NC0006351_Renewal Application_20180525

ROY COOPER
Governor
MICHAEL EL S. REGAN
Sec retcmv
Water Resources LINDA CLTLPEPPER
ENV'R0NME`1TA,. QUAG'TV rn'
Interim:.;.•ectcr
June 04, 2018
Jonna Stein, Manager Operations
Venator Chemicals LLC
PO Box 1330
5910 Pharr Mill Rd
Harrisburg, NC 28075
Subject: Permit Renewal
Application No. NC0006351
Venator Chemicals, LLC
Cabarrus County
Dear Applicant:
The Water Quality Permitting Section acknowledges the May 31, 2018 receipt of your permit renewal application and
supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 150B-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit.
The permit writer will contact you if additional information is required to complete your permit renewal. Please respond
in a timely manner to requests for additional information necessary to allow a complete review of the application and
renewal of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
https://deq.nc.gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,
3ree, sol
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
ec: WQPS Laserfiche File w a lication
Q / PP
State of North Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I Raleigh,North Carolina 27699-1617
919-807-6300

VENATOR
RECEIVED•" cW
'R/OVVICI
MAY fl 2018
May 25, 2018
Water Resources
ectiori
Wren Thedford Permitting
NC DEQ/ Division of Water Resources/Complex NPDES Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: Permit Renewal Application—NPDES Permit No. NC0006351
Venator Chemicals LLC—Harrisburg, NC
Cabarrus County
Dear Mr. Thedford:
The Venator Chemicals LLC (Venator), formerly Chemical Specialties LLC, Harrisburg
facility's NPDES permit for the discharge of treated process wastewater, permit number
NC0006351, expires November 30, 2018. Therefore, the renewal of this permit is requested
in accordance with renewal requirements.
The original and two copies of the NPDES permit application are enclosed to support the
renewal application in accordance with Title 15A of NC Administrative Code Subchapter
2H.0100. The following information is included as part of this application per DENR's
request:
• USEPA Form 1
• Site Location Map
• USEPA Form 2C
• Schematic of Water Flow
• Sludge Management Plan
• Priority Pollutant Analysis Scan
• Name Change Letter
Due to whole effluent toxicity testing results, Venator is conducting ongoing Toxicity
Investigation Evaluation/Toxicity Reduction Evaluation to support Venator's commitment to
mitigate the toxicity source and to remain in compliance with water quality standards.
We appreciate the opportunity to submit this renewal application with supporting information
and hope that it meets with your approval. At the appropriate time, if a meeting could provide
direct communication and allow further clarification about the renewal application, we are
available to meet with you at your convenience. I may be reached via email at
JonnaSchemspec.com or by phone at [phone], if further information is required.
Sincerely,
Jonna Stein
ENS Manager
5910 Pharr Mill Road, Harrisburg, NC 28075, USA
Tel: [phone] Fax: [phone] [e-mail] www.venatorcorp.com

USEPA Form 1

Please print or type in the unshaded areas only
(fill-in areas are spaced for elite type,i.e., 12 characters/inch). For Approved. OMB No.2040-0086. Approval expires 5-31-92
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER
i NA/EPA GENERAL INFORMATION S 71-/A
Consolidated Permits Program F NCD048467427
GENERAL (Read the "General Instructions"before starting.) 1 2 1
LABEL ITEMS GENERAL INSTRUCTIONS
If a preprinted label has been provided,
I. EPA I.D. NUMBER affix it in the designated space.Review the
information carefully; if any of it is
incorrect cross through it and enter the
III. FACILITY NAME correct data in the appropriate fill-in area
below.Also,if any of the preprinted data is
absent (the area to the left of the label
V. FACILITY PLEASE PLACE LABEL IN THIS SPACE space lists the information that shouldappear),please provide it in the proper fill-
MAILING LIST in area(s) below. If the label is complete
and correct you need not complete Items
I, III,V. and VI(except Vl-B which must be
completed regardless). Complete all items
VI. FACILITY if no label has been proved. Refer to the
LOCATION instructions for detailed item descriptions
and for the legal authorization under which
this data is collected.
II. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer"yes"to any
questions,you must submit this form and the supplemental from listed in the parenthesis following the question.Mark"X"in the box in the third column if
the supplemental form is attached. If you answer"no"to each question,you need not submit any of these forms. You may answer"no"if your activity is
excluded from permit requirements;see Section C of the instructions.See also,Section D of the instructions for definitions of bold-faced terms.
SPECIFIC QUESTIONS MARK"X" MARK"X"
YES NO FORM SPECIFIC QUESTIONS FORM
ATTACHED YES NO ATTACHED
A. Is this facility a publicly owned treatment works B. Does or will this facility (either existing or
which results in a discharge to waters of the ❑ ® ❑ proposed) include a concentrated animal ❑ ® ElU.S.?(FORM 2A) feeding operation or aquatic animal
production facility which results in a discharge
16 ' 17 18 to waters of the U.S.?(FORM 28) 19 20 21
C. Is this facility which currently results in ® ❑ ® D. Is this proposal facility(other than those described ❑ ® ❑
discharges to waters of the U.S. other than in A or B above)which will result in a discharge
those described in A or B above?(FORM 2C) 22 23 24 to waters of the U.S.?(FORM 2D) 25 26 27
E. Does or will this facility treat,store, or dispose of F. Do you or will you inject at this facility industrial or
hazardous wastes?(FORM 3) ❑ ® ❑ municipal effluent below the lowermost stratum ❑ ® ❑
containing, within one quarter mile of the well
bore, underground sources of drinking water?
28 29 30 (FORM 4) 31 32 33
G. Do you or will you inject at this facility any H. Do you or will you inject at this facility fluids for
produced water other fluids which are brought to special processes such as mining of sulfer by the
the surface in connection with conventional oil or ❑ ® ❑ Frasch process,solution mining of minerals,in ❑ ® ❑
natural gas production, inject fluids used for situ combustion of fossil fuel,or recovery of
enhanced recovery of oil or natural gas,or inject geothermal energy?(FORM 4)
fluids for storage of liquid hydrocarbons?
(FORM 4) 34 35 36 37 38 39
I. Is this facility a proposed stationary source J. Is this facility a proposed stationary source
which is one of the 28 industrial categories listedwhich is NOT one of the 28 industrial categories
in the instructions and which will potentially emit ❑ ® ❑ listed in the instructions and which will potentially ❑ ® ❑
100 tons per year of any air pollutant regulated emit 250 tons per year of any air pollutant
under the Clean Air Act and may affect or be regulated under the Clean Air Act and may affect
located in an attainment area? FORM 5 40 41 42 or be located in an attainment are? FORM 5 43 44 45
III. NAME OF FACILITY
C SKIP Venator Chemicals LLC
f
15 16-29 30 69
IV. FACILITY CONTACT
A.NAME&TITLE(last, first,&title) B.PHONE(area code&no.)
2 Jonna Stein, EHS Manager 704 455 5181
15 16 45 46 48 49 51 52 55
V. FACILITY MAILING ADDRESS
A.STREET OR P.O.BOX
c P.O. Box 1330 5910 Pharr Mill Rd
15 16 45
B.CITY OR TOWN C.STATE D.ZIP CODE
c Harrisburg NC 28075
4
15 16 40 41 42 47 51
VI. FACILITY LOCATION
A.STREET,ROUTE NO.OR OTHER SPECIFIC IDENTIFIER
C 5910 Pharr Mill Rd
15 16 45 _
B.COUNTY NAME
Cabarrus
46 70
C.CITY OR TOWN D.STATE E.ZIP CODE F.COUNTY CODE
c Harrisburg NC 28075
5 16 40 41 42 47 51 1 52 54
EPA FORM 3510-1(8-90) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII. SIC CODES 4-di.it, in order of.riorit
A.FIRST B.SECOND
c 2819 I (specify) 7 2879 (specify)
6 16 17 Industrial Inorganic Chemicals s 16 1s Pesticide and Agricultural Chemicals
C.THIRD D.FOURTH
7 r (specify) 7 (specify)
15 16 17 15 16 19
VIII. OPERATOR INFORMATION
A.NAME B.Is the name listed in Item
c ( Venator Chemicals LLC VIII-A also the owner?
8
18 19 ❑ YES ❑NO
55
C.STATUS OF OPERATOR(Enter the appropriate letter into the answer box;if"Other,"specify.) D.PHONE(area code&no.)
F=FEDERAL M=PUBLIC(other than federal or state) p (specify) c 704 455 5181
S=STATE 0=OTHER(specify) A
P=PRIVATE 56 15 16 18 19 21 22 25
E.STREET OR PO BOX
P.O. Box 1330
26 55
F.CITY OR TOWN G.STATE H.ZIP CODE IX. INDIAN LAND
c Harrisburg NC 28075 Is the facility located on Indian lands?
B
15 16 40 42 42 47 51 ❑YES ® NO
X. EXISTING ENVIRONMENTAL PERMITS
A.NPDES(Discharges to Surface Water) D.PSD(Air Emissions from Proposed Sources)
C N ' NC0006351 9 P 8 NA
15 16 17 18 30 15 16 17 18 30
B.UIC(Underground Injection of Fluids E.OTHER(specify) (Specify)
s ' NA s T 8 NCS000057 Stormwater
15 16 17 18 30 15 16 17 18 30
C. RCRA(Hazardous Wastes) E.OTHER(specify) (Specify)
9 R ' NCD048467427-R2 s T 8 07488R27 Synthetic Minor Air
=mini 18 30 15 16 17 18 30 Permit
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the ma. area. See instructions for .recise re.uirements.
XII. NATURE OF BUSINESS •rovide a brief descri.tion
Manufacturer of chemicals including pesticides and inorganics which are supplied to wood preserving,
agricultural, and industrial facilities. Products produced include alkaline copper quat(ACQ), chromated copper
arsenate(CCA), arsenic acid, and other copper based pesticides. Inorganics include binary salts of Al, Cu, Mg,
Mn, Ca, Na, and Zn(chlorides and nitrates). Also manufacturer of organic-based pesticides, including Ecolife2.
XIII. CERTIFICATION (see instructions)
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibilit of fine and imprisonment.
A. NAME&OFFICIAL TITLE(type or print) B.SIGNATURE C. DATE SIGNED
Shawn Turner, Plant Manager , i i
COMMENTS FOR OFFICIAL USE ONLY
C
C
15 16 55
EPA FORM 3510-1(8-90)

Site Location Map

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Feet
m Lat.: 35°19'48" USGS Quad Name:Harrisburg! Figure 1
B row n AND • Long.:80°37'28" Concord SE
Receiving Stream:Rocky River Site Location Map
Venator Chemicals LLC
Caldwell • DATE 41182016 StreamClass:C
SCALE AS SHOWN
DRAWN BY AH Stream
Yadkin Pee-Dee
5 CHECKED BY. TN 5910 Pharr Mill Rd,Harrisburg,NC 28075
PROJECT* 152062
SOURCE.ESRI(USGS 7 S-MINUTETOPO QUADS'.HARRISBURG AND CONCORD SE)

USEPA Form 2C

EPA I.D.NUMBER(copy from ltem 1 ofForm I) Form Approved.
NCD048467427 OMB No.2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM U.S.ENVIRONMENTAL PROTECTION AGENCY
APPLICATION FOR PERMIT
DISCHARGE WASTEWATER
ZC \"/EPAEXISTING MANUFACTURING,COMMERC ALO,MINING AND SILVICULTURE OPERATIONS
NPDES Consolidated Permits Program
I.OUTFALL LOCATION
For each outfall,list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A.OUTFALL NUMBER B.LATITUDE C.LONGITUDE
Vast) 1.DEG. 2.MIN. 3.SEC. 1.DEG. 2.MIN. 3.SEC. D.RECEIVING WATER(name)
001 35 19 48 80 37 28 Rocky River
II.FLOWS,SOURCES OF POLLUTION,AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility.Indicate sources of intake water,operations contributing wastewater to the effluent,and treatment units
labeled to correspond to the more detailed descriptions in Item B.Construct a water balance on the line drawing by showing average flows between intakes,operations,
treatment units,and outfalls.If a water balance cannot be determined(e.g.,for certain mining activities),provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of:(1)All operations contributing wastewater to the effluent,including process wastewater,sanitary wastewater,cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3)The treatment received by the wastewater. Continue on additional sheets if
necessary.
1.OUT- 2.OPERATION(S)CONTRIBUTING FLOW 3.TREATMENT
FALL b.AVERAGE FLOW b.LIST CODES FROM
NO.(list) a.OPERATION Psi)) (inchcc%urnrc) a.DESCRIPTION TABLE 2C-1
Inorganic chemicals manufacturing Chemical Precipitation, Settling Lagoon,
001 Discharge to Rocky River 2-C 5-T
Scrubbers
4-A
Boilers and Cooling Towers
Stormwater
OFFICIAL USE ONLY(effluentguidelines.suh-caiegone.r)
EPA Form 3510-2C(8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C.Except for storm runoff,leaks,or spills,are any of the discharges described in Items II-A or B intermittent or seasonal'?
©YES(complete the follon'iug table) ❑NO(go to Section 111)
3.FREQUENCY 4 FLOW
a.DAYS PER B.TOTAL VOLUME
2.OPERATION(s) WEEK b.MONTHS a.FLOW RATE(in n,,¢,) (,pc..(6.with units)
1.OUTFALL CONTRIBUTING FLOW (specify. PER YEAR 1.LONG TERM 2.MAXIMUM 1.LONG TERM 2.MAXIMUM C.DURATION
NUMBER(Itu) (list) are,nxc) (spectfpa,eraxe) AVERAGE DAILY AVERAGE DAILY Onds,v)
001 Discharges occur intermittently from N/A 8 <0.025 MGD 0.025 MGD <0.025 MGD 0.025 MGD 5
lagoon #5 during large storm water
events.
III.PRODUCTION
A.Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility'?
®YES(complete Item 111-H) ❑NO(go to Section IV)
B.Are the limitations in the applicable effluent guideline expressed in terms of production(or other measure of operation)?
YES(complete Item 111-m) ❑NO(go to Sectio,IV)
C. If you answered"yes"to Item III-B,list the quantity which represents an actual measurement of your level of production,expressed in the terms and units used in the
applicable effluent guideline,and indicate the affected outfalls.
1.AVERAGE DAILY PRODUCTION
c.OPERATION,PRODUCT,MATERIAL,ETC. 2.AFFECTED OUTFALLS
a.QUANTITY PER DAY b.UNITS OF MEASURE (list out/all numbers)
(sped(;)
120,000 lb/day Copper nitrate Outfall 001
Copper nitrate batch size (lb) = 40,000 (UPDATE?)
# batches produced per shift = 1.5
Current # shifts per day = 2
Total copper nitrate daily production =
40,000 x 1.5 x 2
IV.IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application?This includes,but is not limited to,
permit conditions,administrative or enforcement orders,enforcement compliance schedule letters,stipulations,court orders,and grant or loan conditions.
❑YES(complete the following table) 12:1 NO(go to hem IV-H)
1.IDENTIFICATION OF CONDITION, 2.AFFECTED OUTFALLS 3.BRIEF DESCRIPTION OF PROJECT 4.FINAL COMPLIANCE DATE
AGREEMENT,ETC.
a.NO. b.SOURCE OF DISCHARGE a.REQUIRED b.PROJECTED
Not applicable. Internal
evaluation is being
conducted for treatment
improvements.
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges)you now have underway or which you plan.Indicate whether each program is now underway or planned,and indicate your actual or planned schedules for
construction.
❑MARK"X"IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C(8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D.NUMBER(copyfromItem I of Form I)
CONTINUED FROM PAGE 2 NCD048467427
V.INTAKE AND EFFLUENT CHARACTERISTICS
A,B,&C: See instructions before proceeding—Complete one set of tables for each outfall—Annotate the outfall number in the space provided.
NOTE:Tables V-A,V-B,and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions,which you know or have reason to believe is discharged or may be discharged
from any outfall.For every pollutant you list,briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT 2.SOURCE 1.POLLUTANT 2.SOURCE
Acetic acid Raw material
Ammonia solution Raw material*
Arsenic trioxide Raw material*
Chromic acid Raw material*
Copper acid Raw material and product
Hydrochloric acid Raw material
Nitric acid Raw material
Phosphoric acid Raw material*
Sodium hydroxide Raw material
Sodium nitrite Raw material and product
Zinc nitrate Raw material and product
* Raw materials that do not go
to the wastewater treatment
system but could enter through
stormwater in the event of a
spill.
VI.POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
YES(list all such pollutants helms ) ❑NO(go to Item VI-R)
Arsenic
Chromium
Cadmium
Copper
Lead
Mercury
Nickel
Zinc
Benzene
Chlorobenzene
Toluene
EPA Form 3510-2C(8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VII.BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
YES(identijr the test(s)and describe their purposes below) El NO(go to Section VIII)
The facility conducted chronic toxicity testing during wastewater discharge and several tests did not pass. A
toxicity identification evaluation/toxicity reduction evaluation (TIE/TRE) is currently in progress.
VIII.CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES(list the name,address,and telephone number of and pollutants analyzed by, NO(go to Section IX)
each such laboratory or,firm below)
A.NAME B.ADDRESS C.TELEPHONE D.POLLUTANTS ANALYZED
(area code&no.) (list)
Pace Analytical Services, Inc. 9800 Kincey Ave., Suite 100 [phone] All parameters
Huntersville, NC 28078
IX.CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and belief true,accurate,and complete.I am aware that there
are significant penalties for submitting false information,including the possibility of fine and imprisonment for knowing violations.
A.NAME&OFFICIAL TITLE(type or print) B.PHONE NO.(area code&no.)
hac,JAu(ner 7o11-4ss—'1137
C.SIGNATURE D.DATE SIGNED
sbs//S?
EPA Form 3510-2C(8-90) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY.You may report some or all of this information EPA I.D.NUMBER(copy from hem I of Form I)
on separate sheets(use the same format)instead of completing these pages. NCD048467427
SEE INSTRUCTIONS.
OUTFALL NO.
V.INTAKE AND EFFLUENT CHARACTERISTICS(continued from page 3 of Fom1 2-C) Data from 2014-2017 DMRs and Oct.20, 2017 PPA o0
i.
PART A-You must provide the results of at least one analysis for every pollutant in this table.Complete one table for each outfall.See instructions for additional details.
3.UNITS 4.INTAKE
2.EFFLUENT (specify tf blank) (optional)
b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
(1) (1) d.NO.OF a.CONCEN- (�) b.NO.OF
1.POLLUTANT CONCENTRATION (2)MASS CONCENTRATION (2)MASS (1)CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Biochemical Oxygen <100 NA NA NA NA NA 1 mg/L d NA NA NA
Demand(BOD) g/ lb/d
b.Chemical Oxygen 95.2 19.83 NA NA NA NA 1 mg/L lb/d NA NA NA
Demand(COD)
c.Total Organic Carbon 1.6 0.33 NA NA NA NA 1 mg/L lb/d NA NA NA
(Mr')
d.Total(Suspended
S11 3.8 10.1 3.8 3.1 0.4 832 m L lb d NA NA NA
Solidss(TSS) 9/ /
e.Ammonia(a.s N) 36 9 32.7 9 18.5 1.6 888 mg/L lb/d NA NA NA
VALUE VALUE VALUE VALUE
f.Flow 0.025 0.025 0.025 1 MGD NA 0.025 NA
g.Temperature VALUE VALUE VALUE VALUE
(winter) 18.2 NA NA 1 °C NA NA
h.Temperature VALUE VALUE VALUE VALUE
(summer) 18.2 NA NA 1 °C NA NA
MINIMUM MAXIMUM MINIMUM IMAXIMUM
i pH 6.64 I 8.55 NA I NA 419 STANDARD UNITS
PART B- Mark"X"in column 2-a for each pollutant you know or have reason to believe is present.Mark"X"in column 2-b for each pollutant you believe to be absent.If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge.Complete one table for each outfall.See the instructions for additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM AVERAGE
AND a. b a.MAXIMUM DAILY VALUE (t1 available) (ifavailable) VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) - b.NO.OF
Of available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
a.Bromide
(24959-67-9) , \X NA NA NA NA NA NA NA NA NA NA NA NA
b.Chlorine,Total X NA NA NA NA NA NA NA NA NA NA NA NA
Residual
c.Color X NA NA NA NA NA NA NA NA NA NA NA NA
d.Fecal Coliform a 155 NA NA NA NA NA 1 CFU/100m NA NA NA NA
e.Fluoride(16984-48-8) u 0.266 0.055 NA NA NA NA 1 mg/L lb/d NA NA NA
(asi�te-Nitrte X 34.2 7.13 NA NA NA NA 1 mg/L lb/d NA NA NA
EPA Form 3510-2C((88-990) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG.VALUE a.LONG TERM
ANDa b. a.MAXIMUM DAILY VALUE (if available) (if available) AVERAGE VALUE
CAS NO. BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(i/'available) PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
g.Nitrogen, \ /
Total Organic(as X NA NA NA NA NA NA NA NA NA NA NA NA
M
h.Oil and u NA NA NA NA NA NA NA NA NA NA NA NA
Grease
i.Phosphorus \ /
(as P),Total X <0.1 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(7723-14-0)
j.Radioactivity
(1)Alpha,Total X NA NA NA NA NA NA NA NA NA NA NA NA
(2)Beta,Total X NA NA NA NA NA NA NA NA NA NA NA NA
(3)Radium, X NA NA NA NA NA NA NA NA NA NA NA NA
Total
(4)Radium 226, X NA NA NA NA NA NA NA NA NA NA NA NA
Total
k.Sulfate
("'tiO') X <2500 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(14808-79-8)
I.Sulfide X <0.05 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(as 1
m.Sulfite
(a''SO.) X <3 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(14265-45-3)
n.Surfactants X NA NA NA NA NA NA NA NA NA NA NA NA
o.Aluminum,
Total
X(7429-90-5) /g/ lb<0.1 NA NA NA NA NA 1 mg/L d NA NA NA
p.Barium,Total
(7440-39-3) X 0.159 0.033 NA NA NA NA 1 mg/L lb/d NA NA NA
q.Boron,Total X
(7440-42-8) NA NA NA NA NA NA NA NA NA NA NA NA
(.Cobalt,Total
(7440-48-4) X NA NA NA NA NA NA NA NA NA NA NA NA
Iron,Total
( 0.1 0.082 NA NA NA NA 1 m L lb d NA NA NA
(7439-89-6) g/ /
t.Magnesium,
Total X <100 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(7439-95-4)
u.Molybdenum,
Total X <0.005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(7439-98-7)
v.Manganese,
Total X 0.105 0.022 NA NA NA NA 1 mg/L lb/d NA NA NA
(7439-96-5)
Tin,w. Total
(7440-31-5) X NA NA NA NA NA NA NA NA NA NA NA NA
x.Titanium,
Total X NA NA NA NA NA NA NA NA NA NA NA NA
(7440-32-6)
EPA Form 3510-2C(8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D.NUMBER(copy from Nem l ofl•orm I) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C NCD048467427 001
PART C- If you are a primary industry and this outfall contains process wastewater,refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for.Mark"X"in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals,cyanides,and total phenols. If you are not required to mark column 2-a(secondary industries,nonprocess wastewater outfalls, and nonrequired GC/MS
fractions),mark"X"in column 2-b for each pollutant you know or have reason to believe is present. Mark"X"in column 2-c for each pollutant you believe is absent.If you mark column 2a for any pollutant,you must
provide the results of at least one analysis for that pollutant.If you mark column 2b for any pollutant,you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater.If you mark column 2b for acrolein,acrylonitrile,2,4 dinitrophenol,or 2-methyl-4,6 dinitrophenol,you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater.Otherwise,for pollutants for which you mark column 2b,you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table(all 7 pages)for each outfall. See instructions for
additional details and requirements.
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(If available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS _CONCENTRATION (2)MASS ANALYSES
METALS,CYANIDE,AND TOTAL PHENOLS
1M.Antimony,Total
(7440-36-0) /<0.005 NA NA 1 mg/ lb NA NA NA L d NA NA NA
2M(74.0-38-2) Total 0.074 0.008 0.042 0.008 0.013 0.001 887 mg/L lb/d NA NA NA
(7440-38-2) g/ /
3M.Beryllium,Total g/
(7440-41-7) <0.001 NA NA NA NA NA 1 m L lb/d NA NA NA
4(7440-43-9)74 Cadmium,Total <0.0 01 NA NA NA NA NA 1 m L lb/d NA NA NA
g/ /
T .Chromium,
Total(7440-47-3) 0.01 0.001 887 mg/L lb 0.02 0.008 0.01 0.008 d NA NA NA
/
6M.Copper,
Total 2.608 0.272 0.97 0.272 0.202 0.023 887 mg/L lb d NA NA NA
(7440-50-8)50-8) g/ /
1774 Lead,-92-Total 0.01 0.008 0.01 0.008 0.010 0.001 887 mg/L lb/d NA NA NA
(7439-92-1) g/ /
8M.
Mercury,Total
<0. NA NA 1 m9/L lb 0002 NA NA NA d NA NA NA
(7439-97-6) /
9M
.002el,Total X/ 51 1.7 46.8 1.7 5.2 0.2 887 mg/L lb d NA NA NA
(7440-02-0) /� g/ /
Total(77Selenium,
0.05 0.041 0.05 0.041 0.046 0.005 887 m L lb d NA NA NA
Total(7782-49-2) � g/ /
11M.
NA NA 1 mg/ lb
(7440-22-4) /Silver,Total
<0.005 NA NA NA L d NA NA NA
12M.Thallium,
<0.01 NA NA NA NA NA 1 m L d NA NA NA
Total(7440-28-0) X g/ lb/d
13M. Total
( 16.56 0.582 14.18 0.582 1.271 0.05 887 m L lb d NA NA NA
(7440--66-6- X 6) /\ g/ /
14Ml Cyanide, X <0.005 NA NA NA NA NA 1 mg/L lb
/d(57-12-5) g/ d NA NA NA15M.
/
Total Phenols, X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
DIOXIN
2,3,7,8-Tetra- X DESCRIBE RESULTS
chlorodibenzo-P- No dioxins manufactured or used
Dioxin(1764-01-6)
EPA Form 3510-2C(8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c a.MAXIMUM DAILY VALUE (tfavailable) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(ifavailable) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS
(107-02-8)
0-02-8)ein <0.1 NA NA NA NA NA 1 mg/L 1 b/d NA NA NA
(07-13-1)nitrile X <0.05 NA NA NA NA NA 1 mg/L lb/d NA NA NA
3V.Benzene X/�
(71-43-2) <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
4V.Bis(Chloro-
methyl)Ether x NA NA NA NA NA NA NA NA NA NA NA NA
(542-88-1)
(5-25r-2)oform X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
6V.Carbon
TetrachlorideX <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(56-23-5)
7V. benzene
<0. 1 mg/L /001 NA NA NA NA NA lb/d NA NA NA
(108-90-7)-90-7) X
8V.Chlorodi- \ /
bromomethane x <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(124-48-1) / `
9V.Chloroethane
(75-00-3) X <0.005 NA NA NA NA NA 1 mg/L 1 b/d NA NA NA
10V.2-Chloro-
ethylvinyl Ether u <0.05 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(110-75-8) , \
11V.Chloroform
(67-66-3) X <0.005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
12V.Dichloro-
(75-27 bromoq)thane X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
131.Dichloro-
difluoromethane <0.005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(75-71-8)
14V.1,1-Dichloro-
ethane(75-34-3) X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
15Vtha e1 (107-06ro-
<0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
ethane(107-06-2) g/ /
1
6Vl ne(75 -4-
e <0.001 NA NA NA NA NA 1 m L lb/d NA NA NA
ethylene(75--355-4) � g/
17V.1,2-Dichloro-
propane(78-87-5) X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
18V.1,3-Dichloro- \
propylene /X\ <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(542-75-6)
19V.Ethylbenzene <0.001 NA NA NA NA NA 1 m L lb d NA NA NA
(100-41-4) 9/ /
20V.Methyl 0.0103 0.002 NA NA NA NA 1 mg/L 1b/d
Bromide(74-63-9) 9/ NA NA NA
21V.Methyl 0.0103 0.002 NA NA NA NA mg/L d NA NA NA
Chloride(74-87-3) 1 lb/d
EPA Form 3510-2C(8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—VOLATILE COMPOUNDS(continued)
22V.Methylene <0.0 0 5 NA NA NA NA NA 1 mg/L 1 d NA NA NA
Chloride(75-09-2) 9/ lb/d
23V.1,1,2,2- ` '
Tetrachloroethane X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(79-34-5)
24V. achloro-
NA 1 mg/L 0.0 01 NA NA NA NA L d NA NA NA
ethyleneylene(127-18-4) 9/ lb/d
25V.Toluene `X/ mg/L NA NA NA NA NA 1 L d NA NA NA
(108-88-3) /\ g/ lb/d
26V.1,2-Trans-
Dichloroethylene X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(156-60-5)
27V.1,1,1-Trichloro-
ethane(71-55-6) X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
28V.1,1,2-Tnchloro- <0.001 NA NA NA NA NA L d NA NA NA
ethane(79-00-5) 1 mg/L lb/d
29Vethylene
oro- <0.0 01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
ethylene(79-01-6) 9/ /
30V.Trichloro-
fluoromethane X <0.005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(75-69-4) / `
31V.Vinyl Chloride <0.001 NA L d NA NA NA
(75-01-4) NA NA NA NA 1 mg/L lb/d
GC/MS FRACTION-ACID COMPOUNDS
(.2-Chlorophenol
X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
-57-8)
2A.2,4-Dichlaro- /\ <0. NA NA 1 m01 NA NA NA L d NA NA NA
phenol(120-83-2) 9/ lb/d
3A.2,4-Dimethyl- <0.01 NA NA NA NA NA 1 m L lb/d NA NA NA
phenol(105-67-9) 9/
Cresol4A. (534-ro-0) <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
Cresol(534-52-1) 9/ /
5A.2,4-Di2 <0.01 NA NA NA NA Llb/d NA NA NA
phenol(51--28-8- NA 1 m9/5)
6A.2-Nitrophenol
(88-75-5) X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
7A.4-Nitrophenol <0.01 NA NA NA L d NA NA NA
(100-02-7) NA NA 1 mg/L lb/d
8A.P-Chloro-M- <0.01 NA NA NA NA NA 1 m L lb d NA NA NA
Cresol(59-50-7) X 9/ /
9A.Pentachloro- <0.01 NA NA NA L d NA NA NA
phenol(87-86-5) NA NA 1 mg/L lb/d
(108-9955-22)) X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(108
phenol
ro- <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
phenol(88-05-2) 9/ /
EPA Form 3510-2C(8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
ANDa. b. c. a.MAXIMUM DAILY VALUE (ijavailable) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS
(8_Acenaphthene)
X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA I
2B.Acenaphtylene
X <0.001 NA NA NA NA NA 1 mg/ lb/d d NA NA NA
(208-96-8) /\ /
3B.Anthracene
(120-12-7) X /<0.001 NA NA NA NA NA 1 mg/ lb/d d NA NA NA
4B.(92-8B7-5)
dine X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
5B.Benzo(a) /�
Anthracene X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(56-55-3)
6B.Benzo(a)
X <0.001 NA NA NA NA NA 1 L d NA NA NA
Pyrene(50-32-8) mg/L lb/d
7B.3,4-Benzo-
tluoranthene X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(205-99-2)
8B.Benzo( -) <0.001 NA NA NA NA NA 1 m L lb/d NA NA NA
Perylene(19191-242) X 9/
98.Benzo(k)
Fluoranthene X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(207-08-9)
10B.Bis(2-Chlora-
erho.rr)Methane
X <0.01 NA NA NA NA NA 1 L d NA NA NA
(111-91-1) mg/L lb/d
11B.Bis(2-('hloro-
rr40 Ether
X <0.01 m NA NA NA NA NA 1 L d NA NA NA
(111-44-4) g/ lb/d
12B.Bis(2-
('hlorousopr'pvl) <0.01 NA NA NA NA NA 1 L d NA NA NA
Ether(102-80-1) m g/ lb/d
13B.Bis(2-l,in'l-
hary/)Phthalate X <0.003 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(117-81-7)
14B.4-BromophenylPhe �/
(101nyl Ether
er X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
158.Butyl Benzyl <0.003 NA NA NA NA NA 1 L lb/d NA NA NA
Phthalate(85-68-7) mg/L
X
16B.2-Chloro-
naphthalene X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(91-58-7)
17B.4-Chloro-
phenyl Phenyl Ether X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(7005-72-3)
18B. a
(218-01-9)01-9) 9/ lb<0.001 NA NA NA NA NA 1 mg/L d NA NA NA
/
19B.Dibenzo(tilt)
Anthracene X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(53-70-3)
B.
benzene(9 a(95-55-5 < mg
0-1)12-DichlXoro-
benzene 0.0 01 NA NA NA NA 1 / /
L lb/d NA NA NA
218.1,3-Di-chloro-
benzene(541-73-1) X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
EPA Form 3510-2C(8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) -' b.NO.OF
(if available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(canoned)
228.1,4-Dich-46- <0.001 NA NA NA NA NA 1 mg/ lb/d d NA NA NA
benzene(106-46-7) /
238.3,3-Dichlo4- <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
benzidine(91-94-1) X 9/ /
P2hthalate
8alate(84-66-2)
l <0.003 NA NA NA NA NA 1 mg/L lb/d NA NA NA
Phthalate(84 66 2) X g/ /
25B.Dimethyl
Phthalate
(131-11-3) X <0.003 NA NA NA NA NA 1 mg/L lb/d NA NA NA
268.Di-N-Butyl <0.003 NA NA NA NA NA 1 m L lb d NA NA NA
Phthalate(84-74-2) 9/ /
2,4-Dinitro-
<<0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
toluene(121-14-2) X g/
2,6-Dinitro-
<<0.01 NA NA NA NA NA 1 mg/L NA NA
toluene(606-20-2) X g/ lb/d/ NA
298.Di-N-Octyl
Phthalate(1(117-84-0) NA NA 1 mg/<0.003 NA NA NA L lb/d NA NA NA
308.1,2-Diphenyl-
hydrazine(as Azo- <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
benzene)(122-66-7)
/
318.Fluoranthene
(206-44-0) <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(8fi73-7)rene X/ <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
33B.Hexachloro- /\
benzene(118-74-1) X <0.001 NA NA NA NA NA 1 mg/L lb/d NA NA NA
3uta i e e(87-68 <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
butadiene(87-68-3) 9/
35B.Hexachloro-
cyclopentadiene
X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(77-47-4) / \
ethane
He(67-72-o-
1) <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
ethane(67-72-1) X g/
37B.Indeno
(1,2,3-cd)Pyrene <0.001 NA NA NA NA
(193-39-5) NA 1 mg/L lb/d NA NA NA
388orone <0.01 NA NA NA NA NA 1 m L lb d NA NA NA
(78-59-1)59-1) g/ /
396.Naphthalene
(91-20-3) lb/d. 1 mg/ lb 001 NA NA NA NA NA L d NA NA NA
408.Nitrobenzene
(98-95-3) X <0.01 NA NA NA NA NA 1 mg/L l b/d NA NA NA
410.N-Nitro-
sodimethylamine X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(62-75-9)
42B.N-Nitrosodi-
ylamine
(621-64-7) X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(621-6
EPA Form 3510-2C(8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
AND a. b. c a.MAXIMUM DAILY VALUE (i/available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
(i/available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION—BASE/NEUTRAL COMPOUNDS(continued)
43B.N-Nitro-
sodiphenylamine X <0.01 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(86-30-6)
Phenanthrene <0.001 NA NA NA NA NA 1 m L lb/d NA NA NA
(85-
(85-01-8) X g/
45B.000
(129-00-0) X <0.001 NA NA NA NA NA 1 m L lb
/d
g/ d NA NA NA/
46B.1,2,4-Tri-
benzene <0.01 NA NA NA NA NA 1 m L lb/d NA NA NA
(120-
(120-82-1) X g/ /
GC/MS FRACTION—PESTICIDES
(3.9100-n g/ lb
(309-00-2) X <0.00005 NA NA NA NA NA 1 mg/L d NA NA NA
/
2P.a-BHC
19-84- ) <0.00005 NA NA NA NA NA 1 m /L lb/d NA NA NA
(319-84-6) X mg
/L
(319-85-7) X mg/L<0.00005 NA NA NA NA NA 1 m L lb/d NA NA NA
(319-8
4P.
(58-89 9) X <0.00005 NA NA NA NA NA 1 mg/L 1 b/d NA NA NA
5P.d-BHC
X <0.00005 NA NA NA NA NA 1 m L 1b
(319-86-8)6Pg/ d NA NA NA
/
(57-74-9)Chl9rdane X <0.0005 NA NA NA NA NA 1 m L lb/d NA NA NA
9/ /
7 4,4'-DDT <0.0 00 05 NA NA NA NA NA 1 mg/L d NA NA NA
(50-29-3) g/ lb/d
8P.4,4'-DDE
(72-55-9) X <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
9P.4,4'-DDD <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(72-54-8) 9/
10P DieldrinX <0.00005 NA NA NA NA NA 1 m L lb
(60-0-577-11) g/ d NA NA NA1 /
(1 5 29-7) lfan X <0.00005 NA NA NA NA NA 1 m L lb/d NA NA NA
(115-29-7) g/ /
0-Endosulfan
(115-29-7)2 X <0.0 0 0 0 5 NA NA NA NA NA 1 mg/L lb/d NA NA NA b l
g/ /
13P.Endosulfan
Sulfate X <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(1031-07-8)
1432 Endrin <0.00005 m 00005 NA NA NA NA NA 1 L lb/d NA NA NA
(72-20-8) X mg/L
15P.Endrin
Aldehyde X <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(7421-93-4)
1634 Heptachlor <0.00005 NA NA NA NA NA 1 m L lb
(76-44-8) 5/ d NA NA NA/
EPA Form 3510-2C(8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA I.D.NUMBER(copy.from Item 1 of Form 1) OUTFALL NUMBER
NCD048467427 001
CONTINUED FROM PAGE V-8
2.MARK"X" 3.EFFLUENT 4.UNITS 5.INTAKE(optional)
1.POLLUTANT b.MAXIMUM 30 DAY VALUE c.LONG TERM AVRG. a.LONG TERM
ANDa. b. c. a.MAXIMUM DAILY VALUE (if available) VALUE(if available) AVERAGE VALUE
CAS NUMBER TESTING BELIEVED BELIEVED (1) (1) (1) d.NO.OF a.CONCEN- (1) b.NO.OF
Of available) REQUIRED PRESENT ABSENT CONCENTRATION (2)MASS CONCENTRATION (2)MASS CONCENTRATION (2)MASS ANALYSES TRATION b.MASS CONCENTRATION (2)MASS ANALYSES
GC/MS FRACTION-PESTICIDES(cannnnecl)
17P.Heptachlor ` ,
Epoxide X <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(1024-57-3)
1534 PCB11 <0.00005 NA NA NA NA 1 m L lb/d NA NA NA
(53469-21-9)) NA g/
19P.
PCB
(11097-69-1) X <0.00005 NA NA NA 1 mg/L 00005 NA NA L lb/d NA NA NA
/�
PCB-1221
X <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(11104-28-2)
21P.PCB-1232
(11141-16-5) X <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
22P.PCB-1248 X
(12672-29-6) <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
23P.PCB-1260
(11096-82-5) X <0.00005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
24P.PCB-1016 X
(12674-11-2) <0.0005 NA NA NA NA NA 1 mg/L lb/d NA NA NA
(8001-35-2)25P.ToxapheneX <0.0 0 0 5 NA NA NA NA NA 1 m L lb/d NA NA NA
g/ /
EPA Form 3510-2C(8-90) PAGE V-9

Schematic of Water Flow

County Water Supply
47,437 gpd
2109 gpd Evap ♦ 1600 gpd Rain 17,229 gpd Evap 25,999 gpd 1500 gpd
• 400 gpd 1 500 gpd• 23,659 gpd r
Water Chemical Cooling Sanitary
Softeners Scrubbers Manufacturing Towers Water
• 200 gpd 329 gpd�--yi 14260 gpd 2340 gpd 1500 gpd
Rain landfills Products
Evap 1793 gpd 500 gpd
2200gpd 440 gpd Evap1500 gpd
Boilers 170Rain000 Septic Tank ►
gpd gpd To Drain Field
• ♦ r •
316 gpd Half-Acre 1170
Waste 9170 gpd ,gpd
Boiler Blow Down Treatment Plant 4 Storage Lagoon4 Storm Water
, 7260 gpd Runoff
•
13,556
Evap 6800 gpd 44 gpd Recirculation 1170 gpd
•
6756 gpd
Rain Two-Acre pH plus Rain
10000 gpd ► i. ° Weir Box ►
Storage Lagoon 6756 Adjustment To Rocky
gpd plus River
Rain
Rainwater amounts are difficult
to quantify due to variability and
changing conditions
Schematic of Water Flow
Venator Chemicals LLC
Harrisburg, NC

Sludge Management Plan

Venator Chemicals LLC—Harrisburg, NC
NPDES Permit No. NC0006351
Supplemental Documentation
Sludge Management Plan Narrative Description
Sludge generated during the wastewater treatment process at the Site is allowed
to settle in the wastewater treatment holding lagoon #5. If it becomes necessary
in the future to remove sludge from the #5 lagoon, it will be properly profiled and
sent to a secure industrial waste facility.
No other sludge is generated or disposed from the wastewater treatment
process.
4111111.41,
/2S/D/
Shawn Turner Date
Plant Manager
Harrisburg SludgeMgtPlan Page 1 of 1

Priority Pollutant Analysis Scan

Priority Pollutant Analysis Scan
Permit No. NC0006351 Month October
Outfall 001/Lagoon#5 Year 2017
Facility Name Ventor Chemicals LLC
Date of sampling October 20,2017
Analytical Laboratory Pace Analytical Services
Quantitation Sample Units of Number of
Parameter Sample Type Analytical Method Level Result Measurement samples
Ammonia(as N) Grab EPA 350.1 0.10 ND mg/L 1
Nitrate/Nitrite Grab EPA 353.2 0.50 34.2 mg/L 1
Total Phosphorus Grab EPA 365.1 0.10 ND mg/L 1
Total suspended solids Grab SM 2540D 1 ND mg/L 1
Metals(total recoverable),cyanide and total phenols
Antimony Grab EPA 200.7 0.005 ND mg/L 1
Arsenic Grab EPA 200.7 0.001 0.00109 mg/L 1
Beryllium Grab EPA 200.7 0.001 ND mg/L 1
Cadmium Grab EPA 200.7 0.001 ND mg/L 1
Chromium Grab EPA 200.7 0.001 ND mg/L 1
Copper Grab EPA 200.7 0.001 0.038 mg/L 1
Lead Grab EPA 200.7 0.001 ND mg/L 1
Mercury Grab EPA 245.1 0.0002 ND mg/L 1
Nickel Grab EPA 200.7 0.001 0.0013 mg/L 1
Selenium Grab EPA 200.7 0.050 ND mg/L 1
Silver Grab EPA 200.7 0.005 ND mg/L 1
Thallium Grab EPA 200.7 0.010 ND mg/L 1
Zinc Grab EPA 200.7 0.010 0.330 mg/L 1
Cyanide Grab EPA 335.4 0.005 ND mg/L 1
Total phenolic compounds Grab EPA 420.1 0.01 ND mg/L 1
Volatile organic compounds
Acrolein Grab EPA 8260B 10 ND ug/L 1
Acrylonitrile Grab EPA 8260B 50 ND ug/L 1
Benzene Grab EPA 8260B 1.0 ND ug/L 1
Bromoform Grab EPA 8260B 1.0 ND ug/L 1
Carbon tetrachloride Grab EPA 8260B 1.0 ND ug/L 1
Chlorobenzene Grab EPA 8260B 1.0 ND ug/L 1
Chlorodibromomethane Grab EPA 8260B 1.0 ND ug/L 1
Chloroethane Grab EPA 8260B 5.0 ND ug/L 1
2-chloroethylvinyl ether Grab EPA 8260B 50 ND ug/L 1
Chloroform Grab EPA 8260B 5.0 ND ug/L 1
Dichlorobromomethane Grab EPA 8260B 1.0 ND ug/L 1
1,1-dichloroethane Grab EPA8260B 1.0 ND ug/L 1
1,2-dichloroethane Grab EPA 8260B 1.0 ND ug/L 1
Trans-1,2-dichloroethylene Grab EPA 8260B 1.0 ND ug/L 1
1,1-dichloroethylene Grab EPA 8260B 1.0 ND ug/L 1
1,2-dichloropropane Grab EPA8260B 1.0 ND ug/L 1
1,3-dichloropropylene Grab EPA8260B 1.0 ND ug/L 1
Ethylbenzene Grab EPA 8260B 1.0 ND ug/L 1
Methyl bromide Grab EPA 8260B 5.0 10.3 ug/L 1
Methyl chloride Grab EPA 8260B 5.0 10.3 ug/L 1
Methylene chloride Grab EPA 8260B 5.0 ND ug/L 1
1,1,2,2-tetrachloroethane Grab EPA8260B 1.0 ND ug/L 1
Tetrachloroethylene Grab EPA 8260B 1.0 ND ug/L 1
Toluene Grab EPA 8260B 1.0 ND ug/L 1
1,1,1-trichloroethane Grab EPA 8260B 1.0 ND ug/L 1 _
1,1,2-trichloroethane Grab EPA 8260B 1.0 ND ug/L 1
Trichloroethylene Grab EPA 8260B 1.0 ND ug/L 1
Vinyl chloride Grab EPA 82606 1.0 ND ug/L 1
Form- DMR-PPA-1 Page 1

Priority Pollutant Analysis Scan
Permit No. NC0006351 Month October
Outfall 001/Lagoon#5 Year 2017
Quantitation Sample Units of Number of
Parameter Sample Type Analytical Method Level Result' Measurement samples
Acid-extractable compounds
P-chloro-m-creso Grab EPA 8270C 10 ND ug/L 1
2-chlorophenol Grab EPA 8270C 10 ND ug/L 1
2,4-dichlorophenol Grab EPA 8270C 10 ND ug/L 1
2,4-dimethylphenol Grab EPA 8270C 10 ND ug/L 1
4,6-dinitro-o-cresol Grab EPA 8270C 10 ND ug/L 1
2,4-dinitrophenol Grab EPA 8270C 10 ND ug/L 1
2-nitrophenol Grab EPA 8270C 10 ND ug/L 1
4-nitrophenol Grab EPA 8270C 10 ND ug/L 1
Pentachlorophenol Grab EPA 8270C 10 ND ug/L 1
Phenol Grab EPA 8270C 10 ND ug/L 1
2,4,6-trichlorophenol Grab EPA 8270C 10 ND ug/L 1
Base-neutral compounds
Acenaphthene Grab EPA 8270C 10 ND ug/L 1
Acenaphthylene Grab EPA 8270C 10 ND ug/L 1
Anthracene Grab EPA 8270C 10 ND ug/L 1
Benzidine Grab EPA 8270C 10 ND ug/L 1
Benzo(a)anthracene Grab EPA 8270C 10 ND ug/L 1
Benzo(a)pyrene Grab EPA 8270C 10 ND ug/L 1
3,4 benzofluoranthene Grab EPA 8270C 10 ND ug/L 1
Benzo(ghi)perylene Grab EPA 8270C 10 ND ug/L 1
Benzo(k)fluoranthene Grab EPA 8270C 10 ND ug/L 1
Bis(2-chloroethoxy)methane Grab EPA 8270C 10 ND ug/L 1
Bis(2-chloroethyl)ether Grab EPA 8270C 10 ND ug/L 1
Bis(2-chloroisopropyl)ether Grab EPA 8270C 10 ND ug/L 1
Bis(2-ethylhexyl)phthalate Grab EPA 8270C 10 ND ug/L 1
4-bromophenyl phenyl ether Grab EPA 8270C 10 ND ug/L 1
Butyl benzyl phthalate Grab EPA 8270C 10 ND ug/L 1
2-chloronaphthalene Grab EPA 8270C 10 ND ug/L 1
4-chlorophenyl phenyl ether Grab EPA 8270C 10 ND ug/L 1
Chrysene Grab EPA 8270C 10 ND ug/L 1
Di-n-butyl phthalate Grab EPA 8270C 10 ND ug/L 1
Di-n-octyl phthalate Grab EPA 8270C 10 ND ug/L 1
Dibenzo(a,h)anthracene Grab EPA 8270C 10 ND ug/L 1
1,2-dichlorobenzene Grab EPA 8270C 10 ND ug/L 1
1,3-dichlorobenzene Grab EPA 8270C 10 ND ug/L 1
1,4-dichlorobenzene Grab EPA 8270C 10 ND ug/L 1
3,3-dichlorobenzidine Grab EPA 8270C 10 ND ug/L 1
Diethyl phthalate Grab EPA 8270C 10 ND ug/L 1
Dimethyl phthalate Grab EPA 8270C 10 ND ug/L 1
2,4-dinitrotoluene Grab EPA 8270C 10 ND ug/L 1
2,6-dinitrotoluene Grab EPA 8270C 10 ND ug/L 1
1,2-diphenylhydrazine Grab EPA 8270C 10 ND ug/L 1
Fluoranthene Grab EPA 8270C 10 ND ug/L 1
Fluorene Grab EPA 8270C 10 ND ug/L 1
Hexachlorobenzene Grab EPA 8270C 10 ND ug/L 1
Hexachlorobutadiene Grab EPA 8270C 10 ND ug/L 1
Hexachlorocyclo-pentadiene Grab EPA 8270C 10 ND ug/L 1 _
Hexachloroethane Grab EPA 8270C 10 ND ug/L 1
Form- DMR- PPA-1 Page 2

Priority Pollutant Analysis Scan
Permit No. NC0006351 Month October
Outfall 001/Lagoon#5 Year 2017
Quantitation Sample Units of Number of
Parameter Sample Type Analytical Method Level Result Measurement samples
Base-neutral compounds(cont.)
Indeno(1,2,3-cd)pyrene Grab EPA8270C 10 ND ug/L 1 _
Isophorone Grab EPA 8270C 10 ND ug/L 1
Naphthalene Grab EPA 8270C 10 ND ug/L 1
Nitrobenzene Grab EPA 8270C 10 ND ug/L 1
N-nitrosodi-n-propylamine Grab EPA 8270C 10 ND ug/L 1
N-nitrosodimethylamine Grab EPA 8270C 10 ND ug/L 1
N-nitrosodiphenylamine Grab EPA 8270C 10 ND ug/L 1
Phenanthrene Grab EPA 8270C 10 ND ug/L 1
Pyrene Grab EPA 8270C 10 ND ug/L 1
1,2,4,-trichlorobenzene Grab EPA 8270C 10 ND ug/L 1
'ND =Parameter not detected above the reported analytical practical quantitation limit
I certify under penalty of law that this document and all attachments were prepared under my direction
and supervision in accordance with a system to design to assure that qualified personnel properly
gather and evaluate the information submitted. Based on my inquiry of the person or persons that
manage the system, or those persons directly responsible for gathering the information, the
information submitted is,to the best of my knowledge and belief,true, accurate and complete. I am
aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations.
StGt,WA'Tut- --
Signature
SI2S1U
Date
Form- DMR-PPA-1 Page 3

Name Change Letter

VENATOR
May 25, 2018
NC DEQ / Division of Water Resources/Complex NPDES Permitting Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Subject: Permit Renewal Application—NPDES Permit No. NC0006351
Venator Chemicals LLC—Harrisburg, NC
Cabarrus County
To Whom It May Concern:
On March 19, 2018, the name of the legal entity for the facility at the above permit
changed from Chemical Specialties LLC to Venator Chemicals LLC. The purpose of
this letter is to inform the Division of Water Resources of this formal name change
associated with the operating permit.
Also enclosed is a copy of the Amendment of Articles of Organization submitted to the
North Carolina Secretary of State notifying them of this change.
If you have any questions or require additional information please do not hesitate to
contact me at 704-455-4171 or [e-mail].
Sincerely,
onna A. Stein
Operations Manager
5910 Pharr Mill Road, Harrisburg, NC 28075, USA
Tel: [phone] Fax: [phone] [e-mail] www.venatorcorp.com

o ARTM
%fir a,,,, V.\
` -,:,„ ,
za:.=, i ,-,-:11 NORTH CAROLINA
-51
``° 4s . P Department of the Secretary of State
To all whom these presents shall come, Greetings:
I, Elaine F. Marshall, Secretary of State of the State of North Carolina, do hereby certify
the following and hereto attached to be a true copy of
ARTICLES OF AMENDMENT
OF
CHEMICAL SPECIALTIES LLC
WHICH CHANGED ITS NAME TO
VENATOR CHEMICALS LLC
the original of which was filed in this office on the 12th day of March, 2018.
•
•
pgPARTiy �, ,.Y�, IN WITNESS WHEREOF, I have hereunto set
\� ,fAY 1D,1))3 /.,.* El .1t. 0 1, c.1
(4g` • % %7.. i},� , my hand and affixed my official seal at the City
r�g_ 4(tAlell N
o of Raleigh, this 12th day of March, 2018.
c,:1-,..t , ii.-1-.y, 0 Aik 1±--ik‹.dpwt d',A.,/te, .....4- vieze...adage
5„.,•_
;.1.-5i„,,„,,f,x ^��= Scan to verify online.
Document Id:0201806403497 Secretary of State
Verify this certificate online at http://www.sosnc.gov/verification

SOS1D: 0096426
Date Filed:3/12/2018 12:38:00 PM
Effective: 3/19/2018
Elaine F.Marshall
North Carolina Secretary of State
C2018 064 03497 _
LIMITED LIABILTY COMPANY
AMENDMENT OF ARTICLES OF ORGANIZATION
Pursuant to §57D-2-22 of the General Statutes of North Carolina the undersigned limited liability
company hereby submits the following Articles of Amendment for the purpose of amending its
Articles of Organization.
1. The name of the limited liability company is Chemical Specialties LLC.
2. The text of each amendment adopted is as follows:
"FIRST: The name of the corporation shall be Venator Chemicals LLC."
3. The amendment was duly adopted by the unanimous vote of the members of the limited
liability company.
4. This Amendment will be effective at 12:01 am (Eastern Time)on ICI (Y1f\l .CN ,
2018.
This the 5 day of MARCH,2018.
Chemical Specialties LLC
By: ��,.
Name: KLIZT ()GIN
Title:
(VIQ� Vl( . A JtENT AND
O-IIEE fNAkciAL (. FIC; Z