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HomeMy WebLinkAboutWQ0010657_Monitoring Reports 2016_20170203Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00010657 MONTH: December YEAR: 2016 FACILITY NAME: Badin Shores Resort COUNTY: Montgomery Flow Monitoring Point: Effluent: LJ Influent: Parameter Monitoring Point: Effluent: ❑ Influent: ❑ ISurface Water (SW): ❑ I SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: Yes: Li No: I Operator D Arrival A Time Operator ORC T 2400 Time on on E Clock Site Site? 50050 Daily Rate (Flow) into Treatment System 00400 50060 00310 00610 00530 Residual BOD -5 pH Chlorine 20°C NH -3-N TSS 31616 00094 00680 NIA Fecal Coliromi (Geo -metric Mean*) Conductivity TOC DOC HRS Y/N GPD UNITS UG/L MG/L ..MG/L MG/L /100ML µmioscm MG/L MG/L .I. • " 0840:., 0.25a,;j 2 0 4 0 F 6 0 �. ,e u 8 0 I 9 1610 -0.25 ya's 0. `ka 101 1 1 0 Operator in Responsible Charge (ORC): Glenn Price Grade: II Phone: 336-996-2841 Check Box if ORC Has Changed: ❑ ORC Certification Number: 987931/20771 Certified Laboratories (1): R & A Laboratories. Inc. (2): Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE (ii0gGE°)1t ��i Ems'`! ��i� Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. FE.9 0 e� 2017 (1n 17 RALEIGH, NC 27699-1617 tf d �r1Jh' SEC-! DENR Form NDAR-1 (5/2003) I I I I I I ---------- o . O --------- Operator in Responsible Charge (ORC): Glenn Price Grade: II Phone: 336-996-2841 Check Box if ORC Has Changed: ❑ ORC Certification Number: 987931/20771 Certified Laboratories (1): R & A Laboratories. Inc. (2): Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE (ii0gGE°)1t ��i Ems'`! ��i� Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. FE.9 0 e� 2017 (1n 17 RALEIGH, NC 27699-1617 tf d �r1Jh' SEC-! DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant ,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non-compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the informounsubmitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penal es fo submittin al information, including the possibility of fines and imprisonment for knowing violations." 11,3a 11201 James M. Cheshire AgUaftire of Pe to * D e (Name of Signing Official -Please print or type) James M. Cheshire (Authorized Agent) President R & A Laboratories (Permittee -Please print or type) 1 Clubhouse Drive New London, NC 28127 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel (Position or Title) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease WQ09 PAN Plant Available) 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W00010657 MONTH: December YEAR: 2016 FACILITY NAME: Badin Shores Resort COUNTY: Montgomery Formulas: Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feet/gallon) x 12 (Inches/foot)] / [Area Sprayed (acres) x 43,560 (square feet/acre) or _ [Volume Applied (gallons) / [Area Sprayed (acres) x 27,152 (gallons/acre-inch). Maximum Hourly Loading (inches) = Daily Loading (Inches) / [Time Irrigated (minutes) / 60 (minutes/hour)] Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (inches/month) / Number of days in the month (days/month )] x 7 (days/week) Did Irrigation Occur At This Facility: Did Irrigation Occur On This Field: Did Irrigation Occur On This Field: Yes: ❑ No: ❑ Yes: ❑ No: ® Yes: ❑ No: ❑ Field Number: 1 Field Number: 2 Area Sprayed (acres): 12.6 Area Sprayed (acres): 12.1 Cover Crop: Fescue Cover Crop: Fescue Permitted Hourly Rate (inches): 10.25 Permitted Hourly Rate (inches): 0.25 r WEATHER CONDITIONS Permitted Yearly Rale (inches): 28.5 Permitted Yearly Rate (Inches): 20.8 D A Weather Temperature Storage Maximum Maximum TL Code' at Precipila- Lagoon Volume Time Daily Hourly Volume Time Daily Hourly L application lion Frec-board Applied Irrigated Loading Loading Applied Irrigated Loading Loading ff) inches feet gallons minutes inches inches gallons minutes inches i inches Total G211nmtMonthly Loading (inches) 4 r° oa :. .^' 's,. `a :x eq..m 12 Month Floating,romi (inches) Ai-crage Weekly Loading (inches)•r �`�'".. * Weather Codes: C -clear, PC -partly cloudy, CI -cloudy, R -rain, Sn-snow, SI -sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: F Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) OBOE= EMEEM r go MEMO= Total G211nmtMonthly Loading (inches) 4 r° oa :. .^' 's,. `a :x eq..m 12 Month Floating,romi (inches) Ai-crage Weekly Loading (inches)•r �`�'".. ,,� c "€- ,, u g,y °..a,-- °;. •. p ,%;. " ec - * Weather Codes: C -clear, PC -partly cloudy, CI -cloudy, R -rain, Sn-snow, SI -sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: F Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement. does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. Eyl 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 4 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4 4. All buffer zones as specified in the permit were maintained during each application. E:�] 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the 4 limits) specified in the permit. If the facility is non-compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the mforma 'on submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant pena les #or submitting information, including the possibility of fines and imprisonment for knowing violations." v of (Permittee -Please print or type) 1 Clubhouse Drive New London, NC 28127 (Permittee Address) 3- .2d James M. Cheshire > to (Name of Signing Official -Please print or type) President R & A Laboratories (Position or Title) (Phone Number) (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 1 of 2 NUN-0ISCHARGF. WASTE �V.4TER :V10NITORING REPORT PERMI'I' NLIMBER: N'OOU106�7 N10NTH: November YEA�R: 201h PACII,ITI' V,4ME: 6adin Shores Rcsurl COUNTY: Ylunleumcrv . . . ' . ■ l� lE ■ � � . • ■ l�l •���������� . .• � ��� ��� ��������� 0���0����-���� 0�-��--------- o��ao��������� a���a��������� m���m��������� A���o��������� ����m��������� o���a��������� ����m��������� m��ao��������■� m���m���������� ����o�������■■ra�� m���m��������� ����a�����o��� ����m��������� m��aa��������� ����m��������� ����a��������� �������������� m������������� ���om��������� ����o��������� m���m��������� ����o��������� ����m��������� m���o��������� ����m��������� m���a��������� ����m��������� ����a��������� m ; . �������� m��������� m��������� ���������� ��������� Uper:imrinKespnnsiblcChar�e(ORC�: GlcnnYricc GraAe: II Phnne: 73fiAY6-2RJ1 Chcck Boz if ORC Has Chan},cd: � ORC Ccrtification Vumbcr: 9ft793U20771 Ccrlilicd L�boralorics (1): R& A I.nborulorics, Inc (2): Pcrson(s) Collcc�ing Mail ORIGIN:AI,:mA "1'��'o COPIh:S �o: ,\'1�"IT': Nun.Uisch:u'�;e Complinnce Onif UE]K ($IGN:ATOHE OI' OPEH:A"fOR IN HF.SPO,NSIBLE CHANGN:) Uicision ol' �\'aler Qualitp 6y this siFnan�re. 1 cerlify Ihat Ihis repnr� is accura�e:�nd I(iI7 Alnil Sen�ice CeNer cnmple�e In Ihe besl ul' mc Ano�� Irdge. H:U.P:IGII.\C 27699-Ifi17 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: I. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non-comnliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. Com liant Y,N) "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the inform ' ubmitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penal ies for ubmitting fal ' nf ation, including the possibility of fines and imprisonment for knowing violations." � �- 2 Z � James M. Cheshire (Si natur of Permitee ate (Name of Signing Official-Please print or type) (Permittee-Please print or type) 1 Clubhouse Drive New London. NC 28127 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BODS 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivi 01042 Co er 00300 Dissolved Ox en 31616 Fecal Coliform 01051 Lead 00927 Ma nesium 71900 Mercu 00610 NH3 as N 01067 Nickel President R & A Laboratories (Position or Title) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN Plant Available) 00400 H 32730 Phenols 00665 Phos horus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Tem erature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use onlv units designated in the reporting, facilit '�s permit for reportin data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per I SA NCAC 2B.0506 (b) (2) (D). � NON-DISCHARGE APPLICATION REPOR'I' SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED Page 2 of 2 PERMIT NUMBER: W00010657 MONTH: November YEAR: 2016 FACILITY NAME: Badin Shores Resort COUNTY: Monteomerv Formulas: Daily Loading (inches) _[Volume Applied (gallons) x 0.1336 (cubic feetlgallon) x 12 (inches/foot)] /[Area Sprayed (acres) x 43,560 (square feeUacre) or _ [Volume Applied (gallons) / [Area Sprayed (acres) x 27,152 (gallons/acre-inch). _ Maximum Hourly Loading (inches) = Daily Loading (inches) /[fime irrigated (minutes) / 60 (minutes/hour)] Monthly Loading (Inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of lhis monlh's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) _[Monthly Loading (Inches/month)! Number of days in the month (days/month )] x 7(days/week) "Wca[hcr Codcs: Gdenr, PC-partly clouJy, CI-cloudy, R-rain, Smsnow, SI-slect Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Mail ORIGINAL and Two COPIES to: ATTN: Non-Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Check Box if ORC I�as Changed� � Division of Water Quality 1617 Mail Service Center RALEIGH, NC 27699-1617 By this signature, I certify that this report is accurate and complete to the best of my Icnowledge. DENR Form NDAR-1 (5/2003) NON-DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N(o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. @ Compliant (Y,N) 4 4 If the facility is non-comnliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the informat' submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalt�es fo submitting f� �formation, including the possibility of fines and imprisonment for knowing violations." of (Permittee-Please print or type) 1 Clubhouse Drive New London, NC 28127 (Permittee Address) � D � James M. Cheshire (Name of Signing Official-Please print or type) President R & A Laboratories (Position or Title) (Phone Number) ' 'Q (Pernut Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). SUBMIT FORM ON YELLOW PAPER ONLY For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 8/2013 mg/L Effluent Total VOCs: mg/L VOC Removal% Siqnature of Permittee (or Authorized Aqent) (Date) DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearfy or Type PERMIT Number: Expiration Date: 30 -Apr -10 Facility Name: Badin Shores Resort, Inc Non -Discharge WQ0010657 UIC Permit Name (if different): NPDES Other Facility Address: No. 1 Clubhouse Drive TYPE OF PERMITTED OPERATION BEING MONITORED New London NC 28127 County Montgomery ■ Lagoon ❑ Remediation: Infiltration Gallery (city) (State) (zip) ■ Spray Field ❑ Remediation: Contact Person:. Mr. Glenn Price Telephone#: (336) 408-7924 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name NE of Sprayfield No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -6 Date sample collected: 11/8/2016 FIELD ANALYSES: WAS Well Depth: 40 ft. Well Diameter: 2 in. pH 00400: 6.7 units Temp. 000lc ts.st oC DRY at Depth to Water Level 82546: 32 .07 ft. below measuring point Screened Interval: 8 ft. to ft. Spec. Cond. 00094: 0.098 IiMhos time of Measuring Point is 2.87 ft. above land surface Relative M.P. Elevation: ft. _4.0 Odor 00065: None sampling, check Volume of water pumped/bailed before sampling: —5.25 gallons Appearance Clear _ here:[] Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/08/2016 - 11/21/2016 Laboratory Name: _ _E_ NCO Laboratories/Pace Certification No. NC 591/16 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 1 /100mL Nitrate (NO3) as N 00620 0.45 mg/L Zn - Zinc 01092 mg/L p Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L z (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units Z issolved Solids:Total 70300 BDL mg/L Al - Aluminum oil o5 mg/L < pH (Lab) 00403 6.2 units Ba - Barium 01007 ug/L TOC oo68o 1 mg/L Ca - Calcium 00916 mg/L ; Chloride 00940 4.4 JB mg/L Cd - Cadmium 01027 d ug/L _ v� Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPOI.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 BDL method # 8260B Total Ammonia oo6lo BDL mg/L Mg- Magnesium 00927 mg/L method # _ (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 8/2013 mg/L Effluent Total VOCs: mg/L VOC Removal% Siqnature of Permittee (or Authorized Aqent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 8/2013 mg/L Effluent Total VOCs: mg/L VOC Removal% Siqnature of Permittee (or Authorized Aqent) (Date) . • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 30 -Apr -10 Facility Name: Badin Shores Resort, Inc Non -Discharge W000106.57_ UIC Permit Name (if different): NPDES Other Facility Address: No. 1 Clubhouse Drive TYPE OF PERMITTED OPERATION BEING MONITORED New London NC 28127 County Montgomery ■ Lagoon ❑ Remediation: Infiltration Gallery (city) (State) (zip) ■ Spray Field ❑ Remediation: Contact Person: Mr. Glenn Price Telephone#: (336) 408-7924 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name SW of Sprayfield No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: from Permit) SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): _ _ _ _ MW -7 Date sample collected: 11/8/2016 FIELD ANALYSES: WAS Well Depth: 40 ft. Well Diameter: 2 in. pH 00400: 4.5 units Temp. 000lc 'C DRY at Depth to Water Level 82546: 26 .42 ft. below measuring point Screened Interval: 10 ft. to 40 ft. Spec. Cond. 00094: 0.068 µMhos time of sampling, Measuring Point is 1.96 ft. above land surface Relative M.P. Elevation: ft. Odor 000e5: None check Volume of water pumped/bailed before sampling: —7.5 gallons Appearance Clear here: ❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field_ acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/08/2016 -11/21/2016 Laboratory Name: ENCO Laboratories/Pace Certification No. NC 591/16 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead olo51 ug/L Coliform: MF Fecal 31616 BDL /100mL Nitrate (NO3) as N 00620 0.59 mg/L Zn -Zinc 01092 mg/L Coliform: MF Total 31504 /100mi- Phosphorus: Total as P oO665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 BDL mg/L Al -Aluminum oil o5 mg/L pH (Lab) 00403 5.6 units Ba - Barium 01007 ug/L TOG 00680 1.6 mg/L Ca - Calcium 00916 mg/L Chloride 00940 9.9 B mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 _ mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 _ mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 BD_L method # 8260B Total Ammonia 00610 BDL mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 8/2013 mg/L Effluent Total VOCs: mg/L VOC Removal% Siqnature of Permittee (or Authorized Aqent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: WIN DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 30 -Apr -1 0 Facility Name: Badin Shores Resort, Inc Non -Discharge WQ0010657 UIC Permit Name (if different): NPDES Other Facility Address: No. 1 Clubhouse Drive TYPE OF PERMITTED OPERATION BEING MONITORED New London NC 26127 County Montgomery ■ Lagoon ❑ Remediation: Infiltration Gallery (city) (State) (zip) ■ Spray Field ❑ Remediation: Contact Person: Mr. Glenn Price Telephone#: (336) 408-7924 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name South of Sprayfield No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -8 Date sample collected: 11/8/2016 FIELD ANALYSES: WAS Well Depth: 32 ft. Well Diameter: 2 in. pH 00400: 5.8 units Temp. 000l( 1764 °C DRY at Depth to Water Level 82546: 15 .56 ft. below measuring point Screened Interval: 8 ft. to 32 ft. Spec. Cond. 00094: 0.357 µMhos time of Measuring Point is 2.34 ft. above land surface Relative M.P. Elevation: ft. Odor o0o85: None sampling, check Volume of water pumped/bailed before sampling: —9.0 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/08/2016 - 11/21/2016 Laboratory Name: ENCO Laboratories/Pace Certification No. NC 591/16 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead oiosi ug[L Coliform: MF Fecal 31616 BDL /100mL Nitrate (NO3) as N 00620 0.13 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P ooms mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 140 mg/L Al -Aluminum oil o5 mg/L pH (Lab) 00403 6.6 units Ba - Barium 01007 ug/L TOC oo6so 9.1 mg/L Ca - Calcium 00916 mg/L Chloride 00940 13 B mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 BDL method # 8260B Total Ammonia 00610 1.2 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only - .. • - • • I certify that, to the best of my knowledge and belief, the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. ColwellAgentPermittee d •. Print . r. GW -59 Rev. 8/2013 SUBMIT FORM ON YELLOW PAPER ONLY For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 8/2013 mg/L Effluent Total VOCs: mg/L VOC Removal% Siqnature of Permittee (or Authorized Aqent) (Date) , • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 30 -Apr -10 Facility Name: Badin Shores Resort, Inc Non -Discharge WQ0010657 UIC Permit Name (if different): NPDES Other Facility Address: No. 1 Clubhouse Drive TYPE OF PERMITTED OPERATION BEING MONITORED New London NC 28127 County Montgomery ■ Lagoon ❑ Remediation: Infiltration Gallery (city) (state) (zip) ■ Spray Field ❑ Remediation: Contact Person: Mr. Glenn Price Telephone#: (336) 408-7924 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name NW of Sprayfield No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -9 Date sample collected: 11/8/2016 FIELD ANALYSES: WAS Well Depth: 23 ft. Well Diameter: 2 in. pH 00400: 6.1 units Temp. 000lc 1959 oC DRY at Depth to Water Level 82546: 6 .41 ft. below measuringpec. point Screened Interval: 8 ft. to 23 ft. S Cond. 00094: 0.131 µMhos time of sampling, Measuring Point is 1.36 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None check Volume of water pumped/bailed before sampling: —9 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/08/2016 - 11/21/2016 Laboratory Name: ENCO Laboratories/Pace Certification No. _ NC 591/16 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 BDL /100mL Nitrate (NO3) as N 00620 0.066 J mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 130 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 7.4 units Ba - Barium 01007 ug/L TOC oosso 0.911 mg/L Ca - Calcium oo916 mg/L Chloride 00940 4.4 JB mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 BDL method # 8260B Total Ammonia oo610 0.11 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 8/2013 mg/L Effluent Total VOCs: mg/L VOC Removal% Siqnature of Permittee (or Authorized Aqent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 812013 mg/L Effluent Total VOCs: mg/L VOC Removal% Signature of Permittee (or Authorized Aqent) (Date) . DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 30 -Apr -10 Facility Name: Badin Shores Resort, Inc Non -Discharge W00010657 UIC Permit Name (if different): NPDES Other Facility Address: No. 1 Clubhouse Drive TYPE OF PERMITTED OPERATION BEING MONITORED New London NC 28127 County Montgomery ■ Lagoon ❑ Remediation: Infiltration Gallery (city) (State) (zip) _ _ ■ Spray Field ❑ Remediation: Contact Person: Mr. Glenn Price Telephone#: (336) 408-7924 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name East of Sprayfield No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -10 Date sample collected: 11/8/2016 FIELD ANALYSES: WAS Well Depth: 50 ft. Well Diameter: 2 in. pH 0040o: 5.8 units Temp. 000lr 163 °C DRY at Depth to Water Level 82546:41 .57 ft. below measuring point Screened Interval: 5 ft. to 50 ft. Spec. Cond. 00094: 0.052 µMhos time of sampling, Measuring Point is 2.34 ft. above land surface Relative M.P. Elevation: ft. Odor 00086: check Volume of water pumped/bailed before sampling: —5.25 gallons Appearance Murky here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/08/2016 -11/21/2016 Laboratory Name: ENCO Laboratories/Pace Certification No. NC 591/16 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N oos15 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 BDL /100mL Nitrate (NO3) as N 00620 0.22 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 _ _ _ mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 BDL mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 6.2 units Ba - Barium 01007 ug/L _ TOC 00680 0.6.8_ J mg/L Ca - Calcium oo916 mg/L Chloride 00940 5.1 B mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 BDL method # 8260B Total Ammonia oo610 0.59 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 812013 mg/L Effluent Total VOCs: mg/L VOC Removal% Signature of Permittee (or Authorized Aqent) (Date) SUBMIT FORM ON YELLOW PAPER ONLY For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 812013 mg/L Effluent Total VOCs: mg/L VOC Removal% Signature of Permittee (or Authorized Apent) (Date) . • • DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER RESOURCES - INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM • • • • 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: 919-807-6306 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 30 -Apr -10 Facility Name: Badin Shores Resort, Inc Non -Discharge WQ0010657 UIC Permit Name (if different): NPDES Other Facility Address: No. 1 Clubhouse Drive TYPE OF PERMITTED OPERATION BEING MONITORED New London ---- - NC - 28127 County Montgomery ■ Lagoon ❑ Remediation: Infiltration Gallery (city) (State) (zip) ■ Spray Field ❑ Remediation: Contact Person: Mr. Glenn Price Telephone#: (336) 408-7924 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name South of New of Sprayfield No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW -11 Date sample collected: 11/8/2016 FIELD ANALYSES: WAS Well Depth: 35 ft. Well Diameter: 2 in. pH 00400: 5.5 units Temp. 000lc ts.aa oC DRY at Depth to Water Level 82546: 26 .43 ft. below measuring point Screened Interval: 5 ft. to 35 ft. Spec. Cond. 00094: 0:071 µMhos time of Measuring Point is 1.9 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: None sampling, check Volume of water pumped/bailed before sampling: —5.1 gallons Appearance Clear here:❑ Samples for metals were collected unfiltered: ❑ YES ❑ NO and field acidified: ❑ YES ❑ NO _ LABORATORY INFORMATION Date sample analyzed: 11/08/2016 - 11/21/2016 Laboratory Name: ENCO Laboratories/Pace Certification. No. NC 591/16 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 BDL /100mL Nitrate (NO3) as N 00620 0.34 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 BDL mg/L AI - Aluminum 01105 mg/L pH (Lab) 00403 6.2 units Ba - Barium 01007 ug/L TOC oomo 1.1 mg/L Ca - Calcium oo916 mg/L Chloride 00940 11 B mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total olo34 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 BDL _ , method # 82606 Total Ammonia omio 0.32 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: K. Ty Colwell -- Agent Permittee (or Authorized Aqent) Name and Title - Please print or type GW -59 Rev. 812013 mg/L Effluent Total VOCs: mg/L VOC Removal% Signature of Permittee (or Authorized Apent) (Date) Q`0- WithersRavene[ Al. Our People. Your Success. November 28, 2016 North Carolina Department of Environmental Quality Division of Water Resources, Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 RE: Trimester Groundwater Monitoring - November 2016 Wastewater Spray Irrigation Permit WQ0010657 Badin Shores Resort New London, Montgomery County, North Carolina WR Project No. 02940519.00 y NC DENR Raleigh Reglonel Office WithersRavenel, Inc. (WR) has prepared this report to document recent groundwater monitoring activities conducted on behalf of Badin Shores Resort Owners Association, Inc. The following describes the results of work completed at the above referenced site for the November 2016 trimester sampling event. Groundwater Mon itoringActivities WR mobilized to the site on November 8, 2016 to collect groundwater samples from monitoring wells MW -6, MW -7, MW -8, MW -9, MW -10, and MW -11 located at the Badin Shores Wastewater Irrigation Facility. Each well was purged and sampled in accordance with standard protocol, and the samples were analyzed as specified in the referenced permit. WR has completed and enclosed GW -59 forms, laboratory reports, and a chain - of -custody record for the collected samples. For QA/QC purposes, WR also prepared an equipment blank while on site and directed the laboratory to analyze the equipment blank and a trip blank for the parameters specified in the permit. The tabulated laboratory results presented herein (Table 1) along with historical data (Table 2) obtained during previous sampling events indicate the following: Total Organic Carbon (TOC) • All TOC concentrations were found below 10 milligrams per liter (mg/L). The TOC levels have now been at or below 10 mg/L for the last three sampling events. The overall results of the l---G-C analyses of samples collected from the monitoring wells were slightly�higher th n those observed in the July 2016 sample results. IE 0 X C=_ G CF) nrn l CD U �= �= A W ® " o - C) Of� W_ �� O_ u M15 MacKenan Drive Cary, NC 27511 6' t:91 469.3340 if: 99.467.6008 1 www.withersravenel.com I License No. C-0832 Cary FGreensboro I Pittsboro I Raleigh I Wilmington '1110 6 —.0 WithersRavenet Our People. Your Success. :Fecal C016(rm Fecal coliform was observed at a concentrations of 1 col/mL in the sample from MW -6, which is equal to the NCDEQ groundwater quality standard. • No fecal coliform was observed at concentrations above detection limits in any of the samples'from the remaining wells. A complete copy of the laboratory analytical report is attached. Conclusions Fluctuations of fecal coliform and TOC concentrations have been observed over the history of the monitoring events conducted at this site. Therefore, we recommend that sampling be continued in accordance with the terms of the permit. It is important to note, however, that no wastewater has been applied to the irrigation fields for over four years. If you have any questions, please do not hesitate to call. Sincerely WithersRavenel 1 K. Ty Colwel I Project Manager Brian J. Bellis, PG Senior Hydrogeologist cc: Mr. Ray Part, Badin Shores Resort Mr. Glenn Price, R&A Laboratories Enclosures Trimester Groundwater Monitoring - November 2016 Event Badin Shores Resort Page 2 of 2 WR Project No. 02940519.00 November 2016 WITHERS p- RAVENEL nunw , ... , ........ No. Duo tlon Data 1 CLUBHOUSE DRNE SITE MAP TABLE 1 Groundwater Analytical Results for July 2016 Sampling Event Badin Shores Resort New London, North Carolina W&R Job # 02940519.00 Analysis: Date' FecaLColiform Total Organic pH (.Q)` Total Disgolved Ammonia . Chloride, Nitrate Volatile - Carbon (TOC) Solids Nitrogen Organics; Units; _ CFU7100 mL, " mg(L ° _ ` mg%L. - -_ - - .- m9/�'.., " mg/Lw .. _ mglL _uglL (1) - MW6 11/8/2016 1.0 1.0 6.2 BDL BDL 4.4 JB 0.45 BDL MW7 11/8/2016 BDL 1.6 5.6 BDL BDL 9.9 B 0.59 BDL MW8 11/8/2016 BDL 9.1 6.6 140 1.20 13 B 0.13 BDL MW9 11/8/2016 BDL 0.91 J 7.4 130 0.11 4.4 JB 0.066 J BDL MW10 11/8/2016 BDL 0.68 J 6.2 BDL 0.59 5.1 B 0.22 BDL MW11 11/8/2016 BDL 1.1 6.2 BDL 0.32 11 B 0.34 BDL Equipment Blank 11/8/2016 BDL BDL 5.0 BDL 1.4 2.5 JB BDL BDL Trip Blank 11/8/2016 BDL BDL 4.6 BDL BDL 2.5 JB BDL BDL NCDENR.Standards or Permit.Specifications 10 N/A 500 NE 250 10 varies Concentrations in bold exceed respective NCDENR standards or permit specifications, where applicable. BDL = Below Detectable Limits. J = The value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit(MRL). Q = Analysis performed outside of method specific holding time. CFU = Colony Forming Units B = The analyte was detected in the associated method blank. D = The sample was analyzed at dilution. 1 = EPA Method 6230D/8260B N/A = Not Applicable. NE = Not Established. NT = Not Tested. * = An elevated Method Reporting Limit was recorded for these samples. According to ENCO, the higher MRL is due to higher suspended solids in the sample. TABLE 2 Historical Groundwater Results from November 1996 to Present for MW6 Badin Shores Resort New London, North Carolina W&R Job # 02940519.00 Analysis: Units: Fecal Coliform CFU/100'mL Total Organic Carbon m /L pH Units Total Dissolved; Solids m /L Amm'oniai Nitrogen, mg/L` Chloride i ; m /L Nitrate m /L Volatile Organics u /L 1 MW6 11/6/2008 BDL BDL 6.8 Q 68 BDL 8.5 B 0.94 BDL 3/10/2009 BDL 0.63 6.1 BDL 0.034 J 5.1 BDL NT 7/9/2009 BDL 0.64 6.1 38 BDL 7.4 0.64 NT 11/6/2009 23 1.00 6.4 Q 62 BDL 7.1 1.1 BDL 3/3/2010 BDL BDL 5.8 80 BDL 8.1 0.11 NT 7/15/2010 7 0.68 J 6.4 76 BDL 7.9 0.83 NT 11/8/2010 1 0.83 6.8 Q 68 BDL 8.0 0.31 BDL 3/7/2011 BDL 0.35 J 7.5 200 BDL 2.2 J 0.18 J BDL 7/6/2011 BDL 0.50 J 6.4 14 BDL 7.5 B 0.87 NT 11/3/2011 44 1.40 6.3 68 BDL 5.6 0.68 BDL 3/21/2012 BDL 0.35 J 7.6 170 BDL 4.5 J 0.05 J NT 7/10/2012 1 2.7 6.3 92 BDL 3.8 J 0.72 NT 11/6/2012 BDL 1.2 7.5 24 BDL 5.4 0.85 BDL 3/13/2013 40 2.8 6.1 180 0.059 JB 3.7 J 0.30 NT 7/17/2013 BDL BDL 5.9 42 BDL 9.8 1.9 NT 11/26/2013 BDL 1.1 7.2 86 BDL 6.9 1.0 BDL 3/28/2014 BDL .93 J 5.7 32 BDL 4.8 J BDL NT 7/7/2014 BDL 0.60 J 6.2 32 BDL 5.8 0.7 NT 11/18/2014 BDL 1.4 6.3 56 0.065 J 6.6 0.87 BDL 3/10/2015 BDL 1.5 5.6 14 BDL 3.9 J 0.33 NT 7/24/2015 BDL 0.64 J 6.7 58 BDL 6.0 0.59 NT 11/23/2015 3.1 0.34 J 5.4 BDL BDL 4.9 J 0.51 J BDL 3/22/2016 BDL 0.45 J 6.4 BDL BDL 5.3 0.48 NT 7/18/2016 BDL 0.63 J 6.5 BDL BDL 4.3 J 0.59 NT 11/8/2016 1.0 1.0 6.2 BDL BDL 4.4 JB 0.45 BDL NT = Not Tested 1 = EPA Method 6230D 2 = EPA Method 625 + 10 peaks J = Estimated Value. Detected below laboratory reporting limits. Q = Analysis performed outside of method specific holding time. B = The analyte was detected in the associated method blank. NS = Not Sampled Concentrations in bold exceed respective NCDENR standards or permit specifications, where applicable. CFU = Colony Forming Units. TABLE 2 Historical Groundwater Results from November 1996 to Present for MW7 Badin Shores Resort New London, North Carolina W&R Job # 02940519.00 Analysis: Units: Fecal Coliform CFU/100>mL Total Organic Carbon m /L pH Units TotaL Dissolved Solids m !L , Aminonia, Nitrogen m /L Chloide m /L Nitrate. j m /L Volatile Organics u /L 1 MW7 11/6/2008 BDL BDL 5.5 32 BDL 13 B BDL BDL 3/10/2009 BDL 0.94 J 5.6 20 BDL 13 0.022 J NT 7/9/2009 48 1.8 5.4 48 0.032 J 16 BDL NT 11/6/2009 31 1.5 5.4 Q 38 0.067 J 16 0.024 J BDL 3/3/2010 BDL 1.2 5.4 68 BDL 19 BDL NT 7/15/2010 1 1.3 5.4 64 BDL 18 BDL NT 11/9/2010 29 1.7 5.7 Q 28.0 BDL 21 BDL BDL 3/7/2011 1 1.2 5.8 70 BDL 21 0.14 J BDL 7/6/2011 3.1 2.3 6.0 20 0.15 26 B 0.048 J NT 11/3/2011 7.5 1.7 5.5 70 0.087 J 22 0.092 J BDL 3/21/2012 11 0.98 J 5.5 40 0.061 J 18 BDL NT 7/10/2012 2.0 1.5 5.5 100 0.049 J 17 0.045 J NT 11/6/2012 1.0 1.1 6.9 32 BDL 15 BDL BDL 3/12/2013 75.0 2.2 5.6 56 0.061 JB 14 0.730 NT 7/17/2013 BDL 0.59 J 5.7 66 BDL 13 0.082 J NT 11/26/2013 BDL 0.82 J 6.0 38 BDL 15 BDL BDL 3/28/2014 BDL 0.87 J 5.4 48 BDL 12 BDL NT 7/7/2014 BDL 0.78 J 5.2 68 BDL 14 0.16 NT 11/18/2014 5.2 2.5 5.4 86 BDL 13 0.083 J BDL 3/10/2015 BDL 1.7 5.0 22 BDL 9.6 1.10 NT 7/24/2015 BDL 1.0 5.4 BDL BDL 12 0.095 J NT 11/23/2015 BDL 1.0 5.6 BDL BDL 7.0 2.80 BDL 3/22/2016 BDL 0.75 J 5.6 BDL BDL 13.0 0.96 NT 7/18/2016 BDL 0.88 J 5.7 52 BDL 10 0.48 NT 11/8/2016 BDL 1.6 5.6 BDL BDL 9.9 B 0.59 BDL NT = Not Tested 1 = EPA Method 6230D 2 = EPA Method 625 + 10 peaks J = Estimated Value. Detected below laboratory reporting limits. Q = Analysis performed outside of method specific holding time. B = The analyte was detected in the associated method blank. NS = Not Sampled Concentrations in bold exceed respective NCDENR standards or permit specifications, where applicable. CFU = Colony Forming Units. TABLE 2 Historical Groundwater Results from November 1996 to Present for MW8 Badin Shores Resort New London, North Carolina W&R Job # 02940519.00 Analysis: Units: Fecal Coliform CFU/100 mL -Total Organic Carbon m /L OH` Units Total Dissolved Solids m 7L, Ammonia; Nitrogen. mg/ L Chloride _ { ! m /L Nitrate. i mg/L. Volatile -Organics u /L (1 MW8 11/6/2008 1.0 11 6.2 Q 160 1.4 D 14 B 0.052 J BDL 3/10/2009 BDL 15 6.4 180 1.6 9.8 0.047 J NT 7/9/2009 BDL 13 6.2 130 0.91 13 0.089 J NT 11/6/2009 BDL 10 6.3 Q 140 0.8 13 0.13 BDL 3/3/2010 BDL 11 6.3 210 0.25 14 0.088 J NT 7/15/2010 BDL 13 6.2 210 0.61 11 0.053 J NT 11/8/2010 BDL 19 6.5 Q 220 1.3 7.8 BDL BDL 3/7/2011 BDL 0.48 J 7.6 170 BDL 14 0.21 J BDL 7/6/2011 BDL 19 6.2 150 2.9 D 7.9 B 0.16 NT 11/3/2011 11.0 4.1 6.1 220 3.4 D 6.9 0.078 J BDL 3/21/2012 BDL 12 6.2 130 2.8 D 7.7 0.047 J NT 7/10/2012 BDL 18 6.4 200 2.6 D 22 0.13 NT 11/6/2012 2.0 13 6.3 150 1.500 12 0.11 BDL 3/12/2013 BDL 12 6.3 180 0.41 BD 10 0.13 NT 7/17/2013 BDL 12 6.2 140 1.6 8.9 0.13 NT 11/26/2013 BDL 14 6.2 120 2.5 D 12 0.099 J BDL 3/28/2014 BDL 13 6.4 160 1.2 D 10 BDL NT 7/7/2014 BDL 8.1 6.2 190 0.96 12 0.11 NT 11/18/2014 BDL 8.1 6.2 180 2.1 D 16 0.11 BDL 3/10/2015 BDL 9.8 6.2 110 1.2 D 13 0.17 NT 7/24/2015 BDL 9.9 6.4 150 1.10 14 0.096 J NT 11/23/2015 BDL 11 6.3 140 1.10 11 BDL BDL 3/22/2016 BDL 10 6.8 110 1.20 15 0.091 J NT 7/18/2016 BDL 7.6 6.3 120 0.87 15 1 0.13 NT 11/8/2016 BDL 9.1 6.6 140 1.20 13 B 0.13 BDL NT = Not Tested 1 = EPA Method 6230D 2 = EPA Method 625 + 10 peaks J = Estimated Value. Detected below laboratory reporting limits. Q = Analysis performed outside of method specific holding time. B = The analyte was detected in the associated method blank. NS = Not Sampled D = This sample was analyzed at dilution. Concentrations in bold exceed respective NCDENR standards or permit specifications, where applicable. CFU = Colony Forming Units. TABLE 2 Historical Groundwater Results from November 1996 to Present for MW9 Badin Shores Resort New London, North Carolina W&R Job # 02940519.00 Analysis: Units: Fecal Coliform CFU/100 r Total Organic Carbon m IL pH units, Total Dissolved Solids m IL Ammoniai Nitrogen. i mg/L' Chloride m !L Nitrate m /L Volatile Organics u IL 1 Mw9 11/6/2008 BDL BDL 7.4 Q 160 BDL 1.8 JB BDL BDL 3/10/2009 BDL 0.40 J 7.9 170 BDL BDL 0.039 J NT 7/9/2009 BDL 0.40 J 7.6 170 BDL 4.2 J 0.035 J NT 11/6/2009 6 Q 0.52 J 7.4 Q 160 BDL 5.2 0.061 J BDL 3/3/2010 BDL BDL 7.5 180 BDL 1.9 J BDL NT 7/15/2010 2 0.88 J 7.3 200 BDL 4.5 J 0.049 J NT 11/9/2010 5 0.74 J 7.8 Q 140 BDL 3.7 0.029 J BDL 3/7/2011 BDL 0.55 J 7.6 180 BDL 1.9 J 0.15 J BDL 7/6/2011 BDL 0.39 J 7.8 100 BDL 4.4 JB 0.059 J NT 11/2/2011 2 0.94 J 6.7 170 BDL 13 0.069 J BDL 3/21/2012 BDL 0.48 J 7.6 160 BDL 4.6 J 0.068 J NT 7/11/2012 190 1.3 7.0 190 BDL 3.7 J 0.034 J NT 11/6/2012 BDL 1.1 7.6 190 BDL 6.4 0.049 J BDL 3/12/2013 BDL 0.71 J 7.5 170 0.055 JB 5.7 0.160 NT 7/17/2013 BDL BDL 7.8 170 BDL BDL 0.065 J NT 11/26/2013 390 0.64 J 7.2 56 BDL 6.1 BDL BDL 3/28/2014 BDL 0.52 J 7.9 140 BDL 2.1 J BDL NT 7/7/2014 BDL BDL 7.5 160 BDL 2.9 J BDL NT 11/18/2014 BDL 1-.1 6.6 100 BDL 5.7 0.097 J BDL 3/10/2015 BDL 1.5 7.2 160 BDL 3.7 J 0.12 NT 7/24/2015 11 0.51 J 6.5 76 BDL 5.9 B 0.14 NT 11/23/2015 BDL BDL 7.2 160 BDL 3.8 J 0.21 J BDL 3/22/2016 BDL BDL 7.8 160 BDL 3.2 J BDL NT 7/18/2016 BDL 0.51 J 7.9 130 BDL 2.9 J BDL NT 11/8/2016 BDL 0.91 J 7.4 130 0.110 4.4 JB 0.066 J BDL NT = Not Tested 1 = EPA Method 6230D 2 = EPA Method 625 + 10 peaks J = Estimated Value. Detected below laboratory reporting limits. Q = Analysis performed outside of method specific holding time. B = The analyte was detected in the associated method blank. NS = Not Sampled Concentrations in bold exceed respective NCDENR standards or permit specifications, where applicable. CFU = Colony Forming Units. TABLE 2 (Continued) Historical Groundwater Results from October 2005 to Present for MW -10 Badin Shores Resort New London, North Carolina W&R Job # 02940519.00 Analysis: Units: Fecal Coliform CFUI100 mL_.- Total Organic -Carbon mg/L,__ _ pW Units. --- Total Dissolved Ammonia Solids Nitrodeo -_ _ m /L _ .m /L Chloride m IL-- -__-' Nitrate m !L _-_ , . Volatile ' Organics _. v !L 7 .- MW10 10/7/2005 4 BDL 5.55 70 BDL 7 BDL NT 11/8/2005 590 3.7 6.24 62 0.1 7 BDL BDL 12/20/2005 4 NT NT NT NT NT NT NT 1/4/2006 BDL NT NT NT NT NT NT NT 3/16/2006 101 3.1 6.28 89 BDL 6 BDL NT 7/11/2006 BDL BDL 6.35 23 BDL 4 BDL NT 11/28/2006 BDL 2.0 5.39 39 0.04 J 5.1 0.62 BDL 3/6/2007 BDL 2.5 6.5 Q 82 0.04 J 10 0.48 NT 7/10/2007 BDL 0.84 J 6.3 Q 46 0.035 J 2.4 0.072 J NT 11/6/2007 BDL 3.5 6.1 Q 26 0.046 J 7.4 BDL BDL 3/4/2008 BDL 0.98 J 6.4 Q 62 0.033 JB 6.4 B 0.37 NT 7/28/2008 BDL BDL 6.3 54 0.015 JB 3.3 JB 0.11 B NT 11/6/2008 BDL BDL 6.6 Q 110 BDL 10B 0.15 BDL 3/11/2009 BDL 0.46 J 6.2 52 0.06 J 2.7 J 0.060 J NT 7/9/2009 2.0 1.7 5.9 36 BDL 5.2 0.12 NT 11/6/2009 BDL 0.83 J 6.1 Q 42 BDL 4.5 J 0.13 BDL 3/3/2010 BDL BDL 5.8 58 BDL 5.3 J 0.093 J NT 7/15/2010 BDL 0.64 J 5.9 68 BDL 6 0.16 NT 11/8/2010 16 1.2 6.4 Q 58 BDL 7.1 BDL BDL 3/7/2011 BDL 0.37 J 7.6 190 BDL 2.6 J 0.16 J BDL 7/6/2011 6.3 1.4 6.4 BDL BDL 8.9 B 0.37 NT 11/2/2011 1.0 0.70 J 5.8 62 BDL 8.8 0.39 BDL 3/21/2012 2.0 0.42 J 6.2 46 BDL 4.0 J 0.17 NT 7/10/2012 1.0 1.8 6.0 84 BDL 3.3 J 0.25 NT 11/6/2012 BDL 0.4 J 6.9 110 BDL 4.0 J 0.22 BDL 3/13/2013 26.0 0.87 J 6.2 120 0.054 JB 6.6 0.23 NT 7/17/2013 BDL BDL 6.1 30 BDL 3.1 J 0.14 NT 11/26/2013 BDL 0.47 J 6.1 16 BDL 9.5 0.68 BDL 3/28/2014 BDL 0.99 J 6.0 38 BDL 2.9 J BDL NT 7/7/2014 BDL BDL 5.8 38 BDL 5.3 0.33 NT 11/18/2014 BDL 0.48 J 6.0 46 BDL 6.4 0.25 BDL 3/10/2015 BDL 1.6 5.8 42 BDL 4.0 J 0.22 NT 7/24/2015 BDL 0.39 J 6.0 BDL BDL 4.9 JB 0.26 NT 11/23/2015 4.1 1.7 6.0 54 BDL 4.9 J 0.32 J BDL 3/22/2016 BDL 0.74 J 6.1 54 BDL 4.7 J 0.22 NT 7/18/2016 BDL 1.3 6.3 BDL BDL 5.2 0.30 NT 11/8/2016 BDL 0.68 J 6.2 BDL 0.590 5.1 B 0.22 BDL J =Estimated Value. Detected below laboratory reporting limits. NT= Not Tested 1 =EPA Method 6230D B = The analyte was detected in the associated method blank. Q = Analysis performed outside of method specific holding time. 2 = EPA Method 625 + 10 Peaks NS = Not Sampled BDL = Below Detection Limit CFU = Colony Forming Units. TABLE 2 (Continued) Historical Groundwater Results from October 2005 to Present for MW -11 Badin Shores Resort New London, North Carolina W&R Job # 02940519.00 Analysis: Units: Fecal Coliform CFUA00 mL Total Organic Carbon mg/L- pH Units' Total Dissolved Solids mg/L ;Ammonia Nitrogen nig/L Chloride mg/L Nitrate mg/L Volatile organics ug/L (1) MW71 10/7/2005 BDL 2.3 5.56 69 BDL 7 0.5 NT 11/8/2005 370 4.3 6.19 69 0.1 9 BDL BDL 12/20/2005 12 NT NT NT NT NT NT NT 1/4/2006 6 NT NT NT NT NT NT NT 3/16/2006 5 3.2 5.92 62 BDL 14 BDL NT 7/11/2006 BDL 7.0 6.34 184 BDL 6 BDL NT 11/28/2006 1 1.0 5.67 49 0.04 J 3.4 BDL BDL 3/6/2007 BDL 0.86 J 5.9 Q 32 0.03 J 6 0.07J NT 7/10/2007 BDL 1.5 8.3 Q 62 0.03 J 3.7 0.18 NT 11/6/2007 BDL 7.1 5.8 Q 76 0.052 J 5.9 0.4 BDL 3/4/2008 BDL 0.63 J 6.3 Q 62 BDL 3.3 JB 0.085 J NT 7/28/2008 BDL BDL 6.0 32 0.014 JB 5.7 B 0.42 B NT 11/6/2008 BDL BDL 6.4 Q 94 BDL 2.7 B 0.77 J BDL 3/11/2009 BDL 0.95 J 5.8 62 0.079 J 4.2 J 0.48 NT 7/9/2009 BDL 3.7 6.1 52 BDL 7.3 0.53 NT 11/6/2009 BDL 1.6 5.7 Q 54 BDL 8.4 0.46 BDL 3/3/2010 BDL 0.42 J 5.5 44 BDL 5.1 0.58 NT 7/15/2010 BDL 1.0 5.9 98 BDL 8.5 0.32 NT 11/8/2010 BDL 1.2 5.8 Q 38 BDL 6.7 BDL BDL 3/7/2011 BDL 0.20 J 5.6 38 BDL 7.5 0.83 J BDL 7/6/2011 BDL 1.7 6.0 24 BDL 8.1 B 0.7 NT 11/2/2011 BDL 0.51 J 5.5 44 BDL 8.5 0.68 BDL 3/21/2012 BDL 0.40 J 5.9 40 BDL 6.5 0.56 NT 7/10/2012 BDL 4.2 5.9 130 0.0511 7.6 0.58 NT 11/6/2012 BDL 0.81 J 6.7 160 BDL 9 0.36 BDL 3/12/2013 BDL 1 6.3 160 0.062 JB 8.2 0.58 NT 7/17/2013 BDL BDL 5.8 44 BDL 7.5 0.48 NT 11/26/2013 BDL 0.55 J 6.5 18 BDL 5.9 0.31 BDL 3/28/2014 BDL 0.81 J 6.0 52 BDL 7.2 BDL NT 7/7/2014 BDL 0.39 J 5.6 44 BDL 7.4 0.46 NT 11/18/2014 BDL 0.66 J 5.6 34 0.045 J 11 0.53 BDL 3/10/2015 BDL 1.2 5.5 12 BDL 8.1 0.52 NT 7/24/2015 BDL 0.47 J 5.9 BDL BDL 10B 0.52 NT 11/23/2015 BDL 0.69 J 5.7 56 BDL 9.3 0.51 J BDL 3/22/2016 BDL 0.69 J 6.0 BDL BDL 7.3 0.25 NT 7/18/2016 BDL 0.72 J 5.8 BDL BDL 8.6 0.48 NT 11/8/2016 BDL 1.1 6.2 BDL 0.320 11 B 0.34 BDL J =Estimated Value. Detected below laboratory reporting limits. NT= Not Tested 1 =EPA Method 6230D B = The analyte was detected in the associated method blank. Q = Analysis performed outside of method specific holding time. 2 =EPA Method 625 + 10 NS = Not Sampled BDL = Below Detection Limit CFU = Colony Forming Units. V pCr O ENCO. Erle Z . bora to �BQRa�coR Accurate. Timely. Responsive., .innovative® 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Monday, November 21, 2016 Withers & Ravenel Environmental (WI009) Attn: Ty Colwell 115 MacKenan Drive Cary, NC 27511 RE: Laboratory Results for Project Number: 02940519.00, Project Blame/Desc: Badin Shores -November ENCO Workorder(s): CZ16292 Dear Ty Colwell, Enclosed is a copy of your laboratory report for test samples received by our laboratory on Tuesday, November 8, 2016. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, Chuck Smith Project Manager Enclosure(s) FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 1 of 30 SCC-, y www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: MW -6 12/06/16 Lab ID: 0216292-01 Sampled: 11/08/16 13:25 Received: 11/08/16 16.58 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 11/08/16 21:20 11/09/16 15:04 11/08/16 17:00 11/09/16 11:50 EPA 350.1 12/06/16 11/22/16 11/15/16 09:03 11/15/16 11:45 EPA 353.2 11/10/16 13:25 11/09/16 08:01 11/09/16 09:39 EPA 353.2 12/06/16 14:00 11/18/16 08:21 11/18/16 12:21 EPA 353.2 08/04/19 11/21/16 10:17 11/21/16 11:03 EPA 826013/62301) 11/22/16 11/08/16 11/09/16 10:34 11/09/16 20:35 SM 2540C-1997 11/15/16 10:20 11/10/16 15:00 11/10/16 15:00 SM 4500CIE-1997 12/06/16 11:37 11/16/16 08:00 11/16/16 10:01 SM 4500H+&2000 11/08/16 13:39 11/11/16 10:20 11/11/16 10:20 SM 53108-2000 12/06/16 Hold Date/Timefs) 11/11/16 11:37 11/11/16 12:06 Client ID: MW -7 Date/Time(s) Colilert 18 Lab ID: CZ16292-02 Sampled: 11/08/16 14:35 Received: 11/08/16 16:58 Parameter Hold Date/Time(s) Prep Date/Time(s) 11/09/16 Analysis Date/Time(s) Colilert 18 11/08/16 22:30 11/09/16 15:04 11/08/16 17:00 11/09/16 11:50 EPA 350.1 12/06/16 EPA 353.2 11/15/16 - 09:03 11/15/16 11:47 EPA 353.2 11/10/16 14:35 11/09/16 08:01 11/09/16 09:40 EPA 353.2 12/06/16 11/18/16 08:21 11/18/16 12:23 EPA 353.2 08/04/19 11/21/16 10:17 11/21/16 11:03 EPA 826013/62301) 11/22/16 11/09/16 10:34 11/09/16 21:05 SM 2540C-1997 11/15/16 11/10/16 14:00 11/10/16 14:00 SM 4500CIE-1997 12/06/16 11/16/16 08:00 11/16/16 10:01 SM 4500H+B-2000 11/08/16 14:49 11/11/16 10:20 11/11/16 10:20 SM 53108-2000 12/06/16 11/11/16 11:37 11/11/16 12:06 Client ID: MW -8 Lab ID: CZ16292-03 Sampled: 11/08/16 13:00 Received: 11/08/16 16:58 Parameter Hold Date/Timefs) Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 11/08/16 20:55 11/09/16 15:04 11/08/16 17:00 11/09/16 11:50 EPA 350.1 12/06/16 11/15/16 09:03 11/15/16 11:49 EPA 353.2 11/10/16 13:00 11/09/16 06:01 11/09/16 09:41 EPA 353.2 12/06/16 11/18/16 08:21 11/18/16 12:24 EPA 353.2 08/04/19 11/21/16 10:17 11/21/16 11:03 EPA 82606/62301) 11/22/16 11/09/16 10:34 11/09/16 21:33 SM 2540C-1997 11/15/16 11/10/16 14:00 11/10/16 14:00 SM 4500CIE-1997 12/06/16 11/16/16 08:00 .11/16/16 10:02 SM 4500H+B-2000 11/08/16 13:14 11/11/16 10:20 11/11/16 10:20 SM 53106-2000 12/06/16 11/11/16 11:37 11/11/16 12:06 Client ID: MW -9 Lab ID: CZ16292-04 Sampled: 11/08/16 14:55 Received: 11/08/16 16:58 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 11/08/16 22:50 11/09/16 15:04 11/08/16 17:00 11/09/16 11:50 EPA 350.1 12/06/16 11/15/16 07:49 11/15/16 08:55 EPA 353.2 11/10/16 14:55 11/09/16 08:01 11/09/16 09:44 EPA 353.2 12/06/16 11/18/16 08:21 11/18/16 12:25 EPA 353.2 08/04/19 11/21/16 10:17 11/21/16 11:03 EPA 82606/62301) 11/22/16 11/09/16 10:34 11/09/16 22:03 SM 254OC-1997 11/15/16 11/10/16 14:00 11/10/16 14:00 SM 45000E-1997 12/06/16 11/16/16 08:00 11/16/16 10:02 SM 4500H+B-2000 11/08/16 15:09 11/11/16 10:20 11/11/16 10:20 SM 53106-2000 12/06/16 11/11/16 11:37 11/11/16 12:06 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 2 of 30 (FJ�Cme) www.encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: MW -10 12/06/16 EPA 353.2 Lab ID: CZ16292-05 Sampled: 11/08/16 12:00 Received: 11/08/16 16:58 Parameter Hold Date/Time(s) 11/10/16 14:00 Prep Date/Time(s) 14:00 11/16/16 Analysis Date/Time(s) 11:37 Colilert18 11/08/16 19:55 11/09/16 15:04 11/08/16 17:00 11/21/16 11/09/16 11:50 EPA 8260B/6230D EPA 350.1 12/06/16 11/09/16 10:34 11/15/16 07:49 11/15/16 11/15/16 08:59 14:00 EPA 353.2 11/10/16 12:00 11/09/16 08:01 11/16/16 11:37 11/09/16 09:45 12:14 EPA 353.2 12/06/16 11/11/16 10:20 SM 5310B-2000 11/18/16 08:21 11/11/16 11/18/16 12:26 Client ID: Trip Blank EPA 353.2 08/04/19 Lab ID: CZ16292-08RE2 Sampled: 11/08/16 12:00 Received: 11/08/16 16:58 11/21/16 10:17 Prep Date/Timefs) 11/21/16 11:03 EPA 350.1 EPA 8260B/6230D 11/22/16 11/15/16 07:49 11/09/16 10:34 11/09/16 22:32 SM 2540C-1997 11/15/16 11/10/16 14:00 11/10/16 14:00 SM 4500CIE-1997 12/06/16 11/16/16 08:00 11/16/16 10:03 SM 4500H+B-2000 11/08/16 12:14 11/11/16 10:20 11/11/16 10:20 SM 5310B-2000 12/06/16 11/11/16 11:37 11/11/16 12:06 Client ID: MW -S1 Lab ID: CZ16292-06 Sampled: 11/08/16 12:25 Received: 11/08/16 16:58 Parameter Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) Colilert18 11/08/16 20:20 11/09/16 15:04 11/08/16 17:00 11/09/16 11:50 EPA 350.1 12/06/16 11/15/16 07:49 11/15/16 09:01 EPA 353.2 11/10/16 12:25 11/09/16 08:01 11/09/16 09:46 EPA 353.2 12/06/16 11/18/16 08:21 11/18/16 12:27 EPA 353.2 08/04/19 11/21/16 10:17 11/21/16 11:03 EPA 8260B/6230D 11/22/16 11/09/16 10:34 11/09/16 23:01 SM 2540C-1997 11/15/16 11/10/16 14:00 11/10/16 14:00 SM 4500CIE-1997 12/06/16 11/16/16 08:00 11/16/16 10:05 SM 4500H+B-2000 11/08/16 12:39 11/11/16 10:20 11/11/16 10:20 SM 5310B-2000 12/06/16 11/11/16 11:37 11/11/16 12:06 Client ID: Equipment Blank #1 Lab ID: CZ16292-07 Sampled: 11/08/16 14:00 Received: 11/08/16 16:58 Parameter Hold Date/Time(s) Prep Date/Timefs) Analysis Date/Time(s) Colilert18 11/08/16 21:55 11/69/16 15:04 11/08/16 17:00 11/09/16 11:50 EPA 350.1 12/06/16 11/15/16 07:49 11/15/16 09:04 EPA 353.2 11/10/16 14:00 11/09/16 08:01 11/09/16 09:47 EPA 353.2 12/06/16 EPA 353.2 08/04/19 EPA 8260B/6230D 11/22/16 SM 254OC-1997 11/15/16 SM 4500CI E-1997 12/06/16 SM 45001-1+6-2000 11/08/16 14:14 11/16/16 14:51 11/16/16 16:30 11/21/16 10:17 11/21/16 11:03 11/09/16 10:34 11/09/16 23:30 11/10/16 14:00 11/10/16 14:00 11/16/16 08:00 11/16/16 11:37 11/11/16 10:20 11/11/16 10:20 SM 53108-2000 12/06/16 11/11/16 11:37 11/11/16 12:06 Client ID: Trip Blank Lab ID: CZ16292-08 Sampled: 11/08/16 12:00 Received: 11/08/16 16:58 Parameter Hold Date/Time(s) Prep Date/Timefs) Analysis Date/Timefs) Colilert18 X1/08/16 19:55 11/09/16 15:04 11/08/16 17:00 11/09/16 11:50 EPA 353.2 11/10/16 12:00 11/09/16 08:01 11/09/16 09:49 EPA 353.2 12/06/16 11/16/16 14:51 11/16/16 16:32 EPA 353.2 08/04/19 11/21/16 10:17 11/21/16 11:03 EPA 8260B/6230D 11/22/16 11/09/16 10:34 11/09/16 23:59 SM 2540C-1997 11/15/16 11/10/16 14:00 11/10/16 14:00 SM 4500CIE-1997 12/06/16 11/16/16 08:00 11/16/16 11:37 SM 45001-1+6-2000 11/08/16 12:14 11/11/16 10:20 11/11/16 10:20 SM 5310B-2000 12/06/16 11/11/16 11:37 - 11/11/16 12:06 Client ID: Trip Blank Lab ID: CZ16292-08RE2 Sampled: 11/08/16 12:00 Received: 11/08/16 16:58 Parameter Hold Date/Timefs) Prep Date/Timefs) Analysis Date/Timefs) EPA 350.1 12/06/16 11/15/16 07:49 11/15/16 13:14 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 3 of 30 eco www.encolabs.com I Client ID: MW -7 Lab ID: CZ16292-02 Anae Results SAMPLE DETECTION SUMMARY MDL PPL unfts Client ID: MW -6 Notes Lab ID: CZ16292-01 9.9 B Analyte' Results Flaci L POL Units Method Notes Chloride 4.4 JB 1.9 5.0 mg/L SM 4500CI E-1997 3-01 Coliform, Fecal 1.0 1.0 1.0 MPN/100 mL Colilert 18 Nitrate as N 0.45 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.45 0.041 0.10 mg/L EPA 353.2 pH 6.2 1.0 1.0 pH SM 45001-1+6-2000 Q-01 Total Organic Carbon 1.0 0.34 1.0 mg/L SM 53108-2000 I Client ID: MW -7 Lab ID: CZ16292-02 Anae Results Flag MDL PPL unfts Method Notes Chloride 9.9 B 1.9 5.0 mg/L SM 4500CI E-1997 J-01 Nitrate as N 0.59 B 0.025 0.10 mg/L EPA 353.2 3-01 Nitrate/Nitrite as N 0.59 0.041 0.10 mg/L EPA 353.2 pH 5.6 1.0 1.0 pH SM 4500H+B-2000 ¢Ol Total Organic Carbon 1.6 0.34 1.0 mg/L_ SM 5310B-2000 Q-01 Client ID: MW -8 1.1 Lab ID: CZ16292-03 mg/L SM 531OB-2000 Anal a Results F iq MDL PPL Units Method Notes Ammonia as N 1.2 Flag 0.045 0.10 mg/L EPA 350.1 Notgs Chloride 13 B 1.9 5.0 mg/L SM 4500CI E-1997 J-01 Nitrate as N 0.086 J 0.025 0.10 mg/L EPA 353.2 3-01 Nitrate/Nitrite as N 0.086 J 0.041 0.10 mg/L EPA 353.2 ¢Ol pH 6.6 1.0 1.0 pH SM 4500H+B-2000 ¢01 Total Dissolved Solids 140 Flact 50 50 mg/L SM 2540C-1997 Notes Total Organic Carbon 9.1 JB 0.34 1.0 mg/L SM 531OB-2000 1-01 Client ID: MW -9 4.6 Lab ID: CZ16292-04 pH SM 4500H+B-2000 Q-01 Analyte Resutts FlanIDLj SQL Units Method Notes Ammonia as N 0.11 0.045 0.10 mg/L EPA 350.1 Chloride 4.4 JB 1.9 5.0 mg/L SM 450001 E-1997 J-01 Nitrate as N 0.066 J 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.066 J 0.041 0.10 mg/L EPA 353.2 pH 7.4 1.0 1.0 pH SM 4500H+B-2000 (-01 Total Dissolved Solids 130 50 50 mg/L SM 2540C-1997 Total Organic Carbon 0.91 J 0.34 1.0 mg/L SM 531OB-2000 Client ID: MW -10 Lab ID: CZ16292-05 Analyte Results Flag L Pg Units Method Notes Ammonia as N 0.59 0.045 0.10 mg/L EPA 350.1 Chloride 5.1 B 1.9 5.0 mg/L SM 4500CI E-1997 J-01 Nitrate as N 0.22 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.22 0.041 0.10 mg/L EPA 353.2 pH 6.2 1.0 1.0 pH SM 4500H+B-2000 ¢01 Total Organic Carbon 0.68 J 0.34 1.0 ma/L SM 531OB-2000 I Client ID: MW -11 Lab ID: CZ16292-06 I Analyte Re-sultsFlan MDL POLL Units Method Notgs Ammonia as N 0.32 0.045 0.10 mg/L EPA 350.1 Chloride 11 B 1.9 5.0 mg/L SM 4500CI E-1997 3-01 Nitrate as N 0.34 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.34 0.041 0.10 mg/L EPA 353.2 pH 6.2 1.0 1.0 pH SM 4500H+B-2000 Q-01 Total Organic Carbon 1.1 0.34 1.0 mg/L SM 531OB-2000 Client ID: Equipment Blank #1 Lab ID: CZ16292-07 Anal a Results Flag MDL E91 Units Method Notgs Ammonia as N 1.4 0.045 0.10 mg/L EPA 350.1 Chloride 2.5 JB 1.9 5.0 mg/L SM 45000 E-1997 3-01 pH 5.0 1.0 1.0 pH SM 4500H+B-2000 ¢Ol Client ID: Trip Blank Lab ID: CZ16292-08 Anal e Results Flact MDL POL, Units Method Notes Chloride 2.5 JB 1.9 5.0 mg/L SM 4500CI E-1997 1-01 pH 4.6 1.0 1.0 pH SM 4500H+B-2000 Q-01 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 of 30 (� C� www.encolabs.com ANALYTICAL RESULTS Description: MW -6 Lab Sample ID:CZ16292-01 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 13:25 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 30 (Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flaa Units DF MDL POL Batch Method Analyzed AM Notes 1,1,1,2 -Tetrachloroethane [630-20-6]A 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,1,1 -Trichloroethane [71-55-6]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK 1,1,2,2 -Tetrachloroethane [79-34-5]A 0.085 U ug/L 1 0.085 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,1,2 -Trichloroethane [79-00-5]A 0.068 U ug/L 1 0.068 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,1-Dichloroethane [75-34-3]A 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,1-Dichloroethene [75-35-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,1-Dichloropropene [563-58-6]A 0.063 U ug/L 1 0.063 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK 1,2,3-Trichlorobenzene [87-61-6]A 0.25 U ug/L 1 0.25 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,2,3-Tdchloropropane[96-18-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,2,4-Trichlorobenzene [120-82-1]A 0.097 U ug/L 1 0.097 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK 1,2,4-Trimethylbenzene [95-63-6]A 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 82608/62301) 11/09/16 20:35 MRK 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,2-Dibromoethane[106-93-4]A 0.27 U ug/L 1 0.27 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,2 -Dichlorobenzene [95-50-1]A 0.062 U ug/L 1 0.062 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,2-Dichloroethane [107-06-2]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK 1,2-Dichloropropane [78-87-5]A 0.098 U ug/L 1 0.098 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,3,5-Trimethylbenzene [108-67-8]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,3 -Dichlorobenzene [541-73-1]A 0.092 U ug/L 1 0.092 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK 1,3-Dichloropropane [142-28-9]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 1,4 -Dichlorobenzene [106-46-7]A 0.10 u ug/L 1 0.10 0.50 6KC9024 EPA 8260B/6230D 11/09/16 20:35 MRK 2,2-Dichloropropane [594-20-7]A 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK 2-Chlorotoluene [95-49-8]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 4-Chlorotoluene [106-43-4]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK 4-Isopropyltoluene [99-87-6]A 0.066 U ug/L 1 0.066 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK Benzene [71-43-2]A 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Bromobenzene [108-86-1]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 82608/62301) 11/09/16 20:35 MRK Bromochloromethane [74-97-5]A 0.11 u ug/L 1 0.11 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK Bromodichloromethane [75-27-4]A 0.010 U ug/L 1 0.010 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Bromoform [75-25-2]A 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Bromomethane [74-83-9]A 0.28 U ug/L 1 0.28 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Carbon Tetrachloride [56-23-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Chlorobenzene [108-90-7]A 0.069 U ug/L 1 0.069 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Chloroethane [75-00-3]A 0.1B U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK Chloroform [67-66-3]A 0.083 U ug/L 1 0.083 0.50 6K09024 EPA 8260B/6230D 11/09/16 20:35 MRK Chloromethane [74-87-3]A 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK cis-1,2-Dichloroethene [156-59-2]A 0.075 U ug/L 1 0.075 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK cis-1,3-Dichloropropene [10061-01-5]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/62301) 11/09/16 20:35 MRK Dibromochloromethane [124-48-1]A 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK Dibromomethane [74-95-3]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Dichlorodifluoromethane [75-71-B]A 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Ethylbenzene [100-41-4]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK Hexachlorobutadiene [87-68-3]A 0.15 U ug/L 1 0.15 0.50 6KC9024 EPA 8260B/6230D 11/09/16 20:35 MRK Isopropyl Ether [108-20-3]A 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK Isopropylbenzene [96-82-8]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 82606/62301) 11/09/16 20:35 MRK m,p-Xylenes[108-38-3/106-42-3]A 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Methylene Chloride [75-09-2]A 0.070 U ug/L 1 0.070 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Methyl-tert-Butyl Ether [1634-04-4]A 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 5 of 30 El�ICO www.encolabs.com ANALYTICAL RESULTS Description: MW -6 Lab Sample ID: CZ16292-01 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 13:25 Work Order: CZ16292 Project: Badin Shores -November Sampled By:Paul Morris Analyte rCAS Numberl Results Volatile Organic Compounds by GCMS POL Batch Method Analyzed Ay Notes Coliform, FecalA 1.0 MPN/100 mL 1 1.0 ' ^ - ENCO Cary certified analyte [NC 591] ^ - ENCO Cary certified analyte [NC 591] RAY Classical Chemistry Parameters Analyte rCAS Numberl Results Flag ni PF MDL PPL, Batch Method Analyzed By Notes Naphthalene [91-20-3]A 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK n -Butyl Benzene [10451-8]A 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK n -Propyl Benzene [103-65-1]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK o -Xylene [95-47-6]A 0.088 U ug/L 1 0.088 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK sec-Butylbenzene [135-98-8]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Styrene [100-42-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK tert-Butylbenzene [98-06-6]A 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Tetrachloroethene [127-18-4]A 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Toluene [108-88-3]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK trans-1,2-Dichloroethene [156-60-5]A 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK trans-1,3-Dichloropropene [10061-02-6]A 0.080 U ug/L 1 0.080 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Trichloroethene [79-01-6]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Trichlorofluoromethane [75-69-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Vinyl chloride [75-01-4]A 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Xylenes (Total) [1330-20-7]A 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 8260B/6230D 11/09/16 20:35 MRK Surrogates R su/ DF PikeLv/ S %Rec "/oRecLim its Batch Method Ana/vied By Notes 4-Bromofluorobenzene 48 1 50.0 96961 53-136 6K09024 EPA 82608/62306 11/09/1620.35 MRK Dibromofluoromethane 51 1 50.0 102 % 67-129 6K09024 EPA 82608/62306 11/09/16 20:35 MRK Toluene -d8 50 1 50.0 99% 59-134 6K09024 EPA 82608/62306 11/09/16 2035 MRK Analyte rCAS Numberl Results (Classical Chemistry Parameters POL Batch Method Analyzed Ay Notes Coliform, FecalA 1.0 MPN/100 mL 1 1.0 6K10025 Colilert 18 ^ - ENCO Cary certified analyte [NC 591] RAY Classical Chemistry Parameters A - ENCO Odando certlfied analyte [NC 424] Analyte rCAS Numberl Results Flan nits DF MDL PDL Batch Method na Notes Ammonia as N [7664-41-7]A 0.045 U mg/L 1 0.045 0.10 6K15006 EPA 350.1 11/15/16 11:45 JLI Chloride [16887-00-6]A 4.4 JB mg/L 1 1.9 5.0 6K16004 SM 4500CI E-1997 11/16/16 10:01 JLI 1-01 Nitrate as N [14797-55-8]A 0.45 mg/L 1 0.025 0.10 61<21022 EPA 353.2 11/21/16 11:03 JLI Nitrate/Nitrite as NA 0.45 mg/L 1 0.041 0.10 6K18005 EPA 353.2 11/18/16 12:21 JU Nitrite as N [14797-65-0]A 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:39 JLI pHA 6.2 pH 1 1.0 1.0 6K11010 3M 4500H+B-200C 11/11/16 10:20 MKS ¢01 Total Dissolved SolidsA 50 U mg/L 1 50 50 6K10004 SM 254OC-1997 11/10/16 15:00 MMR Microbiological Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flan ni DF POL Batch Method Analyzed Ay Notes Coliform, FecalA 1.0 MPN/100 mL 1 1.0 6K10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters A - ENCO Odando certlfied analyte [NC 424] Analyte rCAS Numberl Resufts Flag ni PTF MDL PP L Batch Method Analyzed By Notes Total Organic CarbonA 1.0 mg/L 1 0.34 1.0 6K11030 SM 53106-2000 11/11/16 12:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 6 of 30 Ce G www.encolabs.com ANALYTICAL RESULTS Description: MW -7 Lab Sample ID: CZ16292-02 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 14:35 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 30 (Volatile Organic Compounds by GCMS A - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flaa Units DF MDL POL Batch Method Analyzed By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]A 0.091 U ug/L 1 0.091 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK 1,1,1 -Trichloroethane [71-55-6]A 0.15 U ug/L 1 0.15 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,1,2,2 -Tetrachloroethane [79-34-5]A 0.085 U ug/L 1 0.085 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,1,2 -Trichloroethane [79-00-5]A 0.068 U ug/L 1 0.068 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,1-Dichloroethane[75-34-3]A 0.050 U ug/L 1 0.050 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,1-Dichloroethene [75-35-4]A 0.15 U ug/L 1 0.15 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,1-Dichloropropene [563-58-6]A 0.063 U ug/L 1 0.063 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK 1,2,3-Trichlorobenzene [87-61-6]A 0.25 U ug/L 1 0.25 0.50 6K09024 EPA 82606/62301) 11/09/16 21:05 MRK 1,2,3-Tdchloropropane[96-18-4]A 0.15 U ug/L 1 0.15 0.50 6K09024 EPA 82608/62301) 11/09/16 21:05 MRK 1,2,4-Trichlorobenzene [120-82-1]A 0.097 U ug/L 1 0.097 0.50 6K09024 EPA 82608/62301) 11/09/16 21:05 MRK 1,2,4-Trimethylbenzene [95-63-6]A 0.067 U ug/L 1 0.067 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 U ug/L 1 0.48 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,2-Dibromoethane [106-93-4]A 0.27 U ug/L 1 0.27 0.50 6K09024 EPA 82608/62301) 11/09/16 21:05 MRK 1,2 -Dichlorobenzene [95-50-1]A 0.062 U ug/L 1 0.062 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,2-Dichloroethane [107-06-2]A 0.082 U ug/L 1 0.082 0.50 6K09024 EPA 82608/62301) 11/09/16 21:05 MRK 1,2-Dichloropropane [78-87-5]A 0.098 U ug/L 1 0.098 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,3,5-Trimethylbenzene [108-67-8]A 0.10 U ug/L 1 0.10 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 1,3 -Dichlorobenzene [541-73-1]A 0.092 U ug/L 1 0.092 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK 1,3-Dichloropropane [142-28-9]A 0.15 U ug/L 1 0.15 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK 1,4 -Dichlorobenzene [106-46-7]A 0.10 U ug/L 1 0.10 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK 2,2-Dichloropropane [59420-7]A 0.12 U ug/L 1 0.12 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK 2-Chlorotoluene [95-49-8]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 21:05 MRK 4-Chlorotoluene [106-43-4]A 0.10 U ug/L 1 0.10 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK 4-Isopropyltoluene [99-87-6]A 0.066 U ug/L 1 0.066 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Benzene [71-43-2]A 0.050 U ug/L 1 0.050 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK Bromobenzene [108-86-1]A 0.13 U ug/L 1 0.13 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Bromochloromethane [74-97-5]A 0.11 U ug/L 1 0.11 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK Bromodichloromethane [75-27-4]A 0.010 U ug/L 1 0.010 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Bromoform [75-25-2]A 0.20 U ug/L 1 0.20 0.50 6K09024 EPA 82608/62301) 11/09/16 21:05 MRK Bromomethane [74-83-9]A 0.28 U ug/L 1 0.28 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Carbon Tetrachloride [56-23-5]A 0.082 U ug/L 1 0.082 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK Chlorobenzene [108-90-7]A 0.069 U ug/L 1 0.069 0.50 6K09024 EPA 82608/62301) 11/09/16 21:05 MRK Chloroethane [75-00-3]A 0.18 U ug/L 1 0.18 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK Chloroform [67-66-3]A O.OB3 U ug/L 1 0.083 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Chloromethane [7487-3]A 0.050 U ug/L 1 0.050 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK cis-1,2-Dichloroethene [156-59-2]A 0.075 U ug/L 1 0.075 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK cis-1,3-Dichloropropene [10061-01-5]A 0.073 U ug/L 1 0.073 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK Dibromochloromethane [124-48-1]A 0.067 U ug/L 1 0.067 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Dibromomethane [74-95-3]A 0.13 U ug/L 1 0.13 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK Dichlorodifluoromethane [75-71-8]A 0.091 U ug/L 1 0.091 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Ethylbenzene[100-41-4]A 0.10 U ug/L 1 0.10 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Hexachlorobutadiene [87-66-3]A 0.15 U ug/L 1 0.15 0.50 6K09024 EPA 82608/62301) 11/09/16 21:05 MRK Isopropyl Ether[108-20-3]A 0.20 U ug/L 1 0.20 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK Isopropylbenzene [98-82-B]A 0.13 U ug/L 1 0.13 0.50 6K09024 EPA 8260B/62301) 11/09/16 21:05 MRK m,p-Xylenes[108-38-3/106-42-3]A 0.18 U ug/L 1 0.18 0.50 6K09024 EPA 82606/62301) 11/09/16 21:05 MRK Methylene Chloride [75-09-2]A 0.070 U ug/L 1 0.070 0.50 6K09024 EPA 82606/62301) 11/09/16 21:05 MRK Methyl-tert-Butyl Ether [1634-04-4]A 0.12 U ug/L 1 0.12 0.50 6K09024 EPA 8260B/6230D 11/09/16 21:05 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 7 of 30 EIVCC-' www.encolabs.com ANALYTICAL RESULTS Description: MW -7 Lab Sample ID: CZ16292-02 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 14:35 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris .IVolatile Organic Compounds by GCMS &F Spike Lv/ 0/0 %RecLimits Batch Afth An / By Notes 4-Bromofluombenzene ^ - ENCO Cary certified analyte [NC 5911 1 50.0 9696 53-136 6KO9024 EPA 8260616230L 11/09/1611:05 MRK Classical Chemistry Parameters Dibromoflucromethane 51 Analyte rCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed ft Notes Naphthalene [91-20-3]A 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK n -Butyl Benzene [10451-8]A 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK n -Propyl Benzene [103-65-1]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK o -Xylene [95-47-6]A 0.088 U ug/L 1 0.088 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK sec-Butylbenzene [135-98-8]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK Styrene [100-42-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK tert-Butylbenzene [98-06-6]A 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK Tetrachloroethene [127-18-4]A 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK Toluene [108-88-3]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK trans-1,2-Dichloroethene [156-60-5]A 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK trans-1,3-Dichloropropene [10061-02-6]A 0.080 U ug/L 1 0.080 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK Trichloroethene [79-01-6]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK Trichlorofluoromethane [75-69-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK Vinyl chloride [75-01-4]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK Xylenes (Total) [1330-20-7]A 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:05 MRK srurroaates &F Spike Lv/ 0/0 %RecLimits Batch Afth An / By Notes 4-Bromofluombenzene 48 1 50.0 9696 53-136 6KO9024 EPA 8260616230L 11/09/1611:05 MRK Classical Chemistry Parameters Dibromoflucromethane 51 1 50.0 102% 67-119 6KO9024 EPA 826OB16230L 11/09/1611:05 MRK Toluene -d8 50 1 50.0 100% 59-134 6KO9024 EPA 82608162300 11/09/1611:05 MRK 0.34 1.0 6K13030 SM 531OB-2000 Classical Chemistry Parameters RSA ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag ni PF MDL PDL Batch Metho Analyzed Notes Ammonia as N [7664-41-7]A 0.045 U mg/L 1 0.045 0.10 61(15006 EPA 350.1 11/15/1611:47 JU Chloride [16887-00-6]A 9.9 B mg/L 1 1.9 5.0 6K16004 SM 4500CI E-1997 11/16/16 10:01 JU 3-01 Nitrate as N [14797-55-8]A 0.59 mg/L 1 0.025 0.10 61(21022 EPA 353.2 11/21/16 11:03 JU Nitrate/Nitrite as NA 0.59 mg/L 1 0.041 0.10 61(18005 EPA 353.2 11/18/16 12:23 JU Nitrite as N [14797-65-0]A 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:40 JU pHA 5.6 pH 1 1.0 1.0 61(11010 SM 4500H+B-200C 11/11/16 10:20 MKS Q-01 Total Dissolved Solids^ 50 U mg/L 1 50 50 61(10003 SM 2540C-1997 11/10/16 14:00 MMR Microbiological Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flag Units DF POLL Batch Method Analyzed By Notes Coliform, FecalA 1.0 U MPN/100 mL 1 1.0 6K10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters ^ - ENCO Odando certified analyte [NC 414] Analyte rCAS Numberl Results F a Units DF MDL PDL Batch Method Analyzed _By Notes Total Organic CarbonA 1.6 mg/L 1 0.34 1.0 6K13030 SM 531OB-2000 11/11/16 12:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 8 of 30 C� www.encolabs.com ANALYTICAL RESULTS Description: MW -8 Lab Sample ID:CZ16292-03 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 13:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 30 (Volatile Organic Compounds by GCMS ^ - ENC0 Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flaa Units DF MDL PPL, Batch Method Analyzed By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]^ 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,1,1 -Trichloroethane [71-55-6]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,1,2,2 -Tetrachloroethane [79-34-5]^ 0.085 U ug/L 1 0.085 0.50 6KO9024 EPA 82608/62301) 11/09/16 21:33 MRK 1,1,2 -Trichloroethane [79-00-5]^ 0.068 U ug/L 1 0.068 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,1-Dichloroethane [75-34-3]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/62301) 11/09/16 21:33 MRK 1,1-Dichloroethene [75-35-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,1-Dichloropropene [563-58-6]^ 0.063 U ug/L 1 0.063 0.50 6KO9024 EPA 8260B/62301) 11/09/16 21:33 MRK 1,2,3-Tdchlorobenzene [87-61-6]^ 0.25 U ug/L 1 0.25 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,2,3-Tdchloropropane [96-18-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,2,4-Trichlorobenzene [120-82-1]^ 0.097 U ug/L 1 0.097 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,2,4-Trimethylbenzene [95-63-6]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/62301) 11/09/16 21:33 MRK 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 0.50 6KO9024 EPA 82606/62301) 11/09/16 21:33 MRK 1,2-Dibromoethane [106-93-4]^ 0.27 U ug/L 1 0.27 0.50 6KO9024 EPA 82606/62301) 11/09/16 21:33 MRK 1,2 -Dichlorobenzene [95-50-1]^ 0.062 U ug/L 1 0.062 0.50 6KO9024 EPA 82606/62301) 11/09/16 21:33 MRK 1,2-Dichloroethane [107-06-2]^ 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,2-Dichloropropane [78-87-5]^ 0.098 U ug/L 1 0.098 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,3,5-Trimethylbenzene [108-67-8]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 1,3 -Dichlorobenzene [541-73-1]^ 0.092 U ug/L 1 0.092 0.50 6KO9024 EPA 8260B/62301) 11/09/16 21:33 MRK 1,3-Dichloropropane [142-28-9]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 82606/62301) 11/09/16 21:33 MRK 1,4 -Dichlorobenzene [106-46-7]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 2,2-Dichloropropane [594-20-7]^ 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 2-Chlorotoluene [95-49-8]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82608/62301) 11/09/16 21:33 MRK 4-Chlorotoluene [106-43-4]^ 0.10 u ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK 4-Isopropyltoluene [99-87-6]^ 0.066 U ug/L 1 0.066 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Benzene [71-43-2]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Bromobenzene[108-86-1]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Bromochloromethane [74-97-5]^ 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Bromodichloromethane [75-27-4]^ 0.010 U ug/L 1 0.010 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Bromoform [75-25-2]^ 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 82606/6230D 11/09/16 21:33 MRK Bromomethane [74-83-9]^ 0.28 u ug/L 1 0.28 0.50 6KO9024 EPA 82606/6230D 11/09/16 21:33 MRK Carbon Tetrachloride [56-23-5]^ 0.082 u ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Chlorobenzene[108-90-7]^ 0.069 U ug/L 1 0.069 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Chloroethane [75-00-3]^ 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Chloroform [67-66-3]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Chloromethane [74-87-3]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK cis-1,2-Dichlorcethene [156-59-2]^ 0.075 U ug/L 1 0.075 0.50 6KO9024 EPA 82606/62301) 11/09/16 21:33 MRK cis-1,3-Dichloropropene [10061-01-5]^ 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 82606/62301) 11/09/16 21:33 MRK Dibromochloromethane [124-48-1]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Dibromomethane [74-95-3]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Dichlorodifluoromethane [75-71-8]^ 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Ethylbenzene [100-41-4]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Hexachlorobutadiene [87-68-3]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Isopropyl Ether [108-20-3]A 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Isopropylbenzene [98-82-B]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK m,p-Xylenes[108-38-3/106-42-3]^ 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Methylene Chloride [75-09-2]^ 0.070 U ug/L 1 0.070 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Methyl-tert-Butyl Ether [1634-04-4]^ 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 9 of 30 (ma�Cme) www.encolabs.com ANALYTICAL RESULTS Description: MW -8 Lab Sample ID:CZ16292-03 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 13:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris Surrogates (Volatile Organic Compounds by GCMS DFike L v/ % Rec % Rec Limits Batch Metho Ana/vied By Notes 4-Bromofluorobenzene ^ - ENCO Cary certified anab to [NC 591] 1 50.0 97 % 53-136 6K09024 EPA 8260616230r, 111091162133 MRK DibromoAuoromethane 51 Analyte rCAS Numberl Results Flaq Units DF MDL POLL Batch Method Analyzed By Notes Naphthalene [91-20-3]^ 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK n -Butyl Benzene [104-51-8]A 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK n -Propyl Benzene [103-65-1]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK o -Xylene [95-47-6]A 0.088 U ug/L 1 0.088 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK sec-Butylbenzene [135-98-8]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Styrene [100-42-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK tert-Butylbenzene [98-06-6]A 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Tetrachloroethene[127-18-4]A 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Toluene [108-88-3]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK trans-1,2-Dichloroethene [156-60-5]^ 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK trans-1,3-Dichloropropene [10061-02-6]A 0.080 U ug/L 1 0.080 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Trichloroethene [79-01-6]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Trichlorofluoromethane [75-69-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Vinyl chloride [75-01-4]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Xylenes (Total) [1330-20-7]^ 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 8260B/6230D 11/09/16 21:33 MRK Surrogates Resu/ts DFike L v/ % Rec % Rec Limits Batch Metho Ana/vied By Notes 4-Bromofluorobenzene 48 1 50.0 97 % 53-136 6K09024 EPA 8260616230r, 111091162133 MRK DibromoAuoromethane 51 1 50.0 101 % 67-129 6K09024 EPA 8260B16230L 11/09/1621:33 MRK Toluene -d8 50 1 50.0 10090, 59-134 6K09024 EPA 8260B16230L 111091162133 MRK Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flag MaM DF MDL POL. Batch Method Analyzed Notes Ammonia as N [7664-41-7]^ 1.2 mg/L 1 0.045 0.10 61<15006 EPA 350.1 11/15/1611:49 ]U Chloride [16887-00-6]^ 13 B mg/L 1 1.9 5.0 6K16004 SM 4500CI E-1997 11/16/16 10:02 ]U 3-01 Nitrate as N [14797-55-8]^ 0.086 1 mg/L 1 0.025 0.10 61<21022 EPA 353.2 11/21/16 11:03 ]LJ Nitrate/Nitrite as N^ 0.086 1 mg/L 1 0.041 0.10 61<38005 EPA 353.2 11/18/16 12:24 ILI Nitrite as N [14797-65-0]A 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:41 ]U pHA 6.6 pH 1 1.0 1.0 61<11010 SM 4500H+B-200C 11/11/16 10:20 MKS ¢Ol Total Dissolved Solids^ 140 mg/L 1 50 50 61<10003 SM 2540C-1997 11/10/16 14:00 MMR Microbiological Parameters ^ - ENCO Cary certfied analyte [NC 591] Analyte rCAS Numberl Results flag Units DF pOL Batch Method Analyz Notes Coliform, Fecal^ 1.0 U MPN/100 mL 1 1.0 61<10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results Flag Units DF MDL PSL, Batch Method Analyzed Notes Total Organic Carbon^ 9.1 mg/L 1 0.34 1.0 6KII030 SM 531OB-2000 11/11/16 12:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 10 of 30 C www.encolabs.com ANALYTICAL RESULTS Description: MW -9 Lab Sample ID:CZ16292-04 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 14:55 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 30 (Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 Analyte KAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]^ 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,1,1-Tdchloroethane[71-55-6]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,1,2,2 -Tetrachloroethane [79-34-5]^ 0.085 U ug/L 1 0.085 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,1,2 -Trichloroethane [79-00-5]^ 0.068 U ug/L 1 0.068 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,1-Dichloroethane [75-34-3]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,1-Dichloroethene [75-35-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,1-Dichloropropene [563-58-6]^ 0.063 U ug/L 1 0.063 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,2,3-Tdchlorobenzene [87-61-6]^ 0.25 U ug/L 1 0.25 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK 1,2,3-Trichloropropane [96-18-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,2,4-Trichlorobenzene [120-82-1]A 0.097 U ug/L 1 0.097 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,2,4-Trimethylbenzene [95-63-6]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,2-Dibromo-3-chloropropane L96-12-8]^ 0.48 U ug/L 1 0.48 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,2-Dibromoethane[106-93-4]A 0.27 U ug/L 1 0.27 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK 1,2 -Dichlorobenzene [95-50-1]A 0.062 U ug/L 1 0.062 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,2-Dichloroethane [107-06-2]^ 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:03 MRK 1,2-Dichloropropane [78-87-5]^ 0.098 U ug/L 1 0.098 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,3,5-Trimethylbenzene [108-67-8]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK 1,3 -Dichlorobenzene [541-73-1]A 0.092 U ug/L 1 0.092 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,3-Dichloropropane [142-28-9]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 1,4 -Dichlorobenzene [106-46-7]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK 2,2-Dichloropropane [594-20-7]^ 0.12 U ug/L 1 0.12 0.50 6K09024 EPA 82608/62301) 11/09/16 22:03 MRK 2-Chlorotoluene [95-49-8]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:03 MRK 4-Chlorotoluene [106-43-4]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK 4-Isopropyltoluene [99-87-6]A 0.066 U ug/L 1 0.066 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK Benzene [71-43-2]A 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Bromobenzene [108-86-1]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:03 MRK Bromochloromethane [74-97-5]A 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Bromodichloromethane [75-27-4]^ 0.010 U ug/L 1 0.010 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Bromoform [75-25-2]^ 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Bromomethane [74-83-9]^ 0.28 U ug/L 1 0.28 0.50 6K09024 EPA 82606/62301) 11/09/16 22:03 MRK Carbon Tetrachloride [56-23-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Chlorobenzene [108-90-7]A 0.069 U ug/L 1 0.069 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Chloroethane [75-00-3]A 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK Chloroform [67-66-3]A 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Chloromethane [74-87-3]A 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:03 MRK cis-1,2-Dichloroethene [156-59-2]^ 0.075 U ug/L 1 0.075 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK cis-1,3-Dichloropropene [10061-01-5]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:03 MRK Dibromochloromethane [124-48-1]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Dibromomethane [74-95-3]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Dichlorodifluoromethane [75-71-8]A 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK Ethylbenzene [100-41-4]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:03 MRK Hexachlorobutadiene [87-68-3]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Isopropyl Ether [108-20-3]^ 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Isopropylbenzene [98-82-8]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:03 MRK m,p-Xylenes [108-38-3/106-42-3]A 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Methylene Chloride [75-09-2]A 0.070 U ug/L 1 0.070 0.50 6KC9024 EPA 8260B/62301) 11/09/16 22:03 MRK Methyl-tert-Butyl Ether [1634-04-4]A 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:03 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 11 of 30 www.encolabs.com ANALYTICAL RESULTS Description: MW -9 Lab Sample ID:CZ16292-04 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 14:55 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris Surrogates Volatile Organic Compounds by GCMS DF Sa/ke L v/ % Rec % Rec Limits Batch a ho nA a/vzed By Notes ^ - ENCO Cary certified analyte [NC 5911 49 1 50.0 97961 53-136 6KO9024 EPA 81608/62306 1110911622:03 MRK Dibromofluoromethane Analyte rCAS Numberl Results fLag Units PF MDL POLL Batch Method Analyzed By Notes Naphthalene [91-20-3]A 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK n -Butyl Benzene [104-51-8]A 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK n -Propyl Benzene [103-65-1]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK o -Xylene [95-47-6]A 0.088 U ug/L 1 0.088 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK sec-Butylbenzene [135-98-8]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Styrene [100-42-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK tert-Butylbenzene [98-06-6]A 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 826013/62301) 11/09/16 22:03 MRK Tetrachloroethene [127-18-4]^ 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Toluene [108-88-3]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK trans-1,2-Dichloroethene [156-60-5]A 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK trans-1,3-Dichloropropene [10061-02-6]A 0.080 U ug/L 1 0.080 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Trichloroethene [79-01-6]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Trichlorofluoromethane [75-69-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Vinyl chloride [75-01-4]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 82606/6230D 11/09/16 22:03 MRK Xylenes (Total) [1330-20-7]A 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:03 MRK Surrogates Res / DF Sa/ke L v/ % Rec % Rec Limits Batch a ho nA a/vzed By Notes 4-Bromofluorobenzene 49 1 50.0 97961 53-136 6KO9024 EPA 81608/62306 1110911622:03 MRK Dibromofluoromethane 52 1 50.0 103 % 67-129 6KO9024 EPA 82608/62306 11/09/16 22:03 MRK Toluene -d8 50 1 50.0 10190, 59-134 6KO9024 EPA 62603/62306 11/09/16 22:03 MRK Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL PSL, Batch Method Analyzed Notes Ammonia as N [7664-41-7]^ 0.11 mg/L 1 0.045 0.10 61<15002 EPA 350.1 11/15/16 08:55 ]U Chloride [16887-00-6]^ 4.4 JB mg/L 1 1.9 5.0 61<16004 SM 4500CI E-1997 11/16/16 10:02 ]LI 3-01 Nitrate as N [14797-55-8]^ 0.066 1 mg/L 1 0.025 0.10 61<21022 EPA 353.2 11/21/16 11:03 JU Nitrate/ Nitrite as N^ 0.066 3 mg/L 1 0.041 0.10 6K18005 EPA 353.2 11/18/16 12:25 JU Nitrite as N [14797-65-0]A 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:44 JU pH 7.4 pH 1 1.0 1.0 6K11010 iM 4500H+B-200C 11/11/16 10:20 MKS ¢Ol Total Dissolved Solids ^ 130 mg/L 1 50 50 61<10003 SM 254OC-1997 11/10/16 14:00 MMR Microbiological Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flag Units DF POL Batch Method Ana -By Notes Coliform, Fecal^ 1.0 U MPN/100 mL 1 1.0 61<10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters LLD ^ - ENCO Orlando Cerbried analge [NC 424] Analyte rCAS Numberl Results Flaq Units DF MDL PSL Batch Method Analyzed Notes Total Organic Carbon^ 0.91 3 mg/L 1 0.34 1.0 61<11030 SM 531OB-2000 11/11/16 12:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 12 of 30 www.encolabs.com ANALYTICAL RESULTS Description: MW -10 Lab Sample ID:CZ16292-05 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 12:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 30 (Volatile Organic Compounds by GCMS ^ - ENC0 Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flaa Units DF MDL PDL, Batch Method Analyzed 8y Notes 1,1,1,2 -Tetrachloroethane [630-20-6]^ 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,1,1 -Trichloroethane [71-55-6]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,1,2,2 -Tetrachloroethane [79-34-5]^ 0.085 U ug/L 1 0.085 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,1,2 -Trichloroethane [79-00-5]^ 0.068 U ug/L 1 0.068 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,1-Dichloroethane [75-34-3]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,1-Dichloroethene [75-35-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 82606/6230D 11/09/16 22:32 MRK 1,1-Dichloropropene [563-58-61^ 0.063 U ug/L 1 0.063 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,2,3-Trichlorobenzene [87-61-6]^ 0.25 U ug/L 1 0.25 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,2,3-Tdchloropropane [96-18-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:32 MRK 1,2,4-Trichlorobenzene [120-82-1]^ 0.097 U ug/L 1 0.097 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:32 MRK 1,2,4-Trimethylbenzene [95-63-6]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 0.50 6K09024 EPA 82608/62301) 11/09/16 22:32 MRK 1,2-Dibromoethane [106-93-4]^ 0.27 U ug/L 1 0.27 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,2 -Dichlorobenzene [95-50-1]^ 0.062 u ug/L 1 0.062 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,2-Dichloroethane [107-06-2]^ 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:32 MRK 1,2-Dichloropropane [78-87-5]^ 0.098 U ug/L 1 0.098 0.50 6KO9024 EPA 8260B16230D 11/09/16 22:32 MRK 1,3,5-Trimethylbenzene [108-67-8]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82608/62301) 11/09/16 22:32 MRK 1,3 -Dichlorobenzene [541-73-1]A 0.092 U ug/L 1 0.092 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 1,3-Dichloropropane [142-28-9]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 82608/62301) 11/09/16 22:32 MRK 1,4 -Dichlorobenzene L106 -46-7]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 2,2-Dichloropropane[594-20-7]^ 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK 2-Chlorotoluene [95-49-81^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:32 MRK 4-Chlorotoluene [106-43-4]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:32 MRK 4-Isopropyltoluene [99-87-61^ 0.066 U ug/L 1 0.066 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Benzene [71-43-2]A 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Bromobenzene [108-86-1]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Bromochloromethane [74-97-5]^ 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Bromodichloromethane [75-27-4]^ 0.010 U ug/L 1 0.010 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Bromoform [75-25-2]^ 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Bromomethane [74-83-9]^ 0.28 U ug/L 1 0.28 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Carbon Tetrachloride [56-23-5]^ 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Chlorobenzene[108-90-7]^ 0.069 U ug/L 1 0.069 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Chloroethane [75-00-3]^ 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Chloroform [67-66-3]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Chloromethane [74-87-3]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:32 MRK cis-1,2-Dichloroethene [156-59-2]^ 0.075 U ug/L 1 0.075 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK cis-1,3-Dichloropropene [10061-01-5]^ 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:32 MRK Dibromochloromethane [124-48-1]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Dibromomethane [74-95-3]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Dichlorodifluoromethane [75-71-B1^ 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:32 MRK Ethylbenzene[100-41-4]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Hexachlorobutadiene [87-68-3]^ 0.15 u ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Isopropyl Ether[108-20-3]^ 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Isopropylbenzene[98-82-8]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK m,p-Xylenes[108-38-3/106-42-3]^ 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Methylene Chloride [75-09-2]^ 0.070 U ug/L 1 0.070 0.50 6KO9024 EPA 82606/62301) 11/09/16 22:32 MRK Methyl-tert-Butyl Ether [1634-04-4]^ 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/62301) 11/09/16 22:32 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 13 of 30 (9�ee) www.encolabs.com ANALYTICAL RESULTS Description: MW -10 Lab Sample ID:CZ16292-05 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 12:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris (Volatile Organic Compounds by GCMS DF Spike L v/ o/a Rec % Rec Limits Batch Method An / By Notes 4-8romotluorobenzene 49 ^ - ENCO Cary certified analyte [NC 591] 50.0 97% 53-136 6K09024 EPA 82608/62306 11/09/16 22.32 MRK Dibromofluoromethane 51 1 50.0 Analyte rCAS Numberl Results Flag Units DF MDL PPL, Batch Method Analyzed By Notes Naphthalene [91-20-3]^ 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK n -Butyl Benzene [104-51-8]^ 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK n -Propyl Benzene [103-65-1]^ 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK o -Xylene [95-47-6]^ 0.088 U ug/L 1 0.088 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK sec-Butylbenzene [135-98-8]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Styrene [100-42-5]^ 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK tert-Butylbenzene [98-06-6]^ 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Tetrachloroethene [127-18-4]^ 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Toluene [108-88-3]^ 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK trans-1,2-Dichloroethene [156-60-5]^ 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK trans-1,3-Dichloropropene [10061-02-6]^ 0.080 U ug/L 1 0.080 0.50 6KO9024 EPA 82608/6230D 11/09/16 22:32 MRK Trichloroethene [79-01-6]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Trichlorofluoromethane [75-69-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Vinyl chloride [75-01-4]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Xylenes (Total) [1330-20-7]^ 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 8260B/6230D 11/09/16 22:32 MRK Surroaotes R s DF Spike L v/ o/a Rec % Rec Limits Batch Method An / By Notes 4-8romotluorobenzene 49 1 50.0 97% 53-136 6K09024 EPA 82608/62306 11/09/16 22.32 MRK Dibromofluoromethane 51 1 50.0 103 a/o 67-129 6K09024 EPA 82608/62306 11/09/16 22:32 MRK Toluene -d8 50 1 50.0 101 910 59-134 6K09024 EPA 82608/62306 11/09/16 22:32 MRK Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 5911 Analvte rCAS Numberl Results Fig Units pF MDL PPL Batch Method Analyzed AM Notes Ammonia as N [7664-41-7]^ 0.59 mg/L 1 0.045 0.10 61<15002 EPA 350.1 11/15/16 08:59 JU Chloride [16887-00-6]^ 5.1 B mg/L 1 1.9 5.0 6K36004 SM 4500C1 E-1997 11/16/16 10:03 JL7 3-01 Nitrate as N [14797-55-8]^ 0.22 mg/L 1 0.025 0.10 61<21022 EPA 353.2 11/21/16 11:03 JU Nitrate/Nitrite as N^ 0.22 mg/L 1 0.041 0.10 6K18005 EPA 353.2 11/18/16 12:26 JLJ Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:45 JU pH^ 6.2 pH 1 1.0 1.0 6K11010 SM 4500H+B-200C 11/11/16 10:20 MKS ¢Ol Total Dissolved Solids^ 50 U mg/L 1 50 50 6K10003 SM 254OC-1997 11/10/16 14:00 MMR Microbiological Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flaci UnitsPF P(ZLa ch Method Analyzed By Notes Coliform, Fecal^ 1.0 U MPN/100 mL 1 1.0 61<10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters ^ - ENCO Orlando a Analyte rCAS Numberl Total Organic Carbon^ Results Flan Units DF MDL POL Batch Method Analyzed By Notes 0.68 J mg/L 1 0.34 1.0 6K11030 SM 531OB-2000 11/11/16 12:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 14 of 30 (e� �� www.encolabs.com ANALYTICAL RESULTS Description: MW -11 Lab Sample ID:CZ16292-06 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 12:25 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 30 (Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte (CAS Numberl Results Flaa Units DF MDL Q Batch Method Analyzed By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]A 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK 1,1,1 -Trichloroethane [71-55-6]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK 1,1,2,2 -Tetrachloroethane [79-34-5]A 0.085 U ug/L 1 0.085 0.50 6KO9024 EPA 82606/6230D 11/09/16 23:01 MRK 1,1,2 -Trichloroethane [79-00-5]A 0.068 U ug/L 1 0.068 0.50 6KO9024 EPA 82606/6230D 11/09/16 23:01 MRK 1,1-Dichloroethane [75-34-3]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK 1,1-Dichloroethene [75-35-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK 1,1-Dichloropropene [563-58-6]A 0.063 u ug/L 1 0.063 0.50 6KO9024 EPA 82606/6230D 11/09/16 23:01 MRK 1,2,3-Trichlorobenzene [87-61-6]^ 0.25 U ug/L 1 0.25 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK 1,2,3-Trichloropropane[96-18-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK 1,2,4-Trichlorobenzene [120-82-1]A 0.097 u ug/L 1 0.097 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK 1,2,4-Trimethylbenzene [95-63-6]A 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK 1,2-Dibromo-3-chloropropane [96-12-8]A 0.48 u ug/L 1 0.48 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK 1,2-Dibromoethane [106-93-4]A 0.27 u ug/L 1 0.27 0.50 6K09024 EPA 82606/62301) 11/09/16 23:01 MRK 1,2 -Dichlorobenzene [95-50-1]A 0.062 u ug/L 1 0.062 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK 1,2-Dichloroethane [107-06-2]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK 1,2-Dichloropropane [78-87-5]A 0.098 U ug/L 1 0.098 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK 1,3,5-Trimethylbenzene [108-67-8]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK 1,3 -Dichlorobenzene [541-73-1]A 0.092 U ug/L 1 0.092 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK 1,3-Dichloropropane [142-28-9]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK 1,4 -Dichlorobenzene [106-46-71A 0.10 U ug/L 1 0.10 0.50 6KC9024 EPA 82608/62301) 11/09/16 23:01 MRK 2,2-Dichloropropane [594-20-7]A 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK 2-Chlorotoluene [95-49-8]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK 4-Chlorotoluene [106-43-4]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK 4-Isopropyltoluene [99-87-6]A 0.066 u ug/L 1 0.066 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK Benzene [71-43-2]A 0.050 U ug/L 1 0.050 0.50 6K09024 EPA 82606/62301) 11/09/16 23:01 MRK Bromobenzene [108-86-1]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Bromochloromethane [74-97-5]A 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Bromodichloromethane [75-27-4]^ 0.010 U ug/L 1 0.010 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Bromoform [75-25-2]A 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Bromomethane [74-83-9]A 0.28 U ug/L 1 0.28 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Carbon Tetrachloride [56-23-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Chlorobenzene [108-90-7]A 0.069 U ug/L 1 0.069 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Chloroethane [75-00-3]A 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Chloroform [67-66-3]A 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:01 MRK Chloromethane [74-87-3]A 0.050 u ug/L 1 0.050 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK cis-1,2-Dichloroethene [156-59-2]A 0.075 U ug/L 1 0.075 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK cis-1,3-Dichloropropene [10061-01-5]A 0.073 U ug/L 1 0.073 0.50 6K09024 EPA 8260B/6230D 11/09/16 23:01 MRK Dibromochloromethane [124-48-1]A 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:01 MRK Dibromomethane [74-95-3]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Dichlorodifluoromethane [75-71-8]A 0.091 u ug/L 1 0.091 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Ethylbenzene [100-41-4]^ 0.10 u ug/L 1 0.10 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Hexachlorobutadiene [87-68-3]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Isopropyl Ether [108-20-3]A 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:01 MRK Isopropylbenzene [98-82-8]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK m,p-Xylenes[108-38-3/106-42-3]A 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Methylene Chloride [75-09-21^ 0.070 U ug/L 1 0.070 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK Methyl-tert-Butyl Ether [1634-04-4]A 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:01 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 15 of 30 �IVC� www.encolabs.com ANALYTICAL RESULTS Description: MW -11 Lab Sample ID: CZ16292-06 Received: 11/08/16 16:58 Matrix: Ground Water Sampled: 11/08/16 12:25 Work Order: CZ16292 Project: Badin Shores -November Sampled By:Paul Morris surrogates (Volatile Organic Compounds by GCMS DF Spike L v/ % Rec % Rec Limits Batch Method Ana/vied y Notes 4-8romofluorobenzene ^ - ENCO Cary certirred analyte [NC 591) 1 50.0 95910 53-136 6KO9024 EPA 82608/62306 11/09/16 23:01 MRK Dibromot7uoromethane 52 Analyte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed _By Notes Naphthalene [91-20-3]A 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK n -Butyl Benzene [104-51-8]A 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK n -Propyl Benzene [103-65-1]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK o -Xylene [95-47-6]A 0.088 U ug/L 1 0.088 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK sec-Butylbenzene [135-98-8]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Styrene [100-42-5]A 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK tert-Butylbenzene [98-06-6]A 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Tetrachloroethene [127-18-4]^ 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Toluene [108-88-3]A 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK trans-1,2-Dichloroethene [156-60-5]^ 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK trans-1,3-Dichloropropene [10061-02-6]A 0.080 U ug/L 1 0.080 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Trichloroethene [79-01-6]A 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Trichlorofluoromethane [75-69-4]A 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Vinyl chloride [75-01-4]A 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK Xylenes CTotal) [1330-20-7]^ 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:01 MRK surrogates R u DF Spike L v/ % Rec % Rec Limits Batch Method Ana/vied y Notes 4-8romofluorobenzene 46 1 50.0 95910 53-136 6KO9024 EPA 82608/62306 11/09/16 23:01 MRK Dibromot7uoromethane 52 1 50.0 103 % 67-129 6KO9024 EPA 826OB16230L 11/09/1623.•01 MRK Toluene -d8 50 1 50.0 100910 59-134 6KO9024 EPA 826OB16230L . 11/09/16 23:01 MRK Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flag Units DF MDL IQ Batch Method Analyzed _SC Notes Ammonia as N [7664-41-7]A 0.32 mg/L 1 0.045 0.10 61(15002 EPA 350.1 11/15/16 09:01 JU Chloride [16887-00-6]A 11 B mg/L 1 1.9 5.0 6K16004 SM 4500CI E-1997 11/16/16 10:05 ]U 3-01 Nitrate as N [14797-55-8]A 0.34 mg/L 1 0.025 0.10 6K21022 EPA 353.2 11/21/16 11:03 ]U Nitrate/Nitrite as NA 0.34 mg/L 1 0.041 0.10 6K18005 EPA 353.2 11/18/16 12:27 JU Nitrite as N [14797-65-0]A 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:46 JU pHA 6.2 pH 1 1.0 1.0 6K11010 iM 4500H+B-200C 11/11/16 10:20 MKS Q-01 Total Dissolved Solids^ 50 U mg/L 1 50 50 6K10003 SM 254OC-1997 11/10/16 14:00 MMR Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF POL Batch Method Analyzed _By Notes Coliform; Fecal^ 1.0 U MPN/100 mL 1 1.0 61(10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Numberl Results fLag UnitsDF MDL Q Batch Method Analyzed By Notes Total Organic CarbonA 1.1 mg/L 1 0.34 1.0 61(11030 SM 53108-2000 11/11/16 12:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 16 of 30 www.encolabs.com ANALYTICAL RESULTS Description: Equipment Blank #1 Lab Sample ID:CZ16292-07 Received: 11/08/16 16:58 Matrix: Water Sampled: 11/08/16 14:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris Fig IVolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 5911 MDL Analyte I'CAS Numberl Results 1,1,1,2 -Tetrachloroethane [630-20-6]^ 0.091 1,1,1 -Trichloroethane [71-55-6]^ 0.15 1,1,2,2 -Tetrachloroethane [79-34-5]^ 0.085 1,1,2 -Trichloroethane [79-00-5]^ 0.068 1,1-Dichloroethane [75-34-3]^ 0.050 1,1-Dichloroethene [75-35-4]^ 0.15 1,1-Dichloropropene [563-58-6]^ 0.063 1,2,3-Tdchlorobenzene [87-61-6]^ 0.25 1,2,3-Tdchloropropane [96-18-4]^ 0.15 1,2,4-Tdchlorobenzene [120-82-1]^ 0.097 1,2,4-Trimethylbenzene [95-63-6]^ 0.067 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 1,2-Dibromoethane [106-93-4]^ 0.27 1,2 -Dichlorobenzene [95-50-1]^ 0.062 1,2-Dichloroethane [107-06-2]^ 0.082 1,2-Dichloropropane L78-87-5]^ 0.098 1,3,5-Trimethylbenzene [108-67-8]^ 0.10 1,3 -Dichlorobenzene [541-73-1]^ 0.092 1,3-Dichloropropane [142-28-9]A 0.15 1,4 -Dichlorobenzene [106-46-7]^ 0.10 2,2-Dichloropropane [594-20-7]^ 0.12 2-Chlorotoluene [95-49-8]^ 0.10 47Chlorotoluene [106-43-4]^ 0.10 4-Isopropyltoluene [99-87-6]^ 0.066 Benzene [71-43-2]^ 0.050 Bromobenzene [108-86-1]^ 0.13 Bromochloromethane [74-97-5]^ 0.11 Bromodichloromethane [75-27-4]^ 0.010 Bromoform [75-25-2]^ 0.20 Bromomethane [74-83-9]^ 0.28 Carbon Tetrachloride [56-23-5]^ . 0.082 Chlorobenzene [108-90-7]^ 0.069 Chloroethane [75-00-3]^ 0.18 Chloroform [67-66-3]^ 0.083 Chloromethane [74-87-3]^ 0.050 cis-1,2-Dichloroethene [156-59-2]^ 0.075 cis-1,3-Dichloropropene [10061-01-5]^ 0.073 Dibromochloromethane [124-48-1]^ 0.067 Dibromomethane [74-95-3]^ 0.13 Dichlorodifluoromethane [75-71-8]^ 0.091 Ethylbenzene [100-41-4]^ 0.10 Hexachlorobutadiene [87-68-3]^ 0.15 Isopropyl Ether L108 -20-3]A 0.20 Isopropylbenzene [98-82-8]^ 0.13 m,p-Xylenes'[108-38-3/106-42-3]^ 0.18 Methylene Chloride [75-09-2]^ 0.070 Methyl-tert-Butyl Ether [1634-04-4]" 0.12 Fig Units DF MDL PSL. Batch Method Analyzed By Notes u ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.085 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK u ug/L 1 0.068 0.50 6KO9024 EPA 82606/62301 11/09/16 23:30 MRK U ug/L 1 0.050 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:30 MRK u ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.063 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.25 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK u ug/L 1 0.15 0.50 6KO9024 EPA 82608/62301) 11/09/1623:30 MRK u ug/L 1 0.097 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.067 0.50 6KO9024 .EPA 8260B/62301) .11/09/16 23:30 MRK U ug/L 1 0.48 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:30 MRK U ug/L 1 0.27 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.062 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:30 MRK U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.098 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:30 MRK U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.092 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:30 MRK U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:36 MRK U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.066 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:30 MRK U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.13. 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.11 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:30 MRK U ug/L 1 0.010 0.50 6KO9024 EPA 8260B/62301) 11/09/1623:30 MRK U ug/L 1 - 0.20 0.50' 6K09024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.28 0.50 6KO9024 EPA 82608/62301) 11/69/1623:30 MRK U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.069 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.18 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:30 MRK U ug/L 1 .0.083 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.075 0.50 . 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L . 1 0.13 0.50 6KO9024 EPA 8260B/62300 11/09/16 23:30 MRK U ug/L 1 0.091 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:30 MRK U ug/L 1 0.10 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:30 . MRK U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/1623:30 MRK U ug/L 1 0.20 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:30 MRK U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:30 MRK U ug/L 1 0.18 0.50 - 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK U u9/L 1 0.070 . 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:30 MRK U ug/L 1 0.12 0.50 6KO9024 EPA 82608/6230D 11/09/16 23:30 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 17 of 30 EINCC-� www.encolabs.com ANALYTICAL RESULTS Description: Equipment Blank #1 Lab Sample ID:CZ16292-07 Received: 11/08/16 16:58 Matrix: Water Sampled: 11/08/16 14:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: Paul Morris (Volatile Organic Compounds by GCMS DF ik L v/ % Rec % Rec Limft Batch Metho Ana/vzed By Notes 4-Bromof7uorobenzene 48 ^ - ENCO Cary certified analyte [NC 591J 50.0 96% 53-136 6KO9024 EPA 8260816230C 11/09/1623:30 MRK Dibromofluoromethane 52 1 50.0 Analyte rCAS Numberl Results Flaq Units DF MDL POLL Batch Method Analyzed Notes Naphthalene [91-20-3]^ 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK n -Butyl Benzene [104-51-8]^ 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 826013/62301) 11/09/16 23:30 MRK n -Propyl Benzene [103-65-1]^ 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK o -Xylene [95-47-6]^ 0.088 U ug/L 1 0.088 0.50 6KO9024 EPA 826013/62301) 11/09/16 23:30 MRK sec-Butylbenzene [135-98-8]^ 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK Styrene [100-42-5]^ 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK tert-Butylbenzene [98-06-6]^ 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK Tetrachloroethene [127-18-4]^ 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 826013/623013 11/09/16 23:30 MRK Toluene [108-88-3]^ 0.053 U ug/L 1 0.053 0.50 6KO9024 EPA 826013/6230D 11/09/16 23:30 MRK trans-1,2-Dichloroethene [156-60-5]^ 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK trans-1,3-Dichloropropene [10061-02-6]^ 0.080 U ug/L 1 0.080 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK Trichloroethene [79-01-6]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK Trichlorofluoromethane [75-69-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:30 MRK Vinyl chloride [75-01-4]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 826013/62301) 11/09/16 23:30 MRK Xylenes (Total) [1330-20-7]^ 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:30 MRK Surrogates Resu/ DF ik L v/ % Rec % Rec Limft Batch Metho Ana/vzed By Notes 4-Bromof7uorobenzene 48 1 50.0 96% 53-136 6KO9024 EPA 8260816230C 11/09/1623:30 MRK Dibromofluoromethane 52 1 50.0 105 % 67-129 6KO9024 EPA 826OB16230L 11/09/1623:30 MRK Toluene -d8 51 1 50.0 101 % 59-134 6KO9024 EPA 82 6 0 3/623 0[ 11/09/1623:30 MRK Classical Chemistry Parameters ^ - ENCO Odando certified analyte [NC Analyte rCAS Numberl Total Organic Carbon^ Results Flan Units DF MDL Q Batch Method Analyzed By Notes 0.34 U mg/L 1 0.34 1.0 61(11030 SM 531OB-2000 11/11/1612:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 30 (Classical Chemistry Parameters ' ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results Flag ni PF MDL POL Batch Method Analyzed Notes Ammonia as N [7664-41-7]^ 1.4 mg/L 1 0.045 0.10 61(15002 EPA 350.1 11/15/16 09:04 JU Chloride [16887-00-6]^ 2.5 JB mg/L 1 1.9 5.0 6K16004 SM 4500CIE-1997 11/16/16 11:37 ]LJ 1-01 Nitrate as N [14797-55-8]^ 0.025 U mg/L 1 0.025 0.10 61(21022 EPA 353.2 11/21/16 11:03 IL1 Nitrate/Nitrite as N^ 0.041 U mg/L 1 0.041 0.10 61(16027 EPA 353.2 11/16/16 16:30 JU Nitrite as N [14797-65-0]^ 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:47 JU pHA 5.0 pH 1 1.0 1.0 61(11010 iM 4500H+B-200C 11/11/16 10:20 MKS Q-01 Total Dissolved Solids^ 50 U mg/L 1 50 50 61(10003 SM 254OC-1997 11/10/16 14:00 MMR Microbiological Parameters ^ - ENCO Cary certified analyte [NC 5911 Analyte rCAS Numberl Results F,gg Units DF pQL Batch Method Analyzed Notes Coliform, Fecal^ 1.0 U MPN/100 mL 1 1.0 61(10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters ^ - ENCO Odando certified analyte [NC Analyte rCAS Numberl Total Organic Carbon^ Results Flan Units DF MDL Q Batch Method Analyzed By Notes 0.34 U mg/L 1 0.34 1.0 61(11030 SM 531OB-2000 11/11/1612:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 18 of 30 (0 �Go www.encolabs.com ANALYTICAL RESULTS Description: Trip Blank Lab Sample ID:CZ16292-08 Received: 11/08/16 16:58 Matrix: Water Sampled: 11/08/16 12:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: ENCO FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 30 (Volatile Organic Compounds by GCMS ^ - E1VC0 Cary certified analyte (NC 5911 Analyte fCAS Numberl Results Flaq Units DF MDL POLL Batch Method Analyzed _By Notes 1,1,1,2 -Tetrachloroethane [630-20-6]^ 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:59 MRK 1,1,1 -Trichloroethane [71-55-6]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:59 MRK 1,1,2,2 -Tetrachloroethane [79-34-5]^ 0.085 U ug/L 1 0.085 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,1,2 -Trichloroethane [79-00-5]^ 0.068 U ug/L 1 0.068 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,1-Dichloroethane [75-343]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,1-Dichloroethene [75-35-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,1-Dichloropropene [563-58-6]^ 0.063 U ug/L 1 0.063 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,2,3-Thchlorobenzene [87-61-6]^ 0.25 U ug/L 1 0.25 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:59 MRK 1,2,3-Thchloropropane [96-18-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,2,4-Trichlorobenzene [120-82-1]^ 0.097 U ug/L 1 0.097 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:59 MRK 1,2,4-Tdmethylbenzene [95-63-6]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,2-Dibromo-3-chloropropane [96-12-8]^ 0.48 U ug/L 1 0.48 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,2-Dibromoethane[106-93-4]^ 0.27 U ug/L 1 0.27 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,2 -Dichlorobenzene [95-50-1]^ 0.062 U ug/L 1 0.062 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,2-Dichloroethane [107-06-2]^ 0.062 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:59 MRK 1,2-Dichloropropane [78-87-5]^ 0.098 U ug/L 1 0.098 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:59 MRK 1,3,5-Trimethylbenzene [108-67-8]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:59 MRK 1,3 -Dichlorobenzene [541-73-1]^ 0.092 U ug/L 1 0.092 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:59 MRK 1,3-Dichloropropane [142-28-9]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 1,4 -Dichlorobenzene [106-46-7]A 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 2,2-Dichloropropane[594-20-7]^ 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 2-Chlorotoluene [95-49-8]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 4-Chlorotoluene [106-43-4]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK 4-Isopropyltoluene [99-67-6]^ 0.066 U ug/L 1 0.066 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Benzene [71-43-2]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Bromobenzene[108-86-1]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Bromochloromethane [74-97-5]^ 0.11 U ug/L 1 0.11 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Bromodichloromethane [75-27-4]^ 0.010 U ug/L 1 0.010 0.50 6K09024 EPA 8260B/6230D 11/09/16 23:59 MRK Bromoform [75-25-2]^ 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Bromomethane [74-83-9]^ 0.28 U ug/L 1 0.28 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Carbon Tetrachloride [56-23-5]^ 0.082 U ug/L 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Chlorobenzene [108-90-7]^ 0.069 U ug/L 1 0.069 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Chloroethane [75-00-3]A 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Chloroform [67-66-3]^ 0.083 U ug/L 1 0.083 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:59 MRK Chloromethane [74-87-3]^ 0.050 U ug/L 1 0.050 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:59 MRK cis-1,2-Dichloroethene [156-59-2]^ 0.075 U ug/L 1 0.075 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:59 MRK cis-1,3-Dichloropropene [10061-01-5]^ 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:59 MRK Dibromochloromethane [124-48-1]^ 0.067 U ug/L 1 0.067 0.50 6KO9024 EPA 8260B/62301) 11/09/16 23:59 MRK Dibromomethane [74-95-3]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:59 MRK Dichlorodifluoromethane [75-71-8]^ 0.091 U ug/L 1 0.091 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Ethylbenzene [100-41-4]^ 0.10 U ug/L 1 0.10 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Hexachlorobutadiene [87-68-3]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 82608/62301) 11/09/16 23:59 MRK Isopropyl Ether [108-20-3]A 0.20 U ug/L 1 0.20 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Isopropylbenzene [98-82-8]^ 0.13 U ug/L 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK m,p-Xylenes[108-38-3/106-42-3]^ 0.18 U ug/L 1 0.18 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Methylene Chloride [75-09-2]^ 0.070 U ug/L 1 0.070 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Methyl-tert-Butyl Ether [1634-04-4]^ 0.12 U ug/L 1 0.12 0.50 6KO9024 EPA 82606/62301) 11/09/16 23:59 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 19 of 30 9 �Cme) I www.encolabs.com ANALYTICAL RESULTS Description: Trip Blank Lab Sample ID:CZ16292-08 Received: 11/08/16 16:58 Matrix: Water Sampled: 11/08/16 12:00 Work Order: CZ16292 Project: Badin Shores -November Sampled By: ENCO Sarroaates (Volatile Organic Compounds by GCMS DF 5viketv/ 0/a Rec % Mw Limits Batch Method nA a/vzed By Notes 4-Bromofluorobenzene 48 ^ - ENCO lorry certified analyte [NC 5911 50.0 95% 53-136 6KO9024 EPA 826OB16230L 11/09/16 23:59 MRK Dibromofluoromethane 52 1 50.0 Analyte rCAS Numberl Results Flag Units DF MDL PPL Batch Method Analyzed _By Notes Naphthalene [91-20-3]A 0.086 U ug/L 1 0.086 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK n -Butyl Benzene [104-51-8]A 0.074 U ug/L 1 0.074 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK n -Propyl Benzene [103-65-1]A 0.073 U ug/L 1 0.073 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK o -Xylene [95-47-6]A 0.088 U ug/L 1 0.088 0.50 61(09024 EPA 8260B/6230D 11/09/16 23:59 MRK sec-Butylbenzene [135-98-8]A 0.053 U ug/L. 1 0.053 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Styrene [100-42-5]A 0.082 U ug/L. 1 0.082 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK tert-Butylbenzene [98-06-6]A 0.094 U ug/L 1 0.094 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Tetrachloroethene [127-18-4]A 0.099 U ug/L 1 0.099 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Toluene [108-88-3]A 0.053 U ug/L 1 0.053 0.50 61(09024 EPA 8260B/6230D 11/09/16 23:59 MRK trans-1,2-Dichloroethene [156-60-5]A 0.11 U ug/L. 1 0.11 0.50 61(09024 EPA 8260B/6230D 11/09/16 23:59 MRK trans-1,3-Dichloropropene [10061-02-6]A 0.080 U ug/L. 1 0.080 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Trichloroethene [79-01-6]A 0.13 U ug/L. 1 0.13 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Trichlorofluoromethane [75-69-4]^ 0.15 U ug/L 1 0.15 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Vinyl chloride [75-01-4]^ 0.083 U ug/L 1 0.083 0.50 61(09024 EPA 8260B/6230D 11/09/16 23:59 MRK Xylenes (Total) [1330-20-7]A 0.22 U ug/L 1 0.22 0.50 6KO9024 EPA 8260B/6230D 11/09/16 23:59 MRK Sarroaates Reru/ts DF 5viketv/ 0/a Rec % Mw Limits Batch Method nA a/vzed By Notes 4-Bromofluorobenzene 48 1 50.0 95% 53-136 6KO9024 EPA 826OB16230L 11/09/16 23:59 MRK Dibromofluoromethane 52 1 50.0 104916 67-129 6KO9024 EPA 82608/6230r 11/09/16 23:59 MRK Toluene -d8 50 1 50.0 100901 59-134 6KO9024 EPA 826OB16230L 11/09/1623:59 MRK FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 30 (Classical Chemistry Parameters ^ - ENCO Cary rectified analyte [NC 591] Analyte rCAS Numberl Results Fjiq Units DF MDL PP L Batch Method Analyzed By Notes Ammonia as N [7664-41-7]A 0.045 U mg/L 1 0.045 0.10 6K15002 EPA 350.1 11/15/16 13:14 JU Chloride [16887-00-6]A 2.5 JB mg/L 1 1.9 5.0 6K16004 SM 4500CIE-1997 11/16/16 11:37 JU 3-01 Nitrate as N [14797-55-8]A 0.025 U mg/L 1 0.025 0.10 61(21022 EPA 353.2 11/21/16 11:03 JLI Nitrate/Nitrite as N^ 0.041 U mg/L. 1 0.041 0.10 6K16027 EPA 353.2 11/16/16 16:32 JU Nitrite as N [14797-65-0]A 0.017 U mg/L 1 0.017 0.10 6KO9009 EPA 353.2 11/09/16 09:49 JLI pHA 4.6 pH 1 1.0 1.0 61(11010 5M 4500H+B-200C 11/11/16 10:20 MKS ¢Ol Total Dissolved SolidsA 50 U mg/L 1. 50 50 6K10003 SM 2540C-1997 11/10/16 14:00 MMR Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results F a Units DF PPL Batch Method Analyzed fly Notes Coliform, Fecal^ 1.0 U MPN/100 mL 1 1.0 6K10025 Colilert 18 11/09/16 11:50 RAY Classical Chemistry Parameters ^ - ENCO Orlando rerlifled analyte [NC 424] Analyte rCAS Numberl Results Flaq UnitsDF MDL POL, Batch Method Analyzed By Notes Total Organic Carbon 0.34 U mg/L. 1 0.34 1.0 6K11030 SM 53108-2000 11/11/16 12:06 RSA FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 20 of 30 ElVC9 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6KO9024 - EPA 5030B MS Blank (6K09024-BLK3) Prepared: 11/09/2016 10:34 Analyzed: 11/09/2016 17:12 Analyte Result Flan PPL Units 1,1,1,2 -Tetrachloroethane 0.091 U 0.50 ug/L 1,1,1 -Trichloroethane 0.15 U 0.50 ug/L 1,1,2,2 -Tetrachloroethane 0.085 U 0.50 ug/L 1,1,2 -Trichloroethane 0.068 U 0.50 ug/L 1,1-Dichloroethane 0.050 U 0.50 ug/L 1,1-Dichloroethene 0.15 U 0.50 ug/L 1,1-Dichloropropene 0.063 U 0.50 ug/L 1,2,3-Trichlorobenzene 0.25 U 0.50 ug/L 1,2,3-Trichloropropane 0.15 U 0.50 ug/L 1,2,4-Trichlorobenzene 0.097 U 0.50 ug/L 1,2,4-Trimethylbenzene 0.067 U 0.50 ug/L 1,2-Dibromo-3-chloropropane 0.48 U 0.50 ug/L 1,2-Dibromoethane 0.27 U 0.50 ug/L 1,2 -Dichlorobenzene 0.062 U 0.50 ug/L 1,2-Dichloroethane 0.082 U 0.50 ug/L 1,2-Dichloropropane 0.098 U 0.50 ug/L 1,3,5-Trimethylbenzene 0.10 U 0.50 ug/L 1,3 -Dichlorobenzene 0.092 U 0.50 ug/L 1,3-Dichloropropane 0.15 U 0.50 ug/L 1,4 -Dichlorobenzene 0.10 U 0.50 ug/L 2,2-Dichloropropane 0.12 U 0.50 ug/L 2-Chiorotoluene 0.10 U 0.50 ug/L 4-Chlorotoluene 0.10 U 0.50 ug/L 4-Isopropyltoluene 0.066 U 0.50 ug/L Benzene 0.050 U 0.50 ug/L Bromobenzene 0.13 U 0.50 ug/L Bromochloromethane 0.11 U 0.50 ug/L Bromodichloromethane 0.010 U 0.50 ug/L Bromoform 0.20 U 0.50 ug/L Bromomethane 0.28 U 0.50 ug/L Carbon Tetrachloride 0.082 U 0.50 ug/L Chlorobenzene 0.069 U 0.50 ug/L Chloroethane 0.18 U 0.50 ug/L Chloroform 0.083 U 0.50 ug/L Chloromethane 0.050 U 0.50 ug/L cis-1,2-Dichloroethene 0.075 U 0.50 ug/L cis-1,3-Dichloropropene 0.073 U 0.50 ug/L Dibromochloromethane 0.067 U 0.50 ug/L Dibromomethane 0.13 U 0.50 ug/L Dichlorodifluoromethane 0.091 U 0.50 ug/L Ethylbenzene 0.10 U 0.50 ug/L Hexachlorobutadiene 0.15 U 0.50 ug/L Isopropyl Ether 0.20 U 0.50 ug/L Isopropylbenzene 0.13 U 0.50 ug/L m,p-Xylenes 0.18 U 0.50 ug/L Methylene Chloride 0.070 U 0.50 ug/L Methyl-tert-Butyl Ether 0.12 U 0.50 ug/L Naphthalene 0.086 U 0.50 ug/L n -Butyl Benzene 0.074 U 0.50 ug/L Spike Source %REC RPD Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 21 of 30 eco www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6KO9024 - EPA 50306 MS - Continued Blank (6K09024-BLKI) Continued Prepared: 11/09/2016 10:34 Analyzed: 11/09/2016 17:12 4-8romofluorobenzene 47 u9/L 50.0 94 53-136 Spike Source Dibromofluoromethane %REC RPD Analyte Result Man POL Units Level Result %REC Limits RPD Limit Notes n -Propyl Benzene 0.073 U 0.50 ug/L Prepared: 11/09/2016 10:34 Analyzed: 11/09/2016 16:14 Source: CZ16658-10 o -Xylene 0.088 U 0.50 ug/L Spike Source %REC sec-Butylbenzene 0.053 U 0.50 ug/L Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene Styrene 0.082 U 0.50 ug/L 20 Benzene 19 0.50 ug/L tert-Butylbenzene 0.094 U 0.50 ug/L 0.50 ug/L 20.0 0.069 U 99 83-117 4 16 Tetrachloroethene 0.099 U 0.50 ug/L Toluene 0.053 U 0.50 ug/L trans-1,2-Dichloroethene 0.11 U 0.50 ug/L trans-1,3-Dichloropropene 0.080 U 0.50 ug/L Trichloroethene 0.13 U 0.50 ug/L Trichlorofluoromethane 0.15 U 0.50 ug/L Vinyl chloride 0.083 U 0.50 ug/L Xylenes (Total) 0.22 U 0.50 ug/L 4-Bromofluorobenzene 48 u9/L 50.0 96 53-136 Dibromofluoromethane 47 u9/L 50.0 95 67-129 Toluene -d8 49 u9/L 50.0 97 59-134 LCS (6K09024 -BSI) Prepared: 11/09/2016 10:34 Analyzed: 11/09/2016 15:15 Spike Source %REC RPD Analyte Resul Flan PM Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 0.50 ug/L 20.0 102 75-133 Benzene 21 0.50 ug/L 20.0 103 81-134 Chlorobenzene 20 0.50 ug/L 20.0 102 83-117 Toluene 20 0.50 ug/L 20.0 102 71-118 Trichloroethene 21 0.50 ug/L 20.0 104 74-119 4-Bromofluorobenzene 47 u9/L 50.0 94 53-136 Dibromofluoromethane 47 u9/L 50.0 94 67-129 Toluene -d8 49 u9/L 50.0 98 59-134 Matrix Spike (6K09024 -MSS) Prepared: 11/09/2016 10:34 Analyzed: 11/09/2016 15:45 Source: CZ16658-10 Spike Source %REC RPD Analyte Resul Flan POL Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 20 0.50 ug/L 20.0 0.15 U 100 75-133 Benzene 21 0.50 ug/L 20.0 0.050 U 104 81-134 Chlorobenzene 20 0.50 ug/L 20.0 0.069 U 102 83-117 Toluene 20 0.50 ug/L 20.0 0.053 U 102 71-118 Trichloroethene 21 0.50 ug/L 20.0 0.13 U 104 74-119 4-8romofluorobenzene 47 u9/L 50.0 94 53-136 Dibromofluoromethane 47 u9/L 50.0 94 67-129 Toluene -d8 49 u9/L 50.0 98 59-134 Matrix Spike Dup (6K09024-MSDI) Prepared: 11/09/2016 10:34 Analyzed: 11/09/2016 16:14 Source: CZ16658-10 Spike Source %REC RPD Analyte Resul Flan P2 Units Level Result %REC Limits RPD Limit Notes 1,1-Dichloroethene 18 0.50 ug/L 20.0 0.15 U 92 75-133 9 20 Benzene 19 0.50 ug/L 20.0 0.050 U 97 81-134 7 17 Chlorobenzene 20 0.50 ug/L 20.0 0.069 U 99 83-117 4 16 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 22 of 30 (� i �Csm 0 www.encolabs.com QUALITY CONTROL DATA Volatile Organic Compounds by GCMS - Quality Control Batch 6KO9024 - EPA 5030B MS - Continued Matrix Spike Dup (6K09024-MSDi) Continued Prepared: 11/09/2016 10:34 Analyzed: 11/09/2016 16:14 Source: CZ16658-10 Spike Source %REC RPD Analyte Resul Flan POL units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (6K09009 -BSI) Prepared: 11/09/2016 08:01 Analyzed: 11/09/2016 09:48 Spike Source Spike Source %REC %REC RPD Analyte Resul Flari Q Units Level Result %REC Limits RPD Limit Notes Toluene 20 0.50 ug/L 20.0 0.053 U 98 71-118 5 17 Trichloroethene 19 0.50 ug/L 20.0 0.13 U 97 74-119 7 22 4-Bromofluorobenzene 49 u91L 50.0 97 53-136 Dibromofluoromethane 46 u91L 50.0 92 67-129 Toluene -d8 49 u91L 50.0 its 97 59-134 Notes Classical Chemistry Parameters - Quality Control 1.0 0.10 mg/L 1.00 0.017 U 101 90-110 Batch 6KO9009 - NO PREP Matrix Spike (6K09009-MS2) Prepared: 11/09/2016 08:01 Analyzed: 11/09/2016 09:38 Blank (6K09009-BLK1) Source: CZ15951-01 Prepared: 11/09/2016 08:01 Analyzed: 11/09/2016 09:31 Spike Source %REC RPD Analyte Resul Flan POL units Level Result %REC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (6K09009 -BSI) Prepared: 11/09/2016 08:01 Analyzed: 11/09/2016 09:48 Blank (6K10003-BLKI) Prepared & Analyzed: 11/10/2016 14:00 Spike Source %REC RPD Analyte Resul Flan POL Units Level Resul %REC Limits RPD Maid Notes Total Dissolved Solids 50 U 50 mg/L LCS (6K10003-BS1) Prepared & Analyzed: 11/10/2016 14:00 Spike Source %REC RPD Anal Resul Fla4 POL Units Level Resul %REC Limits RPD Limit Notes Total Dissolved Solids 960 50 mg/L 1000 96 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 30 Spike Source %REC RPD Anala Result Flan POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 102 90-110 Matrix Spike (6K09009 -MSI) Prepared: 11/09/2016 08:01 Analyzed: 11/09/2016 09:32 Source: CZ15948-01 Spike Source %REC RPD Anal Resul Flao POL its Level Resul t %REC Limits RPD Limit Notes Nitdte as N 1.0 0.10 mg/L 1.00 0.017 U 101 90-110 Matrix Spike (6K09009-MS2) Prepared: 11/09/2016 08:01 Analyzed: 11/09/2016 09:38 Source: CZ15951-01 Spike Source %REC RPD Anal Resul Flan POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 Matrix Spike Dup (6K09009-MSD1) Prepared: 11/09/2016 08:01 Analyzed: 11/09/2016 09:35 Source: CZ15948-01 Spike Source %REC RPD Anal a Result Flaa POL Units Level Result %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 0.017 U 100 90-110 1 10 Batch 6K10003 - NO PREP Blank (6K10003-BLKI) Prepared & Analyzed: 11/10/2016 14:00 Spike Source %REC RPD Analyte Resul Flan POL Units Level Resul %REC Limits RPD Maid Notes Total Dissolved Solids 50 U 50 mg/L LCS (6K10003-BS1) Prepared & Analyzed: 11/10/2016 14:00 Spike Source %REC RPD Anal Resul Fla4 POL Units Level Resul %REC Limits RPD Limit Notes Total Dissolved Solids 960 50 mg/L 1000 96 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 23 of 30 Ce 9 S "CMG) www.encolabs.com FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 30 QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6K10003 - NO PREP - Continued Duplicate (61K10003-DUPI) Prepared & Analyzed: 11/10/2016 14:00 Source: CZ15310-01 Spike Source %REC RPD Analyte Result Flao POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 11000 500 mg/L 12000 6 20 Duplicate (6K10003-DUP2) Prepared & Analyzed: 11/10/2016 14:00 Source: CZ15310-03 Spike Source %REC RPD Analyt Result Flaa Q Units Level Resul %REC Limits RPD Limit Notes Total Dissolved Solids 7800 250 mg/L 7800 1 20 Batch 6K20004 - NO PREP Blank (6K10004-BLK1) Prepared & Analyzed: 11/10/2016 15:00 Spike Source %REC RPD Anal a Resul Flau IQ Units Level Result %REC Limits RPD Limi Notes Total Dissolved Solids 50 U 50 mg/L LCS (61(10004-13S1) Prepared & Analyzed: 11/10/2016 15:00 Spike Source %REC RPD Analitte Result Flau 12 Units Level Resul %REC Limits RPD Limit Notes Total Dissolved Solids 950 50 mg/L 1000 95 90-110 Duplicate (61(10004-DUPI) Prepared & Analyzed: 11/10/2016 15:00 Source: CZ15249-01 Spike Source %REC RPD Analyte Result Fla POL Units Level Resul %REC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L 50 U 20 Duplicate (6K10004-DUP2) Prepared & Analyzed: 11/10/2016 15:00 Source: CZ15249-02 Spike Source %REC RPD Analyte Result "a POLL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 1200 50 mg/L 1300 3 20 Batch 6K11010 - NO PREP LCS (61(11010 -BSI) Prepared & Analyzed: 11/11/2016 10:20 Spike Source %REC RPD Analyte Resul Flan POL Units Level Result %REC Limits RPD Limit Notes pH 7.0 1.0 pH 7.00 100 99-101 Duplicate (6K11010-DUP1) Prepared & Analyzed: 11/11/2016 10:20 Source: CZ11267-02 Spike Source %REC RPD Anal Result San POL Units Level Resul %REC Limits RPD kimft Notes pH 7.7 1.0 pH 7.6 2 25 Batch 6K25002 - NO PREP Blank (61K35002-11EILKI) Prepared: 11/15/2016 07:49 Analyzed: 11/15/2016 08:45 Spike Source %REC RPD Analyte Result Flaa IQ Units Level Resu %REC Limits RPD Limit Notes Ammonia as N 0.045 U 0.10 mg/L FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 24 of 30 CICO www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6KIS002 - NO PREP - Continued LCS (61(15002-BS1) Prepared: 11/15/2016 07:49 Analyzed: 11/15/2016 08:47 Source: CZ15210-01RE1 Spike Source %REC RPD Spike Source %REC RPD Result Flaa ED& Analyte Res I - Flan POL Units Level R sul %REC Limits RPD Limit Notes Ammonia as N 1.0 0.10 mg/L 0.989 106 90-110 QM -11 Batch 6KIS006 - NO PREP Matrix Spike (6K15002 -MSI) Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 10:45 Source: CZ15249-05 Prepared: 11/15/2016 07:49 Analyzed: 11/15/2016 08:49 Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 10:41 Source: CZ15210-01RE1 Spike Source %REC RPD Spike Source %REC Analyte Resu Flao POLL Units Level Result %REC Limits RPD klnft Spike Source %REC RPD 0.045 U 0.10 Analyte Result fJA.q POL Units Level R su %REC Limits RPD Limi Notes Ammonia as N 9.2 1.0 mg/L 3.96 5.7 8B 90-110 Source: CZ15249-06 QM -07 Matrix Spike (6K15002-MS2) Prepared: 11/15/2016 07:49 Analyzed: 11/15/2016 08:57 Source: CZ16292-04 Spike Source %REC RPD Anal a Resul Flag PPL Units Level Result %REC Limits RPD Limi Nates Ammonia as N 0.37 Spike Source %REC RPD 0.385 0.045 U 97 90-110 Analyte Resul Flau Q Units Level Result %REC Limits RPD Lima Notes Ammonia as N 0.58 0.10 mg/L 0.385 0.11 122 90-110 QM -07 Matrix Spike Dup (61(35002-MSDI) Prepared: 11/15/2016 07:49 Analyzed: 11/15/2016 08:53 Source: CZ15210-01RE1 Source: CZ15249-05 Analyte Ammonia as N Batch 6K16004 - NO PREP Spike Source %REC Resul F1aa P9L Units Level Result %REC Limits RPD 0.38 0.10 mg/L 0.385 0.045 U 99 90-110 4 RPD Limit Notes 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 30 Spike Source %REC RPD Spike Source %REC Analyte Result Flaa ED& Units Level Result %REC Limits RPD Limit Notes Ammonia as N it 1.0 mg/L 3.96 5.7 129 90-110 16 10 QM -07, mg/L 0.989 104 90-110 Matrix Spike (61(15006-MS1). QM -11 Batch 6KIS006 - NO PREP Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 10:45 Source: CZ15249-05 Blank (61(15006-61.1(1) Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 10:41 Spike Source %REC RPD Spike Source %REC Analyte Resu Flao POLL Units Level Result %REC Limits RPD klnft Notes Ammonia as N 0.045 U 0.10 mg/L 0.37 0.10 LCS (6K35006 -BSI) 0.385 0.045 U 95 90-110 Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 10:43 Matrix Spike (6K15006-MS2) Source: CZ15249-05 Analyte Ammonia as N Batch 6K16004 - NO PREP Spike Source %REC Resul F1aa P9L Units Level Result %REC Limits RPD 0.38 0.10 mg/L 0.385 0.045 U 99 90-110 4 RPD Limit Notes 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 30 Spike Source %REC RPD Analyte Resul Elm JQ Units Level Result %REC Limits RPD Limit Notes Ammonia as N 1.0 0.10 mg/L 0.989 104 90-110 Matrix Spike (61(15006-MS1). Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 10:45 Source: CZ15249-05 Spike Source %REC RPD Anal Resu Flau PDL Units Level Result %REC Limits RPD MMA Notes Ammonia as N 0.37 0.10 mg/L 0.385 0.045 U 95 90-110 Matrix Spike (6K15006-MS2) Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 11:20 Source: CZ15249-06 Spike Source %REC RPD Anal a Resul Flag PPL Units Level Result %REC Limits RPD Limi Nates Ammonia as N 0.37 0.10 mg/L 0.385 0.045 U 97 90-110 Matrix Spike Dup (6K15006-MSD3) Prepared: 11/15/2016 09:03 Analyzed: 11/15/2016 10:49 Source: CZ15249-05 Analyte Ammonia as N Batch 6K16004 - NO PREP Spike Source %REC Resul F1aa P9L Units Level Result %REC Limits RPD 0.38 0.10 mg/L 0.385 0.045 U 99 90-110 4 RPD Limit Notes 10 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 25 of 30 (P�NCO www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6K16004 - NO PREP - Continued Blank (6K16004-BLK1) Prepared: 11/16/2016 08:00 Analyzed: 11/16/2016 09:49 Spike Source %REC RPD Ar 1yt Result Flau POL Units Level Res I %REC Limits RPD Limit Notes Chloride 2.8 3 5.0 mg/L LCS (61(16004-BS3) Prepared: 11/16/2016 08:00 Analyzed: 11/16/2016 09:50 Batch 6K26027 - NO PREP Blank (6K16027-BLK1) Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 15:57 Spike Source %REC RPD Anal Result Flaau PPL Units Level Result %REC Limits RPD Mmft Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (61(16027-BS1) Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 15:55 Spike Source %REC RPD Analyte Result Flag EM Units Level Result %REC Limits RPD Mflift Notes Chloride 98 B •5.0 mg/L 100 98 80-120 Duplicate (6K16004-DUPi) Prepared: 11/16/2016 08:00 Analyzed: 11/16/2016 09:54 Source: CZ15249-03 Source: CZ13598-01 Spike Source %REC RPD RPD Analyte Resul Flaq POL Units Level Resul %REC Limits RPD klnft Notes Chloride 720 BD 50 mg/L 710 2 10 Matrix Spike (61(16004-MS1) Matrix Spike (61(16027-MS2) Prepared: 11/16/2016 08:00 Analyzed: 11/16/2016 09:51 Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 16:21 Source: CZ15249-02 Source: CZ13598-02 Spike Source %REC RPD Spike Source %REC Analyte Result E[Pg POL Units Level Result %REC Limits RPD Limit Notes Chloride 750 B 25 mg/L 200 580 90 80-120 mg/L 0.513 0.041 U 90-110 Matrix Spike Dup (6K16004-MSD1) QM -07 Matrix Spike Dup (61(16027 -MSD!) Prepared: 11/16/2016 08:00 Analyzed: 11/16/2016 09:53 Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 16:17 Source: CZ15249-02 Source: CZ13598-01 Spike Source %REC RPD Spike Source %REC Analyte Result Flag EOL Units Level Result %REC Limits RPD imil; Notes Chloride 740 B 25 mg/L 200 580 83 80-120 2 25 Batch 6K26027 - NO PREP Blank (6K16027-BLK1) Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 15:57 Spike Source %REC RPD Anal Result Flaau PPL Units Level Result %REC Limits RPD Mmft Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (61(16027-BS1) Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 15:55 Spike Source %REC RPD Analyte Result Flan fQ Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.1 0.10 mg/L 1.25 91 90-110 Matrix Spike (61(16027-MS1) Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 16:12 Source: CZ13598-01 Spike Source %REC RPD Analyte Result Elm EOL Units Level Result %REC Limits RPD knift Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L 0.513 0.041 U 90-110 QM -07 Matrix Spike (61(16027-MS2) Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 16:21 Source: CZ13598-02 Spike Source %REC RPD Analyte Resu Fla_u POL Units Level Result %REC Limits RPD imil; Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L 0.513 0.041 U 90-110 QM -07 Matrix Spike Dup (61(16027 -MSD!) Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 16:17 Source: CZ13598-01 Spike Source %REC RPD Analyte R sul Flan EQ Units Level Resul %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 26 of 30 w 6 "E0 www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6K16027 - NO PREP - Continued Matrix Spike Dup (6K16027-MSDi) Continued Prepared: 11/16/2016 14:51 Analyzed: 11/16/2016 16:17 Source: CZ33598-01 Spike Source %REC RPD Analyte Result Flao POLL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L 0.513 0.041 U 90-110 10 QM -07 Batch 6K18005 - NO PREP Blank (6K18005-BLKI) Prepared: 11/18/2016 08:21 Analyzed: 11/18/2016 11:42 Spike Source %REC RPD Analyte Result' Flan PDL Units Level Res %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (6K18005-BS1) Prepared: 11/18/2016 08:21 Analyzed: 11/18/2016 11:44 Batch 6K10025 - NO PREP Duplicate (6K10025-DUPI) Spike Source %REC RPD Source: CZ15190-02 Anal Result Flao POL Units Level Resu %REC Limits RPD Limit Notes Nitrate/Nitrite as N 1.2 0.10 mg/L 1.25 93 90-110 Result Flaa Matrix Spike (61(18005-MS3) Units Level Resul %REC Limits RPD mmft Notes Coliform, Fecal Prepared: 11/18/2016 08:21 Analyzed: 11/18/2016 11:46 U 1.0 Source: CZ15249-04 1.0 U 25 Duplicate (6K10025-DUP2) Prepared: 11/08/2016 15:04 Analyzed: 11/09/2016 10:25 Source: CZ16234-02 Spike Source %REC RPD Analyte Result Flan POL Units Level Resul %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.52 Flaa 0.10 mg/L 0.513 0.041 U 102 90-110 Limit Notes Coliform, Fecal Matrix Spike (6K18005-MS2) U 1.0 MPN/100 mL 1.0 Prepared: 11/18/2016 08:21 Analyzed: 11/18/2016 11:55 Duplicate (61(10025-DUP3) Source: CZ15249-OS Prepared: 11/08/2016 17:15 Analyzed: 11/09/2016 11:50 Source: CZ16292-07 Spike Source %REC RPD Analyte Result E1a4 POL Units Level Resul %REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.52 Coliform, Fecal 0.10 mg/L 0.513 0.041 U 101 90-110 MPN/100 mL 1.0 U Matrix Spike Dup (6K18005-MSD3) Prepared: 11/18/2016 OB:21 Analyzed: 11/18/2016 11:51 Source: CZ15249-04 Spike Source %REC RPD Analyte Result ELq POL Units Level Resul %REC Limits RPD Unift Notes Nitrate/Nitrite as N 0.53 0.10 mg/L 0.513 0.041 U 103 90-110 0.4 10 Microbiological Parameters - Quality Control Batch 6K10025 - NO PREP Duplicate (6K10025-DUPI) Prepared: 11/08/2016 15:04 Analyzed: 11/09/2016 10:25 Source: CZ15190-02 Spike Source %REC RPD Anaa Result Flaa POL Units Level Resul %REC Limits RPD mmft Notes Coliform, Fecal 1.0 U 1.0 MPN/100 mL 1.0 U 25 Duplicate (6K10025-DUP2) Prepared: 11/08/2016 15:04 Analyzed: 11/09/2016 10:25 Source: CZ16234-02 Spike Source %REC RPD Analyte Resul Flaa POL Units Level Result %REC Limits RPD Limit Notes Coliform, Fecal 1.0 U 1.0 MPN/100 mL 1.0 25 Duplicate (61(10025-DUP3) Prepared: 11/08/2016 17:15 Analyzed: 11/09/2016 11:50 Source: CZ16292-07 Spike Source %REC RPD Analyte Resul Elau POL Units Level Resul %REC Limits RPD LifliA Notes Coliform, Fecal 1.0 U 1.0 MPN/100 mL 1.0 U 25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 27 of 30 CICO www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 6K11030 - NO PREP Blank (6K33030-BLK1) Prepared: 11/11/2016 11:37 Analyzed: 11/11/2016 12:06 Spike Source %REC RPD Analyte Result Elao P-QL Units Level Resu %REC Limits RPD Limit Notes Total Organic Carbon 0.34 U 1.0 mg/L LCS (6K11030 -BSI) Prepared: 11/11/2016 11:37 Analyzed: 11/11/2016 12:06 Spike Source %REC RPD Anal Result Flan Q Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 39 1.0 mg/L 40.0 99 85-115 LCS Dup (6K31030-BSD1) Prepared: 11/11/2016 11:37 Analyzed: 11/11/2016 12:06 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 30 Spike Source %REC RPD Analyte Result Flaa POLJU its Level Result %REC Limits RPD Limit Notes Total Organic Carbon 39 1.0 mg/L 40.0 98 85-115 0.7 21 Matrix Spike (6K11030-MS1) Prepared: 11/11/2016 11:37 Analyzed: 11/11/2016 12:06 Source: AZ07872-02 Spike Source %REC RPD Analyte Result Fla Q Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 49 1.0 mg/L 40.0 9.7 98 85-115 Matrix Spike Dup (6K11030-MSD1) Prepared: 11/11/2016 11:37 Analyzed: 11/11/2016 12:06 Source: AZ07872-02 Spike Source %REC RPD Anae Resul Flan IQ Units Level Resul %REC Limits RPD Limit Notes Total Organic Carbon 48 1.0 mg/L 40.0 9.7 95 85-115 2 21 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 28 of 30 ElVCO www.encolabs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. J The reported value is between the laboratory method detection limit (MDL) and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQQ and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a "tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. 3-01 Result may be biased high due to positive results in the associated method blank. Q-01 Analysis performed outside of method - specified holding time. QM -07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM -11 Precision between duplicate matrix spikes of the same sample was outside acceptance limits. FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 29 of 30 Lt— �� � 10775 Central Port Dr. Jacksonville, ExecutivevinePark Court, Suite 111 102-A Woodwinds Industrial Cl. Orlando, FL 32824 Jacksonville, FL 32216-6069 Cary, NC 27511 ' (407) 826.5314 Fax (407) 8506945 (904)29&-3007 Fax(904)2966210 (919) 467.3090 Fax(919)467-3515 Page Of J Client Name Project Number Requested Analyses Requested Turnaround Vtllihtlis if, Rn, -n^1 i-n,rlrrinrlit-nt^I A! 1 `3 n r O� - 1 �( •• DO Cy Times Address Project am JDesc Crj C) if) C, Nolo :Rush requests subject to G �, acceptance b the facility 115 r> �� r{<En. r Drive r+' Ss_ nn .� c� r,, v v City/ST/Zip PO it r Billing Info X ni ' - C . n 011 C. -1r . NC 27511 z C _ Standard Tel ll Fax Reporting Contact f ui Oj MJ r'r (rz J) 469-3.340 J'I �)` .535-4.45 T Colv,;ell C I a C 1 co _ Expedited Sampler(s) Name, Athliation (Print) Billing Contact o n 1 t� Paul UEi ', Accounts Payable M a 7, � a, clti Due Samplor(s) taturo Site Locate Time Zone N E w Lab Workorder czt z i LL Z If- C Z 16 92 Preservation (Sao Codes) (Combine as necessary) Collection Matrix Total A of Item it Samp!o to (Field Ident.hcation) Collection /Daten Time Compp Grab (see codes) Containers Sample Comments -7 1' �l�b l `f_35" �' - —cam R X Y �� YL �c_ X It -IbG IV�,Ad_J _ (g f l �� G G�^� :3 X_X X "VI VV -1 C) _ �l • 1 two G GV'! 8 XPX_ ); X X X — ,il;/tir_.�, cN! 8 X x, x X x X_ (_1uivr )ent Brant, tom' �1 Jilp IVV G VlVJ 8 X X X X X X Trip Blank �� �VJVJ 8 X X x X X X <-- Total M of Containers 1 Sample Kit Prepared By Dat rrimo Relinquish .. Daterrime Recoir By i 1 Dalerrimo J Commerfis/Special Reporting Requirements Rolinquishod By Date/Time R ce ved y Dalelrmo Relinquished By Daterrime Flee ' ed y DateMnio F117 N''s&"Temps on Receipt r l/ L Condit on l�pon Receipt /Acceptable Unacceptable mmiu . ,an uiuw W WJICi au-ouii uw-Vrimanq vvater ,a=-aco,mem bv✓-aunace water W W-WasterIater A -Air U-Umer (detail in comments) Preservallon: I -Ice H-HGI N-HNO3 S-H2SO4 NO-NaOH O.Other (detail In comments) Note: AD samples submitted to ENCO Labs are in accordance with the terms and conditions listed on the reverse of this form, unless prior written agreements exist ^..Sample Preservation Verification, ENCO Cary :. Work Order: CZ1.6292 Project: Badin Shores -November Client: Withers & Ravenel Environmental (WI009) Project #: [none] Logged in: 09 -Nov -16 07:33 Logged By: John C King .:. CZ16292-01 Cont Type Pres (pH) , pH Checked / Requirement In Control t Date/Time pH Ad jutted � Adiusted . Reagent Used -- A 250mLP+H2SO4 <2 / N / NA Y / INA In Control CZ16292-02 Pres {pH) pH,Checked I Date Cont Type � RPre cement equ p H Control / /Time pH Adjusted Reagent. Used/Comments A 250mLP+H2SO4 Requirement In Control Adiusted . 250mLP+1­12SO4 A 260mLP+H2SO4 I N:/ NAY 1 1 NA CZ16209-03 Cont Type RPre cement equ p H Control / pH Adjusted," Ate/Time Reagent UsedlComments' A 250mLP+H2SO4 <2 11E/ N / NA -Y /� / - NA 250mLP+1­12SO4 CZ16292-04 Cont Type Pres (pH) .pH Checked / Requirement I In Control DatelTme pH Adjusted Adjusted Reagent Used/Comments A 250mLP+H2SO4 <2 / N I NA Y 1 ' '/ NA '/ N / NA CZ16292=09 Cont Type Pres (pH) Requirement pH Checked / In Control Date�me pH Adjusted `Reagent Adjusted UsedlComments ' , • . A 25OmLP+H2SO4 <2 '/ N / NA Y /.�l I _NA 250mLP+1­12SO4 CZ16292-06 . Cont Type Pres (pH) pH Checked 1 DatelTme . • ` pH Adjusted e Reagent UsedlComments Requirement•. In Control Adjusted A ' 250mLP+1­12SO4 <2 / N / NA Y / / NA CZ16292-07 Cont Type Pres (pH) pH Checked I DatefTime pH Adjusted Reagent Used/Comments Requirement I • In Control Adjusted A 250rhLP+H2SO4 . <2 49% N / NA Y / / .NA Pres (pH) pH Checked / Date/Time Cont Type pH Adjusted : `Reagent Used/Comments Requirement In Control Adiusted A 250mLP+H2SQ4 <2 Y / N / NA Y 1 N / NA Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT'NUMBER: W00010657 MONTH: September YEAR: 2016 FACILITY NAME: Badin Shores Resort COUNTY: Mont2omery Flow Monitoring Point: Effluent: LJ Influent: Parameter Monitoring Point: Effluent: ❑ Influent: ❑ ISurface Water (SW): ❑ I SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: Yes: Li No: D A 'I' E Operator 50050 00400 50060 00310 00610 00530 31616 1 00094 00680 N/A Arrival Daily Rale Fecal Time Operator ORC (Flow) into Coliform 2400 Time on on Treatment Residual BOD -5 (Geo -metric Clock Site Site? System pH Chlorine 20°C NH -3-N TSS Mean•) Conductivity TOC, DOC HRS Y/N GPD UNITS UG/L MG/L MG/L MG/L /100ML µm os cm MG/L MG/L . 1.: 0859 U_Y: 2 0 4 0 6 0 r " 8 O 10 1120 0.25 Y 0 12 0 °. s 14 1040 0.25 Y 0 _ d �,i X15 a0 S�� ' R� Wn w".F ."i.�41`L'a� { ..�s,. m ..'lo - 16 0 G1 ,.*5 b"R.- 18. 0 oall�6O l 19< Q'` ra ` w4r r b `''•� erx".fF 20. 0 IV L 22 1200 0.25 B 0 �G � - 24 0 2S. Ar r Qx 4 .,,n b._4! •4 is 26 0 28 0 1150 25B�: ,. ' 00 3 .. . '0 .., , Vii.. '":'xT� . _ s tl�. r�i:: �#k",.a. , r �.' . .."vr:�� �.-"':,3., a. x a ,{s"IP`; .. a`t.: -. Average 0 Daily Maximum 0 0 Daily Minimum 0 0 Monthly Limits (s) Composite ©/ Grab (G) Operator in Responsible Charge (ORC): Glenn Price Grade: II Phone: 336-996-2841 Check Box if ORC Has Changed: ❑ ORC Certification Number: 987931/20771 Certified Laboratories (1): R & A Laboratories, Inc. (2): . Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit DENR Division of Water Quality 1617 Mail Service Center RALEIGH, NC 27699-1617 (SIGNATURE OF OPERATOR IN RESPONSIBLE CH) By this signature, I certify that this report is accurate and complete to the best of my knowledge. DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Com liant Y,N) L Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non-compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the inform ons mitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant pen ties for bmittingfal infonation, including the possibility of fines and imprisonment for knowing violations." of print or type) 1 Clubhouse Drive New London, NC 28127 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 31504 Coliform, Total 00094 Conductivity 01042 Co2per 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel James M. Cheshire (Name of Signing Official -Please print or type) President R & A Laboratories (Position or Title) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease WQ09 PAN Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W00010657 MONTH: September YEAR: 2016 _ FACILITY NAME: Badin Shores Resort COUNTY: Montgomery Formulas: Dally Loading (Inches) = [Volume Applied (gallons) x 0.1336 (cubic feet/gallon) x 12 (Inches/foot)] / [Area Sprayed (acres) x 43,560 (square feet/acre) or = [Volume Applied (gallons) / [Area Sprayed (acres) x 27,152 (gallons/acre-Inch). Maximum Hourly Loading (inches) = Daily Loading (inches) / [rime Irrigated (minutes) 160 (minutes/hour)] Monthly Loading (Inches) =Sum of Daily Loading (Inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (Inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (Inches/month) / Number of days In the month (days/month )] x 7 (days/week) Did Irrigation Occur At This Facility: Did Irrigation Occur On This Field: Did Irrigation Occur On This Field: SEEMS 11110�11111111 111110011111 Maximum Hourly .... .. MEN; Loading ENE= 1���� 11111111011011 SOMISMEM Total Callonsfmonthly Loading (Inchm) µ 0P& eIII 0 F0 _ III 0 : *Weather Codes: C -clear, PC -partly cloudy, CI -cloudy, R -rain, Sn-snow, SI -sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 4/ 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 4 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. 4 S. The freeboard in the treatment and/or storage lagoon(s) was not less than the 4 limit(s) specified in the permit. If the facility is non-compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant pen ies r submittin is formation, including the possibility of fines and imprisonment for knowing violations." z 7 James M. Cheshire ( igna e of e itee D (Name of Signing Official -Please print or type) fes M. Cheshire (Authorized Agent) President R & A Laboratories (Permittee -Please print or type) (Position or Title) 1 Clubhouse Drive New London, NC 28127 (Phone Number) (Permit Exp. Date) (Permittee Address) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). Page 2 of 2 NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMIT NUMBER: W00010657 MONTH: August YEAR: 2016 FACILITY NAME: Badin Shores Resort COUNTY: Montgomery Formulas: Daily Loading (inches) = [Volume Applied (gallons) x 0.1336 (cubic feetigallon) x 12 (inches/foot)] /[Area Sprayed (acres) x 43,560 (square feettacre) or = [Volume Applied (gallons) / [Area Sprayed (acres) x 27,152 (gallons/acre-inch). Maximum Hourly Loading (inches) = Daily Loading (inches) / [Time Irrigated (minutes) / 60 (minutes/hour)] Monthly Loading (inches) =Sum of Daily Loading (inches) 12 Month Floating Total (inches) = Sum of this month's Monthly Loading (inches) and previous 11 month's Monthly Loadings (inches) Average Weekly Loading (inches) = [Monthly Loading (inches/month) /Number of days in the month (days/month )] x 7 (days/week) Did Irrigation Occur Al This Facility: Did Irrigation Occur On This Field: Did Irrigation Occur On This Field: Yes: ❑ No: ❑ Yes: ❑ No: ❑ Yes: ❑ No: ❑ Field Number: 1 Field Number: 2 Area Sprayed (acres): 12.6 Area Sprayed (acres):. 12.1 Cover Crop: Fescue Cover Crop: lFescue Permitted Hourly Rale (inches): 0.25 Permitted Hourly Rate (inches): 0.25 WEATHER CONDITIONS Permitted Yearly Rate (inches): 28.5 Permitted Yearly Rate (inches): 20.8 D A Weather Temperature Storage Maximum Maximum T Code* at Preeipita- Lagoon Volume Time Daily Hourly Volume Time Daily Hourly E applicmim, lion Free -board Applied Irrigated Leading Lending Applied Irrigated Loading Leading ff) inches Ret gallons minutes inches inches gallons minutes inches inches *Weather Codes: C -clear, PC -partly cloudy, CI -cloudy, R -rain, Sn-snow, SI -sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By. this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) Total Gallons/Montlily Loading (inches) 7.1;12 %tenth Floalml; Total (inches) Mcr.ge Weekly Lending (im,h.) *Weather Codes: C -clear, PC -partly cloudy, CI -cloudy, R -rain, Sn-snow, SI -sleet Spray Irrigation Operator in Responsible Charge (ORC): Glenn Price Phone: 336-996-2841 ORC Certification Number: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By. this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON -DISCHARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. ETJ 4. All buffer zones as specified in the permit were maintained during each application. 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is lion -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the info tion ubmitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant pen ties fo submitting ,46rmation, including the possibility of fines and imprisonment for knowing violations." James M. Cheshire of Pe tee) D e (Name of Signing Official -Please print or type) 'Yames M. Utieshire (Authorized Agent) President R & A Laboratories (Permittee -Please print or type) (Position or Title) 1 Clubhouse Drive New London, NC 28127 (Phone Number) (Permit Exp. Date) (Permittee Address) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D). Page 1 of 2 NON -DISCHARGE WASTE WATER MONITORING REPORT PERMIT NUMBER: W00010657 MONTH: August YEAR: 2016 FACILITY NAME: Badin Shores Resort COUNTY: Montgomery Flow Monitoring Point: Effluent: LJ Influent: Parameter Monitoring Point: Effluent: Q Influent: ❑ I Surface Water (SW): ❑ I SW Code/Name: Was There Effluent Flow for this Month Generated At This Facility: Yes: Li No: Operator 50050 00400 50060 00310 00610 00530 31616 00094 00680 N/A D Arrival Daily Rate Fecal A Time Operator ORC I (Flow) Into Coliform T 2400 Time on on Treatment Residual BOD -5 (Geo -metric E Clock Site Site? System off Chlorine 20°C NH -3-N TSS Mean*) Conductivity TOC DOC Operator in Responsible Charge (ORC): Glenn Price Grade: I1 Phone: 336-996-2841 Check Box if ORC Has Changed: ❑ ORC Certification Number: 987931/20771 Certified Laboratories (1): R & A Laboratories, Inc. (2): Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) Im EMEMEEMM I In MIN= M�ffimm MEEMEENIM Holm I Composite---------- o --------- Operator in Responsible Charge (ORC): Glenn Price Grade: I1 Phone: 336-996-2841 Check Box if ORC Has Changed: ❑ ORC Certification Number: 987931/20771 Certified Laboratories (1): R & A Laboratories, Inc. (2): Person(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATTN: Non -Discharge Compliance Unit X DENR (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) Division of Water Quality By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of my knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant (Y,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non-compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the inflorm4>a4a,submitted is, to he best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penal es for submitting is iyd�rmation, including the possibility of fines and imprisonment for knowing violations." (S gZnae of.Perma M. Cheshir/e Authorized (Permittee -Please print or type) 1 Clubhouse Drive New London, NC 28127 (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD 2� 31504 Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel James M. Cheshire (Name of Signing Official -Please print or type) President R & A Laboratories (Position or Title) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease WQ09 PAN (Plant Available) 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 Turbidity 01092 Zinc Parameter Code assistance may be obtained by calling the Water Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 213.0506 (b) (2) (D).