NCG210099_DWR Response Letter Recycle Pond Closure_20170403

Iry
Water Resources
Environmental Quality
April 3, 2017
Carl B. Powell
Powell Industries, Inc.
P.O. Box 65
Waynesville, NC 28786
Subject: Closed -Loop Recycle Permit (WQ0015487)
Pond Closure Requirements
Powell Industries, Inc.
Suncrest Chip Mill
Haywood County
Dear Mr. Powell,
ROY COOPER
Governor
MIC14AEL S. REGAN
Secivai,
S. JAY ZIMMERMAN
Director
On January 17, 2017, your legal counsel requested rescission of your current Closed -Loop
Recycle System Permit (WQ0015487) and in the process convert the existing ponds into
stormwater basins.
The purpose of this letter is to inform you of the requirements necessary to close out the
Closed -Loop Recycle System prior to permit rescission. It is important to note that these closure
proceedings will apply to the 0.2 -acre upper pond, referred to as the wastewater recycle pond,
and the 0.3 -acre pond, referred to as the lower stormwater pond. The lower stormwater pond
is included in these closure proceedings because it was improperly used for the storage of
wastewater and wastewater residuals. The closure requirement for these two ponds will be
based on a Division of Water Resources (DWR) document titled Guidelines for the Closure of
Permitted Wastewater Ponds and Lagoons dated June 22, 2012. A copy of these closure
guidelines is enclosed.
The wastewater recycle pond was originally permitted as a non -discharge system for the
collection of wastewater from the company's wet decking operation. But from its inception, the
wastewater recycle pond was used for the collection of stormwater from the roughly 11 -acre
site. Runoff from the chipping mill, log storage yard, maintenance garage area, and access roads
is routed to an open ditch and a number of stormwater drop boxes that discharge directly to
the wastewater recycle pond. Water levels in the wastewater recycle pond were managed by
regularly transferring wastewater to the lower stormwater pond in direct violation of
WQ0015487 permit conditions. While there is no longer a visible outlet to the pond, DWR
'Nothing Compares:''-._.
state orNorth Carolao I Environmental Quality I Water Resources
2090 US, Highway 70, Swannanoa North Carolina 28778
828-296-4500

Carl B. Powell
April 3, 2017
Page 2 of 3
believes that a hydraulic connection exists between the lower stormwater pond and an
adjacent stormwater drain that discharges to Jonathan Creek.
Water samples collected from the wastewater recycle pond by DWR staff and Mountain
Environmental indicate elevated biochemical oxygen demand (BOD), chemical oxygen demand
(COD), total nitrogen, and total phosphorus. In addition, concentrations of toluene, total
phenolic compounds, total suspended solids (TSS), and turbidity exceed the applicable surface
water standards. A copy of the analytical results is enclosed.
Based on these analytical results, the quality of your stormwater would likely exceed the
performance benchmarks (e.g. COD & TSS) contained in the general stormwater permit. The
presence of toluene, phenolic compounds, nutrients, BOD, and turbidity could prohibit the
permitted discharge to Jonathan Creek, a Class C stream with Trout Water designation. It is
highly recommended that you conduct a site audit with a focus on identifying potential waste
streams as well as opportunities to improve stormwater quality.
As part of the closure process, you will be required to dewater the wastewater recycle pond
and remove all wastewater residuals for proper disposal. Sampling of the wastewater residuals
and the native soils beneath the wastewater recycle pond will also be required. An adequate
number of representative and composite samples should be taken and developed respectively.
You will be required to sample for the following parameters:
• Metals — arsenic, cadmium, calcium, chromium, copper, lead, magnesium, mercury,
molybdenum, nickel, selenium, sodium, and zinc
• Nutrients—ammonia nitrogen, nitrate nitrogen, nitrite nitrogen, TKN, and total
phosphorus
• Total phenolic compounds
• Volatile organic compounds
• Semi -volatile organic compounds
Priorto disposal, the wastewater residuals will likely be stored onsite for some extended period
of time and therefore will need to be protected (e.g. tarp) against exposure to rainfall and
erosion. Additionally, you will need to provide documentation verifying the proper disposal of
the wastewater residuals. Please be aware that the wastewater residuals cannot be given away
or land applied without a separate permit.
You will also be required to investigate the hydraulic connection between the lower
stormwater pond and an adjacent stormwater drain that discharges to Jonathan Creek. DWR is
willing to assist with this effort. DWR is proposing that water from the wastewater recycle pond
be transferred to the lower stormwater pond and dosed with an appropriately colored tracking
dye. Conceptually, a discharge will be initiated if the water level in the lower stormwater pond
is raised to within 3 feet of the top of the dam. Powell Lumber will be responsible for

Carl B. Powell
April 3, 2017
Page 3 of 3
transferring the water and DWR will be responsible for dosing the pond with dye and
monitoring the outlet at Jonathan Creek. If a hydraulic connection is confirmed, then the
connection will need to be eliminated before the wastewater recycle permit can be rescinded.
The DWR is interested in being present during the various closure activities. Please keep this
office apprised of your work schedule. More importantly, you will need to contact DWR prior to
transferring any wastewater to the lower stormwater pond. Please do not hesitate to contact
me if you have any additional questions or concerns. I can be reached at [phone] or
brett.laverty@ ncden r.gov.
Sincerely,
L/
Water Quality Regional Operations
Asheville Regional Office
Attached: DWR laboratory data sheets
Pace Analytical laboratory data sheets
Guidelines for the Closure of Permitted Wastewater Ponds and Lagoons
cc: ARO file
cc: Toby Vincent—DEMUR
Bethany Georgoulias - DEMLR
Stan Aiken - DEMUR
Richard Brooks - DEMLR
David Goodrich —DWR
Max Kimel — Mountain Environmental
Billy Clarke - Roberts & Stevens, P.A.

AC29333
Lou. Deah.: POWELL LUMBER4595 JONATHAN CREEK ROAD WAYNESVILLE
Acenaphthene
Sample In
AC29333
County: Havwnod Collecbr: B LAVIE
Uait10
F—LI
PO Number#
208-96-8
ReOioo: ARO Repod To ARO
20
Location ID:
IC44POWELL
Data Repented,
b6rz61ID16
River Basin Jonathan one. Collect Date: 0 612 312 016
Priority
ROUTINE
Time Received'.
06_20
Emergency Wlec[Tlma 16_06
EPA625182700
Sample Matrix:
SDRFACEWATER
LebwoRs LoginlD
MSWIFT
COC YeVNhr Yea Semple Depth NA
Not detected
Loc. Type:
Sto a[w gr_
Delivery Method
NCS
a
benzeneaCellC acid
11 N7
Final Repod Date'. Gol
O
WAsrEw,f-rtl �c ecye l6 QaAW
Final Reoort
CJOHNSON
Report Print Date: ]010612016
If this report is labeled preliminary report the results have not been validated.
Do not use for
Regulatory purposes.
oglL
EPA62518270D
Result/
CJOHNSON
Method Analysis
Benzo(a)pyrene
10
Not detected
tight.
Units
6/3116
CJOHNSON
CAS # Analyte Name
PQL
Quallifer
Not detected
Reference
Date value
60,16
CJOHNSON
LAB
Benzo(g,h,i)perylene
20
Not detected
Sample temperature at receipt by lab
EPA62518270D
1.9
°C
207-66-9
5125116 TASCENZ01
30
Not detected
NUT
EPA625h82200
Mile
CJOHNSON
NH3 as N in liquid
0.02
0,05
mghL a3N
EPA 350.1 REV
5125116 CGREEN
Nitrate as N In liquid
0.02
0.02U
mglL asN
EPA 353.2 REV 2'
5125116 CGREEN
Nitrite as N in liquid
0.01
0.01U
mglL esN
EPA 353,2 REV '
5125116 /DOREEN
1,102+NO3 as N in liquid
0.02
9.92 U
r lL as N
EPA 3532 REV 2
5125116 CGREEN
Phosphorus_ total as P in liquid
0.02
0.52
mall asP
EPA 355.1. REV
5131116 CGREEN
Total Kjeldahl N as N In liquid
0.2
3.5
mg/L es N
EPA 351.2 REV 2
613116 CGREEN
uglL
EPA52WB270D
WET
CJOHNSON
117-81-7
Bis(2-ethylhexypphthalate
Chemical Oxygen Demand in liquid
20
.230
nxi
Hach 6000
612116 DOREEN
Grease and Oil In liquid
10
10 U,12
it lL
EPA 16643
5126116 CGREEN
Bromide
04
0.4U
nalL
EPA 3000 ri1
5125116 CGREEN
Chloride
1.0
8.5
ml
EPA 300.0 rev2.1
5125116 CGREEN
Fluoride
0A
O,;U
nalL
EPA 3600 rev2.1
5125116 CGREEN
Sulfate
2.0
3.9
r lL
EPA 300.0 rev2.1
5125116 CGREEN
Phenolics -Total in liquid 10 800 out. EPA 4204 REV 1 shone DOREEN
Semivolatile Organics IBNAs) in liquid
63-32-9
Acenaphthene
10
Not detected
uga
EPA62518270D
613116
CJOHNSON
208-96-8
Acenaphthylene
20
Not detected
uga
EPA625182700
613116
CJOHNSON
62-533
Aniline
10
Not detected
u01L
EPA625182700
61316
CJOHNSON
120-127
Anthracene
20
Not detected
o91L
EPA62518270D
613116
CJOHNSON
benzeneaCellC acid
11 N7
uglL
EPAe25890D
W3116
CJOHNSON
56-55-3
Benzo(a)anthracener
20
Not detected
oglL
EPA62518270D
BO116
CJOHNSON
50-32-8
Benzo(a)pyrene
10
Not detected
tight.
EPA62518270D
6/3116
CJOHNSON
205-99-2
Benzo(b)fluoranthene
10
Not detected
uOhL
EPA625/8270D
60,16
CJOHNSON
191-24-2
Benzo(g,h,i)perylene
20
Not detected
ughL
EPA62518270D
613116
CJOHNSON
207-66-9
Benzo(k)fluoranthene
30
Not detected
ughL
EPA625h82200
Mile
CJOHNSON
65-85-0
Benzoic acid
100
160 P1
uglL
l EPA625he270D
613116
CJOHNSON
188-51-6
Benzyl alcohol
30
Not detected
ugA.
r EPA625/8270D
all
CJOHNSON
111-91-1
Bls(2-chloroethoxy)methane
10
Not detected
u91L
EPA52518270D
613116
CJOHNSON
fli-043
Bis(2-chlomethyl)ether
10
Not detected
ughL
EPA62WB270D
613/16
CJOHNSON
39830-32-9
Bis(2-chlomisopmpyl)ether
10
Not detected
uglL
EPA52WB270D
613/16
CJOHNSON
117-81-7
Bis(2-ethylhexypphthalate
30
Not detected
uglL
EPA625h8DOD
613/16
CJOHNSON
WSS Che rmil Laboratory» 1623 Mall Service Display, Raleigh, NC 27699-1623 [phone]
Not Detected" or"U" doe. not indicate the sample is one" free but that the analyte is not detected at or ebove the POL.
Page 1 of 6

I 9VC7D11J$, La6amtorySection 9(psufa/Sample Cammemtr/Qmdsfiertpefimtm=
Sample 10: AC29333
CAS #
101-553
Analyte Name
Bromophenyl phenyl ether, 4-
PQL
10
ualifier
Not detected
Units
ag/1-
Reference
EPA625/8270D
Date
heels
Valles
CJOHNSON
85-68-7
Butylbenzyl phthalate
10
Not detected
ug1L
EPA62WB270D
6/3/16
CJOHNSON
59-50-7
Chlom-3-methyl phenol, 4-
10
Not detected
ug/L
EPA625`827OD
Mile
CJOHNSON
106-47-6
Chloreanlllne, 4-
10
Not detected
uyL
EPA525/82701)
8/3/15
CJOHNSON
91-5&7
Chlomnaphthalene, 2-
10
Not detected
uga
EPA625/B270D
6`3/16
CJOHNSON
95-57-6
Chlorophenol, 2-
10
Not detected
ug/L
EPA62WB270D
6/3116
CJOHNSON
700542-3
Chlorophenyl phenyl ether, 4-
20
Not detected
ug1L
EPA625IS270D
W3/16
CJOHNSON
218-01-9
Chrysene
20
Not detected
ug1L
EPA525`8270D
6/3/18
CJOHNSON
53-70-3
Dlbenzo(a,h)anthracene
20
Not detected
ug/L
EPA625/8270D
613/16
CJOHNSON
132-649
Dibenzofuran
20
Not detected
ug1L
EPA62NBVCD
Will
CJOHNSON
95-50-1
Dichlorobenzene, 1,2-
10
Not detected
ug/L
EPAS2518270D
6/3/16
CJOHNSON
541-711
Dichlorobenzene, 1,3
10
Net detected
ug1L
EPA62NBVCD
6`3/16
CJCHNSON
106-464
Dichlorobenzene, 1,4-
10
Not detected
ug/L
EPA62WB270D
6/3/16
CJOHNSON
W-04-1
Dlchlorobenzldlne, 3,3'-
30
Net detected
ug/L
EPA6251627OD'
W3/16.
CJOHNSON
120-63-2
Dichlorophenol, 2,4-
10
Not detected
ug`L
EPA62WB270D
6/3116
CJOHNSON
84-66-2
Diethyl phthalate
20
Net detected
uyl-
EPA52WO270D
8/3/18
CJOHNSON
131-113
Dimethyl phthalate
10
Not detected
ug1L
EPA625`8270D
6/3/16
CJCHNSON
105-67-9
Dimethylphenol, 2,4-
10
Not detected
ug1L
EPA62WB270D
6/3118
CJOHNSON
84-742
Di -n -butyl phthalate
20
Not detected
ug1L
EPA62518270D
6/3/16
CJOHNSON
534-52-1
Dinitro-2-methyl phenol, 4,6-
50
Not detected
ug/L
EPA62518270D
6/3/18
CJOHNSON
51-28-5
Dinitrophenol, 2,4-
50
Not detected J2
ug1L
EPA625`627OD
6/3/16
CJOHNSON
121-14-2
Dinitrotoluene, 2,4-
20
Not detected
ug/L
EPA62WB270D
.6/3118
CJOHNSON
606-20-2
Dinitrotoluene, 2,6-
10
Not detected
ug/L
EPA6250627OD
6/3/16
CJOHNSON
117-84-0
Di-n-octyl phthalate
10
Not detected
ug/L
EPA62518270D
6/3/16
CJOHNSON
ethyl phenol
9.0 N7
ug1L
EPA62516270D
6/3/16
CJOHNSON
206.44-0
Fluoranthene ^ -
--20
- Not detected
ug`L
.EPA62518270D-
6/3116
CJOHNSON
88-73-7
Fluomne
20
Not detected
ug/L
EPA625/6270D
6/3/16
CJOHNSON
118-74-1
Hexachlerobanzene
20
Net detected
ug`L
EPA625132OD
8/3/15
CJOHNSON
87-68-3
Hexachlorobutadiene(SV)
10
Not detected
u9/L
EPA625(827013
WN16
CJOHNSON
77-474
HBxaehloroeyelopentadlene
10
Not detected
ug/L
EPA62513=D
8/3/16
CJOHNSON
67-72-1
Hexachlorcethane
10
Not detected
ug`L
EPA625)690D
8/3/16
CJOHNSON
hydrocinnamic acid
920 N7
eg/L
EPA625(8270D
6MI16
CJOHNSON
193-39-5
Indeno(1,2,3-cd)pyrene
20
Not detected
ug`L
EPA6251827013
WW16
CJOHNSON
78-59-1
SOphoroOe
10
Not detected
ug/L
EPA62518270D
6MI16
CJOHNSON
methylpentanoic acid
20 N7
ug/L
EPA625/82700
813118
CJOHNSON
methyl phenol
260 N1
ug`L
EPA625/8270D
6/3116
CJOHNSON
91-57-6
Methylnaphthalene, 2-
10
Not detected
ug`L
EPA625182700
813116
CJOHNSON
95-48-0
Methylphenol, 2-
10
Not detected
ug`L
EPA62WB270D
613/16
CJOHNSON
100-44-5
Methylphenol, 4-
10
Not detected
ug/L
- EPA625182700
613116
CJOHNSON
91-20-3
Naphthalene(SV)
10
Not detected
ug`L
EPA62518270D
613116
CJOHNSON
8844-4
Nitmaniline, 2-
10
Not detected
ug/L
EPA62518270D
613116
CJOHNSON
99-09-2
Nitmaniline, 3-
50
Not detected
eg/L
EPA62518270D
613116
CJOHNSON
100.016
Ntroanlline, 4-
50
Not detected
ug`L
EPA62518270D
613118
CJOHNSON
WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 [phone]
"Not Detected" or"D" Boas not indices the sample is analyte free butthat the analyte ie not beteated at or above the PDL.
Page 2 of 6

n/D'KX La6omtory Section
AC29333
CAS#
98-95-3
Analyte Name
Nitrobenzene
PQLualifer
10
Not detected
Units
ug/L
Reference
EPA62518270D
Date
813118
vaiuu ieau
CJOHNSON
8875-5
Nitrophenol, 2-
10
Not detected
ugll-
EPAS25182700
6MI16
CJOHNSON
100-02-7
Nitrophenol, 4-
50
Not detected
ug/L
EPA625/8270D
613116
CJOHNSON
621-644
N-nilrosodi-n-propylamine
10
Not detected
ug/L
EPA62518270D
613116
CJOHNSON
86-366
N-nitrosodiphenylamine
10
Not detected
ug/L
EPA525/8270D
813116
CJOHNSON
67-86.5
Pentachlorophenol
30
Not detected
411-
EPA62518270D
6MI16
CJOHNSON
65-01-6
phenanthrene
20
Not detected
ug/L
EPA825/8270D
613116
CJOHNSON
108-95-2
Phenol
50
210 P1
ug/L
EPA62518270D
613116
CJOHNSON
87-e1-6
phenylvaleric acid
1.0
9.6 N7
ug/L
EPA625/82700
613116
CJOHNSON
129-00-0
Pyrene
20
Not detected
ug/L
EPA525/8270D
613118
CJOHNSON
120-82-1
Trichlorobenzene, 1,2,4-
10
Not detected
ug/L
EPAS25182700
613116
CJOHNSON
95-954
Trichlorophenol, 2,4,5-
10
Not detected
ug/L
EPA825/82700
813116
CJOHNSON
88-06-2
Trichlorophenol, 2,4,6-
10
Not detected
ug/L
EPAS2518270D
613116
CJOHNSON
107-06-2
-valeric acid
1.0
24 N7
ug/L
', EPA62518270D °
613116
CJOHNSON
Volatile Organics in liquid
106-93-4
(EDB)1,2-Dibromoethane
1.0
Not detected
ug/L
EPA62418260C
5129/16
CJOHNSON
630-20-6
1,1,12 -Tetrachloroethane
1.0
Not detected
ug/L
EPA624/82600
5127/16
CJOHNSON
71-5578
1,1,1 -Trichloroethane
1.0
Not detected
ug/L
EPA524/8260C
5127118
CJOHNSON
7934-5
1,1,2,2 -Tetrachloroethane
1.0
Not detected
ug/L
EPAS24182600
SP7116
CJOHNSON
79-00-5
1,1,2 -Trichloroethane
i0
Not detected
ug/L
EPA524/8260C
5127116
CJOHNSON
75-34-3
1,1-Dichloroethane
1.0
Not detected
ug/L
EPA62418260C
.5127116
CJOHNSON
75-35-4
1,1-Dlchloroethene
1.0
Not detected
ug/L
EPA52418260C
5127116
CJOHNSON
563-58-6
1,1-Dichloropropene
1.0
Not detected
ug/L
EPA624/8260C
5127116
CJOHNSON
87-e1-6
1,2,3-Trichlorobenzene
1.0
Not detected
ug)L
EPA62418260C
5127116
CJOHNSON
96-18-4
1,2,3-Tdchloropropane - --
--._.1.0-
Not detected
ug/L -.
EPA624/8260C
--5127116,.
.. CJOHNSON ...:
120-82-1
12,4-Trichlorobenzene
1.0
Not detected
ug)L
EPA52418260C
5127116
CJOHNSON
95-63-6
1,2.4-Trlmethylbenzene
1.0
Not detected
ug/L
EPA62VB260C
5127116
CJOHNSON
98-12-8
1,2-Dibromo-3-Chloropropane
2.0
Not detected
ug)L
EPA62418260C
5127116
CJOHNSON
107-06-2
1,2-Dichloroethane
1.0
Not detected
ug1L
EPA624/8260C
5127116
CJOHNSON
7887-5
1,2-Dichloropropane
1.0
Not detected
ug1L
EPA624/8260C
5127116
CJOHNSON
10667-8
1,3,5-Trimethylbenzene
1.0
Not detected
ug1L
EPA62MB260C
5/27116
CJOHNSON
142-28-9
1,3-Dichloropropane
1.0
Not detected
ug)L
EPA624/8260C
U27116
CJOHNSON
59120-7
2,2-Dichloropropane
2.0
Not detected
ug1L
EPA62WO260C
5127/16
CJOHNSON
054P8
2-Chlorotol0ene
7-0
Not detected
ug1L
EPA62418260C
5127116
CJOHNSON
10643-4
4-Chlorolgluene
1.0
Not detected
ug1L
EPA62418260C
5127116
CJOHNSON
VASS Chemlaby Laboratory— 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
"Not nobodies' or 1j" does not indidate the Sample i5 analyte tree but that the analyte la not reverted at or above the PQL.
Page 3 of 6
Alkanes
13 N1
uglL
EPA624/82506
5/27/16
GJUHNSUN
7143-2
Benzene
1.0
Not detected
ug/L
EPA6241S260C
5127/16
CJOHNSON
106864
Bromobenzene
1A
Not detected
ug1L
- EPA62418260C
5/27/16
CJOHNSON
74-97-5
Bromochloromethane
1.0
Not detected
ug/L
EPA62418260C
5/27/16
CJOHNSON
75-27-4
Bromodichloromethane
1.0
Not detected
ug/L
EPA62418260C
5/27/16
CJOHNSON
75-252
Bromoform
2.0
Not detected
ug/L
EPA624/8260C
5rz7/16
CJOHNSON
74-638
Bromomethane
2.0
Not detected
ug/L
EPA62418260C
5/27/18
CJOHNSON
VASS Chemlaby Laboratory— 1623 Mall Service Center, Raleigh, NC 27699-1623 [phone]
"Not nobodies' or 1j" does not indidate the Sample i5 analyte tree but that the analyte la not reverted at or above the PQL.
Page 3 of 6

XC OWX Latiomtory Section PZpraCts/Sample Comment /Qua fuer Definitions
Sample 10: AC29333
CAS#
56-23-5
Analyte Name
Carbon Tetrachloride
PQL
1.0
ualifer
Not detected
Units
ug(L
Reference
EPA62418260C
Date
527118
yank
CJOHNSON
108-90.7
Chlorobenzene
1.0
Not detected
ug)L
EPA6241826OG
5/27116
CJOHNSON
75-00-3
Chloroethane
2.0
Not detected
.,IL
EPA62418260C
5127116
CJOHNSON
67-663
Chloroform
1.0
Not detected
ug/L
EPA62418260C
5127116
CJOHNSON
74-67-3
Chloromethane
2.0
Not detected
uglL
EPA62418260C
5127116
CJOHNSON
156-59-2
cis-1,2-Dichlorcethene
1.0
Not detected
u91L
EPA62418260C
5127116
CJOHNSON
10061-01-5
cis-1,3-Dichloropropene
2.0
Not detected
ug/L
EPA62418260C
5127116
CJOHNSON
12448-1
Dlbromochloromethane
2.0
Not detected
ug1L
EPA62418260C
5127116
CJOHNSON
7495-3
Dibromomethane
1.0
Not detected
ug1L
EPA624/6260C
5127/16
CJOHNSON
75-71-6
Dichlorodifluoromethane
2.0
Not detected
ug/L
EPA52418250C
5127/16
CJOHNSON
Dimethyl sulfide
14 N7
ug/L
EPA624/8260C
5/27/16
CJOHNSON
100-41-4
Ethylbenzene
1.0
Not detected
ug11-
EPA524/8280C
5/27116
GJOHNSON
87-68-3
HBXachlorobotadlene
1.0
Not detected
u,IL
EPA624I62803
5/27/16
CJOHNSON
98-82-8
)sopropylbenzene
1.0
Not detected
ug/L
EPA624B260G'
5/27/16
CJOHNSON
100-38-3
m,p-Xylene
2.0
Not detected
ug/L
EPA6241B260C
527)18
,CJOHNSON
541-73-1
m-Dichlorobenzene(1,3)
1.0
Not tletectetl.
ug/L
EPA62418260C
527116
CJOHNSON
1634-044
Methyl Ted -Butyl Ether
LO
Not detected
ug/L
EPA62418260C
527116
CJOHNSON
75-09-2
Methylene Chloride
1.0
Not detected
ug/L
EPA62418260C
5(27/16
CJOHNSON
91-20-3
Naphthalene
2.0
Not detected
ug)L
EPA624/8260C
5127116
CJOHNSON
104-51-8
n-Butylbenzene
1.0
Not detected
un-
EPA62418260C
5127116
CJOHNSON
103-65-1
n-Propylbenzene
1.0
Not detected
ug)L
EPA62418260C
N27116
CJOHNSON
95-50-1
o-Dlchlorobenzene(1,2)
1.0
Not detected
ug(L
EPA62418260C
5127116
CJOHNSON
95-47-6
o_XyleO&
1.0
Not detected
ug)L
EPA62418260C
U27116
CJOHNSON
106-46-7
p-Dichlorobanzene(1,4)
1.0
Not detected
ug11-
EPA62418260C
6127116
CJOHNSON
99-87-6
p-Isopmpyltoluene
1.0
1.6
uglL
EPA62418260C
5127116
CJOHNSON
185-988,.: .::.
Soo-Butylbenzene -
-'1:0--
Not detected'
"'.:: ug/L,
EPA62418260C.
.5/27116
.., OJOHNSON
100-42-5
Styrene
1.0
Not detected
uglL
EPA62418260C
5127116
GJOHNSON
98-66.6
tert-Butylbenzene
1.0
Not detected
ug1L
EPA62418260C
5127/16
CJOHNSON
127-10-4
Tetrachlonoethene
1.0
Not detected
ug11-
EPA62418260C
5127/16
CJOHNSON
108-88-3
Toluene
1.0
64
can
EPA624/8260C
5127/16
CJOHNSON
156-80-5
tmns-1,2-Dichloroethene
1.0
Not detected
ug/L
EPA624/8260C
5127/18,
CJOHNSON
10061-02-6
trans-1,3-Dichloropropene
2.0
Not detected
ug/L
EPA624I6260C
5/27/16
CJOHNSON
79-01-6
Trichloroethene
1.0
Not detected
u91L
EPA62418260C
5/27/18
CJOHNSON
75-6&4
Trichlorofluoromethane
2.0
Not detected
ug1L
EPA62VB260G
5127/16
GJOHNSON
75-01-4
Vinyl Chloride
2.0
Not detected
ug1L
EPA62NB260C
5/27/16
CJOHNSON
MISS chemistry Laboratory» 1323 Mail Service Center, Raleigh, NC 27399-1623 [phone]
"Not Detect ar'v" does not mcicate the sample is ani free but that the analyte is not tletectetl at or above the POL.
Page 4 of 6

NC9J'WIR La6oratory Seetion R¢ruld/Sampee Commentr/Qun6fieroefinitiion,
Sample In AC29333
Result/ Method Analysis
Sample comments
Ib IJ did not meet acceptance criteria -precision.
to -tentatively Identified by MS library search.
-t analyte failed a LCL in the CV2
l4 ntatively mend by MS library search.
PQL-dilution 5x
Valu
NCDEQ-WSS-Chamistry Lab Data Qualifiers
Al The reported value is an average, where at least one result is qualified with a "I The PQL is used for the qualified result(S) to cab
B1 Coliform -Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all filters repor
B2 Coliform -Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been
B3 Coliform -Countable membranes with more than 60 or 80 colonies. The value reported is calculated using the count from the smaller
B( Coliform -Filters have counts of both >60 or 80 and <20. Reported value is estimated or is a total of the counts on all filters reported
B5 Coliform -Too many colonies were present; too numerous to count (TNTC). TNTC is generally defined as>150 colonies.
B6 Coliform -Estimated Value. Blank contamination evident.
B7 Coliform -Many non -coliform or non -enterococcus colonies or interfering non -coliform or non -enterococcus growth present. In this cc
BB1 MPN-No wells or tubes gave a positive reaction. Value based upon the appropriate MPN Index and reported as a less than "<" valid,
BB2 MPWAII wells or tubes gave positive reactions. Value based upon the MPN Index and reported as a greater than ">" value.
C Total residual chlorine was present in sample upon receipt in the laboratory; value is estimated.
G1 BOD -The dissolved oxygen (DO) depletion of the dilution water blank exceeded 0.2 mg/L.
G2 BOD -The bacterial seed controls did not meet the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at lea:
-. G3 BOp-No sample dilution met the requirement of aDO depletion of at least 2,.O in I1 a90/ora DO residual of at least 1.0 SI
G4 BOD -Evidence of toxicity. This is generally characterized by a significant increase in the BOD value as the sample concentration de
G5 BOD -The glucose/ glutamic acid standard exceeded the range of 198 t 30.5 mg/L.
G6 BOD -The calculated seed correction exceeded the range of 0.610 1.0 ril
G7 BOD -Less than 1 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated for
G8 BOD -Oxygen usage is less than 2 mg/L for all dilutions set. The reported value is an estimated less than value and is calculated for
G9 BOD -The DO depletion of the dilution water blank produced a negative value.
J1 Surrogate recovery limits have been exceeded.
J2 The reported value failed to meet the established quality control criteria for either precision or accuracy.
J3 The sample matrix interfered with the ability to make any accurate determination.
J4 The data is questionable because of improper laboratory or field protocols (e.g., composite sample was collected instead of grab, pl
J5 Temperature limits exceeded (samples frozen or >60C) during transport or not verifiable (e.g., no temperature blank provided): non -
J6 The laboratory analysis was from an unpreserved or improperly chemically preserved sample. The data may not be accurate.
J7 This qualifier is used to identify analyte concentration exceeding the upper calibration range of the analytical instrumenUmethod. Th
J8 Temperature limits exceeded (samples frozen or >60C) during storage, the data may not be accurate.
J9 The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J10 Unidentified peak; estimated value.
J11 The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J12 The calibration verification did not meet the calibration acceptance criterion for field parameters.
M Sample and duplicate results are "out of control". The sample is non-homogenous((e.g., VOA soil). The reported value is the lower,
N1 Presumptive evidence and estimated value. The component has been tentatively identified base on mass spectral library.
N2 There is an indication that the analyte is present, but quality control requirements for confirmation were not met (i.e., presence oY
N3 This code shall be used if the level is loo low to permit accurate quantification, but the estimated concentration is less than the labor
N4 This code shall be used if the level is loo low to permit accurate quantification, but the estimated concentration is less than the labor
N5 The component has been tentatively identified based on a retention time standard.
Q1 Holding time exceeded prior to receipt by lab.
Was Chemistry LaboMorys> 1623 Mail Service Center, Raleigh, NC 27699-1623 19197 7334908
'Not cadaver]" or"U" doaa not indicate the Sample ie a0alya free not that Ole analyte is not detected at or above the PQL.
Page 5 of 6

SVC MX La6oratoySaotio. &,afiv/Sample Commeras/rjuaGfier0efinitirm
sample to AC29333
CAR k Analyte Name POI
Q2 - Holding time exceeded following receipt by lab.
P Elevated PQL' due to matrix interference and/or sample dilution.
S Not enough sample provided to prepare and/or analyze a method -required matrix spike (MS) and/or matrix spike duplicate (MSD).
U Indicates that the analyte was analyzed for but not detected above the reported practical quantitation limit'. The number value repo
X1 Sample not screened for this compound.
X2 Sampled, but analysis lost or not performed -field error.
X3 Sampled, but analysis lost or not performed -lab error.
V Indicates the analyte was detected in both the sample and the associated method blank. Note: The value in the blank shall not be s
V Elevated PQL* due to insufficient sample size.
Z1 Inability to analyze the sample.
Was ChGanstry Laboddi 1623 Mail Service Center, Raleigh, NC 276994623 (919) 7334908
'Nat Detected' or "P does not Indicate the sample is analyte free butthat the singill is net detected at or above the PQL.
Page 6 of 6

AC29419
Lac. Does,.:
County:
Region:
River Deain
Emergency
COC Ysi
North Carolina Division of Water Resources Water Sciences Section Laboratory Results
POWELL LUMBER 4699
JONATHAN CREEK RD
PO Number
ARO
HHAYA'$QOD
Collector:
BLAVERTY
ViaRID
Lebworks LoginlD
ARO
Reparl To
AND
Location ID:
IC44POWELL PL3
Jonathan Creek
Collect Date'.
0512312016
Priomy
ROUTINEICOC
ARO
Called Time'.
19_09
Sample Matrix:
SURFACEWATER
YES
Sample Depth
95
Loc. Type:
Statements,
Final Report
Semple ID:
AC29419
PO Number
ARO
Data Received
06n4ri
Time Received
09_00
Lebworks LoginlD
KJIMIBON2
Delivery Method
Hand delivered
Final Report Date'.
]NH6
Report Print Gate:
01MEri
Validated
If this report is labeled preliminary report the results have not been validated.
Do not use for Regulatory purposes.
Result/
Method
Analysis
CAS# Analyte Name
PDL
Q
Unitsualifier
Reference
Date
Validated
ARO
- BOD, 5 -Day In liquid
2.0
95
m91L
APHAS210B
525/18
ESTAFFORDI
Residue—Suspended in liquid
6.2
34
bol
APHA2549G-20th
51
ESTAFFORDI
Sample temperature at receipt by lab
23
°C
5124/10
RBYRD
Total Dissolved Solids in liquid
12
296
mill
APHA2540C-18 H
5127116
ESTAFFORDI
Turbidity
1
44
NTU
APHA2130D-20th
1 5125116
ESTAFFORDI
I
WSS Chemiatry LahoratoM' 1623 Mail Service Carley Raleigh, NC 2]899-1923(919)]33-3998
Net Detected" or 'U' does not indicate the sample Is analyte time but that the analyle is not detected at or above the PCL.
Page 1 of 1

AC29332 North Carolina Division of Water Resources Water Sciences Section Laboratory Results
Lod. Dead,.:
POWELL LUMBER4595
JONATHAN CREEK ROAD, WAYNESVILLE
mea
County:
Hivvmdd
Collector.
BLAVERTY
VisitlD
PL2
Region.
ARO
Radii
ARO.
Loralmn ID:
IC44POWELL
River Basin
Jonathan Creek
Collect Data
05232016
Priority
ROUTINE
Emergency
0.01U
CollectTime:
14_43
Sample Matrix:
SURFAOEWATER
COC Yes1N0
g
Sample Depth
NA
Led. Type:
st,mm ler
LOWER- S?ORAri7E/L 1`40 Final Report
Sample ID.
AC29332
PO Number #
mea
nate Radeved
061262016
Time Received
00_20
Li bworke LoginlD
Mail
Delivery Method
NC Coal
Final Report Data
6123116
Report Print Date:
07,0612016
0,02 D
hil N
If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes.
Result( Units Method Analysis
CAS# Aral Name - P L Qualifier Reference Date Vali
LAB
Sample temperature at receipt by lab 1.6 °C
5/25116 TASCENZ01
Chemical Oxygen Demand in liquid.
20
NUT
mea
Hach 6060
B/2/16
DOREEN
NI -13 a9 N In liquid
0.02
0.02
uni N
EPA 350.1 REV 2
5/25/16
DOREEN
Nitrate as N in liquid
0.62
0,02 D
hil N
EPA 353.2 REV 2,
Si
CGREEN
Nitrite as N in liquid
0.01
0.01U
nalLaeN
EPA 353,2 REV
525/16
DOREEN
NOP+1103 as N In liquid
0.02
0.02U
miasN
EPA 3532 REV
525W16
DOREEN
Phosphorus total a8 P In liquid
0.02
0.20
mg/Las P
EPA 365.1 REV 2
5/31/16
COREEN
Total Neldahl N as N in liquid
0.2
2,0
mglLae N
EPA 351.2 REV 2
6/3/16
CORDER
Chemical Oxygen Demand in liquid.
20
170
mea
Hach 6060
B/2/16
DOREEN
Grease and Oil In liquid
10
10 U,J3
ni
EPA 166,re
5/26/16
DOREEN
Bromide
0.4
0.4U
mi
EPA 300.0 rav21
rectors
DOREEN
Chloride
1.0
9.9
ni
EPA 300.0 mer2.1
5/25/16
DOREEN
Fluoride
0.4
0.4U
mg1L
EPA 300.5 reap
525/16
DOREEN
Sulfate
2.0
6.0
mglL
EPA 300.0 rev2.1
5/25/16
DOREEN
Phenolics—Total In liquid
10
420
ul
EPA4204 REV
6/8116
DOREEN
Semivolattle Organics (BNAs) in liquid
83-32-9
Acenaphthene
10
Not detected
Jl
ug1L
EPA62518270D
6/3/16
CJOHNSON
208-96-8
Acenaphthylene
20
Not detected
Jl
ug/L
EPA62518270D
6/3/16
CJOHNSON
62-53-3
Aniline
10
Not detected
J1
ug1L
EPA62518270D
0/3/18
CJOHNSON
120'12-7
Anthracene
20
Not detected
Jl
ul
EPA62518270D
613/16
CJOHNSON
benzeneacetlo acid
11
N1
ug1L
EPA62518270D
613/16
CJOHNSON
56-55-3
Benzo a)anthracene
20
Not detected
J1
ul
EPA62518270D
6/3/16
CJOHNSON
50.32-8
Benzo(a)pyrene
10
Not detected
J1
ug/L
EPA62518270D
6/3/16
CJOHNSON
205-99-2
Benzo(b)huomnthene
10
Not detected
J1
ug/L
EPA62518270D
6/3116
CJOHNSON
191-24-2
Benzo(g,h,i)perylene
20
Not detected
JI
ug1L
EPA625/8270D
8/3/16
CJOHNSON
207-08-9
Benzo(k)0uoranthene
30
Not detected
Jl
ug/L
EPA62518270D
613116
COHNSON
6505-0
Benzoic acid
50
68
us-
j EPA62518270D
613/16
CJOHNSON
10051-6
Benzyl alcohol
30
Not detected
ug/L
EPA62518270D
f
613/16
CJOHNSON
111-91-1
BIs(2-Chlomethoxy)methane
10
Not detected
J1
uv-
EPA62518270D
8/3/16
CJOHNSON
11144-4
BIS(2-chlomethyl)ether
10
Not detected
Jl
ug/L
EPA62518270D
613/16
CJOHNSON
39638-32-9
BIs(2-Chlomisopropyl)ether
10
Not detected
J1
uglL
EPA62518270D
Warta
CJOHNSON
117-81-7
Bis(2-ethylhexyl)phthalate
30
Not detected
Jl
ug1L
EPA62518270D
03/16
CJOHNSON
WSS Chemiatry Laboratory+> 1623 Mall Service Center, Raleigh, NC 27899-1622 [phone]
"Not Detected" or"U" does not indicate the ample is and" free but Marine analyte Is not detected at Or above the PCL.
Page 1 of 6

NC rDgt% LaborotmySection 4ZF .Cts/Sarapfe Comments/Qun6jier(Definitzons
Sample ID: AC29332
Result/ Method Analysis
101553
"" - I — — .-
Bromophenyl phenyl ether, 4-
10
ualifier
Not detected J1
units
ug/L
Reference
EPA62SM270D
Date
613116
Widened
CJOHNSON
85-68-7
Butylbenzyl phthalate
10
Not detected J1
ug/L
EPA625/8270D
613116
CJOHNSON
59-50-7
Chloro -3 -methyl phenol, 4-
10
Not detected
ng/L
EPA62SM270D
613116
CJOHNSON
106-47-6
Chloroanlline, 4-
10
Not detected A
ug/L
EPA625/8270D
613116
CJOHNSON
Bt -58-7
Chloronaphthalene, 2-
10
Not detected J7
ug1L
EPA62518270D
613116
CJOHNSON
95-57-8
Chlorophenol, 2-
10
Not detected
ug/L
EPA62518270D
613116
CJOHNSON
7005-72-3
Chlorophenyl phenyl ether, 4-
20
Not detected J1
ug/L
EPA625/8270D
613116
CJOHNSON
218-01-9
Chrysene
20
Not detected J1
uglL
EPA62518270D
813116
CJOHNSON
53-70-3
Dibenzo(a,h)anlhracene
20
Net detected J7
u9/L
EPA62518270D
613116
CJOHNSON
132-64-9
Dlbenzofuran
20
Not detected J7
ug/L
EPA62WB270D
W3/16
CJOHNSON
95-50-1
Dichlorobenzene, 1,2-
10
Net detected J7
u9/L
EPA62518270D
613116
CJOHNSON
541-73-1
Dichlorobenzene, 1,3
10
Not detected J7
ug1L
EPA62&8270D
613/16
CJOHNSON
10&46-7
Dichlorobenzene, 1,4-
10
Not detected J1
ug/L
EPA62518270D
Want,
CJOHNSON
91-94-1
Dichlerobenzldlne, 3,3'-
30
Not detected J7
u9/L
. EPA62518270D
613116
CJOHNSON
120.83-2
DIChlorophen01, 2,4-
10
Not detected
ug/L
EPA6251B270D
.i Want,
CJOHNSON
8466-2
Diethyl phthalate
20
Not detected J7
ug/L
EPA62518270D
6/3/16
CJOHNSON
131-11-3
Dimethyl phthalate
10
Not detected J7
ug/L
EPA62518270D
Rohn
CJOHNSON
10567-9
Dimethylphenol, 2,4-
10
Not detected
ug/L
EPA62518270D
6/3/16
CJOHNSON
84-74-2
Di -n -butyl phthalate
20
Not detected J7
ug/L
EPA625/8270D
613/16
CJOHNSON
534-52-1
Dinitro-2-methyl phenol, 4,6-
50
Not detected
uglL
EPA62518270D
6/3/16
CJOHNSON
51-28-5
Dlnitropheltel, 2,4-
50
Not detected J2
ugll-
EPA62518270D
613/16
CJOHNSON
121-14-2
Dinitrotoluene, 2,4-
20
Not detected J7
uglL
EPA625I8270D
6/3/16
CJOHNSON
606-20-2
Dlnllrotoluene, 2,6-
10
Not detected J1
uglL
EPA625/SVOD
613116
CJOHNSON
117-84'6
Di-n-octyl phthalate
10
Not detected J7
.,IL
EPA625182701)
&3/16
CJOHNSON
286-44-6
Fluoranthene
20
Not detected Jl
ug/L
EPA62WB270D
8/3/16
CJOHNSON
. ,.. 86-73-7.:
F111orene"-"- - - -
20
Not detected Jl
ug/L
EPA52WO270D
8/3/16
CJOHNSON
118-741
HBxachlorobenzene
20
Not detected J1
uglL
EPA62NB270D
6/3/16
CJOHNSON
87-68-3
Hexachlorobutadmne(SV)
10
Not detected J1
ug/L
EPA62USVDD
6/3116
CJOHNSON
77-474
Hexachlorocyclopentadiene
10
Not detected J1
1191E
EPA62WB270D
813115
CJOHNSON
67-72-1
Hexachloroethane
10
Not detected Jl
ug /L
EPA62518270D
6/3116
CJCHNSON
hydrocinnamic acid
520 N1
ug/L
EPA52&8270D
613116
CJCHNSON
193-39-5
Indeno(1,2,3-Cd)pyrene
20
Not detected Jl
eg/L
EPA625/8270D
813116
CJOHNSON
76-59-1
laophorone
10
Not detected J1
ug/L
EPA82WB270D
613116
CJOHNSON
methyl pentanoic acid
14 N1
eg/L
EPA625162701)
613116
CJOHNSON
9157-6
Methylnaphthalene, 2-
10
Not detected J1
ug/L
ERA621Y8270D
613116
CJOHNSON
methylphenol
130 N1
ug1L
EPA625182700
tore
CJOHNSON
9548-0
Methylphenol, 2-
10
Not detected
ug1L
EPA62&8270D
613116
WOHNSON
106-44-5
Methylphenol, 4-
10
Not detected
ug1L
EPA62518270D
&3116
CJOHNSON
91-20-3
Naphthalene(SV)
10
Not detected Jl
ug1L
EPA62518270D
613116
CJOHNSON
66-74-4
Nitroaniline, 2-
10
Not detected J7
ug/L
EPA625M270D
613116
CJOHNSON
99-092
Ndroanlllne, 3-
50
Not detected J7
ug/L
EPA625/8270D
613116
CJOHNSON
100-01-6
Nltmaniline,4
50
Not detected Jl
ug/L
EPA62518270D
613116
CJOHNSON
98-953
Nitrobenzene
10
Not detected J7
u9/L
EPA62518270D
613116
CJOHNSON
WSS Chemiatry LabomtoM' 1623 Mail aeraica Center, Raleigh, NO 27699-1623 [phone]
"Not Detected"or"0"does not indicate the sampleis analyte free but that the aht. is not detected at or shove the PCL.
Page 2 of 6

NCO`hNF, Comments/Qpalifi'er4Jefinitiwu
Semple IDAC29332
Result/ Method Anal
88-75-5
NltrOphenol, 2-
10
ualifier
Not detected
Units
u9IL
Reference
EPA625/8270D
Date
8/3/16
vel
[JOHNSON
10002-0
Nltrophenol, 4-
50
Not tletectetl
u Jl-
EPA02518270D
6/3/16
CJOHNSON
621-64-7
N-nitrosodi-n-propylamime
10
Not detected J1
u9IL
EPA625/8270D
6/3/16
CJOHNSON
06-30-6
N-nitrosodiphenylamine
10
Not detected J1
u9IL
EPA525/8270D
8/3/16
CJOHNSON
87-86-5
PentachlOropheool
30
Not detected
u9IL
EPA625/8270D
6/3/16
CJOHNSON
85at8
Phenanthrene
20
Not detected J1
uglL
EPA625/8270D
8/3/16
[JOHNSON
108-95-2
Phenol
10
110
u9IL
EPA62518=
6/3/16
GJOHNSON
126-000
pyrene
20
Not detected JI
uglL
EPA825/8270D
9/3/18
CJOHNSON
120-82-1
Trichlorobenzene, 1,2,4-
10
Not detected J1
u9IL
EPA625/8270D
6/3/16
[JOHNSON
05-95-4
Trichlorophenol, 2,4,5-
10
Not detected
u,IL
EPAS25/8270D
WW16
GJOHNSON
68-08-2
Trichlorophenol, 2,4,0-
10
Not tleleCletl
uglL
EPA625/8270D
8/3/16
[JOHNSON
.12,4-Trimethyl benzene - -
Valerlc acid
Not detected
12 N1
ugf-
EPA625/8270D
WAS
CJOHNSON
10693-4
(EDB)1,2-Dlbromoethane
VOL
Volatile Organics in liquid
1.0 Not detected
ug/L
EPA824l9280C
.15/27/19
CJOHNSON
6301
1,1,1,2 -Tetrachloroethane
1.0
Not detected
ug/L
EPA624IBZ60C
5/27/16
CJOHNSON
71-55-6
1,1,1 -Trichloroethane
1.0
Not detected
u9IL
EPA524I5260C
5/27/16
OJOHNSON
79-345
1,1,2,2 -Tetrachloroethane
1.0
Not detected
ug/L
EPA62VO260C
5/27/16
CJOHNSON
78005
1,1,2 -Trichloroethane
1.0
Not detected
ug-
EPAB248260C
5127/16
CJOHNSON
75-343
1,1-Dlchlomelhane
1.0
Not detected
ug/L
EPA62VO260C
5/27/16
CJOHNSON
75-354
1,1-Dlchlomethene
1.0
Not detected
ug/L
EPA524/82600
5/27/16
CJOHNSON
56158-6
1,1-Dichloropropene
1.0
Not detected
uglL
EPA52418250C
.5127/16
CJOHNSON
87-61-6
1,2,3-Tpchlorobenzene
1.0
Not detected
ug/L
EPA624A82600
5127/16
CJOHNSON
98-164
1,2,3-Trichloropropane
1.0
Not detected
ugi
EPA62418250C
927/16
aOHNSON
120-92-1
1,2,4-Trichlorobenzene
1.0
Not detected
ug/L
EPA624/8260C
5127116
CJOHNSON
95618
.12,4-Trimethyl benzene - -
- -t-..0---:
Not detected
- u9IL
_EPA62418260C
927/16
...[JOHNSON ...
96-12-8
1,2-Dibrgmo-3-Chloropropane
2.0
Not detected
og/L
EPA624I8360G
51127116
CJOHNSON
107-08-2
1,2-Dichloroethane
1.0
Not detected
u9IL
EPA624/8260C
5127116
CJOHNSON
78-87-5
1,2-Dichicropropane
1.0
Not detected
ug/L
EPA624/8260C
5127/16
CJOHNSON
108-67-8
1,3,5-Trimethylbenzene
1,0
Not detected
ug/L
EPA62418260C
5127116
CJOHNSON
142-28-9
1,3-Dichloropropane
1.0
Not detected
u9/L
EPA624/8260C
5127/16
CJOHNSON
594-20-7
2,2-Dichloropropane
2.0
Not detected
u9I1-
EPA62418260C
5127116
CJOHNSON
95-49-8
2-Chlorotoluene
1.0
Not detected
ug/L
EPA62418260C
927116
CJOHNSON
106-43-4
4-Chlorotoluene
1.0
Not detected
u9IL
EPA62418260C
5127116
CIOHNSON
71-43-2
Benzene
1.0
Not detected
ug/L
EPA62418260C
5127/16
CJOHNSON
108-86-1
Bromobenzene
1.0
Not detected
uglL
EPA62418260C
927116
CJOHNSON
74-97-5
Bromorchloromelhane
1.0
Not detected
u9IL
EPA62418260C
5127/16
CJOHNSON
75-27-4
Bromodichloromethane
1.0
Not detected
ug)L
EPA62418260C
N27116
CJOHNSON
75-25-2
Bromoform
2.0
Not detected
u9IL
- EPA624/8260C
927115
CJOHNSON
74-03-9
Bromomethane
2.0
Not detected
ug/L
EPA62418260C
5127/16
CJOHNSON
55-23-5
Carbon Tetrachloride
1.0
Not detected
ugf-
EPA524/82600
927/15
CJOHNSON
1081
Chlorobenzene
1.0
Not detected
ug/L
EPAS24/8260C
927/16
CJOHNSON
75-00.3
Chloroethane
2.0
Not detected
u9IL
EPAS24/8260C
5/27/16
[JOHNSON
Was opened, Laborai 1623 Mall S.M. center, Raider, NC 276984623 (919) 7334908
"Not Detected' of does not indicate the sample is analyte free but that the analyte is not detected at or above Ne POL.
Page 3 of 6

NC0'4NR. Ggbameory Section 4(�.mCte/SampCe Comment/QuafifierrDefinitioru
Sample 10: AC29332 -
ResulU Method Analysis
67-66-3
Chloroform
1.0
Qualifier
Not detected
Units
ug/L
Reference
EPA62418260C
Date
52]/16
Validated V
CJOHNSON
74-87-3
Chloromethane
2.0
Not
detected
iSIL
EPAS241826OG
5/27/16
CJOHNSON
156-59-2
cis-1,2-Dichloroethene
1.0
Not
detected
ug/L
EPAS2418260C
5/27/18
CJOHNSON
10061-01-5
cis-1,3-Dichloropropene
20
Not
detected
u9IL
EPAS24/82600
.5/27/16
CJOHNSON
124-48-1
Dibromochloromethane
2.0
Not
detected
ug/L
EPA62418260C
527/16
CJOHNSON
74-95-3
Dibromomethabe
1A
Not
detected
ug/L
EPAS2418260C
27/16
CJOHNSON
75-71-6
Dichlorodifluoromethane
2.0
Not
detected
ug/L
EPAS2418260C
5/27/16
CJOHNSON
100-41-4
Ethylbenzene
1,0
Not
detected
ug/L
EPA624/8260C
5127118
CJOHNSON
87-68-3
Hexachlorobutadene
1.0
Not
detected
u9IL
EPA62418260C
5127/16
CJOHNSON
98-82-8
Isopropylbenzene
1.0
Not
detected
u9IL
EPA62418260C
5127116
CJOHNSON
108-3e-3
m,p-Xylene
2.0
Not
defected
uiy-
EPA62418260C
5127/16
CJOHNSON
541-73-1
m-Dichlorobenzene(1,3)
1.0
Not
detected
uglL
EPA624/8260C
N27116
CJOHNSON
1634-04-4
Methyl Tert-Butyl Ether
1.0
Not
detected
ug/L
EPA62418260C
5127/16
CJOHNSON
75-09-2
Methylene Chloride
1L
Not
detected
u9IL
.EPA62418260C
027116
CJOHNSON
91-20-3
Naphthalene
2.0
Not
detected
ug/L
EPA62418260C
5127/16
CJOHNSON
104-51-5
n-Batylbenzene
L0
Not
detected
u9IL
EPA62418260C
U27116
CJOHNSON
103-65-1
n-Propylbenzene
1.0
Not
detected
ug/L
EPA624/8260C
5127116
CJOHNSON
95-50-1
o -Dichlorobenzene (1 2)
1.0
Not
detected
ug/L
EPA62418260C
5127116
CJOHNSON
95-47-6
o -Xylene
1.0
Not
detected
u9/L
EPA624/8260C
5127116
CJOHNSON
10646-7
p-Dichlorobenzene(1,4)
1.0
Not
detected
ue/L
EPA62418260C
5127/16
CJOHNSON
99-87-6
p-isopropylloluene
1.0
0.92 N3
u9IL
EPA624/8260C
5127116
GJOHNSON
135-98-8
sec-Butylbenzene
1t0
Not
detected
ug/L
EPA62418260C
.5127116
CJOHNSON
100-42-5
Styrene
1A
Not
detected
uty-
EPA62418260C
5127116
CJOHNSON
9806-6
tart-Butylbenzene
1.0
Not
detected
ug/L
EPA62418260C
5127/16
CJOHNSON
127-1e-4
Tetrachloroethene
1.0
Not
detected
u9IL
EPA62418260C
5/27116
CJOHNSON
10908-3.-
Toluene- -
-'.10
.'44
--'ug/L
.. EPA62418260C
5127110
•CJOBNSQN,
156-60-5
trans-1,2-DIchlorcethene
10
Not
detected
ug/L
EPA62418260C
5127116
CJOHNSON
10061-02-6
trans-1,3-Dichlompropene
2A
Not
detected
u9IL
EPA62418260C
5127116
CJOHNSON
79-01-6
Trichloroethane
1.0
Not
detected
uglL
EPA62418260C
5127/16
CJOHNSON
75-694
Trichlorofluoromethane
20
Not
detected
ug/L
EPA62418260C
5127/16
CJOHNSON
75-014
Vinyl Chloride
21)
Not
detected
ug/L
EPA62418260C
5/27/16
CJOHNSON
WSS chemist, Laboratory» 1623 all Sellce Cenleq Ralelgb, NC 27889-1623 (818) 7333908
NmDai m' T Eees not inbirate the sample Is analyte free but that the analyte is not detected at or above the POL.
Page 4 of 6

X D'WIR, Laboratory Section %,,a[dSavv le CommesulQya[ifin-Definitions
Sample ID: AC29332
Result/ Method Analysis
Qualifier Units Reference Date validated
sammecamments
I-Estimated-LFM recovery was 59% due to m ll interference.
estimatedleveltoo low to permit separate pupiticatien',
is less than the laboratory PCL limit and greeter than the
analyte felled < LCL in this CV2.
Identified by MS library eeerch
NCDEQ-WSS-Chemistry Lab Data Qualifiers
Al The reported value is an average, where at least one result is qualified with a "U". The PQL is used for the qualified result(S) to cal
B1 Coliform -Countable membranes with less than 20 colonies. Reported value is estimated or is a total of the counts on all fillers repo
B2 Coliform -Counts from all filters were zero. The value reported is based on the number of colonies per 100 ml that would have been
B3 Coliform -Countable membranes with more than 60 or BO colonies. The value reported is calculated using the count from the smalls
B4 Coliform -Filters have counts of both 160 or BO and <20. Reported value is estimated or is a total of the counts on all filters reported
B5 Coliform -Too many colonies were present, too numerous to count (TNTC). TNTC is generally defined as>150 colonies.
B6 Coliform -Estimated Value. Blank contamination evident.
B7 Coliform -Many non -coliform or non -enterococcus colonies or interfering non -coliform or non -enterococcus growth present. In this o
BB1 MPN-No wells or tubes gave a positive reaction. Value based upon the appropriate MPN Index and reported as a less than't'va1L
3132 MPWAII wells or tubes gave positive reactions. Value based upon the MPN Index and reported as a greater than ">" value.
C Total residual chlorine was present in sample upon receipt in the laboratory; value is estimated.
G1 BOD -The dissolved oxygen (DO) depletion of the dilution water blank exceeded 0.2 mg/L.
62 BOD -The bacterial seed controls did not meet the requirement of a DO depletion of at least 2.0 mg/L and/or a DO residual of at lea
G3 ___.. BS)D No.sample dilution met the requirement of a:DO depletion of at (aast,2.Qmg/Land/of.a DO residual of at least 1.0 mg/L., _.
G4 BOD -Evidence of toxicity. This is generally characterized by a significant increase in the BOD value as the sample concentration or
G5 BOD -The glucose/ glutamic acid standard exceeded the range of 196 3 30.5 mg/L.
G6 BOD -The calculated seed correction exceeded the range of 0.6 to 1.0 mg/L.
G7 BOD -Less than 1 mg/L DO remained for all dilutions set. The reported value is an estimated greater than value and is calculated fc
Ge BOD -Oxygen usage is less than 2 mg/L for all dilutions set. The reported value is an estimated less than value and is calculated to
G9 BODTheDO depletion of the dilution water blank produced a negative value.
11 Surrogate recovery limits have been exceeded.
J2 The reported value failed to meet the established quality control criteria for either precision or accuracy.
J3 The sample matrix interfered with the ability to make any accurate determination.
J4 The data is questionable because of improper laboratory or field protocols (e.g., composite sample was collected instead of grab, If
J5 Temperature limits exceeded (samples frozen or WC) during transport or not verifiable (e.g., no temperature blank provided): non
J6 The laboratory analysis was from an unpreserved or improperly chemically preserved sample. The data may not be accurate.
J7 This qualifier is used to identify analyte concentration exceeding the upper calibration range of the analytical instrument/method. TI
JB Temperature limits exceeded (samples frozen or >6-C) during storage, the data may not be accurate.
J9 The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concentration
J10 Unidentified peak; estimated value.
ill The reported value is determined by a one -point estimation rather than against a regression equation. The estimated concenlralior
J12 The calibration verification did not meet the calibration acceptance criterion for field parameters.
M Sample and duplicate results are "out of control". The sample is non-homogenous leg., VOA soil). The reported value is the lower
N1 Presumptive evidence and estimated value. The component has been tentatively identified base on mass spectral library.
N2 There is an indication that the analyte is present, but quality control requirements for confirmation were not met (i.e., presence of'.
N3 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the Iabc
N4 This code shall be used if the level is too low to permit accurate quantification, but the estimated concentration is less than the all
N5 The component has been tentatively identified based on a retention time standard.
Q1 Holdino time exceeded urian to receipt by lab.
WSs chemistry Laboratory» 1623 Mall Service Center, Ralel9b, NC 27699-1623 [phone]
'her Detested' or "P' does ma ndeate the sample is enols. free but that the analyte is not detected at or above the PQL.
Page 5 of 6

NC m'W+R. Laboratory Section P�euCtr/Somp(e Comments/QuaC�tDefinitimu
Sample ID: AC29332
CAS# A..lut. Nem. pint
.yuuucci_ .cicicu..c ._.,
Q2 Holding time exceeded following receipt by lab.
P Elevated PQL` due to matrix interference and/or sample dilution.
S Not enough sample provided to prepare and/or analyze a method -required matrix spike (MS) and/or matrix spike duplicate (MSD).
U Indicates that the analyte was analyzed for but not detected above the reported practical quantitation limit". The number value repo
X1 Sample not screened for this compound.
X2 Sampled, but analysis lost or not performed-feld error.
X3 Sampled, but analysis lost or not performed -lab error.
V Indicates the analyte was detected in both the sample and the associated method blank. Note: The value in the blank shall not be s
Y Elevated PQL" due to insufficient sample size.
Z1 Inability to analyze the sample.
W33 Chemistry Laboratory» 1623 Men Sands. Center, SeleiBh, NC 276991623 (919) 9334988
"Not calectetl" or "U" does not indicate the sample Is anaym tree but that the analyte is net detected at or ebwe the PQL.
Page 6 of 6

Loc. Oeecr.:
County.
Regicn'.
River Basin
Emergency
COC Yes1No
HAYWOOD
ARO
Jonathan Crack
YES
Collector'.
AC29418
Report To
ARO
Collect Date:
0612312016
Collect Tlme:
14_43
Sample Depth
Stor=water
UaillD
AC29418
Location ID,
1CAMPOWELL PL2
Pnably
ROUTINEICOO
Sample Matrix:
SURFACEWATER
Loc Type:
Stor=water
Sample ID:
AC29418
PO Number#
ARO
Data Received:
MoNli
Time Received
09:no
Lusa Un mID
H IMMIS N2
Delivery Method
Hand delivered
Final Report Date:
711116
Report Print Date:
%10652016
WSS Chemistry Laboxtuni 1623 Mail service Centeq Raleigh, NC 27699-1623 (919) 7334908
"Not Detected" or"U" done not indicate the sample is analyte free butthat Ne analyte is not detached at or above the POL.
Page 1 of 1
Final Report
If this reports labeledprelimrnary report, the results have not been validated.
Do not use for Regulatorypurposes.
Result/
Method
Analysis
CAS # Analyte Name
PSC _L Qualifierr
Units
Reference
Data
veli
ARO
BOD, 5 -Day in liquid
2.0 120
nglL
APHAS210B
5125116
ESTAFFORDI
Residue—Suspended in liquid
6.2 64
mg1L
APHA2540D-20th
512V16
ESTAFFORDI
Sample temperature at receipt by lab
2.3
"c
5124116
RBYRD
Total Dissolved Sonde In liquid
12 245
ng1L
APHN254cC-10TH
5127116
ESTAFFORD1
Turbidity
1 43
NTU
APHA213OB-2011
5125116
ESTAFFORDI
WSS Chemistry Laboxtuni 1623 Mail service Centeq Raleigh, NC 27699-1623 (919) 7334908
"Not Detected" or"U" done not indicate the sample is analyte free butthat Ne analyte is not detached at or above the POL.
Page 1 of 1

8081 GCB Pesticides, TCLP
gamma -BHC (Lindane)
Chlordane(Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachindmiphenyl IS)
Tetrachloro-m-xylene IS)
8151 Chlorinate Herbicide TCLP
2,4-0
2,4,5-TP(Silvex)
Surrogates
2,4-DCAA(S)
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium ..
Lead
Selenium
Silver
6010 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, BAR
Sodium Adsorption Ratio
7470 Memory, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4 -Dichlorobenzene
2,4-Dinitrololuene
Hexachlom-1,3-butadiene
Hexachlorobenzene
Date: 11/22/201612:52 PM
Analytical Method: EPA8081 Preparation Method: EPA3510
Leachate Methodl0ate: EPA1311; 11/11/1618:00
ND
ug/L
0.50 1
11/15/1609:22
11/16/162108
58-89-9
NO
Pane Analytical Services, LLC
a4eM,i�l y(11®N
11/15/160922
11/1611621:08.
3335 RivC 2Cf
gnM1eville, NC 38e04
mNyIOOMbatuy
ug/L
0.50 1
[phone]
WAs7EWflTG2
W&Fcyelt
'6
ug/L
0.50 1
11/15/1609:22
ANALYTICAL RESULTS
76-44-8
Project: PCvre1l6-PI101-1A
ug/L
0.50 1
11/15/1609:22
Pace Project Ni 92318984
102457-3
ND
ug/L
Sample: POND
Lab ID: 92318984001 Collected: 11/08/1613:00
Received 11/08/161510 Matrix: Water
Parameters
Results
Units Report Limit DF
Prepared Analyzed CAS No, Qual
8081 GCB Pesticides, TCLP
gamma -BHC (Lindane)
Chlordane(Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Surrogates
Decachindmiphenyl IS)
Tetrachloro-m-xylene IS)
8151 Chlorinate Herbicide TCLP
2,4-0
2,4,5-TP(Silvex)
Surrogates
2,4-DCAA(S)
6010 MET ICP, TCLP
Arsenic
Barium
Cadmium
Chromium ..
Lead
Selenium
Silver
6010 MET ICP
Calcium
Magnesium
Sodium
Sodium Adsorption Ratio, BAR
Sodium Adsorption Ratio
7470 Memory, TCLP
Mercury
8270 MSSV TCLP Sep Funnel
1,4 -Dichlorobenzene
2,4-Dinitrololuene
Hexachlom-1,3-butadiene
Hexachlorobenzene
Date: 11/22/201612:52 PM
Analytical Method: EPA8081 Preparation Method: EPA3510
Leachate Methodl0ate: EPA1311; 11/11/1618:00
ND
ug/L
0.50 1
11/15/1609:22
11/16/162108
58-89-9
NO
ug/L
3.0 1
11/15/160922
11/1611621:08.
57-74-9
ND
ug/L
0.50 1
11/15/1609:22
11/16/162108
72-20-8
NO
ug/L
0.50 1
11/15/1609:22
11/1611621:08
76-44-8
ND
ug/L
0.50 1
11/15/1609:22
11/16/162108
102457-3
ND
ug/L
1000 1
11/1511608:22
"11/1611621:08
72-43-5
ND
ug/L
30 1
11/151160922
11/1611621:0818001-35-2
-
49
%
10-138 1
11/15/1609:22
11/161162108
2051-24-3
60
%
10-110 1
11/15/160922
11/16/162108
877-09-8
Analytical Method:
EPA 8151 Preparation Method. EPA3510
NO
bol
0.010 1
11/1]/1608:50
11/19/1601:55
94-75-7 L3,M0
ND
mi
0.010 1
11/1]/1608:50
11/19/1601:55
9372-1
104
%
39-139 1
11/1]/1608:50
11/19/1601:55
19719-28-9
Analytical Method:
EPA6010 Preparation Method: EPA3010A
Leachate Method/Date:
EPA 1311;
11/09/1618:30 Initial
pH: 2.4; Final pH: 2.4
NO
mg/L
0,050 1
11/10/161]:48
11111/1611:14
]440-38-2
ND
mg/L
0.25 1
11/10/161]:48
11111/1611:14
7440-39-3
NO
mg/L
0.0050 1
11/10/161]48
11111/1611:14
7440-43-9
ND-.,--.mg/L
.0.056 1
.11/10/1617:4811111/1611:14.]4404]3
-
ND
mg/L
0.025 1
11/10/161748
11111/1611:14
7439-92-1
NO
ni
0.10 1
11/10/1617:48
11/11/1611:14
7782-49-2
ND
ni
0025 1
11/10/161]:48
11/11/1611:14
7440-22-4
Analytical Method:
EPA6010 Preparation Method: EPA3010A
28300
ug/L
100 1
11110/1619:05
11/12/1600:42
7440-70-2
8870
all
100 1
11/10/1619:05
11/1211600:42
7439-95-4
5520
ug/L
5000 1
11/10/161905
11/12116 00 42
7440-23-5
Analytical Method
: EPA6010
0.23
meg/L
1
11/15/160654
N2
Analytical Method:
EPA 7470 Preparation Method: EPA 7470
Leachate Method/Dale:
EPA 1311;
11/0911618:30 Initial
pH: 2.4; Final pH: 2.4
NO
mg/L
0.00020 1
11/11/160735
11/1111616:16
7439-97-6
Analytical Method:
EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date:
EPA 1311;
11/11/1616:00
NO
ug/i-
500 1
11/15/1608:00
11/15/1615:12
106-46-7
NO
uglL
500 1
11/15/1608:00
11/15/1615:12
121-14-2
NO
uglL
50.0 1
11/15/1608:00
11/15/1615:12
87-68-3
NO
uglL
50.0 1
11/15/1608:00
11/15/1615:12
118-74-1
REPORT OF LABORATORY ANALYSIS
This mpod shall not be reproduced, except in full.
without the written consent of Pace Analyfical Services, LLC. Page 4 of 40

xWn'p¢vN640 Pf..
ANALYTICAL RESULTS
Pace Analytical Servic05, LLC
2225 Riverside Dr.
AsheNlle, NC 28804
[phone]
Project: Powell 6 -P1101 -1A
Pace Project No.: 92318984
Sample: POND
Lab ID: 92318984001 Collected: 11/08/1613:00
Received 11/08/161510 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared
Analyzed
CAS No, Qual
8270 MSSV TCLP Sep Funnel
Analytical Method:
EPA 8270 Preparation Method:
EPA 3510
Leachate Method/Date: EPA 1311; 11/11/1616:00
Hexachlomelhane
ND
ugi
50.0
1
11/15/16 08:00
11/15/16 15:12
67-72-1
2-Methylphenol(o-Cresol)
ND
ug/L
50.0
1
11/15/16 08:00
11/15/16 15:12
95-48-7
3&4-Melhylphenol(m&p Cresol)
ND
ug/L
50.0
1
11/15/16 08:00
11/15/16 15:12
Nitrobenzene
NO
ug/L
560
1
11/15/16 08:00
11/15/16 15:12
98-95-3
Pentachlorophenol
ND
ug/L
100
1
11/15/16 08:00
11/15/16 15:12
87-86-5
Pyridine
ND
ri
50.0
1
11/15/160800,11/15/16,15:12
110-86-1
2,4,5 -Trichlorophenol
NO
ug/L
50.0
1
11115/16 08:00
11/15/16 15:121
95-95-4. -
2,4,6-Trichlomphenol
NO
ug/L.
50.0
1
11/15/16 08:00
11/15/16 15:12
88-06-2
Surrogates
Nitrobenzene-d5(S)
65
%
12-102
1
11/15/160800
11/15/1615:12
4165-60-0
2-Fluorobiphenyl(S)
57
%
13-107
1
11/15/16 08:00
11/15/1615:12
321-60-8
Terphenyl-dl4(S)
77
%
21-132
1
11/15/16 08:00
11/15/1615:12
171551-0
Phenol-d6(S)
30
%
10-110
1
11/15/160800
11/15/1615:12
13127-88-3
.'2-Fluorophenol(S)
38
%
10-110
1
11115/16 08:00
11/1511615:12
367-12-4
2,4,5Tribromophenol(S)
75
%
27-108
1
11115/16 08:00
11/15/1615:12
11849-6
8280 MSV TCLP
Analytical Method
: EPA 8260
Leachate Method/Date: EPA 1311; 11/11/160621
Benzene
NO
ug/l.
100
20
11/1411616:49
71-43-2
2-Butanone(MEK)
ND
ug/l.
200
20
11/1411616:49
78-93-3
Carbon tetrachloride
ND
ug/L
100
20
11/14/1616:49
56-23-5
Chlorobenzene
ND
ug/l.
100
20
11/1411616:49
108-90-7
Chloroform
ND
ug/L
100
20
11/14/16 16:49
67-66-3
-.. 1,4 -Dichlorobenzene .....,.
- ND
ug/L
100
20
11/14/1616:49
106-46-7
1,2-Dichloroethane
ND
ug/l.
100
20
11/14116 16 49
107-06-2
1,1-Dichloroethene
ND
ug/L
100
20
11/14/1616:49
75-354
Tetrachlomethene
ND
ug/L
100
20
11/14/1616:49
127-18-4
Trichloroethene
ND
ug/l-
100
20
11/14/16 16 49
79-01-6
Vinyl chloride
ND
ug/L
100
20
11/14/1616:49
75-014
Surrogates
1,2-Dichloroethane-d4(S)
99
%
70-130
20
11/14/1616:49
17060-07-0
Toluene-d8(S)
104
%
67-135
20
11/14/1616 49
2037-26-5
4-Bromofluombenzene(S)
102
%
70-130
20
11/14/1616:49
460-004
8260 MSV Low Level
Analytical Method
: EPA8260
Acetone
ND
ug/L
25.0
1
11/1111613:44
67-64-1
Benzene
ND
ugll-
1.0
1
11/11/1613:44
7143-2
Bromobenzene
ND
uglL
1.0
1
11/11/1613:44
108-86-1
Bromochlommethane
NO
ug/l-
1.0
1
11/11/1613"
74-97-5
Bromodichloromethene
ND
ug/l-
1.0
1
11/11/16 13:44
75-27-4
Bromoform
ND
ug/L
1.0
1
11/11/16 13:44
7525-2
Bromomethame
ND
ug/L
2.0
1
-
11/11/1613:44
74-83-9
2-Butanone(MEK)
ND
ugi
5.0
1
r
11/11/1613:44
78-93-3
Carbon tetrachloride
NO
ug/L
1.0
1
11/11/16 13:44
58-23-5
Chlorobenzene
ND
uyl-
1.0
1
11/11/16 13:44
108-90-7
Chloroethane
ND
ug/L
1.0
1
11/11/16 13:44
75-00-3
Chloroform
NO
ug/L
1.0
1
11/11/16 13:44
67-66-3
REPORT OF LABORATORY ANALYSIS
This report shall not be repcduced, except in full,
Date: 11/22/20161252 PM withoutthewntmncensentof Para Analytical Services,LLC.
Page 5 of 40

(� Pace Analytical Services, LLC
a{reAnalyticial a2325 RiversideC
Asheville, NGOr.
2829800
rwxp¢Qal¢be eohl. [phone]
ANALYTICAL RESULTS
Project: Powell 6-PII01-1A
Pace Project No.: 92318984
Sample: POND Lab ID: 92318984881 Collected: 11/0811613:00 Received 1110811615:10 Maltlx: Water
Parameters Results Units Report Limit DE Prepared Analyzed CAS No. Qual
8260 MSV Low Level
Analytical Method:
EPA 8260
Chloromethane
ND
ug1L
1.0
1
11/11/16 13:44
74873
2-Chlomtoluene
ND
ug/L
1.0
1
11/11/16 13:44
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
1
11/11/16 13:44
106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
2.0
1
11/11/16 13:44
96-12-8
Dibromochloromethane
NO
ug/L
1.0
1
11/11/1613:44
124-48-1
1,2-Dlbromoethane(EDB)
NO
ug/L
1.0
1
11/11/1613:44
106-93-4
Dibromomethane
NO
ug/L
1.0
1
. 11/11/16 13:44
74-95-3
1,2 -Dichlorobenzene
NO
ug/L
1.0
1
11/11/16 131441
95-50-1 -
1,3 -Dichlorobenzene
NO
ug/L
1.0
1
11/11/16 13'.44
541 73-1
1,4 -Dichlorobenzene
NO
ug/L
1.0
1
11/11/16 13'.44
106-46-7
Dichlorodiiluoromelhane
NO
ug/L
1.0
1
11/11/16 13:44
75-71-8
1,1-Dichloroethane
NO
ug/L
1.0
1
11/11/16 13
44
75-34-3
1,2-Dichloroethane
NO
ug/L
1 0
1
11/11/16 1344
107-06-2
1,1-Dichloroethene
NO
ug/L
1 0
1
11/11/16 13
44
75-354
cis-1,2-Dichloroethene
NO
ug/L
1D
1
11/11/16 13:44
156-59-2
trans-1,2-Dichloroethene
NO
ug/i.
I'D
1
11/11/16 13:44
156-60-5
1,2-Dichloropropane
ND
ug/L
Ig
1
11/11/16 13:44
78-87-5
1,3-Dichlaropropane
NO
ug/L
1.0
1
11/11/16 13
44
142-28-9
2,2-Dichloropropane
NO
ug/L
1 0
1
11/11/1613:44
594-20-7
1,1-Dichloropropene
NO
ug/L
10
1
11/11/1613:44
563-58-6
cis-1,3-Dichloropropene
NO
ugll-
1.0
1
11/111161344
10061-01-5
(rens-1,3-Dichloropropene
NO
uglL
1.0
1
11/1111613:44
10061-02-6
Diisopropyl ether
ND
ug/L
1.0
1
11/1111613:44
108-20-3
-- 6thylbenzene ....
NO
ugi
10
-.4,..
,. 11/11/1613"
10041-4
Hexachloro-1,3-butadiene
NO
ugi
1D
1
1111111613:44
87-68-3
2-Hexanone
NO
ug/L
5.0
1
11111/1613:44
591-78-6
p-Isopropylloluene
ND
ugi
1.0
1
11111/16 1344
99-87-6
Methylene Chloride
ND
ug1L
2.0
1
11/11/16 13:44
75-09-2
4-Methyl-2-pentanone(MIBIO
ND
ug1L
5.0
1
11/11/1613:44
108-10-1
Methyl-tert-butyl ether
ND
ug1L
1.0
1
11 /11 /16 13:44
163404-4
Naphthalene
ND
ug/L
1.0
1
11/11/16 1344
91-20-3
Styrene
ND
ug1L
1.0
1
11/11/16 13:44
100-42-5
1, 1, 1,2-Tetrachlorooth one
ND
ug1L
1.0
1
11/11/16 13:44
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
1
11/11/16 13:44
79-34-5
Tetrschloroelhene
ND
ugi
1.0
1
11/11/16 13:44
127-18-4
Toluene
6.2
uglL
1.0
1
11/11/16 13:44
108-88-3
1,2,3-Trichlorobenzene
NO
ug/L
1.0
1
11/11/16 13:44
87-61-6
1 2,4-Trichlorobenzene
NO
ug/L
1.0
1
11/11/16 13:44
120-82-1
1,1,1 -Trichloroethane
NO
ug/L
1 0
1
11/11/16 13:44
71-55-6
1,1,2 -Trichloroethane
NO
ug/L
1.0
1
11/11/16 13:44
79-00-5
Trichloroethene
NO
ug/L
1D
1
11/11/16 13:44
79-01-6
Trichlom8uoromethane
NO
ug/L
10
1
11/111161344
75-694
1,2,3-Tdchloropropane
NO
ug/i.
1.0
1 r
11/11/16 13:44
96-184
Vinyl acetate
NO
ug/L
2.0
1
11/11/16 13:44
108-05-4
Vinyl chloride
NO
ug/L
10
1
1111111613:44
75-014
Xylene (Total)
NO
ug/L
10
1
1111111613:44
1330-20-7
m&p-Xylene
NO
ug1L
2.0
1
1111111613:44
179601-23-1
REPORT OF LABORATORY ANALYSIS
L3
This report shell not be reproduced adept in full,
Date: 11/22/201612:52 PM without the wnlen consent of Pace Analytical Ssrvbes,LLC. Page 6 of 40

y j - Pace AnelnlceI services, LLC
aceAnalXiml o 2225 Riv C 25 9r.
Asbev Ile, NC 27104
' .xMMwa Nm.. .(926)254-]96
REPORT OF LABORATORY. ANALYSIS
This reportshall not be reproduced except in full,
Date: 11/22/201612:52 PM eetr.bttb.wrder consent of Pece Analyawl service., LLC Page 7 of 40
ANALYTICAL RESULTS
Project: Powell 6 -P1101 -1A
Pace Project No.: 92318984
Sample: POND
Lab ID: 92318884001 Collected
11/08/161300
Received 11/08/161510 Matrix: Water
Parameters
Results Units Report Limit
OF
Prepared Analyzed
CAS No, Coal
8260 MSV Low Level
Analytical Method : EPA 8260
o -Xylene
NO ug/L
1.0
1
11/11/1613:44
95-47-6'
Surrogates
4-Bromofluombenzene(S)
97 %
70-130
1
11/11/161344
460-00-4
1,2-Dichlowethane-d4(S)
101 %
70-130
1
11/11/16 13:44
17060-07-0
Toluene-us(S)
100 %
70-130
1
11/11/16 13:44
2037-26 5
2540C Total Dissolved Solids
Analytical Method: SM 2540C
Total Unsolved Solids
226 mg/L
25.0
1
11/10/1613:371
4500H+ pill, Electremelric
Analytical Method : SM 4500-1-1+13
pH at 25 Degrees C
7.0 Std. Units
1.0
1
11/14/1613:42
H6
5210B BOD, 5 day
Analytical Method : SM 521013
BOD, 5day
45.0 mg/L
2.0
1
11/09/161]:54 11/14/1611:54
Total Nitrogen Calculation
Analytical Method : TKN+NO3+NO2 Calculation
Total Nitrogen
3.1 mg/L
0.12
1
11/15/1618:14
350.1 Ammonia
Analytical Method: EPA 350.11993 Rev 2.0
Nitrogen, Ammonia
NO mg/L
0.10
1
11/11/1603:18
7664-41-7
351.2 Total Kjoldahl Nitrogen
Analytical Method : EPA 351.2
...... Nitrogen, Kjeldahl, Trial
3.1 m9/L
.2.5,
5..
..........11/15/1600:15
7727-37-9
353.2 Nitrogen, N021NO3 unpms
Analytical Method: EPA353.2
Nitrogen, Nitrate
NO mg/L
0,020
1
11/08/161]:25
Nitrogen, Nitrite
0.11 mg/L
0.020
1
11/09/1617:25
Nitrogen, NO2 plus NO3
0.039 mg/L
0020
1
11/08/1617:25
365.1 Phosphorus, Total
Analytical. Method EPA365.1
Phosphorus
2.2 mg/L
0.050
1
11/11/1622:32
7723-14-0
420.4 Phenolics, Total
Analytical Method: EPA4204
Phenol
0.18 mg/L
0030
3
11/16/1510:08
4500 Chloride
Analytical Method : SM 4500 -CI -E
Chloride
9.8 mglL
1.0
1
11/10/162341
16887-00-6
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
425 mg/L
250
1
_ 11/11/1603:30
53108 TOC
Analytical Method : SM 5310B
Total Organic Carbon
80.4 mg/L
50
5
11/15/161011
744044-0
REPORT OF LABORATORY. ANALYSIS
This reportshall not be reproduced except in full,
Date: 11/22/201612:52 PM eetr.bttb.wrder consent of Pece Analyawl service., LLC Page 7 of 40