NC0088692_Renewal (Application)_20161122 (2)

Water Resources
ENVIRONMENTAL QUALITY.
PAT MCCRORY
Governor
DONALD R. VAN DER VAART
Secretary
S. JAY ZIMMERMAN
Director
December 09, 2016
Mr. Jerry Sparks, President
Sparks Oil Company
412 N. Scales Street
Reidsville, NC 27320-2909
Subject: Permit Renewal
Application No. NCO088692
J.W. Smith/Camp Spring 76
Caswell County
Dear Mr. Sparks:
The Water Quality Permitting Section acknowledges receipt of your permit application and
supporting documentation received,on November 22, 2016. The primary reviewer for this renewal
application is Derek Denard.
The, primary reviewer will review your application, and he will contact you if additional
information is required to complete your permit renewal. Per G.S. 150B-3 your current permit
does not expire until permit decision on the application is made. Continuation of the current permit
is contingent on timely and sufficient application for renewal of the current permit.
Please respond in a timely manner to requests for additional information necessary to
complete the permit application. If you have any additional questions concerning renewal of the
subject permit, please contact.Mr. Denard at 9.19-807-6307 or [e-mail].
cc: Central Files
NPDES
Winston-Salem Office
Sincerely,
?A" %Cie J"d
Wren Thedford
Wastewater Branch
State ofNorth Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
919-807-6300

r
PYRAMt0
ENVIRONMENTAL & ENGINEERING, P.C.
November 14, 2016
Mrs. Dina Sprinkle
NCDEQ / DWQ / Point Source Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: NPDES Permit Renewal Request for
JW Smith / Camp Springs 76 Groundwater Remediation System
8920 Cherry Grove Road
Reidsville, Caswell County, NC
NPDES Permit # NCO088692 RECEIVED/NCDEQ/DWR
Incident#21685
NOV 2 2 2016
Dear Mrs. Sprinkle: Water Quality
As requested by Sparks Oil Company, Pyramid Environmental & Enginee4i'i�g'npCkfi.'as^n
completed a renewal request package for the NPDES Permit # NC0088692. Enclosed
please find the NPDES Permit renewal request package containing all required
documentation.
The Camp Springs. 761JW Smith remediation system has not been changed since the
issuance of the current NPDES permit that expires on May 31, 2017. Please note that
there is an incorrect number of carbon vessels listed in the current permit. The new
permit should list four (4) carbon vessels. Please see the documents in the enclosed
Residuals Management Plan regarding the carbon vessel number.
If you have any questions or need any additional information regarding this permit
renewal request, please call me at 336-335-3174.
Sincerely,
11*AW11e--;
Mika Trifunovic
Project Manager
Enclosures: NPDES Permit Renewal Package
P.O. Box 16265 • Greensboro,. NC 27416
503 Industrial Ave • Greensboro, NC 27406
Phone [phone] o Fax [phone] • Toll Free [phone]
Email: [e-mail]
www.pyramidenvironmental.com '

NC DENR / DWQ / NPDES
Renewal Application Checklist
The following items are REQUIRED for all renewal packages:
'( A cover letter requesting renewal of the permit and documenting any changes at the facility since
issuance of the last permit. Submit one signed original and two copies.
The completed application form (copy attached), signed by the permittee or an Authorized
/ Representative. Submit one signed original and two copies.
ep If an Authorized Representative (such as a consulting engineer or environmental consultant) prepares
the renewal package, written documentation must be provided showing the authority delegated to the
Authorized Representative (see Part II.B.1 Lb of the existing NPDES permit).
A narrative description of the sludge management plan for the facility. Describe how sludge (or other
solids) generated during wastewater treatment are handled and disposed. If your facility has no such
plan (or the permitted facility does not generate any solids), explain this in writing. Submit one signed
original and two copies.
The following items must be submitted b3L ani Municipal or Industrial facilities discharging
process wastewater:
o Industrial facilities classified as Primary Industries (see Appendices A -D to Title 40 of the Code of
Federal Regulations, Part 122) and ALL Municipal facilities with a permitted flow >_ 1.0 MGD must
submit a Priority Pollutant Analysis (PPA) in accordance with 40 CFR Part 122.21.
The above requirement does NOT apply to non industrial facilities.
Send the completed renewal package to:
Mrs. Dina Sprinkle
NC DENR / DWQ / Point Source Branch
1617 Mail Service Center
Raleigh; NC 27699-1617
[phone]

i
PYRAMID
ENVIRONMENTAL & ENGINEERING, P.C.
Authorization for NPDES Renewal Package Preparation
I, Jerry Sparks, the president of Sparks Oil Company, authorize Pyramid Environmental &
Engineering, P.C. to prepare the NPDES Renewal Package for the JW Smith/ Camp Springs 76
groundwater remediation system.
of Sparks Oil Company Date
P.O. Box 16265 • Greensboro, NC 27416
503 Industrial Ave • Greensboro, NC 27406
Phone [phone] • Fax [phone] • Toll Free [phone]
Email: [e-mail]
www.12yramidenvironmental.com

NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
Mail the complete application to:
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
NPDES Permit Number INCO088692
If you are completing this form in computer use the TAB key or the up - down arrows to move from one
field to the next. To check the boxes, click your mouse on top of the box. Otherwise, please print or type.
1. Contact Information:
Owner Name
Facility Name
Mailing Address
City
State / Zip Code
Telephone Number
Fax Number
e-mail Address
Sparks Oil Company
JW Smith / Camp Springs 76 remediation system
412 N Scales Street
Reidsville
NC / 27320-2909
[phone]
[phone]
[e-mail]
2. Location of facility producing discharge:
Check here if same as above ❑
Street Address or State Road
City
State / Zip Code
County
8920 Cherry Grove Road
Reidsville
NC /27320/0227
Caswell
3. Operator Information:
Name of the firm, consultant or other entity that operates the facility. (Note that this is not referring to the
Operator in Responsible Charge or ORC)
Name Pyramid Environmental & Engineering, P.C.
Mailing Address PO Box 16265
City
State / Zip Code
Telephone Number
Fax Number
4. Ownership Status:
Federal ❑
Greensboro
NC / 27416-0265
[phone]
[phone]
State ❑ Private ® Public ❑
Page 1 of 3 C -GW 03/05

NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
5. Products recovered:
Gasoline ❑ Diesel fuel ❑ Solvents ❑ Other Petroleum
contaminated groundwater
6. Number of separate discharge points: 1
Outfall Identification number(s) 1
7. Frequency of discharge: Continuous ® Intermittent ❑
If intermittent:
Days per week discharge occurs: Duration:
S. Treatment System Design flow 0.009 MGD
9. Name of receiving stream(s) (Provide a map showing the exact location of each outfall, including
latitude and longitude):
Unnamed tributary of County Line Creek
10. Please list all additives to the treatment system, including chemicals or nutrients, that
have the potential to be discharged.
none
11. Is this facility located on Indian country? (check one)
Yes ❑ No
12. Additional Information
All applicants (including renewals):
A USGS topographical map (or copy of the relevant portion) which shows all outfalls
A summary of the most recent analytical results (effluent data, if available) containing the
maximum values for each chemical detected
NEW Applicants only:
Engineering Alternative Analysis
Description of remediation treatment system components, capacities, and removal
efficiency for detected compounds.
If the treatment system will discharge to a storm sewer, written approval from the
municipality responsible for the sewer.
A list of any chemicals found in detectable amounts at the site, with the maximum
observed concentration reported for each chemical (the most recent sample must be
collected less than one year prior to the date of this application)
For petroleum -contaminated sites - Analyses for Volatile Organic Compounds (VOC) should
be performed. Analyses for any fuel additives likely to be present at the site and for phenol
and lead should also be performed.
For sites contaminated with solvents or other contaminants - EPA Method 624/625
analysis should be performed.
Page 2 of 3 C -GW 03105

NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
13. Applicant Certification
I certify that I am familiar with the information contained in the application and that to the
best of my knowledge and belief such information is true, complete, and accurate.
Jerry Sparks President
Printed Mme of Person Signing . Title
Date
rb. Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false
ment representation, or certification in any application, record, report, plan, or other document files or
required to be maintained under Article 21 or regulations of the Environmental Management Commission
implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or
monitoring device or method required to be operated or maintained under Article 21 or regulations of the
Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable
by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both. (18 U.S.C. Section
1001 provides a punishment by a fine of not more than $25,000 or imprisonment not more than 5 years, or both,
fora similar offense.)
Page 3 of3 C -GW 03/05

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Sparks Oil Company
Camp Springs 67 Groundwater Rernediation Site
Latitude: 360 17'461, N State Quad• Cherry Grove
Lo ltu!dg; 79P 29142" W Permittee! Flow: 0.009 MG1)
R e c e i i 0 _q §j _ra_aD_- UT to Country Line Crook Stream Class-. W$41 HOW
Dra1na,qe.,FL4s1-
_n,* Romoke River Basin Sub -Basin: 03-02-04/030I0104
Facility
Lovition
41j 31
(not to =10)
NPDES Permit NCO088692
North Caswell County

EFFLtENT
NPDES PERMIT NO. NC 0088692 DISCHARGE NO. 1 MONTH October YEAR 2016
FACILITYNAME J. W. Smith / Camp Springs 76 CLASS NA COUNTY Caswell
CERTIFIED LABORATORY (1) Pace Analytical CERTIFICATION NO. 402
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Danny Oldham GRADED C -10ERTIFICATION NO. 991232
PERSON(S) COLLECTING SAMPLES Danny Oldham ORC PHONE 3 3 6 - 312 - 4 2 83
CHECK BOX IF ORC HAS CHANGED NO FLOW/ DISCHARGE FROM SITE
Mail ORIGINAL and ONE COPY to:
ATTN: CENTRAL FILES,
DIVISION OF WATER QUALITY
1617 MAIL SERVICE CENTER
RALEIGH, NC 27699-1617
0
BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DWQ Form MR -1.] (11{04) Single point totalizing flow meter is used at this remediation system
X1051
.ead
ng/L
:5.0
lone
r3
ENTERPARAMETER CODE
ABOVEAM o AND UNITS
DWQ Form MR -1.] (11{04) Single point totalizing flow meter is used at this remediation system
X1051
.ead
ng/L
:5.0
lone

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) F 7x
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements El
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and.evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
S Oil Cott
(Please print
electronically)
'`dJd-/16 _-
412 N Scales St., Reidsville, NC 27320 336"3498231 www.sparksoil.com May 31,2017
Permittee Address Phone Number e-mail address Permit Expiration Date
ADDITIONAL CERTIFIED LABORATORIES
Certified Laboratory (2)
Certification No.
Certified Laboratory (3)
Certification No.
Certified Laboratory (4)
Certification No.
Certified Laboratory (5)
Certification No.
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/was and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
ORC On Site?: ORC must visit facility anddocument visitation of facility as required per 15A NCAC 8G.0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

1�98XAnalytical'
} wmpacelabsxom
I
October 24, 2016
Mr. Mika Trifunovic
Pyramid Environmental
P.O. Box 16265
Greensboro, NC 27416
RE: Project: JW Smith
Pace Project No.: 92315946
Dear Mr. Trifunovic:
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

aceAnafytical
11 wwwpacefabs.com
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification M 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification M E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification M 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
VirginiaNELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

aceAnalytical o
wrm.pacelabs.com
I
SAMPLE ANALYTE COUNT
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92315946001 INF EPA6010
SH1
1
PASI-A
SM 6200B
CAH
63
PASI-C
SM 2540D
MLS
1
PASI-A
EPA 420.4
DMN
1
PASI-A
92315946002 EFF EPA6010
SH1
1
PASI-A
SM 6200B
CAH
63
PASI-C
SM 2540D
ALC
1
PASI-A
EPA 420.4
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 20

Pace Analytical Services, LLC
aceMalyticale 9800 Kincey Ave. Suite 100
Huntersville, NC 28078
www.pac&bs.com [phone]
ANALYTICAL RESULTS
Project: JW Smith
Pace Project No.: 92315946
Sample: INF
Parameters
Lab ID: 92315946001 Collected: 10/12/1618:00 Received: 10/13/1610:21 Matrix: Water
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP, Lab Filtered
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead, Dissolved
ND
ug/L
5.0
1 10/15/16 01:59
10/21/16 12:26
7439-92-1
6200B MSV
Analytical Method: SM 6200B
Benzene
29.9
ug/L
1.0
2
10/20/16 05:15
71-43-2
Bromobenzene
ND
ug/L
1.0
2
10/20/16 05:15
108-86-1
Bromochloromethane
ND
ug/L
1.0
2
10/20/16 05:15
74-97-5
Bromodichloromethane
ND
ug/L
1.0
2
10/20/16 05:15
75-27-4
Bromoform
ND
ug/L
1.0
2
10/20/16 05:15
75-25-2
Bromomethane
ND
ug/L
10.0
2
10/20/16 05:15
74-83-9
n-Butylbenzene
ND
ug/L
1.0
2
10/20/16 05:15
104-51-8
sec-Butylbenzene
ND
ug/L
1.0
2
10/20/16 05:15
135-98-8
tert-Butylbenzene
ND
ug/L
1.0
2
10/20/16 05:15
98-06-6
Carbon tetrachloride
ND
ug/L
1.0
2
10/20/16 05:15
56-23-5
Chlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
108-90-7
Chloroethane
ND
ug/L
2.0
2
10/20/16 05:15
75-00-3
Chloroform
ND
ug/L
1.0
2
10/20/16 05:15
67-66-3
Chloromethane
ND
ug/L
2.0
2
10/20/16 05:15
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
2
10/20/16 05:15
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
2
10/20/16 05:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
2
10/20/16 05:15
96-12-8
Dibromochloromethane
ND
ug/L
1.0
2
10/20/16 05:15
124-48-1
1,2-Dibromoethane (EDB)
2.5
ug/L
1.0
2
10/20/16 05:15
106-93-4
Dibromomethane
ND
ug/L
1.0
2
10/20/16 05:15
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
2
10/20/16 05:15
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
2
10/20/16 05:15
75-34-3
1,2-Dichloroethane
1.8
ug/L
1.0
2
10/20/16 05:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
2
10/20/16 05:15
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
1.0
2
10/20/16 05:15
156-59-2
trans- l,2-Dichloroethena
ND
ug/L
1.0
2
10/20/16 05:15
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
2
10/20/16 05:15
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
1.0
2
10/20/16 05:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
2
10/20/16 05:15
10061-02-6
Diisopropyl ether
1.0
ug/L
1.0
2
10/20/16 05:15
108-20-3
Ethylbenzene
16.4
ug/L
1.0
2
10/20/16 05:15
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
4.0
2
10/20/16 05:15
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
1.0
2
10/20/16 05:15
98-82-8
Methylene Chloride
4.0
ug/L
4.0
2
10/20/16 05:15
75-09-2 C9
Methyl-tert-butyl ether
119
ug/L
1.0
2
10/20/16 05:15
1634-04-4
Naphthalene
44.2
ug/L
4.0
2
10/20/16 05:15
91-20-3
n-Propylbenzene
ND
ug/L.
1.0
2
10/20/16 05:15
103-65-1
Styrene
ND
ug/L
1.0
2
10/20/16 05:15
100-42-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM
without the written consent of Pace Analytical Services, LLC.
Page 4 of 20

aceAnalytical
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I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JW Smith
Pace Project No.: 92315946
Sample: INF
Lab ID: 92315946001 Collected: 10/12/16 18:00
Received: 10/13/16 10:21 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed
CAS No. Qual
6200B MSV
Analytical Method:
SM 6200B
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
- .2
10/20/16 05:15
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
2
10/20/16 05:15
79-34-5
Tetrachloroethene
ND
ug/L
1.0
2
10/20/16 05:15
127-18-4
Toluene
223
ug/L
1.0
2
10/20/16 05:15
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
4.0
2
10/20/16 05:15
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
4.0
2
10/20/16 05:15
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
1.0
2
10/20/16 05:15
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
1.0
2
10/20/16 05:15
79-00-5
Trichloroethene
ND
ug/L
1.0
2
10/20/16 05:15
79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
2
10/20/16 05:15
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
96-18-4
1,2,4-Trimethylbenzene
73.1
ug/L
1.0
2
10/20/16 05:15
95-63-6
1,3;5-Trimethylbenzene
31.5
ug/L
1.0
2
10/20/16 05:15
108-67-8
Vinyl chloride
ND
ug/L
2.0
2
10/20/16 05:15
75-01-4
m&p-Xylene
193
ug/L
2.0
2
10/20/16 05:15
179601-23-1
o -Xylene
160
ug/L
1.0
2
10/20/16 05:15
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
2
10/20/16 05:15
17060-07-0
4-Bromofluorobenzene (S)
96
%
70-130
2
10/20/16 05:15
460-00-4
Toluene -d8 (S) ,
105
%
70-130
2
10/20/16 05:15
2037-26-5
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND' mg/L 12.5 1 10/17/16 11:51
420.4 Phenolics, Total Analytical Method: EPA 420.4
Phenol 0.047 mg/L 0.010 1 10/21/1613:50
I
Date: 10/24/2016 12:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 20

aeeAnalyflcal
www.pacefta.mm
f
l
ANALYTICAL RESULTS
Project: JW Smith
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Pace Project No.: 92315946
Sample: EFF Lab ID: 92315946002 Collected: 10/12/16 18:30 Received: 10/13/16 10:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6010 MET ICP, Lab Filtered
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead, Dissolved
ND
ug/L
5.0
1 10/15/1601:59
10121/1612:29
7439-92-1
62008 MSV
Analytical Method: SM 6200B
Benzene
ND
ug/L
0.50
1
10/20/16 04:07
71-43-2
Bromobenzene
ND
ug/L
0.50
1
10/20/16 04:07
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
10/20/16 04:07
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
10/20/16 04:07
75-27-4
Bromoform
ND
ug/L
0.50
1
10/20/16 04:07
75-25-2
Bromomethane,
ND
ug/L
5.0
1
10/20/16 04:07
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
104-51-8
sec -Butyl benzene
ND
ug/L
0.50
1
10/20/16 04:07
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
10/20/16 04:07
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
108-90-7
Chloroethane
ND
ug/L
1.0
1
10/20/16 04:07
75-00-3
Chloroform
ND
ug/L
0.50
1
10/20/16 04:07
67-66-3
Chloromethane
ND
ug/L
1.0
1
10/20/16 04:07
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
10/20/16 04:07
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
10/20/16 04:07
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
10/20/16 04:07
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
10/20/16 04:07
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
10/20/16 04:07
106-93-4
Dibromomethane
ND
ug/L
0.50
1
10/20/16 04:07
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
10/20/16 04:07
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
10/20/16 04:07
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
10/20/16 04:07
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
10/20/16 04:07
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
1
10/20/16 04:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
10/20/16 04:07
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
10/20/16 04:07
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
10/20/16 04:07
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
10/20/16 04:07
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
10/20/1604:07
563-58-6
cis- 1,3-Dichloropropene
ND
ug/L
0.50
1
10/20/16 04:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
10/20/16 04:07
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
10/20/16 04:07
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
10/20/16 04:07
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
10/20/16 04:07
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
10/20/1604:07
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
10/20/16 04:07
1634-04-4
Naphthalene
ND
ug/L
2.0
1
10/20/16 04:07
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
103-65-1
Styrene
ND
ug/L
0.50
1
10/20/16 04:07
100-42-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 20

1�;?XAnalyftal"
www.pacefabs.com'
I
ANALYTICAL RESULTS
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: EFF
Lab ID: 92315946002 Collected: 10/12/16 18:30
Received: 10/13/1610:21 Matrix: Water
Parameters
Results
Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
1,1,1,2 -Tetrachloroethane
ND
ug/L
0.50
1
10/20/16 04:07 630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
0.50
1
10/20/16 04:07 79-94-5
Tetrachloroethene
ND
ug/L
0.50
1
10/20/16 04:07 127-18-4
Toluene
ND
ug/L
0.50
1
10/20/16 04:07 108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
10/20/16 04:07 87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
1
10/20/16 04:07 120-82-1
1,1,1 -Trichloroethane
ND
ug/L
0.50
1
10/20/1604:07 71-55-6
1,1,2 -Trichloroethane
ND
ug/L
0.50
1
10/20/16 04:07 79-00-5
Trichloroethene
ND
ug/L
0.50
1
10/20/16 04:07 79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
10/20/16 04:07 75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
10/20/16 04:07 96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
10/20/1604:07 95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
10/20/16 04:07 108-67-8
Vinyl chloride
ND
ug/L
1.0
1 -
10/20/16 04:07 75-01-4
m&p-Xylene
ND
ug/L
1.0
1
10/20/16 04:07 179601-23-1
o -Xylene
ND
ug/L
0.50
' 1
10/20/16 04:07 95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
10/20/16 04:07 17060-07-0
4-Bromofluorobenzene (S)
95
%
70-130
1
10/20/16 04:07 460-00-4
Toluene -d8 (S)
101
%
70-130
1
1,0/20/16 04:07 2037-26-5
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 5.0 1 10/17/16 14:39
420.4 Phenolics, Total Analytical Method: EPA 420.4
Phenol 0.017 mg/L 0.010 1 10/21/1613:50
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 20

aceAnalytical "
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QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333151 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET Filtered Diss.
Associated Lab Samples: 92315946001, 92315946002
METHOD BLANK: 1846102 Matrix: Water
Associated Lab Samples: 92315946001, 92315946002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead, Dissolved ug/L ND 5.0 10/21/16 11:20
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1846103
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Lead, Dissolved ug/L 500 482 96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1846104 1846105
MS MSD
92315870003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Lead, Dissolved ug/L ND 500 500 450 453 90 91 75-125 1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 20

1�5a'ceAnaljftal
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I
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333782 Analysis Method: SM 62006
QC Batch Method: SM 6200B Analysis Description: 6200B MSV
Associated Lab Samples: 92315946001, 92315946002
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
METHOD BLANK: 1849729 Matrix: Water
Associated Lab Samples: 92315946001, 92315946002
Blank Reporting
Parameter Units Result Limit
Analyzed Qualifiers
1,1,1,2 -Tetrachloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1,1 -Trichloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1,2,2 -Tetrachloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1,2 -Trichloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1-Dichloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1-Dichloroethene
ug/L
ND
0.50
10/20/16 01:01
1,1-Dichloropropene
ug/L
ND
0.50
10/20/16 01:01
1,2,3-Trichlorobenzene
ug/L
ND
2.0
10/20/16 01:01
1,2,3-Trichloropropane
ug/L
ND
0,50
10/20/16,01:01
1,2,4-Trichlorobenzene
ug/L
ND
2.0
10/20/16 01:01
1,2,4-Trimethylbenzene
ug/L
ND
0.50
10/20/16 01:01
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
10/20/16 01:01
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
10/20/16 01:01
1,2 -Dichlorobenzene
ug/L
ND
0.50
10/20/1601:01
1,2-Dichloroethahe
ug/L
ND
0.50
10/20/16 01:01
1,2-Dichloropropane
ug/L
ND
0.50
10/20/16 01:01
1,3,5-Trimethylbenzene
ug/L
ND
0.50
10/20/16 01:01
1,3 -Dichlorobenzene
ug/L
ND
0.50
10/20/16 01:01
1,3-Dichloropropane
ug/L
ND
0.50
10/20/16 01:01
1,4 -Dichlorobenzene
ug/L
ND
0.50
10/20/16 01:01
2,2-Dichloropropane
ug/L
ND
0.50
10/20/16 01:01
2-Chlorotoluene
ug/L
ND
0.50
10/20/1.6 01:01
4-Chlorotoluene
ug/L
ND -
0.50
10/20/16 01:01
Benzene
ug/L
ND
0.50
10/20/16 01:01
Bromobenzene
ug/L
ND
0.50
10/20/16 01:01
Bromochloromethane
ug/L
ND
0.50
10/20/16 01:01
Bromodichloromethane ,
ug/L
ND
0.50
10/20/16 01:01
Bromoform
ug/L
ND
0.50
10/20/16 01:01
Bromomethane
ug/L
ND
5.0
10/20/16 01:01
Carbon tetrachloride
ug/L
ND
0.50
10/20/16 01:01
Chlorobenzene
ug/L
ND
0.50
10/20/16 01:01
Chloroethane
ug/L
ND
1.0
10/20/16 01:01
Chloroform
ug/L
ND
0.50
10/20/16 01:01
Chloromethane
ug/L
ND
1.0
10/20/16 01:01
cis-1,2-Dichloroethene
ug/L
ND
-0.50
10/20/16 01:01
cis-1,3-Dichloropropene
ug/L
ND
0.50
10/20/16 01:01
Dibromoch lorom ethane
ug/L
ND
0.50
10/20/16 01:01
Dibromomethane
ug/L
ND
0.50
10/20/16 01:01
Dichlorodifluoromethane
ug/L
ND
0.50
10/20/16 01:01
Diisopropyl ether
ug/L
ND
0.50
10/20/16 01:01
Ethylbenzene
ug/L
ND
0.50
10/20/16 01:01
Results presented onthis
page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT. OF LABORATORY
ANALYSIS
This report shall not.be reproduced, except in full,
Date: 10/24/2016 12:50 PM
without the written consent of
Pace Analytical Services, LLC.
Page 9 of 20

axAnalytical
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QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
METHOD BLANK: 1849729
Associated Lab Samples: 92315946001, 92315946002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
10/20/16 01:01
Isopropylbenzene (Cumene)
ug/L
ND
0.50
10/20/16 01:01
m&p-Xylene
ug/L
ND
1.0
10/20/16 01:01
Methyl-tert-butyl ether
ug/L
ND
0.50
10/20/16 01:01
Methylene Chloride
ug/L
ND
2.0
10/20/16 01:01
n-Butylbenzene
ug/L
ND
0.50
10/20/16 01:01
n-Propylbenzene
ug/L
ND
0.50
10/20/16 01:01
Naphthalene
ug/L
ND
2.0
10/20/16 01:01
o -Xylene
ug/L
ND
0.50
10/20/16 01:01
sec-Butylbenzene
ug/L
ND
0.50
10/20/16 01:01
Styrene
ug/L
ND
0.50
10/20/16 01:01
tert-Butylbenzene
ug/L
ND
0.50
10/20/16 01:01
Tetrachloroethene
ug/L
ND
0.50
10/20/16 01:01
Toluene
ug/L
ND
0.50
10/20/16 01:01
trans- 1,2-Dichloroethene
ug/L
ND
0.50
10/20/16 01:01
trans-1,3-Dichloropropene
ug/L
ND
0.50
10/20/16 01:01
Trichloroethene
ug/L
ND
0.50
10/20/16 01:01
Trichlorofluoromethane
ug/L
ND
1.0
10/20/16 01:01
Vinyl chloride
ug/L
ND
1.0
10/20/16 01:01
1,2-Dichloroethane-d4 (S)
%
117
70-130
10/20/16 01:01
4-Bromofluorobenzene (S)
%
93
70-130
10/20/16 01:01
Toluene -d8 (S)
%
102
70-130
10/20/16 01:01
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1849730
Units
Spike
Conc.
LCS
Result
LCS
% Rec .
% Rec
Limits
1,1,1,2 -Tetrachloroethane
ug/L
50
48.6
97
60-140
1,1,1 -Trichloroethane
ug/L
50
53.8
108
60-140
1,1,2,2 -Tetrachloroethane
ug/L
50
45.4
91
60-140
1,1,2 -Trichloroethane
ug/L
50
49.3
99
60-140
1,1-Dichloroethane
ug/L
50
51.9
104
60-140
1,1-Dichloroethene
ug/L
50
59.3
119
60-140
1,1-Dichloropropene
ug/L
50
49.7
99
60-140
1,2,3-Trichlorobenzene
ug/L
50
45.7
91
60-140
1,2,3-Trichloropropane
ug/L
50
47.5
95
60-140
1,2,4-Trichlorobenzene
ug/L
50
47.0
94
60-140
1,2,4-Trimethylbenzene
ug/L
50
50.6
101
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
53.0
106
60-140
1,2-Dibromoethane (EDB)
ug/L
50
51.2
102
60-140
1,2 -Dichlorobenzene
ug/L
50
49.6
99
60-140
1,2-Dichloroethane
ug/L
50
47.7
95
60-140
1,2-Dichloropropane
ug/L
50
48.7
97
60-140
1;3,5-Trimethylbenzene
ug/L
50
49.5
99
60-140
1,3 -Dichlorobenzene
ug/L
50
47.3
95
60-140
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20

aceAnalytical
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Project: JW Smith
Pace Project No.: 92315946
LABORATORY CONTROL SAMPLE: 1849730
Parameter
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Spike LCS LCS % Rec
Units Conc. Result % Rec Limits Qualifiers
1,3-Dichloropropane
ug/L
50
45.7
91
60-140
1,4 -Dichlorobenzene
ug/L
50
46.7
93
60-140
2,2-Dichloropropane
ug/L
50
48.7
97
60-140
2-Chlorotoluene
ug/L
50
50.5
101
60-140
4-Chlorotoluene
ug/L
50
49.7
99
60-140
Benzene
ug/L
50
49.2
98
60-140
Bromobenzene
ug/L
50
50.8
102
60-140
Bromochloromethane
ug/L
50
49.7
99
60-140
Bromodichloromethane
ug/L
50
51.2
.102
60-140
Bromoform
ug/L
50
47.7
95
60-140
Bromomethane
ug/L
50
44.3
89
60-140
Carbon tetrachloride
ug/L
50
54.9
110
60-140 '
Chlorobenzene
ug/L
50
48.0
96
60-140
Chloroethane
ug/L
50
35.4
71
60-140
Chloroform
ug/L
50
49.5
99
60-140
Chloromethane
ug/L
50
62.7
125
60-140
cis-1,2-Dichloroethene
ug/L
50
55.1
110
60-140
cis-1,3-Dichloropropene
ug/L
50
48.7
97
60-140
Dibromochloromethane
ug/L
50
50.0
100
60-140
Dibromomethane
ug/L
50
43.8
88
60-140
Dichlorodifluoromethane
ug/L
50
60.5
121
60-140
Diisopropyl ether
ug/L
50
65.7.
131
60-140
Ethylbenzene
ug/L
50
48.9
98
60-140
Hexachloro-1,3-butadiene
ug/L
50
46.5
93
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.7
97
60-140
m&p-Xylene
ug/L
100
97.0
97
60-140
Methyl-tert-butyl ether
ug/L
50
56.4
113
60-140
Methylene Chloride
ug/L
50
56.0
112
60-140
n-Butylbenzene
ug/L
50
49.5
99
60-140
n-Propylbenzene
ug/L
50
47.7
95
60-140
Naphthalene
ug/L
50
49.7
99
60-140
o -Xylene
ug/L
50
48.5
97
60-140
sec-Butylbenzene
ug/L
50
49.0
98
60-140
Styrene
ug/L
50
51.1
102
60-140
tert-Butylbenzene
ug/L
50
40.7
81
60-140
Tetrachloroethene
ug/L
50
44.2
88
60-140 CU
Toluene
ug/L
50
48.4
97
60-140
trans-1,2-Dichloroethene
ug/L
50
55.9
112
60-140
trans-1,3-Dichloropropene
ug/L
50
47.1
94
60-140
Trichloroethene
ug/L
50
47.2
94
60-140
Trichlorofluoromethane
ug/L
50
39.8
80
60-140
Vinyl chloride
ug/L
50
42.9
86
60-140
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene -d8 (S)
%
102
70-130
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 20

aceAnalytical"
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QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1849731
MS
92316212007 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1849732
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2 -Tetrachloroethane
ug/L
ND
20
20
20.3
20.1
102
101
60-140
1
1,1,1 -Trichloroethane
ug/L
ND
20
20
23.9
24.0
119
120
60-140
1
1,1,2,2 -Tetrachloroethane
ug/L
ND
20
20
19.9
19.1
100
95
60-140
4
1,1,2 -Trichloroethane
ug/L
ND
20
20
20.8
19.8
104
99
60-140
5
1,1-Dichloroethane
ug/L
ND
20
20
23.0
22.6
115
113
60-140
2
1,1-Dichioroethene
ug/L
ND
20
20
27.0
26.9
135
135
60-140
0
1,1-Dichloropropene
ug/L
ND
20
20
22.5
22.1
112
110
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
20
20
21.1
20.1
106
100
60-140
5
1,2,3-Trichloropropane
ug/L
ND
20
20
20.0
19.2
100
96
60-140
4
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.9
19.9
104
99
60-140
5
1,2,4-Trimethylbenzene
ug/L
ND
20
20
22.7
21.4
113
107
60-140
6
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
23.7
22.0
119
110
60-140
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.8
21.0
109
105
60-140
4
1,2 -Dichlorobenzene
ug/L
ND
20
20
22.2
20.9
111
104
60-140
6
1,2-Dichloroethane
ug/L
ND
20
20
21.2
21.8
105
108
60-140
3
1,2-Dichloropropane
ug/L
ND
20
20
20.8
20.5
104
102
60-140
2
1,3,5-Trimethylbenzene
ug/L
ND
20
20
22.3
21.0
112
105
60-140
6
1,3 -Dichlorobenzene
ug/L
ND
20
20
21.1
19.8
106
99
60-140
6
1,3-Dichloropropane
ug/L
ND
20
20
19.7
18.8
98
94
60-140
5
1,4 -Dichlorobenzene
ug/L
ND
20
20
-21.1
19.7
105
98
60-140
7
2,2-Dichloropropane
ug/L
ND
20
20
21.7
21.2
108
106
60-140
2
2-Chlorotoluene
ug/L
ND
20
20
23.0
21.6
115
108
60-140
6
4-Chlorotoluene
ug/L
ND
20
20
22.4
21.2
112
106
60-140
6
Benzene
ug/L
ND
20
20
21.4
20.7
107
103
60-140
4
Bromobenzene
ug/L
ND
20
20
22.7
21.1
113
105
60-140
7
Bromochloromethane
ug/L
ND
20
20
21.3
20.6
106
103
60-140
3
Bromodichloromethane
ug/L
ND
20
20
22.0
21.2
110
106
60-140
4
Bromoform
ug/L
ND
20
20
18.8
18.3
94
92
60-140
3
Bromomethane
ug/L
ND
20
20
21.1
21.9
106
109
60-140
4
Carbon tetrachloride
ug/L
ND
20
20
25.5
24.5
127
123
60-140
4
Chlorobenzene
ug/L
ND
20
20
21.2
20.5
106
103
60-140
3
Chloroethane
ug/L
ND
20
20
15.9
17.7
80
88
60-140
10
Chloroform
ug/L
ND
20
20
21.9
21.6
109
108
60-140
1
Chloromethane
ug/L
ND
20
20
27.5
29.2
136
145
60-140
6 M1
cis-1,2-Dichloroethene
ug/L
ND
20
20
24.1
23.9
120
120
60-140
1
cis-1,3-Dichloropropene
ug/L
ND
20
20
20.3
19.7
102
98
60-140
3
Dibromochloromethane
ug/L
ND
20
20
21.1
20.3
105
101
60-140
4
Dibromomethane
ug/L
ND
20
20
1.8.7
18.0
93
90
60-140
4
Dichlorodifluoromethane
ug/L
ND
20
20
28.2
28.8
141
144
60-140
2 M1
Diisopropyl ether
ug/L
ND
20
20
27.5
27.0
137
135
60-140
2
Ethylbenzene
ug/L
ND
20
20
22.0
20.9
110
105
60-140
5
Hexachloro-1,3-butadiene
ug/L
ND
20
20
23.0
21.1
114
105
60-140
9
Isopropylbenzene (Cumene)
ug/L
ND
20
20
21.5
20.9
108
104
60-140
3
m&p-Xylene
ug/L
ND
40
40
43.6
42.0
109
105
60-140
4
Methyl-tert-butyl ether
ug/L
ND
20
20
24.2
23.6
120
117
60-140
3
Methylene Chloride
ug/L
ND
20
20
23.9
23.5
119
118
60-140
1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 20

aceAnalytical
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i
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JW Smith
Pace Project No.: 92315946
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1849731
1849732
MS
MSD
92316212007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Clual
n-Butylbenzene
ug/L
ND
20
20
23.1
21.5
116
108
60-140
7
n-Propylbenzene
ug/L
ND
20
20
22.0
20.7
110
104
60-140
6
Naphthalene
ug/L
ND
20
20
22.7
21.1
113
105
60-140
7
o -Xylene
ug/L
ND
20
20
21.1
20.4
106
102
60-140
4
sec-Butylbenzene
ug/L
ND
20
20
22.8
21.5
114
107
60-140
6
Styrene
ug/L
ND
20
20
21.5
21.1
107
105
60-140
2
tert-Butylbenzene
ug/L
ND
20
20
18.8
17.6
94
88
60-140
6
Tetrachloroethene
ug/L
ND
20
20
20.0
19.3
100
96
60-140
4
Toluene
ug/L
ND
20
20
21.5
20.9
108
105
60-140
3
trans-1,2-Dichloroethene
ug/L
ND
20
20
25.2
24.4
126
122
60-140
3
trans-1,3-Dichloropropene
ug/L
ND
20
20
19.3
19.0
97
95
60-140
2
Trichloroethene
ug/L
ND
20
20
20.6
20.0
103
100
60-140
3
Trichlorofluoromethane
ug/L
ND
20
20
19.3
20.3
96
102
60-140
5
Vinyl chloride
ug/L
ND
20
20
21.6
21.8
108
109
60-140
1
1,2-Dichloroethane-d4 (S)
%
104
112
70-130
4-Bromofluorobenzene (S)
%
94
95
70-130
Toluene -d8 (S)
%
102
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20

aceAnalytical
( www.pacetabs.com
I
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333350 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92315946001
METHOD BLANK: 1847344
Associated Lab Samples: 92315946001
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE:
Parameter
1847345
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1847346
Parameter
Units
Total Suspended Solids
mg/L
SAMPLE DUPLICATE: 1847347
Parameter
Units
Total Suspended Solids
mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 10/17/1611:43
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 240 96 90-110
92315796001 Dup
Result Result RPD Qualifiers
ND ND
92315824001 Dup
Result Result RPD Qualifiers `
18.7 19.0 2
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20

,�aceAnalyfical
wwwpacelabs.com
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333411 Analysis Method: SM 2540D
QC Batch Method: SM 2540D Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92315946002
METHOD BLANK: 1847742
Associated Lab Samples: 92315946002
Parameter Units
Total Suspended Solids mg/L
LABORATORY CONTROL SAMPLE: 1847743
Parameter Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 1847744
Parameter Units
Total Suspended Solids mg/L
SAMPLE DUPLICATE: 1847745
Parameter
Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 10/17/1614:39
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 230 92 90-110
92315946002 Dup
Result Result RPD Qualifiers
ND ND
92315996001 Dup
Units Result Result
mg/L ND ND
RPD Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 20

1a
ceAna1j cal'
",wpamlabs.com
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333927 Analysis Method: EPA 420.4
QC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92315946001, 92315946002
METHOD BLANK: 1850808 Matrix: Water
Associated Lab Samples: 92315946001, 92315946002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg/L ND 0.010 10/21/1613:26
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1850809
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rec Limits Qualifiers
Phenol mg/L .05 0.050 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1850810 1850811
MS MSD
92315167005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Phenol mg/L 175 .05 .05 0.16 0.16 -31 -37 90-110 2 M1
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1850812 1850813
MS MSD
92315180001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Phenol mg/L 0.017 .05 .05 0.064 0.064 94 93 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 20

aceAnaljftal
www.pacelabs.com
f
QUALIFIERS
Project: JW Smith
Pace Project No.: 92315946
DEFINITIONS
DF : Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
CU The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below
reporting limits in associated samples. Results unaffected by high bias.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 20

aC6MaIXical e
( www.pacelabs.com
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
92315946001
INF
EPA 3010
333151
EPA 6010
92315946002
EFF
EPA 3010
333151
EPA 6010
92315946001
INF
SM 62008
333782
92315946002
EFF
SM 6200B
333782
92315946001
INF
SM 2540D
333350
92315946002
EFF
SM 2540D
333411
92315946001
INF
EPA 420.4
333927
92315946002
EFF
EPA 420.4
333927
Date: 10/24/2016 12:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
333298
333298
Page 18 of 20

Document Name: Document Revised: Sept. 21, 2016
o Sample Condition Upon Receipt(SCUR) Page 1 of 2
Ice
Analytical Document No.: Issuing Authority:
F-CAR-CS-033-Rev.00 Pace Quality Office
Page 2 of 2 for Internal Use ONLY
W0 :9 15 94
1111111111311111111
923g39�16
•11 • • Client Name: �/�"t-t,��
Project #:
Courier: ❑Fed Ex []UPS []USPS ❑Client
❑ Commercial [Pace ❑Other:
Custody Seal Present? ❑Yes WNo Seals Intact? ❑Yes [7,VNo
Date/initials Person Examining Contents: ,1t'3 6-
Packing Material: ❑Bubble Wrap (Bubble Bags ❑None ❑Other:
Thermometer:KWet ❑Blue
❑None []samples on ice, cooling process has begun
❑ IR Gun ID: - Type of ice:.0
Correction Factor: Cooler Temp Corrected (°C): Biological Tissue Frozen? []Yes®No []N/A
Temp should be above freezing to 6'C
USDA Regulated Soil ( ❑ N/A, water sample)
Did samples originate In a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
.-n_.
;-1 U� nd D—rhn RV nti riYAS (i—iC No
LJres IIjJIVU
.._.___._„ _
Comments/Discrepancy:
Chain of Custody Present?
MYes
❑No
❑N/A
1..
Samples Arrived within Hold Time?
Yes
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
No
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
, No
❑N/A
4.
Sufficient Volume?
®Yes
[--]No
[]N/A
S.
Correct Containers Used?
-Pace Containers Used?
(Yes
MYes
[]No
[]No.._
[]N/A
[]N/A
6.
Containers Intact?
Yes
❑No
❑N/A
7.
Samples Field Filtered?
❑Yes
No
[]N/A
8. Note If sediment is visible in the dissolved container
Sample Labels Match COC? /PYes
-Includes Date/Time/ID/Analysis Matrix: l d
❑No
❑N/A
9.
All containers needing acid/base preservation have been
checked and documented on page two of SCURF? )Yes
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015
(water) DOC, LLHg
Samples checked for dechlorination? []Yes
[:]No
®No
❑N/A
[I N/A
10.
11.
Headspace in VOA Vials (>5-6mm)?
❑Yes
WNo
❑N/A
12.
Trip Blank Present?
Trip Blank Custody Seals Present?
Pace Trip Blank Lot d (if purchased):
[]Yes
❑Yes
PNo
PNo
[]N/A
❑N/A
13.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample
Discrepancy:
Date/Time:
Field Data Required? LJYes UNo
Project Manager SCURF Review: N ((� Date: 16 C. t 6
Project Manager SRF Review: ! U V ° t Date: `(jl
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Ifarolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville19 Raleigh❑ Mechanicsville[]
Page 19 of 20

PaceAnalydcal '
PTP mincglabs.con1
Section A
Rnn,dr A r:llont W-11—
CHAIN-OF-CUSTODY / Analytical Bequest Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section B Section C
Roaulred Project Information: Invoice Information:
0
N
O
Page: { of € of
S Y b s! FA fY "Y R 9
Company: Report To: AIR, -
Attention:
U A, :t U 3
Address: " r Copy To:
J
Company Name;
REGULATORY AGENCY
r }
��ry
,✓ NPDES F' GROUNDWATER I DRINKING WATER
r-' UST F RCRA I_. OTHER
r� i !
Address:
Email To:. } } Purchase order No.: isPace
Quote
Rufuroneo;
P one:. Project Name: •—r' r ,-^ `^}. f
F...
Paco Pro)oct x Z -
anasort , 1r�
Site Location
STATE:
AICRequested
Duebate TA7 ,S ,,t qq,,, a R Project Number. )� _ ' �*/
is 7"il u j ,j
Paco Prorilo 0:
Requested
Analysis
Filtered
(YIN)
Section D Matrix Codes
Required Cllent Information MATRIX I CODE
o
E,z
COLLECTED
Preservatives
3:
Drinking Water DW
;,
�
O
Water WT
Waste water ww
—
1.
m
COMPOSITE
START
COMPOSITE
ENe!GRAa
Z
Product P
Solitsotid SL
C
a
U)it
Y
}
SAMPLE ID Oil OL
Wi
Wipe WP
=
�
O
w
(A -Z, 0-9 1 :) Air AR
Sample IDs MUST BE UNIQUE Tissue TS
p
U
w
o
a
w
Z
•q
Z
F
In
`
G�
o
U
g
Other OT
a
F—
a
a
Q
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Plan Prepared by:
Mika Trifunovic
Project Engineer
Residuals Management Plan
J.W. Smith / Camp Springs 76
Groundwater' Remediation System
8920 Cherry Grove Road
Reidsville, Caswell County, NC
NPDES Permit # NCO088692
NCDEQ Incident # 21685
Prepared for:
Sparks Oil Company
412 N. Scales Street
Reidsville, NC 27320
Plan Reviewed by:
<q),N - . Z '-�)
MichaeltMan
Operatioer
Pyramid Environmental & Engineering, P.C.
P.O. Box 16265
503 Industrial Ave.
Greensboro, NC 27416-0265

Residuals Collection, Handling, Processing, Storage & Disposal
As requested by the Construction Grants and Loans Section of Division of Water Quality of
North Carolina Department of Environmental Quality (NCDEQ), collection, handling,
processing, storage and disposal of residuals generated in the product storage drum, oil water
separator (OWS), bag filter, aggregate filter, carbon vessels, ion exchange vessels, and backwash
filter are addressed in this plan.
Oil Water Separator and Product Storage Drum
Free product from the OWS discharges by gravity to a 65 gallon polyethylene product storage
drum installed outside of the system building. The product storage drum is equipped with a high-
level switch to shut down operation of the remediation system. Residuals from the OWS and
product storage drum are collected and handled by a contractor in accordance with all applicable
regulations on an as needed basis. After the collection of the residuals, the contractor
immediately hauls the residuals off the site. The contractor is also responsible for the proper
disposal or storage/processing of residuals.
Bag Filter
The bag filter is changed every month during scheduled monthly maintenance events. The used
bag filters are removed from the bag filter housing using disposable gloves and placed in a sealed
plastic container. The used bags are immediately shipped as a non -hazardous waste for proper
disposal. Pyramid is responsible for the collection, handling, and disposal of used bag filters.
Aggregate Filter and Carbon Vessels
The aggregate filter and carbon vessels are exchanged every six months by a contractor in
accordance with all applicable regulation. Used aggregate filter and carbon vessels are
immediately hauled off the site. The contractor is responsible for the residuals handling and
proper disposal or storage/processing.
Ion Exchange Vessels
Two ion exchange vessels were replaced with carbon vessels in May 2012. The NCDEQ
approved this change, however the number of carbon vessels has never been changed in the
current NPDES permit that expires on May 31, 2017. Please see the enclosed correspondence
between Pyramid and NCDEQ.
Backwash Filter
The used backwash filter media is collected and handled by a contractor in accordance with all
applicable regulations on an as needed basis. After the collection of the used media, the
contractor immediately removes the filter media from the site for processing and/or disposal. The
contractor is also responsible for proper disposal or storage/processing of the used media.
Camp Springs 76/JW Smith — Residuals Management Plan 1

Mika Trifunovic
From: Mika Trifunovic <[e-mail]>
Sent: Wednesday, June 20, 2012 11:38 AM
To: 'Bob Guerra ([e-mail])'
cc: Mike Jones ([e-mail])
Subject: JW Smith/Camp Springs 76 NPDES Permit # NCO088692
Good morning Bob,
I have just received the referenced NPDES permit form our client and I've noticed that the Supplement to Permit Cover
Sheet (attached as a PDF file) contains an incorrect number of carbon vessels.
There should be four (4 ) carbon vessels listed on the sheet because two (2) ion exchange vessels have been converted
to carbon vessels. Please see the forwarded emails.
Could you please email me the NPDES permit with the correct number of carbon vessels.
Thank you.
Mika
From: Guerra, Bob [mailto:bob.guerra(&ncdenr.gov]
Sent: Wednesday, March 14, 2012 1:26 PM
To: Mika Trifunovic
Subject: RE: Modification of JW Smith/Camp Springs 76 Remediation System
I will be including this request and incorporate the changes into your permit when I issue it.
From: Mika Trifunovic fmailto:mika@r)yramidenvironmental.coml
Sent: Wednesday, March 14, 2012 12:12 PM
To: Corporon, Joe; Guerra, Bob
Subject: Modification of JW Smith/Camp Springs 76 Remediation System
Good afternoon Joe and Bob,
As I mentioned during our conversation, we have intent to modify the JW Smith/Camp Springs 76 petroleum
contaminated groundwater remediation system which holds the NPDES Individual Permit # NC0088692.
The modification will include, conversion of two existing ion exchange vessels into carbon filter vessels. Detailed
information about the modification is provided in the attached PDF file.
Please let me know if you need any additional information or clarification.
Since the permit is currently being renewed, I would like to ask you to include this proposed modification into the
permit.
Thank you.
Mika Trifunovic
Project Manager
Pyramid Environmental & Engineering

L*OQfs,, JW Smith/Camp Springs 76 Petroleum Contaminated Groundwater
Remediation System - NPDES Permit # NCO088692
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