANCAS ISOPROPYLBENZENE ND UG/L 1 BLANKA-1 LANCAS M+P-XYLENE ND UG/L .8 BLANKA-1 LANCAS DEQ-CFW 00025424 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: FTA-2002 (Batch continued from previous page) January 6, 2003 Page 2 AnaLYtek:/Parameter Result Unit MDL RPR RPD Lab Sample ID Method Blan 0-XYLENE ND UG/L .8 BLANKA-1 LANCAS TOLUENE ND UG/L .7 BLANKA-1 LANCAS Matrix Spike: 1,2,4-TRIMETHYLBENZENE 114 3955464-1 LANCAS 1,3,5-TRIMETHYLBENZENE 113 3955464-1 LANCAS BENZENE 102 3955464-1 LANCAS ETHYLBENZENE 122 3955464-1 LANCAS ISOPROPYLBENZENE 122 3955464-1 LANCAS M+P-XYLENE 124 3955464-1 LANCAS 0-XYLENE 118 3955464-1 LANCAS TOLUENE 122 3955464-1 LANCAS Matrix Spike Dup€irate: 1,2,4-TRIMETHYLBENZENE 112 2 3955464-1 LANCAS 1,3,5-TRIMETHYLBENZENE 110 2 3955464-1 LANCAS BENZENE 100 2 3955464-1 LANCAS ETHYLBENZENE 119 3 3955464-1 LANCAS ISOPROPYLBENZENE 121 1 3955464-1 LANCAS M+P-XYLENE 121 2 3955464-1 LANCAS 0-XYLENE 119 0 3955464-1 LANCAS TOLUENE 119 3 3955464-1 LANCAS Batch Identifier Method Number: 8270C Prep Method: 3510C Pre -prep: Batch Start Date: 09DECO2 Instrument: 067540 Batch Number: 9 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID LeveL FAY-G-FTA-01 04DECO2 3955464-1 LANCAS QC FAY-G-FTA-02 04DECO2 3955465-1 LANCAS QC AnaLYte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1-METHYLNAPHTHALENE 78 LCS-1 LANCAS 2-METHYLNAPHTHALENE 82 LCS-1 LANCAS ACENAPHTHENE 91 LCS-1 LANCAS ACENAPHTHYLENE 91 LCS-1 LANCAS ANTHRACENE 97 LCS-1 LANCAS BENZO(A)ANTHRACENE 98 LCS-1 LANCAS BENZO(A)PYRENE 100 LCS-1 LANCAS BENZO(B)FLUORANTHENE 96 LCS-1 LANCAS BENZO(G,H,I)PERYLENE 93 LCS-1 LANCAS BENZO(K)FLUORANTHENE 103 LCS-1 LANCAS CHRYSENE 94 LCS-1 LANCAS DIBENZ(A,H)ANTHRACENE 98 LCS-1 LANCAS FLUORANTHENE 97 LCS-1 LANCAS FLUORENE 94 LCS-1 LANCAS INDENO(1,2,3-CD)PYRENE 91 LCS-1 LANCAS NAPHTHALENE 77 LCS-1 LANCAS PHENANTHRENE 96 LCS-1 LANCAS PYRENE 92 LCS-1 LANCAS Method Blank: 1-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS 2-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHYLENE ND UG/L 1 BLANK-1 LANCAS ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)PYRENE ND UG/L 1 BLANK-1 LANCAS BENZO(B)FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS BENZO(G,H,I)PERYLENE ND UG/L 1 BLANK-1 LANCAS BENZO(K)FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS CHRYSENE ND UG/L 1 BLANK-1 LANCAS DIBENZ(A,H)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS DEQ-CFW 00025425 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: FTA-2002 (Batch continued from previous page) AnaLyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Method Blank: FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS FLUORENE ND UG/L 1 BLANK-1 LANCAS INDENO(1,2,3-CD)PYRENE ND UG/L 1 BLANK-1 LANCAS NAPHTHALENE ND UG/L 1 BLANK-1 LANCAS PHENANTHRENE ND UG/L 1 BLANK-1 LANCAS PYRENE ND UG/L 1 BLANK-1 LANCAS Matrix Spike: 1-METHYLNAPHTHALENE 69 3955464-1 LANCAS 2-METHYLNAPHTHALENE 69 3955464-1 LANCAS ACENAPHTHENE 74 3955464-1 LANCAS ACENAPHTHYLENE 79 3955464-1 LANCAS ANTHRACENE 73 3955464-1 LANCAS BENZO(A)ANTHRACENE 75 3955464-1 LANCAS BENZO(A)PYRENE 78 3955464-1 LANCAS BENZO(B)FLUORANTHENE 73 3955464-1 LANCAS BENZO(G,H,I)PERYLENE 77 3955464-1 LANCAS BENZO(K)FLUORANTHENE 80 3955464-1 LANCAS CHRYSENE 74 3955464-1 LANCAS DIBENZ(A,H)ANTHRACENE 83 3955464-1 LANCAS FLUORANTHENE 72 3955464-1 LANCAS FLUORENE 74 3955464-1 LANCAS INDENO(1,2,3-CD)PYRENE 75 3955464-1 LANCAS NAPHTHALENE 68 3955464-1 LANCAS PHENANTHRENE 73 3955464-1 LANCAS PYRENE 72 3955464-1 LANCAS Matrix Spike Duplicate: 1-METHYLNAPHTHALENE 69 0 3955464-1 LANCAS 2-METHYLNAPHTHALENE 70 1 3955464-1 LANCAS ACENAPHTHENE 73 2 3955464-1 LANCAS ACENAPHTHYLENE 76 3 3955464-1 LANCAS ANTHRACENE 74 1 3955464-1 LANCAS BENZO(A)ANTHRACENE 73 3 3955464-1 LANCAS BENZO(A)PYRENE 75 4 3955464-1 LANCAS BENZO(B)FLUORANTHENE 71 2 3955464-1 LANCAS BENZO(G,H,I)PERYLENE 71 8 3955464-1 LANCAS BENZO(K)FLUORANTHENE 76 6 3955464-1 LANCAS CHRYSENE 72 3 3955464-1 LANCAS DIBENZ(A,H)ANTHRACENE 77 7 3955464-1 LANCAS FLUORANTHENE 72 0 3955464-1 LANCAS FLUORENE 74 0 3955464-1 LANCAS INDENO(1,2,3-CD)PYRENE 70 7 3955464-1 LANCAS NAPHTHALENE 69 1 3955464-1 LANCAS PHENANTHRENE 71 3 3955464-1 LANCAS PYRENE 72 0 3955464-1 LANCAS Comments: 8270C (1-METHYLNAPHTHALENE): The matrix spike and spike duplicate recoveries were outside control limits. Lab control spike recovery met acceptance criteria. 8270C (INDENO(1,2,3-CD)PYRENE): The matrix spike and spike duplicate recoveries were outside control limits. Lab control spike recovery met acceptance criteria. 8270C (ACENAPHTHYLENE): The matrix spike duplicate recovery was outside control limits. Lab control spike recovery met acceptance criteria. 8270C (SENZO(A)ANTHRACENE): The matrix spike duplicate recovery was outside control Limits. Lab control spike recovery met acceptance criteria. 8270C (BENZO(A)PYRENE): The matrix spike duplicate recovery was outside control limits. Lab control spike recovery met acceptance criteria. rt< DEQ-CFW 00025426 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 6, 2003 Project Name: FTA-2002 Page 4 Batch Identifier Method Number: 8270C Prep Method: 3510C Pre -prep: Batch Start Date: 10DECO2 Instrument: 067770 Batch Number: 6 The following field samples are included in this batch: Date 0C Sample Name Sampled Lab Sample ID Level FAY-G-FTA-03 04DECO2 3955466-1 LANCAS QC AnaLytelParameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1-METHYLNAPHTHALENE 89 LCS-1 LANCAS 2-METHYLNAPHTHALENE 89 LCS-1 LANCAS ACENAPHTHENE 92 LCS-1 LANCAS ACENAPHTHYLENE 94 LCS-1 LANCAS ANTHRACENE 90 LCS-1 LANCAS BENZO(A)ANTHRACENE 95 LCS-1 LANCAS BENZO(A)PYRENE 102 LCS-1 LANCAS BENZO(B)FLLJORANTHENE 91 LCS-1 LANCAS BENZO(G,H,I)PERYLENE 100 LCS-1 LANCAS BENZO(K)FLUORANTHENE 99 LCS-1 LANCAS CHRYSENE 97 LCS-1 LANCAS DIBENZ(A,H)ANTHRACENE 108 LCS-1 LANCAS FLUORANTHENE 95 LCS-1 LANCAS FLUORENE 90 LCS-1 LANCAS INDENO(1,2,3-CD)PYRENE 99 LCS-1 LANCAS NAPHTHALENE 86 LCS-1 LANCAS PHENANTHRENE 90 LCS-1 LANCAS PYRENE 94 LCS-1 LANCAS Lab Control Spike Duplicate: 1-METHYLNAPHTHALENE 92 4 LCSD-1 LANCAS 2-METHYLNAPHTHALENE 92 3 LCSD-1 LANCAS ACENAPHTHENE 95 4 LCSD-1 LANCAS ACENAPHTHYLENE 96 2 LCSD-1 LANCAS ANTHRACENE 95 5 LCSD-1 LANCAS BENZO(A)ANTHRACENE 98 3 LCSD-1 LANCAS BENZO(A)PYRENE 106 4 LCSD-1 LANCAS BENZO(B)FLUORANTHENE 95 4 LCSD-1' LANCAS SENZO(G,H,I)PERYLENE 105 5 LCSD-1 LANCAS BENZO(K)FLUORANTHENE 103 4 LCSD-1 LANCAS CHRYSENE 99 3 LCSD-1 LANCAS DIBENZ(A,H)ANTHRACENE 113 5 LCSD-1 LANCAS FLUORANTHENE 101 5 LCSD-1 LANCAS FLUORENE 92 2 LCSD-1 LANCAS INDENO(1,2,3-CD)PYRENE 102 4 LCSD-1 LANCAS NAPHTHALENE 89 4 LCSD-1 LANCAS PHENANTHRENE 94 5 LCSD-1 LANCAS PYRENE 96 2 LCSD-1 LANCAS Method Blank: 1-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS 2-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHYLENE ND UG/L 1 BLANK-1 LANCAS ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)PYRENE ND UG/L 1 BLANK-1 LANCAS BENZO(B)FLLJORANTHENE ND UG/L 1 BLANK-1 LANCAS BENZO(G,H,I)PERYLENE ND UG/L 1 BLANK-1 LANCAS BENZO(K)FLUORANTHENE ND UG/L I BLANK-1 LANCAS CHRYSENE ND UG/L I BLANK-1 LANCAS DIBENZ(A,H)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS FLUORENE ND UG/L 1 BLANK-1 LANCAS INDENO(1,2,3-CD)PYRENE ND UG/L 1 BLANK-1 LANCAS NAPHTHALENE ND UG/L 1 BLANK-1 LANCAS PHENANTHRENE ND UG/L 1 BLANK-1 LANCAS PYRENE ND UG/L 1 BLANK-1 LANCAS DEQ-CFW-00025427 Meat Hj"md 0 Box-1242.5LancastF-I , I . e a n, H e at I I nc;U' tv Suminfi3r VIP ivl�'dlod of Shbrina FT/\ LiSt VViAj 140 1 HO J t i H PC DEQ-CFW-00025428 - ., R•v w 3.-W:+ �j b� b"M ✓" 9?:'h.(- Y:' /�i ,iB�4 y7 �� % }�' f�j �j"j ( y � 1 �-`! /1�/ 25) tt r °, , s t ! 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'T- -,I, �' M , , - 471 DEQ-CFW 00025429 64 a d,Ienry H o I I a n d 10 b a> 1 J4z , Lancaster. . <—_.._.�..__.__. ._.._ _�—.______._—._.____..... .,.._ .. .__. .. a• Zxt.. ."1,., %,_.-,�_�_._...-.t—._..._._._....__.a �._�_..� ' :t,;Pf)nt F-,ive'tt , 170 -3F 663 jr;f eaa?t I i._ CYir,.: i a.1' Shin, _ iTelephone rJuteal7 r �Tt FnSteSitt a �aaiTia� iTw�i��d e�ioey¢cosridaFr _._,...,..... i 1 C nartL i"yr,.Ft taidr j _I7�' ir2 i17 _r. _ .11._ , ___.. _.m ..,._... t r_...-.� r._.?tire^..,. i-e`r9nc�gg(t•mP %�fisiraq,, H aOl _ w r xE�r� w Saver i;i2v' mei Jor i n,fethod of Handling i I 1 r C- fi g t I 1 ®1. l j0.-. 1 tet i... ; i t jot f t I 1 .. +lZ __ _. F VvV !40 1 H{ I .. i a s 5 µ l� t!` -S Received t. e .ain .lbi9'cU by aIJ` 1t;t- i df'i'f8 �✓� ji'Rec iye d by t I M�vvi�ilb y�m�1 ,.1 tL.h t, 39..i+.Gtril7'w� i. ��... .._?.,„ vi1 I..°rSi:�i l ltY4i? 6J6, 12 #s Cate DEQ-CFW 00025430 ...... ..N...e..v...v Holland Bco. '­Q.>. Lam,?ster, PA 17f"V5-)A25 ....... �4r A, H r -'r, d- Method of Saver 7 1 p t F f - C� - F TA, Q i - Ali 'S 0 0 �J' 4C f- i,,lA-U I 4VI 5 U00 i N! a 2 "_,2 0 3 1 HIN03 1 B �A - — ------ ----- !I IIAN 101)0 1 khMW 1 2 B i .......... A 1 ttilleiinqyishEd b \b, I -Iondition of Samples Upon arrival at Finai Destination es --- -- ---- - � rqt-_..,Lf3rst 1 ime Zi L eV 11 VI I C ------- ------ • oe A/If DEQ-CFW-00025431 d 0 c' x. 1 ---- --------- UE cni: Fn o �!�tv Suncrvicr d 1 i i Vvvv lv,. .......... - -- ----- --------------- -- lnrol.fles Kella4ished by 'rTles m f0aicei-hirle I tiet,vl{fF?ta 11 ne 2 191 - - - ----------- .3-E-5041 03 Ar . ......... ..... . ..... . ...... ;� of Shippin 5mi L �- ateil itine I C'� can ILI+ a, r i .Ind ­425. Lancat�Aei% PA 1760!5-2425 ;�..�uPont Favettvim-_, r/04-362..6633 I �aci!RV Name, i,4mr-0e.r L 1 cIllfv u n M, o r I,,_4hzr Emp!ciyees(s) Rand}t.q ot. ViAN In -Ofj i HNO3 1_.1 'VVVkf I I f C, 0 1 T%t lla2S20 1 8 1 r4 Ill 1644 05-604,103 [ErpiqgtjAv Oer­ ru - dern I ExDrec;s mmrwter P-4ime Mlethod ,,f U�7�9a C TI NQ c a D,jte h DEQ-CFW-00025433 V3 '0 SwF 2-4,25, Lancasiew, PA 760-5­ 5 - ---------- R;f Tpkmhonse. Nun*4�r !'rrqnm,,)rtv.r Name i it %Jv%vv� rlWT\ K y _e' z@41 ocl I j.Qj '.' ... . ...... ... . ..... F lu 3 ijv iN W-0 .. . .. .... . ,rt. ...... ..... J_citics Refinauished bv !atei Firne 1A IZ2coffles Received] 6 191 r_r:7O -r ?:dfdrnn 'S" Savii�t af m a - " �w ­ p. 0 �aml­--z on S - 5 041 CK-1 G F2,2iL? A&t- AHevvHolland 72A5 Box 1, PA 105-2 -nt Faveft, 7 -362-663, 3 [.0/1 .4 o v � j;t m Num, bsr Nnmc, ;rdr�l tlE! A'7 !Qcv liil Favelf-ville WC '21".302 -xpres, ---- -- - ---of S.111 -cdr7 Pt inn = its t, 10 "p fL_h,! tg-I I2 °P-4270Afs',Nrita=PbNi,r-m,,r7�PI els, ,r7 e Ila Volrq=Pr iervafilll nuanwv G,. F TA.- 0:1 0 WIN i5oo 1 HNO 13 00 1 viq I0 NWS2 NWS203 2, of jiWQ 6j n Al DEQ-CFW-00025435 5 e -2v H o 111 -f I d C) r of 1242U. Laricastef, PA 17PD!7,-2/,?,7 - ----------- ------ iT (43 i --- -- ------ ....... E'JuPont 04-382-6633 �Z, n; v 2 1 -.,1 Iv Niur"A"or, Nano -a .. .... . .. ......... . .......... A r i 01,{') r-"t-aveiti,ill- fJC �+ ln F TA' rtei,nau�shed b j C20 '104 103 Mzsihod of -- - ------- Us DEQ-CFW-00025436 New Hollanc 10 'Bo, 12425Lan aster ---P-- A---- I-A105-242.J ..... ....... cr nt F:-"�vrl JI:,, kA. cthcd of ��Nppftlg, an, alter ------- --- FA.A.,,AY2 .... ......... ..... . ....... I loan t ,- JT I a !ReCefvEd b%J .4 ivne ;3_yiwil�s r"n Al'al'AA DEQ-CFW-00025437 � =%^ ------�—'-----------1 \ Or "Wes Refinciuis 1 al'21P 1-411—lZa gja�;�Recsive -Jime i!i:2n of Sam. les L'Don a i at Final Destination 6 on An lVal Q u DuPont Corporate EnvironmentalDatabase 11'reliminary Administration Review Project Sheet Verify location/jobname in sampletable Project Backstop Disk Deliverable Integrity QC Batch Integrity (Correct problems/Pull backstop as necessary) Completeness Check Samples x 11` Tests x rr Parameters 100% Accuracy Check 1 Results i Copy Lab Reports I I � Laboratory Services 1 1 1' I 1' Overview ReviewReport Cover/,•- for customer Report1 1 Copy and { Kelly Rinehimer Certified by 1 •1 DEQ-CFW 00025439 I The following process is followed on all projects where data is delivered to the Corporate Environmental Database (CED) and a report is generated from the CED. All projects that bypass the CED (Le., are directly reported by a laboratory) do not receive the rigorous treatment presented below. Preliminary Administration To begin a report, the reporting coordinator checks out the file and updates the reporting schedule. A review of the project sheet is the next step to familiarize the coordinator with specifications and special instructions. Finally, the location and jobname is either added, corrected, or verified to ensure all samples are properly identified as in the project. Project Backstop First, the backstop is used to check the disk deliverable integrity of all project data. This tool checks the CED readiness of the data. Second, quality control batch integrity is checked by the backstop. It is verified that all samples for each test have appropriate quality control samples attached. Completeness Check Data completeness is checked against project specifications. First, all sample points are identified as 100% complete. Then, all tests for each sample point are checked for 100% completeness. A parameter (or analyte) count is verified for each sample and test. A 100% parameter check and/or reporting threshold check can be done if requested in project specifications. Accuracy Check The results reported by disk and located in the CED are checked against the hard copy laboratory reports for accuracy. This stage is a 100% check of the accuracy of the data. Comments/Narrative Review Three steps are included in the comments/narrative review. First, any comments made by the laboratory are located in the hard copy reports. Second, the quality control section(s) of the laboratory reports are reviewed for obvious quality control deficiencies (matrix spike or replicate outside control limits without appropriate comment). If questionable, the laboratory is contacted for verification. Finally, the appropriate comments are entered into the CED. A person familiar with the project (usually the customer service representative) reviews the completed report and the reviewer produces a cover letter. Report Finis ailing The final step is to copy, bind, and mail the report to the client(s) in the format specified in the project specifications. d:\trmsfer\forrna\fayetteville\2002\ccdckist 1. doc DEQ-CFW-00025440 Corporate Environmental Database Lab Analysis Report Summary of Positive Results Location: FAYETTEVILLE Job Name: SWMU6-2002 AnatyteZParameter Sampling Point: SWMU06-01A C of C Sampteid: FAY-S-SWMU06-01A(4-5) Date Sampled: Dec 10, 2002 Sample Type- SOIL QC Level: QC (ADOM QC Process) ACENAPHTHENE ANTHRACENE BENZO(A)ANTHRACENE BENZO(A)PYRENE BENZO(B)FLUORANTHENE BENZO(K)FLUORANTHENE CHRYSENE FLUORANTHENE FLUORENE PHENANTHRENE PYRENE January 7, 2003 Page 1 Result Unit MDL POL Method No. 45. J UG/KG 36. 360. 8270C 71. 1 UG/KG 36- 360. 8270C 210. J UG/KG 36. 360. 8270C 91. 1 UG/KG 36. 360. 8270C 160. 1 UG/KG 36. 360. 8270C 55. J UG/KG 36. 360. 8270C 250. J UG/KG 36. 360- 8270C 990. UG/KG 36. 360. 8270C 68. J UG/KG 36. 360. 8270C 400. UG/KG 36. 360. 8270C 800. UG/KG 36. 360. 8270C Sampling Point: SWMU06-01A C of C SampLeid: FAY-S-SWMU06-01A(4-5)-DUP Date Sampled: Dec 10, 2002 Sample Type: SOIL QC Level: QC (ADQM QC Process) BENZO(A)ANTHRACENE 91. 1 UG/KG 37. 370. BENZO(A)PYRENE 46. 1 UG/KG 37. 370. BENZO(B)FLUORANTHENE -71. J UG/KG 37. 370. CHRYSENE 88. J UG/KG 37. 370. FLUORANTHENE 450. UG/KG 37. 370. FLUORENE 39. 1 UG/KG 37. 370. PHENANTHRENE 210. J UG/KG 37. 370. PYRENE 400. UG/KG 37. 370. Qualifiers: i The result is between MDL and PQL and should be considered an estimate. 8270C 8270C 8270C 8270C 8270C 8270C 8270C 8270C DEQ-CFW-00025441 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6-2002 Batch Identifier Method Number: 160.3 MOD. Prep Method: Batch Start Date: 13DECO2 Instrument: 009001 Batch Number: 1 January 7, 2003 Page 1 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-S-SWMU06-01A(4-5)-DUP 10DECO2 3958279-1 LANCAS QC Analyte/parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: MOISTURE 100 LCS-1 LANCAS Replicate: MOISTURE 10.7 % 6 3955876-1 LANCAS Batch Identifier Method Number: 160.3 MOD. Prep Method: Pre -prep: Batch Start Date: 17DECO2 Instrument: 009001 Batch Number• 1 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-S-SWMU06-01A(4-5) 10DECO2 3958278-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: MOISTURE 100 LCS-1 LANCAS Replicate: MOISTURE 9.82 Y 5 3958278-1 LANCAS Batch Identifier Method Number: 8270C Prep Method: 3510C Pre -prep: Batch Start Date: 12DECO2 Instrument: 055250 Batch Number: 4 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-K-EQBLK-NAFGW-DAY2 10DECO2 3958316-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1-METHYLNAPHTHALENE 90 LCS-1 LANCAS 2-METHYLNAPHTHALENE 92 LCS-1 LANCAS ACENAPHTHENE 97 LCS-1 LANCAS ACENAPHTHYLENE 100 LCS-1 LANCAS ANTHRACENE 90 LCS-1 LANCAS BENZO(A)ANTHRACENE 97 LCS-1 LANCAS BENZO(A)PYRENE 104 LCS-1 LANCAS BENZO(B)FLUORANTHENE 98 LCS-1 LANCAS BENZO(G,H,I)PERYLENE 97 LCS-1 LANCAS BENZO(K)FLUORANTHENE 102 LCS-1 LANCAS CHRYSENE 94 LCS-1 LANCAS DIBENZ(A,H)ANTHRACENE 104 LCS-1 LANCAS FLUORANTHENE 92 LCS-1 LANCAS FLUORENE 98 LCS-1 LANCAS INDENO(1,2,3-CD)PYRENE 97 LCS-1 LANCAS NAPHTHALENE 91 LCS-1 LANCAS PHENANTHRENE 92 LCS-1 LANCAS PYRENE 92 LCS-1 LANCAS DEQ-CFW 00025442 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6-2002 (Batch continued from previous page) January 7, 2003 Page 2 Analyte/Parameter Result Unit MDL RPR RPD Lab Sande ID Lab Control Spike Duplicate: 1-METHYLNAPHTHALENE 91 1 LCSD-1 LANCAS 2-METHYLNAPHTHALENE 93 1 LCSD-1 LANCAS ACENAPHTHENE 96 1 LCSD-1 LANCAS ACENAPHTHYLENE 101 1 LCSD-1 LANCAS ANTHRACENE 90 0 LCSD-1 LANCAS BENZO(A)ANTHRACENE 98 1 LCSD-1 LANCAS BENZO(A)PYRENE 103 2 LCSD-1 LANCAS BENZO(B)FLUORANTHENE 98 0 LCSD-1 LANCAS BENZO(G,H,I)PERYLENE 96 1 LCSD-1 LANCAS BENZO(K)FLUORANTHENE 100 1 LCSD-1 LANCAS CHRYSENE 95 1 LCSD-1 LANCAS DISENZ(A,H)ANTHRACENE 103 1 LCSD-1 LANCAS FLUORANTHENE 91 1 LCSD-1 LANCAS FLUORENE 98 0 LCSD-1 LANCAS INDENO(1,2,3-CD)PYRENE 95 2 LCSD-1 LANCAS NAPHTHALENE 93 2 LCSD-1 LANCAS PHENANTHRENE 91 1 LCSD-1 LANCAS PYRENE 95 3 LCSD-1 LANCAS Method Blank: 1-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS 2-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHYLENE ND UG/L 1 BLANK-1 LANCAS ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)PYRENE ND UG/L 1 BLANK-1 LANCAS BENZO(B)FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS BENZO(G,H,I)PERYLENE ND UG/L 1 BLANK-1 LANCAS BENZO(K)FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS CHRYSENE ND UG/L 1 BLANK-1 LANCAS DIBENZ(A,H)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS FLUORENE ND UG/L 1 BLANK-1 LANCAS INDENO(1,2,3-CD)PYRENE ND UG/L 1 BLANK-1 LANCAS NAPHTHALENE ND UG/L 1 BLANK-1 LANCAS PHENANTHRENE ND UG/L 1 BLANK-1 LANCAS PYRENE ND UG/L 1 BLANK-1 LANCAS Comments: 8270C: The matrix spike and spike duplicate were not performed due to insufficient sample. The laboratory control sample and control sample duplicate were analyzed to measure accuracy and precision at the batch Level. Batch Identifier Method Number: 8270C Prep Method: 3550B Pre -prep: Batch Start Date: 12DECO2 Instrument: 055250 Batch Number: 4 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-S-SWMU06-01A(4-5) 10DECO2 3958278-1 LANCAS QC FAY-S-SWMU06-01A(4-5)-DUP 10DECO2 3958279-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1-METHYLNAPHTHALENE 92 LCS-1 LANCAS 2-METHYLNAPHTHALENE 95 LCS-1 LANCAS ACENAPHTHENE 96 LCS-1 LANCAS ACENAPHTHYLENE 97 LCS-1 LANCAS ANTHRACENE 87 LCS-1 LANCAS BENZO(A)ANTHRACENE 95 LCS-1 LANCAS BENZO(A)PYRENE 97 LCS-1 LANCAS BENZO(B)FLUORANTHENE 93 LCS-1 LANCAS BENZO(G,H,I)PERYLENE 92 LCS-1 LANCAS DEQ-CFW 00025443 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 7, 2003 Project Name: SWMU6-2002 Page 3 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: BENZO(K)FLUORANTHENE 99 LCS-1 LANCAS CHRYSENE 93 LCS-1 LANCAS DIBENZ(A,H)ANTHRACENE 98 LCS-1 LANCAS FLUORANTHENE 91 LCS-1 LANCAS FLUORENE 96 LCS-1 LANCAS INDENO(1,2,3-CD)PYRENE 93 LCS-1 LANCAS NAPHTHALENE 93 LCS-1 LANCAS PHENANTHRENE 89 LCS-1 LANCAS PYRENE 92 LCS-1 LANCAS Method Blank: 1-METHYLNAPHTHALENE ND UG/KG 33 BLANK-1 LANCAS 2-METHYLNAPHTHALENE ND UG/KG 33 BLANK-1 LANCAS ACENAPHTHENE ND UG/KG 33 BLANK-1 LANCAS ACENAPHTHYLENE ND UG/KG 33 BLANK-1 LANCAS ANTHRACENE ND UG/KG 33 BLANK-1 LANCAS BENZO(A)ANTHRACENE ND UG/KG 33 BLANK-1 LANCAS SENZO(A)PYRENE ND UG/KG 33 BLANK-1 LANCAS BENZO(B)FLUORANTHENE ND UG/KG 33 BLANK-1 LANCAS BENZO(G,H,I)PERYLENE ND UG/KG 33 BLANK-1 LANCAS BENZO(K)FLUORANTHENE ND UG/KG 33 BLANK-1 LANCAS CHRYSENE ND UG/KG 33 BLANK-1 LANCAS DIBENZ(A,H)ANTHRACENE ND UG/KG 33 BLANK-1 LANCAS FLUORANTHENE ND UG/KG 33 BLANK-1 LANCAS FLUORENE ND UG/KG 33 BLANK-1 LANCAS INDENO(1,2,3-CD)PYRENE ND UG/KG 33 BLANK-1 LANCAS NAPHTHALENE ND UG/KG 33 BLANK-1 LANCAS PHENANTHRENE ND UG/KG 33 BLANK-1 LANCAS PYRENE ND UG/KG 33 BLANK-1 LANCAS Matrix Spike: 1-METHYLNAPHTHALENE 83 3958278-1 LANCAS 2-METHYLNAPHTHALENE 87 3958278-1 LANCAS ACENAPHTHENE 87 3958278-1 LANCAS ACENAPHTHYLENE 88 3958278-1 LANCAS ANTHRACENE 83 3958278-1 LANCAS BENZO(A)ANTHRACENE 87 3958278-1 LANCAS BENZO(A)PYRENE 89 3958278-1 LANCAS BENZO(B)FLUORANTHENE 86 3958278-1 LANCAS BENZO(G,H,I)PERYLENE 88 3958278-1 LANCAS BENZO(K)FLUORANTHENE 92 39582Z8-1 LANCAS CHRYSENE 85 39582 8-1 LANCAS DIBENZ(A,H)ANTHRACENE 95 3958278-1 LANCAS FLUORANTHENE 75 3958278-1 LANCAS FLUORENE 87 3958278-1 LANCAS INDENO(1,2,3-CD)PYRENE 88 3958278-1 LANCAS NAPHTHALENE 85 3958278-1 LANCAS PHENANTHRENE 84 3958278-1 LANCAS PYRENE 84 3958278-1 LANCAS Matrix Spike Duplicate: 1-METHYLNAPHTHALENE 91 10 3958278-1 LANCAS 2-METHYLNAPHTHALENE 95 9 3958278-1 LANCAS ACENAPHTHENE 96 10 3958278-1 LANCAS ACENAPHTHYLENE 97 10 3958278-1 LANCAS ANTHRACENE 91 9 3958278-1 LANCAS BENZO(A)ANTHRACENE 97 10 3958278-1 LANCAS BENZO(A)PYRENE 99 10 3958278-1 LANCAS BENZO(B)FLUORANTHENE 94 8 3958278-1 LANCAS BENZO(G,H,I)PERYLENE 105 17 3958278-1 LANCAS SENZO(K)FLUORANTHENE 100 8 3958278-1 LANCAS CHRYSENE 95 11 3958278-1 LANCAS DIBENZ(A,H)ANTHRACENE 110 15 3958278-1 LANCAS FLUORANTHENE 83 8 3958278-1 LANCAS FLUORENE 98 11 3958278-1 LANCAS INDENO(1,2,3-CD)PYRENE 102 15 3958278-1 LANCAS NAPHTHALENE 93 10 3958278-1 LANCAS PHENANTHRENE 89 6 3958278-1 LANCAS PYRENE 98 13 3958278-1 LANCAS DEQ-CFW 00025444 Corporate Environmental Database Lab Analysis QAQC Report Location: mverTsx uc January 7, 2003 Project Name: Swmu8'2002 Page 4 Batch Identifier wetomu Number: oxLur7'ono/Prwp Method: oxLuFT-omVpre'prep: Batch Start Date: 13usc02 Instrument: 005388 Batch Number: 24 The following field samples are included in this batch: Date QC SagpLe Name Sameled! Lab Sampte ID Level Fmx m'sooLK-mwFow'wna 10nso02 3958316'1 mmcAs ou Result Unit MDL RPR RPD Lab SaMpLe ID Lab Control Spike: Tpo-oxo o$ Lco-1 LxwCAo Lob Control Spike Duplicate: rPx oeo 95 1 Lnom-1 Lxwcxo Method Blank: Tpo-neo wu us/L 25 BLANK-1 Lxwcxn Comments: coLur7'onn/8815 (TpV-uno): The matrix spike and spike duplicate were not performed due to insufficient sample. The Laboratory control oemp!c and control sample duplicate were analyzed to measure accuracy and precision at the batch |evci' Batch Identifier Method Number: cxLurT'onn/p,ep method: unLuFT-oxn/pre'prep: Batch Start Date: 17usc02 Instrument: 005386 Batch Number: 25 The following field samples are included in this botch: Date oc Sample Name Sampled Lab Sample ID Level Fx,'o-owmo06-01x(4'5) 10mcn02 3958278-1 wmCAm QC nn-S-owmu06'01x(4'5)'oup )noccVZ 3958279'1 mNcxo on AnalytelParameter Result Unit MDL RPR RPD Lab SampLe ID Lab Control Spike, rpx ' omo 68 Lcu'1 LAwcxo Method Blank: npx - oxo wo ws/ua 10 BLANK-1 LxwoxV Matrix Spike: TPo' mw 85 3958278-1 umoAS Matrix Spike Duplicate: A - f- U ^ ' ' I 1-44J. Noww%ow Lancagier , avoratories 7035-504103 00 2425 New Holland 0 Box 12425, Lancaster, PA 17605-2425 i Proiect Nurnter �DuPont Fayetti- 1 Facirity Name Togo no Number 9 Route 87 South Fayeftevillie NC 28302' Facility Address Transporter Addmss Bryan Heath Express Saver v-Supendo—r—.- Method of Shipft 'SWMU6 GW-2002 �rocess Producing Sample S p ec!��Ing Instructions MetEth Methanol; 8270 APPIX; Cl-, F- (300.0) QtherE21=s) Handling Sample Dmnpfion '[Bottles Relinquished by.#71-4*w�;h - ------r. - Condition of Samples Uporh arrival at Final Destination Ae elve un- jDaterrime c d byfl I LU IMWWAWW�Ifflm�l :Ii4u Temp, of Saff,19les 01 an Arrival .1 # 1* 4 MR I T' lif�14014ff-Till -- DEQ-CFW-00025446 t� ial�+lr Far; Lancaster, 760J �+?a � �' P � _ Cj t�IEJ' lJ v iai ii� tioJ(�r r't t b t h ? �"7 1 roe . �.,�..�7.f,3 T.. _.._. �°�., .. __.__......._ __._..__,._. _...._LL._.{_.— IL 04._a�,ti..., � _,a,Prai &.r s.. , �tT�i�trz„hntl,� h�lstrll��? i'arljir,•Iltl r ._ 1I ra^a -virte:r kddrocr, ; irn.tk>a('i 't•"i�ai:ii ,kr�:Xf:>i��a �7�v'�"i" s{ ..ilia.+ rUUa e,'ii ii#'.triiirl 'all �hii);sin t t:, I .., £•(s— F !"11 d ______ _,.ai... _. _.-..—-.......,..--.._...._....,,......_....,..-.. � n ti*V-4 1500 j tione 1. I L---=- - - --- --- _ _.. ,€_ rui��. ► � �� i yr. �{ 1 f,i iJl l,t(IJc) ItJk! 5) !)l t )ii_t!%ilLSe_ . OW Lsv1._Ltll yti+l;ll�ilJtj J�rt' �1 L�JJ l l�%i7� SWh25 None i_ I ��...__I_.._,...1__. t�1'�( t r Ni y t'�/uc v._Ili)ci---Sl^r jAGO `�— I hstyta i I t3 I I „f _ 7 StIMU6.01ft. )-Ms 1IZCt � 25 j 1 I ,' Q_VVML1B(s1 USED ._ I;jZjj tPLI,100 SR 1500 . .Mine .. 'r r _ '� t,. 442 ..__._... � r d n s _� r3 tr.rt it,IQ IDateff jr-oo i i baler i ii s to Bcltt(c.v t~'acwivzd ! a Ef��t� nettfi.u�t! a �a liras flirnF E E Recelt+an py Uaip-Illtil Ilcl71� fl Sa a :. _ ..:, ...F . : . i . J1. CM salts;: a aiw 4:Ct'Ji'll t)":;d s t L,ata.f hilt � U'- f^•, f DEQ-CFW 00025447 UI'7T1I"T.ArI= DATE: January 16, 2003 TO: Bryan Heath — URS Diamond FROM: Kelly Rinehimer RE: Analytical Data for Fayetteville Enclosed please find the report for the Fayetteville SW­W9-2002 project. As per the Fayetteville RCRA Phase I Work Plan, an equipment blank will be collected per day. Samples were collected on December 10; 2002 with no associated equipment blank. Please see report for other quality control issues. Please call with questions. I= DEQ-CFW-00025448 DuPont CRG Corporate 1 r e Database Preliminary Administration Review Project Verify •ir ►is Project Backstop Disk Deliverable Integrity QC Batch Integrity (Correct problems/Pull backstop as necessary) Completeness Check Samples X� 100% Tests X 100% Parameters 100% or X <100% Accuracy CED Results vs. Hard Copy Lab Reporl Comments/Narrative Review Laboratory i1 1 1 Review Report letter/titleCover o; customer Report 1 i Copy and s: f Mail to Client(s Kelly Rinehimer Certified by 1/16/03 Date DEQ-CFW 00025449 The following process is followed on all projects where data is delivered to the Corporate Environmental Database (CED) and a report is generated from the CED. All projects that bypass the CED (Le., are directly reported by a laboratory) do not receive the rigorous treatment presented below. Preliminary Administration To begin a report, the reporting coordinator checks out the file and updates the reporting schedule. A review of the project sheet is the next step to familiarize the coordinator with specifications and special instructions. Finally, the location and Jobname is either added, corrected, or verified to ensure all samples are properly identified as in the project. Project Backstop First, the backstop is used to check the disk deliverable integrity of all project data. This tool checks the CED readiness of the data. Second, quality control batch integrity is checked by the backstop. It is verified that all samples for each test have appropriate quality control samples attached. Completeness Check Data completeness is checked against project specifications. First, all sample points are identified as 100% complete. Then, all tests for each sample point are checked for 100% completeness. A parameter (or analyte) count is verified for each sample and test. A 100% parameter check and/or reporting threshold check can be done if requested in project specifications. The results reported by disk and located in the CED are checked against the hard copy laboratory reports for accuracy. This stage is a 100% check of the accuracy of the data. Comments/Narrative Review Three steps are included in the comments/narrative review. First, any comments made by the laboratory are located in the hard copy reports. Second, the quality control section(s) of the laboratory reports are reviewed for obvious quality control deficiencies (matrix spike or replicate outside control limits without appropriate comment). If questionable, the laboratory is contacted for verification. Finally, the appropriate comments are entered into the CED. A person familiar with the project (usually the customer service representative) reviews the completed report and the reviewer produces a cover letter. 0 The final step is to copy, bind, and mail the report to the client(s) in the format specified in the project if spec ications. d:\trmsfer\fom \fayettevillc\2002\cedcklst I doc DEQ-CFW-00025450 Corporate Environmental Lab Analysis Report Location: nnsTTsv/us January 16, 2003 Job Name: nwmu9-2002 page 1 u of c nmmp|eid: pAY'o-soaLm-owmu09uAr1 Sampling point/ sueLK-mwwo09omY1 Date o ied oecsmasm 9, 2002 Lab Sampte ID: 3958284'1 xnu!yoio Lab: Lxwcxm Sample Type: BLANK wxren QC Level: oc (Aoum QC Process) AnaLytelParameter Dilution Result Unit MDL POL Date Analyzed Prep/Method: 301OA/6010B coxonIum 1 wo u ms/L 0'0020 0'0050 Dec 13, 2002 Le«o 1 NO u mo/L 0.0089 0-0200 Dec 13, 2002 NICKEL 1 NO u Ms/L 8'0019 0-0050 Dec 13, 2002 Method: 8015B msrxxwoL (BY ozxscr IwJscrIow) 1 wu u uo/L 288' 1000' Dec 20, 2002 Surrogates: xcEToms 1 99'0 mpn Dec 20, 2002 1,1,1,2'rsTxAuoLnwosroxwE 1 wo u uo/L 1' 5' Dec 13, 3002 7,1,1-rwzcxc000s7muwE 1 NO u us/L 0,8 5- Dec 13, 2002 1,1,2,2'TsraxcxLoxocmAwE 1 NO u uo/L 1' 5' Dec 13, 2002 1,1,2'TmzcxLonosT*mws 1 wo o us/L 0.8 5' Dec 13, 2002 1,1-oIcxLomosroxNs 1 wo o us/L 1' 5' Dec 13, 2002 1,1-uIcxconosrocwc 1 wo u us/L 0'8 5- Dec YJ, 2082 1,2,3-7ozc*Loxopnnp*wE 1 wn u ua/L 1' 5' Dec 13, ZUUZ 1,2'oIVnomo-3-u*Lunornor*wE 1 wo u us/L 2' 5- Dec 13, 2002 1,2-oIomomosm*ws 1 wo u uG/L 1. 5' Dec 13, 2002 1,2-ozCoLoncmcwzswE 1 wm u uo/L 1' 5' Dec 13' 2002 1,2-mIoxLonnsm*we 1 wo u uo/L 1' 5' Dec 15, 3008 1,2-nIcxLomopRopwwc 1 NO u us/L 1' 5' Dec 13, 2002 1,3-oIcxLonoaewzEws 1 wo o 'uo/L 1' 5' Dec 13, 2002 1,4-oIcxLmmmasNcsws I wo o us/L 1' 5' Dec 13, 2002 1,4-uzoxAws 1 wm u uu/L 70' 250' Dec 13, 2002 2'murxwows 1 wo u oo/L 3' 10' Dec 13, 2002 2-,C*Lono-1,3-ooTxozsws 1 wo u uo/L 1' 5- Dec 13, 2002 z'xExwmnms 1 wo u ms/L ]' 10- Dec 13, 2002 4-METHYL-2 pewTxmowc 1 wn u mo/L 3' 10' Dec 13, 2002 AcE7ows 1 wn o os/L b' /O' Dec 13, 2002 AcsrowImILs 1 wo o us/L 25' 100' Dec 13, 2002 ALLYL uxLoozos 1 wo u um/L 1' 5. Dec 13, 2002 BEwzsws 1 wo u uG/L 0'5 5. Dec 13, 2002 enomonrcoLonoms/oxws 1 wo o um/L 1' 5. Dec 13, 2002 onomoponm 1 wo o ms/L 1' 5' Dec 13, 2002 anoMomsmAws 1 wo u uu/L 1' 5' Dec 13, 2002 cAnoow mIouLFzos 1 wu o us/L 1' 5' Dec 13, 2002 c*noom TsTnxCoLon/os 1 NO o us/L 1' 5' Dec 13, 2002 coLownaswZswE 1 wn u ua/L o'a 5' Dec 13, 2002 ooLomosrHANs 1 ww u ua/L 1' 5' Dec 13, 2002 coLonoFonm 1 wo u um/L 0.8 5' Dec 13, 2002 coLonomsTVAes I wn u us/L 1' 5' Dec 13, 2002 o;o-1,2-oIcoLoxosTncws 1 wn u uo/L 0'0 5' Dec 13, 2002 o/o'1 3'mzCxLowupmupsws 1 mo o us/L 1 ' 5 Deco�� �� 2002 o/mn�/mc��umomsrmvms 1 wo o us/� 1' ' s- Dec 13' 2002 o/ennMomsrHANs 1 wn u us/L 1' 5' Dec 13, 2002 oIuxLononzrLuonoMsTo*ws 1 wo u uu/L 2' 5' Dec 13, 2002 ETHYL msTowcnYLxTs 1 wo u mo/L 1' 5' Dec 13, 2002 sToYLaswzsws 1 wo u ua/L 0'8 5' Dec 13, 2002 InoeuT,L x0000L 1 wo u uu/L 100' 250' Dec 13, 2002 ms7xacmYLowz7erLs 1 wu o uo/L 10' 50' Dec 13, 2002 METHYL IooIos I wo u uu/L 1' s' Dec 13, ZVVa wsrxYL wsrownoYLxrc 1 wn u us/L 1' 5- Dec 13, 2002 mc7oYLsms coLox/ns 1 wo o uG/L o. 5' Dec 13, 2002 psw7xCxLomosrxxws 1 wu o us/L 1' 5' Dec 13, 2002 pxnpIuw/rx/Ls 1 wo u uo/L 30' 100' Dec 13, 2802 aTrmswE 1 wm u us/L 1' 5' Dec 13, 2002 rcraxcxLcmosTxsw* 1 wm u un/L O'o 5' Dec 13, 2002 TOLUENE 1 mo u us/L 0'7 5' Dec 13, 2002 Tn*wn'1'2-oIcxL000s7xswc 1 wn u om/L 0'8 5' Dec 13, 2002 roxwo 1,]'nICxLonoPnoPcws 1 wo u us/L 1. 5' Dec 13' 2002 mxws 1 4'o/cxLnno-2-ou/sws 1 wu u ms/� 15 ' 5U ' Dec 13' 2002 mIceLO�usrxews 1 wn u uo/L 1' s. Dec 132002 mIoxLnnnpLuonomeTxxwe 1 wo u uo/L 2' 5' Dec 13, 2002 VINYL acsrxre I wo o uo/L a' 10' Dec 13. 2002 VINYL coLox/os 1 wm u ua/L 1' n. Dec 13, 2002 xYLsws (TOTAL) 1 wm o uo/L u'u 5' Dec 13, 2002 OEQ-CFVV_00025451 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name- SWMU19-2002 C of C Sampleid: FAY-K-EQBLK-SWMU09DAY1 Sampling Point: EQBLK-SWMU09DAY1 Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3958264-1 Analysis Lab: LANCAS 'SampLe Type: BLANK WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution RPR ----------------- -------- --- Surrogates: 1,2-DICHLOROETHANE-D4 1 101.0 RPR 4-BROMOFLUOROBENZENE 1 99.0 RPR DIBROMOFLUOROMETHANE 1 103.0 RPR TOLUENE-D8 1 103.0 RP? Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 2 MEM, Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 DEQ-CFW-00025452 Corporate Environmental Database Lab Analysis Report Location; FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampleid: FAY-K-EQBLK-SWMU09DAY1-ACR Sampling Point: EQBLK-SWMU09DAYI Date Sampted: DECEMBER 9, 2002 Lab Sample ID: 3959518-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution Result Prep/Method: 503OB18260B ACROLEIN 1 ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 102.0 RPR 4-BROMOFLUOROBENZENE 1 96.0 RPR DIBROMOFLUOROMETHANE 1 101.0 RPR TOLUENE-D8 1 102.0 RPR Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 3 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 16, 2002 UG/L 4. 20. Dec 16, 2002 DEQ-CFW-00025453 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 16, 2003 Job Name: SWMU9-2002 Page 4 C of C SampLeid: FAY-K-EQBLK-SWMU9-DAY1 Sampling Point: EQBLK-SWMU9-DAY1 Date Sampled: DECEMBER 12, 2002 Lab Sample ID: 3960936-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 5030BZ82608 1,1,1,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,1,1-TRICHLOROETHANE I NO U UG/L 0.8 5. Dec 23, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 23, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,1-DICHLOR6ETHENE 1 ND U UG/L 0.8 5. Dec 23, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 NO U UG/L 2. 5. Dec 23, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROETHANE T ND U UGIL 1. 5. Dec 23, 2002 1,2-DICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 23, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 23, 2002 1,4-DIOXANE 1 ND U UG/L 70. 250. Dec 23, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 23, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 23, 2002 2-HEXANONE I ND U UG/L 3. 10. Dec 23, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 23, 2002 ACETONE 1 ND U UG/L 6. 20. Dec 23, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 23, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 23, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 23, 2002 BROMODICHLOROMETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 23, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 23, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 23, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 23, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 CHLOROFORM 1 NO U UG/L 0.8 5. Dec 23, 2002 CHLOROMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 CIS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 23, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 23, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 DICHLORODIFLUOROMETHANE 1 NO U UG/L 2. 5. Dec 23, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 23, 2002 ETHYLBENZENE 1 NO U UG/L 0.8 5. Dec 23, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 23, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 23, 2002 METHYL IODIDE 1 ND U UG/L 1. 5. Dec 23, 2002 METHYL METHACRYLATE I ND U UG/L 1. 5. Dec 23, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 23, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 PROPIONITRILE 1 NO U UG/L 30. 100. Dec 23, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 23, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 23, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 23, 2002 TRANS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 23, 2002 TRANS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 23, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 NO U UG/L 15. 50. Dec 23, 2002 TRICHLOROETHENE 1 ND U UG/L 1. 5. Dec 23, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 23, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 23, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 23, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 23, 2002 Surrogates: 1,2-DICHLOROETHANE-D4 1 105.0 RPR Dec 23, 2002 4-BROMOFLUOROBENZENE 1 96.0 RPR Dec 23, 2002 DIBROMOFLUOROMETHANE 1 102.0 RPR Dec 23, 2002 TOLUENE-D8 1 102.0 RPR Dec 23, 2002 Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025454 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampleid: FAY-G-MW-10D Sampling Point: MW-10D Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958262-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnatyteZParameter Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 301OA/6010B CHROMIUM 1 0.0572 MG/L 0.0020 0.0050 Dec 13, 2002 LEAD 1 0.190 MG/L 0.0089 0.0200 Dec 13, 2002 NICKEL 1 0.0189 MG/L 0.0019 0.0050 Dec 13, 2002 Method: 80158 METHANOL (BY DIRECT INJECTION) 1 NO U UG/L 200. 1000. Dec 20, 2002 Surrogates: ACETONE 1 98.0 RPR Dec 20, 2002 Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,1,2,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 13, 2002 1,2-DIBROMOETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,4-DIOXANE 1 ND U UG/L 70. 250. Dec 13, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 2-CHLORO-1,3-BUTADIENE 1 NO U UG/L 1. 5. Dec 13, 2002 2-HEXANONE 1 NO U UGIL 3. 10. Dec 13, 2002 4-METHYL-2-PENTANONE 1 NO U UG/L 3. 10. Dec 13, 2002 ACETONE 1 NO U UGIL 6. 20. Dec 13, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 13, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 13, 2002 BROMODICHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 BROMOFORM 1 NO U UG/L 1. 5. Dec 13, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CARBON DISULFIDE 1 NO U UG/L 1. 5. Dec 13, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 13, 2002 CHLOROBENZENE 1 NO U UG/L 0.8 5. Dec 13, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CIS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 13, 2002 DIBROMOCHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 DIBROMOMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 DICHLORODIFLUOROMETHANE 1 NO U UG/L 2. 5. Dec 13, 2002 ETHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 13, 2002 ETHYLBENZENE 1 NO U UG/L 0.8 5. Dec 13, 2002 ISOBUTYL ALCOHOL 1 NO U UG/L 100. 250. Dec 13, 2002 METHACRYLONITRILE 1 NO U UG/L 10. 50. Dec 13, 2002 METHYL IODIDE I ND U UG/L 1. 5. Dec 13, 2002 METHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 13, 2002 PENTACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 PROPIONITRILE 1 ND U UG/L 30- 100. Dec 13, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 13, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 13, 2002 TRANS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 TRANS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 13, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 13, 2002 TRICHLOROETHENE 1 NO U UG/L 1. 5. Dec 13, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 13, 2002 VINYL CHLORIDE 1 NO U UG/L 1. 5. Dec 13, 2002 XYLENE (TOTAL) 1 ND U UGIL 0.8 5. Dec 13, 2002 DEQ-CFW-00025455 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampteid: FAY-G-MW-10D Sampling Point: MW-IOD Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958262-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) AnaLyte/Parameter Dilution RPR ----------------- -------- --- Surrogates: 1,2-DICHLOROETHANE-D4 1 102.g 4-BROMOFLUOROBENZENE 1 96. DIBROMOFLUOROMETHANE 1 100.0 R TOLUENE-D8 1 103.0 R1 Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 6 Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 DEQ-CFW-00025456 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWML19-2002 C of C SampLeid: FAY-G-MW-10D-ACR Sampling Point: MW-IOD Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3959516-1 Analysis Lab: LANCAS SampLe Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution Result PrepZMethod: 503OB/82608 ACROLEIN 1 ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 103.0 RPR 4-BROMOFLUOROBENZENE 1 97.0 RPR DIBROMOFLUOROMETHANE 1 100.0 RPR TOLUENE-D8 1 101.0 RPR Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 7 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 16, 2002 UG/L 4. 20. Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 DEQ-CFW-00025457 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampteid: FAY-G-MW-12S Sampling Point: MW-12S Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3958263-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) Lab: LANCAS January 16, 2003 Page 8 AnaLyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 3010AI6010B CHROMIUM 1 0.0023 1 MG/L 0.0020 0.0050 Dec 13, 2002 LEAD I ND U MG/L 0.0089 0.0200 Dec 13, 2002 NICKEL 1 0.0038 1 MG/L 0.0019 0.0050 Dec 13, 2002 Method: 8015B METHANOL (BY DIRECT INJECTION) 1 ND U UG/L 200. 1000. Dec 20, 2002 Surrogates: ACETONE 1 97.0 RPR Dec 20, 2002 PrepZMethod: 5030BL8260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,1-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,2-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 13, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROETHANE I ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,3-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,4-DIOXANE 1 ND U UG/L 70. 250. Dec 13, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UGIL 1. 5. Dec 13, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 13, 2002 4-METHYL-2-PENTANONE I ND U UGIL 3. 10. Dec 13, 2002 ACETONE 1 ND U UG/L 6. 20. Dec 13, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 13, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 13, 2002 BROMODICHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 13, 2002 BROMOMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 13, 2002 DIBROMOCHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 13, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 13, 2002 METHYL IODIDE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 13, 2002 PENTACHLOROETHANE 1 ND U UGIL 1. 5. Dec 13, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 13, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 13, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 13, 2002 TRANS-1,2-DICHLOROETHENE I ND U UG/L 0.8 5. Dec 13, 2002 TRANS-1,3-bICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 13, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 13, 2002 TRICHLOROETHENE 1 ND U UG/L 1. 5. Dec 13, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 13, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 13, 2002 DEQ-CFW-00025458 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampteid: FAY-G-MW-12S Sampling Point: MW-12S Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3958263-1 Analysis Lab: LANCAS Sample Type- GROUND WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution RPR ----------------- -------- --- 1,2-DICHLOROETHANE-D4 1 103.0 RPX 4-BROMOFLUOROBENZENE 1 95.0 RPR DIBROMOFLUOROMETHANE 1 100.0 RPR TOLUENE-D8 1 103.0 RPR Qualifiers: U The constituent should be considered not detected. J The result is between MDL and PQL and should be considered an estimate. January 16, 2003 Page 9 Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 DEQ-CFW-00025459 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-G-MW-12S-ACR Sampling Point: MW-12S Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3959517-1 Analysis Lab: LANCAS Sample Type: GROUND WATER OC Level: OC (ADQM OC Process) AnatytelParameter Dilution Result Prep/Method: 5030BL8260B ACROLEIN 1 ND U ACRYLONITRILE 1 NO U Surrogates: 1,2-DICHLOROETHANE-D4 1 103.0 RPR 4-BROMOFLUOROBENZENE 1 97.0 RPR DIBROMOFLUOROMETHANE 1 96.0 RPR TOLUENE-D8 1 103.0 RPR Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 10 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 16, 2002 UG/L 4. 20. Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 DEQ-CFW-00025460 Corporate Environmental Database Lab Analysis Report Location: F*,sTrsvzus Job Name: owmu9-2002 c of o Lid: FA,-m'm+1S nemp\onn Point: MW-10 Date Sampled: oecsmaco 3, 2002 Lab Sample /o: 9955483-1 4^uivuiu Lab, L*wcxn Type:Sample GROUND WATER uc Level: QC (aoum nc Process) Dilution ResultPrep/Method: 301OA/6010B coRomzmM 1 0'0004 1 Lsmo 1 0'0145 1 wzoKcL Y 0'0089 January 18, 2003 Page 11 Unit MDL PQL Date Analyzed ws/L 0'0028 0'0050 Dec 12, 2002 mo/c 0'0089 0.0200 Dec 12, 2002 Ms/L 0'0019 0'0050 Dec 12, 2002 Comments: Meld personnel did not sign end/or date several of the cocs associated with nwMu09-2082 upon receipt of the Qualifiers: i The result is between MDL and POL and should be considered an estimate. OEQ-CFVV_00025461 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-G-MW-1S Sampling Point: MW-1S Date Sampled: DECEMBER 12, 2002 Lab Sample ID: 3960930-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) Lab: LANCAS January 16, 2003 Page 12 AnaLyteLParameter Dilution Result Unit MDL POL Date Analyze Method: 8015B METHANOL (BY DIRECT INJECTION) I ND U UG/L 200. 1000. Dec 30, 2002 Surrogates: ACETONE 1 106.0 RPR Dec 30, 2002 Prep/Method: 5030BL8260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 23, 2002 1,1,2,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 23, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,1-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 23, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 23, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,3-DICHLOROBENZENE I ND U UG/L 1. 5. Dec 23, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 23, 2002 1,4-DIOXANE 1 ND U UG/L 70. 250. Dec 23, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 23, 2002 2-CHLORO-1,3-BUTADIENE 1 NO U UG/L 1. 5. Dec 23, 2002 2-HEXANONE 1 NO U UG/L 3. 10. Dec 23, 2002 4-METHYL-2-PENTANONE 1 NO U UG/L 3. 10. Dec 23, 2002 ACETONE 1 NO U UG/L 6. 20. Dec 23, 2002 ACETONITRILE 1 NO U UG/L 25. 100. Dec 23, 2002 ALLYL CHLORIDE 1 NO U UG/L 1. 5. Dec 23, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 23, 2002 BROMODICHLOROMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 23, 2002 BROMOMETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 23, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 23, 2002 CHLOROBENZENE 1 NO U UG/L 0.8 5. Dec 23, 2002 CHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 CHLOROFORM 1 NO U UG/L 0.8 5. Dec 23, 2002 CHLOROMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 CIS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 23, 2002 CIS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 23, 2002 DIBROMOCHLOROMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 DIBROMOMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 23, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 23, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 23, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 23, 2002 METHACRYLONITRILE 1 NO U UGIL 10. 50. Dec 23, 2002 METHYL IODIDE 1 NO U UG/L 1. 5. Dec 23, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 23, 2002 METHYLENE CHLORIDE 1 NO U UG/L 2. 5. Dec 23, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 23, 2002 STYRENE 1 NO U UG/L 1. 5. Dec 23, 2002 TETRACHLOROETHENE 1 NO U UG/L 0.8 5. Dec 23, 2002 TOLUENE 1 NO U UG/L 0.7 5. Dec 23, 2002 TRANS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 23, 2002 TRANS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 23, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 23, 2002 TRICHLOROETHENE 1 NO U UG/L 1. 5. Dec 23, 2002 TRICHLOROFLUOROMETHANE I NO U UG/L 2. 5. Dec 23, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 23, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 23, 2002 XYLENE (TOTAL) 1 NO U UG/L 0.8 5. Dec 23, 2002 DEQ-CFW-00025462 Corporate Environmental Database Lab Analysis Report Location: FA«sTrsvIue January 18' ZVVI Job Name: owmu9-2002 Page 13 c of c i id: wn'o'mw'1n Sampling Point: MW-10 DateSampled: osoEMBam 12, 2002 Lob Sample ID: 3980990-1 xno(p,im Loh: mwcx» Type:Sample snouwo *A7sn QC Level: QC (ADQM QC Process) &noLyte/Poromwter Dilution RPR Date Analyzed 1,2-oxCHLOROETHANE-D4 1 103-0nPR nec23, 2002 4'BmomoFLuomnmEmZswE 1 97'0 mw Dec 23, 2002 nIVnoMnFLomoons7mme 1 102'0 npn Dec 23, 2002 roLocms'oG 1 100-0 npn Dec 29, 2002 Comments: 0015m (METHANOL (BY DzoscT zwJECT/nw)>: Sample was analyzed outside of hold time by four day(s) due to Laboratory prror' ouoiifiern: u The constituent should be considered not detected' Corporate Environmental, Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampteid: FAY-G-MW-IS-ACR Sampling Point: MW-1S Date Sampled: DECEMBER 12, 2002 Lab Sample ID: 3960931-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLyteZParameter Dilution Result Prep/Method: 5030BL8260B ACROLEIN 1 NO U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 96.0 RPR 4-BROMOFLUOROBENZENE 1 90.0 RPR DIBROMOFLUOROMETHANE 1 101.0 RPR TOLUENE-D8 1 92.0 RPR Qualifiers: U The constituent should be considered not detected. I January 16, 2003 Page 14 Unit MDL PQL Date Ana Lyzed UG/L 40. 100. Dec 17, 2002 UG/L 4. 20. Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 DEQ-CFW-00025464 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampleid: FAY-G-MW-2S Sampling Point: MW-2S Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3958258-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Lab: LANCAS January 16, 2003 Page 15 AnaLyteLParameter Dilution Result Unit MDL PQL Date Analyze Prep/Method: 3010AL6010B CHROMIUM 1 0.0023 1 MG/L 0.0020 0.0050 Dec 13, 2002 LEAD 1 0.0962 MG/L 0.0089 0.0200 Dec 13, 2002 NICKEL 1 0.0049 1 MG/L 0.0019 0.0050 Dec 13, 2002 Method: 80158 METHANOL (BY DIRECT INJECTION) I ND U UG/L 200. 1000. Dec 20, 2002 Surrogates: ACETONE 1 101.0 RPR Dec 20, 2002 Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 NO U UG/L 2. 5. Dec 13, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROPROPANE I NO U UG/L 1. 5. Dec 13, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1.4-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,4-DIOXANE 1 NO U UG/L 70. 250. Dec 13, 2002 2-BUTANONE 1 NO U UG/L 3. 10. Dec 13, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 13, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 13, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 ACETONE 1 NO U UG/L 6. 20. Dec 13, 2002 ACETONITRILE 1 NO U UG/L 25. 100. Dec 13, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 BENZENE 1 NO U UG/L 0.5 5. Dec 13, 2002 BROMODICHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 13, 2002 BROMOMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 13, 2002 CHLOROBENZENE 1 NO U UG/L 0.8 5. Dec 13, 2002 CHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CHLOROFORM 1 ND U UGIL 0.8 5. Dec 13, 2002 CHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CIS-1,3-DICHLOROPROPENE I ND U UG/L 1. 5. Dec 13, 2002 DIBROMOCHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 DICHLORODIFLUOROMETHANE I ND U UG/L 2. 5. Dec 13, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 ETHYLBENZENE 1 NO U UG/L 0.8 5. Dec 13, 2002 ISOBUTYL ALCOHOL 1 NO U UG/L 100. 250. Dec 13, 2002 METHACRYLONITRILE 1 NO U UG/L 10. 50. Dec 13, 2002 METHYL IODIDE 1 NO U UG/L 1. 5. Dec 13, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 13, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 13, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 PROPIONITRILE 1 NO U UG/L 30. 100. Dec 13, 2002 STYRENE I ND U UG/L 1. 5. Dec 13, 2002 TETRACHLOROETHENE I ND U UG/L 0.8 5. Dec 13, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 13, 2002 TRANS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TRANS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 13, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 NO U UG/L 15. 50. Dec 13, 2002 TRICHLOROETHENE 1 NO U UG/L 1. 5. Dec 13, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 13, 2002 VINYL CHLORIDE I ND U UG/L 1. 5. Dec 13, 2002 XYLENE (TOTAL) 1 NO U UG/L 0.8 5. Dec 13, 2002 DEQ-CFW-00025465 Lab Analysis Report Location: FAYsT7evIus Job Name: Swmu9'2002 C of o i id: wn's'mW'2o Sampling Point: Mw-2S DateSampled: oscsmos* 9, 2002 Lab Sample ID: 3958258-1 *na(vnio Lob: mwCAm Type:Sample GROUND WATER xna(yte/porometer Dilution xpn --- Surrogates: January 16, 2003 Page 16 Dec 13' anVa Dec 13, 2002 Dec 19, 2002 Comments: Field personnel wrote over the date and/or time of collection on some of the cucu associated with owmu09'2002 instead of lining out the mistake, dating and initialing the mistake and entering the correct infnrnmtinn' Qualifiers: u The constituent should be considered not detected' J The result is between moL and poL and ohouid be considered an estimate. Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampleid: FAY-G-MW-2S-ACR Sampling Point: MW-2S Date Sampled: DECEMBER 9, 2002 .Lab Sample ID: 3959512-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLytelParameter Dilution Result PrepZMethod: 5030818260B ACROLEIN 1 ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 103.0 RPR 4-BROMOFLUOROBENZENE 1 97.0 RPR DIBROMOFLUOROMETHANE 1 100.0 RPR TOLUENE-D8 1 103.0 RPR Qualifiers: U The constituent should be considered not detected. Unit MDL POL Date Analyzed UG/L 40. 100. Dec 14, 2002 UG/L 4. 20. Dec 14, 2002 Dec 14, 2002 Dec 14, 2002 Dec 14, 2002 Dec 14, 2002 DEQ-CFW-00025467 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampleid: FAY-G-MW-5D Sampling Point: MW-5D Date Sampled: DECEMBER 10, 2002 Lab Sampte ID: 3958259-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) January 16, 2003 Page 18 AnaLyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 3010AI6010B CHROMIUM 1 0.0028 1 MG/L 0.0020 0.0050 Dec 13, 2002 LEAD 1 0.0175 1 MG/L 0.0089 0.0200 Dec 13, 2002 NICKEL 1 0.0064 MG/L 0.0019 0.0050 Dec 13, 2002 Method: 80158 METHANOL (BY DIRECT INJECTION) 1 ND U UG/L 200. 1000. Dec 20, 2002 Surrogates: ACETONE 1 98.0 RPR Dec 20, 2002 Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,1-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,2-TRICHLOROETHANE I ND U UG/L 0.8 5. Dec 13, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1-DICHLOROETHENE I ND U UG/L 0.8 5. Dec 13, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 13, 2002 1,2-DIBROMOETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROBENZENE I ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROPROPANE I ND U UG/L 1. 5. Dec 13, 2002 1,3-DICHLOROBENZENE I ND U UG/L 1. 5. Dec 13, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,4-DIOXANE 1 NO U UG/L 70. 250. Dec 13, 2002 2-BUTANONE 1 NO U UG/L 3. 10. Dec 13, 2002 2-CHLORO-1,3-BUTADIENE 1 NO U UG/L 1. 5. Dec 13, 2002 2-HEXANONE 1 NO U UG/L 3. 10. Dec 13, 2002 4-METHYL-2-PENTANONE 1 NO U UG/L 3. 10. Dec 13, 2002 ACETONE 1 NO U UG/L 6. 20. Dec 13, 2002 ACETONITRILE 1 NO U UGA 25. 100. Dec 13, 2002 ALLYL CHLORIDE 1 NO U UG/L 1. 5. Dec 13, 2002 BENZENE 1 NO U UG/L 0.5 5. Dec 13, 2002 BROMODICHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 BROMOFORM I NO U UG/L 1. 5. Dec 13, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROBENZENE 1 NO U UG/L 0.8 5. Dec 13, 2002 CHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CIS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 CIS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 13, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 DIBROMOMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 ETHYL METHACRYLATE I ND U UG/L 1. 5. Dec 13, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 13, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 13, 2002 METHYL IODIDE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 13, 2002 PENTACHLOROETHANE 1 ND U UGIL 1. 5. Dec 13, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 13, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 13, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 13, 2002 TRANS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TRANS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 13, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 13, 2002 TRICHLOROETHENE 1 ND U UG/L 1. 5. Dec 13, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 13, 2002 VINYL CHLORIDE I ND U UG/L 1. 5. Dec 13, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 13, 2002 DEQ-CFW-00025468 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 16, 2003 Job Name: SWNU9-2002 Page 19 C of C Sampteid: FAY-G-MW-5D Sampling Point: MW-5D Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958259-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) AnaLyte/Parameter Dilution RPR Date Analyzed ----------------- -------- --- ------------- 1,2-DICHLOROETHANE-D4 1 102.0 RPR Dec 13, 2002 4-BROMOFLUOROBENZENE 1 101.0 RPR Dec 13, 2002 DIBROMOFLUOROMETHANE 1 100.0 RPR Dec 13, 2002 TOLUENE-D8 1 104.0 RPR Dec 13, 2002 Comments: Lab personnel received several broken vials for the samples collected as part of the SWMU09-2002 project. The Lab was able to run the requested analyses from the remaining vials. Qualifiers: U The constituent should be considered not detected. J The result is between MDL and POL and should be considered an estimate. DEQ-CFW-00025469 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampleid: FAY-G-MW-5D-ACR Sampling Point: MW-5D Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3959513-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution Result Prep/Method: 5030B/8260B ACROLEIN 1 ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 101.0 RPR 4-BROMOFLUOROBENZENE 1 97.0 RPR DIBROMOFLUOROMETHANE 1 100.0 RPR TOLUENE-D8 1 101.0 RPR Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 20 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 14, 2002 UG/L 4. 20. Dec 14, 2002 Dec 14, 2002 Dec 14, 2002 Dec 14, 2002 Dec 14, 2002 DEQ-CFW-00025470 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 16, 2003 Job Name: SWMU9-2002 Page 21 C of C Sampleid: FAY-G-MW-8S Sampling Point: MW-8S Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958260-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADOM OC Process) AnaLyteZParameter Dilution Result Unit MIL PQL Date Analyze Prep ZMethod: 3010AZ6010B CHROMIUM 9 0.155 MG/L 0.0020 0.0050 Dec 13, 2002 LEAD 1 0.0474 MG/L 0.0089 0.0200 Dec 13, 2002 NICKEL 1 0.0203 MG/L 0.0019 0.0050 Dec 13, 2002 Method: 8015B METHANOL (BY DIRECT INJECTION) I ND U UG/L 200. 1000. Dec 20, 2002 Surrogates: ACETONE 1 100.0 RPR Dec 20, 2002 Prep,/Method: 5030BL8260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,2-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 13, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,4-DIOXANE 1 ND U UG/L 70. 250. Dec 13, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 13, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 13, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 ACETONE 1 ND U UG/L 6. 20. Dec 13, 2002 ACETONITRILE 1 NO U UG/L 25. 100.1 Dec 13, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 13, 2002 BROMODICHLOROMETHANE 1 NO U UGIL 1. 5. Dec 13, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 13, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CARBON DISULFIDE 1 ND U UG/L 1- 5. Dec 13, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UGIL 1. 5. Dec 13, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5- Dec 13, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 ETHYLBENZENE 1 NO U UG/L 0.8 5. Dec 13, 2002 ISOBUTYL ALCOHOL 1 ND U UGIL 100. 250. Dec 13, 2002 METHACRYLONITRILE 1 NO U UG/L 10. 50. Dec 13, 2002 METHYL IODIDE 1 NO U UG/L 1. 5. Dec 13, 2002 METHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYLENE CHLORIDE 1 NO U UG/L 2. 5. Dec 13, 2002 PENTACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 13, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 13, 2002 TETRACHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 13, 2002 TRANS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 TRANS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 13, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 13, 2002 TRICHLOROETHENE 1 ND U UG/L 1. 5. Dec 13, 2002 TRICHLOROFLUOROMETHANE 1 NO U UGIL 2. 5. Dec 13, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 13, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 13, 2002 DEQ-CFW-00025471 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 16, 2003 Job Name: SWMU9-2002 Page 22 C of C Sampteid: FAY-G-MW-8S Sampling Point: MW-8S Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958260-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) AnaLyte/Parameter Dilution RPR Date Analyzed ----------------- -------- --- ------------- Surrogates: 1,2-DICHLOROETHANE-D4 1 104.0 RPR Dec 13, 2002 4-BROMOFLUOROBENZENE 1 97.0 RPR Dec 13, 2002 DIBROMOFLUOROMETHANE 1 101.0 RPR Dec 13, 2002 TOLUENE-D8 1 103.0 RPR Dec 13, 2002 Comments: Two different times of collection (i.e., 810/1035) were recorded for sample FAY-G-MW-8S on the COCs. Since the database only allows one time of collection per sample, the tab recorded the time as 1035. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025472 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-G-MW-8S-ACR Sampling Point: MW-8S Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3959514-1 Analysis Lab: LANCAS Sample Type: GROUND WATER ,QC Level: QC (ADQM QC Process) AnalyteZParameter Dilution Result PrepLMethod: 5030BZ8260B ACROLEIN 1 NO U ACRYLOMITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 104.0 RPR 4-BROMOFLUOROBENZENE 1 96.0 RPR DIBROMCIFLUOROMETHANE 1 102.0 RPR TOLUENE-D8 1 102.0 RPR Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 23 Unit MDL POL Date Analyzed UG/L 40. 100. Dec 14, 2002 UG/L 4. 20. Dec 14, 2002 j DEQ-CFW-00025473 Corporate Environmental Database Lab Analysis Report Location- FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-G-MW-8S-ACR-DUP Sampling Point: MW-8S Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3959515-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution Result Prep/Method: 5030818260B ACROLEIN 1 NO U ACRYLONITRILE 1 NO U Surrogates: 1,2-DICHLOROETHANE-D4 1 99.0 RPR 4-BROMOFLUOROBENZENE 1 98.0 RPR DIBROMOFLUOROMETHANE 1 98.0 RPR TOLUENE-D8 1 103.0 RPR Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 24 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 16, 2002 UG/L 4. 20. Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 DEQ-CFW-00025474 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 16, 2003 Job Name: SWMU9-2002 Page 25 C of C SampLeid: FAY-G-MW-8S-DUP Sampling Point: MW-8S Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958261-1 Analysis Lab: LANCAS 'Sample Type: GROUND WATER QC Level: QC (ADQM OC Process) Analyte/Parameter Dilution Result Unit MDL PQL Date Analyze Prep/Method: 3010AL6010B CHROMIUM 1 0.171 MG/L 0.0020 0.0050 Dec 13, 2002 LEAD 1 0.0486 MG/L 0.0089 0.0200 Dec 13, 2002 NICKEL 1 0.0194 MG/L 0.0019 0.0050 Dec 13, 2002 Method• 8015B METHANOL (BY DIRECT INJECTION) 1 ND U UG/L 200. 1000. Dec 20, 2002 Surrogates: ACETONE 1 97.0 RPR Dec 20, 2002 Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,1,2,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,1-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,1-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 1,2,3-TRICHLOROPROPANE 1 NO U UG/L. 1. 5. Dec 13, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 NO U UG/L 2. 5. Dec 13, 2002 1,2-DIBROMOETHANE I NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 13, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,4-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 13, 2002 1,4-DIOXANE 1 NO U UG/L 70. 250. Dec 13, 2002 2-BUTANONE 1 NO U UG/L 3. 10. Dec 13, 2002 2-CHLORO-1,3-BUTADIENE 1 NO U UG/L 1. 5. Dec 13, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 13, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 ACETONE 1 ND U UG/L 6. 20. Dec 13, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 13, 2002 ALLYL CHLORIDE 1 ND U UGIL 1. 5. Dec 13, 2002 BENZENE I NO U UG/L 0.5 5. Dec 13, 2002 BROMODICHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 BROMOFORM 1 NO U UG/L 1. 5. Dec 13, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CARBON DISULFIDE 1 NO U UG/L 1. 5. Dec 13, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 13, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROFORM 1 NO U UG/L 0.8 5. Dec 13, 2002 CHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 CIS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 13, 2002 CIS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 13, 2002 DIBROMOCHLOROMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 DIBROMOMETHANE 1 NO U UG/L 1. 5. Dec 13, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 13, 2002 METHACRYLONITRILE 1 NO U UG/L 10. 50. Dec 13, 2002 METHYL IODIDE 1 NO U UG/L 1. 5. Dec 13, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 13, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 13, 2002 PENTACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 13, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 13, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 13, 2002 TRANS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TRANS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 13, 2002 TRANS-1,4-DICHLORO-2-BUTENE I ND U UG/L 15. 50. Dec 13, 2002 TRICHLOROETHENE 1 NO U UG/L 1. 5. Dec 13, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 13, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 13, 2002 DEQ-CFW-00025475 Corporate Environmental ootobnme Lab Analysis Report Location: pxYsTTEVous January 10, 2003 Job Name: uwMu9-2002 Page 26 of C oampipid; FAY-u-mw-Ds-nup Sampling Point: Mw'8n Date Sampled: oECsmuse 10, ZOUZ Lab Sample ID: 3958261-1 Analysis Lab: Lwwo«o Sample Type: anuowo wmTen ou Level: oc (xoum uc p,oneno) e^aiyte/pu,emeter Dilution RPm Date Analyzed ourronateu: 1,2'oIcoLonosTHAws'n4 1 102.0 npn Dec 13, 2002 4-ouoMopLuonooENZsws 1 97.0 nPn Dec 13, 2002 DIVnnwopLuoxumcrHAwe 1 100-0 xpn Dec 13, 2002 Tocusws-m8 1 108'0 upx Dec 13, 2003 Comments: Two different times of collection (i.e., 810/10]5) were recorded for sample F*v's-mw-8o-oup on the coco' Since the database only allows one time of collection per sample, the Lau recorded the time as 1035' Qualifiers: Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-G-NAF4-ACR Sampling Point: NAK Date Sampled: DECEMBER 12, 2002 Lab Sample ID: 3960934-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) Analyte/Parameter Dilution Result Prep/Method 503OB/8260B ACROLEIN 1 ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 93.0 RPR 4-BROMOFLUOROBENZENE 1 90.0 RPR DIBROMOFLUOROMETHANE 1 100.0 RPR TOLUENE-D8 1 91.0 RPR Qualifiers: U The constituent should be considered not detected. January 16, 2003 Page 27 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 17, 2002 UG/L 4. 20. Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 DEQ-CFW-00025477 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-G-NAF4P-ACR Sampling Point: NAF4P Date Sampled: DECEMBER 12, 2002 Lab Sample ID: 3960935-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Levet: QC (ADGM QC Process) AnaLyte/Parameter Dilution Result PreplMethod: 5030BZ8260B ACROLEIN I ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 96.0 RPR 4-BROMOFLUOROBENZENE 1 89.0 RPR DIBROMOFLUOROMETHANE 1 100.0 RPR TOLUENE-D8 1 89.0 RPR Quatifiers: U The constituent should be considered not detected. January 16, 2003 Page 28 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 17, 2002 UG/L 4. 20. Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 DEQ-CFW-00025478 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 16, 2003 Job Name: SWML19-2002 Page 29 C of C Sampleid: FAY-K-TBLK-DAY2-SWMU09 Sampling Point: TBLK-DAY2-SWMU09 Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3958266-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADGM QC Process) Analyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Method• 8015B METHANOL (BY DIRECT INJECTION) 1 ND U UG/L 200. 1000. Dec 20, 2002 Surrogates: ACETONE 1 98.0 RPR Dec 20, 2002 Prep/Method: 5030BZ8260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,1-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1,2-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,1-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 13, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,2-DICHLOROETHANE 1 ND U UGIL 1. 5. Dec 13, 2002 1,2-DICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 13, 2002 1,3-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 13, 2002 1,4-DICHLOROBENZENE 1 ND U UGIL 1. 5. Dec 13, 2002 1,4-DIOXANE 1 ND U UG/L 70. 250. Dec 13, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 13, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 13, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 13, 2002 ACETONE 1 ND U UG/L 6. 20. Dec 13, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 13, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 13, 2002 BROMODICHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 13, 2002 BROMOMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 13, 2002 CHLOROMETHANE I ND U UG/L 1. 5. Dec 13, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 13, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 13, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 13, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 13, 2002 METHYL IODIDE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 13, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 13, 2002 PENTACHLOROETHANE 1 ND U UG/L 1. 5. Dec 13, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 13, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 13, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 13, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 13, 2002 TRANS-1,2-DICHLOROETHENE I ND U UG/L 0.8 5. Dec 13, 2002 TRANS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 13, 2002 TRANS-1,4-DICHLORO-2-BUTENE I ND U UG/L 15. 50. Dec 13, 2002 TRICHLOROETHENE 1 ND U UG/L 1. 5. Dec 13, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 13, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 13, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 13, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 13, 2002 DEQ-CFW-00025479 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-K-TBLK-DAY2-SWMU09 Sampling Point: TBLK-DAY2-SWMU09 Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3958266-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution RPR ----------------- -------- --- Surrogates: DICHLOROETHANE-D4 1 103.0 REM 4-BROMOFLUOROBENZENE 1 99.0 R D I BROMOFLLX)ROMETHANE 1 100.0 Rl' TOLUENE-D8 1 104.0 R * January 16, 2003 Page 30 Date Analyzed ------------- Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 Comments: Field personnel did not include the date/time of collection for the trip blanks on COCs 65502/65576. Since these fields are required in the database, the Lab entered the earliest date/time of the associated sample. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025480 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C SampLeid: FAY-K-TBLK-DAY2-SWMU09-ACR Sampling Point: TBLK-DAY2-SWMU09 Date Sampled: DECEMBER 9, 2002 Lab Sample ID: 3959519-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: OC (ADQM QC Process) AnaLyte/Parameter Dilution Result Prep/Method: 5030BL8260B ACROLEIN 1 ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 101.0 RPR 4-BROMOFLUOROBENZENE 1 98.0 RPR DIBROMOFLUOROMETHANE 1 98.0 RPR TOLUENE-D8 1 102.0 RPR January 16, 2003 Page 31 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 16, 2002 UG/L 4. 20. Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Dec 16, 2002 Comments: Lab personnel did not analyze sample FAY-K-TBLK-DAY1-SWMU09 since two trip blanks were received in the same cooler. -TBLK-DAY2-SWMU09 was analyzed for voLatiLes. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025481 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 16, 2003 Jab Name: SWMU9-2002 Page 32 C of C Sampleid: FAY-K-TBLK-NAFGW-4 Sampling Point: TBLK-NAFGW-4 Date Sampled: DECEMBER 12, 2002 Lab Sample ID: 3960932-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution Result Unit MDL PDL Date Analyzed PrepZ ethod: 503OB182608 1,1,1,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 23, 2002 1,1,2,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 23, 2002 1,1-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,1-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 23, 2002 1,2,3-TRICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 23, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 NO U UG/L 2. 5. Dec 23, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,2-DICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 23, 2002 1,3-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 23, 2002 1,4-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 23, 2002 1,4-DIOXANE 1 NO U UG/L 70. 250. Dec 23, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 23, 2002 2-CHLORO-1,3-BUTADIENE 1 NO U UG/L 1. 5. Dec 23, 2002 2-HEXANONE 1 NO U UG/L 3. 10. Dec 23, 2002 4-METHYL-2-PENTANONE 1 NO U UG/L 3. 10. Dec 23, 2002 ACETONE 1 NO U UG/L 6. 20. Dec 23, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 23, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 23, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 23, 2002 BROMODICHLOROMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 BROMOFORM 1 NO U UG/L 1. 5. Dec 23, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 CARBON DISULFIDE 1 NO U UG/L 1. 5. Dec 23, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 23, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 23, 2002 CHLOROETHANE 1 NO U UGIL 1. 5. Dec 23, 2002 CHLOROFORM 1 NO U UG/L 0.8 5. Dec 23, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 CIS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 23, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 23, 2002 DIBROMOCHLOROMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 DIBROMOMETHANE 1 NO U UG/L 1. 5. Dec 23, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 23, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 23, 2002 ETHYLBENZENE 1 NO U UG/L 0.8 5. Dec 23, 2002 ISOBUTYL ALCOHOL 1 NO U UG/L 100. 250. Dec 23, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 23, 2002 METHYL IODIDE 1 NO U UG/L 1. 5. Dec 23, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 23, 2002 METHYLENE CHLORIDE 1 NO U UG/L 2. 5. Dec 23, 2002 PENTACHLOROETHANE 1 ND U UG/L 1. 5. Dec 23, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 23, 2002 STYRENE 1 NO U UG/L 1. 5. Dec 23, 2002 TETRACHLOROETHENE 1 NO U UG/L 0.8 5. Dec 23, 2002 TOLUENE 1 NO U UGIL 0.7 5. Dec 23, 2002 TRANS-I,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 23, 2002 TRANS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 23, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 23, 2002 TRICHLOROETHENE 1 NO U UG/L 1. 5. Dec 23, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 23, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 23, 2002 VINYL CHLORIDE 1 NO U UG/L 1. 5. Dec 23, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 23, 2002 Surrogates: 1,2-DICHLOROETHANE-D4 1 105.0 RPR Dec 23, 2002 4-BROMOFLUOROBENZENE 1 95.0 RPR Dec 23, 2002 DIBROMOFLUOROMETHANE 1 101.0 RPR Dec 23, 2002 TOLUENE-D8 1 101.0 RPR Dec 23, 2002 Qualifiers: U The constituent should be considered not detected. DEQ-CFW 00025482 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU9-2002 C of C Sampleid: FAY-K-TBLK-NAFGW-4-ACR Sampling Point: TBLK-NAFGW-4 Date Sampled: DECEMBER 12, 2002 Lab Sample ID: 3960933-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADGM QC Process) AnaLyte/Parameter Dilution Result Prep/Method: 503OB18260B ACROLEIN I ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 95.0 RPR 4-BROMOFLUOROBENZENE 1 94.0 RPR DIBROMOFLUOROMETHANE 1 101.0 RPR TOLUENE-D8 1 95.0 RPR Qualifiers: U The constituent should be considered not detected. 11< Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 17, 2002 UG/L 4. 20. Dec 17, 2002 Dec 17, 2002 Dec 17, 2002 Dec 17,2002 Dec 17, 2002 DEQ-CFW-00025483 Corporate Environmental Database Lab Analysis Report Summary of Positive Results Location: FAYETTEVILLE January 16, 2003 Job Name: SWML19-2002 Page I AnalyteZParameter Result Unit MDL POL Method No. Sampling Point: MW-IOD C of C Sampleid: FAY-G-MW-10D Date Sampled: Dec 10, 2002 Sample Type: GROUND WATER QC Level: QC MOM QC Process) CHROMIUM 0.0572 MG/L 0.0020 0.0050 6010B LEAD 0.190 MG/L 0.0089 0.0200 6010B NICKEL 0.0189 MG/L 0.0019 0.0050 6010B Sampling Point: MW-12S C of C Sampleid: FAY-G-MW-12S Date Sampled: Dec 9, 2002 Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) CHROMIUM 0.0023 J MG/L 0.0020 0.0050 6010B NICKEL 0.0038 1 MG/L 0.0019 0.0050 6010B Sampling Point: MW-IS C of C Sampleid: FAY-G-MW1-1S Date Sampled: Dec 3, 2002 Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) CHROMIUM 0.0034 J MG/L 0.0020 0.0050 60108 LEAD 0.0145 J MG/L 0.0089 0.0200 6010B NICKEL 0.0089 MG/L 0.0019 0.0050 60108 Sampling Point: MW-2S C of C Sampleid: FAY-G-MW-2S Date Sampled: Dec 9, 2002 Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) CHROMIUM 0.0023 J MG/L 0.0020 0.0050 6010B LEAD 0.0962 MG/L 0.0089 0.0200 6010B NICKEL 0.0049 1 MG/L 0.0019 0.0050 6010B Sampling Point: MW-5D C of C Sampleid: FAY-G-MW-5D Date Sampled: Dec 10, 2002 Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) CHROMIUM 0.0028 1 MG/L 0.0020 0.0050 6010B LEAD 0.0175 J MG/L 0.0089 0.0200 6010B NICKEL 0.0064 MG/L 0.0019 0.0050 6010B Sampling Point: MW-8S C of C Sampleid: FAY-G-MW-8S Date Sampled: Dec 10, 2002 Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) CHROMIUM 0.155 MG/L 0.0020 0.0050 6010B LEAD 0.0474 MG/L 0.0089 0.0200 6010B NICKEL 0.0203 MG/L 0.0019 0.0050 6010B Sampling Point: MW-8S C of C Sampleid: FAY-G-MW-8S-DUP Date Sampled: Dec 10, 2002 Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) CHROMIUM 0.171 MG/L 0.0020 0.0050 6010B LEAD 0.0486 MG/L 0.0089 0.0200 6010B NICKEL 0.0194 MG/L 0.0019 0.0050 6010B DEQ-CFW-00025484 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 January 16, 2003 Page 1 Batch identifier Method Number: 6010B Prep Method: 3010A Pre -prep: Batch Start Date: 11DECO2 Instrument: 005478 Batch Number: 5 The following'field samples are included in this batch: Date QC Sample Name Sa led Lab Sample ID Level FAY-G-MW-lS 03DECO2 3955463-1 LANCAS 0C AnaLyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control. Spike: CHROMIUM 103 LCS-1 LANCAS LEAD 101 LCS-1 LANCAS NICKEL 101 LCS-1 LANCAS Method Blank: CHROMIUM ND MG/L .002 BLANK-1 LANCAS LEAD ND MG/L .0089 BLANK-1 LANCAS NICKEL ND MG/L .0019 BLANK-1 LANCAS Matrix Spike: CHROMIUM 110 3955464-1 LANCAS LEAD 101 3955464-1 LANCAS NICKEL 103 3955464-1 LANCAS Matrix Spike Duplicate: CHROMIUM 105 4 3955464-1 LANCAS LEAD 103 2 3955464-1 LANCAS NICKEL 101 1 3955464-1 LANCAS Replicate: CHROMIUM 0.0186 MG/L 0 3955464-1 LANCAS LEAD 0.0105 MG/L 0 3955464-1 LANCAS NICKEL 0.0164 MG/L 0 3955464-1 LANCAS Batch Identifier Method Number: 6010B Prep Method: 3010A Pre -prep: Batch Start Date: 12DECO2 Instrument: 005478 Batch Number: 5 The following field samples are included in this batch: Date 0C Sample Name Sampled Lab Sample ID Level FAY-G-MW-10D 10DECO2 3958262-1 LANCAS QC FAY-G-MW-12S 09DECO2 3958263-1 LANCAS QC FAY-G-MW-2S 09DECO2 3958258-1 LANCAS QC FAY-G-MW-5D 10DECO2 3958259-1 LANCAS QC FAY-G-MW-8S 10DECO2 3958260-1 LANCAS QC FAY-G-MW-8S-DUP 10DECO2 3958261-1 LANCAS QC FAY-K-EQBLK-SWMU09DAY1 09DECO2 3958264-1 LANCAS QC AnalyteLParameter Result Unit MDL RPR RPD Lab Sample ID Lab Control. Spike: CHROMIUM 102 LCS-1 LANCAS LEAD 101 LCS-1 LANCAS NICKEL 103 LCS-1 LANCAS Method Blank: CHROMIUM ND MG/L .002 BLANK-1 LANCAS LEAD ND MG/L .0089 BLANK-1 LANCAS NICKEL ND MG/L .0019 BLANK-1 LANCAS DEQ-CFW-00025485 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 (Batch continued from previous page) Analvte/Parameter Matrix Spike: CHROMIUM LEAD NICKEL Matrix Spike Duplicate: CHROMIUM LEAD NICKEL Replicate: CHROMIUM LEAD NICKEL Result Unit MDL 0.132 MG/L 0.0376 MG/L 0.0148 MG/L RPR RPD Lab Sample ID 102 3958260-1 LANCAS 101 3958260-1 LANCAS 105 3958260-1 LANCAS 101 1 3958260-1 LANCAS 101 0 3958260-1 LANCAS 104 1 3958260-1 LANCAS 16 3958260-1 LANCAS 0 3958260-1 LANCAS 0 3958260-1 LANCAS Comments: 6010B (NICKEL): The result for the original sample or the replicate was less than five times the PQL. The difference between the results was outside +/- the PQL. Batch Identifier Method Number: 8015B Prep Method: Pre -prep: Batch Start Date: 19DECO2 Instrument: 002739 Batch Number: 25 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-MW-10D 10DECO2 3958262-1 LANCAS QC FAY-G-MW-12S 09DECO2 3958263-1 LANCAS QC FAY-G-MW-2S 09DECO2 3958258-1 LANCAS QC FAY-G-MW-5D 10DECO2 3958259-1 LANCAS QC FAY-G-MW-8S 10DECO2 3958260-1 LANCAS QC FAY-G-MW-8S-DUP 10DECO2 3958261-1 LANCAS QC FAY-K-EQBLK-SWMU09DAY1 09DECO2 3958264-1 LANCAS QC FAY-K-TBLK-DAY2-SWMU09 09DECO2 3958266-1 LANCAS QC Analvte/Parameter Lab Control Spike: METHANOL (BY DIRECT INJECTION) Method Blank: METHANOL (BY DIRECT INJECTION) Matrix Spike: METHANOL (BY DIRECT INJECTION) Matrix Spike Duplicate: METHANOL (BY DIRECT INJECTION) Batch Identifier Method Number: 8015B Prep Method: Batch Start Date: 30DECO2 Instrument: 002739 Batch Number: 14 Result Unit MDL ND UG/L 200 RPR RPD Lab Sample ID 96 LCS-1 LANCAS BLANK-1 LANCAS 96 3958260-1 LANCAS 100 4 3958260-1 LANCAS The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-MW-1S 12DECO2 3960930-1 LANCAS QC DEQ-CFW 00025486 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 (Batch continued from previous page) AnaLyte/Parameter Lab Control Spike: METHANOL (BY DIRECT INJECTION) Method Blank: METHANOL (BY DIRECT INJECTION) Matrix Spike: METHANOL (BY DIRECT INJECTION) Matrix Spike Duplicate: METHANOL (BY DIRECT INJECTION) Result Unit ND UG/ L January 16, 2003 Page 3 MDL RPR RPD Lab Sample ID 96 LCS-1 LANCAS 200 BLANK-1 LANCAS 92 3960930-1 LANCAS 92 0 3960930-1 LANCAS Batch identifier Method Number: 8260B Prep Method: 5030B Pre -prep: Batch Start Date: 12DECO2 Instrument: 067200 Batch Number: 2 The following field samples are included in this batch: Date QC Sample Name Sag!pLed Lab Sample ID Level FAY-G-MW-10D 10DECO2 3958262-1 LANCAS 0C FAY-G-MW-12S 09DECO2 3958263-1 LANCAS 0C FAY-G-MW-2S 09DECO2 3958258-1 LANCAS QC FAY-G-MW-5D IODECO2 3958259-1 LANCAS QC FAY-G-MW-8S 10DECO2 3958260-1 LANCAS 0C FAY-G-MW-8S-DUP 10DECO2 3958261-1 LANCAS QC FAY-K-EQBLK-SWMU09DAY1 09DECO2 3958264-1 LANCAS QC FAY-K-TBLK-DAY2-SWMU09 09DECO2 3958266-1 LANCAS QC AnaLyteLParameter Result Unit MDL RPR gRPD Lab Sample ID Lab Control Spike: 1,1,1,2-TETRACHLOROETHANE 97 LCS-1 LANCAS 1,1,1-TRICHLOROETHANE 86 LCS-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 118 LCS-1 LANCAS 1,1,2-TRICHLOROETHANE 103 LCS-1 LANCAS 1,1-DICHLOROETHANE 110 LCS-1 LANCAS 1,1-DICHLOROETHENE 94 LCS-1 LANCAS 1,2,3-TRICHLOROPROPANE 105 LCS-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 101 LCS-1 LANCAS 1,2-DIBROMOETHANE 103 LCS-1 LANCAS 1,2-DICHLOROBENZENE 96 LCS-1 LANCAS 1,2-DICHLOROETHANE 101 LCS-1 LANCAS 1,2-DICHLOROPROPANE 112 LCS-1 LANCAS 1,3-DICHLOROBENZENE 94 LCS-1 LANCAS 1,4-DICHLOROBENZENE 96 LCS-1 LANCAS 1,4-DIOXANE 109 LCS-1 LANCAS 2-BUTANONE 114 LCS-1 LANCAS 2-CHLORO-1,3-BUTADIENE 101 LCS-1 LANCAS 2-HEXANONE 108 LCS-1 LANCAS 4-METHYL-2-PENTANONE 107 LCS-1 LANCAS ACETONE 105 LCS-1 LANCAS ACETONITRILE 105 LCS-1 LANCAS ACROLEIN 98 LCS-1 LANCAS ACRYLONITRILE 101 LCS-1 LANCAS ALLYL CHLORIDE 93 LCS-1 LANCAS BENZENE 109 LCS-1 LANCAS BROMODICHLOROMETHANE 101 LCS-1 LANCAS BROMOFORM 90 LCS-1 LANCAS BROMOMETHANE 81 LCS-1 LANCAS CARBON DISULFIDE 110 LCS-1 LANCAS CARBON TETRACHLORIDE 84 LCS-1 LANCAS CHLOROSENZENE 100 LCS-1 LANCAS CHLOROETHANE 91 LCS-1 LANCAS CHLOROFORM 104 LCS-1 LANCAS CHLOROMETHANE 101 LCS-1 LANCAS CIS-1,2-DICHLOROETHENE 101 LCS-1 LANCAS CIS-1,3-DICHLOROPROPENE 106 LCS-1 LANCAS DIBROMOCHLOROMETHANE 99 LCS-1 LANCAS DIBROMOMETHANE 102 LCS-1 LANCAS DEQ-CFW-00025487 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 16, 2003 Project Name. SWMU9-2002 Page 4 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: DICHLORODIFLUOROMETHANE 83 LCS-1 LANCAS ETHYL METHACRYLATE 104 LCS-1 LANCAS ETHYLBENZENE 94 LCS-1 LANCAS ISOBUTYL ALCOHOL 115 LCS-1 LANCAS METHACRYLONITRILE 114 LCS-1 LANCAS METHYL IODIDE 93 LCS-1 LANCAS METHYL METHACRYLATE 101 LCS-1 LANCAS METHYLENE CHLORIDE 101 LCS-1 LANCAS PENTACHLOROETHANE 85 LCS-1 LANCAS PROPIONITRILE 120 LCS-1 LANCAS STYRENE 94 LCS-1 LANCAS TETRACHLOROETHENE 88 LCS-1 LANCAS TOLUENE 99 LCS-1 LANCAS TRANS-1,2-DICHLOROETHENE 96 LCS-1 LANCAS TRANS-1,3-DICHLOROPROPENE 100 LCS-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE 103 LCS-1 LANCAS TRICHLOROETHENE 98 LCS-1 LANCAS TRICHLOROFLUOROMETHANE 70 LCS-1 LANCAS VINYL ACETATE 121 LCS-1 LANCAS VINYL CHLORIDE 92 LCS-1 LANCAS XYLENE (TOTAL) 96 LCS-1 LANCAS Method Blank: 1,1,1,2-TETRACHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1,1-TRICHLOROETHANE NO UG/L .8 BLANKA-1 LANCAS 1,1,2,2-TETRACHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1,2-TRICHLOROETHANE NO UG/L .8 BLANKA-1 LANCAS 1,1-DICHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS 1,2,3-TRICHLOROPROPANE NO UG/L 1 BLANKA-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE NO UG/L 2 BLANKA-1 LANCAS 1,2-DIBROMOETHANE NO UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROBENZENE NO UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROPROPANE NO UG/L 1 BLANKA-1 LANCAS 1,3-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,4-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,4-DIOXANE ND UG/L 70 BLANKA-1 LANCAS 2-BUTANONE ND UG/L 3 BLANKA-1 LANCAS 2-CHLORO-1,3-BUTADIENE ND UG/L 1 BLANKA-1 LANCAS 2-HEXANONE ND UG/L 3 BLANKA-1 LANCAS 4-METHYL-2-PENTANONE ND UG/L 3 BLANKA-1 LANCAS ACETONE ND UG/L 6 BLANKA-1 LANCAS ACETONITRILE ND UG/L 25 BLANKA-1 LANCAS ACROLEIN NO UG/L 40 BLANKA-1 LANCAS ACRYLONITRILE ND UG/L 4 BLANKA-1 LANCAS ALLYL CHLORIDE NO UG/L 1 BLANKA-1 LANCAS BENZENE NO UG/L .5 BLANKA-1 LANCAS BROMODICHLOROMETHANE NO UG/L 1 BLANKA-1 LANCAS BROMOFORM NO UG/L 1 BLANKA-1 LANCAS BROMOMETHANE NO UG/L 1 BLANKA-1 LANCAS CARBON DISULFIDE NO UG/L 1 BLANKA-1 LANCAS CARBON TETRACHLORIDE NO UG/L 1 BLANKA-1 LANCAS CHLOROBENZENE NO UG/L .8 BLANKA-1 LANCAS CHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS CHLOROFORM ND UG/L .8 BLANKA-1 LANCAS CHLOROMETHANE ND UG/L 1 BLANKA-1 LANCAS CIS-1,2-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS CIS-1,3-DICHLOROPROPENE ND UG/L 1 BLANKA-1 LANCAS DIBROMOCHLOROMETHANE ND UG/L 1 BLANKA-1 LANCAS DIBROMOMETHANE ND UG/L 1 BLANKA-1 LANCAS DICHLORODIFLUOROMETHANE ND UG/L 2 BLANKA-1 LANCAS ETHYL METHACRYLATE ND UG/L 1 BLANKA-1 LANCAS ETHYLBENZENE ND UG/L .8 BLANKA-1 LANCAS ISOBUTYL ALCOHOL NO UG/L 100 BLANKA-1 LANCAS METHACRYLONITRILE ND UG/L 10 BLANKA-1 LANCAS METHYL IODIDE NO UG/L 1 BLANKA-1 LANCAS METHYL METHACRYLATE NO UG/L 1 BLANKA-1 LANCAS METHYLENE CHLORIDE ND UG/L 2 BLANKA-1 LANCAS PENTACHLOROETHANE NO UG/L 1 BLANKA-1 LANCAS PROPIONITRILE NO UG/L 30 BLANKA-1 LANCAS DEQ-CFW 00025488 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 (Batch continued from previous page) January 16, 2003 Page 5 AnaLyte/Parameter Result Unit MDL RPR RPD Lab SaMpLe ID Method Blank: STYRENE ND UG/L 1 BLANKA-1 LANCAS TETRACHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS TOLUENE ND UG/L .7 BLANKA-1 LANCAS TRANS-1,2-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS TRANS-I,3-DICHLOROPROPENE ND UG/L 1 BLANKA-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE ND UG/L 15 BLANKA-1 LANCAS TRICHLOROETHENE ND UG/L 1 BLANKA-1 LANCAS TRICHLOROFLUOROMETHANE ND UG/L 2 BLANKA-1 LANCAS VINYL ACETATE NO UG/L 2 BLANKA-1 LANCAS VINYL CHLORIDE ND UG/L 1 BLANKA-1 LANCAS XYLENE (TOTAL) ND UG/L .8 BLANKA-1 LANCAS Matrix Spike: 1,1,1,2-TETRACHLOROETHANE 98 3958260-1 LANCAS 1,1,1-TRICHLOROETHANE 96 3958260-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 121 3958260-1 LANCAS 1,1,2-TRICHLOROETHANE 105 3958260-1 LANCAS 1,1-DICHLOROETHANE 118 3958260-1 LANCAS 1,1-DICHLOROETHENE 106 3958260-1 LANCAS 1,2,3-TRICHLOROPROPANE 109 3958260-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 96 3958260-1 LANCAS 1,2-DIBROMOETHANE 105 3958260-1 LANCAS 1,2-DICHLOROBENZENE 101 3958260-1 LANCAS 1,2-DICHLOROETHANE 109 3958260-1 LANCAS 1,2-DICHLOROPROPANE 120 3958260-1 LANCAS 1,3-DICHLOROBENZENE 99 3958260-1 LANCAS 1,4-DICHLOROBENZENE 100 3958260-1 LANCAS 1,4-DIOXANE 109 3958260-1 LANCAS 2-BUTANONE 112 3958260-1 LANCAS 2-CHLORO-1,3-BUTADIENE 115 3958260-1 LANCAS 2-HEXANONE 108 3958260-1 LANCAS 4-METHYL-2-PENTANONE 110 3958260-1 LANCAS ACETONE 95 3958260-1 LANCAS ACETONITRILE 110 3958260-1 LANCAS ACROLEIN 94 3958260-1 LANCAS ACRYLONITRILE 105 3958260-1 LANCAS ALLYL CHLORIDE 110 3958260-1 LANCAS BENZENE 118 3958260-1 LANCAS BROMODICHLOROMETHANE 106 3958260-1 LANCAS BROMOFORM 91 3958260-1 LANCAS BROMOMETHANE 84 3958260-1 LANCAS CARBON DISULFIDE 119 3958260-1 LANCAS CARBON TETRACHLORIDE 97 3958260-1 LANCAS CHLOROBENZENE 107 3958260-1 LANCAS CHLOROETHANE 99 3958260-1 LANCAS CHLOROFORM 109 3958260-1 LANCAS CHLOROMETHANE 108 3958260-1 LANCAS CIS-1,2-DICHLOROETHENE 107 3958260-1 LANCAS CIS-1,3-DICHLOROPROPENE 110 3958260-1 LANCAS DIBROMOCHLOROMETHANE 99 3958260-1 LANCAS DIBROMOMETHANE 106 3958260-1 LANCAS DICHLORODIFLUOROMETHANE 96 3958260-1 LANCAS ETHYL METHACRYLATE 107 3958260-1 LANCAS ETHYLBENZENE 102 3958260-1 LANCAS ISOBUTYL ALCOHOL 118 3958260-1 LANCAS METHACRYLONITRILE 118 3958260-1 LANCAS METHYL IODIDE 95 3958260-1 LANCAS METHYL METHACRYLATE 105 3958260-1 LANCAS METHYLENE CHLORIDE 103 3958260-1 LANCAS PENTACHLOROETHANE 86 3958260-1 LANCAS PROPIONITRILE 119 3958260-1 LANCAS STYRENE 96 3958260-1 LANCAS TETRACHLOROETHENE 95 3958260-1 LANCAS TOLUENE 108 3958260-1 LANCAS TRANS-1,2-DICHLOROETHENE 103 3958260-1 LANCAS TRANS-I,3-DICHLOROPROPENE 102 3958260-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE 102 3958260-1 LANCAS TRICHLOROETHENE ill 3958260-1 LANCAS TRICHLOROFLUOROMETHANE 79 3958260-1 LANCAS VINYL ACETATE 128 3958260-1 LANCAS VINYL CHLORIDE 101 3958260-1 LANCAS DEQ-CFW 00025489 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike: XYLENE (TOTAL) 98 3958260-1 LANCAS Matrix Spike Duplicate: 1,1,1,2-TETRACHLOROETHANE 95 3 3958260-1 LANCAS 1,1,1-TRICHLOROETHANE 94 2 3958260-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 116 5 3958260-1 LANCAS 1,1,2-TRICHLOROETHANE 103 2 3958260-1 LANCAS 1,1-DICHLOROETHANE 121 3 3958260-1 LANCAS 1,1-DICHLOROETHENE 107 1 3958260-1 LANCAS 1,2,3-TRICHLOROPROPANE 105 3 3958260-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 95 1 3958260-1 LANCAS 1,2-DIBROMOETHANE 103 2 3958260-1 LANCAS 1,2-DICHLOROBENZENE 91 10 3958260-1 LANCAS 1,2-DICHLOROETHANE 109 0 3958260-1 LANCAS 1,2-DICHLOROPROPANE 117 3 3958260-1 LANCAS 1,3-DICHLOROBENZENE 91 8 3958260-1 LANCAS 1,4-DICHLOROBENZENE 91 9 3958260-1 LANCAS 1,4-DIOXANE 125 14 3958260-1 LANCAS 2-BUTANONE 114 2 3958260-1 LANCAS 2-CHLORO-1,3-BUTADIENE 117 2 3958260-1 LANCAS 2-HEXANONE 110 2 3958260-1 LANCAS 4-METHYL-2-PENTANONE 113 3 3958260-1 LANCAS ACETONE 100 6 3958260-1 LANCAS ACETONITRILE 118 7 3958260-1 LANCAS ACROLEIN 99 5 3958260-1 LANCAS ACRYLONITRILE 108 3 3958260-1 LANCAS ALLYL CHLORIDE 109 1 3958260-1 LANCAS BENZENE 115 3 3958260-1 LANCAS BROMODICHLOROMETHANE 103 3 3958260-1 LANCAS BROMOFORM 89 2 3958260-1 LANCAS BROMOMETHANE 83 2 3958260-1 LANCAS CARBON DISULFIDE 120 1 3958260-1 LANCAS CARBON TETRACHLORIDE 92 5 3958260-1 LANCAS CHLOROBENZENE 101 5 3958260-1 LANCAS CHLOROETHANE 97 2 3958260-1 LANCAS CHLOROFORM 106 2 3958260-1 LANCAS CHLOROMETHANE fill 3 3958260-1 LANCAS CIS-1,2-DICHLOROETHENE 105 2 3958260-1 LANCAS CIS-1,3-DICHLOROPROPENE 108 2 3958260-1 LANCAS DIBROMOCHLOROMETHANE 98 2 3958260-1 LANCAS DIBROMOMETHANE 104 2 3958260-1 LANCAS DICHLORODIFLUOROMETHANE 97 1 3958260-1 LANCAS ETHYL METHACRYLATE 104 3 3958260-1 LANCAS ETHYLBENZENE 100 3 3958260-1 LANCAS ISOBUTYL ALCOHOL 122 4 3958260-1 LANCAS METHACRYLONITRILE 116 1 3958260-1 LANCAS METHYL IODIDE 92 3 3958260-1 LANCAS METHYL METHACRYLATE 104 0 3958260-1 LANCAS METHYLENE CHLORIDE 103 1 3958260-1 LANCAS PENTACHLOROETHANE 78 10 3958260-1 LANCAS PROPIONITRILE 121 2 3958260-1 LANCAS STYRENE 95 0 3958260-1 LANCAS TETRACHLOROETHENE 93 3 3958260-1 LANCAS TOLUENE 106 2 3958260-1 LANCAS TRANS-I,2-DICHLOROETHENE 103 0 3958260-1 LANCAS TRANS-1,3-DICHLOROPROPENE 104 1 3958260-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE 116 12 3958260-1 LANCAS TRICHLOROETHENE 104 7 3958260-1 LANCAS TRICHLOROFLUOROMETHANE 79 1 3958260-1 LANCAS VINYL ACETATE 128 0 3958260-1 LANCAS VINYL CHLORIDE 105 3 3958260-1 LANCAS XYLENE (TOTAL) 100 2 3958260-1 LANCAS DEQ-CFW 00025490 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 Batch Identifier Method Number: 8260B Batch Start Date: 14DECO2 Instrument: 067200 Batch Number: 1 January 16, 2003 Page 7 The following field samples are included in this batch: Date QC Sample Name _Sam lamed Lab Sample ID Level FAY-G-MW-10D-ACR 10DECO2 39,59516-1 LANCAS QC FAY-G-MW-12S-ACR 09DECO2 3959517-1 LANCAS QC FAY-G-MW-2S-ACR 09DECO2 3959512-1 LANCAS QC FAY-G-MW-5D-ACR 10DECO2 3959513-1 LANCAS QC FAY-G-MW-8S-ACR 10DECO2 3959514-1 LANCAS QC FAY-G-MW-8S-ACR-DUP 10DECO2 3959515-1 LANCAS QC FAY-K-EQBLK-SWMU09DAY1-ACR 09DECO2 3959518-1 LANCAS QC FAY-K-TBLK-DAY2-SWMU09-ACR 09DECO2 3959519-1 LANCAS QC AnalyteLParameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: ACROLEIN 83 LCS-1 LANCAS ACRYLONITRILE 91 LCS-1 LANCAS Method Blank: ACROLEIN ND UG/L 40 BLANKA-1 LANCAS ACRYLONITRILE ND UG/L 4 BLANKA-1 LANCAS ACROLEIN ND UG/L 40 BLANKB-1 LANCAS ACRYLONITRILE ND UG/L 4 BLANKS-1 LANCAS Matrix Spike: ACROLEIN 80 3959514-1 LANCAS ACRYLONITRILE 93 3959514-1 LANCAS Matrix Spike Duplicate: ACROLEIN 94 16 3959514-1 LANCAS ACRYLONITRILE 100 7 3959514-1 LANCAS Batch Identifier Method Number: 82608 Prep Method: 5030B Pre -prep: Batch Start Date: 17DECO2 Instrument: 083630 Batch Number: 2 The following field samples are included in this batch: Date QC Sample Name Sa led Lab Sample ID Level FAY-G-MW-IS-ACR 12DECO2 3960931-1 LANCAS QC FAY-G-NAF4-ACR 12DECO2 3960934-1 LANCAS QC FAY-G-NAF4P-ACR 12DECO2 3960935-1 LANCAS QC FAY-K-TBLK-NAFGW-4-ACR 12DECO2 3960933-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: ACROLEIN 92 LCS-1 LANCAS ACRYLONITRILE 107 LCS-1 LANCAS Method Blank: ACROLEIN ND UG/L 40 BLANKA-1 LANCAS ACRYLONITRILE ND UG/L 4 BLANKA-1 LANCAS Matrix Spike: ACROLEIN 89 3960931-1 LANCAS ACRYLONITRILE 102 3960931-1 LANCAS Matrix Spike Duplicate: ACROLEIN 89 0 3960931-1 LANCAS ACRYLONITRILE 102 0 3960931-1 LANCAS DEQ-CFW 00025491 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 Batch Identifier Method Number: 8260B Batch Start Date: 23DECO2 Instrument: 067200 Batch Number: 1 The fallowing field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-MW-lS 12DECO2 3960930-1 LANCAS QC FAY-K-EQBLK-SWMU9-DAY1 12DECO2 3960936-1 LANCAS QC FAY-K-TBLK-NAFGW-4 12DECO2 3960932-1 LANCAS QC AnalyteZParameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1,1,1,2-TETRACHLOROETHANE 95 LCS-1 LANCAS 1,1,1-TRICHLOROETHANE 87 LCS-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 109 LCS-1 LANCAS 1,1,2-TRICHLOROETHANE 100 LCS-1 LANCAS 1,1-DICHLOROETHANE 106 LCS-1 LANCAS 1,1-DICHLOROETHENE 93 LCS-1 LANCAS 1,2,3-TRICHLOROPROPANE 100 LCS-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 87 LCS-1 LANCAS 1,2-DIBROMOETHANE 98 LCS-1 LANCAS 1,2-DICHLOROBENZENE 93 LCS-1 LANCAS 1,2-DICHLOROETHANE 101 LCS-1 LANCAS 1,2-DICHLOROPROPANE 108 LCS-1 LANCAS 1,3-DICHLOROBENZENE 93 LCS-1 LANCAS 1,4-DICHLOROBENZENE 92 LCS-1 LANCAS 1,4-DIOXANE 91 LCS-1 LANCAS 2-BUTANONE 118 LCS-1 LANCAS 2-CHLORO-1,3-BUTADIENE 99 LCS-1 LANCAS 2-HEXANONE 101 LCS-1 LANCAS 4-METHYL-2-PENTANONE 97 LCS-1 LANCAS ACETONE 121 LCS-1 LANCAS ACETONITRILE 101 LCS-1 LANCAS ALLYL CHLORIDE 89 LCS-1 LANCAS BENZENE 105 LCS-1 LANCAS BROMODICHLOROMETHANE 99 LCS-1 LANCAS BROMOFORM 89 LCS-1 LANCAS BROMOMETHANE 78 LCS-1 LANCAS CARBON DISULFIDE 104 LCS-1 LANCAS CARBON TETRACHLORIDE 88 LCS-1 LANCAS CHLOROBENZENE 97 LCS-1 LANCAS CHLOROETHANE 87 LCS-1 LANCAS CHLOROFORM 100 LCS-1 LANCAS CHLOROMETHANE 93 LCS-1 LANCAS CIS-1,2-DICHLOROETHENE 100 LCS-1 LANCAS CIS-1,3-DICHLOROPROPENE 101 LCS-1 LANCAS DIBROMOCHLOROMETHANE 99 LCS-1 LANCAS DIBROMOMETHANE 103 LCS-1 LANCAS DICHLORODIFLUOROMETHANE 80 LCS-1 LANCAS ETHYL METHACRYLATE 97 LCS-1 LANCAS ETHYLBENZENE 92 LCS-1 LANCAS ISOBUTYL ALCOHOL 103 LCS-1 LANCAS METHACRYLONITRILE 108 LCS-1 LANCAS METHYL IODIDE 90 LCS-1 LANCAS METHYL METHACRYLATE 96 LCS-1 LANCAS METHYLENE CHLORIDE 96 LCS-1 LANCAS PENTACHLOROETHANE 86 LCS-1 LANCAS PROPIONITRILE 113 LCS-1 LANCAS STYRENE 90 LCS-1 LANCAS TETRACHLOROETHANE 90 LCS-1 LANCAS TOLUENE 98 LCS-1 LANCAS TRANS-1,2-DICHLOROETHENE 92 LCS-1 LANCAS TRANS-I,3-DICHLOROPROPENE 99 LCS-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE 102 LCS-1 LANCAS TRICHLOROETHENE 97 LCS-1 LANCAS TRICHLOROFLUOROMETHANE 78 LCS-1 LANCAS VINYL ACETATE 117 LCS-1 LANCAS VINYL CHLORIDE 87 LCS-1 LANCAS XYLENE (TOTAL) 88 LCS-1 LANCAS DEQ-CFW 00025492 Corporate Environmental Databasz Lab AnaLysis QAQC Report Location: FAYETTEVILLE January 16, 2003 Project Name: SWMU9-2002 Page 9 (Batch continued from previous page) Anatyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Method Blank: 1,1,1,2-TETRACHLOROETHANE NO UG/L 1 BLANKA-1 LANCAS 1,1,1-TRICHLOROETHANE NO UG/L .8 BLANKA-1 LANCAS 1,1,2,2-TETRACHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1,2-TRICHLOROETHANE ND UG/L .8 BLANKA-1 LANCAS 1,1-DICHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS 1,2,3-TRICHLOROPROPANE NO UG/L 1 BLANKA-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE NO UG/L 2 BLANKA-1 LANCAS 1,2-DIBROMOETHANE ND UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROPROPANE ND UG/L 1 BLANKA-1 LANCAS 1,3-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,4-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,4-DIOXANE ND UG/L 70 BLANKA-1 LANCAS 2-BUTANONE ND UG/L 3 BLANKA-1 LANCAS 2-CHLORO-1,3-BUTADIENE ND UG/L 1 BLANKA-1 LANCAS 2-HEXANONE ND UG/L 3 BLANKA-1 LANCAS 4-METHYL-2-PENTANONE ND UG/L 3 BLANKA-1 LANCAS ACETONE ND UG/L 6 BLANKA-1 LANCAS ACETONITRILE ND UG/L 25 BLANKA-1 LANCAS ALLYL CHLORIDE ND UG/L 1 BLANKA-1 LANCAS BENZENE ND UG/L .5 BLANKA-1 LANCAS BROMODICHLOROMETHANE ND UG/L 1 BLANKA-1 LANCAS BROMOFORM ND UG/L 1 BLANKA-1 LANCAS BROMOMETHANE ND UG/L 1 BLANKA-1 LANCAS CARBON DISULFIDE ND UG/L 1 BLANKA-1 LANCAS CARBON TETRACHLORIDE ND UG/L 1 BLANKA-1 LANCAS CHLOROBENZENE ND UG/L .8 BLANKA-1 LANCAS CHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS CHLOROFORM NO UG/L .8 8LANKA-1 LANCAS CHLOROMETHANE ND UG/L 1 BLANKA-1 LANCAS CIS-1,2-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS CIS-1,3-DICHLOROPROPENE NO UG/L 1 BLANKA-1 LANCAS DIBROMOCHLOROMETHANE ND UG/L 1 BLANKA-1 LANCAS DIBROMOMETHANE ND UG/L 1 BLANKA-1 LANCAS DICHLORODIFLUOROMETHANE ND UG/L 2 BLANKA-1 LANCAS ETHYL METHACRYLATE ND UG/L 1 BLANKA-1 LANCAS ETHYLBENZENE ND UG/L .8 BLANKA-1 LANCAS ISOBUTYL ALCOHOL ND UG/L 100 BLANKA-1 LANCAS METHACRYLONITRILE ND UG/L 10 BLANKA-1 LANCAS METHYL IODIDE ND UG/L 1 BLANKA-1 LANCAS METHYL METHACRYLATE ND UG/L 1 BLANKA-1 LANCAS METHYLENE CHLORIDE ND UG/L 2 BLANKA-1 LANCAS PENTACHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS PROPIONITRILE ND UG/L 30 BLANKA-1 LANCAS STYRENE ND UG/L 1 BLANKA-1 LANCAS TETRACHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS TOLUENE ND UG/L .7 BLANKA-1 LANCAS TRANS-1,2-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS TRANS-I,3-DICHLOROPROPENE ND UG/L 1 BLANKA-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE ND UG/L 15 BLANKA-1 LANCAS TRICHLOROETHENE NO UG/L 1 BLANKA-1 LANCAS TRICHLOROFLUOROMETHANE ND UG/L 2 BLANKA-1 LANCAS VINYL ACETATE ND UG/L 2 BLANKA-1 LANCAS VINYL CHLORIDE ND UG/L 1 BLANKA-1 LANCAS XYLENE (TOTAL) ND UG/L .8 BLANKA-1 LANCAS Matrix Spike: 1,1,1,2-TETRACHLOROETHANE 95 3960930-1 LANCAS 1,1,1-TRICHLOROETHANE 90 3960930-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 106 3960930-1 LANCAS 1,1,2-TRICHLOROETHANE 99 3960930-1 LANCAS 1,1-DICHLOROETHANE 105 3960930-1 LANCAS 1,1-DICHLOROETHENE 94 3960930-1 LANCAS 1,2,3-TRICHLOROPROPANE 98 3960930-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 88 3960930-1 LANCAS 1,2-DIBROMOETHANE 95 3960930-1 LANCAS 1,2-DICHLOROBENZENE 92 3960930-1 LANCAS 1,2-DICHLOROETHANE 98 3960930-1 LANCAS 1,2-DICHLOROPROPANE 105 3960930-1 LANCAS DEQ-CFW 00025493 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU9-2002 (Batch continued from previous page) January 16, 2003 Page 10 Anatyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike: 1,3-DICHLOROBENZENE 91 3960930-1 LANCAS 1,4-DICHLOROBENZENE 88 3960930-1 LANCAS 1,4-DIOXANE 79 3960930-1 LANCAS 2-BUTANONE 98 3960930-1 LANCAS 2-CHLORO-I,3-BUTADIENE 101 3960930-1 LANCAS 2-HEXANONE 94 3960930-1 LANCAS 4-METHYL-2-PENTANONE 96 3960930-1 LANCAS ACETONE 88 3960930-1 LANCAS ACETONITRILE 92 3960930-1 LANCAS ALLYL CHLORIDE 96 3960930-1 LANCAS BENZENE 105 3960930-1 LANCAS BROMODICHLOROMETHANE 98 3960930-1 LANCAS BROMOFORM 87 3960930-1 LANCAS BROMOMETHANE 82 3960930-1 LANCAS CARBON DISULFIDE 109 3960930-1 LANCAS CARBON TETRACHLORIDE 91 3960930-1 LANCAS CHLOROBENZENE 95 3960930-1 LANCAS CHLOROETHANE 100 3960930-1 LANCAS CHLOROFORM 101 3960930-1 LANCAS CHLOROMETHANE 101 3960930-1 LANCAS CIS-1,2-DICHLOROETHENE 97 3960930-1 LANCAS CIS-1,3-DICHLOROPROPENE 98 3960930-1 LANCAS DIBROMOCHLOROMETHANE 95 3960930-1 LANCAS DIBROMOMETHANE 100 3960930-1 LANCAS DICHLORODIFLUOROMETHANE 91 3960930-1 LANCAS ETHYL METHACRYLATE 91 3960930-1 LANCAS ETHYLBENZENE 91 3960930-1 LANCAS ISOBUTYL ALCOHOL 99 3960930-1 LANCAS METHACRYLONITRILE 106 3960930-1 LANCAS METHYL IODIDE 90 3960930-1 LANCAS METHYL METHACRYLATE 93 3960930-1 LANCAS METHYLENE CHLORIDE 94 3960930-1 LANCAS PENTACHLOROETHANE 86 3960930-1 LANCAS PROPIONITRILE 110 3960930-1 LANCAS STYRENE 88 3960930-1 LANCAS TETRACHLOROETHENE 91 3960930-1 LANCAS TOLUENE 96 3960930-1 LANCAS TRANS-1,2-DICHLOROETHENE 93 3960930-1 LANCAS TRANS-1,3-DICHLOROPROPENE 96 3960930-1 LANCAS TRANS-1,4-DICHLORO-2-BUTENE 100 3960930-1 LANCAS TRICHLOROETHENE 98 3960930-1 LANCAS TRICHLOROFLUOROMETHANE 87 3960930-1 LANCAS VINYL ACETATE 112 3960930-1 LANCAS VINYL CHLORIDE 95 3960930-1 LANCAS XYLENE (TOTAL) 87 3960930-1 LANCAS Matrix Spike Duplicate: 1,1,1,2-TETRACHLOROETHANE 92 3 3960930-1 LANCAS 1,1,1-TRICHLOROETHANE 91 1 3960930-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 109 3 3960930-1 LANCAS 1,1,2-TRICHLOROETHANE 99 0 3960930-1 LANCAS 1,1-DICHLOROETHANE 107 1 3960930-1 LANCAS 1,1-DICHLOROETHENE 99 5 3960930-1 LANCAS 1,2,3-TRICHLOROPROPANE 102 4 3960930-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 95 7 3960930-1 LANCAS 1,2-DIBROMOETHANE 98 3 3960930-1 LANCAS 1,2-DICHLOROBENZENE 97 6 3960930-1 LANCAS 1,2-DICHLOROETHANE 101 3 3960930-1 LANCAS 1,2-DICHLOROPROPANE 106 1 3960930-1 LANCAS 1,3-DICHLOROBENZENE 90 1 3960930-1 LANCAS 1,4-DICHLOROBENZENE 90 2 3960930-1 LANCAS 1,4-DIOXANE 85 8 3960930-1 LANCAS 2-BUTANONE 101 2 3960930-1 LANCAS 2-CHLORO-1,3-BUTADIENE 107 6 3960930-1 LANCAS 2-HEXANONE 99 6 3960930-1 LANCAS 4-METHYL-2-PENTANONE 99 2 3960930-1 LANCAS ACETONE 90 2 3960930-1 LANCAS ACETONITRILE 98 6 3960930-1 LANCAS ALLYL CHLORIDE 100 5 3960930-1 LANCAS BENZENE 105 0 3960930-1 LANCAS BROMODICHLOROMETHANE 98 0 3960930-1 LANCAS DEQ-CFW 00025494 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 16, 2003 Project Name: SNMU9-2002 Page 11 (Batch continued from previous page) AnaLyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike Duplicate: BROMOFORM 87 1 3960930-1 LANCAS BROMOMETHANE 82 0 3960930-1 LANCAS CARBON DISULFIDE 112 3 3960930-1 LANCAS CARBON TETRACHLORIDE 89 2 3960930-1 LANCAS CHLOROBENZENE 98 2 3960930-1 LANCAS CHLOROETHANE 97 3 3960930-1 LANCAS CHLOROFORM 103 2 3960930-1 LANCAS CHLOROMETHANE 104 3 3960930-1 LANCAS CIS-1,2-DICHLOROETHENE 98 1 3960930-1 LANCAS CIS-1,3-DICHLOROPROPENE 97 2 3960930-1 LANCAS DIBROMOCHLOROMETHANE 95 1 3960930-1 LANCAS DIBROMOMETHANE 99 0 3960930-1 LANCAS DICHLORODIFLUOROMETHANE 90 1 3960930-1 LANCAS ETHYL METHACRYLATE 96 5 3960930-1 LANCAS ETHYLBENZENE 93 2 3960930-1 LANCAS ISOBUTYL ALCOHOL 100 1 3960930-1 LANCAS METHACRYLONITRILE 106 1 3960930-1 LANCAS METHYL IODIDE 89 1 3960930-1 LANCAS METHYL METHACRYLATE 96 2 3960930-1 LANCAS METHYLENE CHLORIDE 96 2 3960930-1 LANCAS PENTACHLOROETHANE 85 2 3960930-1 LANCAS PROPIONITRILE 110 0 3960930-1 LANCAS STYRENE 90 2 3960930-1 LANCAS TETRACHLOROETHENE 91 1 3960930-1 LANCAS TOLUENE 98 1 3960930-1 LANCAS TRANS-I,2-DICHLOROETHENE 95 2 3960930-1 LANCAS TRANS-I,3-DICHLOROPROPENE 97 1 3960930-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE 103 2 3960930-1 LANCAS TRICHLOROETHENE 102 5 3960930-1 LANCAS TRICHLOROFLUOROMETHANE 89 3 3960930-1 LANCAS VINYL ACETATE 118 6 3960930-1 LANCAS VINYL CHLORIDE 100 4 3960930-1 LANCAS XYLENE (TOTAL) 90 4 3960930-1 LANCAS DEQ-CFW 00025495 1171646 New Holland BoY 12425. Lancast y 1G Order er, PA 17605-2425_ZOLUt&�' InU129 I 7035504103-' To--] Proiect Number '!DuPont Fayettviije IFecleral ExpressL,i�Llity Name�04-362-6633 Telephone Number Name I Telephone Number --ie TOC�i,jf South Favettville NC 28302 z-iril'fty Addr?Fs iTransporter Address IRryan Heath Er xpress Save 14 Method of Shippina lsm-mu Process Producing Sample 9 Special Shipping Instructions Metals=Pb,Cr,Ni(G0*1 OTR) Erriplolleis) amp ing 10ther Employees(s) Handling DEQ-CFW-00025496 i 035-504-101--77- 4 425 New Holland Pit Box 12425. Lancaster, PA 17606-2425 --,I CID Proiect Number )uPont Faveftvillf� 104-362-6633 , . pr . e . ss--jowgo cii ism rITI122L;jn9 N�mkLer -117ransporter Name Tole tone PLumbtr ',OUte 87 SOUth Fa-yettville NC 2833021 Facility Address Transporter Address Oyan Heath Express Saver Method of ShInDina ,WMUg-2002 "rocess Producing Sample I Special Shipping Instructions M,,ztEth= Methanol I e i, o S ampling Lther Employ -em(P-LUF 2 DEQ-CFW-00025497 i N! lUb . %,.$ � -P -zi " 425 New Holland '0 Box -12425. Lancaster, PA 176055-2425 12001 (a 10M Ij/ rqup_J_G jFe.,sral Express -1646 7035-504103. )0 r49t--Number— DUPOIlt Fayett", 1704-362-6633 r!Tty. Nf T-) e�. . I Telephone Number Transporter Name -a Rc-no) ut-- 817 SOLIth Fsaye�,�-,illle- NOct C W- Facility j�,ddre.sc Tr'smsporter Address Pryan Heath lExpress Saver !racilitv Suioarvior i Method of Produch-1-- '3ample 32(30=APPIlX Sppecizl SNpplrg Instructions I. LOW) iEmplw em, Lem [qAtef Employeas(s) H2ndlin_ DEQ-CFW-00025498 117"1646 4103-. 50 2A 25 New Holland PO Box 12425. Lancaster, PA 17605-2425 ibgr- '['IuPmt 172yettville f04-362-6633 lFaderal Express Telephone I I'viliN Name Telephone Number Transvotter Mime raLeiL . ......... ------------- nut�, 67 SOUth Fayettrills NO 28302 F -n c.; I lity A d d, r. -z i6ryan Heath JExpress-Saver i Method of Shi P\A/POUP-2002 e 1 Special $hIpping Imstruction-s Prc"rs Prod city Sampt f Metals= Pb, Cr, N i (601 OTR) ,\,, ecA� iEm toe 'amrilinq Ct thor E�nR!!?\Letl(2) 1±!ndfin�4_. C16te tnd Time -arr. U ID'AS-'rvafiv QL1811tfly E.'ON iFAY-G-iViVV-8S 1 )0 VI(V'V 1500 I HNO3 I B 41 �C- L v-vvv 5C.0 i HNQ3 I B ....... .. ..... HFAY-f, I IV LYA 'I I VON 500 1 HNO3 1 1 B ix I1IFAY-G-l0Vi/-8S-DUP I orm 1 my 1500 1 HNIO I I I B I ix 1� JDatefFime Received bv x 'Fime X 'AAA C cj eimquiGi-led by Dalo7in* Received by clate—i-cri I SarVes an Atri'val c ii-ne Received b 'i 1 VJUIZ4 1 a --e. !Date vj /I as , DEQ-CFW-00025499 1646 ITV 20 02 ix --jDate/Time Conditl Of Samples Upon anival at Final Destination ` I 14 t 1040 2425 New Holl-and P. -) Box 124245. Lancaster, PA 17605-2426 50'o'—n*t--F 2--v-p-,-ttvi I I e Federal ExpressFacility Name LFelephone Number Transporter Name Telephone 14_umber, RMute 8-7 Sn-uth Faye-thAlile- NIC 28302 Facility AdIdrezz Trnntprter Addrern:, Bryan Heath jExpress Saver FaciislYSupeprior (Method of SWMUP.-2002 Procu-s "roducing -Samp!e Special -Shipping Instructions O=APPIX iota to s Sampfinq Other Employees(2) �Handllt��__ iR L1Q uisned by Dateffime Q/fO/O'?- IWO Received by(-J#,W.4q V,� J(92,4W DatefTime XA'za_� _- Llen'iiiquished bX Ly\� Da,,WT Ime Received DateiTime Temp. of Sapiples on iv aI--LI,— CO Reof Daied-i inleD4/11� Signatu -e id h ad by C-4 DEQ-CFW-00025501 ~ 1 Facility Name ITO—IlehonsNumber Transporter Name �hone Number South Fayettville NC 28302 ___IjkLq Bryan Heath r- press Saver Lx Prvc�" Producing Sample S�ecia1_3hippinR Instructions �ee�s) Sampling e Bottles Received by Datefrime i Received by _A ID&teMme wiz) v;i(//f4-/ 2425 New Holland I Box 12425. Lanc"-W, PA 17605-2425 0(714 b &IM � JAAe 4 11171646 7035-504103-7 0 lGrourig I HD Pro ig Number OuPont F2,vettviii- 04-362-6633 r, -ct d eExpress .E.;Lc'2Y—"J—mt"e T�jShone Number Name IT Route 87 South Fayet-tville NC 283nT— Facility Address Transporter Addres., 'Bryan Heah t D'Y mxpress Sever Fgi'rft'v Method of Shipp 8WMU9-2002 Pror�ez- Producing Sample 9 Spedal *hlpp)nq Instructions %r MetEth=Methanol 1 � e 1�1 Ens plolPee(s) arnpling ,Other Employees(s) Hanolinq_ 0 t In, Dale he I Sam{ , ITYPe QuyntifY 156 Ty,Ipe er p n '-D 0 VVVV 140 pf) NOS- 2 v Bottles Relinguished bZ at�— Date/Tirne 11 f Bottles Received bv kateffim\e !Condition of SaWRIOS Uponrarrival at Final Destination _ReLnqLr- Pj1AuvW Date I irrie I'ZI DateMme by 1 Daterrim's Recei'ved by /I 0 emp, OT Samples an Aipyai c efflrn� 'IDat -T pecshmd P NI aw rh Mm e 8ign-aturea fj&y�, Date RM71 DEQ-CFW-00025503 i ottles Relingui he v Lpb-lZL ime 061, ISM Bottles Received bv IVA4� ID'ate/Time\ lConamon of Samples Upon a a[ Destiriation `I I T1 646 0 Ya - 5 N:: �O3 - ill 2425 New L�jLtt�-' Holland, D Box 12425. Lancaster, P -2242tLjjloj &41.4d,6 q��, I Ptoject number - - ---- -- - ----- L DuPont Payettvilie 7b4-36f6633 lFedera Express Facility Name Telephone Number Transporter -Name ITelep, no Number. ROLAeUSouth Faye illeNC 28302 l- Facility Addr,-"- 6ansporter Address Bryan Heath 'Ex press Saver Eadr-lbqqP-W—Vi pi I Method of Shipna -qWMU9-2002 PrPrQducirq Samptle UGUMI� zi-cclal shipplrl-q 1 �tr remm S ettalsz:Fb, Cc, Ni(Q0,11 OTFR) E § Date/Time 1 SIT Bottles Received by A '4mvFV" DatelTime lCondition of Samples Upono'grival gt Final Destination ve.� Lielinquisfied by IDatelTime Ileceived �y Datel-M-ne Received b Datemme e.mp, of sa,,nples on Arrival C 0 Rellrim,,flshed b�; ID?tn-Mmo R e c e lve. d hy at A 1 /1,-, -51 Qsjfjjj q's t- 4 DEQ-CFW-00025505 w I -T- 00 C-1 Ef I/ / j 1171646 7005-504103-; flew Holland F Box 12425. Lancaster, PA 1 !425 52425 aO Irl Pro ed Nitimber )uPont F2yettvihu -mor 04-362-6633 (Federal press I Tole hone Number __ �TranS orter Name - -- jo_le2hoLie. Number Route Eli Sotlth Fayeth.!ilie NC 28302 Facility Address Transporter Address 3rya.n Heath Express Saver :g gypervior Method of Shipman 3wMUq ?racesu Prcducing Sample Special shipping Instructions r AW\-� MetEthM =ethanof m10,=s e() 1" Sample Dale Time SaMPIP INOILIMe iantit PMServalive Quy Bottle I q I�Ypa e F� I I IType rI -i FAY-G-111AI-2S JUJOID'Ll 'flo I 'V'VVV 40 1 HCl 1 2 V X 30ttles Relinouished bv DatefFime 1116JO J5K Bottles Received bv Date I inn Condition of Sameles URon arrival at Final Destination _ Le L t I- jDateMme I�,IIVIDZ ISO)' Received Dateri Ime -ied I 'Y Dlaterrlme\' Received by NIS Dater -Pale Temp. of San on ArrlyqI C 0 �elln,�,,jlshsd bw J,-- PatefTlrrie Received b Datefflmee fall M3 i-Signabure %I I J-Pato dg-4M - DEQ-CFW-00025506 No, tD:DF+vZ -tboratto!plez 0 Spy 12425 Lancaster DEQ-CFW-00025507 L a n c, s te, -tw-ow, ina 35--5041 033-"_ 2426 New Holland D Boy. 12425. Lancaster, PA, 17W5-2425 110,uPont Fayetbw,.- i Fa.cilltv Narvio IRnute- 87 SOUth Fayettville N(.'28302 1 F, --� (., - 1, i I t Y Ad � 1, r e—, !Bryan Heat (Facility Sunervior 1-SwMUP-2002 ! Flmcess Producina PPIXII 10therPnininvear(s) Handling ig ro A eweral Express:UP Transporter Name rrmnworter Address -xpress Saver Method of Ship Sm,ial Shlorl-na instruc-tions T--, - pit{ I -VA - ' -' Si q gilt . . ... ...... FA Y'- K-TB L ik- DXY-I--,-S4vv rVI U09 j — — ---- VVVV np 40 FICI 3 i v L------ Bottles RelinLu Strad b Datef-Fime 11)61, 1,57b Bottles Recei me ADateiTime Condition of SaMples Upon arriv at Final Destination [Reiingmsheed, by jDaterlime]2)'IDIOZ, )SOD RecOved bv 0 lei rit jDaIerfitne I i - 'I by :TL !Datefflme iss tefTimi, Received by /I --------------- - - - - - - - - - - - - - �) 72 'ecelve'd by I � Datel—I ime —eff tit —TH— c 0 'a Arzi, Temp, of Sias an Ar Sic, ature. Mez�cate/vk Cb IK'7 A 3 I R DEQ-CFW-00025508 caster 11171646 7035-504 -(7 — I'.." . .1. 11 - . "I !DuPont F2vettviim L'UVI I I VjFjw 1704-362-9633 17f 9 roar lu BFecleral Express IrIUMUL Nufflut:1 I Far catty Rlarle Telephone Number Transporter Name TelMhor!.* Number Route 87 South FavP-ffvflHe [,,!C 28302 3ri=it Addrr,,�s y Address dress its cyan Heath 'Express Saver !Facility Suoarvior Method of Shi F, -"-2002 Producinrl; Sample 32ecial ShIlEpin g lnEtructiopr, jL:rjp1oyee(s),6a finq LQthtr_Ffpp L yiat;00 Handling _ IllhiI; -- -,- --P,G—te S arn P!,-j Time ISampic I)VO111m.e h-e-r-3live Quantity FP'tle jjFAY-K-TBLK-DA:Y2-SV4MU09 Pipe (mQ P I .- i . 40 1 HCl 3 Type I. I V ffiVVV'V .................. PDQL es meljriqulshedibv�p, DatelTime 11 iL"- `B®tiles Received by Mateffime\ tCondition of Samr)les Uvon arrival at Final Destination 0:'o-litiouished U" L Datefrime )VIVOL Received (y I i i iU:Siled b) Datem, me Received b(z� Datefti0e Mits. OT Sualpple5�on PAval LRl Eei!n iE ithzd by DatarinpccNed by/ SiSignaturew Date AAW7L ,� o a VA DEQ-CFW-00025509 � PICIV A JLM C--., r­-------------- [11;W -716 ;(J 35---] 7050 To ' 2425 New Holland 0 Box 12425. Lancaster, PA 17605-2425 J-Q1 ripr I D iPrnieci Number DuPont FayPttvj,.-- 704-3K-6633 IFaaer2l Express Fa' drcv Name Telephone Number Tr.nsppr -r aTLP 17relep L NuM§er __I t� qt__ oute 87 South Fayerftmille NC '28302 cr. illty Addr7ns �Bryan Heath jl=xpress Saver If acilityAqee-�Qdq—�- . I.Method of Shinpina 'SW AUg-2002 Process Producing Szimp!e Special Shipping Instructions —IMetE-:th= Methanol EmploVee(e) Sampling C", .Mpip I Ime 30m IVOII me Pinesservalive Innfil M--B p!e I' 'U Type i FA(-K-TBLK-DAY2-SVVNIU09. I VVVV 140 1 HCI 2 if V. IX 'Condition b21!!ts i ellnc aimed by JJLk,-A, Datefflime 15WS- lBottles Received by JDateftTime of SaMR es on arr' t Final Destination Z�Uwll� Datei`11rfle Received by - -- ----- IDirielTime 11, d bpi Received ajFpfes on N71va! DEQ-CFW-0002551 0 V- Q. IUZ r425 New Holland F Box 12425. Lancaster, PA 17605-2425 171646 7035-50410 Proiect QW r ID I Number DuPont'Favetville 704-362-6633 Federal Express ITelephone lTransporterName Number ROUte 8-7 South F-Pye-ittville NC 28302 FBcilfty. Ad -dress iTransporter.Address 3ryan 1-16ath F-Wess Saver -2 Sup rvior Method of Shi Tg? 3WM(JP-2002 Pnoces-- rroducing Sample Special Ship2ing in54ructions jMP.tals=Pb,Cr,Ni(GO10TR) Dther Fi!2pjn_yetg(q) Handlinq___ W 3ottles Refinguis edb Date/Time It o- Ism— Bottles Received Z%QoW1DatefTjmaX Condition of I-JaMDIeS UDOn arrival at Tina l Destination jty!gUishefj by Date/Time V/ )SW Received by LeLinq_.wished by Received by Datemme Temp. of Samples on AITIVal jDate/Time Receivedgnp—&91 K—��-- e -all I inn-21-11 Signature J�A� perrl� Date ed 5-0q rl U DEQ-CFW-00025511 Lancaster 1 -mboratorle.,_- 2425 New Hoiland D Box 12425, Lancaster, PA 17605-2425 DuPont Favettvi,— Route. 8*17 Scuthl FayetbAlle NO 28302 Facility Addr---zt Bryan Heath Facilitv SuDervior SMOUg-2002 YI 11171646 q T G Feaeral Express Transter )orter Name TelaoF Transporter Addre-,5 Express Saver Method of Shippin g Irs—peclai —ShIpAng instructions 3=APPIX -1035-5041037 Bottles -Relinquished by �K /-kALzL !DatefTin I Suh Bottles Received by Date[Tim lCondition of Samples Upon anival at Final Destination RelinCiLlished by -Akay:�:- JDate/Time 1500 Received by Date/Time Received Dateffime Temp. or Sari les on Arrival Reling.fthod b y nutefTime Received, Vigrature, � 0 L( DEQ-CFW-00025512 I-ft�u AAUIIIJ sox 124215. Lancaster, PA 1705-2425 7035-504T-073--T7 el Lti IPrajeci Number Z�L uPont Fayettville acRty yntt-.— 1704-362-6633 Telephone Number -Z� federal Express I Trancr)orter Name rTelepho mber ---T- _ otite 8.7 SO-Ulih ITransportler acillitv Addrevs Addre". ryan Heath Express Saver Method of Ship WMI.JQ-2002 rocess Producing Sample -pe,.!-,l Shipping Instructions reffEth=Methanol l v ip! Vee(s) ,.r nye,es(s) Handling a M p D--A-Y"l- BM= JgB r V?""' ,;Iinciulshed Irvf m "ratenle IR.caived bv IlDatei'rinie [renli). OTSari:4 n-25 On Arrival 01 c I )l 0,0 37 1, DEQ-CFW-00025513 61-flu y 1-5 v /I q IVI 71646, 7035-504-103- JO 42,,ToIlTn �,7 New D Box 12425, Lancaster, PA 17605-24256 Project Lumber ()O� 6tljj.� -/� IDuPont F2yettvl,,- 1704.362-66333 (Federal Express Facilit Name Telephone N!:Lm Transporter Name Tole on _ter um or -Oute A-7, Scuth Feyellteille NC 26302 IT'ransporter Facjlibj Addre- Address Bryan Heath Express Swer IF3CilIP Suparvior N-x2lthod of'Shoil —P WMU - , > Q-2002 Proce!:s Producing SMRL,-� -Special Shipping instructions Ni(5010TR) \No., Y\ jMetaIs=Pb,C Em 10 e%4(Pling shamIhrn( Other Emplayess(p) Handling ii!FAY-C-.- Dats,71me RudVed I V Sarrides on a E Date DEQ-CFW-00025514 1.4 /W /) UY / t G--" Lanuamm" '"mrazuriez , 2425 New Holland 0 Box 12425. Lancaster, PA 17605-2425 4 11 1646 --j-7035-504103- )0 I Proiect Nu mher -(ar= A 11[2 DuPuit Fayettviiie 704-36 633 Federal Express Fa6fi I Telephone Number Transporter Name Telephone Number---_ Route 87 South FayettAlle NC 28,3102 Facility .Address (Transporter Addrer-.A. yan Heath Express Saver 172cilitv Sme Method of ShiaRbg___ SWMUg-2002 Process Produdnq Sample SEeclal Shipping Instrucutions Methanol e US n .40 Other Emplo ees(si Handling -��Eth= 108'r"Ve. I!Volume 1. LI jPreservalive lQuanfily VoIlle Type. ],',FAY-G-h4IjL-1 2S__. IZ WW -L-Elf 40 HCI 2 x lBottles Relinquished by ti�A,11)atelTirne IY4j- Bottles Received by:, I _ DateFl Condition of Samples Upon arrival at Final Destination -Refinquishad by IDateMme 1900 Received b Date/Time IDateMme Received b DateMme emp, of Sapples on Arrival 50 Relln,]Lfthed b y IDatr �mme Ran-Oved by( J�k� fz"I Dat e../Tlme 4P41 9 1551si Date 10( Uf i 4e I f IN r P DEQ-CFW-00025515 N, V. r— 'ILIO r ID TO --I -117,1646 1 70305-5041 03 2, -2425 24251 New Holland i. Lincaster, PA W605 Ar ID ecLt LI -7 Dupont Faveltlific AN 7 4-362-6633 1FQdPrai express —ge 1 NA1110 Tolophons Numbar NAme -----LT -p—jiqne mint r rn.c;I!tv Addrsss !Trnnsp orter Addrr., sr - • ryan HewLI"-) xpres$ Saver IF2Cil!tV Supervior Method of il�--l-,�i�---*-'-'�-���-�,11--�--�-�,'�-,---"��� T­-- �SAAIMUP-2002 -,-ocess 1-m-ducing Sample Special Ship-EIng IrstructioM 1-0260=APRA OthAr Emnlnvaeg(O Handling T-� Jmple Vol11 -, tPres rvatl Uant y .... ...... vv- 12. s I W-1-1-ID771 UviJU i4G i HCI 1 3 1 V I In I -T— - mqjIqr--"jD tei .h )Lat�effim -T im Condition of Samples UDon allival at Final Dastination Bottles Relinaui- Bottles Rpr, a Rel-inqui Daterrifirie"thp/w, W Received by Daiwfiffie,\ E, -! fecv- In 3mpl/C0 iseby Damrrime Reeied bY emp. of 3pv bDatems Recelved1 Signatur Date L4 4,3 DEQ-CFW-00025516 1 !me 11716646 OT OEQ-CFVV_00025517 -5 Box 15425. Lancaster, PA 17605-2425 Aw 242,F) Mlevv, Holland �'Fvlp­ it S-ACR vff,' UUMe L40 J. 3 1 v 1------4 4-- ------ !Boffie-, 961irmlished V Daie/Timt, jfldd:;- Bottles Received r lDatefT*ime lCondition of Samples JpoH arrival at Final Destination I I.-X 1'r! iinclu"ished by DateiThie 4NO Received by Daleifirrle 1 Received b 0 of Saigles on ArNal f`aMed by ate. nrm"ecelved by i ADateM-ne gpatmcwNSignature , fIemp, � Efate 2-1 LA) r DEQ-CFW-00025518 r * liorratoriez 1-1 1171646 ij)35-504'103- 4425 New Holland 0 Box 12425. Lancaster, PA 17605-2425Nb Q 116 3 6 94 --- 4Q,—, 'ar cutu er )UPont Fw1gitvilla f7114-_'262-B621 1F--PdLqr2i P-Yprpr..-, Te'lep -Er ngLoqq, Mime Number- IF jLtXName Tele hone Number _q__ Route 87 South Faiyet.Mlje NC 28302 rociffityAddress rter Address 'Transpo 113tyan Heath Express Saver lFacilitv Sunervior "rec- zm'* Pr7ducInq f�'amplu 'r: 5per'hl shipping lnVruct1QM-" 604 lon tmukee(siyampiing 10ther Ernplovses(r,) Handling Ak' Time II q resc- ah,(fir" Puanli!y PuMe r2 3 - - ------ V i j- . . . . . . . . . . !Boitles Refin uishet bi' ij�A, iDateF1'iine IM lBottles Recaivkby DatefTime CondMon of Sam u I at Final Destinati _Tm"s M a 'Va )y a"efrime ,�ceived bv jDateifirne IRt e 'u)'31-led by Mn kleceNad by /I enip, 07 --laniges on'N'riva! -.W- A Signature , ate;7 ),/Zld OA1 0012M'T�Q 6) a by CO LA5 q 0 C 0 DEQ-CFW-00025519 — rBry',11-1 Heath �Express Saver IRWIN Ennployee(s) Sampling, C/�O -A6 � it -) - IZZ, 0 L an c. t e r &t P4 to wal es - -------- 12 1-1171646 7035-50'4-103-—)C—)71 lGri d, LPr-oLeq:E—N!!-rTdb—er-- H0 1;nd fax D 19 n ?G. La"ster, PA 176T.5- E 2421�33�- FlIff i TP o- n' -t- —Fa y--e'-t t- v- i i i e 1704-%4-6 313-- Feder -al Express I F y mnsporte a ebtRtone Number atilis �mo Ttte n �ju btr IT rN me 'Pcute 87 South Favett"Aille! NC 28302 Fr4rlPt' Ad,,Irrrs lTransport ter Adldrerr. Bryan Heath bExpress Saver Method of Shir)pLng__._ ISMA19-2002 [!-'—Cr—Acn=Acroleir,/Acrylor)itrile PIFAY-G-t, DatelTime )M9A7?- ISOD of Samples on DEQ-CFW-00025521 xjyj/j� 4r 4mm D:D=U 22425 New Holland 0 Box 12425. Lancaste.r,.PA 1.760-15-2425 t77 argLect Dumber -4 IDUPont P=Vattvji,�. 704-362-6633 Express illuiitv Name Telephone Number lTrans-porterName,, Tftp -iono -Number avetiville NC 28302 FHlj+VAddrTrs [TrMIS"llolter Addres's E,; ya n H e at"i i OE,'xpress Saver �Facili' Swervior Method of Shirmi ahlppinq !nztructlonr, 4 . % !ArrAcii=Acrolaiii/Acryloni'Lrile iFAY -G-iVlVV-6S-AGRiv - S-Ap -Ito r P:l WitV 40 v VWV 140 1 None 1 3 1 V Received of Slawles on Arrival 1,450 C 0 DEQ-CFW-00025522 bfi;tt�f V';WYff J %0 -4 �j I AF— 251 New Holland to Box 12425. Lancaster, PA 1760.155.2425 "4s e 5 2425 IeIF a --r--I �i 71.46 IGMgg# 10rdpc ID 7035-50410350-`11 I Proiect Numb r R-- - 66 0,jPc,nt FavetIcv,.— 704-362- 33 Feaeril Express ETI �F�k.651.y Name. AT. S37. S o uth Fayethiiile NC 28302 lephone Number Transporter Name F:1.cilftv Avddrev.� ITrannportsr Address Pryan Heath lExpress Saver ! EqcL ijtyAq ior _ ---- -pq�v GWMUO-2002 n Method of Ship g., - R!_ ___ ,Process Producing Sample t' Af\ I Special Shipping Instructions FAcI Acn=r"icr�,-Ieit)/Act-ylonitrile Em 10� e'ampling - — P— -e lotlw- Ernk)loyeem(s) Handling Y-G-IVIVV-1 UBM ��IMK M. i zelinquished by DeteFi ime V�� baterl itne lReceived by YA- 71��7 1 D'ateMme !ReCEived bv /I— Dateffirne I'so- C 0 17'eralQuis"Ied 4v kmp. ol Samples on An lVal Received 2� DEQ-CFW-00025523 Y--)UrrZ.---' � "-;1)7J'j�1;j%,AV I MCI %""'M 1 'J LUI9UWUI;Q' I- ' --"QVrFAVUF'IeU -&(- 1-7005-5041002 2425 New Holland D Box 12425. Lancaster, PA 17605-24, DuPont Fayetvil—, LQLIPI 1rWdmer Feaeral Eypress �--- ]7--f Telephone Number Transporter Name Telephone Number-----___-- ROLI'm 87 South Fayettville NC 28302 Facility Address Transporter Addr-e", !Bryan Heath Express Saver F i� wy - - Y-qkIP I Method of Shi - �;WMLJ9-2002 - c ass Prcducln@ Sam le 3"Pecial Shipping lnstructlon5 I tV An 40'T AcrAcn=A;.,roleinfAcryloriiti,iie PI'lier Prmpinvepq(�� �HandilrLq_ V lBottle., Refinoui Dateffime I I wo 2.- sy� Bottles Received bv I Datef-Fime\ lCondition of Samles Upon arfwW at Final Destination 1-- ---1. kefinquished by b12/P? 6Dl), Recelved!�Y -- =Date,Tirne helb Date,,-71n le Received b y A Temp. of Sal*es on ArrNA z IDateffif DEQ-CFW-00025524 - . >7 L4V A-_j V / / C-1 0.:J-Cjt -/ .J— -C/-u I V%J. v%OO a f .1 4F 11-171CA6- ------T;7-035-5041 —0 r " —UUMEVITOU — — . 10 -5-2425 2425 Nemv Holland 3 Box 12425, Lancaster, PA 1760 I Proiect NuyLber Jil r 0 r IQ 74��hl --L EP�ni fEa�ve&h— 1704-362-6633 IFederal Express I Facility Name Telephone Number TrapSp2rter Name TeIaDhone Number is 'Cute� 87 South F-eyeitville NC 28302 Grvom Heath lExpress Saver IF;aciIifv Smarvior tl--WNAU9-2002 � Dwa p i llp-zrlal SMpping imftructions Yee samplim � !qther_gmpfqyee r -A( L�q!L H n irIg __. I ril uff#.X roil -. 1Ro!3,3pas oAlmlRe iQW s1ad bv lfee1ar, . za.4ll a t e4f- Oq ff DEQ-CFW-00025525 171646 2425 New Holland D Bop 12425. Lancaster, PA 17605-2425 0� � _ � 2__1�tr !�10rder ID ---- --- `_---- -- � 7035-5041 03- ._I P.r_olect Number ) !DuPont Fave-tt�,iiik-e 704-362-6633 Federal Express I Facilit�,r Name Telephone Number Transporter Name Telephone Number _ ROL!ttl- 8,7 9rL!+h Fayet'tville NC 28302 F=c.illty Addrr.as I_ Transporter Addrssz jBryan Heath Express Saver i a4iliiv Suoervior Method of Shipping I �CW{1J1f 9-2002 Process Producing Sam le � W• ecial Sh's wing instru- t,cns iAcrAcn=,r'l� crolein/Acrylonitrile i I i0th w Fmplouees(s)Handling Im Received pv {' .ff tt�'�� ,ttyy rrpp�� i�c^%c�11cFi u' �i✓dlelTiifi ��i"tR�. Qf Sar (�lvs on err t%i `T 1/� v 01 IRo i u�ict. e 9 m a r,ve.1 �f ` $macE �``�i!?icw €an .tLrP C diA�')a!n ,, ,1:,., tt d t y Lat tT:m P Cyr 3'1 DEQ-CFW 00025526 V � Y ;15 It (V I C-=,/ NO. Q 1 4U0 Lancaster ,oratories j, 7035-504103-' 10 2425 New Holland I Box 12425. Lancaster, PA 17605-2425 Pr --- ',DuPont Fayettville !704-362-6633 lFederal Express —acility Name Telephone Number I Transporter Name JOT-7777, ------ ----- ---- - - --- -- - --- ----- ---------- ----- --- Poute 87 South Fayettville NC 28302 ------ - - - -------- -- — - ------ — — ----- — --- — ------ ------------------- Bryan Heath Day AM -- - - - -- ------- - - - - ----- ---- - - ----- - - - - ------ - - - ------- -- - - - - -- ------- — ----- -- Facility-&ver --ndo ---- - — - - — - - - - -- — -- --- - ---- — ---- - ----- — - ---------------- of 2Sr hipp na SWMU9-2002 Employee(s)_ Sampli._4 , 1'j�, - Ij - -------- - Other Employses(s) _HandftL____ �ample = M�W�W MEN ,Desodplion I --- — — — -� W'Ruvwx Battles Relinquished DateMme/dm/1-0-,�-- Condalon of Sampl4s Up4n arrival 4 Final Destination 'Received by Aulshed by 111 iTtmp._ of Samples on Arrival _011 - -- - ---- — - ------ - -- - ----------- - - - DEQ-CFW-00025527 I- lf4.a (/ Lanca3yer - -ooratorm RV, Myj R -2 2 7035-504103 00 2425 New Holland' 10 Box 12425. Lancaster, PA17605-2425,ftI14 Prgiect Number :Order I D — -- -- - --- ---- --- - IDuPont Payettwim TTO-4-216 3 Z-663b 11 Federal Express _FAcilit Name - 0 Num e "Transporter Name Telet)hone Number Route 87 South Fayettville NC 28302 Facility Address IlTransporter Address ---- - — ------ - - — ---------- i Bryan Heath - ---------- - - - - -------- - - ------------ - ----- - ---- ;'!Next Day AM Facililt-SuDeryj jor Method of Ship . . ........ - ----- - ---- - - -------------- - - - ------ -- - ---------- --- - ---------- -- !SWMU9-2002 Prooess Producing Sample - - - --------------- - -------- - - - - ------ - ---- AcrAcn=Acrolein/Acrylonitrile EmplQyeets) SamRfins-- �OtherErnye-es(s) Hanling _pf od ILFAMUITak X.01 WAMWAM Boftles Refing !shed by - -WIZE1, WMIK/lim ;Condition of Sample -s U nwW at Final DesUnation I Wh - - ------- - ------ - --- --- - _Relinquished by_ K femp. of Samples on Arrfql W, C71T- I rsh e �db W/ Sl.-2— DEQ-CFW-00025528 Lancaster ' iboratories 1172923 J7035-5041U, )00 Pri 2425 New Hollan PO Box 12425. Lancaster, PA 17605-2425,q/ltlz Nq�,, awjD— I Project biuMber PuPont Fayettvitie 1704-362-6633 Federal Express NumbtL- Route 87 outh Fayettville NC 28302 FacHity Address �Transperter Address WanHeatK­ -- - ----- - - ----- - ------ - -------- - - ------------- - --- - --- - - ---- --- - ----- - -- ------------ Next Day AM !F2ClIkV-SUDWfAor- -- - ------ - - - - -- - ------ - - ------------ - - - -------- — - ----- - — -------- -- — ---- --- ------- - lWethod of Shipping SWMU6-GW2002 Process PrOucing Sample Special ShipVing Instructions AcrAcn=Acrolein/Acrylonitrile LUMPIWER5UN�mEmomm Him 0 DEQ-CFW-00025529 ,-f I x ---) Co 61 / 6--1 LOnuagater '0011-010FW3 172924 1 7035-5041 M 00 ---------------- IDuPont Fayettvioe -TFede—r2i Express I Facility Name �Jehe J.'gorleNumber Transporter Name 87 f6_309 Facility Address BEL Rryan Heath �Neekt Day AM Facility Supervior Method of Shipping ----- ------ - - ----- - ----- ---------- - - --- ---- 1--7wjC-4OSNPoduc!4OampIe - -- - --- --- - ------------ — ---------- - lal ShWing Instructions AAA AM _mR1oyeeLsLS e ! Other Emplqyees(s) HandLling - ---- — ------ 1�sample - - II DescAption � ---------- -- -- ---------------------------- - 4 - ---- - B ottles Relinguhisked by !Condition of Samples Upon arrival at Mnal Daytination Relinquis;hed 01, baterrimo 'Temp. of Samplespn Arrival C - ----- WMA' I f - f r V ) DEQ-CFW-00025530 DuPont '` Corporate Environmental Database Check List KAR Preliminary Administration Review Project Sheet Verify location/jobname in sample table KAR Project Backstop Disk Deliverable Integrity QC Batch Integrity (Correct problems/Pull backstop as necessary) KAR Completeness Check Samples x 100% Tests x 100% Parameters 100% or x <100% KAR Accuracy Check CED Results vs. Hard Copy Lab Reports KAR Comments/Narrative Review KAR Laboratory Services Coordinator Overview Review Report Cover letter/title page for customer KAR Report Finish Copy and Bind KAR Mail to Client(s) Kelly Rinehimer 1/7/03 Certified by Date DEQ-CFW 00025531 The following process is followed on all projects where data is delivered to the Corporate Environmental Database (CED) and a report is generated from the CED. All projects that bypass the CED (Le., are directly reported by a laboratory) do not receive the rigorous treatment presented below. Preliminary Administration To begin a report, the reporting coordinator checks out the file and updates the reporting schedule. A review of the project sheet is the next step to familiarize the coordinator with specifications and special instructions. Finally, the location and Jobname is either added, corrected, or verified to ensure all samples are properly identified as in the project. Project Backstop First, the backstop is used to check the disk deliverable integrity of all project data. This tool checks the CED readiness of the data. Second, quality control batch integrity is checked by the backstop. It is verified that all samples for each test have appropriate quality control samples attached. Completeness Check Data completeness is checked against project specifications. First, all sample points are identified as 100% complete. Then, all tests for each sample point are checked for 100% completeness. A parameter (or analyte) count is verified for each sample and test. A 100% parameter check and/or reporting threshold check can be done if requested in project specifications. The results reported by disk and located in the CED are checked against the hard copy laboratory reports for accuracy. This stage is a 100% check of the accuracy of the data. Comments/Narrative Review Three steps are included in the comments/narrative review. First, any comments made by the laboratory are located in the hard copy reports. Second, the quality control section(s) of the laboratory reports are reviewed for obvious quality control deficiencies (matrix spike or replicate outside control limits without appropriate comment). If questionable, the laboratory is contacted for verification. Finally, the appropriate comments are entered into the CED. A person familiar with the project (usually the customer service representative) reviews the completed report and the reviewer produces a cover letter. Report Finis ailing The final step is to copy, bind, and mail the report to the client(s) in the format specified in the project specifications. d:\transfer\forma\fayetteville\2002\cedckist 1. due DEQ-CFW-00025532 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6-2002 C of C SampLeid: FAY-K-EQBLK-NAFGW-DAY2 Sampling Point: EQBLK-NAFGW-DAY2 Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958316-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) AnalyteZParameter Dilution Result Prep/Method: 351OC/8270C 1-METHYLNAPHTNALENE 1 ND 2-METHYLNAPHTHALENE 1 ND ACENAPHTHENE 1 ND ACENAPHTHYLENE 1 ND ANTHRACENE 1 ND BENZOMANTHRACENE 1 ND BENZO(A)PYRENE 1 ND BENZO(B)FLLJORANTHENE 1 ND BENZO(G,H,I)PERYLENE 1 ND BENZOMFLUORANTHENE 1 ND CHRYSENE 1 ND DIBENZ(A,H)ANTHRACENE 1 ND FLUORANTHENE 1 ND FLUORENE 1 ND INDENO(1,2,3-CD)PYRENE 1 ND NAPHTHALENE 1 ND PHENANTHRENE I ND PYRENE 1 ND Surrogates: 2-FLUOROBIPHENYL NITROBENZENE-D5 TERPHENYL-D14 1 Prep/Method: CALUFT-DRO/8015/CALUFT-DRO/8 TPH-DRO 1 Surrogates: ORTHOTERPHENYL Comments: E ND U 102.0 RPR January 7, 2003 Page I Unit MDL POL Date Analyzed UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 UG/L 1. 10. Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 UG/L 26. 100. Dec 16, 2002 Dec 16, 2002 The TPH DRO bottle Label IDs were FAY-K-EQBLK-SWMU6-DAY2. Lab personnel togged in the sample per the CDC sample ID. Field personnel lined out items from CDC 66830 without dating and initiating the Lined -out items. Lab personnel received sample, FAY-K-EQBLK-NAFGW-DAY2, at 1.5 degrees C. Since the sample was received intact, the QC Reviewer believes the data is acceptable for use. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025533 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6-2002 C of C Sampteid: FAY-S-SWMU06-01A(4-5) Sampling Point: SWMU06-01A Date Sampled: DECEMBER 10, 2002 Lab sample ID: 3958278-1 Analysis Lab: LANCA Sample Type: SOIL QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution Method: 160.3 MOD. MOISTURE 1 Prep/Method: 3550B/8270C 1-METHYLNAPHTHALENE 1 2-METHYLNAPHTHALENE 1 ACENAPHTHENE 1 ACENAPHTHYLENE 1 ANTHRACENE I BENZO(A)ANTHRACENE 1 BENZO(A)PYRENE I BENZO(B)FLUORANTHENE I BENZO(G,H,I)PERYLENE I BENZO(K)FLUORANTHENE 1 CHRYSENE 1 DIBENZ(A,H)ANTHRACENE 1 FLUORANTHENE 1 FLUORENE 1 INDENO(1,2,3-CD)PYRENE 1 NAPHTHALENE 1 PHENANTHRENE 1 PYRENE 1 Surrogates: 2-FLUOROBIPHENYL 1 NITROBENZENE-D5 I TERPHENYL-D14 1 Prep/Method: CALUFT-DRO/8015/CALUFT-DRO/8 TPH - DRO 1 Surrogates: ORTHOTERPHENYL January 7, 2003 Page 2 Result Unit MDL PQL Date Analyzed 9.33 % 0.50 0.50 Dec 17, 2002 ND U UG/KG 36. 360. Dec 13, 2002 ND U UG/KG 36. 360. Dec 13, 2002 45. J UG/KG 36. 360. Dec 13, 2002 ND U UG/KG 36. 360. Dec 13, 2002 71. J UG/KG 36. 360. Dec 13, 2002 210. J UG/KG 36. 360. Dec 13, 2002 91. 1 UG/KG 36. 360. Dec 13, 2002 160. J UG/KG 36. 360. Dec 13, 2002 ND U LIG/KG 36. 360. Dec 13, 2002 55. J UG/KG 36. 360. Dec 13, 2002 250. J UG/KG 36. 360. Dec 13, 2002 ND U UG/KG 36. 360. Dec 13, 2002 990. UG/KG 36. 360. Dec 13, 2002 68. J UG/KG 36. 360. Dec 13, 2002 ND U UG/KG 36. 360. Dec 13, 2002 ND U UG/KG 36. 360. Dec 13, 2002 400. UG/KG 36. 360. Dec 13, 2002 800. UG/KG 36. 360. Dec 13, 2002 ND U MG/KG 11. 33. 75.0 RPR Comments: ALL RESULTS AND LIMITS ARE REPORTED ON A DRY WEIGHT BASIS Qualifiers: U The constituent should be considered not detected. J The result is between MDL and PQL and should be considered an estimate. Dec 13, 2002 Dec 13, 2002 Dec 13, 2002 Dec 19, 2002 Dec 19, 2002 DEQ-CFW-00025534 Corporate Environmental Database Lab Analysis Report Location- FAYETTEVILLE Job Name- SWMU6-2002 C of C Sampteid: FAY-S-SWMU06-01A(4-5)-DUP Sampling Point: SWMU06-01A Date Sampled: DECEMBER 10, 2002 Lab Sample ID: 3958279-1 Analysis Lab: LANCAS Sample Type: SOIL QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution Result Method: 160.3 MOD. MOISTURE 1 11.2 Prep/Method: 35508/8270C Unit MDL POL Date Analyzed % 0.50 0.50 Dec 13, 2002 1-METHYLNAPHTHALENE 1 ND U UG/KG 37. 370. Dec 16, 2002 2-METHYLNAPHTHALENE I NO U UG/KG 37. 370. Dec 16, 2002 ACENAPHTHENE 1 NO U UG/KG 37. 370. Dec 16, 2002 ACENAPHTHYLENE 1 NO U UG/KG 37. 370. Dec 16, 2002 ANTHRACENE 1 NO U UG/KG 37. 370. Dec 16, 2002 BENZO(A)ANTHRACENE 1 91. 1 UG/KG 37. 370. Dec 16, 2002 BENZO(A)PYRENE 1 46. 1 UG/KG 37. 370. Dec 16, 2002 BENZO(B)FLUORANTHENE 1 71. 1 UG/KG 37. 370. Dec 16, 2002 BENZO(G,H,I)PERYLENE 1 ND U UG/KG 37. 370. Dec 16, 2002 BENZO(K)FLUORANTHENE 1 ND U UG/KG 37. 370. Dec 16, 2002 CHRYSENE 1 88. 1 UG/KG 37. 370. Dec 16, 2002 DIBENZ(A,H)ANTHRACENE 1 ND U UG/KG 37. 370. Dec 16, 2002 FLUORANTHENE 1 450. UG/KG 37. 370. Dec 16, 2002 FLUORENE 1 39. J UG/KG 37. 370. Dec 16, 2002 INDENO(1,2,3-CD)PYRENE 1 ND U UG/KG 37. 370. Dec 16, 2002 NAPHTHALENE 1 NO U UG/KG 37. 370. Dec 16, 2002 PHENANTHRENE 1 210. 1 UG/KG 37. 370. Dec 16, 2002 PYRENE 1 400. UG/KG 37. 370. Dec 16, 2002 Surrogates: 2-FLUOROBIPHENYL 1 97.0 RPR Dec 16, 2002 NITROBENZENE-D5 1 91.0 RPR Dec 16, 2002 TERPHENYL-D14 1 95.0 RPR Dec 16, 2002 Prep/Method: CALUFT-DRO/8015/CALUFT-DROZ8 TPH - DRO 1 NO U MG/KG 11. 34. Dec 19, 2002 Surrogates: ORTHOTERPHENYL d Comments: ALL RESULTS AND LIMITS ARE REPORTED ON A DRY WEIGHT BASIS Qualifiers: U The constituent should be considered not detected. J The result is between MDL and PQL and should be considered an estimate. Dec 19, 2002 DEQ-CFW-00025535 Corporate Environmental Database Lab Analysis Report Location: mwsTTEv/LLs January 9, 2000 Job Name: nwMmh ow'2002 puye 1 c of : numpleid: rxx-K-somLK-wApaw'mwY1 Sampling Point: EugLK-wArow-ox,1 Date Sampled: oEcsmeen 5, 2002 Lab Sample ID: 3955487'1 xnuiyuia Lab: L*wcxx Sample Type, nLxwm uwTsn uc Level: oc (xuum oc Process) Dilution Result Unit MDL PQL Date Analyzed Method: 300.0 xmumIus 5 mu u mG/L 1'5 3'0 Dec 18^ znoZ FLUORIDE 5 wn u mo/L 0'40 0'50 Dec 18, zooz Method: 8015B nsroAwoL (a, oInsu7 INJECTION) 1 wu u uo/L 200' 1000' Dec 13, 2002 Surrogates: ACETONE 1 101.0 npn Dec 13, 2002 /,1,1,2-rsreAoxLonusrwme l NO u us/L 1' 5' Dec 12, 2002 1,1,1-rn/c*LomosTmwE 1 NO u us/L 0.8 5' Dec 12, 2002 1,1,2,2-rsTm*cxLOmosrwws 1 NO u uu/L 1' 5' Dec 12, 2002 1,1,2'TnzuoLoxus7oxws 1 NO o ua/L 0'8 5- Dec 12, 2002 1,1-ozcoLonosmAws 1 NO o uo/L 1' 5' Dec 12, 2002 1,1-oIoxLuwosrxsws 1 NO u us/L 0'8 5' Dec 12, 2002 1,2,3-TnIcxLnxoPnon*ws 1 NO o ou/L 1' 5' Dec 13, 2002 1.2'oIanowo-3-c*LoxopnoPxws I wn o ua/L 2' 5' Dec 12, 2002 1,2-uIononosmxwe 1 xo u os/L 1' y. Dec 12, 2002 1,2-uIcoLoxoBswzsws 1 wn u uo/L �. 5' Dec 12, 2002 1,2-oICoLowocTxawc 1 wo u uu/L 1' 5' Dec 12, znOZ 1.2-oIcxLomopmopxwE 1 wo o oo/L 1, 5' Dec 12, 2002 1,3-oIcocnxooswzsws 1 wo o uu/L 1' 5- Dec 12, 2002 1,4-mIcxLonomswZsmE 1 wo u uo/L 1- 5' Dec 12, 2002 2-uurAwows 1 wo u us/L 3' 10' Dec 12' ZnnZ 2'cxLono-1,3-Bur*uIsws 1 wu u uu/L 1' 5. Dec 12, 2002 2'xExawows 1 wo o os/L 3' 10- Dec 12, 2002 4'mETovL-2-psmTAwows 1 wo u oa/L 3- 10. Dec 12, 2002 wcsrnws 1 wo y uo/L a' 20. Dec 12, 2002 x:sTowITnILs 1 wo u oo/L 25- 100' Dec 12, 2002 «LoL cxLonIos 1 wo u um/L 1' s- Dec 12^ 2002 aswcsws 1 wo u wu/L 0-5 ]' Dec 12, 2002 mnnMnoIcxLomomsro*wE 1 wo u ou/L 1- s' Dec 12, 2002 onownponm 1 wo u wo/L 1' 5' Dec 12, 2002 onnmnnErxAws 1 wo u uo/L 1' 5' Dec 12, 2002 ounmow oIouLrznc 1 NO u oo/L 1' 5' Dec 12, zouz ownmow 7ETnAcxLonIus 1 wn u oa/L 1' 5' Dec 12, 2002 uoLonunEwZEws 1 wo u um/L 0'8 5' Dec 12, 2002 c*Lowosrx*ws 1 wu u yu/L 1' 5' Dec 12, 2002 cxLoworonn l wn u ou/L Q'& 5' Dec 12, 2002 CoLonons7xmws 1 wo u uo/L 1' 5' Dec 12, 2002 CIS-1,2-oIcoLoanETxEwE 1 NO u us/L 0'8 n' Dec 12, 2002 cIs-1,3-oIcoLoaopnopswE 1 NO u ua/L 1' 5' Dec 12, 2002 oIanoM000LomomsTm*wE 1 NO u us/L 1' 5' Dec 12, 2802 oIunoMowsr*xwe 1 NO u ua/L 1' 5' Dec 12, 2002 oIcxLomouzrLuonmwE7xx*s 1 wm u us/L Z' 5' Dec 12, 2002 ETHYL mETowcn,L*7s 1 NO u us/L 1' 5' Dec 12' 2002 cmYLoswasws 1 NO u oo/L n'B 5' Dec 12, ZOOZ ImouurrL xLmoxoL 1 NO u mu/L 100' asu' Dec 12, 2802 msT*xcavLowImILs 1 NO u uu/L 10. 50' Dec 12, 2002 msrxYL IooIms 1 wo u us/L 1. 5' Dec 12, 2003 METHYL msrxAnuYLxrE 1 wo u uu/L 1' s' Dec 12, 2002 msrxvLsws cxLonIos 1 wu u uG/L Z' 5' Dec 12, 2002 pEw7xcoLonoeToAws 1 wn u uu/L 1' 5' Dec 12, 2002 pxoPIowz7aILc 1 wn o uo/L 30' 100. Dec 12, 2002 mrYxsws 1 wo u us/L 1' 5' Dec 12, ZUVz TETRxoxLonos7xsws 1 NO u uo/L 0'9 5' Dec 12, 2002 rnLuswe 1 NO u ua/L 0'7 5' Dec 12, 2002 mxwo 1'a o/c*LonosTxsws 1 NO u us/L o'a 5' Dec 12. 2002 rmAwn-1,3'ozcxLomopRopswc 1 NO o um/L 1' 5' Dec 12, 2002 7nxws-1 4-nzc*Lono-2-euTsws 1 NO u us/L 15. 50 ' Dec1Z ' aonZ mI:oLO�osTxswp 1 wo o uo/� 1' 5' Dec 122002 r*/cxLoxopLoonnMeTx«ws 1 NO o ms/L Z' s' Dec 12, 2002 VINYL AcsraTc 1 wn y uo/L c. 10' Dec 12. 2002 VINYL coLoeIos 1 wm u oo/L 1' 5' Dec 12, 2002 xrLEwE (TOTAL) I NO u us/L o'o s' Dec 12, 2002 Corporate Environmental Database Lab Analysis Report Locations FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 2 C of C Sampleid: FAY-K-EQBLK-NAFGW-DAY1 Sampling Point: EQBLK-NAFGW-DAY1 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3955487-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution RPR Date Analyzed ----------------- -------- ---------------- �1 1,2-DICHLOROETHANE-D4 1 102.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 98.0 RPR Dec 12, 2002 DISROMOFLUOROMETHANE 1 101.0 RPR Dec 12, 2002 TOLUENE-D8 1 104.0 RPR Dec 12, 2002 Prep/Method: 351OCZ8270C 1,2,4,5-TETRACHLOROSENZENE 1 NO U UG/L 2. 11. Dec 16, 2002 1,2,4-TRICHLOROBENZENE 1 NO U UG/L 1. 11. Dec 16, 2002 1,3,5-TRINITROBENZENE 1 NO U UG/L 5. 21. Dec 16, 2002 1,3-DINITROBENZENE 1 ND U UG/L 2. 11. Dec 16, 2002 1,4-DIOXANE 1 NO U UG/L 1. 5. Dec 16, 2002 1,4-NAPHTHOQUINONE 1 ND U UG/L 11. 110. Dec 16, 2002 1,4-PHENYLENEDIAMINE 1 NO U UG/L 64. 210. Dec 16, 2002 1-NAPHTHYLAMINE 1 NO U UG/L 5. 27. Dec 16, 2002 2,3,4,6-TETRACHLOROPHENOL 1 NO U UG/L 2. 11. Dec 16, 2002 2,4,5-TRICHLOROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2,4,6-TRICHLOROPHENOL 1 NO U UG/L 1. 11. Dec 16, 2002 2,4-DICHLOROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2,4-DIMETHYLPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2,4-DINITROPHENOL 1 ND U UG/L 21. 64. Dec 16, 2002 2,4-DINITROTOLUENE 1 ND U UG/L 1. 11. Dec 16, 2002 2,6-DICHLOROPHENOL 1 ND U UG/L 2. 11. Dec 16, 2002 2,6-DINITROTOLUENE 1 ND U UG/L 1. 11. Dec 16, 2002 2-ACETYLAMINOFLUORENE 1 ND U UG/L 2. 11. Dec 16, 2002 2-CHLORONAPHTHALENE 1 ND U UG/L 1. 11. Dec 16, 2002 2-CHLOROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2-METHYLNAPHTHALENE 1 ND U UG/L 1. 11. Dec 16, 2002 2-METHYLPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2-NAPHTHYLAMINE 1 ND U UG/L 5. 27. Dec 16, 2002 2-NITROANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 2-NITROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2-PICOLINE 1 ND U UG/L 2. 11. Dec 16, 2002 3,31-DICHLOROBENZIDINE 9 ND U UG/L 1. 11. Dec 16, 2002 3,31-DIMETHYLBENZIDINE 1 ND U UG/L 5. 27. Dec 16, 2002 3-METHYLCHOLANTHRENE 1 ND U UG/L 2. 11. Dec 16, 2002 3-NITROANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 4,6-DINITRO-2-METHYLPHENOL 1 NO U UG/L 5. 27. Dec 16, 2002 4-AMINOBIPHENYL 1 ND U UG/L 2. 11. Dec 16, 2002 4-BROMOPHENYL-PHENYLETHER 1 NO U UG/L 1. 11. Dec 16, 2002 4-CHLORO-3-METHYLPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 4-CHLOROANILINE 1 NO U UG/L 1. 11. Dec 16, 2002 4-CHLOROPHENYL-PHENYLETHER 1 ND U UG/L 1. 11. Dec 16, 2002 4-METHYLPHENOL 1 ND U UG/L 2. 11. Dec 16, 2002 4-NITROANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 4-NITROPHENOL 1 ND U UG/L 11. 53. Dec 16, 2002 4-NITROQUINOLINE-1-OXIDE 1 ND U UG/L 21. 110. Dec 16, 2002 5-NITRO-0-TOLUIDINE 1 ND U UG/L 3. 11. Dec 16, 2002 7,12-DIMETHYLBENZIA)ANTHRACENE 1 ND U UG/L 2. 11. Dec 16, 2002 A,A-DIMETHYLPHENETHYLAMINE 1 ND U UG/L 1. 53. Dec 16, 2002 ACENAPHTHENE 1 ND U UG/L 1. 11. Dec 16, 2002 ACENAPHTHYLENE 1 IND U UG/L 1. 11. Dec 16, 2002 ACETOPHENONE 1 ND U UG/L 2. 11. Dec 16, 2002 ANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 ANTHRACENE 1 NO U UG/L 1. 11. Dec 16, 2002 ARAMITE 1 ND U UG/L 1. 53. Dec 16, 2002 BENZO(A)ANTHRACENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZO(A)PYRENE 1 NO U UG/L 1. 11. Dec 16, 2002 BENZO(B)FLUORANTHENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZO(G,H,I)PERYLENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZO(K)FLUORANTHENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZYL ALCOHOL 1 ND U UG/L 5. 21. Dec 16, 2002 BIS(2-CHLOROETHOXY)METHANE 1 ND U UG/L 1. 11. Dec 16, 2002 BIS(2-CHLOROETHYL)ETHER 1 ND U UG/L 1. 11. Dec 16, 2002 SIS(2-CHLOROISOPROPYL)ETHER 1 NO U UG/L 1. 11. Dec 16, 2002 BIS(2-ETHYLHEXYL)PHTHALATE 1 ND U UG/L 2. 11. Dec 16, 2002 BUTYLBENZYLPHTHALATE 1 ND U UG/L 2. 11. Dec 16, 2002 CHLOROBENZILATE 1 ND U UG/L 3. 21. Dec 16, 2002 DEQ-CFW 00025537 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 3 C of C SampLeid: FAY-K-EQBLK-NAFGW-DAY1 Sampling Point: EQBLK-NAFGW-DAYI Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3955487-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) AnaLytelParameter Dilution Result Unit MDL PQL Date Analyzed CHRYSENE 1 ND U UG—T T.- 11. Dec 16, 2002 DI-N-BUTYLPHTHALATE 1 ND U UG/L 2. 11. Dec 16, 2002 DI-N-OCTYLPHTHALATE 1 ND U UG/L 2. 11. Dec 16, 2002 DIALLATE TRANS/CIS 1 NO U UG/L 1. 11. Dec 16, 2002 DIBENZ(A,H)ANTHRACENE 1 ND U UG/L 1. 11. Dec 16, 2002 DIBENZOFURAN 1 ND U UG/L 1. 11. Dec 16, 2002 DIETHYLPHTHALATE 1 ND U UG/L 2. 11. Dec 16, 2002 DIMETHOATE 1 NO U UG/L 3. 21. Dec 16, 2002 DIMETHYLPHTHALATE 1 ND U UG/L 2. 11. Dec 16, 2002 ETHYL METHANESULFONATE 1 ND U UG/L 2. 11. Dec 16, 2002 FLUORANTHENE 1 ND U UG/L 1. 11. Dec 16, 2002 FLUORENE 1 ND U UG/L 1. 11. Dec 16, 2002 HEXACHLOROBENZENE I ND U UG/L 1. 11. Dec 16, 2002 NEXACHLOROBUTADIENE 1 NO U UG/L 1. 11. Dec 16, 2002 HEXACHLOROCYCLOPENTADIENE 1 ND U UG/L 5. 27. Dec 16, 2002 HEXACHLOROETHANE 1 ND U UG/L 1. 11. Dec 16, 2002 HEXACHLOROPROPENE I ND U UG/L 2. 11. Dec 16, 2002 INDENO(1,2,3-CD)PYRENE I ND U UG/L 1. 11. Dec 16, 2002 ISODRIN 1 ND U UG/L 1. 11. Dec 16, 2002 ISOPHORONE 1 ND U UG/L 1. 11. Dec 16, 2002 ISOSAFROLE 1 ND U UG/L 1. 11. Dec 16, 2002 METHAPYRILENE 1 ND U UG/L 3. 11. Dec 16, 2002 METHYL METHANESULFONATE 1 ND U UG/L 1. 11. Dec 16, 2002 N-NITROSO-DI-N-PROPYLAMINE 1 ND U UG/L 1. 11. Dec 16, 2002 N-NITROSODI-N-BUTYLAMINE 1 NO U UG/L 2. 11. Dec 16, 2002' N-NITROSODIETHYLAMINE 1 ND U UG/L 2. 11. Dec 16, 2002 N-NITROSODIMETHYLAMINE 1 ND U UG/L 2. 11. Dec 16, 2002 N-NITROSODIPHENYLAMINE I ND U UG/L 2. 11. Dec 16, 2002 N-NITROSOMETHYLETHYLAMINE 1 ND U UG/L 2. 11. Dec 16, 2002 N-NITROSOMORPHOLINE 1 ND U UG/L 2. 11. Dec 16, 2002 N-NITROSOPIPERIDINE 1 ND U UG/L 2. 11. Dec 16, 2002 N-NITROSOPYRROLIDINE 1 NO U UG/L 2. 11. Dec 16, 2002 NAPHTHALENE 1 ND U UG/L 1. 11. Dec 16, 2002 NITROBENZENE 1 ND U UG/L 1. 11. Dec 16, 2002 0,0,0-TRIETHYLPHOSPHOROTHIOATE 1 ND U UG/L 2. 11. Dec 16, 2002 O-TOLUIDINE 1 ND U UG/L 1. 11. Dec 16, 2002 P-DIMETHYLAMINOAZOBENZENE I ND U UG/L 2. 11. Dec 16, 2002 PENTACHLOROBENZENE 1 ND U UG/L 2. 11. Dec 16, 2002 PENTACHLORONITROBENZENE 1 ND U UG/L 2. 11. Dec 16, 2002 PENTACHLOROPHENOL 1 NO U UG/L 3. 27. Dec 16, 2002 PHENACETIN 1 ND U UG/L 2. 11. Dec 16, 2002 PHENANTHRENE 1 ND U UG/L 1. 11. Dec 16, 2002 PHENOL 1 NO U UG/L 1. 11. Dec 16, 2002 PRONAMIDE 1 ND U UG/L 1. 11. Dec 16, 2002 PYRENE 1 ND U UG/L 1. 11. Dec 16, 2002 PYRIDINE 1 ND U UG/L 2. 11. Dec 16, 2002 SAFROLE 1 ND U UG/L 2. 11. Dec 16, 2002 TETRAETHYLDITHIOPYROPHOSPHATE I ND U UG/L 1. 11. Dec 16, 2002 THIONAZIN 1 ND U UG/L 2. 11. Dec 16, 2002 Surrogates: 2,4,6-TRIBROMOPHENOL 1 97.0 RPR Dec 16, 2002 2-FLLIOROBIPHENYL 1 99.0 RPR Dec 16, 2002 2-FLUOROPHENOL 1 61.0 RPR Dec 16, 2002 NITROBENZENE-D5 1 97.0 RPR Dec 16, 2002 PHENOL-D6 1 39.0 RPR Dec 16, 2002 TERPHENYL-D14 1 90.0 RPR Dec 16, 2002 8270C (3-METHYLPHENOL and 4-METHYLPHENOL): These compounds cannot be resolved under the chromatographic conditions used for sample analysis. The result reported for 4-MethyLphenoL represents the combined total of both compounds. 8270C: Due to insufficient sample, the reporting limits for the semivotatile compounds were raised. 8270C (ARAMITE and A,A-DIMETHYLPHENETHYLAMINE): These cpds. were calibrated for using a single point standard at 50 ppm. 8270C (N-NITROSODIPHENYLAMINE): N-Nitrosodiphenytamine decomposes in the GC inlet forming diphenyLamine. The result reported represents the combined total of both compounds. DEQ-CFW-00025538 Corporate Environmental Databam-9 Lab Analysis Report I Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF1 Sampling Point: NAF1 Date Sampled: DECEMBER 6, 2002 Lab Sample ID: 3956307-1 Analysis Sample Type; GROUND WATER QC Level: QC (ADQM QC Process) Lab: LANCAS January 9, 2003 Page 5 AnatyteLParameter Dilution Result Unit MDL PQL Date Analyzed Method: 300.0 FLUORIDE 5 ND U MG/L 0.40 0.50 Dec 17, 2002 Method: 8015B METHANOL (BY DIRECT INJECTION) 1 NO U UG/L 200. 1000. Dec 13, 2002 Surrogates: ACETONE 1 102.0 RPR Dec 13, 2002 Prep/Method: 503OB/8260B 1,1,1,2-TETRACHLOROETHANE I NO U UG/L 1. 5. Dec 12, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 12, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L. 1. 5. Dec 12, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 12, 2002 1,4-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 12, 2002 2-BUTANONE 1 NO U UGA 3. 10. Dec 12, 2002 2-CHLORO-1,3-BUTADIENE 1 NO U UG/L 1. 5. Dec 12, 2002 2-HEXANONE 1 NO U UG/L 3. 10. Dec 12, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 12, 2002 ACETONE 1 ND U UG/L 6. 20. Dec 12, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 12, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 BENZENE 1 NO U UG/L 0.5 5. Dec 12, 2002 BROMODICHLOROMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 BROMOFORM 1 NO U UGA 1. 5. Dec 12, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 12, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 12, 2002 CHLOROBENZENE 1 ND U UG/L. 0.8 5. Dec 12, 2002 CHLOROETHANE 1 ND U UG/L. 1. 5. Dec 12, 2002 CHLOROFORM 1 2. 1 UGA 0.8 5. Dec 12, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 12, 2002 DIBROMOCHLOROMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 DIBROMOMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 DICHLORODIFLUOROMETHANE 1 NO U UG/L 2. 5. Dec 12, 2002 ETHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 12, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 12, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 12, 2002 METHYL IODIDE I ND U UG/L 1. 5. Dec 12, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 12, 2002 METHYLENE CHLORIDE 1 NO U UG/L 2. 5. Dec 12, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 PROPIONITRILE 1 NO U UG/L. 30. 100. Dec 12, 2002 STYRENE 1 NO U UG/L 1. 5. Dec 12, 2002 TETRACHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 12, 2002 TRANS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 TRANS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 12, 2002 TRICHLOROETHENE 1 NO U UG/L 1. 5. Dec 12, 2002 TRICHLOROFLUOROMETHANE I NO U UGIL 2. 5. Dec 12, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 12, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 XYLENE (TOTAL) 1 NO U UG/L 0.8 5. Dec 12, 2002 DEQ-CFW-00025539 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 6 C of C Sampteid: FAY-G-NAF1 Sampling Point: NAF1 Date Sampled: DECEMBER 6, 2002 Lab Sample IDe 3956307-1 Analysis Labe LANCAS Sample Type: GROUND WATER QC Level, QC (ADQM QC Process) Analyte/Parameter Dilution RPR Date Analyzed _________________ -------- ___ Surrogates: 1,2-DICHLOROETHANE-D4 1 103.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 98.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 101.0 RPR Dec 12, 2002 TOLUENE-D8 1 102.0 RPR Dec 12, 2002 Prep/Method: 351OCZ8270C 1,2,4,5-TETRACHLOROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 1,2,4-TRICHLOROBENZENE 1 ND U UG/L 1. 10. Dec 17, 2002 1,3,5-TRINITROBENZENE 1 ND U UG/L 5. 20. Dec 17, 2002 1,3-DINITROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 1,4-DIOXANE 1 NO U UG/L 1. 5. Dec 17, 2002 1,4-NAPHTHOQUINONE 1 ND U UG/L 10. 100. Dec 17, 2002 1,4-PHENYLENEDIAMINE 1 NO U UG/L 60. 200. Dec 17, 2002 1-NAPHTHYLAMINE 1 ND U UG/L 5. 25. Dec 17, 2002 2,3,4,6-TETRACHLOROPHENOL 1 ND U UG/L 2. 10. Dec 17, 2002 2,4,5-TRICHLOROPHENOL 1 NO U UG/L 1. 10. Dec 17, 2002 2,4,6-TRICHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4-DICHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4-DIMETHYLPHENOL 1 NO U UG/L 1. 10. Dec 17, 2002 2,4-DINITROPHENOL 1 ND U UG/L 20. 60. Dec 17, 2002 2,4-DINITROTOLUENE 1 ND U UG/L 1. 10. Dec 17, 2002 2,6-DICHLOROPHENOL 1 ND U UG/L 2. 10. Dec 17, 2002 2,6-DINITROTOLUENE 1 ND U UG/L 1. 10. Dec 17, 2002 2-ACETYLAMINOFLUORENE 1 ND U UG/L 2. 10. Dec 17, 2002 2-CHLORONAPHTHALENE 1 ND U UG/L 1. 10. Dec 17, 2002 2-CHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2-METHYLNAPHTHALENE 1 ND U UG/L 1. 10. Dec 17, 2002 2-METHYLPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2-NAPHTHYLAMINE 1 ND U UG/L 5. 25. Dec 17, 2002 2-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 2-NITROPHENOL 1 NO U UG/L 1. 10. Dec 17, 2002 2-PICOLINE 1 ND U UG/L 2. 10. Dec 17, 2002 3,31-DICHLOROBENZIDINE 1 ND U UG/L 1. 10. Dec 17, 2002 3,3°-DIMETHYLBENZIDINE 1 ND U UG/L 5. 25. Dec 17, 2002 3-METHYLCHOLANTHRENE 1 ND U UG/L 2. 10. Dec 17, 2002 3-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 4,6-DINITRO-2-METHYLPHENOL 1 ND U UG/L 5. 25. Dec 17, 2002 4-AMINOBIPHENYL 1 ND U UG/L 2. 10. Dec 17, 2002 4-BROMOPHENYL-PHENYLETHER 1 ND U UG/L 1. 10. Dec 17, 2002 4-CHLORO-3-METHYLPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 4-CHLOROANILINE 1 NO U UG/L 1. 10. Dec 17, 2002 4-CHLOROPHENYL-PHENYLETHER 1 ND U UG/L 1. 10. Dec 17, 2002 4-METHYLPHENOL 1 ND U UG/L 2. 10. Dec 17; 2002 4-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 4-NITROPHENOL 1 ND U UG/L 10. 50. Dec 17, 2002 4-NITROQUINOLINE-1-OXIDE 1 ND U UG/L 20. 100. Dec 17, 2002 5-NITRO-0-TOLUIDINE 1 ND U UG/L 3. 10. Dec 17, 2002 7,12-DIMETHYLBENZIA)ANTHRACENE 1 ND U UG/L 2. 10. Dec 17, 2002 A,A-DIMETHYLPHENETHYLAMINE 1 ND U UG/L 1. 50. Dec 17, 2002 ACENAPHTHENE 1 ND U UG/L 1. 10. Dec 17, 2002 ACENAPHTHYLENE 1 NO U UG/L 1. 10. Dec 17, 2002 ACETOPHENONE 1 NO U UG/L 2. 10. Dec 17, 2002 ANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 ANTHRACENE 1 ND U UG/L 1. 10. Dec 17, 2002 ARAMITE 1 ND U UG/L 1. 50. Dec 17, 2002 BENZO(A)ANTHRACENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(A)PYRENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(B)FLUORANTHENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(G,H,I)PERYLENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(K)FLUORANTHENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZYL ALCOHOL 1 ND U UG/L 5. 20. Dec 17, 2002 BIS(2-CHLOROETHOXY)METHANE 1 ND U UG/L 1. 10. Dec 17, 2002 BIS(2-CHLOROETHYL)ETHER 1 ND U UG/L 1. 10. Dec 17, 2002 BIS(2-CHLOROISOPROPYL)ETHER 1 ND U UG/L 1. 10. Dec 17, 2002 BIS(2-ETHYLHEXYL)PHTNALATE 1 ND U UG/L 2. 10. Dec 17, 2002 BUTYLBENZYLPHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 CHLOROBENZILATE 1 ND U UG/L 3. 20. Dec 17, 2002 DEQ-CFW 00025540 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C Sampleid: FAY-G-NAF1 Sampling Point: NAF1 Date Sampled: DECEMBER 6, 2002 Lab Sample ID: 3956307-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) January 9, 2003 Page 7 Anatyte/Parameter Dilution Result Unit MDL PQL Date Analyzed CHRYSENE 1 ND U UG­/L TT 10. Dec 17, 2002 DI-N-BUTYLPHTHALATE 1 ND U UGIL 2. 10. Dec 17, 2002 DI-N-OCTYLPHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 DIALLATE TRANS/CIS 1 NO U UG/L 1. 10. Dec 17, 2002 DIBENZ(A,H)ANTHRACENE 1 NO U UG/L 1. 10. Dec 17, 2002 DIBENZOFURAN 1 ND U UG/L 1. 10. Dec 17, 2002 DIETHYLPHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 DIMETHOATE 1 ND U UG/L 3. 20. Dec 17, 2002 DIMETHYLPHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 ETHYL METHANESULFONATE 1 ND U UG/L 2. 10. Dec 17, 2002 FLUORANTHENE 1 ND U UG/L 1. 10. Dec 17, 2002 FLUORENE 1 NO U UG/L 1. 10. Dec 17, 2002 HEXACHLOROBENZENE 1 NO U UG/L 1. 10. Dec 17, 2002 HEXACHLOROBUTADIENE 1 NO U UG/L 1. 10. Dec 17, 2002 HEXACHLOROCYCLOPENTADIENE 1 ND U UG/L 5. 25. Dec 17, 2002 HEXACHLOROETHANE 1 ND U UG/L 1. 10. Dec 17, 2002 HEXACHLOROPROPENE 1 ND U UG/L 2. 10. Dec 17, 2002 INDENO(1,2,3-CD)PYRENE 1 ND U UG/L 1. 10. Dec 17, 2002 ISODRIN 1 NO U UG/L 1. 10. Dec 17, 2002 ISOPHORONE 1 ND U UG/L 1. 10. Dec 17, 2002 ISOSAFROLE 1 ND U UG/L 1. 10. Dec 17, 2002 METHAPYRILENE 1 ND U UG/L 3. 10. Dec 17, 2002 METHYL METHANESULFONATE 1 ND U UG/L 1. 10. Dec 17, 2002 N-NITROSO-DI-N-PROPYLAMINE 1 NO U UG/L 1. 10. Dec 17, 2002 N-NITROSODI-N-BUTYLAMINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSODIETHYLAMINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITkOSODIMETHYLAMINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSODIPHENYLAMINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSOMETHYLETHYLAMINE 1 NO U UG/L 2. 10. Dec 17, 2002 N-NITROSOMORPHOLINE 1 NO U UG/L 2. 10. Dec 17, 2002 N-NITROSOPIPERIDINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSOPYRROLIDINE 1 ND U UG/L 2. 10. Dec 17, 2002 NAPHTHALENE 1 ND U UG/L 1. 10. Dec 17, 2002 NITROBENZENE 1 ND U UG/L 1. 10. Dec 17, 2002 0,0,0-TRIETHYLPHOSPHOROTHIOATE 1 ND U UG/L 2. 10. Dec 17, 2002 O-TOLUIDINE 1 ND U UG/L 1. 10. Dec 17, 2002 P-DIMETHYLAMINOAZOBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 PENTACHLOROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 PENTACHLORONITROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 PENTACHLOROPHENOL 1 NO U UG/L 3. 25. Dec 17, 2002 PHENACETIN 1 ND U UG/L 2. 10. Dec 17, 2002 PHENANTHRENE 1 ND U UG/L 1. 10. Dec 17, 2002 PHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 PRONAMIDE I ND U UG/L 1. 10. Dec 17, 2002 PYRENE 1 ND U UG/L 1. 10. Dec 17, 2002 PYRIDINE 1 ND U UG/L 2. 10. Dec 17, 2002 SAFROLE 1 ND U UG/L 2. 10. Dec 17, 2002 TETRAETHYLDITHIOPYROPHOSPHATE 1 ND U UG/L 1. 10. Dec 17, 2002 THIONAZIN 1 ND U UG/L 2. 10. Dec 17, 2002 Surrogates: 2,4,6-TRIBROMOPHENOL 1 88.0 RPR Dec 17, 2002 2-FLUOROBIPHENYL 1 81.0 RPR Dec 17, 2002 2-FLUOROPHENOL 1 48.0 RPR Dec 17, 2002 NITROBENZENE-D5 1 88.0 RPR Dec 17, 2002 PHENOL-D6 1 30.0 RPR Dec 17, 2002 TERPHENYL-D14 1 80.0 RPR Dec 17, 2002 Comments: Field personnel Lined out sample FAY-G-NAF1 for 8015B analysis from CDC 66825 without dating and initiating next to the Lined -out item. 8270C (3-METHYLPHENOL and 4-METHYLPHENOL): These compounds cannot be resolved under the chromatographic conditions used for sample analysis. The result reported for 4-Methylphenot represents the combined total of both compounds. 8270C (ARAMITE and A,A-DIMETHYLPHENETHYLAMINE): These cpds. were calibrated for using a single point standard at 50 ppm. 8270C (N-NITROSODIPHENYLAMINE): N-Nitrosodiphenytamine decomposes in the GC inlet forming diphenyLamine. The result reported represents the combined total of both compounds. DEQ-CFW-00025541 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 9 C of C SampLeid: FAY-G-NAF1 Sampling Point: NAF1 Date Sampled: DECEMBER 6, 2002 Lab Sample ID: 3956307-2 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) AnalyteZParameter Dilution Result Unit MDL PQL Date Analyzed Method: 300.0 CHLORIDE 20 47.1 MG/L 6.0 8.0 Dec 18, 2002 Comments: Field personnel entered sample FAY-G-NAF-1 on COC 66796 for 82608. The sample ID should read FAY-G-NAF1 to be consistent with the other requested analyses. DEQ-CFW-00025542 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF1-ACR Sampling Point: NAF1 Date Sampled: DECEMBER 6, 2002 Lab Sample ID: 3956308-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: OC (ADOM QC Process) Anatyte/Parameter Dilution Result Prep/Method: 503OB18260B ACROLEIN I NO U ACRYLONITRILE 1 NO U Surrogates: 1,2-DICHLOROETHANE-D4 1 92.0 RPR 4-BROMOFLUOROBENZENE 1 104.0 RPR DIBROMOFLUOROMETHANE 1 90.0 RPR TOLUENE-D8 1 105.0 RPR Qualifiers: U The constituent should be considered not detected. January 9, 2003 Page 10 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 10, 2002 UG/L 4. 20. Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 DEQ-CFW-00025543 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF-2-ACR-DUP Sampling Point: NAF2 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956312-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution Result Prep,/Method:_5030B/8260B ACROLEIN 1 ND U ACRYLONITRILE 1 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 94.0 RPR 4-BROMOFLUOROBENZENE 1 106.0 RPR DIBROMOFLUOROMETHANE 1 62.0 RPR TOLUENE-D8 1 106.0 RPR January 9, 2003 Page 11 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 10, 2002 UG/L 4. 20. Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Comments: 8260B (DIBROMOFLUOROMETHANE): Recovery values for surrogate were outside control Limits in the initial and reanalysis, indicating a matrix effect. The pH of this sample is 11. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025544 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C Sampleid: FAY-G-NAF-2-DUP Sampling Point: NAF2 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956311-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) Lab: LANCAS January 9, 2003 Page 12 AnaLyteLParameter Dilution Result Unit MDL POL Date Analyze Method: 300.0 CHLORIDE 200 325. MG/L 60. 80. Dec 18, 2002 FLUORIDE 200 230. MG/L 16. 20. Dec 18, 2002 Method• 8015B METHANOL (BY DIRECT INJECTION) 1 1200. UG/L 200. 1000. Dec 13, 2002 Surrogates: ACETONE 1 113.0 RPR Dec 13, 2002 Prep/Method: 503OB/826OB 1,1,1,2-TETRACHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,1,1-TRICHLOROETHANE 2.5 ND U UG/L 2. 13. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,1,2-TRICHLOROETHANE 2.5 ND U UG/L 2. 13. Dec 12, 2002 1,1-DICHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,1-DICHLOROETHENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 2.5 NO U UGIL 5. 13. Dec 12, 2002 1,2-DIBROMOETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,2-DICHLOROBENZENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,2-DICHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,2-DICHLOROPROPANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 1,3-DICHLOROBENZENE 2.5 NO U UG/L 3. 13. Dec 12, 2002 1,4-DICHLOROBENZENE 2.5 NO U UG/L 3. 13. Dec 12, 2002 2-BUTANONE 2.5 ND U UG/L 8. 25. Dec 12, 2002 2-CHLORO-1,3-BUTADIENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 2-HEXANONE 2.5 ND U UG/L 8. 25. Dec 12, 2002 4-METHYL-2-PENTANONE 2.5 ND U UG/L 8. 25. Dec 12, 2002 ACETONE 2.5 45. J UG/L 15. 50. Dec 12, 2002 ACETONITRILE 2.5 ND U UG/L 63. 250. Dec 12, 2002 ALLYL CHLORIDE 2.5 ND U UG/L 3. 13. Dec 12, 2002 BENZENE 2.5 ND U UG/L 1. 13. Dec 12, 2002 BROMODICHLOROMETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 BROMOFORM 2.5 ND U UG/L 3. 13. Dec 12, 2002 BROMOMETHANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 CARBON DISULFIDE 2.5 5. 1 UG/L 3. 13. Dec 12, 2002 CARBON TETRACHLORIDE 2.5 NO U UG/L 3. 13. Dec 12, 2002 CHLOROBENZENE 2.5 NO U UG/L 2. 13. Dec 12, 2002 CHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 CHLOROFORM 2.5 ND U UGIL 2. 13. Dec 12, 2002 CHLOROMETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 DIBROMOCHLOROMETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 DIBROMOMETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 DICHLORODIFLUOROMETHANE 2.5 NO U UG/L 5. 13. Dec 12, 2002 ETHYL METHACRYLATE 2.5 ND U UG/L 3. 13. Dec 12, 2002 ETHYLBENZENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 ISOBUTYL ALCOHOL 2.5 ND U UG/L 250. 630. Dec 12, 2002 METHACRYLONITRILE 2.5 ND U UG/L 25. 130. Dec 12, 2002 METHYL IODIDE 2.5 NO U UG/L 3. 13. Dec 12, 2002 METHYL METHACRYLATE 2.5 ND U UG/L 3. 13. Dec 12, 2002 PENTACHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 PROPIONITRILE 2.5 ND U UG/L 75. 250. Dec 12, 2002 STYRENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 TETRACHLOROETHENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 TOLUENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 TRANS-1,2-DICHLOROETHENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 TRANS-1,3-DICHLOROPROPENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 TRANS-1,4-DICHLORO-2-BUTENE 2.5 ND U UG/L 38. 130. Dec 12, 2002 TRICHLOROETHENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 TRICHLOROFLUOROMETHANE 2.5 ND U UG/L 5. 13. Dec 12, 2002 VINYL ACETATE 2.5 NO U UG/L 5. 25. Dec 12, 2002 VINYL CHLORIDE 2.5 ND U UG/L 3. 13. Dec 12, 2002 XYLENE (TOTAL) 2.5 ND U UG/L 2. 13. Dec 12, 2002 DEQ-CFW-00025545 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 13 C of C Sampleid: FAT-G-NAF-2-DUP Sampling Point: NAF2 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956311-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution RPR Date Analyzed ----------------- -------- --- Surrogates: 1,2-DICHLOROETHANE-D4 1 104.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 98.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 102.0 RPR Dec 12, 2002 TOLUENE-D8 1 102.0 RPR Dec 12, 2002 Prep/Method: 351OC18270C 1,2,4,5-TETRACHLOROBENZENE 1 NO U UG/L 2. 10. Dec 17, 2002 1,2,4-TRICHLOROBENZENE 1 NO U UG/L 1. 10. Dec 17, 2002 1,3,5-TRINITROBENZENE 1 ND U UG/L 5. 20. Dec 17, 2002 1,3-DINITROBENZENE 1 NO U UG/L 2. 10. Dec 17, 2002 1,4-DIOXANE 1 2. J UG/L 1. 5. Dec 17, 2002 1,4-NAPHTHDQUINONE 1 ND U UG/L 10. 100. Dec 17, 2002 1,4-PHENYLENEDIAMINE 1 ND U UG/L 60. 200. Dec 17, 2002 1-NAPHTHYLAMINE 1 ND U UG/L 5. 25. Dec 17, 2002 2,3,4,6-TETRACHLOROPHENOL 1 ND U UG/L 2. 10. Dec 17, 2002 2,4,5-TRICHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4,6-TRICHLOROPHENOL 1 NO U UG/L 1. 10. Dec 17, 2002 2,4-DICHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4-DIMETHYLPHENOL 1 NO U UG/L 1. 10. Dec 17, 2002 2,4-DINITROPHENOL 1 NO U UG/L 20. 60. Dec 17, 2002 2,4-DINITROTOLUENE 1 NO U UG/L 1. 10. Dec 17, 2002 2,6-DICHLOROPHENOL 1 NO U UG/L 2. 10. Dec 17, 2002 2,6-DINITROTOLUENE 1 NO U UG/L 1. 10. Dec 17, 2002 2-ACETYLAMINOFLUORENE 1 NO U UG/L 2. 10. Dec 17, 2002 2-CHLORONAPHTHALENE 1 NO U UG/L 1. 10. Dec 17, 2002 2-CHLOROPHENOL 1 NO U UG/L 1. 10. Dec 17, 2002 2-METHYLNAPHTHALENE 1 NO U UG/L 1. 10. Dec 17, 2002 2-METHYLPHENOL 1 NO U UG/L 1. 10. Dec 17, 2002 2-NAPHTHYLAMINE 1 NO U UG/L 5. 25. Dec 17, 2002 2-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 2-NITROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2-PICOLINE 1 ND U UG/L 2. 10. Dec 17, 2002 3,31-DICHLOROBENZIDINE 1 ND U UG/L 1. 10. Dec 17, 2002 3,3°-DIMETHYLBENZIDINE 1 ND U UG/L 5. 25. Dec 17, 2002 3-METHYLCHOLANTHRENE 1 ND U UG/L 2. 10. Dec 17, 2002 3-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 4,6-DINITRO-2-METHYLPHENOL 1 ND U UG/L 5. 25. Dec 17, 2002 4-AMINOBIPHENYL 1 ND U UG/L 2. 10. Dec 17, 2002 4-BROMOPHENYL-PHENYLETHER 1 NO U UG/L 1. 10. Dec 17, 2002 4-CHLORO-3-METHYLPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 4-CHLOROANILINE 1 NO U UG/L 1. 10. Dec 17, 2002 4-CHLOROPHENYL-PHENYLETHER 1 NO U UG/L 1. 10. Dec 17, 2002 4-METHYLPHENOL 1 NO U UG/L 2. 10. Dec 17, 2002 4-NITROANILINE 1 NO U UG/L 1. 10. Dec 17, 2002 4-NITROPHENOL 1 NO U UG/L 10. 50. Dec 17, 2002 4-NITROQUINOLINE-1-OXIDE 1 NO U UG/L 20. 100. Dec 17, 2002 5-NITRO-0-TOLUIDINE 1 NO U UG/L 3. 10. Dec 17, 2002 7,12-DIMETHYLBENZIA)ANTHRACENE 1 NO U UG/L 2. 10. Dec 17, 2002 A,A-DIMETHYLPHENETHYLAMINE 1 NO U UG/L 1. 50. Dec 17, 2002 ACENAPHTHENE 1 NO U UG/L 1. 10. Dec 17, 2002 ACENAPHTHYLENE 1 NO U UG/L 1. 10. Dec 17, 2002 ACETOPHENONE 1 NO U UG/L 2. 10. Dec 17, 2002 ANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 ANTHRACENE 1 NO U UG/L 1. 10. Dec 17, 2002 ARAMITE 1 NO U UG/L 1. 50. Dec 17, 2002 BENZO(A)ANTHRACENE 1 NO U UG/L 1. 10. Dec 17, 2002 BENZO(A)PYRENE 1 NO U UG/L 1. 10. Dec 17, 2002 BENZO(B)FLUORANTHENE 1 NO U UG/L 1. 10. Dec 17, 2002 BENZO(G,H,I)PERYLENE 1 NO U UG/L 1. 10. Dec 17, 2002 BENZO(K)FLUORANTHENE 1 NO U UG/L 1. 10. Dec 17, 2002 BENZYL ALCOHOL 1 11. J UG/L 5. 20. Dec 17, 2002 BIS(2-CHLOROETHOXY)METHANE 1 NO U UG/L 1. 10. Dec 17, 2002 B1S(2-CHLOROETHYL)ETHER 1 NO U UG/L 1. 10. Dec 17, 2002 BIS(2-CHLOROISOPROPYL)ETHER 1 NO U UG/L 1. 10. Dec 17, 2002 BIS(2-ETHYLHEXYL)PHTHALATE 1 3. J UG/L 2. 10. Dec 17, 2002 BUTYLBENZYLPHTHALATE 1 NO U UG/L 2. 10. Dec 17, 2002 CHLOROBENZILATE 1 NO U UG/L 3. 20. Dec 17. 2002 DEQ-CFW 00025546 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF-2-DUP Sampling Point: NAF2 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956311-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Lab: LANCAS January 9, 2003 Page 14 Analyte/Parameter Dilution Result Unit MDL POL Date Analyzed CHRYSENE 1 ND U UG-/--L T-. 10. Dec 17, 2002 DI-N-BUTYLPHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 DI-N-OCTYLPHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 DIALLATE TRANS/CIS 1 NO U UG/L 1. 10. Dec 17, 2002 DIBENZ(A,H)ANTHRACENE 1 ND U UG/L 1. 10. Dec 17, 2002 DIBENZOFURAN 1 ND U UG/L 1. 10. Dec 17, 2002 DIETHYLPHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 DIMETHOATE 1 ND U UG/L 3. 20. Dec 17, 2002 DIMETHYLPHTHALATE 1 NO U UG/L 2. 10. Dec 17, 2002 ETHYL METHANESULFONATE 1 NO U UG/L 2. 10. Dec 17, 2002 FLUORANTHENE 1 NO U UG/L 1. 10. Dec 17, 2002 FLUORENE 1 NO U UG/L 1. 10. Dec 17, 2002 HEXACHLOROBENZENE 1 NO U UG/L 1. 10. Dec 17, 2002 HEXACHLOROBUTADIENE 1 NO U UG/L 1. 10. Dec 17, 2002 HEXACHLOROCYCLOPENTADIENE 1 ND U UG/L 5. 25. Dec 17, 2002 NEXACHLOROETHANE 1 NO U UG/L 1. 10. Dec 17, 2002 HEXACHLOROPROPENE 1 ND U UG/L 2. 10. Dec 17, 2002 INDENO(1,2,3-CD)PYRENE 1 NO U UG/L 1. 10. Dec 17, 2002 ISODRIN 1 NO U UG/L 1. 10. Dec 17, 2002 ISOPHORONE 1 NO U UG/L 1. 10. Dec 17, 2002 ISOSAFROLE 1 NO U UG/L 1. 10. Dec 17, 2002 METHAPYRILENE 1 NO U UG/L 3. 10. Dec 17, 2002 METHYL METHANESULFONATE 1 ND U UG/L 1. 10. Dec 17, 2002 N-NITROSO-DI-N-PROPYLAMINE 1 NO U UG/L 1. 10. Dec 17, 2002 N-NITROSODI-N-BUTYLAMINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSODIETHYLAMINE I ND U UG/L 2. 10. Dec 17, 2002 N-NITROSODIMETHYLAMINE, 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSODIPHENYLAMINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSOMETHYLETHYLAMINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSOMORPHOLINE 1 ND U UG/L 2. 10. Dec 17, 2002 N-NITROSOPIPERIDINE 1 NO U UG/L 2. 10. Dec 17, 2002 N-NITROSOPYRROLIDINE 1 ND U UG/L 2. 10. Dec 17, 2002 NAPHTHALENE 1 1. 1 UG/L 1. 10. Dec 17, 2002 NITROBENZENE 1 ND U UG/L 1. 10. Dec 17, 2002 0,0,0-TRIETHYLPHOSPHOROTHIOATE I ND U UG/L 2. 10. Dec 17, 2002 O-TOLUIDINE 1 ND U UG/L 1. 10. Dec 17, 2002 P-DIMETHYLAMINOAZOBENZENE 1 NO U UG/L 2. 10. Dec 17, 2002 PENTACHLOROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 PENTACHLORONITROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 PENTACHLOROPHENOL 1 ND U UG/L 3. 25. Dec 17, 2002 PHENACETIN 1 ND U UG/L 2. 10. Dec 17, 2002 PHENANTHRENE 1 ND U UG/L 1. 10. Dec 17, 2002 PHENOL 1 1. 1 UG/L 1. 10. Dec 17, 2002 PRONAMIDE 1 ND U UG/L 1. 10. Dec 17, 2002 PYRENE 1 NO U UG/L 1. 10. Dec 17, 2002 PYRIDINE 1 NO U UG/L 2. 10. Dec 17, 2002 SAFROLE 1 NO U UG/L 2. 10. Dec 17, 2002 TETRAETHYLI)ITHIOPYROPHOSPHATE 1 NO U UG/L 1. 10. Dec 17, 2002 THIONAZIN 1 NO U UG/L 2. 10. Dec 17, 2002 Surrogates: 2,4,6-TRIBROMOPHENOL 1 76.0 RPR Dec 17, 2002 2-FLUOROBIPHENYL 1 77.0 RPR Dec 17, 2002 2-FLUOROPHENOL 1 44.0 RPR Dec 17, 2002 NITROBENZENE-D5 1 85.0 RPR Dec 17, 2002 PHENOL-D6 1 29.0 RPR Dec 17, 2002 TERPHENYL-D14 1 80.0 RPR Dec 17. 2002 Comments: 8270C (3-METHYLPHENOL and 4-METHYLPHENOL): These compounds cannot be resolved under the chromatographic conditions used for sample analysis. The result reported for 4-MethyLphenoL represents the combined total of both compounds. 8270C (ARAMITE and A,A-DIMETHYLPHENETHYLAMINE): These cpds. were calibrated for using a single point standard at 50 ppm. 8270C (N-NITROSODIPHENYLAMINE): N-NitrosodiphenyLamine decomposes in the GC inlet forming diphenytamine. The result reported represents the combined total of both compounds. DEQ-CFW-00025547 Corporate Environmental Database Lab Analysis Report Location: p*reTTsvILLs January 0, 2083 Job Name: mwmm\ aw-2002 Page 16 C of c anmpieid: pxY-s-wxp-Z'oup Sampling Point: war2 Date Sampled: mscEmoEm 5, 2002 Lab Sample ID: 3956311-2 anaiynin Lab: LeNcxn Sample Type: snoumn uw7Ex uc Level: Oc (xunw oc Process) Dilution Result� Unit MDL PQL Date AnalyzePrep/Method: 503OB18260B cummxntm: 8Z8Vo (msrxvLsms cxumros): Due to the Level of methvi*ne chloride, the reporting Limits for all oc/Mn vniotiiw compounds were raised. Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWML16 GW-2002 C of C SampLeid: FAY-G-NAF2 Sampling Point: NAF2 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956309-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution Result Unit MDL PQL Date Analyze Method: 300.0 CHLORIDE 100 332. MG/L 30. 40. Dec 18, 2002 FLUORIDE 100 250. MG/L 8.0 10. Dec 18, 2002 Method: 8015B METHANOL (BY DIRECT INJECTION) 1 1900. UG/L 200. 1000. Dec 13, 2002 Surrogates: ACETONE 1 120.0 RPR Dec 13, 2002 Prep/Method: 503OB/8260B 1,1,1,2-TETRACHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,1,1-TRICHLOROETHANE 2.5 NO U UG/L 2. 13. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,1,2-TRICHLOROETHANE 2.5 ND U UG/L 2. 13. Dec 12, 2002 1,1-DICHLOROETHANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 1,1-DICHLOROETHENE 2.5 NO U UG/L 2. 13. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 2.5 NO U UG/L 5. 13. Dec 12, 2002 1,2-DIBROMOETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,2-DICHLOROBENZENE 2.5 NO U UG/L 3. 13. Dec 12, 2002 1,2-DICHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,2-DICHLOROPROPANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 1,3-DICHLOROBENZENE 2.5 NO U UG/L 3. 13. Dec 12, 2002 1,4-DICHLOROBENZENE 2.5 NO U UG/L 3. 13. Dec 12, 2002 2-BUTANONE 2.5 NO U UG/L 8. 25. Dec 12, 2002 2-CHLORO-1,3-BUTADIENE 2.5 NO U UG/L 3. 13. Dec 12, 2002 2-HEXANONE 2.5 NO U UG/L 8. 25. Dec 12, 2002 4-METHYL-2-PENTANONE 2.5 ND U UG/L 8. 25. Dec 12, 2002 ACETONE 2.5 35. J UG/L 15. 50. Dec 12, 2002 ACETONITRILE 2.5 ND U UG/L 63. 250. Dec 12, 2002 ALLYL CHLORIDE 2.5 NO U UG/L 3. 13. Dec 12, 2002 BENZENE 2.5 ND U UG/L 1. 13. Dec 12, 2002 BROMODICHLOROMETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 BROMOFORM 2.5 ND U UG/L 3. 13. Dec 12, 2002 BROMOMETHANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 CARBON DISULFIDE 2.5 ND U UG/L 3. 13. Dec 12, 2002 CARBON TETRACHLORIDE 2.5 NO U UG/L 3. 13. Dec 12, 2002 CHLOROBENZENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 CHLOROETHANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 CHLOROFORM 2.5 ND U UG/L 2. 13. Dec 12, 2002 CHLOROMETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 2.5 ND U UG/L 2. m Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 DIBROMOCHLOROMETHANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 DIBROMOMETHANE 2.5 NO U UG/L 3. 13. Dec 12, 2002 DICHLORODIFLUOROMETHANE 2.5 NO U UG/L 5. 13. Dec 12, 2002 ETHYL METHACRYLATE 2.5 NO U UG/L 3. 13. Dec 12, 2002 ETHYLBENZENE 2.5 NO U UG/L 2. 13. Dec 12, 2002 ISOBUTYL ALCOHOL 2.5 NO U UG/L 250. 630. Dec 12, 2002 METHACRYLONITRILE 2.5 ND U UG/L 25. 130. Dec 12, 2002 METHYL IODIDE 2.5 ND U UG/L 3. 13. Dec 12, 2002 METHYL METHACRYLATE 2.5 ND U UG/L 3. 13. Dec 12, 2002 PENTACHLOROETHANE 2.5 ND U UG/L 3. 13. Dec 12, 2002 PROPIONITRILE 2.5 NO U UG/L 75. 250. Dec 12, 2002 STYRENE 2.5 NO U UG/L 3. 13. Dec 12, 2002 TETRACHLOROETHENE 2.5 ND U UG/L 2. 13. Dec 12, 2002 TOLUENE 2.5 NO U UG/L 2. 13. Dec 12, 2002 TRANS-1,2-DICHLOROETHENE 2.5 NO U UGIL 2. 13. Dec 12, 2002 TRANS-1,3-DICHLOROPROPENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 TRANS-1,4-DICHLORO-2-BUTENE 2.5 ND U UG/L 38. 130. Dec 12, 2002 TRICHLOROETHENE 2.5 ND U UG/L 3. 13. Dec 12, 2002 TRICHLOROFLUOROMETHANE 2.5 NO U UG/L 5. 13. Dec 12, 2002 VINYL ACETATE 2.5 ND U UG/L 5. 25. Dec 12, 2002 VINYL CHLORIDE 2.5 ND U UG/L 3. 13. Dec 12, 2002 XYLENE (TOTAL) 2.5 NO U UG/L 2. 13. Dec 12, 2002 DEQ-CFW-00025549 Corporate Environmental Database Lab Analysis Report Location: Job Name: C of C Sampleid: Sampling Point: Date Sampled: Lab Sample ID: Sample Type: QC Level: Analyte/Parameter ----------------- FAYETTEVILLE SWMU6 GW-2002 FAY-G-NAF2 NAF2 DECEMBER 5, 2002 3956309-1 Analysis GROUND WATER QC (ADQM QC Process) r-11-AKETr Dilution RPR 1,2-DICHLOROETHANE-D4 1 101.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 99.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 99.0 RPR Dec 12, 2002 TOLUENE-D8 1 102.0 RPR Dec 12, 2002 Prep/Method: 3510C/8270C 1,2,4,5-TETRACHLOROBENZENE 1 ND U UG/L 2. 12. Dec 16, 2002 1,2,4-TRICHLOROBENZENE 1 NO U UG/L 1. 12. Dec 16, 2002 1,3,5-TRINITROBENZENE 1 ND U UG/L 6. 25. Dec 16, 2002 1,3-DINITROBENZENE 1 NO U UG/L 2. 12. Dec 16, 2002 1,4-DIOXANE 1 2. J UG/L 1. 6. Dec 16, 2002 1,4-NAPHTHOQUINONE 1 ND U UG/L 12. 120. Dec 16, 2002 1,4-PHENYLENEDIAMINE 1 ND U UG/L 75. 250. Dec 16, 2002 1-NAPHTHYLAMINE 1 ND U UG/L 6. 31. Dec 16, 2002 2,3,4,6-TETRACHLOROPHENOL 1 ND U UG/L 2. 12. Dec 16, 2002 2,4,5-TRICHLOROPHENOL 1 NO U UG/L 1. 12. Dec 16, 2002 2,4,6-TRICHLOROPHENOL 1 NO U UG/L 1. 12. Dec 16, 2002 2,4-DICHLOROPHENOL 1 ND U UG/L 1. 122. Dec 16, 2002 2,4-DIMETHYLPHENOL 1 ND U UG/L 1. 12. Dec 16, 2002 2,4-DINITROPHENOL 1 ND U UG/L 25. 75. Dec 16, 2002 2,4-DINITROTOLUENE 1 ND U UG/L 1. 12. Dec 16, 2002 2,6-DICHLOROPHENOL 1 NO U UG/L 2. 12. Dec 16, 2002 2,6-DINITROTOLUENE 1 ND U UG/L 1. 12. Dec 16, 2002 2-ACETYLAMINOFLUORENE 1 NO U UG/L 2. 12. Dec 16, 2002 2-CHLORONAPHTHALENE 1 ND U UG/L 1. 12. Dec 16, 2002 2-CHLOROPHENOL 1 ND U UG/L 1. 12. Dec 16, 2002 2-METHYLNAPHTHALENE 1 ND U UG/L 1. 12. Dec 16, 2002 2-METHYLPHENOL 1 ND U UG/L 1. 12. Dec 16, 2002 2-NAPHTHYLAMINE 1 ND U UG/L 6. 31. Dec 16, 2002 2-NITROANILINE 1 ND U UG/L 1. 12. Dec 16, 2002 2-NITROPHENOL 1 ND U UG/L 1. 12. Dec 16, 2002 2-PICOLINE 1 ND U UG/L 2. 12. Dec 16, 2002- 3,31-DICHLOROBENZIDINE 1 ND U UG/L 1. 12. Dec 16, 2002 3,31-DIMETHYLBENZIDINE 1 ND U UG/L 6. 31. Dec 16, 2002 3-METHYLCHOLANTHRENE 1 ND U UG/L 2. 12. Dec 16, 2002 3-NITROANILINE 1 ND U UG/L 1. 12. Dec 16, 2002 4,6-DINITRO-2-METHYLPHENOL 1 ND U UG/L 6. 31. Dec 16, 2002 4-AMINOBIPHENYL 1 NO U UG/L 2. 12. Dec 16, 2002 4-BROMOPHENYL-PHENYLETHER 1 ND U UG/L 1. 12. Dec 16, 2002 4-CHLORO-3-METHYLPHENOL 1 ND U UG/L 1. 12. Dec 16, 2002 4-CHLOROANILINE 1 ND U UG/L 1. 12. Dec 16, 2002 4-CHLOROPHENYL-PHENYLETHER 1 ND U UG/L 1. 12. Dec 16, 2002 4-METHYLPHENOL 1 ND U UG/L 2. 12. Dec 16, 2002 4-NITROANILINE 1 ND U UG/L 1. 12. Dec 16, 2002 4-NITROPHENOL 1 NO U UG/L 12. 62. Dec 16, 2002 4-NITROQUINOLINE-1-OXIDE 1 ND U UG/L 25. 120. Dec 16, 2002 5-NITRO-0-TOLUIDINE 1 ND U UG/L 4. 12. Dec 16, 2002 7,12-DIMETHYLBENZ[AIANTHRACENE 1 ND U UG/L 2. 12. Dec 16, 2002 A,A-DIMETHYLPHENETHYLAMINE 1 NO U UG/L 1. 62. Dec 16, 2002 ACENAPHTHENE 1 ND U UG/L 1. 12. Dec 16, 2002 ACENAPHTHYLENE 1 NO U UG/L 1. 12. Dec 16, 2002 ACETOPHENONE 1 NO U UG/L 2. 12. Dec 16, 2002 ANILINE 1 ND U UG/L 1. 12. Dec 16, 2002 ANTHRACENE 1 NO U UG/L 1. 12. Dec 16, 2002 ARAMITE 1 NO U UG/L 1. 62. Dec 16, 2002 BENZO(A)ANTHRACENE 1 NO U UG/L 1. 12. Dec 16, 2002 BENZO(A)PYRENE 1 NO U UG/L 1. 12. Dec 16, 2002 BENZO(B)FLUORANTHENE 1 NO U UG/L 1. 12. Dec 16, 2002 BENZO(G,H,I)PERYLENE 1 NO U UG/L 1. 12. Dec 16, 2002 BENZO(K)FLUORANTHENE 1 NO U UG/L 1. 12. Dec 16, 2002 BENZYL ALCOHOL 1 15. J UG/L 6. 25. Dec 16, 2002 BIS(2-CHLOROETHOXY)METHANE 1 ND U UG/L 1. 12. Dec 16, 2002 BIS(2-CHLOROETHYL)ETHER 1 ND U UG/L 1. 12. Dec 16, 2002 BIS(2-CHLOROISOPROPYL)ETHER 1 ND U UG/L 1. 12. Dec 16, 2002 BIS(2-ETHYLHEXYL)PHTHALATE 1 ND U UG/L 2. 12. Dec 16, 2002 BUTYLBENZYLPHTHALATE 1 ND U UG/L 2. 12. Dec 16, 2002 CHLOROBENZILATE 1 ND U UG/L 4. 25. Dec 16, 2002 DEQ-CFW 00025550 Corporate Environmental Database Lob Analysis Report Location: FArsrrevILLs January 9, 2003 Job Name: SwMu6 ow-2002 pog* 19 o of c oompieid: rxv'n'm*pZ Sampling Point: wxF2 Date Sampled: nEceMoEn 5, 2002 Lob Sample ID: 3958309-1 Analysis Lab: Lxwcxo Sample Type: snoowo wxrEm Ac Levei: nc (xomw uc Process) Result ��� �L fQL Date Analyze mxY�NE � mm o uu/L i 7 12' Dec 16, 2002 nI-m'ouTYupormmuns 1 wo u uo/L 2. 12' Dec 16, 2002 n/-m-ocTYLpxTmxuns 1 wo u uu/L 2' 12' Dec 16, 2002 o/ALLAJE rnAwm/oIo 1 wn u ou/L 1' 12' Dec 16, 2002 uzBswZ(x x)xwmn*cswE 1 wo u Va/L 1' 12. Dec 18, 2002 nIoswzorunAw 1 NO u uo/L 1' 12' Dec 18, 2002 ozsTo,LpoTxnLxTs 1 wo u UG/L 2' 12' Dec 18, 2002 o/msToowrs 1 NO o um/L 4' 25' Dec 16, 2002 ozmaTo,LpxrxALA7s / wo u wo/L 2' 12' Dec 16, 2002 ETHYL Ms7oxNeouLFow*7s 1 wo u ua/L 2' 12' Dec 16, 2002 pLuom^wTxswE NO o uo/L 1' 12' Dec 16, 2002 pLuuxsws 1 NO u uo/L 1' 12' Dec 16, 2002 usxAoxLnxoeswzswc 1 wm u us/L 1' 12' Dec 18, 2002 oExxcxLnnoouT*o/swE 1 wo u uo/L 1' 12' Dec 16. 2002 xsxaCxLonocYcLopswrxoIEms 1 wo o uo/L 6' 31' Dec 18, 2002 osxAuoLonnETxAmE 1 wn o ua/L 1' 12' Dec 16, 2002 xsxnc*Lowopmopswc l wu u mo/L 2' 12' Dec 16, 2002 Iwuewn(1,2.3-co)p,nsws 1 wu u uo/L 1' 12' Dec 16, 2002 InonRIw 1 wo u uo/L 1' 12' Dec 16, 2002 IooPxnmnwE 1 wo u uo/L )' 12' Dec 16, 2002 zooSxpnnLs 1 wo u us/L l' 12' Dec 18, 2002 msroapYnILswe 1 wo o uo/L 4. 12' Dec 16, ZVUZ METHYL ws/*xwsmuLFowATs 1 wu o ua/L 1' 12' Dec 16, 2002 u-wI,mumo-oz-w Pmop,Lm*Iws 1 mn u mn/L 1' 12' Dec 16, 2002 w-w/7oonnnI-w-guTvLmMIws 1 wn u uo/L 2' 12' Dec 16, 2002 w-wI7u000mIEToYLAmIws 1 wo o us/L Z' 12' Dec 16, ZUVZ w-mzTn0000ImsTxyLAnIwE 1 wu o uu/L 2' 12' Dec 18, 2002 w'w/mumumIpxewrLxmIwe 1 mo u um/L 2' 12' Dec 16, 2002 w-wsrnmonwsroYLsrxYLmmIwE l mo u ma/L Z' 13' Dec 16, 2002 w'wITnomoMOnpooLIme 1 wn o us/L 2' 12. Dec 18, 2003 w'wzTnusoPIpsnzozws 1 wo o uo/L 2' 12' Dec 16' 2002 m'w/monopYxxoLzoIws 1 mo u us/L 2' 12' Dec 16, 2003 w*p*7*xLems l wn u uo/L 1' 12' Dec 16' 2002 wIrnoeewzcws 1 wo u os/L 1' 12' Dec 16, 2002 o'n o-m�s/*,�Pxonp*onoTo�uxrc � mo u uu/� Z ' 1z ' Dec 16' 2002 O'r�LumIws 1 wo u uu/L 1 12 Dec 18, 2002 p-nImsmYLAmIwoxZoBswrswE 1 wn u UGxL 2' 12. Dec 18' 2002 pswrAcxLonouswzsws 1 NO o �yL z' 12' Dec 16' 2002 pswTxcoLonowIrnomswzsws 1 NO o m/L Z' 12. Dec 18, ZUUZ psmTAooLonopxswoL 1 NO u uo/L 4' 31' Dec 16' 2002 poswxcsrzw 1 NO o us/L a' 12' Dec 16' 2002 pxswAwTmnsws 1 mu o uo/L 1' 12' Dec 16' 2002 pxcmoL 3' 1 uu/L 1' 12' Dec 18' 2002 pxowAmzuc 1 wo u uu/L 1' 12. Dec 18' 2002 pYoENs 1 NO o um/L 1' 12' Dec 16' 2002 prmIo/ws 1 NO o ua/L Z' 12' Dec 16' 2002 n*FnoLs l NO u us/L 2' 12' Dec 16' 2002 TsTRnsrxYmI7xIopYmmp*mapox7s 1 wo u us/L 1' 12' Dec 16' 2002 7x/omxZzw 1 wo o ua/L z' 12' Dec 16. ZnnZ Surrogates: 2,4 6'rmIeRuMoposuou 1 ao'O npm Dec 18, 2082 Z-FLuonooIpoEwrL 1 80'0 npn Dec 16, 2002 2-FLuonopxcwoL 1 55'0 npR Dec 16. 2002 wzrnooswZsws-ms 1 ar'o npx Dec 16, znuu posmoL-ob 1 37'0 mpn Dec 18, 2002 TsnpxswYL-o14 1 ao'o npn Dec 18, 2002 Comments: Field personnel did not enter the date/time of collection of sample mY-s-wmpZ on con 68795' Lab personnel obtained the date/time of collection from con 66826' Varno (3'ms7xvLposwoL and 4 msroyLrxswoL): These compounds cannot be renni,ed under the chromatographic conditions used for sample anelyoio' The result reported for 4-wemviphenot represents the combined total mboth uamc: Due to insufficient sampLe,the reporting Limits nzrnc (xnxmI7c and x,x-oIwsToYLposwsm,L^mzws): These standard at 50 ppm 8270c (w-w/rn000nIpxswvLmwIws): w-witmnod4, cnvLamine The result reported represents the combined total for the ocm voiatiie compounds were raiued' cpds- were calibrated for using a single point decomposes in the sc inlet forming diphenyiamhme' of both compounds. OEQ-CFVV_00025551 Corporate Environmental Database Lab Analysis Report Location: m,ETTEV)us January 9, 2003 Job Name: mwMuh GW+2002 poee 21 c of c m ieid: nn-a-wxpZ Sampling point: wmF2 Date Sampled: oEcEmasn 5, 2002 Lob Sample zn, 3958309-2 Analysis Lab: LxwcxS Sample Type: anouNu wwrsn QC Level: mc (xoom oo Process) Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 503OB/8260B msmrLswE cxLonInE 50 6700' us/L 100- 258. Dec 12, 2002 Comments: R*id personnel Lined out nxmpip nn's'wxF2 for 8015o anm(voio from Con 66826 without dating and intialinm the Lined -out item' 8260m (Msrx,LEws noumIoc); nun to the Level of methviene rh(oride, the reporting Limits for all mc/mn volatile compounds were raised. Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C Sampteid: FAY-G-NAF2-ACR Sampling Point: NAF2 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956310-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution Result PrepLMethod: 503OB/8260B ACROLEIN 1 NO U ACRYLONITRILE 1 NO U Surrogates: 1,2-DICHLOROETHANE-D4 1 93.0 RPR 4-BROMOFLUOROBENZENE 1 103.0 RPR DIBROMOFLUOROMETHANE 1 63.0 RPR TOLUENE-D8 1 102.0 RPR January 9, 2003 Page 22 Unit MDL PQL Date Analyzed UG/L 40. 100. Dec 10, 2002 UG/L 4. 20. Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Comments: Field personnel wrote over the date of collection on COC 66835 instead of lining out the mistake, dating and initialing the mistake and entering the correct information. 8260B (DIBROMOFLUOROMETHANE): Recovery values for surrogate were outside control limits in the initial and reanalysis, indicating a matrix effect. The pH of this sample is 11. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025553 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C Sampleid: FAY-G-NAF2P Sampling Point: NAF2P Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956313-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Lab: LANCAS January 9, 2003 Page 23 Analyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,2-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 12, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 12, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-BUTANONE 1 5. J UG/L 3. 10. Dec 12, 2002 2-CHLORO-I,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 12, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 12, 2002 ACETONE 1 24. UG/L 6. 20. Dec 12, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 12, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 12, 2002 BROMODICHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 BROMOFORM T ND U UG/L 1. 5. Dec 12, 2002 BROMOMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CARBON DISULFIDE 1 5. UG/L 1. 5. Dec 12, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 CHLOROBENZENE 1 NO U UG/L 0.8 5. Dec 12, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 12, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 12, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 ISOBUTYL ALCOHOL 1 NO U UG/L 100. 250. Dec 12, 2002 METHACRYLONITRILE 1 NO U UG/L 10. 50. Dec 12, 2002 METHYL IODIDE 1 NO U UG/L 1. 5. Dec 12, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 12, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 PROPIONITRILE 1 NO U UG/L 30. 100. Dec 12, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 12, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 12, 2002 TRANS-I,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 TRANS-I,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 TRANS-I,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 12, 2002 TRICHLOROETHENE 1 NO U UG/L 1. 5. Dec 12, 2002 TRICHLOROFLUOROMETHANE 1 NO U UG/L 2. 5. Dec 12, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 12, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 12, 2002 Surrogates: 1,2-DICHLOROETHANE-D4 1 101.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 99.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 99.0 RPR Dec 12, 2002 TOLUENE-D8 1 102.0 RPR Dec 12, 2002 Comments: Field personnel tined out the time of collection for FAY-G-NAF2P from CDC 66800 without dating and initialing the Lined -out item. DEQ-CFW 00025554 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF2P-ACR Sampling Point: NAF2P Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956314-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) AnaLyte/Parameter Dilution Result Prep/Method: 503OB18260B ACROLEIN 2 ND U ACRYLONITRILE 2 ND U Surrogates: 1,2-DICHLOROETHANE-D4 1 94.0 RPR 4-BROMOFLUOROBENZENE 1 104.0 RPR DIBROMOFLUOROMETHANE 1 82.0 RPR TOLUENE-D8 1 104.0 RPR Unit MDL POL Date Analyzed UG/L 80. 200. Dec 10, 2002 UG/L 8. 40. Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Comments: 8260B: The reporting Limits were raised for the GC/MS volatile compounds due to sample foaming. 8260B (DIBROMOFLUOROMETHANE): Recovery values for surrogate were outside control Limits in the initial and reanalysis, indicating a matrix effect. The pH of this sample is 11. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025555 Corporate Environmental. Database Lab Analysis Report Location: FAYETTexuLe January 9, 2003 Job Name: swMu6 mw'2002 Page 27 c of c o ieid: FAY-u-wxp3 Sampling Point: m*F3 Date Sampled: occennEn 5, 2002 Lab Sample ID: 3956315-1 xnmiynio Lab: LAwoxu Sample 7ype: sxouwo uxrEn uu cpvpi: uc (Aoom mc prmcoms) Dilution Result Unit MDL POL Date AnaLyzed Method: 300.0 FLuonIos 5 12.5 mu/L 0.40 0'50 Dec 17^ 2002 Method; 8015B meJoxwoL (o, ozmec/ IwJecrIum) 1 wm u UG/L 200. 1000' Dec 13, 2002 Surrogates: xzETows 1 100'0 npn Dec 13' 2002 1,1,1,2'/ErwncwLneoeroxNc 1 wo u us/L 1' 5' Dec 12, 2002 1,1,1-To/coLoxusrHAws 1 NO u um/L 0-8 5. Dec 12, 2002 1,1,3'2-TsTn*o*LonosT**ws 1 NO u ua/L 1' 5' Dec 12, 2002 1,1,2'roIcoLcmosTx*ms 1 NO u un/L 0.8 5. Dec 12, 2082 1.1-ozuxLcmosTxxws 1 NO u uo/L 1' 5' Dec 12, 2002 1,1-oIcxLonoeT*sws 1 NO u uu/L 0'8 5' Dec 12, 2002 1,2,3-rmzcxLonoPwopAwc 1 NO u ua/c 1- 5' Dec 12^ 2002 1^2-nIenomo-3-coLonoPRop*ws 1 wo u ms/L 2' 5' Dec 12, 2002 1,2'ozmRmmosTmmwe 1 NO u uo/L 1' 5' Dec 12, 2002 1,2-nIcoLonoesmZsws 7 mo o ms/L 1' 5' Dec 12, 2002 1,2-uzcxLoonsroxwc 1 wu u ws/L 1' 5' Dec 13, 2002 1 2-nICoLowoPRoPxwc 1 wn u os/L 1 ' � ' Dec 12' 2002 1�3'm/co�ononem�sws 1 wn u us/L 1 5 Dec 122002 1,4-oIcuummmswzswE 1 NO u uo/L 1. 5' Dec 12, 2002 2-murxwowE 1 NO u uo/L 3' 10' Dec 12, 2002 2'xmLoxo-1'3-euTxoIsws 1 NO u UG/L 1- 5' Dec 12, 2002 2-xsxAwows 1 wo u uu/L 3' 10' Dec 12, 2002 4ivsTxYL-2-pewTxwnws 1 wu o oo/L o- m' Dec 12, 2002 xcsrows 1 NO u un/L a' Zn. Dec 12, 2002 mcsrowzTnzLE 1 wo u us/L 25. 100' Dec 12, 002 *uvL cxLmmzms 1 wo u u:/c 1' 5. Dec 72, 2002 uEwZsws 1 NO u us/L 0.5 5' Dec 12. 2002 onomonIcoLmmnmsrmwc 1 wn u uo/L 1' 5. Dec 12, 2002 anomoFonm 1 wm u uo/L 1' 5' Dec 12, aooZ onommwerxmws 1 wo u um/L 1. 5' Dec 12, 2002 cxnuow uIouLrIos 1 NO u uo/L 1' 5' Dec 12, 2002 c^wonw rsrmxuoLoxIns 1 NO u uo/L 1' 5' Dec 12, 2002 cxLoonmswZEws 1 NO u us/L n'V 5' Dec 12, 2002 coLonos7xaws 1 NO u um/L 1' s' Dec 12, 2002 CoLuxoponm 1 NO u us/L 0.8 5' Dec 12, 2002 o*LuoonsTxows 1 NO o os/L 1' 5. Dec 12, 2002 c/o'1,2'n/uoLoxosToews 1 wo u uo/L O'D 5' Dec 12, uooZ CIS-1 u-ozcxLonopnopews 1 mu u ua/L 1 ' � Dec 12' 2002 nIax��co�000msrx�ms 1 wn u uo/� � �' Dec 12' 2002 »/enomomsToxws 1 wu u os/L 1. 5' Dec 12' 3002 oIc*LonooIpLuonomsTxAws 1 NO u us/L Z- 5' Dec 12' 2002 ETHYL msTxxcx,Lxrs 1 NO u mo/L 1' 5' Dec 12' 2002 cmYmswzsmE 1 wo u ms/L n-D 5' Dec 12' 2002 zuoou7rL aLc000L 1 wo u ms/L 100' 250' Dec 12' 2002 msTxAuxYLowIrwzLe 1 NO u ms/L 10' 50' Dec 12" 2002 msT*,L Iouzos 1 NO u uo/L 1' n' Dec 12" 2002 Mc7xrL meToxcxYLars 1 NO u ma/L 1' 5. Dec 12' 2002 msTorLEwe CoLonIos 1 4' 1 us/L z' o' Dec 12' 2002 pswTxcoLomosroxws 1 NO u ms/L 1' 5. Dec 12^ 2002 pmopIowI7nILE 1 NO u um/L 30' 180' Dec 12' 2002 sr,xswe 1 NO u ua/L 1' 5' Dec 12' 2002 Ts/xxcoLoxosrosws 1 NO u uo/L 0-8 5' Dec 122002 TOLUENE 1 NO u uo/L 0'7 s' Dec 12, 2002 Tnxmo'1,2'oIcxLomosTxsws 1 mo u us/L U-a s' Dec 12, 2002 rnAmm-1.3-ozcoccmopnnPsws 1 wo u uo/L 1' s' Dec 12, 2002 rnxwo'1 4-oIuoLomo-2-eursms 1 wm u mu/L 15 ' 5o ' Dec 12' 2002 mzcxLo�osrxsws � wo u uu/� �' n' Dec 12' zooa mIuxLuKopLuumomsrxxws 1 NO u ua/L Z' x' Dec 123002 VINYL xcs/*re 1 NO o ua/L 2' 10' Dec 12, 2002 VINYL mLonIos 1 NO u uu/L 1' 5' Dec 12, 2002 x,Lsws (TOTAL) 1 NO u uo/L 0.8 5. Dec 12' 2002 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 28 C of C Sampleid: FAY-G-NAF3 Sampling Point: NAF3 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956315-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution RPR Date Analyzed ----------------- -------- --- ------------- Surrogates: 1,2-DICHLOROETHANE-D4 1 103.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 99.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 100.0 RPR Dec 12, 2002 TOLUENE-D8 1 104.0 RPR Dec 12, 2002 Prep/Method: 351OCZ8270C 1,2,4,5-TETRACHLOROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 1,2,4-TRICHLOROBENZENE 1 ND U UG/L 1. 10. Dec 17, 2002 1,3,5-TRINITROBENZENE 1 ND U UG/L 5. 20. Dec 17, 2002 1,3-DINITROBENZENE 1 ND U UG/L 2. 10. Dec 17, 2002 1,4-DIOXANE 1 1. J UG/L 1. 5. Dec 17, 2002 1,4-NAPHTHOQUINONE 1 ND U UG/L 10. 100. Dec 17, 2002 1,4-PHENYLENEDIAMINE 1 ND U UG/L 62. 200. Dec 17, 2002 1-NAPHTHYLAMINE 1 ND U UG/L 5. 26. Dec 17, 2002 2,3,4,6-TETRACHLOROPHENOL 1 ND U UG/L 2. 10. Dec 17, 2002 2,4,5-TRICHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4,6-TRICHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4-DICHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4-DIMETHYLPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2,4-DINITROPHENOL 1 ND U UG/L 20. 62. Dec 17, 2002 2,4-DINITROTOLUENE 1 ND U UG/L 1. 10. Dec 17, 2002 2,6-DICHLOROPHENOL 1 NO U UG/L 2. 10. Dec 17, 2002 2,6-DINITROTOLUENE 1 ND U UG/L 1. 10. Dec 17, 2002 2-ACETYLAMINOFLUORENE 1 ND U UG/L 2. 10. Dec 17, 2002 2-CHLORONAPHTHALENE 1 ND U UG/L 1. 10. Dec 17, 2002 2-CHLOROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2-METHYLNAPHTHALENE 1 ND U UG/L 1. 10. Dec 17, 2002 2-METHYLPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2-NAPHTHYLAMINE 1 ND U UG/L 5. 26. Dec 17, 2002 2-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 2-NITROPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 2-PICOLINE 1 ND U UG/L 2. 10. Dec 17, 2002 3,31-DICHLOROBENZIDINE 1 ND U UG/L 1. 10. Dec 17, 2002 3,31-DIMETHYLBENZIDINE 1 ND U UG/L 5. 26. Dec 17, 2002 3-METHYLCHOLANTHRENE 1 ND U UG/L 2. 10. Dec 17, 2002 3-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 4,6-DINITRO-2-METHYLPHENOL 1 ND U UG/L 5. 26. Dec 17, 2002 4-AMINOBIPHENYL 1 ND U UG/L 2. 10. Dec 17, 2002 4-BROMOPHENYL-PHENYLETHER 1 ND U UG/L 1. 10. Dec 17, 2002 4-CHLORO-3-METHYLPHENOL 1 ND U UG/L 1. 10. Dec 17, 2002 4-CHLOROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 4-CHLOROPHENYL-PHENYLETHER 1 ND U UG/L 1. 10. Dec 17, 2002 4-METHYLPHENOL 1 ND U UG/L 2. 10. Dec 17, 2002 4-NITROANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 4-NITROPHENOL 1 NO U UG/L 10. 51. Dec 17, 2002 4-NITROQUINOLINE-I-OXIDE 1 ND U UG/L 20. 100. Dec 17, 2002 5-NITRO-0-TOLUIDINE 1 ND U UG/L 3. 10. Dec 17, 2002 7,12-DIMETHYLBENZCA)ANTHRACENE 1 NO U UG/L 2. 10. Dec 17, 2002 A,A-DIMETHYLPHENETHYLAMINE 1 NO U UG/L 1. 51. Dec 17, 2002 ACENAPHTHENE 1 ND U UG/L 1. 10. Dec 17, 2002 ACENAPHTHYLENE 1 NO U UG/L 1. 10. Dec 17, 2002 ACETOPHENONE 1 NO U UG/L 2. 10. Dec 17, 2002 ANILINE 1 ND U UG/L 1. 10. Dec 17, 2002 ANTHRACENE 1 ND U UG/L 1. 10. Dec 17, 2002 ARAMITE 1 ND U UG/L 1. 51. Dec 17, 2002 BENZO(A)ANTHRACENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(A)PYRENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(B)FLUORANTHENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(G,H,I)PERYLENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZO(K)FLUORANTHENE 1 ND U UG/L 1. 10. Dec 17, 2002 BENZYL ALCOHOL 1 ND U UG/L 5. 20. Dec 17, 2002 BIS(2-CHLOROETHOXY)METHANE 1 ND U UG/L 1. 10. Dec 17, 2002 BIS(2-CHLOROETHYL)ETHER 1 ND U UG/L 1. 10. Dec 17, 2002 BIS(2-CHLOROISOPROPYL)ETHER 1 ND U UG/L 1. 10. Dec 17, 2002 BIS(2-ETHYLHEXYL)PHTHALATE 1 ND U UG/L 2. 10. Dec 17, 2002 BUTYLBENZYLPHTHALATE 1 NO U UG/L 2. 10. Dec 17, 2002 CHLOROBENZILATE 1 ND U UG/L 3. 20. Dec 17, 2002 DEQ-CFW 00025557 Corporate Environmental, Database Lab Analysis Report Location: Fx,sTTemus Job Name: mWMU6 GW-2002 c of c i id: FAY-s-wAp3 nompl\ma Point: wxr3 Date Sampled: necewocn 5, 2002 Lab Sample ID: 3056315-1 xna[vuiu Type:Sample GROUND WATER QC Level: QC (ADGM QC Process) Lab: LANCAS January 9"2003 Page 29 AnaLyte/Parameter Dilution Result Unit � �� �� Cxx,uuwE � wo u us/L i ' i0' Dec 17, 2002 oI-w-BurrLpoTuxL*Ts 1 wn y um/L 2' 10' Dec 17' 2002 DI-w ocrYLporxxLArs 1 mo o ms/L 2' 10' Dec 17' 2002 oIALLoTE Tnowm/cIo 1 wo o ma/L 1' 10' Dec 17' 2008 oImcwa(*,x)uw7xmxcsws 1 NO u us/c 1' 10' Dec 17' 2002 nImswzoruxxw 1 wu u uo/L 1' 10' Dec 17' 2002 o/sT*YLporxxLxTs 1 NO u uu/L Z' 10' Dec 17' 2002 ozwsrooxTs 1 NO o mm/L 3' 20' Dec 17' 2002 uzms7xreoT*xLxTE 1 wu o um/L 2' 10' Dec 17' 2002 ETHYL mc7xxwcSuLpowArc 1 wu u us/L Z. 10' Dec 17' 2002 rLmuw*wTxsws 1 NO u ua/L 1' 10' Dec 17' 2002 FLuoxsws 1 mn u um/L 1' 10' Dec 17" 2002 xsxxcxLnnoncwzEwe 1 wm u uo/L 1. 10' Dec 17' 2002 xExxc*LenoouTxoIsws 1 wn u us/L 1. 10' Dec 17, 2002 xexxcxLmmocrcLoPEwTaozsws 1 wn o us/L 5' 26. Dec 17' 2802 xsxAcoLownsTxxwE 1 wo u uo/L 1. 10' Dec 17' 2002 xsaxcoLonopnnpsmE 1 wu u us/L 2. 18' Dec 17' 2002 IwnEwo(1,2,3'cu)pYnEwe 1 NO u ua/L 1. 10. Dec 17' 2002 /000nzw 1 wm u mo/L 1' 10' Dec 17' 2002 zsopxoanms 1 wm u mm/L Y' 10' Dec 17" 2002 InooxrnoLc 1 ou u us/L 1. 10' Dec 17' 2002 METoApYnzLsws 1 mo u ua/L 3' 10' Dec 17" 2002 METHYL wsTxxwsouLpow*rs 1 wo o uG/L 1' 10' Dec 17' 2002 w-wIrnnSn'nI'w-pnopYLxmIws 1 wu u uG/L 1' 10' Dec 17" 2002 w-wIroomooI'w-aur,LwmIwe 1 NO u ms/L 2' 10' Dec 17' 2002 w'wITmusonIsTxYLxmIws 1 wo u ms/L Z' 10- Dec 17" 2002 m'mI7monooIme7oYLxmIws 1 NO u uo/L 2. 10. Dec 17" 2002 w-wIronmooIpVswYLxwIws 1 NO u mo/L Z' 10- Dec 17, 2002 w-wIrxonowsmYLcmYLAwIws 1 NO u ua/L z' 10' Dec 17' 2002 w'wI7mosomnxpxoL/ws 1 NO u uo/L Z' 10' Dec 17^ ZVVZ w-wIrmnnoPzpsnIoIus 1 NO u uo/L 2' 10' Dec 17' 2003 w-wIrxouoPrnmoLIoIwc 1 NO u um/L Z' 10, Dec 17' 2002 wxpxTxALsws 1 NO u uo/L 1' 10- Dec 17^ 2002 wI7noasw7sms 1 NO o us/L 1' 10' Dec 17' ZVVZ u,o o-m/eToYLpxoSpeoxurozu^rs 1 NO u us/L 2 10 ' Dec 17" 2002 o-T�LuxoIws 1 NO u ms/L 1' 10 Dec 17' 2002 p'oImeTo,mmrwo*zooswzsws 1 NO u oo/L u' 10' Dec 17, 2002 pcwTAcxLomoopwZsws 1 NO u wo/L 2' 10' Dec 17' 2002 PsmTxcxLonow/Tnooswzsws 1 wo u us/L Z' 10' Dec 17^ 2002 pswrxcxLumopxswnL 1 NO u us/L ]' 26' Dec 17" 2002 Pxeu*csTzw 1 wn u oa/L z' 10' Dec 17' zoUZ pxcmxwmnsws 1 NO u uG/L 1' 10' Dec 17' 2002 poswoL 1 wu u uo/L 1' 10- Dec 17^ 2002 pnnwwm/os 1 NO u ua/L 1' 10' Dec 17' zuoz PYncws 1 wo u uo/L 1' 10' Dec 17' 2002 PYRIDINE I NO u uo/L z' Yu- Dec 17' 2002 mmFooLs 1 wo u oo/L 2. 10' Dec 17' 2002 rs7uxsTo,co/TxzoPYxupouupo*Ts 1 wo u uo/L 1' 10' Dec 172002 ToIuwwZIw wu u us/L 2' 10' Dec 17' 3002 Surrogates: 2,4 0-rxIBxomoposwnL 1 81.0 wpw Dec 17' 2002 2'r�unnooIpxsmrL 1 73'0 xpn Dec 17' ZVVZ a-FLumnoposwoL 1 51'0 npo Dec 17' zOoz wITmooswzsws-u5 1 81.0 xpx Dec 17' 2002 pxswnL-o6 1 34.0 npo Dec 17' 2002 rsnPosmYL'o14 1 77'0 npn Dec 172002 Field personnel wrote over the dates on coc 06798 instead of lining out the date, dating and initialing the mistake and entering the correct information. neruc (9'Msro,LposwnL and 4woovLposmoL), These compounds cannot be resolved under the chromatographic conditions used for sample analysis. The result reported for 4-methvlpmeno| represents the combined total of both compounds. �q�u u' 8270c: Due to irmvff,r`ont sample, the reporting Limits for the oemi"niatiie compounds were raised. 8270u (xnxmITE and x,x oIn*Tx,LPo�ws/oYLmwIws): These cpdv' were calibrated for using o single point standard at m ppm' 8270c (w'wImonom\poswYLxwzwc): w wit,000d4, enyLamine decomposes in the ac inlet forming uipmenviamine' The result reported represents the combined total of uum compounds. Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF3-ACR Sampling Point: NAF3 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956316-1 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) Anatyte,(Parameter Dilution Result Prep/Method: 503OB/8260B ACROLEIN I NO U ACRYLONITRILE 1 NO U Surrogates: 1,2-DICHLOROETHANE-D4 1 95.0 RPR 4-BROMOFLUOROBENZENE 1 103.0 RPR DIBROMOFLUOROMETHANE 1 90.0 RPR TOLUENE-D8 1 106.0 RPR Unit MDL POL Date Analyzed UG/L 40. 100. Dec 10, 2002 UG/L 4. 20. Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Dec 10, 2002 Comments: Field personnel wrote over the date/time of collection on CDC 66811 without dating and initiating next to the tined -out item. Qualifiers: U The constituent should be considered not detected. DEQ-CFW-00025559 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF4 Sampling Point: NAF4 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3955485-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADOM QC Process) 7.1 AnaLyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Method: 300.0 FLUORIDE 5 3.21 MG/L 0.40 0.50 Dec 18, 2002 Method• 8015B METHANOL (BY DIRECT INJECTION) 1 NO U UG/L 200. 1000. Dec 13, 2002 Surrogates: ACETONE 1 118.0 RPR Dec 13, 2002 Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,1-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,1,2-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,1-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,1-DICHLOROETHENE I ND U UG/L 0.8 5. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 NO U UG/L 2. 5. Dec 12, 2002 1,2-DIBROMOETHANE I ND U UGIL 1. 5. Dec 12, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,3-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 12, 2002 1,4-DICHLOROBENZENE 1 NO U UG/L 1. 5. Dec 12, 2002 2-BUTANONE 1 NO U UG/L 3. 10. Dec 12, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 12, 2002 4-METHYL-2-PENTANONE 1 NO U UG/L 3. 10. Dec 12, 2002 ACETONE 1 13. J UG/L 6. 20. Dec 12, 2002 ACETONITRILE 1 NO U UG/L 25. 100. Dec 12, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 BENZENE 1 NO U UG/L 0.5 5. Dec 12, 2002 BROMODICHLOROMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 BROMOFORM 1 NO U UG/L 1. 5. Dec 12, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 CARBON DISULFIDE 1 2. 1 UG/L 1. 5. Dec 12, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 12, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 CHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 CHLOROFORM 1 NO U UG/L 0.8 5. Dec 12, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOCHLOROMETHANE I NO U UG/L 1. 5. Dec 12, 2002 DIBROMOMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 ETHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 12, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 12, 2002 METHACRYLONITRILE 1 NO U UG/L 10. 50. Dec 12, 2002 METHYL IODIDE 1 ND U UG/L 1. 5. Dec 12, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 12, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 PROPIONITRILE I ND U UG/L 30. 100. Dec 12, 2002 STYRENE 1 NO U UG/L 1. 5. Dec 12, 2002 TETRACHLOROETHENE I NO U UG/L 0.8 5. Dec 12, 2002 TOLUENE 1 NO U UG/L 0.7 5. Dec 12, 2002 TRANS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 TRANS-1,3-DICHLOROPROPENE I ND U UG/L 1. 5. Dec 12, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 NO U UG/L 15. 50. Dec 12, 2002 TRICHLOROETHENE 1 2. 1 UG/L 1. 5. Dec 12, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 12, 2002 VINYL CHLORIDE 1 NO U UG/L 1. 5. Dec 12, 2002 XYLENE (TOTAL) 1 NO U UG/L 0.8 5. Dec 12, 2002 DEQ-CFW-00025560 Corporate Environmental Database Lab Analysis Report Location: Job Name: C of C Sampleid Sampling Point: Date Sampled: Lab Sample ID: Sample Type: QC Level: Analyte/Parameter ----------------- Surrogates: FAYETTEVILLE SWMU6 GW-2002 FAY-G-NAF4 NAF4 DECEMBER 5, 2002 3955485-1 Analysis GROUND WATER QC (ADQM QC Process) Lab: LANCAS Dilution RPR January 9, 2003 Page 34 1,2-DICHLOROETHANE-D4 1 102.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 98.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 100.0 RPR Dec 12, 2002 TOLUENE-D8 1 101.0 RPR Dec 12, 2002 PreWMethod: 3510C/8270C 1,2,4,5-TETRACHLOROBENZENE 1 ND U UG/L 2. 11. Dec 16, 2002 1,2,4-TRICHLOROBENZENE 1 ND U UG/L 1. 11. Dec 16, 2002 1,3,5-TRINITROBENZENE 1 ND U UG/L 5. 21. Dec 16, 2002 1,3-DINITROBENZENE 1 ND U UG/L 2. 11. Dec 16, 2002 1,4-DIOXANE 1 ND U UG/L 1. 5. Dec 16, 2002 1,4-NAPHTHOQUINONE 1 ND U UG/L 11. 110. Dec 16, 2002 1,4-PHENYLENEDIAMINE 1 ND U UG/L 64. 210. Dec 16, 2002 1-NAPHTHYLAMINE 1 ND U UG/L 5. 26. Dec 16, 2002 2,3,4,6-TETRACHLOROPHENOL 1 NO U UG/L 2. 11. Dec 16, 2002 2,4,5-TRICHLOROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2,4,6-TRICHLOROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2,4-DICHLOROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2,4-DIMETHYLPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2,4-DINITROPHENOL 1 ND U UG/L 21. 64. Dec 16, 2002 2,4-DINITROTOLUENE 1 ND U UG/L 1. 11. Dec 16, 2002 2,6-DICHLOROPHENOL 1 NO U UG/L 2. 11. Dec 16, 2002 2,6-DINITROTOLUENE 1 NO U UG/L 1. 11. Dec 16, 2002 2-ACETYLAMINOFLUORENE 1 NO U UG/L 2. 11. Dec 16, 2002 2-CHLORONAPHTHALENE 1 ND U UG/L 1. 11. Dec 16, 2002 2-CHLOROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2-METHYLNAPHTHALENE 1 ND U UG/L 1. 11. Dec 16, 2002 2-METHYLPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2-NAPHTHYLAMINE 1 ND U UG/L 5. 26. Dec 16, 2002 2-NITROANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 2-NITROPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 2-PICOLINE 1 NO U UG/L 2. 11. Dec 16, 2002 3,31-DICHLOROBENZIDINE 1 NO U UG/L 1. 11. Dec 16, 2002 3,31-DIMETHYLBENZIDINE 1 ND U UG/L 5. 26. Dec 16, 2002 3-METHYLCHOLANTHRENE 1 ND U UG/L 2. 11. Dec 16, 2002 3-NITROANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 4,6-DINITRO-2-METHYLPHENOL 1 ND U UG/L 5. 26. Dec 16, 2002 4-AMINOBIPHENYL 1 ND U UG/L 2. 11. Dec 16, 2002 4-BROMOPHENYL-PHENYLETHER 1 ND U UG/L 1. 11. Dec 16, 2002 4-CHLORO-3-METHYLPHENOL 1 ND U UG/L 1. 11. Dec 16, 2002 4-CHLOROANILINE 1 NO U UG/L 1. 11. Dec 16, 2002 4-CHLOROPHENYL-PHENYLETHER 1 ND U UG/L 1. 11. Dec 16, 2002 4-METHYLPHENOL T ND U UG/L 2. 11. Dec 16, 2002 4-NITROANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 4-NITROPHENOL 1 ND U UG/L 11. 53. Dec 16, 2002 4-NITROQUINDLINE-I-OXIDE 1 ND U UG/L 21. 110. Dec 16, 2002 5-NITRO-0-TOLUIDINE 1 ND U UG/L 3. 11. Dec 16, 2002 7,12-DIMETHYLBENZCAIANTHRACENE 1 NO U UG/L 2. 11. Dec 16, 2002 A,A-DIMETHYLPHENETHYLAMINE 1 NO U UG/L 1. 53. Dec 16, 2002 ACENAPHTHENE 1 ND U UG/L 1. 11. Dec 16, 2002 ACENAPHTHYLENE 1 NO U UG/L 1. 11. Dec 16, 2002 ACETOPHENONE 1 ND U UG/L 2. 11. Dec 16, 2002 ANILINE 1 ND U UG/L 1. 11. Dec 16, 2002 ANTHRACENE 1 ND U UG/L 1. 11. Dec 16, 2002 ARAMITE 1 ND U UG/L 1. 53. Dec 16, 2002 BENZO(A)ANTHRACENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZO(A)PYRENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZO(B)FLUORANTHENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZO(G,H,I)PERYLENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZO(K)FLUORANTHENE 1 ND U UG/L 1. 11. Dec 16, 2002 BENZYL ALCOHOL 1 ND U UG/L 5. 21. Dec 16, 2002 BIS(2-CHLOROETHOXY)METHANE 1 NO U UG/L 1. 11. Dec 16, 2002 BIS(2-CHLOROETHYL)ETHER 1 NO U UG/L 1. 11. Dec 16, 2002 BIS(2-CHLOROISOPROPYL)ETHER 1 ND U UG/L 1. 11. Dec 16, 2002 BIS(2-ETHYLHEXYL)PHTHALATE 1 3. J UG/L 2. 11. Dec 16, 2002 BUTYLBENZYLPHTHALATE 1 ND U UG/L 2. 11. Dec 16, 2002 CHLOROSENZILATE 1 ND U UG/L 3. 21. Dec 16, 2002 DEQ-CFW 00025561 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C Sampteid: FAY-G-NAF4 Sampling Point: NAF4 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3955485-1 Analysis Sample Type- GROUND WATER QC Level: QC (ADQM QC Process) AnaLytelParameter Dilution Result Unit MDL PQL Date Analyzed CHRYSENE 1 NO U UG—/L TT 11. Dec 16, 2002 DI-N-BUTYLPHTHALATE 1 NO U UG/L 2. 11. Dec 16, 2002 DI-N-OCTYLPHTHALATE 1 NO U UG/L 2. 11. Dec 16, 2002 DIALLATE TRANS/CIS 1 NO U UG/L 1. 11. Dec 16, 2002 DIBENZ(A,H)ANTHRACENE I NO U UG/L 1. 11. Dec 16, 2002 DIBENZOFURAN 1 NO U UG/L 1. 11. Dec 16, 2002 DIETHYLPHTHALATE 1 NO U UG/L 2. 11. Dec 16, 2002 DIMETHOATE 1 NO U UG/L 3. 21. Dec 16, 2002 DIMETHYLPHTHALATE 1 NO U UG/L 2. 11. Dec 16, 2002 ETHYL METHANESULFONATE 1 ND U UG/L 2. 11. Dec 16, 2002 FLUORANTHENE 1 NO U UG/L 1. 11. Dec 16, 2002 FLUORENE 1 NO U UG/L 1. 11. Dec 16, 2002 HEXACHLOROBENZENE 1 ND U UG/L 1. 11. Dec 16, 2002 HEXACHLOROBUTADIENE 1 NO U UG/L 1. 11. Dec 16, 2002 HEXACHLOROCYCLOPENTADIENE 1 NO U UG/L 5. 26. Dec 16, 2002 HEXACHLOROETHANE 1 NO U UG/L 1. 11. Dec 16, 2002 HEXACHLOROPROPENE 1 NO U UG/L 2. 11. Dec 16, 2002 INDENO(1,2,3-CD)PYRENE 1 NO U UG/L 1. 11. Dec 16, 2002 ISODRIN 1 NO U UG/L 1. 11. Dec 16, 2002 ISOPHORONE 1 NO U UG/L 1. 11. Dec 16, 2002 ISOSAFROLE 1 NO U UG/L 1. 11. Dec 16, 2002 METHAPYRILENE 1 NO U UG/L 3. 11. Dec 16, 2002 METHYL METHANESULFONATE 1 NO U UG/L 1. 11. Dec 16, 2002 N-NiTROSO-DI-N-PROPYLAMINE 1 NO U UG/L 1. 11. Dec 16, 2002 N-NITROSODI-N-BUTYLAMINE 1 NO U UG/L 2. 11. Dec 16, 2002 N-NITROSODIETHYLAMINE 1 NO U UG/L 2. 11. Dec 16, 2002 N-NITROSODIMETHYLAMINE 1 NO U UG/L 2. 11. Dec 16, 2002 N-NITROSODIPHENYLAMINE 1 NO U UG/L 2. 11. Dec 16, 2002 N-NITROSOMETHYLETHYLAMINE 1 NO U UG/L 2. 11. Dec 16, 2002 N-NITROSOMORPHOLINE 1 NO U UG/L 2. 11. Dec 16, 2002 N-NITROSOPIPERIDINE 1 NO U UG/L 2. 11. Dec 16, 2002 N-NITROSOPYRROLIDINE I NO U UG/L 2. 11. Dec 16, 2002 NAPHTHALENE I NO U UG/L 1. 11. Dec 16, 2002 NITROBENZENE I NO U UG/L 1. 11. Dec 16, 2002 0,0,0-TRIETHYLPHOSPHOROTHIOATE I NO U UG/L 2. 11. Dec 16, 2002 O-TOLUIDINE 1 NO U UG/L 1. 11. Dec 16, 2002 P-DIMETHYLAMINOAZOBENZENE 1 NO U UG/L 2. 11. Dec 16, 2002 PENTACHLOROBENZENE 1 NO U UG/L 2. 11. Dec 16, 2002 PENTACHLORONITROBENZENE 1 NO U UG/L 2. 11. Dec 16, 2002 PENTACHLOROPHENOL 1 NO U UG/L 3. 26. Dec 16, 2002 PHENACETIN 1 NO U UG/L 2. 11. Dec 16, 2002 PHENANTHRENE 1 NO U UG/L 1. 11. Dec 16, 2002 PHENOL 1 NO U UG/L 1. 11. Dec 16, 2002 PRONAMIDE 1 NO U UG/L 1. 11. Dec 16, 2002 PYRENE 1 NO U UG/L 1. 11. Dec 16, 2002 PYRIDINE 1 NO U UG/L 2. 11. Dec 16, 2002 SAFROLE 1 NO U UG/L 2. 11. Dec 16, 2002 TETRAETHYLDITHIOPYROPHOSPHATE 1 NO U UG/L 1. 11. Dec 16, 2002 THIONAZIN 1 NO U UG/L 2. 11. Dec 16, 2002 Surrogates: 2,4,6-TRIBROMOPHENOL 1 101.0 RPR Dec 16, 2002 2-FLUOROBIPHENYL, 1 99.0 RPR Dec 16, 2002 2-FLUOROPHENOL 1 59.0 RPR Dec 16, 2002 NITROBENZENE-D5 1 95.0 RPR Dec 16, 2002 PHENOL-D6 1 38.0 RPR Dec 16, 2002 TERPHENYL-D14 1 72.0 RPR Dec 16, 2002 Comments: Field personnel did not enter the date/time the bottles were received on COCs 66791-93, 66802, 66805 and 66829. 8270C (3-METHYLPHENOL and 4-METHYLPHENOL): These compounds cannot be resolved under the chromatographic conditions used for sample analysis. The result reported for 4-MethyLphenoL represents the combined total of both compounds. 8270C: Due to insufficient sample, the reporting Limits for the semivotatiLe compounds were raised. 8270C (ARAMITE and A,A-DIMETHYLPHENETHYLAMINE): These cpds. were calibrated for using a single point standard at 50 ppm. 8270C (N-NITROSODIPHENYLAMINE): N-NitrosodiphenyLamine decomposes in the GC inlet forming diphenyLamine. The result reported represents the combined total of both compounds. DEQ-CFW-00025562 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF4 Sampling Point: NAF4 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3955485-2 Analysis Lab: LANCAS Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution Result Method: 300.0 CHLORIDE 20 90.6 Prep/Method: 5030B/8260B METHYLENE CHLORIDE 100 5000. January 9, 2003 Page 37 Unit MDL PQL Date Analyzed MG/L 6.0 8.0 Dec 24, 2002 UG/L 200. 500. Dec 13, 2002 Comments: Lab personnel received all vials for samples FAY-G-NAF4-ACR and FAY-G-NAF4P-ACR broken, therefore acrolein and acryLonitriLe were not reported for these samples. DEQ-CFW-00025563 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 C of C SampLeid: FAY-G-NAF4P Sampling Point: NAF4P Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3955486-1 Analysis Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) WT-TIRTITOM AnaLyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 50308/82608 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,1-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,2-TRICHLOROETHANE I ND U UG/L 0.8 5. Dec 12, 2002 1,1-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,1-DICHLORDETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 NO U UG/L 2. 5. Dec 12, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,3-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 12, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-HEXANONE 1 NO U UG/L 3. 10. Dec 12, 2002 4-METHYL-2-PENTANONE 1 NO U UG/L 3. 10. Dec 12, 2002 ACETONE 1 8. j UG/L 6. 20. Dec 12, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 12, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 BENZENE 1 NO U UG/L 0.5 5. Dec 12, 2002 BROMODICHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 12, 2002 BROMOMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 12, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 12, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 12, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 ISOBUTYL ALCOHOL I ND U UG/L 100. 250. Dec 12, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 12, 2002 METHYL IODIDE 1 ND U UG/L 1. 5. Dec 12, 2002 METHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 12, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 12, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 12, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 12, 2002 TRANS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 TRANS-1,3-DICHLOROPROPENE 1 NO U UG/L 1. 5. Dec 12, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 NO U UG/L 15. 50. Dec 12, 2002 TRICHLOROETHENE 1 ND U UG/L 1. 5. Dec 12, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 VINYL ACETATE 1 NO U UG/L 2. 10. Dec 12, 2002 VINYL CHLORIDE 1 ND U UGIL 1. 5. Dec 12, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 12, 2002 Surrogates: 1,2-DICHLOROETHANE-D4 1 104.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 97.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 101.0 RPR Dec 12, 2002 TOLUENE-D8 1 103.0 RPR Dec 12, 2002 Qualifiers: U The constituent should be considered not detected. J The result is between MDL and PQL and should be considered an estimate. DEQ-CFW-00025564 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 40 C of C Sampleid: FAY-K-TBLK-NAFGW-DAY1 Sampling Point: TBLK-NAFGW-DAY1 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3955488-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) Analyte/Parameter Dilution Result Unit MDL PQL Date Analyzed Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,1-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,2-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,1-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 ND U UG/L 2. 5. Dec 12, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,3-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 12, 2002 2-CHLORO-I,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-HEXANONE 1 ND U UG/L 3. 10. Dec 12, 2002 4-METHYL-2-PENTANONE 1 ND U UG/L 3. 10. Dec 12, 2002 ACETONE 1 ND U UG/L 6. 20. Dec 12, 2002 ACETONITRILE 1 ND U UG/L 25. 100. Dec 12, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 12, 2002 BROMODICHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 12, 2002 BROMOMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CARBON DISULFIDE 1 ND U UG/L 1. 5. Dec 12, 2002 CARBON TETRACHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 CHLOROBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 CHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CHLOROFORM 1 ND U UG/L 0.8 5. Dec 12, 2002 CHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DICHLORODIFLUOROMETHANE 7 ND U UG/L 2. 5. Dec 12, 2002 ETHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 12, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 ISOBUTYL ALCOHOL 1 ND U UG/L 100. 250. Dec 12, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 12, 2002 METHYL IODIDE 1 ND U UG/L 1. 5. Dec 12, 2002 METHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 12, 2002 METHYLENE CHLORIDE 1 ND U UG/L 2. 5. Dec 12, 2002 PENTACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 PROPIONITRILE 1 ND U UG/L 30. 100. Dec 12, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 12, 2002 TETRACHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 TOLUENE 1 ND U UG/L 0.7 5. Dec 12, 2002 TRANS-I,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 TRANS-I,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 12, 2002 TRICHLOROETHENE 1 ND U UG/L 1. 5. Dec 12, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 12, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 12, 2002 Surrogates: 1,2-DICHLOROETHANE-D4 1 103.0 RPR Dec 12, 2002 4-BROMOFLUOROBENZENE 1 98.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 100.0 RPR Dec 12, 2002 TOLUENE-D8 1 103.0 RPR Dec 12, 2002 Comments: Lab personnel entered the date/time of sample FAY-K-TBLK-NAFGW-DAY1 as 05-DEC-02/1315 (date/time of the earliest associated sample) into their system since the fields were empty on COC 66805. These are required fields in the database. DEQ-CFW 00025565 Corporate Environmental Database Lab Analysis Report Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 42 C of C SampLeid: FAY-K-TBLK-NAFGW-DAY2 Sampling Point: TBLK-NAFGW-DAY2 Date Sampled: DECEMBER 5, 2002 Lab Sample ID: 3956317-1 Analysis Lab: LANCAS Sample Type: BLANK WATER QC Level: QC (ADQM QC Process) AnalytelParameter Dilution Result Unit MDL POL Date Analyzed Method: 80158 METHANOL (BY DIRECT INJECTION) 1 NO U UG/L 200. 1000. Dec 13, 2002 Surrogates: ACETONE 1 99.0 RPR Dec 13, 2002 Prep/Method: 503OB18260B 1,1,1,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,1-TRICHLOROETHANE 1 ND U UG/L 0.8 5. Dec 12, 2002 1,1,2,2-TETRACHLOROETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,1,2-TRICHLOROETHANE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,1-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,1-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 1,2,3-TRICHLOROPROPANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,2-DIBROMO-3-CHLOROPROPANE 1 NO U UG/L 2. 5. Dec 12, 2002 1,2-DIBROMOETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 1,2-DICHLOROPROPANE 1 ND U UG/L 1. 5. Dec 12, 2002 1,3-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 1,4-DICHLOROBENZENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-BUTANONE 1 ND U UG/L 3. 10. Dec 12, 2002 2-CHLORO-1,3-BUTADIENE 1 ND U UG/L 1. 5. Dec 12, 2002 2-HEXANONE 1 NO U UG/L 3. 10. Dec 12, 2002 4-METHYL-2-PENTANONE 1 NO U UG/L 3. 10. Dec 12, 2002 ACETONE 1 NO U UG/L 6. 20. Dec 12, 2002 ACETONITRILE 1 NO U UG/L 25. 100. Dec 12, 2002 ALLYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 BENZENE 1 ND U UG/L 0.5 5. Dec 12, 2002 BROMODICHLOROMETHANE I ND U UG/L 1. 5. Dec 12, 2002 BROMOFORM 1 ND U UG/L 1. 5. Dec 12, 2002 BROMOMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 CARBON DISULFIDE 1 NO U UG/L 1. 5. Dec 12, 2002 CARBON TETRACHLORIDE 1 NO U UG/L 1. 5. Dec 12, 2002 CHLOROBENZENE 1 NO U UG/L 0.8 5. Dec 12, 2002 CHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 CHLOROFORM 1 NO U UG/L 0.8 5. Dec 12, 2002 CHLOROMETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 CIS-1,2-DICHLOROETHENE 1 ND U UG/L 0.8 5. Dec 12, 2002 CIS-1,3-DICHLOROPROPENE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOCHLOROMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DIBROMOMETHANE 1 ND U UG/L 1. 5. Dec 12, 2002 DICHLORODIFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 ETHYL METHACRYLATE 1 NO U UG/L 1. 5. Dec 12, 2002 ETHYLBENZENE 1 ND U UG/L 0.8 5. Dec 12, 2002 ISOBUTYL ALCOHOL 1 NO U UG/L 100. 250. Dec 12, 2002 METHACRYLONITRILE 1 ND U UG/L 10. 50. Dec 12, 2002 METHYL IODIDE 1 NO U UG/L 1. 5. Dec 12, 2002 METHYL METHACRYLATE 1 ND U UG/L 1. 5. Dec 12, 2002 METHYLENE CHLORIDE 1 NO U UG/L 2. 5. Dec 12, 2002 PENTACHLOROETHANE 1 NO U UG/L 1. 5. Dec 12, 2002 PROPIONITRILE 1 NO U UG/L 30. 100. Dec 12, 2002 STYRENE 1 ND U UG/L 1. 5. Dec 12, 2002 TETRACHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 TOLUENE 1 NO U UG/L 0.7 5. Dec 12, 2002 TRANS-1,2-DICHLOROETHENE 1 NO U UG/L 0.8 5. Dec 12, 2002 TRANS-1,3-DICHLOROPROPENE 11 ND U UG/L 1. 5. Dec 12, 2002 TRANS-1,4-DICHLORO-2-BUTENE 1 ND U UG/L 15. 50. Dec 12, 2002 TRICHLOROETHENE I ND U UG/L 1. 5. Dec 12, 2002 TRICHLOROFLUOROMETHANE 1 ND U UG/L 2. 5. Dec 12, 2002 VINYL ACETATE 1 ND U UG/L 2. 10. Dec 12, 2002 VINYL CHLORIDE 1 ND U UG/L 1. 5. Dec 12, 2002 XYLENE (TOTAL) 1 ND U UG/L 0.8 5. Dec 12, 2002 Surrogates: 1,2-DICHLOROETHANE-D4 1 102.0 RPR Dec 12, 2002 4-BROMOIFLUOROBENZENE 1 96.0 RPR Dec 12, 2002 DIBROMOFLUOROMETHANE 1 102.0 RPR Dec 12, 2002 TOLUENE-D8 1 101.0 RPR Dec 12, 2002 DEQ-CFW-00025566 Corporate Environmental Database Lab Analysis Report Location: wYsTTsvuLs Job Name: owmu8 GW+2002 c of c ( id: FAY'K'roLc'e*Fmw-oxr2 Sampling Point: TBLm-wxrou-mx,z Date Sampled: occsmoem 5, 2002 Lab Sample ID: 3958317'1 4naivoin Lob: LAwoxo Sample Type: BLANK Wwrco uo Level: oc (*nom mo Process) mno(yte/paruxmtor Dilution xpu _________ ____ --- Comments: January 9, 2003 Page 43 Lab personnel entered the time of collection for sample FAY-x-TmLo mAFuw-nAY2 as 1500 (earliest time of associated i*> into their system since the time was omitted and this is v required field in the database. Vials were received for 8015B. Qualifiers: u The constituent should be considered not detected. Corporate Environmental nutabono Lab Analysis Report Location: FxYsTTsvILcs Job Name: owmo6 ou-2002 c of c s Lid: FAY-K'TBLu'wmruu-nxyZ-Aum Sampling Point: TaLo'w*pow-oxY2 Date Sampled: oECa*mEn 6, 2002 Lab Sample ID: 3950318-1 Analysis Lob: u^wo^S Sample Type: oLxwu wwrsm ou Level: oo (xopm nc Process) AnatytelParameter Dilution Result AcnoLEIw 1 wo u xon,LowzTmILs 1 wu u Surrogates: 1,2-oIcoLomosToxws-o4 1 94'0 mpn 4-BwummFLoonoBEmZEws 1 106'0 npn uI000morLuonoMsToAws 1 91.0 mpw roLoswe'o8 1 186'0 xpx January9, 2003 Page 44 Unit MDL POL Date Analyzed uu/L 40, 100- Dec 10. 2002 un/L 4' 20' Dec YU, 2002 Dec 10, 2002 Dec 10^ 2002 Dec YO, 2002 Dec 10, 2002 nmnmu^tu: Lab personnel entered the time of collection for sample FAY-K'naLK'wxrm+oAY2-*cm as 1100 (earliest time of associated sample) into their system since the time was omitted and this is a required field in the database. Qualifiers: Corporate Environmental Database Lab Analysis Report Summary of Positive Results Location: FAYETTEVILLE January 9, 2003 Job Name: SWMU6 GW-2002 Page 1 AnaLyte/Parameter Result Unit MDL POL Method No. Sampling Point: NAF1 C of C Sampleid: FAY-G-NAF1 Date Sampled: Dec 6, 2002 Sample Type: GROUND WATER CC Level: CC (ADQM CC Process) CHLORIDE 47.1 MG/L 6.0 8.0 300.0 CHLOROFORM 2. 1 UG/L 0.8 5. 8260B Sampling Point: NAF2 C of C Sampleid: FAY-G-NAF-2-DUP Date Sampled: Dec 5, 2002 Sample Type: GROUND WATER CC Level: CC (ADQM CC Process) CHLORIDE 325. MG/L 60. 80. 300.0 FLUORIDE 230. MG/L 16. 20. 300.0 METHANOL (BY DIRECT INJECTION) 1200. UG/L 200. 1000. 8015B ACETONE 45. J UGA 15. 50. 8260B CARBON DISULFIDE 5. 1 UG/L 3. 13. 8260B METHYLENE CHLORIDE 6100. UG/L 100. 250. 8260B 1,4-DIOXANE 2. 1 UG/L 1. 5. 8270C BENZYL ALCOHOL 11. J UG/L 5. 20. 8270C BIS(2-ETHYLHEXYL)PHTHALATE 3. 1 UG/L 2. 10. 8270C NAPHTHALENE 1. 1 UG/L 1. 10. 8270C PHENOL 1. 1 UG/L 1. 10. 8270C Sampling Point: NAF2 C of C Sampleid: FAY-G-NAF2 Date Sampled: Dec 5, 2002 Sample Type: GROUND WATER CC Level: CC (ADQM CC Process) CHLORIDE 332. MG/L 30. 40. 300.0 FLUORIDE 250. MG/L 8.0 10. 300.0 METHANOL (BY DIRECT INJECTION) 1900. UG/L 200. 1000. 8015B ACETONE 35. J UGIL 15. 50. 8260B METHYLENE CHLORIDE 6700. UG/L 100. 250. 8260B 1,4-DIOXANE 2. j UG/L 1. 6. 8270C BENZYL ALCOHOL 15. 1 UG/L 6. 25. 8270C PHENOL 2. 1 UGIL 1. 12. 8270C Sampling Point: NAF2P C of C Sampleid: FAY-G-NAF2P Date Sampled: Dec 5, 2002 Sample Type: GROUND WATER CC Level: CC (ADQM CC Process) 2-BUTANONE 5. 1 UG/L 3. 10. 8260B ACETONE 24. UG/L 6. 20. 82608 CARBON DISULFIDE 5. UG/L 1. 5. 8260B METHYLENE CHLORIDE 6000. UG/L 40. 100. 8260B Sampling Point: NAF3 C of C Sampleid: FAY-G-NAF3 Date Sampled: Dec 5, 2002 Sample Type: GROUND WATER CC Level: CC (ADQM CC Process) CHLORIDE 82.0 MG/L 6.0 8.0 300.0 FLUORIDE 12.5 MG/L 0.40 0.50 300.0 METHYLENE CHLORIDE 4. J UG/L 2. 5. 8260B 1,4-DIOXANE 1. 1 UG/L 1. 5. 8270C Sampling Point: NAF4 C of C Sampleid: FAY-G-NAF4 Date Sampled: Dec 5, 2002 Sample Type: GROUND WATER CC Level: CC (ADQM CC Process) CHLORIDE 90.6 MG/L 6.0 8.0 300.0 DEQ-CFW-00025569 Corporate Environmental Database Lab Analysis Report Summary of Positive Results Location: FAYETTEVILLE Job Name: SWMU6 GW-2002 January 9, 2003 Page 2 AnaLyteZParameter Result Unit MDL PQL Method No. FLUORIDE 3.21 MG7—L U740 U—.50 300.0 ACETONE 13. 1 UG/L 6. 20. 8260B CARBON DISULFIDE 2. 1 UG/L 1. 5. 82608 METHYLENE CHLORIDE 5000. UG/L 200. 500. 82608 TRICHLOROETHENE 2. 1 UG/L 1. 5. 82608 BIS(2-ETHYLHEXYL)PHTHALATE 3. 1 UG/L 2. 11. 8270C Sampling Point: NAF4P C of C Sampleid: FAY-G-NAF4P Date Sampled: Dec 5, 2002 Sample Type: GROUND WATER QC Level: QC (ADQM QC Process) ACETONE 8. 1 UGIL 6. 20. 8260B METHYLENE CHLORIDE 1500. UG/L 40. 100. 8260B Qualifiers: i The result is between MDL and PQL and should be considered an estimate. DEQ-CFW-00025570 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 Batch Identifier Method Number: 300.0 Prep Method: Batch Start Date: 17DECO2 Instrument: 008022 Batch Number: 1 The following field samples are included in this batch: Date QC Sample Name SamnpLed Lab Sample ID Level FAY-G-NAF-2-DUP 05DECO2 3956311-1 LANCAS QC FAY-G-NAF1 06DECO2 3956307-1 LANCAS QC FAY-G-NAF1 06DECO2 3956307-2 LANCAS QC FAY-G-NAF2 05DECO2 3956309-1 LANCAS QC FAY-G-NAF3 05DECO2 3956315-1 LANCAS QC FAY-G-NAF3 05DECO2 3956315-2 LANCAS QC Analyte/Parameter Lab Control Spike: CHLORIDE FLUORIDE Method Blank: CHLORIDE FLUORIDE Matrix Spike: CHLORIDE FLUORIDE Replicate: CHLORIDE FLUORIDE Batch Identifier Method Number: 300.0 Prep Method: Batch Start Date: 17DECO2 Instrument: 008022 Batch Number: 2 Result Unit MDL NO MG/L .3 ND MG/L .08 332. MG/L 250. MG/L Pre -prep: RPR RPD Lab Sample ID 99 LCS-1 LANCAS 95 LCS-1 LANCAS BLANK-1 LANCAS BLANK-1 LANCAS 0 3956309-1 LANCAS 0 3956309-1 LANCAS The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-NAF4 05DECO2 3955485-1 LANCAS QC FAY-G-NAF4 05DECO2 3955485-2 LANCAS QC FAY-K-EQBLK-NAFGW-DAY1 05DECO2 3955487-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: CHLORIDE 99 LCS-1 LANCAS FLUORIDE 95 LCS-1 LANCAS Method Blank: CHLORIDE ND MG/L .3 BLANK-1 LANCAS FLUORIDE ND MG/L .08 BLANK-1 LANCAS Matrix Spike: FLUORIDE 98 3958005-1 LANCAS CHLORIDE 112 3958005-2 LANCAS Replicate: FLUORIDE NO MG/L 0 3958005-1 LANCAS CHLORIDE 7030. MG/L 6 3958005-2 LANCAS Comments: 300.0 (CHLORIDE): The matrix spike recovery was outside control limits. Lab control spike recovery met acceptance criteria. 300.0 (CHLORIDE): The RPD between replicate samples was outside control Limits. DEQ-CFW 00025571 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 Batch Identifier Method Number: 8015B Prep Method: Batch Start Date: 12DECO2 Instrument: 002739 Batch Number: 26 Pre -prep: January 9, 2003 Page 2 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-NAF-2-DUP 05DECO2 3956311-1 LANCAS QC FAY-G-NAF1 06DECO2 3956307-1 LANCAS QC FAY-G-NAF2 05DECO2 3956309-1 LANCAS QC FAY-G-NAF3 05DECO2 3956315-1 LANCAS QC FAY-G-NAF4 05DECO2 3955485-1 LANCAS QC FAY-K-EQBLK-NAFGW-DAY1 05DECO2 3955487-1 LANCAS QC FAY-K-TBLK-NAFGW-DAY2 05DECO2 3956317-1 LANCAS QC Analyte(Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: METHANOL (BY DIRECT INJECTION) 104 LCS-1 LANCAS Method Blank: METHANOL (BY DIRECT INJECTION) ND UG/L 200 BLANK-1 LANCAS Matrix Spike: METHANOL (BY DIRECT INJECTION) 108 3956309-1 LANCAS Matrix Spike Duplicate: METHANOL (BY DIRECT INJECTION) 112 2 3956309-1 LANCAS Batch Identifier Method Number: 8260B Prep Method: 50308 Batch Start Date: 10DECO2 Instrument: 083630 Batch Number: 1 Pre -prep: The following field samples are included in this batch: Date QC Sample Name Sampled Lab SaMple ID Level FAY-G-NAF-2-ACR-DUP 05DECO2 3956312-1 LANCAS QC FAY-G-NAF1-ACR 06DECO2 3956308-1 LANCAS QC FAY-G-NAF2-ACR 05DECO2 3956310-1 LANCAS QC FAY-G-NAF2P-ACR 05DECO2 3956314-1 LANCAS QC FAY-G-NAF3-ACR 05DECO2 3956316-1 LANCAS QC FAY-K-TBLK-NAFGW-DAY2-ACR 06DECO2 3956318-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1,2,4-TRIMETHYLBENZENE 102 LCS-1 LANCAS 1,3,5-TRIMETHYLBENZENE 102 LCS-1 LANCAS ACROLEIN 114 LCS-1 LANCAS ACRYLONITRILE 87 LCS-1 LANCAS BENZENE 96 LCS-1 LANCAS ETHYLBENZENE 107 LCS-1 LANCAS ISOPROPYLBENZENE 110 LCS-1 LANCAS M+P-XYLENE 110 LCS-1 LANCAS 0-XYLENE 108 LCS-1 LANCAS TOLUENE 104 LCS-1 LANCAS Method Blank: 1,2,4-TRIMETHYLBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,3,5-TRIMETHYLSENZENE ND UG/L 1 BLANKA-1 LANCAS ACROLEIN ND UG/L 40 BLANKA-1 LANCAS ACRYLONITRILE ND UG/L 4 BLANKA-1 LANCAS BENZENE ND UG/L .5 BLANKA-1 LANCAS ETHYLBENZENE ND UG/L .8 BLANKA-1 LANCAS ISOPROPYLBENZENE ND UG/L 1 BLANKA-1 LANCAS M+P-XYLENE ND UG/L .8 BLANKA-1 LANCAS 0-XYLENE ND UG/L .8 BLANKA-1 LANCAS TOLUENE ND UG/L .7 BLANKA-1 LANCAS DEQ-CFW 00025572 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike: 1,2,4-TRIMETHYLBENZENE 114 3955464-1 LANCAS 1,3,5-TRIMETHYLBENZENE 113 3955464-1 LANCAS BENZENE 102 3955464-1 LANCAS ETHYLBENZENE 122 3955464-1 LANCAS ISOPROPYLBENZENE 122 3955464-1 LANCAS M+P-XYLENE 124 3955464-1 LANCAS 0-XYLENE 118 3955464-1 LANCAS TOLUENE 122 3955464-1 LANCAS ACROLEIN 0 3956310-1 LANCAS ACRYLONITRILE 87 3956310-1 LANCAS Matrix Spike Duplicate: 1,2,4-TRIMETHYLBENZENE 112 2 3955464-1 LANCAS 1,3,5-TRIMETHYLBENZENE 110 2 3955464-1 LANCAS BENZENE 100 2 3955464-1 LANCAS ETHYLBENZENE 119 3 3955464-1 LANCAS ISOPROPYLBENZENE 121 1 3955464-1 LANCAS M+P-XYLENE 121 2 3955464-1 LANCAS O-XYLENE 119 0 3955464-1 LANCAS TOLUENE 119 3 3955464-1 LANCAS ACROLEIN 0 0 3956310-1 LANCAS ACRYLONITRILE 87 0 3956310-1 LANCAS Comments: 8260B (ACROLEIN): The matrix spike and spike duplicate recoveries were outside control limits. Lab control spike recovery met acceptance criteria. Batch Identifier Method Number: 82608 Prep Method: 5030B Pre -prep: Batch Start Date: 12DECO2 Instrument: 067200 Batch Number: 1 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-NAF-2-DUP 05DECO2 3956311-1 LANCAS QC FAY-G-NAF-2-DUP 05DECO2 3956311-2 LANCAS QC FAY-G-NAF1 06DECO2 3956307-1 LANCAS QC FAY-G-NAF2 05DECO2 3956309-1 LANCAS QC FAY-G-NAF2 05DECO2 3956309-2 LANCAS QC FAY-G-NAF2P 05DECO2 3956313-1 LANCAS QC FAY-G-NAF2P 05DECO2 3956313-2 LANCAS QC FAY-G-NAF3 05DECO2 3956315-1 LANCAS QC FAY-G-NAF4 05DECO2 3955485-1 LANCAS QC FAY-G-NAF4 05DECO2 3955485-2 LANCAS QC FAY-G-NAF4P 05DECO2 3955486-1 LANCAS QC FAY-G-NAF4P 05DECO2 3955486-2 LANCAS QC FAY-K-EQBLK-NAFGW-DAY1 05DECO2 3955487-1 LANCAS QC FAY-K-TBLK-NAFGW-DAY1 05DECO2 3955488-1 LANCAS QC FAY-K-TBLK-NAFGW-DAY2 05DECO2 3956317-1 LANCAS QC Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1,1,1,2-TETRACHLOROETHANE 96 LCS-1 LANCAS 1,1,1-TRICHLOROETHANE 92 LCS-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 116 LCS-1 LANCAS 1,1,2-TRICHLOROETHANE 104 LCS-1 LANCAS 1,1-DICHLOROETHANE ill LCS-1 LANCAS 1,1-DICHLOROETHENE 95 LCS-1 LANCAS 1,2,3-TRICHLOROPROPANE 105 LCS-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 93 LCS-1 LANCAS 1,2-DIBROMOETHANE 104 LCS-1 LANCAS 1,2-DICHLOROBENZEN£ 95 LCS-1 LANCAS 1,2-DICHLOROETHANE 106 LCS-1 LANCAS 1,2-DICHLOROPROPANE 112 LCS-1 LANCAS 1,3-DICHLOROBENZENE 95 LCS-1 LANCAS DEQ-CFW 00025573 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SNMU6 GG-2002 Page 4 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1,4-DICHLOROBENZENE 93 LCS-1 LANCAS 2-BUTANONE 133 LCS-1 LANCAS 2-CHLORO-1,3-BUTADIENE 108 LCS-1 LANCAS 2-HEXANONE 113 LCS-1 LANCAS 4-METHYL-2-PENTANONE 107 LCS-1 LANCAS ACETONE 144 LCS-1 LANCAS ACETONITRILE 109 LCS-1 LANCAS ALLYL CHLORIDE 108 LCS-1 LANCAS BENZENE 108 LCS-1 LANCAS BROMODICHLOROMETHANE 103 LCS-1 LANCAS BROMOFORM 90 LCS-1 LANCAS BROMOMETHANE 87 LCS-1 LANCAS CARBON DISULFIDE 112 LCS-1 LANCAS CARBON TETRACHLORIDE 88 LCS-1 LANCAS CHLOROBENZENE 99 LCS-1 LANCAS CHLOROETHANE 102 LCS-1 LANCAS CHLOROFORM 103 LCS-1 LANCAS CHLOROMETHANE 118 LCS-1 LANCAS CIS-1,2-DICHLOROETHENE 103 LCS-1 LANCAS CIS-1,3-DICHLOROPROPENE 107 LCS-1 LANCAS DIBROMOCHLOROMETHANE 98 LCS-1 LANCAS DIBROMOMETHANE 103 LCS-1 LANCAS DICHLORODIFLUOROMETHANE 94 LCS-1 LANCAS ETHYL METHACRYLATE 103 LCS-1 LANCAS ETHYLBENZENE 95 LCS-1 LANCAS ISOBUTYL ALCOHOL 107 LCS-1 LANCAS METHACRYLONITRILE 114 LCS-1 LANCAS METHYL IODIDE 94 LCS-1 LANCAS METHYL METHACRYLATE 103 LCS-1 LANCAS METHYLENE CHLORIDE 102 LCS-1 LANCAS PENTACHLOROETHANE 84 LCS-1 LANCAS PROPIONITRILE 119 LCS-1 LANCAS STYRENE 93 LCS-1 LANCAS TETRACHLOROETHENE 90 LCS-1 LANCAS TOLUENE 101 LCS-1 LANCAS TRANS-1,2-DICHLOROETHENE 99 LCS-1 LANCAS TRANS-1,3-DICHLOROPROPENE 102 LCS-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE 115 LCS-1 LANCAS TRICHLOROETHENE 102 LCS-1 LANCAS TRICHLOROFLUOROMETHANE 77 LCS-1 LANCAS VINYL ACETATE 128 LCS-1 LANCAS VINYL CHLORIDE 101 LCS-1 LANCAS XYLENE (TOTAL) 91 LCS-1 LANCAS Method Blank: 1,1,1,2-TETRACHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1,1-TRICHLOROETHANE ND UG/L .8 BLANKA-1 LANCAS 1,1,2,2-TETRACHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1,2-TRICHLOROETHANE ND UG/L .8 BLANKA-1 LANCAS 1,1-DICHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,1-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS 1,2,3-TRICHLOROPROPANE ND UG/L 1 BLANKA-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE ND UG/L 2 BLANKA-1 LANCAS 1,2-DIBROMOETHANE ND UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS 1,2-DICHLOROPROPANE ND UG/L 1 BLANKA-1 LANCAS 1,3-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 1,4-DICHLOROBENZENE ND UG/L 1 BLANKA-1 LANCAS 2-BUTANONE ND UG/L 3 BLANKA-1 LANCAS 2-CHLORO-I,3-BUTADIENE ND UG/L 1 BLANKA-1 LANCAS 2-HEXANONE ND UG/L 3 BLANKA-1 LANCAS 4-METHYL-2-PENTANONE ND UG/L 3 BLANKA-1 LANCAS ACETONE ND UG/L 6 BLANKA-1 LANCAS ACETONITRILE ND UG/L 25 BLANKA-1 LANCAS ALLYL CHLORIDE ND UG/L 1 BLANKA-1 LANCAS BENZENE ND UG/L .5 BLANKA-1 LANCAS BROMODICHLOROMETHANE ND UG/L 1 BLANKA-1 LANCAS BROMOFORM ND UG/L 1 BLANKA-1 LANCAS BROMOMETHANE ND UG/L 1 BLANKA-1 LANCAS CARBON DISULFIDE ND UG/L 1 BLANKA-1 LANCAS DEQ-CFW 00025574 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 (Batch continued from previous page) January 9, 2003 Page 5 Analyte/Parameter Result Unit MDL RPR RPD Lab Sande ID Method Blank: CARBON TETRACHLORIDE NO UG/L 1 BLANKA-1 LANCAS CHLOROBENZENE ND UG/L .8 BLANKA-1 LANCAS CHLOROETHANE ND UG/L 1 BLANKA-1 LANCAS CHLOROFORM ND UG/L .8 BLANKA-1 LANCAS CHLOROMETHANE NO UG/L 1 BLANKA-1 LANCAS CIS-1,2-DICHLOROETHENE ND UG/L .8 BLANKA-1 LANCAS CIS-1,3-DICHLOROPROPENE ND UG/L 1 BLANKA-1 LANCAS DIBROMOCHLOROMETHANE ND UG/L 1 BLANKA-1 LANCAS DIBROMOMETHANE ND UG/L 1 BLANKA-1 LANCAS DICHLORODIFLUOROMETHANE ND UG/L 2 BLANKA-1 LANCAS ETHYL METHACRYLATE NO UG/L 1 BLANKA-1 LANCAS ETHYLBENZENE ND UG/L .8 BLANKA-1 LANCAS ISOBUTYL ALCOHOL NO UG/L 100 BLANKA-1 LANCAS METHACRYLONITRILE NO UG/L 10 BLANKA-1 LANCAS METHYL IODIDE NO UG/L 1 BLANKA-1 LANCAS METHYL METHACRYLATE ND UG/L 1 BLANKA-1 LANCAS METHYLENE CHLORIDE ND UG/L 2 BLANKA-1 LANCAS PENTACHLOROETHANE NO UG/L 1 BLANKA-1 LANCAS PROPIONITRILE NO UG/L 30 BLANKA-1 LANCAS STYRENE NO UG/L 1 BLANKA-1 LANCAS TETRACHLOROETHENE NO UG/L .8 BLANKA-1 LANCAS TOLUENE ND UG/L .7 BLANKA-1 LANCAS TRANS-I,2-DICHLOROETHENE NO UG/L .8 BLANKA-1 LANCAS TRANS-1,3-DICHLOROPROPENE ND UG/L 1 BLANKA-1 LANCAS TRANS-I,4-DICHLORO-2-BUTENE NO UG/L 15 BLANKA-1 LANCAS TRICHLOROETHENE ND UG/L 1 BLANKA-1 LANCAS TRICHLOROFLUOROMETHANE ND UG/L 2 BLANKA-1 LANCAS VINYL ACETATE NO UG/L 2 BLANKA-1 LANCAS VINYL CHLORIDE ND UG/L 1 BLANKA-1 LANCAS XYLENE (TOTAL) ND UG/L .8 BLANKA-1 LANCAS METHYLENE CHLORIDE ND UG/L 2 BLANKB-1 LANCAS Matrix Spike: 1,1,1,2-TETRACHLOROETHANE 97 3956309-1 LANCAS 1,1,1-TRICHLOROETHANE 90 3956309-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 108 3956309-1 LANCAS 1,1,2-TRICHLOROETHANE 100 3956309-1 LANCAS 1,1-DICHLOROETHANE 112 3956309-1 LANCAS 1,1-DICHLOROETHENE 100 3956309-1 LANCAS 1,2,3-TRICHLOROPROPANE 99 3956309-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 90 3956309-1 LANCAS 1,2-DIBROMOETHANE 100 3956309-1 LANCAS 1,2-DICHLOROBENZENE 93 3956309-1 LANCAS 1,2-DICHLOROETHANE 105 3956309-1 LANCAS 1,2-DICHLOROPROPANE 112 3956309-1 LANCAS 1,3-DICHLOROBENZENE 93 3956309-1 LANCAS 1,4-DICHLOROBENZENE 93 3956309-1 LANCAS 2-BUTANONE 163 3956309-1 LANCAS 2-CHLORO-1,3-BUTADIENE 109 3956309-1 LANCAS 2-HEXANONE 148 3956309-1 LANCAS 4-METHYL-2-PENTANONE 110 3956309-1 LANCAS ACETONE 148 3956309-1 LANCAS ACETONITRILE 70 3956309-1 LANCAS ALLYL CHLORIDE 105 3956309-1 LANCAS BENZENE 106 3956309-1 LANCAS BROMODICHLOROMETHANE 101 3956309-1 LANCAS BROMOFORM 84 3956309-1 LANCAS BROMOMETHANE 90 3956309-1 LANCAS CARBON DISULFIDE 116 3956309-1 LANCAS CARBON TETRACHLORIDE 91 3956309-1 LANCAS CHLOROBENZENE 98 3956309-1 LANCAS CHLOROETHANE 103 3956309-1 LANCAS CHLOROFORM 102 3956309-1 LANCAS CHLOROMETHANE 103 3956309-1 LANCAS CIS-1,2-DICHLOROETHENE- 101 3956309-1 LANCAS CIS-1,3-DICHLOROPROPENE 101 3956309-1 LANCAS DIBROMOCHLOROMETHANE 94 3956309-1 LANCAS DIBROMOMETHANE 98 3956309-1 LANCAS DICHLORODIFLUOROMETHANE 96 3956309-1 LANCAS ETHYL METHACRYLATE 100 3956309-1 LANCAS ETHYLBENZENE 95 3956309-1 LANCAS DEQ-CFW 00025575 Corporate Environmental Database Lab Analysis QA®C Report Location: FAYETTEVILLE Project Name: SWMU6 6W-2002 (Batch continued from previous page) January 9, 2003 Page 6 Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike; ISOBUTYL ALCOHOL 88 3956309-1 LANCAS METHACRYLONITRILE 101 3956309-1 LANCAS METHYL IODIDE 91 3956309-1 LANCAS METHYL METHACRYLATE 96 3956309-1 LANCAS METHYLENE CHLORIDE -1101 3956309-1 LANCAS PENTACHLOROETHANE 80 3956309-1 LANCAS PROPIONITRILE 97 3956309-1 LANCAS STYRENE 92 3956309-1 LANCAS TETRACHLOROETHENE 93 3956309-1 LANCAS TOLUENE 102 3956309-1 LANCAS TRANS-1,2-DICHLOROETHENE 96 3956309-1 LANCAS TRANS-I,3-DICHLOROPROPENE 97 3956309-1 LANCAS TRANS-1,4-DICHLORO-2-BUTENE 77 3956309-1 LANCAS TRICHLOROETHENE 103 3956309-1 LANCAS TRICHLOROFLUOROMETHANE 79 3956309-1 LANCAS VINYL ACETATE 129 3956309-1 LANCAS VINYL CHLORIDE 98 3956309-1 LANCAS XYLENE (TOTAL) 92 3956309-1 LANCAS Matrix Spike Duplicate: 1,1,1,2-TETRACHLOROETHANE 96 0 3956309-1 LANCAS 1,1,1-TRICHLOROETHANE 90 0 3956309-1 LANCAS 1,1,2,2-TETRACHLOROETHANE 108 0 3956309-1 LANCAS 1,1,2-TRICHLOROETHANE 103 3 3956309-1 LANCAS 1,1-DICHLOROETHANE ill 1 3956309-1 LANCAS 1,1-DICHLOROETHENE 94 6 3956309-1 LANCAS 1,2,3-TRICHLOROPROPANE 104 5 3956309-1 LANCAS 1,2-DIBROMO-3-CHLOROPROPANE 88 2 3956309-1 LANCAS 1,2-DIBROMOETHANE 102 2 3956309-1 LANCAS 1,2-DICHLOROBENZENE 96 3 3956309-1 LANCAS 1,2-DICHLOROETHANE 106 1 3956309-1 LANCAS 1,2-DICHLOROPROPANE 113 1 3956309-1 LANCAS 1,3-DICHLOROBENZENE 93 1 3956309-1 LANCAS 1,4-DICHLOROBENZENE 95 2 3956309-1 LANCAS 2-BUTANONE 154 6 3956309-1 LANCAS 2-CHLORO-I,3-BUTADIENE 104 4 3956309-1 LANCAS 2-HEXANONE 152 3 3956309-1 LANCAS 4-METHYL-2-PENTANONE ill 1 3956309-1 LANCAS ACETONE 117 21 3956309-1 LANCAS ACETONITRILE 69 2 3956309-1 LANCAS ALLYL CHLORIDE 103 2 3956309-1 LANCAS BENZENE 108 1 3956309-1 LANCAS BROMODICHLOROMETHANE 101 0 3956309-1 LANCAS BROMOFORM 88 4 3956309-1 LANCAS BROMOMETHANE 89 0 3956309-1 LANCAS CARBON DISULFIDE 114 2 3956309-1 LANCAS CARBON TETRACHLORIDE 86 6 3956309-1 LANCAS CHLOROBENZENE 100 2 3956309-1 LANCAS CHLOROETHANE 100 2 3956309-1 LANCAS CHLOROFORM 104 2 3956309-1 LANCAS CHLOROMETHANE 103 0 3956309-1 LANCAS CIS-1,2-DICHLOROETHENE 102 1 3956309-1 LANCAS CIS-1,3-DICHLOROPROPENE 103 2 3956309-1 LANCAS DIBROMOCHLOROMETHANE 99 4 3956309-1 LANCAS DIBROMOMETHANE 106 8 3956309-1 LANCAS DICHLORODIFLUOROMETHANE 95 1 3956309-1 LANCAS ETHYL METHACRYLATE 103 2 3956309-1 LANCAS ETHYLBENZENE 94 0 3956309-1 LANCAS ISOBUTYL ALCOHOL 79 12 3956309-1 LANCAS METHACRYLONITRILE 105 4 3956309-1 LANCAS METHYL IODIDE 92 0 3956309-1 LANCAS METHYL METHACRYLATE 99 3 3956309-1 LANCAS METHYLENE CHLORIDE -945 1 3956309-1 LANCAS PENTACHLOROETHANE 81 1 3956309-1 LANCAS PROPIONITRILE 93 5 3956309-1 LANCAS STYRENE 93 1 3956309-1 LANCAS TETRACHLOROETHENE 92 2 3956309-1 LANCAS TOLUENE 101 0 3956309-1 LANCAS TRANS-1,2-DICHLOROETHENE 98 2 3956309-1 LANCAS TRANS-1,3-DICHLOROPROPENE 101 4 3956309-1 LANCAS TRANS-1,4-DICHLORO-2-BUTENE 66 16 3956309-1 LANCAS DEQ-CFW 00025576 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 (Batch continued from previous page) January 9, 2003 Page 7 AnaLyteLParameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike Duplicate: TRICHLORCETHENE 101 2 3956309-1 LANCAS TRICHLOROFLUOROMETHANE 76 5 3956309-1 LANCAS VINYL ACETATE 131 2 3956309-1 LANCAS VINYL CHLORIDE 96 3 3956309-1 LANCAS XYLENE (TOTAL) 91 1 3956309-1 LANCAS Comments: 8260B (2-BUTANONE): The matrix spike and spike duplicate recoveries were outside control limits. Lab control spike recovery met acceptance criteria. 8260B (2-NEXANONE): The matrix spike and spike duplicate recoveries were outside control Limits. Lab control spike recovery met acceptance criteria. 8260B (ACETONE): The matrix spike recovery was outside control Limits. Lab control spike recovery met acceptance criteria. 82609 (METHYLENE CHLORIDE): The matrix spike and spike duplicate recoveries were outside control Limits due to the native concentration being significantly greater than the spike concentration. Batch Identifier Method Number: 8270C Prep Method: 3510C Pre -prep: Batch Start Date: 09DECO2 Instrument: 067550 Batch Number: 7 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-NAF4 05DECO2 3955485-1 LANCAS 0C FAY-K-EQBLK-NAFGW-DAY1 05DECO2 3955487-1 LANCAS 0C Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 1,2,4,5-TETRACHLOROBENZENE 88 LCS-1 LANCAS 1,2,4-TRICHLOROBENZENE 80 LCS-1 LANCAS 1,2-DICHLOROBENZENE 77 LCS-1 LANCAS 1,3,5-TRINITROBENZENE 82 LCS-1 LANCAS 1,3-DICHLOROBENZENE 74 LCS-1 LANCAS 1,3-DINITROBENZENE 99 LCS-1 LANCAS 1,4-DICHLOROBENZENE 73 LCS-1 LANCAS 1,4-DIOXANE 65 LCS-1 LANCAS 1,4-NAPHTHOQUINONE 14 LCS-1 LANCAS 1,4-PHENYLENEDIAMINE 0 LCS-1 LANCAS 1-NAPHTHYLAMINE 65 LCS-1 LANCAS 2,3,4,6-TETRACHLOROPHENOL ill LCS-1 LANCAS 2,4,5-TRICHLOROPHENOL 98 LCS-1 LANCAS 2,4,6-TRICHLOROPHENOL 97 LCS-1 LANCAS 2,4-DICHLOROPHENOL 95 LCS-1 LANCAS 2,4-DIMETHYLPHENOL 95 LCS-1 LANCAS 2,4-DINITROPHENOL 96 LCS-1 LANCAS 2,4-DINITROTOLUENE 101 LCS-1 LANCAS 2,6-DICHLOROPHENOL 98 LCS-1 LANCAS 2,6-DINITROTOLUENE 96 LCS-1 LANCAS 2-ACETYLAMINOFLUORENE 94 LCS-1 LANCAS 2-CHLORONAPHTHALENE 91 LCS-1 LANCAS 2-CHLOROPHENOL 93 LCS-1 LANCAS 2-METHYLNAPHTHALENE 90 LCS-1 LANCAS 2-METHYLPHENOL 86 LCS-1 LANCAS 2-NAPHTHYLAMINE 70 LCS-1 LANCAS 2-NITROANILINE 101 LCS-1 LANCAS 2-NITROPHENOL 97 LCS-1 LANCAS 2-PICOLINE 89 LCS-1 LANCAS 3,31-DICHLOROBENZIDINE 84 LCS-1 LANCAS 3,3--DIMETHYLBENZIDINE 51 LCS-1 LANCAS 3-METHYLCHOLANTHRENE 102 LCS-1 LANCAS 3-NITROANILINE 93 LCS-1 LANCAS 4,6-DINITRO-2-METHYLPHENOL 97 LCS-1 LANCAS 4-AMINOBIPHENYL 39 LCS-1 LANCAS 4-BROMOPHENYL-PHENYLETHER 96 LCS-1 LANCAS 4-CHLORO-3-METHYLPHENOL 103 LCS-1 LANCAS DEQ-CFW-00025577 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SWMU6 GW-2002 page 8 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 4-CHLOROANILINE 88 LCS-1 LANCAS 4-CHLOROPHENYL-PHENYLETHER 93 LCS-1 LANCAS 4-METHYLPHENOL 80 LCS-1 LANCAS 4-NITROANILINE 85 LCS-1 LANCAS 4-NITROPHENOL 51 LCS-1 LANCAS 4-NITROQUINOLINE-1-OXIDE 85 LCS-1 LANCAS 5-NITRO-0-TOLUIDINE 81 LCS-1 LANCAS 7,12-DIMETHYLBENZEA]ANTHRACENE 74 LCS-1 LANCAS A,A-DIMETHYLPHENETHYLAMINE 91 LCS-1 LANCAS ACENAPHTHENE 98 LCS-1 LANCAS ACENAPHTHYLENE 93 LCS-1 LANCAS ACETOPHENONE 93 LCS-1 LANCAS ANILINE 84 LCS-1 LANCAS ANTHRACENE 99 LCS-1 LANCAS ARAMITE 77 LCS-1 LANCAS BENZO(A)ANTHRACENE 95 LCS-1 LANCAS BENZO(A)PYRENE 101 LCS-1 LANCAS BENZO(B)FLUORANTHENE 101 LCS-1 LANCAS BENZO(G,H,I)PERYLENE 97 LCS-1 LANCAS BENZO(K)FLUORANTHENE 99 LCS-1 LANCAS BENZYL ALCOHOL 83 LCS-1 LANCAS BIS(2-CHLOROETHOXY)METHANE 104 LCS-1 LANCAS BIS(2-CHLOROETHYL)ETHER 93 LCS-1 LANCAS BIS(2-CHLOROISOPROPYL)ETHER 116 LCS-1 LANCAS BIS(2-ETHYLHEXYL)PHTHALATE 92 LCS-1 LANCAS BUTYLBENZYLPHTHALATE 95 LCS-1 LANCAS CHLOROBENZILATE 90 LCS-1 LANCAS CHRYSENE 98 LCS-1 LANCAS DI-N-BUTYLPHTHALATE 96 LCS-1 LANCAS DI-N-OCTYLPHTHALATE 95 LCS-1 LANCAS DIALLATE TRANS/CIS 101 LCS-1 LANCAS DIBENZ(A,H)ANTHRACENE 106 LCS-1 LANCAS DIBENZOFURAN 93 LCS-1 LANCAS DIETHYLPHTHALATE 91 LCS-1 LANCAS DIMETHOATE 53 LCS-1 LANCAS DIMETHYLPHTHALATE 83 LCS-1 LANCAS ETHYL METHANESULFONATE 96 LCS-1 LANCAS FLUORANTHENE 95 LCS-1 LANCAS FLUORENE 94 LCS-1 LANCAS HEXACHLOROBENZENE 98 LCS-1 LANCAS HEXACHLOROBUTADIENE 67 LCS-1 LANCAS HEXACHLOROCYCLOPENTADIENE 62 LCS-1 LANCAS HEXACHLOROETHANE 64 LCS-1 LANCAS HEXACHLOROPRQPENE 70 LCS-1 LANCAS INDENO(1,2,3-CD)PYRENE 100 LCS-1 LANCAS ISODRIN 100 LCS-1 LANCAS ISOPHORONE 94 LCS-1 LANCAS ISOSAFROLE 86 LCS-1 LANCAS METHAPYRILENE 18 LCS-1 LANCAS METHYL METHANESULFONATE 63 LCS-1 LANCAS N-NITROSO-DI-N-PROPYLAMINE 99 LCS-1 LANCAS N-NITROSODI-N-BUTYLAMINE 91 LCS-1 LANCAS N-NITROSODIETHYLAMINE 97 LCS-1 LANCAS N-NITROSODIMETHYLAMINE 68 LCS-1 LANCAS N-NITROSODIPHENYLAMINE 92 LCS-1 LANCAS N-NITROSOMETHYLETHYLAMINE 93 LCS-1 LANCAS N-NITROSOMORPHOLINE 92 LCS-1 LANCAS N-NITROSOPIPERIDINE 96 LCS-1 LANCAS N-NITROSOPYRROLIDINE 94 LCS-1 LANCAS NAPHTHALENE 90 LCS-1 LANCAS NITROBENZENE 95 LCS-1 LANCAS 0,0,0-TRIETHYLPHOSPHOROTHIOATE 97 LCS-1 LANCAS 0-TOLUIDINE 78 LCS-1 LANCAS P-DIMETHYLAMINOAZOBENZENE 90 LCS-1 LANCAS PENTACHLOROBENZENE 97 LCS-1 LANCAS PENTACHLORONITROBENZENE 97 LCS-1 LANCAS PENTACHLOROPHENOL 91 LCS-1 LANCAS PHENACETIN 98 LCS-1 LANCAS PHENANTHRENE 98 LCS-1 LANCAS PHENOL 44 LCS-1 LANCAS PRONAMIDE 95 LCS-1 LANCAS DEQ-CFW 00025578 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control. Spike: PYRENE 99 LCS-1 LANCAS PYRIDINE 66 LCS-1 LANCAS SAFROLE 96 LCS-1 LANCAS TETRAETHYLDITHIOPYROPHOSPHATE 99 LCS-1 LANCAS THIONAZIN 96 LCS-1 LANCAS Lab Controt Spike Duplicate: 1,2,4,5-TETRACHLOROBENZENE 90 2 LCSD-1 LANCAS 1,2,4-TRICHLOROBENZENE 85 5 LCSD-1 LANCAS 1,2-DICHLOROBENZENE 78 1 LCSD-1 LANCAS 1,3,5-TRINITROBENZENE 84 2 LCSD-1 LANCAS 1,3-DICHLOROBENZENE 76 3 LCSD-1 LANCAS 1,3-DINITROBENZENE 101 1 LCSD-1 LANCAS 1,4-DICHLOROBENZENE 75 3 LCSD-1 LANCAS 1,4-DIOXANE 61 5 LCSD-1 LANCAS 1,4-NAPHTHOQUINONE 12 10 LCSD-1 LANCAS 1,4-PHENYLENEDIAMINE 0 0 LCSD-1 LANCAS 1-NAPHTHYLAMINE 38 52 LCSD-1 LANCAS 2,3,4,6-TETRACHLOROPHENOL 115 4 LCSD-1 LANCAS 2,4,5-TRICHLOROPHENOL 99 1 LCSD-1 LANCAS 2,4,6-TRICHLOROPHENOL 97 0 LCSD-1 LANCAS 2,4-DICHLOROPHENOL 97 2 LCSD-1 LANCAS 2,4-DIMETHYLPHENOL 95 0 LCSD-1 LANCAS 2,4-DINITROPHENOL 98 2 LCSD-1 LANCAS 2,4-DINITROTOLUENE 102 1 LCSD-1 LANCAS 2,6-DICHLOROPHENOL 101 3 LCSD-1 LANCAS 2,6-DINITROTOLUENE 96 0 LCSD-1 LANCAS 2-ACETYLAMINOFLUORENE 100 6 LCSD-1 LANCAS 2-CHLORONAPHTHALENE 93 2 LCSD-1 LANCAS 2-CHLOROPHENOL 93 0 LCSD-1 LANCAS 2-METHYLNAPHTHALENE 90 0 LCSD-1 LANCAS 2-METHYLPHENOL 86 1 LCSD-1 LANCAS 2-NAPHTHYLAMINE 46 42 LCSD-1 LANCAS 2-NITROANILINE 102 1 LCSD-1 LANCAS 2-NITROPHENOL 100 3 LCSD-1 LANCAS 2-PICOLINE 88 1 LCSD-1 LANCAS 3,31-DICHLOROBENZIDINE 78 6 LCSD-1 LANCAS 3,31-DIMETHYLBENZIDINE 42 19 LCSD-1 LANCAS 3-METHYLCHOLANTHRENE 102 0 LCSD-1 LANCAS 3-NITROANILINE 76 20 LCSD-1 LANCAS 4,6-DINITRO-2-METHYLPHENOL 101 4 LCSD-1 LANCAS 4-AMINOBIPHENYL 36 6 LCSD-1 LANCAS 4-BROMOPHENYL-PHENYLETHER 100 4 LCSD-1 LANCAS 4-CHLORO-3-METHYLPHENOL 103 1 LCSD-1 LANCAS 4-CHLOROANILINE 59 39 LCSD-1 LANCAS 4-CHLOROPHENYL-PHENYLETHER 94 2 LCSD-1 LANCAS 4-METHYLPHENOL 79 1 LCSD-1 LANCAS 4-NITROANILINE 81 5 LCSD-1 LANCAS 4-NITROPHENOL 63 21 LCSD-1 LANCAS 4-NITROQUINOLINE-I-OXIDE 81 5 LCSD-1 LANCAS 5-NITRO-0-TOLUIDINE 73 10 LCSD-1 LANCAS 7,12-DIMETHYLBENZ[AIANTHRACENE 72 2 LCSD-1 LANCAS A,A-DIMETHYLPHENETHYLAMINE 93 3 LCSD-1 LANCAS ACENAPHTHENE 99 1 LCSD-1 LANCAS ACENAPHTHYLENE 94 0 LCSD-1 LANCAS ACETOPHENONE 94 1 LCSD-1 LANCAS ANILINE 72 15 LCSD-1 LANCAS ANTHRACENE 102 3 LCSD-1 LANCAS ARAMITE 77 0 LCSD-1 LANCAS BENZO(A)ANTHRACENE 97 2 LCSD-1 LANCAS BENZO(A)PYRENE 100 1 LCSD-1 LANCAS BENZO(B)FLUORANTHENE 103 2 LCSD-1 LANCAS BENZO(G,H,I)PERYLENE 98 0 LCSD-1 LANCAS BENZO(K)FLUORANTHENE 98 1 LCSD-1 LANCAS BENZYL ALCOHOL 83 1 LCSD-1 LANCAS BIS(2-CHLOROETHOXY)METHANE 105 1 LCSD-1 LANCAS BIS(2-CHLOROETHYL)ETHER 94 1 LCSD-1 LANCAS BIS(2-CHLOROISOPROPYL)ETHER 118 1 LCSD-1 LANCAS BIS(2-ETHYLHEXYL)PHTHALATE 93 2 LCSD-1 LANCAS BUTYLBENZYLPHTHALATE 98 3 LCSD-1 LANCAS CHLOROBENZILATE 91 1 LCSD-1 LANCAS DEQ-CFW 00025579 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SWMU6 GW-2002 Page 10 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike Duplicate: CHRYSENE 100 2 LCSD-1 LANCAS DI-N-BUTYLPHTHALATE 100 4 LCSD-1 LANCAS DI-N-OCTYLPHTHALATE 94 0 LCSD-1 LANCAS DIALLATE TRANS/CIS 109 7 LCSD-1 LANCAS DIBENZ(A,H)ANTHRACENE 107 1 LCSD-1 LANCAS DIBENZOFURAN 96 2 LCSD-1 LANCAS DIETHYLPHTHALATE 91 1 LCSD-1 LANCAS DIMETHOATE 47 12 LCSD-1 LANCAS DIMETHYLPHTHALATE 83 1 LCSD-1 LANCAS ETHYL METHANESULFONATE 98 1 LCSD-1 LANCAS FLUORANTHENE 96 1 LCSD-1 LANCAS FLUORENE 95 1 LCSD-1 LANCAS HEXACHLOROBENZENE 100 1 LCSD-1 LANCAS HEXACHLOROBUTADIENE 70 5 LCSD-1 LANCAS HEXACHLOROCYCLOPENTADIENE 60 3 LCSD-1 LANCAS HEXACHLOROETHANE 65 2 LCSD-1 LANCAS HEXACHLOROPROPENE 73 5 LCSD-1 LANCAS INDENO(1,2,3-CD)PYRENE 101 1 LCSD-1 LANCAS ISODRIN 108 8 LCSD-1 LANCAS ISOPHORONE 94 0 LCSD-1 LANCAS ISOSAFROLE 90 5 LCSD-1 LANCAS METHAPYRILENE 20 9 LCSD-1 LANCAS METHYL METHANESULFONATE 61 3 LCSD-1 LANCAS N-NITROSO-DI-N-PROPYLAMINE 101 3 LCSD-1 LANCAS N-NITROSODI-N-BUTYLAMINE 96 5 LCSD-1 LANCAS N-NITROSODIETHYLAMINE 102 5 LCSD-1 LANCAS N-NITROSODIMETHYLAMINE 68 0 LCSD-1 LANCAS N-NITROSODIPHENYLAMINE 95 2 LCSD-1 LANCAS N-NITROSOMETHYLETHYLAMINE 91 2 LCSD-1 LANCAS N-NITROSOMORPHOLINE 92 0 LCSD-1 LANCAS N-NITROSOPIPERIDINE 100 4 LCSD-1 LANCAS N-NITROSOPYRROLIDINE 95 2 LCSD-1 LANCAS NAPHTHALENE 92 2 LCSD-1 LANCAS NITROBENZENE 96 1 LCSD-1 LANCAS 0,0,0-TRIETHYLPHOSPHOROTHIOATE 102 5 LCSD-1 LANCAS 0-TOLUIDINE 54 38 LCSD-1 LANCAS P-DIMETHYLAMINOAZOBENZENE 95 5 LCSD-1 LANCAS PENTACHLOROBENZENE 99 3 LCSD-1 LANCAS PENTACHLORONITROBENZENE 105 8 LCSD-1 LANCAS PENTACHLOROPHENOL 91 0 LCSD-1 LANCAS PHENACETIN 102 4 LCSD-1 LANCAS PHENANTHRENE 101 3 LCSD-1 LANCAS PHENOL 43 1 LCSD-1 LANCAS PRONAMIDE 101 7 LCSD-1 LANCAS PYRENE 102 3 LCSD-1 LANCAS PYRIDINE 65 2 LCSD-1 LANCAS SAFROLE 99 3 LCSD-1 LANCAS TETRAETHYLDITHIOPYROPHOSPHATE 103 4 LCSD-1 LANCAS THIONAZIN 100 4 LCSD-1 LANCAS Method Blank: 1,2,4,5-TETRACHLOROBENZENE ND UG/L 2 BLANK-1 LANCAS 1,2,4-TRICHLOROBENZENE NO UG/L 1 BLANK-1 LANCAS 1,2-DICHLOROBENZENE NO UG/L 1 BLANK-1 LANCAS 1,3,5-TRINITROBENZENE NO UG/L 5 BLANK-1 LANCAS 1,3-DICHLOROBENZENE NO UG/L 1 BLANK-1 LANCAS 1,3-DINITROBENZENE NO UG/L 2 BLANK-1 LANCAS 1,4-DICHLOROBENZENE NO UG/L 1 BLANK-1 LANCAS 1,4-DIOXANE ND UG/L 1 BLANK-1 LANCAS 1,4-NAPHTHOQUINONE ND UG/L 10 BLANK-1 LANCAS 1,4-PHENYLENEDIAMINE ND UG/L 60 BLANK-1 LANCAS 1-NAPHTHYLAMINE ND UG/L 5 BLANK-1 LANCAS 2,3,4,6-TETRACHLOROPHENOL ND UG/L 2 BLANK-1 LANCAS 2,4,5-TRICHLOROPHENOL ND UG/L 1 BLANK-1 LANCAS 2,4,6-TRICHLOROPHENOL ND UG/L 1 BLANK-1 LANCAS 2,4-DICHLOROPHENOL ND UG/L 1 BLANK-1 LANCAS 2,4-DIMETHYLPHENOL ND UG/L 1 BLANK-1 LANCAS 2,4-DINITROPHENOL ND UG/L 20 BLANK-1 LANCAS 2,4-DINITROTOLUENE ND UG/L 1 BLANK-1 LANCAS 2,6-DICHLOROPHENOL ND UG/L 2 BLANK-1 LANCAS 2,6-DINITROTOLUENE ND UG/L 1 BLANK-1 LANCAS DEQ-CFW 00025580 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SHMU6 GU-2002 Page 11 (Batch continued from previous page) Ana[ytejParameter Result Unit MDL RPR RPD Lab Sample ID Method Blank: 2-ACETYLAMINOFLUORENE ND UG/L 2 BLANK-1 LANCAS 2-CHLORONAPHTHALENE ND UG/L 1 BLANK-1 LANCAS 2-CHLOROPHENOL ND UG/L 1 BLANK-1 LANCAS 2-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS 2-METHYLPHENOL ND UG/L 1 BLANK-1 LANCAS 2-NAPHTHYLAMINE ND UG/L 5 BLANK-1 LANCAS 2-NITROANILINE ND UG/L 1 BLANK-1 LANCAS 2-NITROPHENOL ND UG/L 1 BLANK-1 LANCAS 2-PICOLINE ND UG/L 2 BLANK-1 LANCAS 3,31-DICHLOROBENZIDINE ND UG/L 1 BLANK-1 LANCAS 3,31-DIMETHYLBENZIDINE ND UG/L 5 BLANK-1 LANCAS 3-METHYLCHOLANTHRENE ND UG/L 2 BLANK-1 LANCAS 3-NITROANILINE ND UG/L 1 BLANK-1 LANCAS 4,6-DINITRO-2-METHYLPHENOL ND UG/L 5 BLANK-1 LANCAS 4-AMINOBIPHENYL ND UG/L 2 BLANK-1 LANCAS 4-BROMOPHENYL-PHENYLETHER ND UG/L 1 BLANK-1 LANCAS 4-CHLORO-3-METHYLPHENOL ND UG/L 1 BLANK-1 LANCAS 4-CHLOROANILINE ND UG/L 1 BLANK-1 LANCAS 4-CHLOROPHENYL-PHENYLETHER ND UG/L 1 BLANK-1 LANCAS 4-METHYLPHENOL ND UG/L 2 BLANK-1 LANCAS 4-NITROANILINE ND UG/L 1 BLANK-1 LANCAS 4-NITROPHENOL ND UG/L 10 BLANK-1 LANCAS 4-NITROQUINOLINE-1-OXIDE ND UG/L 20 BLANK-1 LANCAS 5-NITRO-0-TOLUIDINE ND UG/L 3 BLANK-1 LANCAS 7,12-DIMETHYLBENZ[AIANTHRACENE ND UG/L 2 BLANK-1 LANCAS A,A-DIMETHYLPHENETHYLAMINE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHYLENE ND UG/L 1 BLANK-1 LANCAS ACETOPHENONE ND UG/L 2 BLANK-1 LANCAS ANILINE ND UG/L 1 BLANK-1 LANCAS ANTHRACENE ND UG/L 1 BLANK-1 LANCAS ARAMITE ND UG/L 1 BLANK-1 LANCAS BENZO(A)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)PYRENE ND UG/L 1 BLANK-1 LANCAS BENZO(B)FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS BENZO(G,H,I)PERYLENE ND UG/L 1 BLANK-1 LANCAS BENZO(K)FLUORANTHENE NO UG/L 1 BLANK-1 LANCAS BENZYL ALCOHOL ND UG/L 5 BLANK-1 LANCAS SIS(2-CHLOROETHOXY)METHANE ND UG/L 1 BLANK-1 LANCAS BIS(2-CHLOROETHYL)ETHER ND UG/L 1 BLANK-1 LANCAS BIS(2-CHLOROISOPROPYL)ETHER NO UG/L 1 BLANK-1 LANCAS BIS(2-ETHYLHEXYL)PHTHALATE ND UG/L 2 8LANK-1 LANCAS BUTYLBENZYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS CHLOROBENZILATE ND UG/L 3 BLANK-1 LANCAS CHRYSENE ND UG/L 1 BLANK-1 LANCAS DI-N-BUTYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS DI-N-OCTYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS DIALLATE TRANS/CIS ND UG/L 1 BLANK-1 LANCAS DIBENZ(A,H)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS DIBENZOFURAN ND UG/L 1 BLANK-1 LANCAS DIETHYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS DIMETHOATE ND UG/L 3 BLANK-1 LANCAS DIMETHYLPHTHALATE NO UG/L 2 BLANK-1 LANCAS ETHYL METHANESULFONATE ND UG/L 2 BLANK-1 LANCAS FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS FLUORENE NO UGIL 1 BLANK-1 LANCAS HEXACHLOROBENZENE ND UG/L 1 8LANK-1 LANCAS HEXACHLOROBUTADIENE ND UG/L 1 BLANK-1 LANCAS HEXACHLOROCYCLOPENTADIENE ND UG/L 5 SLANK-1 LANCAS HEXACHLOROETHANE ND UG/L 1 BLANK-1 LANCAS HEXACHLOROPROPENE ND UG/L 2 BLANK-1 LANCAS INDENO(1,2,3-CD)PYRENE ND UG/L 1 BLANK-1 LANCAS ISODRIN ND UG/L 1 BLANK-1 LANCAS ISOPHORONE ND UG/L 1 BLANK-1 LANCAS ISOSAFROLE ND UG/L 1 BLANK-1 LANCAS METHAPYRILENE ND UG/L 3 BLANK-1 LANCAS METHYL METHANESULFONATE ND UG/L 1 BLANK-1 LANCAS N-NITROSO-DI-N-PROPYLAMINE ND UG/L 1 BLANK-1 LANCAS N-NITROSODI-N-BUTYLAMINE ND UGIL 2 BLANK-1 LANCAS N-NITROSODIETHYLAMINE ND UG/L 2 BLANK-1 LANCAS N-NITROSODIMETHYLAMINE ND UG/L 2 BLANK-1 LANCAS DEQ-CFW 00025581 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 (Batch continued from previous page) Analyte/Parameter Method Blank: N-NITROSODIPHENYLAMINE N-NITROSOMETHYLETHYLAMINE N-NITROSOMORPHOLINE N-NITROSOPIPERIDINE N-NITROSOPYRROLIDINE NAPHTHALENE NITROBENZENE 0,0,0-TRIETHYLPHOSPHOROTHIOATE 0-TOLUIDINE P-DIMETHYLAMINOAZOBENZENE PENTACHLOROBENZENE PENTACHLORONITROBENZENE PENTACHLOROPHENOL PHENACETIN PHENANTHRENE PHENOL PRONAMIDE PYRENE PYRIDINE SAFROLE TETRAETHYLDITHIOPYROPHOSPHATE THIONAZIN Comments - January 9, 2003 Page 12 Result Unit MDL RPR RPD Lab Sample ID NO UG/L 2 BLANK-1 LANCAS NO UG/L 2 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS NO UG/L 2 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS ND UG/L 3 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS NO UG/L 2 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS ND UG/L 1 BLANK-1 LANCAS ND UG/L 2 BLANK-1 LANCAS 8270C (1,4-PHENYLENEDIAMINE): The laboratory control spike and spike duplicate recoveries were outside control Limits due to the problematic nature of the compound. 8270C: The matrix spike and spike duplicate were not performed due to insufficient sample. The Laboratory control sample and control sample duplicate were analyzed to measure accuracy and precision at the batch Level. 8270C (METHAPYRILENE): The Laboratory control spike and spike duplicate recoveries were outside control Limits. Since the windows are advisory, no further action was taken. 8270C (1-NAPHTHYLAMINE): The RPD between Laboratory control spike/control spike duplicate samples was outside control limits. 8270C (2-NAPHTHYLAMINE): The RPD between Laboratory control spike/control spike duplicate samples was outside control Limits. 8270C (0-TOLUIDINE): The RPD between laboratory control spike/control spike duplicate samples was outside control limits. Batch Identifier Method Number: 8270C Prep Method: 3510C Pre -prep: Batch Start Date: 10DECO2 Instrument: 067560 Batch Number: 4 The following field samples are included in this batch: Date QC Sample Name Sampled Lab Sample ID Level FAY-G-NAF-2-DUP 05DECO2 3956311-1 LANCAS QC FAY-G-NAF1 06DECO2 3956307-1 LANCAS QC FAY-G-NAF2 05DECO2 3956309-1 LANCAS QC FAY-G-NAF3 05DECO2 3956315-1 LANCAS QC Analyte Parameter Lab Control Spike: 1,2,4,5-TETTACHLOROBENZENE 1,2,4-TRICHLOROBENZENE 1,3,5-TRINITROBENZENE 1,3-DINITROBENZENE 1,4-DIOXANE 1,4-NAPHTHOQUINONE 1,4-PHENYLENEDIAMINE 1-NAPHTHYLAMINE 2,3,4,6-TETRACHLOROPHENOL 2,4,5-TRICHLOROPHENOL 2,4,6-TRICHLOROPHENOL 2,4-DICHLOROPHENOL 2,4-DIMETHYLPHENOL Result Unit MDL RPR RPD Lab Sample ID 79 LCS-1 LANCAS 71 LCS-1 LANCAS 74 LCS-1 LANCAS 91 LCS-1 LANCAS 52 LCS-1 LANCAS 96 LCS-1 LANCAS 0 LCS-1 LANCAS 37 LCS-1 LANCAS 83 LCS-1 LANCAS 88 LCS-1 LANCAS 86 LCS-1 LANCAS 86 LCS-1 LANCAS 88 LCS-1 LANCAS DEQ-CFW 00025582 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SWML16 GW-2002 Page 13 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: 2,4-DINITROPHENOL 92 LCS-1 LANCAS 2,4-DINITROTOLUENE 94 LCS-1 LANCAS 2,6-DICHLOROPHENOL 78 LCS-1 LANCAS 2,6-DINITROTOLUENE 86 LCS-1 LANCAS 2-ACETYLAMINOFLUORENE 74 LCS-1 LANCAS 2-CHLORONAPHTHALENE 81 LCS-1 LANCAS 2-CHLOROPHENOL 82 LCS-1 LANCAS 2-METHYLNAPHTHALENE 77 LCS-1 LANCAS 2-METHYLPHENOL 78 LCS-1 LANCAS 2-NAPHTHYLAMINE 43 LCS-1 LANCAS 2-NITROANILINE 91 LCS-1 LANCAS 2-NITROPHENOL 90 LCS-1 LANCAS 2-PICOLINE 74 LCS-1 LANCAS 3,3--DICHLOROBENZIDINE 76 LCS-1 LANCAS 3,31-DIMETHYLBENZIDINE 47 LCS-1 LANCAS 3-METHYLCHOLANTHRENE 77 LCS-1 LANCAS 3-NITROANILINE 77 LCS-1 LANCAS 4,6-DINITRO-2-METHYLPHENOL 98 LCS-1 LANCAS 4-AMINOBIPHENYL 32 LCS-1 LANCAS 4-BROMOPHENYL-PHENYLETHER 89 LCS-1 LANCAS 4-CHLORO-3-METHYLPHENOL 96 LCS-1 LANCAS 4-CHLOROANILINE 63 LCS-1 LANCAS 4-CHLOROPHENYL-PHENYLETHER 86 LCS-1 LANCAS 4-METHYLPHENOL 70 LCS-1 LANCAS 4-NITROANILINE 79 LCS-1 LANCAS 4-NITROPHENOL 48 LCS-1 LANCAS 4-NITROQUINOLINE-I-OXIDE 40 LCS-1 LANCAS 5-NITRO-0-TOLUIDINE 53 LCS-1 LANCAS 7,12-DIMETHYLBENZ[A)ANTHRACENE 73 LCS-1 LANCAS A,A-DIMETHYLPHENETHYLAMINE 66 LCS-1 LANCAS ACENAPHTHENE 89 LCS-1 LANCAS ACENAPHTHYLENE 81 LCS-1 LANCAS ACETOPHENONE 78 LCS-1 LANCAS ANILINE 68 LCS-1 LANCAS ANTHRACENE 91 LCS-1 LANCAS ARAMITE 59 LCS-1 LANCAS BENZO(A)ANTHRACENE 89 LCS-1 LANCAS BENZO(A)PYRENE 91 LCS-1 LANCAS BENZO(B)FLUORANTHENE 91 LCS-1 LANCAS BENZO(G,H,I)PERYLENE 90 LCS-1 LANCAS BENZOM FLUORANTHENE 90 LCS-1 LANCAS BENZYL ALCOHOL 71 LCS-1 LANCAS BIS(2-CHLOROETHOXY)METHANE 90 LCS-1 LANCAS BIS(2-CHLOROETHYL)ETHER 83 LCS-1 LANCAS BIS(2-CHLOROISOPROPYL)ETHER 99 LCS-1 LANCAS BIS(2-ETHYLHEXYL)PHTHALATE 85 LCS-1 LANCAS BUTYLBENZYLPHTHALATE 87 LCS-1 LANCAS CHLOROBENZILATE 75 LCS-1 LANCAS CHRYSENE 87 LCS-1 LANCAS DI-N-BUTYLPHTHALATE 88 LCS-1 LANCAS DI-N-OCTYLPHTHALATE 87 LCS-1 LANCAS DIALLATE TRANS/CIS 77 LCS-1 LANCAS DIBENZ(A,H)ANTHRACENE 95 LCS-1 LANCAS DIBENZOFURAN 84 LCS-1 LANCAS DIETHYLPHTHALATE 86 LCS-1 LANCAS DIMETHOATE 44 LCS-1 LANCAS DIMETHYLPHTHALATE 79 LCS-1 LANCAS ETHYL METHANESULFONATE 73 LCS-1 LANCAS FLUORANTHENE 88 LCS-1 LANCAS FLUORENE 83 LCS-1 LANCAS HEXACHLOROBENZENE 91 LCS-1 LANCAS HEXACHLOROBUTADIENE 59 LCS-1 LANCAS HEXACHLOROCYCLOPENTADIENE 47 LCS-1 LANCAS HEXACHLOROETHANE 54 LCS-1 LANCAS HEXACHLOROPROPENE 50 LCS-1 LANCAS INDENO(1,2,3-CD)PYRENE 89 LCS-1 LANCAS ISODRIN 79 LCS-1 LANCAS ISOPHORONE 82 LCS-1 LANCAS ISOSAFROLE 63 LCS-1 LANCAS METHAPYRILENE 18 LCS-1 LANCAS METHYL METHANESULFONATE 45 LCS-1 LANCAS DEQ-CFW 00025583 Corporate Environmental Database Lab Anatysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SWMU6 GW-2002 Page 14 (Batch Continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Lab Control Spike: N-NITROSO-DI-N-PROPYLAMINE 80 LCS-1 LANCAS N-NITROSODI-N-BUTYLAMINE 65 LCS-1 LANCAS N-NITROSODIETHYLAMINE 71 LCS-1 LANCAS N-NITROSODIMETHYLAMINE 57 LCS-1 LANCAS N-NITROSODIPHENYLAMINE 87 LCS-1 LANCAS N-NITROSOMETHYLETHYLAMINE 70 LCS-1 LANCAS N-NITROSOMORPHOLINE 75 LCS-1 LANCAS N-NITROSOPIPERIDINE 75 LCS-1 LANCAS N-NITROSOPYRROLIDINE 72 LCS-1 LANCAS NAPHTHALENE 80 LCS-1 LANCAS NITROBENZENE 84 LCS-1 LANCAS 0,0,0-TRIETHYLPHOSPHOROTHIOATE 67 LCS-1 LANCAS 0-TOLUIDINE 55 LCS-1 LANCAS P-DIMETHYLAMINOAZOBENZENE 65 LCS-1 LANCAS PENTACHLOROBENZENE 71 LCS-1 LANCAS PENTACHLORONITROBENZENE 78 LCS-1 LANCAS PENTACHLOROPHENOL 90 LCS-1 LANCAS PHENACETIN 82 LCS-1 LANCAS PHENANTHRENE 88 LCS-1 LANCAS PHENOL 39 LCS-1 LANCAS PRONAMIDE 75 LCS-1 LANCAS PYRENE 87 LCS-1 LANCAS PYRIDINE 54 LCS-1 LANCAS SAFROLE 68 LCS-1 LANCAS TETRAETHYLDITHIOPYROPHOSPHATE 75 LCS-1 LANCAS THIONAZIN 78 LCS-1 LANCAS Method Blank: 1,2,4,5-TETTACHLOROBENZENE NO UG/L 2 BLANK-1 LANCAS 1,2,4-TRICHLOROBENZENE NO UG/L 1 BLANK-1 LANCAS 1,3,5-TRINITROBENZENE ND UG/L 5 BLANK-1 LANCAS 1,3-DINITROBENZENE ND UG/L 2 BLANK-1 LANCAS 1,4-DIOXANE ND UG/L 1 BLANK-1 LANCAS 1,4-NAPHTHOQUINONE ND UG/L 10 BLANK-1 LANCAS 1,4-PHENYLENEDIAMINE ND UG/L 60 BLANK-1 LANCAS 1-NAPHTHYLAMINE ND UG/L 5 BLANK-1 LANCAS 2,3,4,6-TETRACHLOROPHENOL NO UG/L 2 BLANK-1 LANCAS 2,4,5-TRICHLOROPHENOL ND UG/L 1 BLANK-1 LANCAS 2,4,6-TRICHLOROPHENOL ND UG/L 1 BLANK-1 LANCAS 2,4-DICHLOROPHENOL NO UG/L 1 BLANK-1 LANCAS 2,4-DIMETHYLPHENOL NO UG/L 1 BLANK-1 LANCAS 2,4-DINITROPHENOL NO UG/L 20 BLANK-1 LANCAS 2,4-DINITROTOLUENE NO UG/L 1 BLANK-1 LANCAS 2,6-DICHLOROPHENOL NO UG/L 2 BLANK-1 LANCAS 2,6-DINITROTOLUENE NO UG/L 1 BLANK-1 LANCAS 2-ACETYLAMINOFLUORENE ND UG/L 2 BLANK-1 LANCAS 2-CHLORONAPHTHALENE NO UG/L 1 BLANK-1 LANCAS 2-CHLOROPHENOL ND UG/L 1 BLANK-1 LANCAS 2-METHYLNAPHTHALENE ND UG/L 1 BLANK-1 LANCAS 2-METHYLPHENOL ND UG/L 1 BLANK-1 LANCAS 2-NAPHTHYLAMINE ND UG/L 5 BLANK-1 LANCAS 2-NITROANILINE NO UG/L 1 BLANK-1 LANCAS 2-NITROPHENOL ND UG/L 1 BLANK-1 LANCAS 2-PICOLINE ND UG/L 2 BLANK-1 LANCAS 3,31-DICHLOROBENZIDINE ND UG/L 1 BLANK-1 LANCAS 3,3--DIMETHYLBENZIDINE NO UG/L 5 BLANK-1 LANCAS 3-METHYLCHOLANTHRENE ND UG/L 2 BLANK-1 LANCAS 3-NITROANILINE NO UG/L 1 BLANK-1 LANCAS 4,6-DINITRO-2-METHYLPHENOL NO UG/L 5 BLANK-1 LANCAS 4-AMINOBIPHENYL NO UG/L 2 BLANK-1 LANCAS 4-BROMOPHENYL-PHENYLETHER NO UG/L 1 BLANK-1 LANCAS 4-CHLORO-3-METHYLPHENOL NO UG/L 1 BLANK-1 LANCAS 4-CHLOROANILINE NO UG/L 1 BLANK-1 LANCAS 4-CHLOROPHENYL-PHENYLETHER NO UG/L 1 BLANK-1 LANCAS 4-METHYLPHENOL ND UG/L 2 BLANK-1 LANCAS 4-NITROANILINE ND UG/L 1 BLANK-1 LANCAS 4-NITROPHENOL ND UG/L 10 BLANK-1 LANCAS 4-NITROQUINOLINE-I-OXIDE ND UG/L 20 BLANK-1 LANCAS 5-NITRO-0-TOLUIDINE ND UG/L 3 BLANK-1 LANCAS 7,12-DIMETHYLBENZ[AIANTHRACENE ND UG/L 2 BLANK-1 LANCAS A,A-DIMETHYLPHENETHYLAMINE ND UG/L 1 BLANK-1 LANCAS DEQ-CFW 00025584 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SWMUb GW-2002 Page 15 (Batch continued from previous page) Analyte/Parameter Result Unit MDL RPR RPD Lab Sample ID Method Blank: ACENAPHTHENE ND UG/L 1 BLANK-1 LANCAS ACENAPHTHYLENE ND UG/L 1 BLANK-1 LANCAS ACETOPHENONE NO UG/L 2 BLANK-1 LANCAS ANILINE NO UG/L 1 BLANK-1 LANCAS ANTHRACENE ND UG/L 1 BLANK-1 LANCAS ARAMITE NO UG/L 1 BLANK-1 LANCAS BENZO(A)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS BENZO(A)PYRENE ND UG/L 1 BLANK-1 LANCAS BENZO(B)FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS BENZO(G,H,I)PERYLENE ND UG/L 1 BLANK-1 LANCAS BENZO(K)FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS BENZYL ALCOHOL ND UG/L 5 BLANK-1 LANCAS BIS(2-CHLOROETHOXY)METHANE ND UG/L 1 BLANK-1 LANCAS BIS(2-CHLOROETHYL)ETHER ND UG/L 1 BLANK-1 LANCAS BIS(2-CHLOROISOPROPYL)ETHER ND UG/L 1 BLANK-1 LANCAS BIS(2-ETHYLHEXYL)PHTHALATE NO UG/L 2 BLANK-1 LANCAS BUTYLBENZYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS CHLOROBENZILATE NO UG/L 3 BLANK-1 LANCAS CHRYSENE NO UG/L 1 BLANK-1 LANCAS DI-N-BUTYLPHTHALATE NO UG/L 2 BLANK-1 LANCAS DI-N-OCTYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS DIALLATE TRANS/CIS ND UG/L 1 BLANK-1 LANCAS DIBENZ(A,H)ANTHRACENE ND UG/L 1 BLANK-1 LANCAS DIBENZOFURAN ND UG/L 1 BLANK-1 LANCAS DIETHYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS DIMETHOATE ND UG/L 3 BLANK-1 LANCAS DIMETHYLPHTHALATE ND UG/L 2 BLANK-1 LANCAS ETHYL METHANESULFONATE ND UG/L 2 BLANK-1 LANCAS FLUORANTHENE ND UG/L 1 BLANK-1 LANCAS FLUORENE ND UG/L 1 BLANK-1 LANCAS HEXACHLOROBENZENE ND UG/L 1 BLANK-1 LANCAS HEXACHLOROBUTADIENE ND UG/L 1 BLANK-1 LANCAS HEXACHLOROCYCLOPENTADIENE ND UG/L 5 BLANK-1 LANCAS HEXACHLOROETHANE NO UG/L 1 BLANK-1 LANCAS HEXACHLOROPROPENE NO UG/L 2 BLANK-1 LANCAS INDENO(1,2,3-CD)PYRENE NO UG/L 1 BLANK-1 LANCAS ISODRIN ND UG/L 1 BLANK-1 LANCAS ISOPHORONE ND UG/L 1 BLANK-1 LANCAS ISOSAFROLE NO UG/L 1 BLANK-1 LANCAS METHAPYRILENE ND UG/L 3 BLANK-1 LANCAS METHYL METHANESULFONATE ND UG/L 1 BLANK-1 LANCAS N-NITROSO-DI-N-PROPYLAMINE ND UG/L 1 BLANK-1 LANCAS N-NITROSODI-N-BUTYLAMINE ND UG/L 2 8LANK-1 LANCAS N-NITROSODIETHYLAMINE NO UG/L 2 8LANK-1 LANCAS N-NITROSODIMETHYLAMINE NO UG/L 2 BLANK-1 LANCAS N-NITROSODIPHENYLAMINE ND UG/L 2 BLANK-1 LANCAS N-NITROSOMETHYLETHYLAMINE ND UG/L 2 BLANK-1 LANCAS N-NITROSOMORPHOLINE ND UG/L 2 BLANK-1 LANCAS N-NITROSOPIPERIDINE ND UG/L 2 BLANK-1 LANCAS N-NITROSOPYRROLIDINE ND UGIL 2 BLANK-1 LANCAS NAPHTHALENE NO UG/L 1 BLANK-1 LANCAS NITROBENZENE ND UG/L 1 BLANK-1 LANCAS 0,0,0-TRIETHYLPHOSPHOROTHIOATE NO UG/L 2 BLANK-1 LANCAS 0-TOLUIDINE ND UG/L 1 BLANK-1 LANCAS P-DIMETHYLAMINOAZOBENZENE ND UG/L 2 BLANK-1 LANCAS PENTACHLOROBENZENE ND UG/L 2 BLANK-1 LANCAS PENTACHLORONITROBENZENE ND UG/L 2 BLANK-1 LANCAS PENTACHLOROPHENOL ND UG/L 3 BLANK-1 LANCAS PHENACETIN ND UG/L 2 BLANK-1 LANCAS PHENANTHRENE ND UG/L 1 BLANK-1 LANCAS PHENOL ND UG/L 1 BLANK-1 LANCAS PRONAMIDE ND UG/L 1 BLANK-1 LANCAS PYRENE ND UG/L 1 BLANK-1 LANCAS PYRIDINE ND UG/L 2 BLANK-1 LANCAS SAFROLE ND UG/L 2 BLANK-1 LANCAS TETRAETHYLDITHIOPYROPHOSPHATE ND UG/L 1 BLANK-1 LANCAS THIONAZIN ND UG/L 2 BLANK-1 LANCAS DEQ-CFW 00025585 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SWMU6 GW-2002 Page 16 (Batch continued from previous page) Analvte/Parameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike: 1,2,4,5-TETRACHLOROBENZENE 75 3956309-1 LANCAS 1,2,4-TRICHLOROBENZENE 73 3956309-1 LANCAS 1,3,5-TRINITROBENZENE 25 3956309-1 LANCAS 1,3-DINITROBENZENE 87 3956309-1 LANCAS 1,4-DIOXANE 54 3956309-1 LANCAS 1,4-NAPHTHOQUINONE 0 3956309-1 LANCAS 1,4-PHENYLENEDIAMINE 0 3956309-1 LANCAS 1-NAPHTHYLAMINE 32 3956309-1 LANCAS 2,3,4,6-TETRACHLOROPHENOL 83 3956309-1 LANCAS 2,4,5-TRICHLOROPHENOL 83 3956309-1 LANCAS 2,4,6-TRICHLOROPHENOL 81 3956309-1 LANCAS 2,4-DICHLOROPHENOL 81 3956309-1 LANCAS 2,4-DIMETHYLPHENOL 79 3956309-1 LANCAS 2,4-DINITROPHENOL 69 3956309-1 LANCAS 2,4-DINITROTOLUENE 86 3956309-1 LANCAS 2,6-DICHLOROPHENOL 86 3956309-1 LANCAS 2,6-DINITROTOLUENE 82 3956309-1 LANCAS 2-ACETYLAMINOFLUORENE 84 3956309-1 LANCAS 2-CHLORONAPHTHALENE 76 3956309-1 LANCAS 2-CHLOROPHENOL 77 3956309-1 LANCAS 2-METHYLNAPHTHALENE 74 3956309-1 LANCAS 2-METHYLPHENOL 70 3956309-1 LANCAS 2-NAPHTHYLAMINE 6 3956309-1 LANCAS 2-NITROANILINE 89 3956309-1 LANCAS 2-NITROPHENOL 83 3956309-1 LANCAS 2-PICOLINE 75 3956309-1 LANCAS 3,3--DICHLOROBENZIDINE 61 3956309-1 LANCAS 3,31-DIMETHYLBENZIDINE 25 3956309-1 LANCAS 3-METHYLCHOLANTHRENE 87 3956309-1 LANCAS 3-NITROANILINE 73 3956309-1 LANCAS 4,6-DINITRO-2-METHYLPHENOL 82 3956309-1 LANCAS 4-AMINOBIPHENYL 38 3956309-1 LANCAS 4-BROMOPHENYL-PHENYLETHER 82 3956309-1 LANCAS 4-CHLORO-3-METHYLPHENOL 87 3956309-1 LANCAS 4-CHLOROANILINE 9 3956309-1 LANCAS 4-CHLOROPHENYL-PHENYLETHER 77 3956309-1 LANCAS 4-METHYLPHENOL 63 3956309-1 LANCAS 4-NITROANILINE 74 3956309-1 LANCAS 4-NITROPHENOL 48 3956309-1 LANCAS 4-NITROQUINOLINE-I-OXIDE 0 3956309-1 LANCAS 5-NITRO-0-TOLUIDINE 61 3956309-1 LANCAS 7,12-DIMETHYLBENZEA)ANTHRACENE 73 3956309-1 LANCAS A,A-DIMETHYLPHENETHYLAMINE 85 3956309-1 LANCAS ACENAPHTHENE 82 3956309-1 LANCAS ACENAPHTHYLENE 77 3956309-1 LANCAS ACETOPHENONE 79 3956309-1 LANCAS ANILINE 43 3956309-1 LANCAS ANTHRACENE 81 3956309-1 LANCAS ARAMITE 26 3956309-1 LANCAS BENZO(A)ANTHRACENE 83 3956309-1 LANCAS BENZO(A)PYRENE 85 3956309-1 LANCAS BENZO(B)FLUORANTHENE 84 3956309-1 LANCAS BENZO(G,H,I)PERYLENE 82 3956309-1 LANCAS BENZO(K)FLUORANTHENE 84 3956309-1 LANCAS BENZYL ALCOHOL 68 3956309-1 LANCAS BIS(2-CHLOROETHOXY)METHANE 92 3956309-1 LANCAS BIS(2-CHLOROETHYL)ETHER 97 3956309-1 LANCAS BIS(2-CHLOROISOPROPYL)ETHER 101 3956309-1 LANCAS BIS(2-ETHYLHEXYL)PHTHALATE 79 3956309-1 LANCAS BUTYLBENZYLPHTHALATE 65 3956309-1 LANCAS CHLOROBENZILATE 37 3956309-1 LANCAS CHRYSENE 81 3956309-1 LANCAS DI-N-BUTYLPHTHALATE 72 3956309-1 LANCAS DI-N-OCTYLPHTHALATE 77 3956309-1 LANCAS DIALLATE TRANS/CIS 86 3956309-1 LANCAS DIBENZ(A,H)ANTHRACENE 88 3956309-1 LANCAS DIBENZOFURAN 76 3956309-1 LANCAS DIETHYLPHTHALATE 54 3956309-1 LANCAS DIMETHOATE 5 3956309-1 LANCAS DIMETHYLPHTHALATE 18 3956309-1 LANCAS ETHYL METHANESULFONATE 88 3956309-1 LANCAS DEQ-CFW 00025586 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE Project Name: SWMU6 GW-2002 (Batch continued from previous page) January 9, 2003 Page 17 AnaLytelParameter Result Unit MDL RPR RPD Lab SampLe ID Matrix Spike: FLUORANTHENE 78 3956309-1 LANCAS FLUORENE 76 3956309-1 LANCAS HEXACHLOROBENZENE 82 3956309-1 LANCAS HEXACHLOROBUTADIENE 68 3956309-1 LANCAS HEXACHLOROCYCLOPENTADIENE 42 3956309-1 LANCAS HEXACHLOROETHANE 65 3956309-1 LANCAS HEXACHLOROPROPENE 75 3956309-1 LANCAS INDENO(1,2,3-CD)PYRENE 81 3956309-1 LANCAS ISODRIN 55 3956309-1 LANCAS ISOPHORONE 83 3956309-1 LANCAS ISOSAFROLE 77 3956309-1 LANCAS METHAPYRILENE 23 3956309-1 LANCAS METHYL METHANESULFONATE 53 3956309-1 LANCAS N-NITROSO-DI-N-PROPYLAMINE 82 3956309-1 LANCAS N-NITROSODI-N-BUTYLAMINE 71 3956309-1 LANCAS N-NITROSODIETHYLAMINE 89 3956309-1 LANCAS N-NITROSODIMETHYLAMINE 59 3956309-1 LANCAS N-NITROSODIPHENYLAMINE 79 3956309-1 LANCAS N-NITROSOMETHYLETHYLAMINE 82 3956309-1 LANCAS N-NITROSOMORPHOLINE 83 3956309-1 LANCAS N-NITROSOPIPERIDINE 88 3956309-1 LANCAS N-NITROSOPYRROLIDINE 80 3956309-1 LANCAS NAPHTHALENE 78 3956309-1 LANCAS NITROBENZENE 83 3956309-1 LANCAS 0,0,0-TRIETHYLPHOSPHOROTHIOATE 84 3956309-1 LANCAS 0-TOLUIDINE 10 3956309-1 LANCAS P-DIMETHYLAMINOAZOBENZENE 47 3956309-1 LANCAS PENTACHLOROBENZENE 82 3956309-1 LANCAS PENTACHLORONITROBENZENE 86 3956309-1 LANCAS PENTACHLOROPHENOL 70 3956309-1 LANCAS PHENACETIN 88 3956309-1 LANCAS PHENANTHRENE 81 3956309-1 LANCAS PHENOL 38 3956309-1 LANCAS PRONAMIDE 84 3956309-1 LANCAS PYRENE 80 3956309-1 LANCAS PYRIDINE 56 3956309-1 LANCAS SAFROLE 82 3956309-1 LANCAS TETRAETHYLDITHIOPYROPHOSPHATE 76 3956309-1 LANCAS THIONAZIN 80 3956309-1 LANCAS Matrix Spike Duplicate: 1,2,4,5-TETRACHLOROSENZENE 83 9 3956309-1 LANCAS 1,2,4-TRICHLOROBENZENE 81 11 3956309-1 LANCAS 1,3,5-TRINITROBENZENE 26 2 3956309-1 LANCAS 1,3-DINITROBENZENE 88 2 3956309-1 LANCAS 1,4-DIOXANE 50 7 3956309-1 LANCAS 1,4-NAPHTHOQUINONE 0 0 3956309-1 LANCAS 1,4-PHENYLENEDIAMINE 0 0 3956309-1 LANCAS 1-NAPHTHYLAMINE 32 1 3956309-1 LANCAS 2,3,4,6-TENRACHLOROPHENOL 74 12 3956309-1 LANCAS 2,4,5-TRICHLOROPHENOL 78 6 3956309-1 LANCAS 2,4,6-TRICHLOROPHENOL 73 10 3956309-1 LANCAS 2,4-DICHLOROPHENOL 77 4 3956309-1 LANCAS 2,4-DIMETHYLPHENOL 75 4 3956309-1 LANCAS 2,4-DINITRQPHENOL 55 22 3956309-1 LANCAS 2,4-DINITROTOLUENE 92 7 3956309-1 LANCAS 2,6-DICHLOROPHENOL 81 6 3956309-1 LANCAS 2,6-DINITROTOLUENE 87 6 3956309-1 LANCAS 2-ACETYLAMINOFLUORENE 84 0 3956309-1 LANCAS 2-CHLORONAPHTHALENE 82 9 3956309-1 LANCAS 2-CHLOROPHENOL 71 8 3956309-1 LANCAS 2-METHYLNAPHTHALENE 84 12 3956309-1 LANCAS 2-METHYLPHENOL 66 6 3956309-1 LANCAS 2-NAPHTHYLAMINE 6 1 3956309-1 LANCAS 2-NITROANILINE 89 0 3956309-1 LANCAS 2-NITROPHENOL 78 7 3956309-1 LANCAS 2-PICOLINE 72 4 3956309-1 LANCAS 3,31-DICHLOROBENZIDINE 65 6 3956309-1 LANCAS 3,31-DIMETHYLBENZIDINE 29 15 3956309-1 LANCAS 3-METHYLCHOLANTHRENE 90 4 3956309-1 LANCAS 3-NITROANILINE 71 3 3956309-1 LANCAS DEQ-CFW 00025587 Corporate Environmental Database Lab Analysis QAQC Report Location: FAYETTEVILLE January 9, 2003 Project Name: SWMU6 GW-2002 Page 18 (Batch continued from previous page) AnalytelParameter Result Unit MDL RPR RPD Lab Sample ID Matrix Spike Duplicate: 4,6-DINITRO-2-METHYLPHENOL 74 10 3956309-1 LANCAS 4-AMINOBIPHENYL 36 4 3956309-1 LANCAS 4-BROMOPHENYL-PHENYLETHER 90 10 3956309-1 LANCAS 4-CHLORO-3-METHYLPHENOL 84 4 3956309-1 LANCAS 4-CHLOROANILINE 11 14 3956309-1 LANCAS 4-CHLOROPHENYL-PHENYLETHER 83 7 3956309-1 LANCAS 4-METHYLPHENOL 59 8 3956309-1 LANCAS 4-NITROANILINE 71 4 3956309-1 LANCAS 4-NITROPHENOL 47 3 3956309-1 LANCAS 4-NITROQUINOLINE-I-OXIDE 0 0 3956309-1 LANCAS 5-NITRO-0-TOLUIDINE 56 9 3956309-1 LANCAS 7,12-DIMETHYLBENZEA]ANTHRACENE 78 6 3956309-1 LANCAS A,A-DIMETHYLPHENETHYLAMINE 73 15 3956309-1 LANCAS ACENAPHTHENE 89 8 3956309-1 LANCAS ACENAPHTHYLENE 83 7 3956309-1 LANCAS ACETOPHENONE 83 5 3956309-1 LANCAS ANILINE 39 12 3956309-1 LANCAS ANTHRACENE 91 12 3956309-1 LANCAS ARAMITE 36 34 3956309-1 LANCAS BENZO(A)ANTHRACENE 88 5 3956309-1 LANCAS BENZO(A)PYRENE 90 5 3956309-1 LANCAS BENZO(B)FLUORANTHENE 89 5 3956309-1 LANCAS BENZO(G,H,I)PERYLENE 91 10 3956309-1 LANCAS BENZO(K)FLUORANTHENE 91 8 3956309-1 LANCAS BENZYL ALCOHOL 67 2 3956309-1 LANCAS BIS(2-CHLOROETHOXY)METHANE 91 1 3956309-1 LANCAS BIS(2-CHLOROETHYL)ETHER 95 2 3956309-1 LANCAS BIS(2-CHLOROISOPROPYL)ETHER 101 0 3956309-1 LANCAS BIS(2-ETHYLHEXYL)PHTHALATE 82 4 3956309-1 LANCAS BUTYLBENZYLPHTHALATE 72 10 3956309-1 LANCAS CHLOROBENZILATE 51 30 3956309-1 LANCAS CHRYSENE 87 7 3956309-1 LANCAS DI-N-BUTYLPHTHALATE 80 11 3956309-1 LANCAS DI-N-OCTYLPHTHALATE 83 7 3956309-1 LANCAS DIALLATE TRANS/CIS 88 2 3956309-1 LANCAS DIBENZ(A,H)ANTHRACENE 94 7 3956309-1 LANCAS DIBENZOFURAN 85 10 3956309-1 LANCAS DIETHYLPHTHALATE 58 8 3956309-1 LANCAS DIMETHOATE 5 0 3956309-1 LANCAS DIMETHYLPHTHALATE 19 4 3956309-1 LANCAS ETHYL METHANESULFONATE 85 3 3956309-1 LANCAS FLUORANTHENE 85 9 3956309-1 LANCAS FLUORENE 80 5 3956309-1 LANCAS HEXACHLOROBENZENE 89 9 3956309-1 LANCAS HEXACHLOROBUTADIENE 75 10 3956309-1 LANCAS HEXACHLOROCYCLOPENTADIENE 45 6 3956309-1 LANCAS HEXACHLOROETHANE 68 3 3956309-1 LANCAS HEXACHLOROPROPENE 79 6 3956309-1 LANCAS INDENO(1,2,3-CD)PYRENE 88 9 3956309-1 LANCAS ISODRIN 62 11 3956309-1 LANCAS ISOPHORONE 82 1 3956309-1 LANCAS ISOSAFROLE 79 4 3956309-1 LANCAS METHAPYRILENE 23 1 3956309-1 LANCAS METHYL METHANESULFONATE 52 2 3956309-1 LANCAS N-NITROSO-DI-N-PROPYLAMINE 83 1 3956309-1 LANCAS N-NITROSODI-N-BUTYLAMINE 73 3 3956309-1 LANCAS N-NITROSODIETHYLAMINE 86 4 3956309-1 LANCAS N-NITROSODIMETHYLAMINE 54 10 3956309-1 LANCAS N-NITROSODIPHENYLAMINE 87 9 3956309-1 LANCAS N-NITROSOMETHYLETHYLAMINE 79 4 3956309-1 LANCAS N-NITROSOMORPHOLINE 83 0 3956309-1 LANCAS N-NITROSOPIPERIDINE 87 0 3956309-1 LANCAS N-NITROSOPYRROLIDINE 80 0 3956309-1 LANCAS NAPHTHALENE 83 7 3956309-1 LANCAS NITROBENZENE 86 4 3956309-1 LANCAS 0,0,0-TRIETHYLPHOSPHOROTHIOATE 85 1 3956309-1 LANCAS O-TOLUIDINE 13 29 3956309-1 LANCAS P-DIMETHYLAMINOAZOBENZENE 56 17 3956309-1 LANCAS PENTACHLOROBENZENE 84 3 3956309-1 LANCAS PENTACHLORONITROBENZENE 89 4 3956309-1 LANCAS PENTACHLOROPHENOL 56 22 3956309-1 LANCAS DEQ-CFW 00025588 Corporate Environmental Database Lab Analysis QAQC Report Location: omonsxzus January 9, 2003 Project Name: mwmu6 ow-2002 pome 19 (Batch continued from previous page) AnaLytelParameter Result� Unit MDL RPR RPD Lab Sample ID Matrix Spike Duplicate: pxsNxnsTIw 87 Z 3956309-1 u^wn4o p*EwAmTxxsms 80 8 3956309-1 LxwCAn posNoL 35 7 3958309'1 Lxwcxo pnowmwIos 88 2 3956309-1 Lxwcxn pYnEws 87 9 3956309-1 LAwcxm pYn/oIms 54 5 3956309-1 Lxwx*m SxpnnLs 90 7 3956309'1 Lxwuwn rsTxxcrormzTxIopYnop000pnaTe BY 8 3958309'1 L*woxs ToIow*zIw 83 3 3956309'1 Lwwmws Comments: 8270c (1,4-posmYLswsoImwIws): The Laboratory control spike recovery was outside control limits. The associated oumpi=o were reoxtrectod and reanalyzed outside of hold time and comparable results were vbmprved' Trial one was reported. ozron (A,A'ozMsTxYLpxswE7oYLnmzws): The Laboratory control spike recovery was outside control iimitu- The associated samples were rrpxtrocted and reanalyzed outside of hold time and comparable results were observed. Trial one was reported. 8270c (AoAm/7s): The Laboratory control spike recovery was outside control limits. The associated samples were reextructed and reanalyzed outside of hold time and comparable sample ,eovito were obuerved- Trial one was reported. 8270c (IonuwpnoLs): The laboratory control spike recovery was outside control limits. The associated samples were rcaxtroct*d and reanalyzed outside of hold time and comparable results were ubtained' Trial one was reported' 8270c (MsTxxpYnILEws): The laboratory control spike recovery was outside control Limits. The associated samples were reextroctmd and reanalyzed outside of hold time and comparable results were ubtainrd' Trial one was reportaJ- 827uo (w'wIrnosooIs7xyLxmrws): The laboratory control spike recovery was outside control iimits' The associated samples were reevtronted and reanalyzed outside of hold time and comparable results were observed. Trial one was reported. 8270c (w'mI7n000msTxYaroYLxnIws): The Laboratory control spike recovery was outside control limits. The ouunuiuted samples were rmextroctcd and reanalyzed outside of hold time and comparable reouLtu were vbmerved-Triui one was reported. 8270c (w'wz7noVopIpsxIozwe): The |uhvrutnry control spike recovery was outside control Limits. The associated samples were rpextracted and reanalyzed outside of hniu time and comparable results were mbmerved' Trial one was reported. 8270n (m,o,o'mzsTmYLp*onpxoxnr*IowTE): The laboratory control spike recovery was outside control iimito' The associated numpiou were roe^tracted and reanalyzed outside of hold time and comparable results were observed. rrroi one was reported. 8270n (puuwmnIos): The laboratory control spike recovery was outside control Limits. The associated samples were reextmcted and reanalyzed outside of hold time and comparable results were observed. Trial one was reported' 8270u (oxpnoLs): The Laboratory control spike recovery was outside control Limits. The associated uompiom were reevtrmoted and reanalyzed outside of xvid time and comparable results were vbtoineu' Trial one was reported. 8270c (1,4'wapmonouIwowE): The matrix spike and spike duplicate recoveries were outside control iimita' mt control spike recovery met acceptance criteria. 8270C (1,4PxswYLcwce/xn;wE): The matrix spike and spike duplicate recoveries were outside control Limits. 8270c (4-w/rw000IwoLIws-1-ox;us): The matrix spike and spike duplicate recoveries were outside control Limits. Lob control spike recovery me, acceptance criteria. 8270c (Ae*mIrc): The matrix spike and spike duplicate recoveries were outside control Limits. 8270c (IaommIm): The matrix spike and spike duplicate recoveries were outside control Limits. Lab control spike recovery met acceptance criteria. 8270c (mc7xxpvnzLswE): The matrix spike and spike duplicate recoveries were outside control limits. 8270c (0-7oLuzozwe): The matrix spike and spike duplicate recoveries were outside control Limits. Lab control spike recovery met acceptance criteria. 8270n (2^3 4,8'TsTnAcxLonoPxswoL): The matrix spike duplicate recovery was outside control Limits. Lob control spike recovery met acceptance criteria. 8270C (wnAmIrs): The opo between matrix spike/matrix spike duplicate samples was outside control Limits. [Mo. %J%j f a.J Lanual3ter wratories w d 5 � — ---------- - ----- -- - -- - --- --- ---- - -- — — — — --ill' — i 71- 10-2- 2425 New Holland, 3 Box 12425. Lancaster, PA 17605-2425 kt� "ProiectNumber ----- - - - - --------- i 'DuPont Fayetteville 4-362-6633 rIlTelephone Federal Express Facility Name Number Transporter Name �Route 87 South Fayettevillie NC 28302 Faciffty Address �ransporter Address - - ----- — -------- - - - - ------- ------ --- --- - -- - ---- - --------- ----- -- - -- 'Express Saver Method of Shipping MU6 GW-2002 Process Producing Sample Special Shipping Instructions et t et ano H2ndling Other EmploII ainple Oyees(s) �U��DesOpfion !FAY-G-NAF4 FAY-G-NAF4 F 'Bottles Relinquished by X IDatefTime fl6do, 0%6, i'tBottles Received -by _Alzrzr�_ I —Destinatin Condkion of Sample s U on jtal at FIWo P Dateffime) �1_4? - ---- tsvo MEN& 17M MIKE 'Pateffhme 1, Received by �j ����Temp. of Sarrples on Antval �Relingulshe by A I M1.1- V�11 LI,7 ("fa/ 0 2�a a DEQ-CFW-00025590 01 2425 New . . i ;r t r .: r ii. '�. - i4' . .. � -. Express Facility hone Number � Transporter Name —r-Tolopb9nek Nu . oute 87 South Fayettevillie NC 28302 AddressFaclifty ..Address - - ath -------- _ —;Express Saver irity-Swervior Method of Shipping__ « I0 Process Sample Special ShippingInstructions 6+ • f --------------- f KOM a, ftlesReli`': ` i.a�: / . - I :. 1 : ' • �- r r� ftil.�aG/ r r r . r s • r e on r IW► ` r , `. � 'Received J [Relinquished by SYMEWWWWR M,-4A DEQ—CFW 00025591 f- eB5-71 NO. TjvQU4 Lancaster boratories 1172563 70 5-504103 00 2425 New Holland !0 Box 12425. Lancaster, PA 17605-2425 43 + 3q 5 5q 4 , I Order I D [ProlerA NumhtE-_ DuPont F2yett8VIIIe Federal Express Facility Name Trans Telephone Number iRoute 87 South Fayettevillie NC 28302 FacilityAddress - -- — ------ - — -------- ------ - -------- — - - ----- — ----------- - - - - - -------- — - - - ------ Address----- - - ---- — ------- rvan Heath 9 M —�M "IJ\ I. �Lok0o-,\ - ---- ---- --- lateMme I UVO t 60 v #I - 11, 00 �0 C*-;7 I Instructions m M of SamDles on ArrWal DEQ-CFW-00025592 IwAtc 1741#11- A-- Cl- -<-n-I No. 'DUO.'V -7035�504105 JO IRM! Mof a 704-362-6633 ----- - - - - ------------ -- ------- - 1 - -- --- --- Federal Express 1 Telephone Number —Transporter Name MT 17 z 9 -1 z Facility Addreea ��.aperter Address =Heath ,Express Saver mJ1 Method of Shippjn« �WMU6 GW-2002 Process Producina Samde Special Shipping Instructions ----- anol; 8270 APPfX; Cl-, F- (300.0) ,Other Emplpless(s) Handling I iSample ; 9 esodplion - -- -------- ---- "Bottles Relinquished by �q�teime - ---- -- --- — ----- tondgkon 0 Samnles UponarrW at final Destination DateMme 'D-ateMme -Relin by . ....... ULM= W Temp. of Simples on k w - 1 7 CE; fielinquisneci py_.. ---- - - -- - ----- - - - ------ -------- - - ---- - I �AIPM g,/ 61 V d DEQ-CFW-00025593 --ancaster ' Ivratodw 2425 Rew Holland 0 Box 12425. Lancaster, PA 17605-243,& DuPont F2yetteville Facility Name A Route 87 South Fayettevillie NC 28302 Facility Address ::Bryan Heath FaRilfty sunervigr SWMU6 GW-2b02 W�h, 43 O=— FA of Samples on V DEQ-CFW-00025594 DuPont F2yetteVille Facility Name iRoute 87 South Fayettevillie NC 28302 Facilfty Address 3 lFederal Express rya e� 0,A A crAcn = Acrolein/Acrylonitrile &-it' Ir I �m V DEQ-CFW-00025595 P W�� Lancaster , -coratories 1 - ------- '0 (06 V -1E 7-1,�, Lu*v#,�NM, �P7035-50410311 2425 New Hollan; Box 12425. Lancaster, PA 1 *5-2Q5 -5&30-�- _3 r4 Malp roject Wri ber DuPont Fayetteville ;Fe cieral Express ! Facilfty Name -- 1 1 1 51-Transporter Name — — ---- — ------ TefthQna Nttmber. ----------- Route 87 South Fayettevillie NC 2 63 02 Fadifty Address ransporter Address Bryan Heath �jExpress Saver aciW-SwaMo-r Method of Shipp SWMU6 GW-2002 Process Producing Sample - ------- Special ShIppina instructions Employee(s) Sampling Other Employees(s) Handling ------ ---- - -- ----- I--le lDesc6pflon 44 MIME Mil IMIME1111 MMMM M" MUMMEWM4. MIUMX= rolirAIAMWMW-7�1 iDatefrime /&100 liconddion Of-SaMdes Upon ainival _at FW,,(Destination VMMVI�W*Aeceived emR. of Sampleson ArTtval 'C i R6141shedby DEQ-CFW-00025596 Lancaster I -horatorles i INO.. OOOZZ) - 35-504103. TO 2425 New Holland 0 Box 12425. Lancaster, PA 17605-24�R IDuPont Fayiefteviii-d lFacifAyName rRoute 87 South Fayettevillle NC 28302 Familfty Addres3 ,Bryan Heath i Facifity Suvervior II SWMU6 GW-2002 Process Produsho Savi -iJe IIUAE�= -362.6633 1 �phone Number MetEth — Methanol; wiam! wafm�� MEAM MfflffEM elf 2-1 /* 0 e :') E DEQ-CFW-00025597 Lancamer, noraicones MA --- - - ----- - - - - - --------- - - -- ------ - -- 11035-504103- jo !Project 2425 New Holland 0 Box 12425. Lancaster, PA 17605-2425 0 Number IDuPont Fayetteville i,704-362-663s -MIM OR - Facility Name i� Telephone Num TelepYone Numb -or ; IR oute 87 South FajeftWilfk �N 3(if i Facility Address —6ansporter LK Address - — - — — Bryan Heath - - — - — --- — — ----- - - — ------- — - - - - ---------- - --- -------- - --- xpress Saver facilfty-S-uveMor ------ - — - - ------ — - -------- !'Method of Ship ing -p ----------- - SWMU6 GW-2002 Process Producing3ample - ------ - - Speqlal Shipping Instructions Emploffe(s) plina ----- - --- ------- --- -- - -- - ------------ — ------- — ------ -Amm Ernpla"es(c) Handling _Other IIp ple DescAplion 1. �Mmm��Mmmmmmmm �V%r O,�, DateMme — ------- - - — ---- jlm� min _R ellnqWshedW Ar rernp.ofsarnpiesqn rivai MAMA M (fC� ?0 7 y /.V 14 e" DEQ-CFW-00025598 Lancaster ' -boratorles 2425 New Holland 10 Box 12425, Lancaster, PA 17605-2425 �b 3o S-- -:7 A DuPont Fayetteviiie Federal Express 11 Facility Name Tq[q �hqne Number ransporter—Nam e- Route 87 South Fayettevilile NC 28302 Facility Address Bryan Heath 'Facift gupgAor SWMU6 M. FROM N NO. vvo4rj 135-504103 �>— 0 of Samples on Arr"I. —j—,-C DEQ-CFW-00025599 w&A!jL*IAUAl LanGa3ler loratorlle5 q3 I —1172563 -- !I 13-5-5-041-0-3-- )-0--- 2425 New Holland I D Box 12425. Lancaster, PA 17605-2425 , iOrrt--cbQ PrQlect Number I[Du Pont. Fayetteville - - - -------- 764.362 6(423 Federal S�press I Facility Name Tole hone NImber !Transporter p one No Name NCO 1.7-173K !I IM i; RouteVSouth FayettevillleNC 28302 Facility Address p �ransorter Address iBryan Heath =[Express Saver facility SUDervior -- Method Of Shippina --------- - -- - — ------- - - ---------- - - --------- ---- - ------ GW-2002 - ------- -- ----- - - --------------------- --------- ----- - --- --------- ---- -------- -- ----- - ---- -------------- --------- ---- - IPWIVIL16 F rocess Producinu Sample al ShIppigg struv lons 60 APPIX - ---- ------- -- - ---- - - ----- ---- Employee(s) Samolino 'j7W MJ — 'Other Emplqyees(s) Handling ------- mum M� 'Condition of Samples Upon arrival at Final Destination. WIM2, -b Received ------ ---------- - ---- ------iu y �Relinquishecl----- -c�dji Ic lRelingulsqed,g" Nib III OWN, SIMI CO '70 /-cc, J, DEQ-CFW-00025600 I'll 7 2 6 -6 -3 m &ITEWIT-111 :,Order ID— Talanhona Nu ber Transporter Name Facility Address ransporter Address Process Producing Sample al SW �ping Instructions �mu OEQ-CFVV_00025601 RMKM. 7035-504103- TO-1 2425 New Holland c) 3 Box 12425. Lancaster, PA 17605-2425 _he Proiec-t-Mun _.L_ jDuPont Payetteviiie 704-362-6633 !F6deral Facilfty Name Transporter Name Route 81-South Fayettevilile NC 28302 4ranspo Facilfty Address — - - — - ------------ — - ----------------- - - - - - ---------------- - ----- ---------- - ----------- dd rter Aress Bryan Heath !EXpress Saver Supgndor-- - ------------- - - ---- - ----- --- -- - ------- -- - - - ------- ---- - - -- --------- - - -- - - -------- - --- -- - - ----------- Method of Shwing ,SWMU6 GW-2002 Process Producing Sample Speelal Shipping Instructions - ----- ------ --------------- -------- — --- --- Ac cn Acrolein/Acrylonitrile Employee s Sampling Other Employees(c) Handling W/M MOM, %fAjDztteM 0 - - — ---- -♦----- ' Re------ celved by �PateMrne A�Ished ple on "I Temp. of,§am 9 Ic i,Re!�gu'lshed q Oy LiL Uc On "(--/0 fi s- DEQ-CFW-00025602 I MI..,M LdIIUd5ICr• i2425. 563 7035-5041 O�-- 10 2425 New Holland Box Lancaster, PA Aect Number �DuPont Fayetteville 6 facirgyName— ---------- — - ------ Route 87 South Fayettevillle NC 28302 --- -- - -- -- - - -- --- - - - - ---------- - --- --- - ----- Facility Address ------------- — -------------- .—I�ransporter Address 'Bryan H-eath --- -- --- - - — - - ----------- ---m! —Express Saver FacilitV Supervior- - - - ------- - ------- --- ------ 8WMU6 GW-2002 - - ----- --- ---- -- -- --------------- - --- ----- - — ----------- ---- ------ - — ------- Process Producing Sample IJ I Special Shipping Instructions V,260 APPIX plotee s S.1 a A 'Im molinNIM .'Other Ernplq3Lees(s) Handling — --- — ------ COMM 'Sample Pescaplion IBMI FWAVE Mi 0, WO Iff. 71-rit. =I- L-=- �MAMIRecelved by Refinquished by 0 Ternp. oT Samples on ArrIval./ -C ied by I ,, 0 "'.4 1%; DEQ-CFW-00025603 r LaTcaster I ",toratoriez- 2425 New Holland 1 3 Box 12425, Lancaster. PA 17605-2425 r-jo. VUQ' 35-504103-'. ,DuPont F2yetteville Route 87 South Fayettevilile NC 28302 Facility Address Bryan Heath I I Facil,W Sumervior ,SWMU6 GW-2002 Process Producila SanlDle ,Fe e I Express AZT ,Transporter Name ��nsporter Address _�tr[o f SDeclal Shimina Instructions ST1191 IUMINF4 JA 1010-2, LAMMAM Ej DEQ-CFW-00025604 TTOINE�� Lancaster -iorawries q,,3�,r 3 077--/ff -?�-I L� 7035-504103- 10 2425 New HDIland 0 Box 12425. Lancaster, PA 17605-2425 -3 7L Project-Vulff ber ------ - ----- - - ------- -- DuPont Fayetteville 111704-362 3 e'd I EXpress 8 Facility Name Telephone j;ymber' J�rans ofter Name 0-777-30- !Route 87 South Fayettevillie NC 28302 ---------- - - - ---------- - -------- ----- - - - ------ - ------ - - --------- - --- Facifity Addres3 mnsparter Address — - --------- - - - - ------ - - - -- - - - ------ - - --------- - ------- - — ------------ press Save• Method of Shipping -7 i SWIVIU6 GW-2002 Process Producing Sample SpecialShip n ------ — - -- ------ - �MetEth Methanol; 8270 APPIX; Cl-, F- (300.0) ',_grppjqyee s mDlina 6, A_LSa 1 - I tr EmployeevCcj 1-bandlin I q .. . .... ---------- -- ---- ---- - - - ---------- -- sample "1-3111117, �,�WIVEE Dm�pflon low JAMP Eff, 0�= -- - ----------- - -------- - -- - --- ---- -- - �Relinguished by DateMme 01 femp. of Samples on Arrival 12, R pli t =MJAIIIW�� EMMA. DEQ-CFW-00025605 70VMM�:: ! !� LdFIGUZU.'Ir iorgtone4, 2 b 04103 jo 2425 New Holland 0 Box 12425. Lancaster, PA 1760-24M -e ( nber jDuPont Fayetteville -�r�. 704-362- Facility Name LTelephone-MU!, Route 87 South Fayettevillie NC 28:302 Facility Address ----- ----- —'�rransporter Address - Pryan Heath ------- ,iE&xp ess Saver Method-of-SWIpping - PWMU6 GW-2W� - --- -- ---- - -------- - -- ------ - - Process Producing Sample — ----------- - — --------- -- Special Shipping Instructions AcrAcn Acrolein/Acrylonitriile Employee(s) Sanvih9l — - ----- - -- - - - ------ - ---- Other Employees(s) Handling ------------ MON InT NeVUrz-11-41 ,flott'lesRefinquished Lry F11- ----------- b 'bateMm e Relingulshed by b, -jI fill Temp. of Samples on C ...... ---- - Relinquisfie"ciby_ it - IM, 401) 00 -?o DEQ-CFW-00025606 Lqkm. +r•. Lancaster ' - Ioratories DuPont Fayetteville Facilfty Name ,Route 87 South Fayetteviffle NC 28302 Facility Address 3 3 9,64 3 0 6 33 FeHeral Express Number'Transporter Name Transporter Address MEMO= 1.5111MIXI DatefPme 0 I PWReceived i4" by POPS ingafion -Gondition gfl�arnp gm U on arrinl at Fin—aWest Rq Relinquished by 1���WR efved by z I MOMMME Temp-aNjarvjplesonAnival_ "Relinquished by I DEQ-CFW-00025607 . IL A.- !-- j I . NO. 0100 1 0 6 ON � Y3 1 72563 7035-SCF41-0 3 )0 2425 New Holland 0 Box 12425. Lancaster, PA 17605-2425 - --■- � Pmject Nurn-ber — - - - -------- IDuPont Fayetteville 1704-:362-663 ress i Facility Name Telephone Num jmqsponter f4ame Route 87 South Fayettevillie NC 28302 i Facility Address Transporter Address Express Saver 'SWMU6 OW-2002 Process Producing_ _ _ _ __ /, Al S"m le — - ---- -- --- - -- ----------- - Special Shipping Instructions — — - --------- AcrAcn Acrolein/Acrylonitrile Employee(s) S mpling �P�therEm�loy��aCs) andlin _g . . . ............. . . . ...... . . ..... ...... ,_K__ Oim-ple Description 1 -1 JO rl,.� W-0-MUM 'Relinquished by Temp. of Samples on Arrival Da—te/iiQ Oci DEQ-CFW-00025608 Lancaster --joratories WK, 0 7035-5041 W. A-1 0 Box 12425. Lancaster, PA 17605. 2425 New Holland 2425 .3;f a I Praiect-W-7ther- !DuPont F2yetteville 1104-:362- 6A- Facilky Name Telephone Num! 'Route 87 South Fayettevillie NC 26-302 Facility Addres5 M,�Trmmpprter Addre55 lBryan Heath �xpress Saver Facift-Suos )r El Method of Shipping SWMU6 GW-2002 Process Producing Sample Special Shipping Instructions crAcn crole n/Acrylonitrile pjgAes) Sampring L ----- - --- - ------- ----- --------- -- - ----------------- - -- - -- - -- - ---------- - — - - - ------ — ----- — - - ----- .Other _EMM0Y"9(8)_ tt2 dina _W0 -- - -- - -------------- — - ----- - -- -- b-a-m-ple---- DesOptlon N rq I�Mmw, 12-TV M.M. I agwar"MYREMOTINIMOU MMMM l'ID---a---t -A PLI-Ik, WAW----- a-- Art -e---M--- me eceveyM5 - a--e--------m--e- ---------- ---- --------------- Temp. M_�arnp! n ArrWal I A fshed Py 5 :, ---; I f - m DEQ-CFW-00025609 SWNIU Number and Name: SWMU 6 — Process Sewer System (Common Sump) Criteria for Individual SVVNWs-. Criteria for prioritization: I U 1 2 3 Unknown High Low NFA Potential Release to Air: 1 X Potential Direct Contact: Potential Releases to Groundwater: Potential Releases to Surface Water: I X IN Notes:(include prioritization reasoning, and modifying factors such as interim measures, discharge permits, and possession of data suitable for comparison to screening criteria) Organic constituents were detected in soils during the CS and Phase I RFI above MDL values but the total concentration of the constituents is less than I% by weight. Organic constituents were detected in soils during the CS and Phase I RFI above MDL values, but were below EPA Region IX industrial soil concentrations. Detected constituents are located in subsurface soils (more than 2 feet below grade) where exposure via this pathway is not expected. The presence of volatile organic compounds in groundwater, the shallow nature of groundwater and the proximity of buildings leads to an unknown ranking. Organic and inorganic constituents were detected in soils during the CS and Phase I RFI above MDL values, but are below Region III industrial soil concentrations. Detected constituents are located in subsurface soils (more than 2 feet below grade) where exposure potential is low. Institutional and operational controls exist to prevent excavation without taking proper measures and to minimize the potential for exposures via this pathway. Chromium and iron were detected in soils slightly above NC SSL concentrations. Chloride, fluoride, and methylene chloride were detected in the groundwater at levels above the DENR 2L groundwater quality standards. Groundwater flow is expected to be towards the Cape Fear River therefore, there are no potable sources for down gradient groundwater use. The presence of the underlying clay layer reduces the potential for vertical groundwater migration. This unit is designed to operate with a freeboard and as such would not overflow to a surface water body. A wet weather channel is present approximately 400 feet to the northeast of the unit. The presence of seepage faces along the channel banks are unknown as well as the presence of the clay layer base in the flood plain. The unit is overlain by a thick cover of soil and lies on relatively flat ground that does not promote runoff. Additional Comments: DEQ-CFW-0002561 0 I SWMU Number and Name: SWMU 7 — Storm Sewer System Criteria for prioritization: Notes:(include prioritization reasoning, and modifying factors such as interim measures, discharge hermits, and possession of data suitable for comuarison to screenin2 criteria) No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. Additional Comments: DEQ-CFW-00025611 k I I , - I # "Ok i t I Criteria for Individual SWMUs: Criteria for prioritization: U 1 2 3 1 Unknown High Low NFA Potential Fire or Explosion Hazards: I I I I X X X X X Notes:(include prioritization reasoning, and modifying factors such as interim measures, discharge permits, and possession of data suitable for comparison to screening criteria) Methanol was detected in only one soil sample above the PQL during the CS. Acetone was detected in four soil samples above the PQL. These constituents are present at concentrations less than 1% by weight. Environmental data for the upper 2-foot interval was not collected because the closure of this unit included the removal of its contents and the installation of a Moot silty sand cap. Access to this area is controlled by site security (e.g., fence, guards, etc.) Iron, nickel, acetone, and methanol were detected in soils above PQL or backgrounds levels, but are below Region III industrial soil concentrations. Constituent concentrations are located in subsurface soils (more than 2 feet below grade) where exposure potential via this pathway is not expected. Institutional and operational controls exist to prevent excavation without taking proper measures and to minimize the potential for exposures via this pathway. Iron was detected in soils above North Carolina SSL concentrations. Chromium was detected in the upgradient monitoring well and one downgradient monitoring well and lead was detected in the upgradient monitoring well and four downgradient monitoring wells above the NC 2L standards (Cr = 0.00175 mg/l; Ph = 0.015 mg/1). However no significant difference between upgradient and downgradient groundwater concentrations was observed. Groundwater flow is expected to be towards the Cape Fear River therefore no potable sources for down gradient groundwater use. Nearest surface water is approximately 1900 feet from this area. Constituents are located in subsurface soils with a thick soil cover that does not lend itself to runoff. The surrounding area is also relatively flat preventing seepage development. Groundwater flow in the shallow surficial aquifer in the vicinity of the unit is in a southwesterly direction away from the Cape Fear River. Additional Comments: DEQ-CFW-00025612 SWNTU Number and Name: SWMU 9 C — Former WWTP Lagoon Rankin g Criteria for Individual SWNWs: Criteria for prioritization: U 1 2 3 Unknown High Low NFA Potential Fire or Explosion Hazards: X Potential Release to Air: X Potential Direct Contact: X Potential Releases to Groundwater: X Potential Releases to Surface Water: X Notes:(include prioritization reasoning, and modifying factors such as interim measures, discharge hermits. and nossession of data suitable for comparison to screening criteria) No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. Additional Comments: DEQ-CFW-00025613 SWMU Number and Name: AOC-C — Former Ag Products UST Area Criteria for prioritization: Notes: (include prioritization reasoning, and modifying factors such as interim measures, discharge permits, and possession of data suitable for comparison to screening criterial Potential Fire or Explosion Hazards, No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. No constituents were identified above background or PQL values during confirmatory sampling activities. Additional Comments: DEQ-CFW-00025614 SWNIU Number and Name: Fire Training Area Ranking Criteria for Individual SWNIUs: Criteria for prioritization: U 1 2 1 1 3 Unknown Hi2h Low NFA Potential Fire or Explosion Hazards: Potential Release to Air: Potential Direct Contact: Potential Releases to Groundwater: Potential Releases to Surface Water: X X X X X Notes:(include prioritization reasoning, and modifying factors such as interim measures, discharge permits, and possession of data suitable for comparison to screenina criteria) A limited area of TPH impacted soil remains in the area after extensive excavation activities of contaminated soils. The limited area of TPH impacted soil is approximately 11 to 13 feet below the ground surface. No buildings are in the vicinity of the area. Volatile organic constituents were not detected in the RFI groundwater samples. A majority of the contaminated soil was excavated during road construction. A limited TPH impacted area remains at depth. Institutional controls are in place to prevent unauthorized excavation. The area is capped by an asphalt road and excavation in this area is unlikely. Nickel was detected above the PQL values. Lead was detected between the MDL and PQL; however, the concentration detected slightly exceeded the North Carolina 21, Standards. There are no potable sources for down gradient groundwater use. Volatile organic constituents were not detected in the RFI groundwater samples. The presence of the underlying clay layer retards the vertical migration of groundwater. The area is relatively flat terrain and does not promote runoff. Nearest surface water is approximately 1900 feet from this area. Additional Comments: DEQ-CFW-00025615 1�1# ��MVHIIIHKPUI 1 I!IMIRAWMA�# �VNVIIWUIDHT-�� SWMU Number and Name: AOC GW — Groundwater Criteria for prioritization: X X X X X Notes: (include prioritization reasoning, and modifying factors such as interim measures, discharge permits, and possession of data suitable for comparison to screening criteria) Groundwater was not encountered during soil sample activities. Constituents detected in soils were present in concentrations lass than 1% in soil, therefore it is not expected to present in groundwater at concentrations greater than 1%. Groundwater samples were collected from monitor wells associated with SWMU 9 A, B. C and did not contain constituents with flash noints < 140' F. No constituents exceeded Region IX soil screening concentrations. Groundwater is found at depths ranging from 6 to 13 feet below ground surface and therefore exposure via this pathway is not expected. Groundwater is found at depths approximately 6 to 13 feet below ground surface. Institutional controls are in place to prevent unauthorize excavations. Constituents detected in soils were below Region III industrial soil concentrations, therefore exposure via this pathway is not expected. The presence of the clay layer beneath the shallow surfacial aquifer limits the vertical migration of groundwater. It is expected that shallow groundwater discharges into the Cape Fear River which is located approximately 1900 feet from the manufacturiniz area. DEQ-CFW-00025616