NC0088692_Renewal (Application)_20161122

NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
Mail the complete application to:
N. C. Department of Environment and Natural Resources
Division of Water Quality / NPDES Unit
1617 Mail Service Center, Raleigh, NC 27699-1617
NPDES Permit Number INCO088692
If you are completing this form in computer use the TAB key or the up — down arrows to move from one
field to the next. To check the boxes, click your mouse on top of the box. Otherwise, please print or type.
1. Contact Information:
Owner Name Sparks Oil Company
Facility Name JW Smith / Camp Springs 76 remediation system
Mailing Address 412 N Scales Street
City Reidsville -
State / Zip Code NC / 27320-2909
Telephone Number [phone]
Fax Number [phone]
e-mail Address [e-mail]
CEIVE®/PdCL)E0/DWR
2. Location of facility producing discharge:
NOV 22 Z016
Check here if same as above ❑
Street Address or State Road 8920 Cherry Grove Road
dater Quality
Ppraus;-t'R---G- i.ti0n
City Reidsville
State / Zip Code NC /27320/0227
County Caswell
J
3. Operator Information:
Name of the firm, consultant or other entity that operates the facility. (Note that
this is not referring to the
Operator in Responsible Charge or ORC)
Name Pyramid Environmental & Engineering, P.C.
Mailing Address PO Box 16265
City Greensboro
r
State / Zip Code NC / 27416-0265
Telephone Number [phone]
Fax Number [phone]
4. Ownership Status:
Federal ❑ State ❑ Private ® Public ❑
Page 1 of 3 C -GW 03/05

NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
5. Products recovered:
Gasoline ❑ Diesel fuel ❑ Solvents ❑ Other Petroleum
contaminated groundwater
6. Number of separate discharge points: 1
Outfall Identification number(s) 1
7. Frequency of discharge: Continuous ® Intermittent ❑
If intermittent:
Days per week discharge occurs: Duration:
8. Treatment System Design flow 0.009 MGD
9. Name of receiving stream(s) (Provide a map showing the exact location of each outfall, including
latitude and longitude):
Unnamed tributary of County Line Creek
10. Please list all additives to the treatment system, including chemicals or nutrients, that
have the potential to be discharged.
none
11. Is this facility located on Indian country? (check one)
Yes ❑ No
12. Additional Information
All applicants (including renewals):
A USGS topographical map (or copy of the relevant portion) which shows all outfalls
A summary of the most recent analytical results (effluent data, if available) containing the
maximum values for each chemical detected
NEW Applicants only:
Engineering Alternative Analysis
Description of remediation treatment system components, capacities, and removal
efficiency for detected compounds.
D If the treatment system will discharge to a storm sewer, written approval from the
municipality responsible for the sewer.
A list of any chemicals found in detectable amounts at the site, with the maximum
observed concentration reported for each chemical (the most recent sample must be
collected less than one year prior to the date of this application)
For petroleum -contaminated sites - Analyses for Volatile Organic Compounds (VOC) should
be performed. Analyses for any fuel additives likely to be present at the site and for phenol
and lead should also be performed.
For sites contaminated with solvents or other contaminants - EPA Method 624/625
analysis should be performed.
Page 2 of 3 C -GW 03/05

NPDES PERMIT APPLICATION - SHORT FORM C - GW
For discharges associated with groundwater treatment facilities.
13. Applicant Certification
I certify that I am familiar with the information contained in the application and that to the
best of my knowledge and belief such information is true, complete, and accurate.
Jerry Sparks President
Printed Mme of Person Signing Title
Date
2-111 Carolina General Statute 143-215.6 (b)(2) provides that: Any person who knowingly makes any false
atement representation, or certification in any application, record, report, plan, or other document files or
required to be maintained under Article 21 or regulations of the Environmental Management Commission
implementing that Article, or who falsifies, tampers with, or knowingly renders inaccurate any recording or
monitoring device or method required to be operated or maintained under Article 21 or regulations of the
Environmental Management Commission implementing that Article, shall be guilty of a misdemeanor punishable
by a fine not to exceed $25,000, or by imprisonment not to exceed six months, or by both. (18 U.S.C. Section
1001 provides a punishment by a fine of riot more than $25,000 or imprisonment not more than 5 years, or both,
for a similar offense.)
0M
Page 3 of 3 C -GW 03105

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Sparks Oil Company -
Camp Springs 67 Groundwater Remediation Site
Latitude; 36" 17' 46" N State Quad; Cherry Grove
L_onaltude; 791 29' 42" W Permitted Flow: 0.009 MGb
Receivi stye . U7 t0 Country Line Creek stream Class: W$ -II HQW
Drainage 6asln: Roanoke Mar Basin Sub -Basin: 03"02-04103010104
�i El,,�.T, ,,. �SL
)Facility �r�.:�1(}$ ��gj`��ladl��h! ^os:
L7ocIr��
ation
l.�!!` 1.iP.�lyltiis.�4lli{f�Iti�rl;��fRh
(not to so-ale),llr;;�nk•
NPDES Permit NG0088692
North. Caswell County

EFFLUENT
NPDES PERMIT NO. NC 0088692 DISCHARGE NO. 1 MONTH October YEAR 2016
FACILITY NAME J. W. Smith / Camp Springs 76 CLASS
NA COUNTY Caswell
CERTIFIED LABORATORY (1) Pace Analytical CERTIFICATION NO. 402
(list additional laboratories on the backside/page 2 of this form)
OPERATOR IN RESPONSIBLE CHARGE (ORC) Danny Oldham GRADEP C-10ERTIFICATION NO. 991232
PERSON(S) COLLECTING SAMPLES Danny Oldham ORC PHONE [phone]
CHECK BOX IF ORC HAS CHANGED ED NO FLOW / DISCHARGE FROM SITE
Mail ORIGINAL and ONE COPY to: �%�,�
ATTN: CENTRAL FILES x �� {� �" A91,
DIVISION OF WATER QUALITY (SIGNATURE OF OPERATOR IN RESPONSIBLE CHARGE) DATE
1617 MAIL SERVICE CENTER BY THIS SIGNATURE, I CERTIFY THAT THIS REPORT IS
RALEIGH, NC 27699-1617 ACCURATE AND COMPLETE TO THE BEST OF MY KNOWLEDGE.
DWQForm MR -1.1 (11/04) 1
Single point totalizing flow meter is used at this remediation system
01051
Lead
1<5.0
None
1 1
• 1®
1 1®�
1 1
®�®�I����
_r,?jM
ENTER PARAMETER 11
ABOVE
BELOW 1
ImIIMl11;1���©�Ifl©Ill�l��llll�lil©1i:�7©1i�7©��III�
Monthly Limit
DWQForm MR -1.1 (11/04) 1
Single point totalizing flow meter is used at this remediation system
01051
Lead
1<5.0
None

Facility Status: (Please check one of the following)
All monitoring data and sampling frequencies meet permit requirements
(including weekly averages, if applicable) Fx
Compliant
All monitoring data and sampling frequencies do NOT meet permit requirements EJ
Noncompliant
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially
threatens public health or the environment. Any information shall be provided orally within 24 hours from the time the
permittee became aware of the circumstances. A written submission shall also be provided within 5 days of the time the
permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for
improvements to be made as required by Part II.E.6 of the NPDES permit.
"I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted. Based on my inquiry of the person or persons who managed the system, or those persons directly responsible
for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and
complete. I am aware that there are significant penalties for submitting false information, including the possibility of
fines and imprisonment for knowing violations."
sparks Oil Company
ermi ee (Please print orIVA
* Date
ed electronically)
412 N Scales St., Reidsville, NC 27320 May 31,2017
336 49-8231 www.sparksoil.com Y
Permittee Address Phone Number e-mail address Permit Expiration Date
Certified Laboratory (2)
Certified Laboratory (3)
Certified Laboratory (4)
Certified Laboratory (5)
ADDITIONAL CERTIFIED LABORATORIES
PARAMETER CODES
Certification No.
Certification No.
Certification No.
Certification No.
Parameter Code assistance may be obtained by calling the NPDES Unit at [phone] or by visiting the Surface
Water Protection Section's web site at h2o.enr.state.nc.us/was and linking to the unit's information pages.
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be
entered for all of the parameters on the DMR for the entire monitoring period.
** ORC On Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then the delegation of the signatory authority must be on
file with the state per 15A NCAC 2B .0506(b)(2)(D).
Page 2

(�Iacmnalyficaf'
www.pacelabs.com
October 24, 2016
Mr. Mika Trifunovic
Pyramid Environmental
P.O. Box 16265
Greensboro, NC 27416
RE: Project: JW Smith
Pace Project No.: 92315946
Dear Mr. Trifunovic:
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on October 13, 2016.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
X,X,
Nicole Gasiorowski
[e-mail]
Project Manager
Enclosures
pCCI{FQ
r
gyp° „C
9eORA'ro�
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

1�55'neAnalytical"
( www.pacelabs.com
I
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

1eAnalyfical"
www.pacelabs.com
SAMPLE ANALYTE COUNT
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analytes
Reported
Laboratory
92315946001 INF EPA 6010
SH1
1
PASI-A
SM 62008
CAH
63
PASI-C
SM 2540D
MLS
1
PASI-A
EPA420.4
DMN
1
PASI-A
92315946002 EFF EPA 6010
SH1
1
PASI-A
SM 62006
CAH
63
PASI-C
SM 2540D
ALC
1
PASI-A
EPA420.4
DMN
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 20

aceAnalytical
wwwpacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LIC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JW Smith
Pace Project No.: 92315946
Sample: INF Lab ID: 92315946001 Collected: 10/12/16 18:00 Received: 10/13/16 10:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
6010 MET ICP, Lab Filtered
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead, Dissolved
ND
ug/L
5.0
1 10/15/16 01:59
10/21/16 12:26
7439-92-1
62008 MSV
Analytical Method:
SM 6200B
Benzene
29.9
ug/L
1.0
2
10/20/16 05:15
71-43-2
Bromobenzene
ND
ug/L
1.0
2
10/20/16 05:15
108-86-1
Bromochloromethane
ND
ug/L
1.0
2
10/20/16 05:15
74-97-5
Bromodichloromethane
ND
ug/L
1.0
2
10/20/16 05:15
75-27-4
Bromoform
ND
ug/L
1.0
2
10/20/16 05:15
75-25-2
Bromomethane
ND
ug/L
10.0
2
10/20/16 05:15
74-83-9
n-Butylbenzene
ND
ug/L
1.0
2
10/20/16 05:15
104-51-8
sec-Butylbenzene
ND
ug/L
1.0
2
10/20/16 05:15
135-98-8
tert-Butylbenzene
ND
ug/L
1.0
2
10/20/16 05:15
98-06-6
Carbon tetrachloride
ND
ug/L
1.0
2
10/20/16 05:15
56-23-5
Chlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
108-90-7
Chloroethane
ND
ug/L
2.0
2
10/20/16 05:15
75-00-3
Chloroform
ND
ug/L
1.0
2
10/20/16 05:15
67-66-3
Chloromethane
ND
ug/L
2.0
2
10/20/16 05:15
74-87-3
2-Chlorotoluene
ND
ug/L
1.0
2
10/20/16 05:15
95-49-8
4-Chlorotoluene
ND
ug/L
1.0
2
10/20/16 05:15
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
2.0
2
10/20/16 05:15
96-12-8
Dibromochloromethane
ND
ug/L
1.0
2
10/20/16 05:15
124-48-1
1,2-Dibromoethane (EDB)
2.5
ug/L
1.0
2
10/20/16 05:15
106-93-4
Dibromomethane
ND
ug/L
1.0
2
10/20/16 05:15
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
1.0
2
10/20/16 05:15
106-46-7
Dichlorodifluoromethane
ND
ug/L
1.0
2
10/20/16 05:15
75-71-8
1,1-Dichloroethane
ND
ug/L
1.0
2
10/20/16 05:15
75-34-3
1,2-Dichloroethane
1.8
ug/L
1.0
2
10/20/16 05:15
107-06-2
1,1-Dichloroethene
ND
ug/L
1.0
2
10/20/16 05:15
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
1.0
2
10/20/16 05:15
156-59-2
trans- 1,2-Dichloroethene
ND
ug/L
1.0
2
10/20/16 05:15
156-60-5
1,2-Dichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
78-87-5
1,3-Dichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
142-28-9
2,2-Dichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
594-20-7
1,1-Dichloropropene
ND
ug/L
1.0
2
10/20/16 05:15
563-58-6
cis- 1,3-Dichloropropene
ND
ug/L
1.0
2
10/20/16 05:15
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
1.0
2
10/20/16 05:15
10061-02-6
Diisopropyl ether
1.0
ug/L
1.0
2
10/20/16 05:15
108-20-3
Ethylbenzene
16.4
ug/L
1.0
2
10/20/16 05:15
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
4.0
2
10/20/16 05:15
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
1.0
2
10/20/16 05:15
98-82-8
Methylene Chloride
4.0
ug/L
4.0
2
10/20/16 05:15
75-09-2 C9
Methyl-tert-butyl ether
119
ug/L
1.0
2
10/20/16 05:15
1634-04-4
Naphthalene
44.2
ug/L
4.0
2
10/20/16 05:15
91-20-3
n-Propylbenzene
ND
ug/L
1.0
2
10/20/16 05:15
103-65-1
Styrene
ND
ug/L
1.0
2
10/20/16 05:15
100-42-5
REPORT OF LABORATORY ANALYSIS
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Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 20

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ANALYTICAL RESULTS
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: INF Lab ID: 92315946001 Collected: 10/12/16 18:00 Received: 10/13/16 10:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
6200B MSV Analytical Method: SM 6200B
1,1,1,2 -Tetrachloroethane
ND
ug/L
1.0
2
10/20/16 05:15
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
1.0
2
10/20/16 05:15
79-34-5
Tetrachloroethene
ND
ug/L
1.0
2
10/20/16 05:15
127-18-4
Toluene
223
ug/L
1.0
2
10/20/16 05:15
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
4.0
2
10/20/16 05:15
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
4.0
2
10/20/16 05:15
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
1.0
2
10/20/16 05:15
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
1.0
2
10/20/16 05:15
79-00-5
Trichloroethene
ND
ug/L
1.0
2
10/20/16 05:15
79-01-6
Trichlorofluoromethane
ND
ug/L
2.0
2
10/20/16 05:15
75-69-4
1,2,3-Trichloropropane
ND
ug/L
1.0
2
10/20/16 05:15
96-18-4
1,2,4-Trimethylbenzene
73.1
ug/L
1.0
2
10/20/16 05:15
95-63-6
1,3,5-Tdmethylbenzene
31.5
ug/L
1.0
2
10/20/16 05:15
108-67-8
Vinyl chloride
ND
ug/L
2.0
2
10/20/16 05:15
75-01-4
m&p-Xylene
193
ug/L
2.0
2
10/20/16 05:15
179601-23-1
o -Xylene
160
ug/L
1.0
2
10/20/16 05:15
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
2
10/20/16 05:15
17060-07-0
4-Bromofluorobenzene (S)
96
%
70-130
2
10/20/16 05:15
460-00-4
Toluene -d8 (S)
105
%
70-130
2
10/20/16 05:15
2037-26-5
2540D Total Suspended Solids Analytical Method: SM 2540D
Total Suspended Solids ND mg/L 12.5 1 10/17/16 11:51
420.4 Phenolics, Total Analytical Method: EPA420.4
Phenol 0.047 mg/L 0.010 1 10/21/1613:50
Date: 10/24/2016 12:50 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
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ANALYTICAL RESULTS
Pace Analytical Services, LIC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JW Smith
Pace Project No.: 92315946
Sample: EFF Lab ID: 92315946002 Collected: 10/12/16 18:30 Received: 10/13/16 10:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
6010 MET ICP, Lab Filtered
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Lead, Dissolved
ND
ug/L
5.0
1 10/15/16 01:59
10/21/16 12:29
7439-92-1
6200B MSV
Analytical Method: SM 62008
Benzene
ND
ug/L
0.50
1
10/20/16 04:07
71-43-2
Bromobenzene
ND
ug/L
0.50
1
10/20/16 04:07
108-86-1
Bromochloromethane
ND
ug/L
0.50
1
10/20/16 04:07
74-97-5
Bromodichloromethane
ND
ug/L
0.50
1
10/20/16 04:07
75-27-4
Bromoform
ND
ug/L
0.50
1
10/20/16 04:07
75-25-2
Bromomethane
ND
ug/L
5.0
1
10/20/16 04:07
74-83-9
n-Butylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
135-98-8
tert-Butyl benzene
ND
ug/L
0.50
1
10/20/16 04:07
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
1
10/20/16 04:07
56-23-5
Chlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
108-90-7
Chloroethane
ND
ug/L
1.0
1
10/20/16 04:07
75-00-3
Chloroform
ND
ug/L
0.50
1
10/20/16 04:07
67-66-3
Chloromethane
ND
ug/L
1.0
1
10/20/16 04:07
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
1
10/20/16 04:07
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
1
10/20/16 04:07
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
1
10/20/16 04:07
96-12-8
Dibromochloromethane
ND
ug/L
0.50
1
10/20/16 04:07
124-48-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
1
10/20/16 04:07
106-93-4
Dibromomethane
ND
ug/L
0.50
1
10/20/16 04:07
74-95-3
1,2 -Dichlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
0.50
1
10/20/16 04:07
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
1
10/20/16 04:07
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
1
10/20/16 04:07
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
1
10/20/16 04:07
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
1
10/20/16 04:07
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
0.50
1
10/20/16 04:07
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
1
10/20/16 04:07
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
1
10/20/16 04:07
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
1
10/20/16 04:07
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
1
10/20/16 04:07
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
1
10/20/16 04:07
563-58-6
cis- 1,3-Dichloropropene
ND
ug/L
0.50
1
10/20/16 04:07
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
0.50
1
10/20/16 04:07
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
1
10/20/16 04:07
108-20-3
Ethylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1
10/20/16 04:07
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
1
10/20/16 04:07
98-82-8
Methylene Chloride
ND
ug/L
2.0
1
10/20/16 04:07
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
1
10/20/16 04:07
1634-04-4
Naphthalene
ND
ug/L
2.0
1
10/20/16 04:07
91-20-3
n-Propylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
103-65-1
Styrene
ND
ug/L
0.50
1
10/20/16 04:07
100-42-5
REPORT
OF LABORATORY
ANALYSIS
This report shall not be
reproduced, except in full,
Date: 10/24/2016 12:50 PM
without the written consent of Pace Analytical Services, LLC.
Page 6 of 20

1�5a'neAnalyfical"
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I
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: JW Smith
Pace Project No.: 92315946
Sample: EFF Lab ID: 92315946002 Collected: 10/12/16 18:30 Received: 10/13/16 10:21 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 62006
1,1,1,2 -Tetrachloroethane
ND
ug/L
0.50
1
10/20/16 04:07
630-20-6
1,1,2,2 -Tetrachloroethane
ND
ug/L
0.50
1
10/20/16 04:07
79-34-5
Tetrachloroethene
ND
ug/L
0.50
1
10/20/16 04:07
127-18-4
Toluene
ND
ug/L
0.50
1
10/20/16 04:07
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
1
10/20/16 04:07
87-61-6
1,2,4-Tdchlorobenzene
ND
ug/L
2.0
1
10/20/16 04:07
120-82-1
1,1,1 -Trichloroethane
ND
ug/L
0.50
1
10/20/16 04:07
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
0.50
1
10/20/16 04:07
79-00-5
Trichloroethene
ND
ug/L
0.50
1
10/20/16 04:07
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
1
10/20/16 04:07
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
1
10/20/16 04:07
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
1
10/20/16 04:07
108-67-8
Vinyl chloride
ND
ug/L
1.0
1
10/20/16 04:07
75-01-4
m&p-Xylene
ND
ug/L
1.0
1
10/20/16 04:07
179601-23-1
o -Xylene
ND
ug/L,
0.50
1
10/20/16 04:07
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
93
%
70-130
1
10/20/16 04:07
17060-07-0
4-13romofluorobenzene (S)
95
%
70-130
1
10/20/16 04:07
460-00-4
Toluene -d8 (S)
101
%
70-130
1
10/20/16 04:07
2037-26-5
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
ND
mg/L
5.0
1
10/17/16 14:39
420.4 Phenolics, Total
Analytical Method: EPA420.4
Phenol
0.017
mg/L
0.010
1
10/21/1613:50
REPORT OF LABORATORY
ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM
without the written consent of Pace Analytical Services, LLC.
Page 7 of 20

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QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333151 Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET Filtered Diss.
Associated Lab Samples: 92315946001, 92315946002
METHOD BLANK: 1846102 Matrix: Water
Associated Lab Samples: 92315946001, 92315946002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Lead, Dissolved ug/L ND 5.0 10/21/16 11:20
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1846103
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Lead, Dissolved ug/L 500 482 96 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1846104 1846105
MS MSD
92315870003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Lead, Dissolved ug/L ND 500 500 450 453 i 90 91 75-125 1
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 20

1��alcieAnalj&cal'
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I
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333782
QC Batch Method: SM 6200B
Associated Lab Samples: 92315946001, 92315946002
Analysis Method:
Analysis Description:
SM 6200B
6200B MSV
METHOD BLANK: 1849729
Matrix: Water
Associated Lab Samples: 92315946001,
92315946002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
1,1,1,2 -Tetrachloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1,1 -Trichloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1,2,2 -Tetrachloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1,2 -Trichloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1-Dichloroethane
ug/L
ND
0.50
10/20/16 01:01
1,1-Dichloroethene
ug/L
ND
0.50
10/20/16 01:01
1,1-Dichloropropene
ug/L
ND
0.50
10/20/16 01:01
1,2,3-Trichlorobenzene
ug/L
ND
2.0
10/20/16 01:01
1,2,3-Trichloropropane
ug/L
ND
0.50
10/20/16 01:01
1,2,4-Trichlorobenzene
ug/L
ND
2.0
10/20/16 01:01
1,2,4-Trimethylbenzene
ug/L
ND
0.50
10/20/16 01:01
1,2-Dibromo-3-chloropropane
ug/L
ND
1.0
10/20/16 01:01
1,2-Dibromoethane (EDB)
ug/L
ND
0.50
10/20/16 01:01
1,2 -Dichlorobenzene
ug/L
ND
0.50
10/20/16 01:01
1,2-Dichloroethane
ug/L
ND
0.50
10/20/16 01:01
1,2-Dichloropropane
ug/L
ND
0.50
10/20/16 01:01
1,3,5-Trimethylbenzene
ug/L
ND
0.50
10/20/16 01:01
1,3 -Dichlorobenzene
ug/L
ND
0.50
10/20/16 01:01
1,3-Dichloropropane
ug/L
ND
0.50
10/20/16 01:01
1,4 -Dichlorobenzene
ug/L
ND
0.50
10/20/16 01:01
2,2-Dichloropropane
ug/L
ND
0.50
10/20/16 01:01
2-Chlorotoluene
ug/L
ND
0.50
10/20/16 01:01
4-Chlorotoluene
ug/L
ND
0.50
10/20/16 01:01
Benzene
ug/L
ND
0.50
10/20/16 01:01
Bromobenzene
ug/L
ND
0.50
10/20/16 01:01
Bromochloromethane
ug/L
ND
0.50
10/20/16 01:01
Bromodichloromethane
ug/L
ND
0.50
10/20/16 01:01
Bromoform
ug/L
ND
0.50
10/20/16 01:01
Bromomethane
ug/L
ND
5.0
10/20/16 01:01
Carbon tetrachloride
ug/L
ND
0.50
10/20/16 01:01
Chlorobenzene
ug/L
ND
0.50
10/20/16 01:01
Chloroethane
ug/L
ND
1.0
10/20/16 01:01
Chloroform
ug/L
ND
0.50
10/20/16 01:01
Chloromethane
ug/L
ND
1.0
10/20/16 01:01
cis-1,2-Dichloroethene
ug/L
ND
0.50
10/20/16 01:01
cis-1,3-Dichloropropene
ug/L
ND
0.50
10/20/16 01:01
Dibromochloromethane
ug/L
ND
0.50
10/20/16 01:01
Dibromomethane
ug/L
ND
0.50
10/20/16 01:01
Dichlorodifluoromethane
ug/L
ND
0.50
10/20/16 01:01
Diisopropyl ether
ug/L
ND
0.50
10/20/16 01:01
Ethylbenzene
ug/L
ND
0.50
10/20/16 01:01
Qualifiers
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20

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QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
METHOD BLANK: 1849729
Associated Lab Samples: 92315946001, 92315946002
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Hexachloro-1,3-butadiene
ug/L
ND
2.0
10/20/16 01:01
Isopropylbenzene (Cumene)
ug/L
ND
0.50
10/20/16 01:01
m&p-Xylene
ug/L
ND
1.0
10/20/16 01:01
Methyl-tert-butyl ether
ug/L
ND
0.50
10/20/16 01:01
Methylene Chloride
ug/L
ND
2.0
10/20/16 01:01
n-Butylbenzene
ug/L
ND
0.50
10/20/16 01:01
n-Propylbenzene
ug/L
ND
0.50
10/20/16 01:01
Naphthalene
ug/L
ND
2.0
10/20/16 01:01
o -Xylene
ug/L
ND
0.50
10/20/16 01:01
sec-Butylbenzene
ug/L
ND
0.50
10/20/16 01:01
Styrene
ug/L
ND
0.50
10/20/16 01:01
tert-Butylbenzene
ug/L
ND
0.50
10/20/16 01:01
Tetrachloroethene
ug/L
ND
0.50
10/20/16 01:01
Toluene
ug/L
ND
0.50
10/20/16 01:01
trans- 1,2-Dichloroethene
ug/L
ND
0.50
10/20/16 01:01
trans- 1,3-Dichloropropene
ug/L
ND
0.50
10/20/16 01:01
Trichloroethene
ug/L
ND
0.50
10/20/16 01:01
Trichlorofluoromethane
ug/L
ND
1.0
10/20/16 01:01
Vinyl chloride
ug/L
ND
1.0
10/20/16 01:01
1,2-Dichloroethane-d4 (S)
%
117
70-130
10/20/16 01:01
4-Bromofluorobenzene (S)
%
93
70-130
10/20/16 01:01
Toluene -d8 (S)
%
102
70-130
10/20/16 01:01
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1849730
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,1,1,2 -Tetrachloroethane
ug/L
50
48.6
97
60-140
1,1,1 -Trichloroethane
ug/L
50
53.8
108
60-140
1,1,2,2 -Tetrachloroethane
ug/L
50
45.4
91
60-140
1,1,2 -Trichloroethane
ug/L
50
49.3
99
60-140
1,1-Dichloroethane
ug/L
50
51.9
104
60-140
1,1-Dichloroethene
ug/L
50
59.3
119
60-140
1,1-Dichloropropene
ug/L
50
49.7
99
60-140
1,2,3-Trichlorobenzene
ug/L
50
45.7
91
60-140
1,2,3-Trichloropropane
ug/L
50
47.5
95
60-140
1,2,4-Trichlorobenzene
ug/L
50
47.0
94
60-140
1,2,4-Trimethylbenzene
ug/L
50
50.6
101
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
53.0
106
60-140
1,2-Dibromoethane (EDB)
ug/L
50
51.2
102
60-140
1,2 -Dichlorobenzene
ug/L
50
49.6
99
60-140
1,2-Dichloroethane
ug/L
50
47.7
95
60-140
1,2-Dichloropro pane
ug/L
50
48.7
97
60-140
1,3,5-Trimethylbenzene
ug/L
50
49.5
99
60-140
1,3 -Dichlorobenzene
ug/L
50
47.3
95
60-140
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 20

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1849730
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,3-Dichloropropane
ug/L
50
45.7
91
60-140
1,4 -Dichlorobenzene
ug/L
50
46.7
93
60-140
2,2-Dichloropropane
ug/L
50
48.7
97
60-140
2-Chlorotoluene
ug/L
50
50.5
101
60-140
4-Chlorotoluene
ug/L
50
49.7
99
60-140
Benzene
ug/L
50
49.2
98
60-140
Bromobenzene
ug/L
50
50.8
102
60-140
Bromochloromethane
ug/L
50
49.7
99
60-140
Bromodichloromethane
ug/L
50
51.2
102
60-140
Bromoform
ug/L
50
47.7
95
60-140
Bromomethane
ug/L
50
44.3
89
60-140
Carbon tetrachloride
ug/L
50
54.9
110
60-140
Chlorobenzene
ug/L
50
48.0
96
60-140
Chloroethane
ug/L
50
35.4
71
60-140
Chloroform
ug/L
50
49.5
99
60-140
Chloromethane
ug/L
50
62.7
125
60-140
cis-1,2-Dichloroethene
ug/L
50
55.1
110
60-140
cis-1,3-Dichloropropene
ug/L
50
48.7
97
60-140
Dibromochloromethane
ug/L
50
50.0
100
60-140
Dibromomethane
ug/L
50
43.8
88
60-140
Dichlorodifluoromethane
ug/L
50
60.5
121
60-140
Diisopropyl ether
ug/L
50
65.7
131
60-140
Ethylbenzene
ug/L
50
48.9
98
60-140
Hexachloro-1,3-butadiene
ug/L
50
46.5
93
60-140
Isopropylbenzene (Cumene)
ug/L
50
48.7
97
60-140
m&p-Xylene
ug/L
100
97.0
97
60-140
Methyl-tert-butyl ether
ug/L
50
56.4
113
60-140
Methylene Chloride
ug/L
50
56.0
112
60-140
n-Butylbenzene
ug/L
50
49.5
99
60-140
n-Propylbenzene
ug/L
50
47.7
95
60-140
Naphthalene
ug/L
50
49.7
'99
60-140
o -Xylene
ug/L
50
48.5
97
60-140
sec-Butylbenzene
ug/L
50
49.0
98
60-140
Styrene
ug/L
50
51.1
102
60-140
tert-Butyl benzene
ug/L
50
40.7
81
60-140
Tetrachloroethene
ug/L
50
44.2
88
60-140 CU
Toluene
ug/L
50
48.4
97
60-140
trans-1,2-Dichloroethene
ug/L
50
55.9
112
60-140
trans-1,3-Dichloropropene
ug/L
50
47.1
94
60-140
Trichloroethene
ug/L
50
47.2
94
60-140
Trichlorofluoromethane
ug/L
50
39.8
80
60-140
Vinyl chloride
ug/L
50
42.9
86
60-140
1,2-Dichloroethane-d4 (S)
%
106
70-130
4-Bromofluorobenzene (S)
%
98
70-130
Toluene -d8 (S)
%
102
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 20

aceAnalj4ical
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1
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LVC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1849731
MS
92316212007 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1849732
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
1,1,1,2 -Tetrachloroethane
ug/L
ND
20
20
20.3
20.1
102
101
60-140
1
1,1,1 -Trichloroethane
ug/L
ND
20
20
23.9
24.0
119
120
60-140
1
1,1,2,2 -Tetrachloroethane
ug/L
ND
20
20
19.9
19.1
100
95
60-140
4
1,1,2 -Trichloroethane
ug/L
ND
20
20
20.8
19.8
104
99
60-140
5
1,1-Dichloroethane
ug/L
ND
20
20
23.0
22.6
115
113
60-140
2
1,1-Dichloroethene
ug/L
ND
20
20
27.0
26.9
135
135
60-140
0
1,1-Dichloropropene
ug/L
ND
20
20
22.5
22.1
112
110
60-140
2
1,2,3-Trichlorobenzene
ug/L
ND
20
20
21.1
20.1
106
100
60-140
5
1,2,3-Trichloropropane
ug/L
ND
20
20
20.0
19.2
100
96
60-140
4
1,2,4-Trichlorobenzene
ug/L
ND
20
20
20.9
19.9
104
99
60-140
5
1,2,4-Trimethylbenzene
ug/L
ND
20
20
22.7
21.4
113
107
60-140
6
1,2-Dibromo-3-chloropropane
ug/L
ND
20
20
23.7
22.0
119
110
60-140
8
1,2-Dibromoethane (EDB)
ug/L
ND
20
20
21.8
21.0
109
105
60-140
4
1,2 -Dichlorobenzene
ug/L
ND
20
20
22.2
20.9
111
104
60-140
6
1,2-Dichloroethane
ug/L
ND
20
20
21.2
21.8
105
108
60-140
3
1,2-Dichloropropane
ug/L
ND
20
20
20.8
20.5
104
102
60-140
2
1,3,5-Trimethylbenzene
ug/L
ND
20
20
22.3
21.0
112
105
60-140
6
1,3 -Dichlorobenzene
ug/L
ND
20
20
21.1
19.8
106
99
60-140
6
1,3-Dichloropropane
ug/L
ND
20
20
19.7
18.8
98
94
60-140
5
1,4 -Dichlorobenzene
ug/L
ND
20
20
21.1
19.7
105
98
60-140
7
2,2-Dichloropropane
ug/L
ND
20
20
21.7
21.2
108
106
60-140
2
2-Chlorotoluene
ug/L
ND
20
20
23.0
21.6
115
108
60-140
6
4-Chlorotoluene
ug/L
ND
20
20
22.4
21.2
112
106
60-140
6
Benzene
ug/L
ND
20
20
21.4
20.7
107
103
60-140
4
Bromobenzene
ug/L
ND
20
20
22.7
21.1
113
105
60-140
7
Bromochloromethane
ug/L
ND
20
20
21.3
20.6
106
103
60-140
3
Bromodichloromethane
ug/L
ND
20
20
22.0
21.2
110
106
60-140
4
Bromoform
ug/L
ND
20
20
18.8
18.3
94
92
60-140
3
Bromomethane
ug/L
ND
20
20
21.1
21.9
106
109
60-140
4
Carbon tetrachloride
ug/L
ND
20
20
25.5
24.5
127
123
60-140
4
Chlorobenzene
ug/L
ND
20
20
21.2
20.5
106
103
60-140
3
Chloroethane
ug/L
ND
20
20
15.9
17.7
80
88
60-140
10
Chloroform
ug/L
ND
20
20
21.9
21.6
109
108
60-140
1
Chloromethane
ug/L
ND
20
20
27.5
29.2
136
145
60-140
6 M1
cis-1,2-Dichloroethene
ug/L
ND
20
20
24.1
23.9
120
120
60-140
1
cis- 1,3-Dichloropropene
ug/L
ND
20
20
20.3
19.7
102
98
60-140
3
Dibromochloromethane
ug/L
ND
20
20
21.1
20.3
105
101
60-140
4
Dibromomethane
ug/L
ND
20
20
18.7
18.0
93
90
60-140
4
Dichlorodifluoromethane
ug/L
ND
20
20
28.2
28.8
141
144
60-140
2 M1
Diisopropyl ether
ug/L
ND
20
20
27.5
27.0
137
135
60-140
2
Ethylbenzene
ug/L
ND
20
20
22.0
20.9
110
105
60-140
5
Hexachloro-1,3-butadiene
ug/L
ND
20
20
23.0
21.1
114
105
60-140
9
Isopropylbenzene (Cumene)
ug/L
ND
20
20
21.5
20.9
108
104
60-140
3
m&p-Xylene
ug/L
ND
40
40
43.6
42.0
109
105
60-140
4
Methyl-tert-butyl ether
ug/L
ND
20
20
24.2
23.6
120
117
60-140
3
Methylene Chloride
ug/L
ND
20
20
23.9
23.5
119
118
60-140
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 20
Pace Analytical Services, LLC
aceAnalytical ®
100
980�Hunte
sv Ile, NC1te
28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE:
1849731
1849732
MS
MSD
92316212007
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua]
n-Butylbenzene
ug/L
ND
20
20
23.1
21.5
116
108
60-140
7
n-Propylbenzene
ug/L
ND
20
20
22.0
20.7
110
104
60-140
6
Naphthalene
ug/L
ND
20
20
22.7
21.1
113
105
60-140
7
o -Xylene
ug/L
ND
20
20
21.1
20.4
106
102
60-140
4
sec-Butylbenzene
ug/L
ND
20
20
22.8
21.5
114
107
60-140
6
Styrene
ug/L
ND
20
20
21.5
21.1
107
105
60-140
2
tert-Butylbenzene
ug/L
ND
20
20
18.8
17.6
94
88
60-140
6
Tetrachloroethene
ug/L
ND
20
20
20.0
19.3
100
96
60-140
4
Toluene
ug/L
ND
20
20
21.5
20.9
108
105
60-140
3
trans- 1,2-Dichloroethene
ug/L
ND
20
20
25.2
24.4
126
122
60-140
3
trans-1,3-Dichloropropene
ug/L
ND
20
20
19.3
19.0
97
95
60-140
2
Trichloroethene
ug/L
ND
20
20
20.6
20.0
103
100
60-140
3
Trichlorofluoromethane
ug/L
ND
20
20
19.3
20.3
96
102
60-140
5
Vinyl chloride
ug/L
ND
20
20
21.6
21.8
108
109
60-140
1
1,2-Dichloroethane-d4 (S)
%
104
112
70-130
4-Bromofluorobenzene (S)
%
94
95
70-130
Toluene -d8 (S)
%
102
101
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 20
Pace Analytical Services, LLC
Mv
9800 Kincey Ave. Suite 100
a/ Iyfili
cal
Huntersville, NC 28078
www.pacelabs.com
[phone]
QUALITY CONTROL DATA
'Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333350
Analysis Method: SM 2540D
QC Batch Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Associated Lab Samples: 92315946001
METHOD BLANK: 1847344
Matrix: Water
Associated Lab Samples: 92315946001
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Suspended Solids
mg/L
ND 2.5 10/17/16 11:43
LABORATORY CONTROL SAMPLE: 1847345
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Suspended Solids
mg/L
250 240 96 90-110
SAMPLE DUPLICATE: 1847346
92315796001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
ND ND
SAMPLE DUPLICATE: 1847347
92315824001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Suspended Solids
mg/L
18.7 19.0 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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acmnaljftalo
www.pacelabs.com
Project: JW Smith
Pace Project No.: 92315946
QC Batch: 333411
QC Batch Method: SM 2540D
Associated Lab Samples: 92315946002
METHOD BLANK: 1847742
Dup
Associated Lab Samples: 92315946002
Units
Parameter
Units
Total Suspended Solids
mg/L
ND
LABORATORY CONTROL SAMPLE: 1847743
Parameter
Units
Total Suspended Solids
mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Analysis Method: SM 2540D
Analysis Description: 2540D Total Suspended Solids
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.5 10/17/1614:39
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
250 230 92 90-110
SAMPLE DUPLICATE: 1847744
92315946002
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
SAMPLE DUPLICATE: 1847745
92315996001
Dup
Parameter
Units
Result
Result RPD Qualifiers
Total Suspended Solids
mg/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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1�l5aceAnalyfical"
( www.pacelabs.com
I
QUALITY CONTROL DATA
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QC Batch: 333927
Analysis Method: EPA 420.4
QC Batch Method: EPA 420.4
Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92315946001, 92315946002
METHOD BLANK: 1850808
Matrix: Water
Associated Lab Samples: 92315946001, 92315946002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Phenol mg/L
ND 0.010
10/21/1613:26
LABORATORY CONTROL SAMPLE: 1850809
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Phenol mg/L
.05
0.050
101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1850810
1850811
MS
MSD
92315167005
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Phenol mg/L 175
.05
.05 0.16
0.16 -31 -37
90-110
2 M1
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1850812
1850813
MS
MSD
92315180001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Phenol mg/L 0.017
.05
.05 0.064
0.064 94 93
90-110
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/24/2016 12:50 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 20

lacmnalytical"
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QUALIFIERS
Project: JW Smith
Pace Project No.: 92315946
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
C9 Common Laboratory Contaminant.
CU The continuing calibration for this compound is outside of Pace Analytical acceptance limits. Analyte presence below
reporting limits in associated samples. Results unaffected by high bias.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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1�55'neAnalyfical'
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I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: JW Smith
Pace Project No.: 92315946
Pace Analytical Services, LLt;
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Date: 10/24/2016 12:50 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 18 of 20
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch Analytical Method
Batch
92315946001
INF
EPA 3010
333151 EPA 6010
333298
92315946002
EFF
EPA 3010
333151 EPA 6010
333298
92315946001
INF
SM 6200B
333782
92315946002
EFF
SM 6200B
333782
92315946001
INF
SM 2540D
333350
92315946002
EFF
SM 2540D
333411
92315946001
INF
EPA 420.4
333927
92315946002
EFF
EPA 420.4
333927
Date: 10/24/2016 12:50 PM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
Page 18 of 20

_ 2eAnalytical'
Document Name:
Sample Condition Upon Receipt(SCUR)
Document. Revised: Sept. 21, 2016
Page 1 oft
Document No.:
F-CAR-CS-033-Rev.00
Issuing Authority:
Pace Quality Office
�- Page 2 of 2 for Internal Use ONLY
Client Name: PP' Project #: Flo 9 1
-5946
Courier: ❑Fed Ex []UPS [-]USPS ❑Client
❑ Commercial Pace ❑other:
y Seal Present? ❑ 92386946
Custody Yes I4�wNo Seals Intact? ❑Yes WNci
Date/Initials Person Examining Contents:ALI' N36 -
Packing
Packing Material: ❑Bubble Wrap NBubble Bags ❑None ❑Other:
Thermometer:f (Wet ❑Blue
❑ IR Gun ID: �5 Type of Ice: R6 r
Correction Factor: Cooler Temp Corrected (°C): e 3.6
Temp should be above freezing to 6`C
USDA Regulated Soil ( ❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC (check maps)?
r -1V . 1711,1
[]None []Samples on ice, cooling process has begun
Biological Tissue. Frozen? ❑Yes [PNo ❑N/A
Did samples originate from a foreign source (Internationally,
includine Hawaii and Puerto Rico)? Dyes ®No
CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes [:]No
Person Contacted: Date/Time:
Comments/Sample
Discrepancy:
Project Manager SCURF Review: N �(Kn .l1, Date:
: I
Project Manager SRF ReviewV V ° - Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ HuntersvilleRaleigh❑ Mechanicsville❑
Page 19 of 20
Comments/Discrepancy:
Chain of Custody Present?
MYes
ONO
❑N/A
1.
Samples Arrived within Hold Time?
liyes
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
[]Yes
®No
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
, No
❑N/A
4.
Sufficient Volume?
Yes
❑No
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
P)Yes
MYes
[]No
❑No
[]N/A
❑N/A
6.
Containers intact?
, Yes
[]No
❑N/A
7.
Samples Field Filtered?
❑Yes
jANo
❑N/A
8. Note if sediment is visible in the dissolved container
Sample Labels Match COC?
-Includes Date/Time'/ID/Analysis Matrix:
".�^` pyes
Gt r
❑No
❑N/A
9;
Ali containers needing acid/base preservation have been
checked and documented on page two of SCURF? )Yes
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015
(water) DOC, LLHg
Samples checked for dechlorination? []Yes
❑No
No
❑N/A
❑N/A
10.
11.
Headspace in VOA Vials (>5-6mm)?
❑Yes
WNo
[]N/A
12.
Trip Blank Present?
Trip Blank Custody Seals Present?
Pace Trip Blank Lot # (if purchased):
❑Yes
❑Yes
[PNo
PO No
❑N/A
❑N/A
13.
CLIENT NOTIFICATION/RESOLUTION Field Data Required? ❑Yes [:]No
Person Contacted: Date/Time:
Comments/Sample
Discrepancy:
Project Manager SCURF Review: N �(Kn .l1, Date:
: I
Project Manager SRF ReviewV V ° - Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ HuntersvilleRaleigh❑ Mechanicsville❑
Page 19 of 20

PaceAnalytical-
CHAIN-OF-CUSTODY / Analytical Request Document
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
n Y+ VY
Section A Section B Section C
Page. % ofCN
(D
Required Client Information: Required Project Information: Invoice Information:
Report To: /7rAttention:
2042705Company:rn•
mai.
Address: C r Copy To: Company Name:
3 — ry J ; r
REGULATORY AGENCY
�-�
i + Address:
NPDES F GROUND WATER f- DRINKING WATER
F UST I- RCRA ? OTHER
Email Tei �. t Purchase Order No.: , Pace Ouote
Reference:
Pro1ect Name:
Poner LI f Peror. o
Site Locationtana
STATE:
r
Requested Dueate AT: ••� �' q� 1 Project Number. ^�
'r t'� i n Pace Profile a:
-t^fJ• �
Requested
Analysis
Filtered
(Y/N)
Section D Matrix Codes
c^z
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Roqutred ClientInformition MATRIX r Coos
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:
.COLLECTED
Preservatives
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Drinking Water DW
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Water WT
Waste Water WW
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COMPOSITE
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DATE TIME
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ADDITIONAL COMMENTS
RELINQUISHED BY l AFFILIATION
DATE
TIME ACCEPTED BY I AFFILIATION
DATE
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SAMPLE CONDITIONS
ORIGINAL
SAMPLERNAMEAND SIGNATURE
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PRINT Name of SAMPLER, p • i '" /
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'Imponunt Note: By signing this form you are accepting Paces NET 30 daypaymert terms and amecing to late charges of 1.5% per month for any invoices not'Yaid wilhin 30 days, F-ALL-0-020rev.07, 15 -May -2007

Plan Prepared by:
Mika Trifunovic
Project Engineer
Residuals Management Plan
J.W. Smith / Camp Springs 76
Groundwater Remediation System
8920 Cherry Grove Road
Reidsville, Caswell County, NC
NPDES Permit # NCO088692
NCDEQ Incident # 21685
Prepared for:
Sparks Oil Company
412 N. Scales Street
Reidsville, NC 27320
Plan Reviewed by:
MichaeltMan
Operatioer
Pyramid Environmental & Engineering, P.C.
P.O. Box 16265
503 Industrial Ave.
Greensboro, NC 27416-0265

Residuals Collection, Handling, Processing, Storage & Disposal
As requested by the Construction Grants and Loans Section of Division of Water Quality of
North Carolina Department of Environmental Quality (NCDEQ), collection, handling,
processing, storage and disposal of residuals generated in the product storage drum, oil water
separator (OWS), bag filter, aggregate filter, carbon vessels, ion exchange vessels, and backwash
filter are addressed in this plan.
Oil Water Separator and Product Storage Drum
Free product from the OWS discharges by gravity to a 65 gallon polyethylene product storage
drum installed outside of the system building. The product storage drum is equipped with a high-
level switch to shut down operation of the remediation system. Residuals from the OWS and
product storage drum are collected and handled by a contractor in accordance with all applicable
regulations on an as needed basis. After the collection of the residuals, the contractor
immediately hauls the residuals off the site. The contractor is also responsible for the proper
disposal or storage/processing of residuals.
Bag Filter
The bag filter is changed every month during scheduled monthly maintenance events. The used
bag filters are removed from the bag filter housing using disposable gloves and placed in a sealed
plastic container. The used bags are immediately shipped as a non -hazardous waste for proper
disposal. Pyramid is responsible for the collection, handling, and disposal of used bag filters.
Aggregate Filter and Carbon Vessels
The aggregate filter and carbon vessels are exchanged every six months by a contractor in
accordance with all applicable regulation. Used aggregate filter and carbon vessels are
immediately hauled off the site. The contractor is responsible for the residuals handling and
proper disposal or storage/processing.
Ion Exchange Vessels
Two ion exchange vessels were replaced with carbon vessels in May 2012. The NCDEQ
approved this change, however the number of carbon vessels has never been changed in the
current NPDES permit that expires on May 31, 2017. Please see the enclosed correspondence
between Pyramid and NCDEQ.
Backwash Filter
The used backwash filter media is collected and handled by a contractor in accordance with all
applicable regulations on an as needed basis. After the collection of the used media, the
contractor immediately removes the filter media from the site for processing and/or disposal. The
contractor is also responsible for proper disposal or storage/processing of the used media.
Camp Springs 76/JW Smith — Residuals Management Plan 1

Mika Trifunovic
From: Mika Trifunovic <[e-mail]>
Sent: Wednesday, June 20, 2012 11:38 AM
To: 'Bob Guerra ([e-mail])'
Cc: Mike Jones ([e-mail])
Subject: 1W Smith/Camp Springs 76 NPDES Permit # NCO088692
Good morning Bob,
I have just received the referenced NPDES permit form our client and I've noticed that the Supplement to Permit Cover
Sheet (attached as a PDF file) contains an incorrect number of carbon vessels.
There should be four (4 ) carbon vessels listed on the sheet because two (2) ion exchange vessels have been converted
to carbon vessels. Please see the forwarded emails.
Could you please email me the NPDES permit with the correct number of carbon vessels.
Thank you.
Mika
From: Guerra, Bob [mailto:[e-mail]]
Sent: Wednesday, March 14, 2012 1:26 PM
To: Mika Trifunovic
Subject: RE: Modification of JW Smith/Camp Springs 76 Remediation System
I will be including this request and incorporate the changes into your permit when I issue it.
From: Mika Trifunovic rma i Ito: mika Oboyra midenvironmental.com]
Sent: Wednesday, March 14, 2012 12:12 PM
To: Corporon, Joe; Guerra, Bob
Subject: Modification of JW Smith/Camp Springs 76 Remediation System
Good afternoon Joe and Bob,
As I mentioned during our conversation, we have intent to modify the JW Smith/Camp Springs 76 petroleum
contaminated groundwater remediation system which holds the NPDES Individual Permit # NC0088692.
The modification will include. conversion of two existing ion exchange vessels into carbon filter vessels. Detailed
information about the modification is provided in the attached PDF file.
Please let me know if you need any additional information or clarification.
Since the permit is currently being renewed, I would like to ask you to include this proposed modification into the
permit.
Thank you.
Mika Trifunovic
Project Manager
Pyramid Environmental & Engineering

I P
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JW Smith/Camp Springs 76 Petroleum Contaminated Groundwater
Remediation System - NPDES Permit # NCO088692
SEAL
5 000
AIR STRIPPER
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0 6 GPM `��� VENT TO Shallow Tray
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Flow Rate; 2-115 GPM
NOTE: This sump may be Nr Flow: Min, 600 CEM
integrated in the —�
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into carbon filter vessels.
Conversion process:
(2) Berkely BVM SS Multi Stage - vacuum ion exchange media from the vessels{
1 HP Centrifugal Pumps
- rinse empty vessels
- haul the ion exchange media and rinse water z{
off site for proper disposal
I LEVEL FLO - fill the vessels with virgin carbon }{
PUMP ON
[ There will be no backwash of the carbon
_ _ J filter vessels. {�
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and 320 -gallon tank will be removed. �{
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AGGREGATE CARBON CARBON 5 =�
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