WQ0000485_Monitoring - 11-2016_20161230 (2)

Nor
VALLEY PROTEINS , INC.
December 28, 2016
Division of Water Quality
Atten: Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Valley Proteins, Inc. — Rose Hill Division
Permit Number: WQ0000485
Dear Sir;
DEQ 3 0
70 vojv
Please find enclosed the Wastewater Residual Monitoring Wells Report for our
Rose Hill, NC division for the third reporting period of 2016.
If you require any additional information or wish to discuss the matter, please feel
free to call me at [phone] ext. 25110
Sincerely,
3z"� �d4vtD
Steve Lester
General Manager
cc: Corp Office
Malting a Sustainable Difference.
DEC 3 0 2016
PO Box 1026
469 Yellow Cut Road
Rose Hill, NC 28458
O 910.289.2083
0 866.936.0740
valleyproteins.com

GLV -59A COMPLIANCE REPORT' FORM Permit # W00000485
(Suhmit ane each auneilnring period frith GIP 59 fiuuu.)
)
Enter date monitoring results were due. (12131116 ) Will this monitoring report (GW -59 and GW -59A)
NO
be submitted after the established due date?
Z
Was any required information missing on the GW -59 report forms?
NO
IF the answer to question 1 or 2 is "YES', list in the space provided below the well identification number(s) and explain the
problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing identification
NO
plate, area overgrown, etc.)'. f f the answer is "Yes ", contact Me Regional Q(hce ar gi icko-
4
Are any monitored constituents equal to or above the established standards?
YES
If the answer to question 4 is "NO'; skip to section 8.
U the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding
standards in the space provided below., MW 1 pH 5.4, MW 7A pH 5.0, MW 8A pH 5.5, MW 9 pH 6. 0, MW 9 TOC 34.3, MW
10A pH 5.50, MW 10A TDS 616, MW 11A pH 5.6, MW 1 1 TDS 944, MW 12B pH 5.2, MW 12B TDS 758, MW 13A pH 6.4,
MW 14A pH 5.5, MW 14A TDS 778
5
For the constituents identified in question 4 above, have standards been exceeded previously for the same
YES
constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO'; skip to section B.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards,
concentration(s) reported, and sample collection dale for each occurrence (for the last two years). SEE ATTACHED
GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
G
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the
Regional Office.
7
is the permittee implementing previously approved actions required by the Division involving this groundwater quality
YES
problem?
If the answer to question 7 is "YES" describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
Additional monitoring was performed to identify constituents of TOC in MW No.g. The facility has been
communicating with Mr. Geoff Kegley in the Wilmington Regional Office.
8
The person completing this portion (GW -59A) of the monitoring report should sign below and submit this form with
GW -59 forms for required wells to the address provided at the top of the current GW -59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this report
(Compliance Repo GW -59A) is true and complete to the best of my knowledge.
1
Signature of Permittee (or Authorized Agent) Date
GW -59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
�.� DEPARTISION OF_ V1RQNMENT S NATURAL RESOURCES "• _.
• •
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
mg/L Effluent Total virus:
ty« vvL. M2111luvar/0
Steve Lester General Manager
(or Authorized Agent) Name and Title -1 Please print or type ) Signature of Permittee (or Authorized Agent) (Date)
GW -59 Rev. 812013 l
DEPARTMENT OF EN
GROUNDWATER QUALITY MONITORING:
WATER RESOURCES INFORMATIQN PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAILS ERVICI~.CENTEK, kA1 E1GK, Nd127699 1697 ' Phone: 919-807-&306
FACILITY INFORMATION.
Please Print Clearly orpe
PERMIT Number: WQ0000485 Expiration Date: 10/31/2019
Facility Name:
Valle Proteins Inc.lRose
Hill
Non -Discharge UIC
Permit Name (if different):
NPDES Other
Rd.
Facility Address: 469 Yellow Cu
TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill. NC 28458
County Duplin
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
(City) (State) i7jPi
Contact Person: William Gerrell
Telephone#: (91 O) 214-9024
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
l
from Permit
if WELL
SAMPLING INFORMATION
WAS
WELL ID NUMBER (from Permit): MW -1
Date sample collected: 11/9/2016
_ FIELD ANALYSES:
Well Depth: 12.46 ft.
Well Diameter: 2 in.
pH 00400: 5.40 units Temp. 000lo: 49 °C
DRY at
time of
Depth to Water Level 82546: 6.0
Screened Interval: 12.46 ft. to 2.46 ft. Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 1.17 ft. above land surface
Relative M.P. Elevation; ft,
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
4.9
gallons
Appearance
here:❑
Samples for metals were collected unfiltered:
X YES ❑ NO
i and field acidified: X YES ❑ NO
LABORATORY INFORMATION
I
Date sample analyzed: 1.119/16 - 11/22/16
(Laboratory Name: Microbac Fayetteville Division Certification No. DWQ411
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite
(NO2) as N 00615
rng/L Pb - Lead o1o51 ug/L
Coliform. --MF Fecal 31616 <1
/100mL
Nitrate
(NO3) as N 00620 <0.05
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/1OOmL
Phosphor
s: Total as P 00665 <0.050
mg/L
(Note: Use MPN method for highly turbid samples)
O
hophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 126
mg/L
t i -Aluminum 01105
mg/L Sodium 6.87 mg/L
pH (Lab) 00403 5.40
units
E Ba - Barium 01007
ug1L
TOC omao 4.26
Trig/L
lCa - Calcium oo916
mg/L
Chloride 00940 2.76
mg/L
Gd
- Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium:
Total 01034
ug/L
Grease and Oils 00552
mg/L
, Cu - Copper o1o42
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 19
mg%L
Hg - Mercury 71900
ug/L Lab Report Attached? [] Yes (0) El No (0)
pecific Conductance 000mµMhos
i
VOC 78732: # SW8260B
0.100
Total Ammonia o0610<0.100
mg/L
M g.
�-Potassiumg
Magnesium 00927
mg/L method #
(Ammonia. Nitrogen: NH3as N; Ammonia Nitrogen, Total)
Mn
l_ Manganese of o55
ug/L method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:
mg/L Effluent Total virus:
ty« vvL. M2111luvar/0
Steve Lester General Manager
(or Authorized Agent) Name and Title -1 Please print or type ) Signature of Permittee (or Authorized Agent) (Date)
GW -59 Rev. 812013 l

CI IRMIT PnpKfi nimyr-I 1-rwi PAPER t'MNl Y
For Remediation Systems Only (Attach Lab Reports): Influerl Total VOCs
Steve Lester
GW -59 Rev. 812013
mg/L trfluent rota) vvus.
(or
11'lylL V V%, r%ei116val /D
• •
•
DEPARTMENT OF,ENWIRQNMENT 81 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING;
DIVISION OF WATER RESOURCES ,INFORMATION PROCESSING;UNIT
COMPLIANCE REPORT FORM
COMPLIANCE
I
• •
•
19.807-6306 ;' • ,
tS1;7 MAIL SERVICE CENTER, RALEIGH; NC 27699 1617 -Phone; 919.807-6530&-
FACILITY INFORMATION
Please Print Cfeadyol,T)
pe
PERMIT Number: WQ0000485 Expiratl'z-Date: 10/3112019
Facility Name:
Valley Proteins Inc.-
Rose Hill-
Non -Discharge UIC
Permit Name (if different):
NPDES Other
Rd.
Facility Address:469
Yellow Cut
TYPE OF PERMITTED OPERATION BEING MONITORED
County Duplin
Rose Hill, NC 28458
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray field ❑ Remediation:,
(city) (szte> (zip)
Contact. Person: William GerrellTelephone#:
[phone]
❑ Rotary, Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat. Pump ❑ Other:
from Permit
if WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW -2
i Date sample collected: 11/9/2016
FIELD ANALYSES:
WAS
Well Depth: 31;00 ft.
Well Diameter: 2 in,
o
pH 00400: 6.70 units Temp. 000io: 's C
DRY at
time
Depth to Water Level 8254.6: 22.0 ft. below measuring point
p 9 P
Screened Interval: 30.15 ft. to 20.15 ft, Spec. Cond. 00094; µMhos
li
sampling,
Measuring Point is 3 ft. above land surface:
Relative M.P. Elevation: ft.
Odor ooam: a
check
Volume of water um ed/balled before sampling:
P P P g:
4.4
gallo
s
Clear
Appearance ar
here:
Samples formetalswere collected unfiltered:
X YES ❑ NO
and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: 11/9/16 -11/22/16
Laboratory Name: Microbac Fayetteville Division Certification No., DW4#11
PARAMETERS NOTE: Values should reflect
dissolved and colloidal
concentrations.
COD oo335
mg/L
Nitri
a (NO2) as N 00615
mg/L Pb - Lead oimi ug/L
Coliform: ;MF Fecal 31sls <1
_ /100mL
Nitrate
(NO3) as N 00620 0.413
mg/L Zn - Zinc 01092 mg/L
Coliform: MFTotal 315o4
/100mL
Phosphorus:
Total as P oosss <0.050
mg/L
(Note: use MPN method for highly turbld samples)
Or!bophosphate
70507
mg/L Other (Specify Compounds and Concentration 'Units):
issolved Solids: Total 70300 346
mg/L
Al
- Aluminum ol105 _
mg/L Sodium 21.7 mg/L
PH (Lab) 00403 6.70
units
Barium 01007
ug/L
TOC oomo 6.85
m 9/L
Ca Calcium 00916
mg/L
Chloride 00940 8.92
mg/L
Cid
- Cadmium 01027 _ _ _
ug/L
Arsenic 01002
ug/L
Ch
omium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
wglL
Fe -Iron 01 045
(Specify . ATTACH LAB REPORT,)
ug/L (Spec test and ..method #
Sulfate 00945 3.2
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
- Potassium 00937
mg/L VOC 78732: , method # SW8260B
Total Ammonia oo610 X0,100
mg/L
Mgt-
Magnesium oo927 _
mg/L method #
(Ammonia Nitrogen; NH3as_N; Ammonia Nitrogen, Total)
Mn
I Manganese o1D55
ug/L method #
TKN as N oo625
mg/L
Ni - Nickel' 0:1067
ug/L method
For Remediation Systems Only (Attach Lab Reports): Influerl Total VOCs
Steve Lester
GW -59 Rev. 812013
mg/L trfluent rota) vvus.
(or
11'lylL V V%, r%ei116val /D

SUBMIT FORM ON YELLOW PAPER ONLY
Steve Lester General Manager ! L4 a_41�
(or Authorized Agent)'Name and Title - Please Print or type I Signature of Permittee (or Authorized Aqent) (Date)
GW -59 Rev. 8/2013
7
DERARTMENT OF ENVIRONMENT &.NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
'
DIVISION OF WATER'RESOURCES INFORMATION PROCESSING. UNIT
COMPLIANCE REPORT FORM
a
1617 MAIL SERVICE CENTER; RALEIGH, NC2769P;116147' Phonec'91"07-6306.
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: WQ0000485 Expiration Date. 10/31/2019
Facility Name: Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
Permit Name (if different):
NPDES Other
Facility Address: 469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
Rose rtu NC 28458
; County Duplin
❑ Lagoon ❑ Remediation: Infiltration Gallery
(city) (State) (zip)
X Spray Field ❑ Remediation:
Contact Person: William Gerrell
I
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
ElWater Source Heat Pump ElOther:
from Permit
If WELL
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): MW -4
Date sample collected: 11/9/2016
FIELD ANALYSES: WAS
Well Depth: 28.93 'ft.
I Well Diameter: 2 in,
RY at
pH 00400: 6.90 units Temp. 000lo: 70 or Dme of
Depth to Water Level 82545 `6.7 ft. below measuring point Screened Interval: 28.93 ft. to 18.93
ft. Spec. Cond. 00094: µMhos
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
None
Odor 000a5 check
Volume of water pumped/bailed before sampling: 11.0
gallon's
Appearance Clear here:.❑
Samples for metals were collected unfiltered: X YES ❑ NO rand field acidified: X YES ❑ NO
LABORATORY INFORMATION_
Date sample analyzed: 11/9/16 -11/22/16
Laboratory Name;_ Microbac Fayetteville Division Certification No, D1NQ#11
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD oo335 mg1L
Nitrite (NO2) as N o0615
mg/L Pb - Lead 01051 ug1L
Coliform: MF Fecal 31616 <1 /100mL
Nitrate (NO3) as N 00620 <0.050
mg/L Zn - Zinc 01092 mg/L
Coliform:.MF Total 31504 /100mL
Phosphorus: Total as P oo665 <0.050
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids.Totai 70300 212 mg/L
al - Aluminum 01105
mg/L Sodium 9.42 mg/L
pH (Lab) 00403 6.90 units
I Ba -Barium 01007
ug/L
TOC oo680 5.80 mg/L
a - Calcium 00916
mg/L
Chloride 00940 3.39 mg/L
Cd - Cadmium 01027
ug1L
-
Arsenic o1002 ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552 mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730 ug1L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <0.25 mg/L
,Hg - Mercury 71900
ug1L Lab Report Attached? ❑ Yes (0) ❑ No (0)
pecific Conductance 00095 µMhos
{ - Potassium 00937
mg/L VOC 78732. method # SW8260B
Total Ammonia oo610 <0.100 mg/L
Mg Magnesium oo927 -
mg/L method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn ! Manganese o1o55
ug/L ; method #
TKN as N 00525 mg/L
Ni - Nickel 01067
ug1L method #
For Remediation Systems Only (Attach Lab Reports):
InfiuentlTotal VOCs: mg/L
Effluent Total VOCs: mg/L VOC Removal%
Steve Lester General Manager ! L4 a_41�
(or Authorized Agent)'Name and Title - Please Print or type I Signature of Permittee (or Authorized Aqent) (Date)
GW -59 Rev. 8/2013

NDWATER QUALITY MONITORING-
LIANCE REPORT FORM
ty Name:
it Name (if
(y Address:
(City)
act Person: William
Location/Site Name:
LID NUMBER (from Permit): MW 7A
Depth: 16 ft.
to Water Level 62546: 7.0 ft. below measuring point
wring Point is 2.42 ft. above land surface
ne of water pumped/bailed before sampling: 4.4
ales for metals were collected unfiltered: X YES ❑
Date sample analyzed:
1119116 -
11/22116_
PARAMETERS NOTE: Values should reflect dissolved and
COD 00335
Sodium 88.7 mg/L
mg/L
Coliform: MF Fecal 31616
<1
/100mL
Coliform: MF Total 31504
/100mL Pho
.(Note. Use MPN method for highly turbid samples)
Dissolved Solids:Total 70300
386
mg/L
pH (Lab) 00403
5.00
units
TOC oo68o
5.4
mg/L
Chloride 00940
33.4
mg/L
Arsenic 01002
mg/L
ug1L
Grease and Oils 00552
mg/L
mg/L
Phenol 32730
ug/L
uglL
Sulfate 00945
7.6
mg/L
Specific Conductance 00095
uMhos
Total Ammonia oo610
<0.100
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
TKN as N 00625
mg1L
Only
99-1617 Phbne;'919.807-6306 , _
Lose Hill Non -Discharge UIC
NPDES Other
Rd. TYPE OF PERMITTED OPERATION BEING MONITORED
County Duplin ❑ ,Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
No. of wells to be sampled: 11 ❑ 'Water Source Heat Pump []Other:
(from Permit)
Date sample collected: 11/9/201,6 FIELD ANALYSES: WAS
Well Diameter: 2 in. pH 00400: 5.00 units Temp. 000lo: 19 °C DRY at
Screened Interval: 16 ft. to 6 ft. Spec.. Cond. 00094: uMhos time of
Relative M.P. Elevation: ft. Odor 00085 None sampling,
s Appearance Clear checlF--t
and field acidified: X YES ❑ NO here: _J
Laboratory Name: Microbac Fayetteville Division
Idal concentrations.
:e (NO,) as N oo615 mg/L Pb - Lead oio51
3 (NO3) as N 00620 <0.05 mg/L Zn - Zinc 01092
is: Total as P 00665 <0.05 mg/L
Certification No. DWQ#11
ug/L
mg/L
hophosphate 70507 _
mg/L
Other (Specify Compounds and Concentration Units):
kI - Aluminum o1105
mg/L
Sodium 88.7 mg/L
Ba - Barium 01007
ug/L
Ca - Calcium 00916
mg/L
d - Cadmium 01027
ug/L
omium: Total 01034
ug/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Fe = Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT:)
Hg - Mercury 71900
ug/L
Lab Report Attached? []Yes (0) ❑ No (0)
C - Potassium 00937
mg/L
VOC 78732: method # SW8260B
- Magnesium 00927
mg/L
method #
- Manganese olo55
ug/L
method #
Ni - Nickel 01067
ug/L
method #
(or Authorized Agent) Name and Title - Please print or type I Signature of Permittee (or
mg1L

DEPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES
ROUNC)WATER QUALITY MONITORING'
DIVISION OF W11TR RESOURCES INFORMA710N PROCESSfNG UNIT
ONIPLIANCE REPORT FORMi 1617 MAILS RVICECENTER, RALEIGH NC 27699 1617 ';Phone. 91s 867-630G
„.��__. .n/nnnnnA4G cvr lra� nn rh4c 1()/3117(119
1-AVILII i nirVRIyIN.11yyj -' - '
Facility Name: Valley Proteins Inc.
Permit Name (if different)` ?
Facility Address: 469 Yellow Cuf
Rose Hilt. NC 28458 I
Rose Hill _
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Rota
ot rr Distributor ❑ Land Application of Sludge
❑ Rotary
Source Heat Pump [] Other:
_
FIELD ANALYSES:
19
Rd.
County Duplin
Tele hone#: 910 214=9024
- (
No. of wells to be sampled: 11
.(from Permit)
(cnyl estate) tzipi
ContactWilliam Gerrell
Well L ocation/S9te Name I
I LII`lu wAry RItlIN 1'IVIY
L ID NUMBER (from Permit): MW -8A
Microbac Fayetteville. Division
Date sample collected: 11/9/2016
FIELD ANALYSES:
19
Coliform: MF Fecal 3M6,
WAS
Depth: 16 ft.
E
Well Diameter: 2 in.
pH 00400: 5.50 units Temp. 000io: °C
/100ml-
DRY at
h to Water Level az546: 8.0 ft. below measuring point
`,
Screened Interval: 16 ft. to �6 ft.
i
Spec. Cond. 00094: WMhos
118
of
time li
sampling,
curing Point is 2.5 ft. above land surface
pH (Lab) 00403
Relative M.P. Elevation. ft:
Odor 00085: None
Clear
checl
ne iof water pumped/bailed before sampling: 3.9
gallons
I
..._ . ....�. r , .,
Appearance
5.6
harp
Date sample analyzed: 11/9/16 11/22/16
PARAMETERS NOTE: Values should reflect dissolved and col
COD oo33,5
Microbac Fayetteville. Division
mg/L
Nil
Coliform: MF Fecal 3M6,
6
/100mL
Nitn
Coliform: MF Total 31504
0.459 mg/L
/100ml-
Phosphc
(Note Use MPN method for highly turbid samples)
-thophosphate 70507
Dissolved Solids:Total 79300
118
mg/L
mg/L
pH (Lab) 00403
5.50
units
TOC 00680
2.93
mg/L
?.d - Cadmium 01027 _
Chloride 00940
5.6
mg/L
ug/L
Arsenic 01002
Cu - Copper 01042
ug/L
C
Grease and Oils 00552
ug/L
mg/L
Hg - Mercury 71900
Phenol 32730
Lab Report Atta
ug/L
mg/L
Sulfate 00945
35
mg/L
Specific Conductance.00095
ug/L
µMhos
Ni - Nickel 01067
Total Ammonia 00610
<0.100
mg/L
N
(Ammonia Nitrogen; NH3 as N; Ammonia
Nitrogen•Total).
IV
TKN' as N 00625
mg/L
and Title-
Laboratory Name:
Microbac Fayetteville. Division
3idal concentrations.
ite (NO2) as N 9os15
mg/L
Pb - Lead o1o51
to (NO3) as N 00620
0.459 mg/L
Zn - Zinc 01092
'us: Total as P 00665
<0.050 mg1L
-thophosphate 70507
mg/L
Other (Specify
Al -Aluminum ol105
mg/L
Ba - Barium 01007
ug/L
Ca - Calcium 00916
mg/L
?.d - Cadmium 01027 _
_ ug/L
iromium: Total 01034
ug/L
Cu - Copper 01042
mg/L
ORGANICS,
Fe - Iron 01045
ug/L
(Specify test a
Hg - Mercury 71900
ug/L
Lab Report Atta
K - Potassium 00937
mg/L
VOC 78732:
d - Magnesium 00927
mg/L
I - Manganese 01055
ug/L
Ni - Nickel 01067
ug/L
Certification No. DWQ#11
ug/L
mg/L
Compounds and Concentration Units):
Sodium 4.12 mg/L
by GC, GC/MS, HPLC)
nd method #. ATTACH LAB REPORT.)
ched? E] Yes (0) ❑ No (0)
method # SW8260B
method #
method #
method #

DEPARTMENT' ENVIRONMENT-& NATUPAL'RESOURCES
GROUNDWATER QUALITY MONITORING:
�'
DIVISIONOFWATER RESOURCES=,INFORMATIONPRO.CESSINGPNIT '
COMPLIANCE REPORT FORM
1817 -MAIL SERVICE CENTER,'RALEI611­11, NC 27699.1697 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or
PERMIT Number: W00000485 Expiration Date: 10/31/2019
Facility Name:
Valley Proteins Inc;
Rose_ Hill
Non -Discharge UIC
Permit Name (if different): I
NPDES Other
_
Facility Address:
469 Yellow C't
Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill. NC 28458
County Duplin _ _
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
(city) (state) (zip) !
Contact Person: William G_ errell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
-
—
_
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
-
-
(from Permit)
SAMPLING INFORMATION
J
If WELL
WELL ID NUMBER (from Permit): MW -9
Date sample collected: 1179/2016
FIELD ANALYSES:
WAS
Well Depth: 13.73 ft.
Well Diameter: 2 in.
pH oo400: 6.00 units Temp. 000lo: 18 OC
DRY at
Depth to Water Level 82546: 6 ft. below measuring point
Screened Interval: 13.73 ft. to
3:73
ft. Spec. Cond. 00094: uMhos
time of
Measuring Point is 3.00 ft. above land surface
l Relative M.P. Elevation: ft.
Odor 00085: None
sampling,
Volume of water pumped/bailed before sampling:
3.90
gallons
Appearance Clear
chect
Samples for metals were collected unfiltered:
X YES
NO
and field acidified: X YES ❑ NO
here.. —J
LABORATORY INFORMATION
Date sample analyzed: 11/9/16 - 11/22/16
Laboratory Name: Microbac Fayetteville Division Certification No. DWQ#11.
PARAMETERS NOTE.: Values should reflect
dissolved and colloidal
concentrations.
COD 00335
mg/L
Nitrite
(NO2) as N 00615
mg/L
Pb - Lead o1o51 `r!g/L
Coliform: MF Fecal 31616 24
/100mL
Nitrate
(NO3) as N 00620 0,449
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus:
Total as P 00665 <0.050
mg/L
(Note:: Use MPN method for highly turbid samples)
Orthophosphate
70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 282
mg1L
Al - Aluminum o11o5
mg/L
Sodium 22.3 mg/L
pH (Lab) 00403 6.00
units
Ba - Barium 01007
ug/L
Chloroform 0.942 ug/L
TOC 0o68o 34.3
mg/L
I Ca - Calcium 00916
mg/L
Chloride 00940 10.3
mg/L
lCd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium:
Total 01034
ug/L
Grease and Oils 00552
mg/L
+ Cu - Copper 01042
mg/L
ORGANICS:. (by GC, GC/MS, HPLC)
Phenol32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 11
mg/L
I Hg - Mercury 71900
ug/L
Lab Report Attached? p Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 78732: method # SW8260B
Total Ammonia 00610 <0.100
mg/L
Mg
- Magnesium 00927
mg/L
method #
(Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen, Total).
Mt
Manganese 01055 _
ug/L
. method #
TKN as N 00625 - ,
mg/L
Ni - Nickel 01067
ug/L
method #

DEPARTMENT OF -,ENVIRONMENT '& NATURAL RESOURCES -'
GROUNDWATER QUALITY MONITORING:
I
DIUISIONpPWATER.RESOURCES-INFORMATIONPROCESSINGUNIT `
SERVICE CENTER, -RALEIGH, NC -27,699.1617._ Phone; 919-807.-6306 =
COMPLIANCE REPORT FORM
I
1817 MKIL ,
FACILITY INFORMATION
Please Print Clearly o.
Type
PERMIT Number: WQ0000485 Expiration Date: 10/31/2019
Facility Name:
Valley Proteins Inc t-
Rose Hill'
Non -Discharge UIC
Permit Name (if different):
469 Yellow Cut
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
Rd.
Facility Address:
Rose Hill. NC 28458 -
❑ Lagoon ❑ Remediation: Infiltration Gallery
County Duplin
X Spray Field ❑ Remediation:.
lute (state) (zip)
Contact Person: William Gerrell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Others
- -
I
(from Permit)
L
If WELL
SAMPLING INFORMATiON
WELL ID NUMBERP.(from Permit), MW -10A
I' Date sample collected: 1/19/2016
FIELD ANALYSES:
WAS
Well Depth: 16 ft.
Well Diameter 2 in.
9 oC
pH 00400: 5.50 units Temp. 000 (uMhos
Depth to Water Level 82546: 4.5 ft below measuring point
Screened Interval. 16 ft. to
6 . Spec. Cond. 00094: .
ft
me
Dam
Measuring Point is - ° 3 ft, above land surface
Relative M.P. Elevation. ft.
Odor 00085: None
saRY
mpling,'
p 'g,'
Volume of water pumped/bailed before sampling:
5.60
gallons
Appearance Clear
chec4� -
Samples for metals were collected unfiltered:
X YES
NO
I and field acidified: X YES NO
here:_U
LABORATORY INFORMATION
Date sample analyzed: 11/9/16 - 11/22/16
Laboratory Name: Microbac Fayetteville Division Certification No. DWQ#11
PARAMETERS NOTE: Values should reflect dissolved and colloidal
concentrations.
COD 00335
mg/L
Ni
rite (NO2) as N oo615
mg/L Pb - Lead oio51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitr
ite (NO3) as N 00620 0:0505
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
1100mL Phosph(,,
rus: Total as P00665 0.37
mg/L
(Note: Use MPN method for highly turbid samples)
6rthophosphate 70507 _mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 616
mg/L
l Al -Aluminum 01105
mg/L, Sodium 176 mg/L
pH (Lab) 00403 5.50
units
Ba - Barium 01007
ug/L
TOC oo6so 8.93
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 231
mg/L
Cd - Cadmium 01027
ug/L
Arsenic oloo2
ug/L,
hr
Grease and Oils 00552
mg/L
U
CuCopper 01042
ORGANICS:(C,ATTACHPL)
Phenol 32730
ug/L
Fe Iron 01045
gL (Specify and hod #. LAB REPORT.)
Sulfate 00945 110
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? ❑Yes (0) ED No (0)
Specific Conductance 00095
uMhos
K - Potassium 00937
mg/L VOC 78732: method # SW8260B
Total Ammonia oo6io <0.100
mg/L
Mg
- Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen; Total)
n — Manganese 01055 _
ug/L. , method #
TKN as N 00825
mg/L
Ni - Nickel 01067
ug/L method #
_
_. r_._,.,�.._. «.n
Asa,, ,•r �l�inr^�• mn/l VOCRPmnval%

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
ity Name:
lit Name (if different):
ity Address:
ntact Person:
:II Location/Site Name
Type
Hill
County Duplin.
Telephone#: [phone]
No. of wells to be sampled: 11
(from Permit)
IEPARTMENT OF ENVIRONMENT Nf►t UKYi4KCJtlurtt,ca
11VISION OF WATER: RESOURCES - INFORMATION PROCESSING UNIT
617 MAIL SERVICE CENTER, RALEIGH,, NC 27699-1617 'Phone-: 919-807-6306.
on -Discharge UIC
PDES Other
YPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL ID NUMBER (from Permit). MW -11A i Date sample collected: 11/9/2016
Well Depth: 16 ft, Well Diameter:. 2 in.
Depth to Water Level 82546: 5 1 Screened Interval: 16 ft: to 6 ft.
Measuring Point is 3.3 ft. above land surface I Relative M.P. Elevation: ft.
Volume of water pumped/bailed before sampling: 5_.40 gal Ions
Samples for metals were collected unfiltered: X YES M NO, and field acidified: X YES ❑ NO
ite sample analyzed: 11/9/16 -11/22/16
kRAMETERS NOTE: Values should reflect dissolved and
COD 00335
mg/L
mg/L
Coliform: MF Fecal 31616
<1
/100mL I
Coliform: MF Total 31504
ug/L
/100mL Phos
(Note: Use MPN method for highly
turbid samples)
solved Solids:Total 70300
944
mg/L
pH (Lab) 00403
5.60
units'
TOC 0o5eo
6.26
mg/L
Chloride oo9Ao
62.3
mg/L
Arsenic 01002
ug/L
ug/L
Grease and Oils 00552
mg/L
mg/L
Phenol 52730
mg/L
ug/L
Sulfate 00945
43:0
mg/L
lecific Conductance 00095.
ug/L
µMhos
Total Ammonia oo610
<0A00
mg/L
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen,Total)'
TKN as N' 00625
mg1L
FIELD ANALYSES: WAS
pH 00400: 5.60 units Temp. mou Se °C, DRY at_
Spec. Cond. 00094: µMhos
time of
Odor 000m: None . sampling,
Appearance Clear check) -7
Laboratory Name: Microbac Fayetteville Division Certification No. DWQ#11
loidal concentrations.
-ite (NQZ) as N 00615 mg/L Pb - Lead oio51 ug/L
ite (NO3) as N 00620 0.0715 mg/L Zn - Zinc 01092 mg/L
rus: Total as P o0665 <0.050 mg/L
rthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
AI -Aluminum 01105
mg/L
Sodium 187 mg/L
Ba - Barium 01007
ug/L
Ca - Calcium oogi6
mg/L
Cd - Cadmium 01027
ug/L
iromium: Total 01034
ug/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury 71900
ug/L
Lab Report Attached? []Yes (0) ❑ No (0)
K - Potassium 00937
mg/L
VOC 78732: method # SW8260B
3 - Magnesium 00927
mg/L
method #
i - Manganese 01055
ug/L
method #
Ni - Nickel 01067
ug/L
„ method #
Permittee (or Authorized Agent) Name and Title -Please print or type ISignature of Permittee (or

i
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name: Valley. Proteins Inc. -
Permit Name (if different)
Facility Address: 469 Yellow Cul
., Rose Hill . NC 28458
(city) (state) (zip)
Contact Person: William Gerrell
Well Location/Site Name:
_L ID NUMBER (from Permit): MW -12B
I Depth: 16 ft.
th to Water Level 82546: 7.0 ft. below measuring, point
Isuring Point is 3 ft. above land surface
Ime of water pumped/bailed before sampling: 6.4 gall
ioles for metals were collected unfiltered: X YES ❑ NO
Date sample analyzed: 11/9/16 - 11/22/16
PARAMETERS NOTE: Values should reflect dissolved and col
COD 00335
DEPARTMENT`OF ENVIRONM•ENT;&'NATURAL RESOURCES'
mg/L
Ni
Coliform` MF Fecal 31616
<1.0
/100mL
Nitr
Coliform: MF Total 31504
Pe
/100mL
Phosph(
'(Note Use.41PN method for highly turbid samples)
Non -:Discharge UIC_
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
I] Lagoon ❑ Remediation: Infiltration Gallery
hophosphate 70507
)issolved Solids:Total 7o3oo
758
mg/L
mg/L
pH (Lab) 00403
5.20
units
❑ Rotary Distributor Land Application of Sludge
TOC 00680
7.03
mg/L
:d - Cadmium 01027
Chloride 00940
51.5
mg/L
ug/L
Arsenic 01002
Cu -Copper 01042
ug/L
C
Grease and Oils 00552
ug/L
mg/L
Hg - Mercury 71900
Phenol 32730
Lab Report At
ug/L
mg/L
Sulfate 00945
68
mg/L
SpecificConductance00095
ug/L
µMhos
Ni - Nickel 01067
Total Ammonia oo610
x.100
mg/L
R
.(Ammonia Nitrogen;. NH3 as N; Ammonia
Nitrogen, Total).
IV
TKN as N 00625
mg/L
- Please print or
Date sample collected: 11/9/2016 FIELD ANALYSES:
Well Diameter: 2 in. pH oo400: 5.20 units Temp. 00010: 19 °C
Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: µMhos
Relative M.P. Elevation: ft. Odor00085: None
Appearance Clear
and field acidified: X YES n NO
Laboratory Name:
DEPARTMENT`OF ENVIRONM•ENT;&'NATURAL RESOURCES'
idal concentrations.
DIVISION_OF WATER RESOURCES— INFORMATION-PROCESSING UNIT
:e (NO2) as N 00615
..
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617.- Phone: [phone]
s (NO3) as N 00620
Pe
PERMIT Number: W00000485 Expiration Date: 10/31/2019
is: Total as P 00665
Rose Hill_
-
Non -:Discharge UIC_
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
I] Lagoon ❑ Remediation: Infiltration Gallery
hophosphate 70507
mg/L
Rd.
County Duplin
mg/L
X Spray Field ❑ Remediation:
Ba - Barium 01007
Telephone#: [phone]
❑ Rotary Distributor Land Application of Sludge
;
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other.
:d - Cadmium 01027
(from. Permit).
-omium: Total 01034
Date sample collected: 11/9/2016 FIELD ANALYSES:
Well Diameter: 2 in. pH oo400: 5.20 units Temp. 00010: 19 °C
Screened Interval: 20 ft. to 10 ft. Spec. Cond. 00094: µMhos
Relative M.P. Elevation: ft. Odor00085: None
Appearance Clear
and field acidified: X YES n NO
Laboratory Name:
Microbac Fayetteville Division
idal concentrations.
:e (NO2) as N 00615
mg/L
Pb - Lead o1o51
s (NO3) as N 00620
0.103 mg/L
Zn - Zinc 01092
is: Total as P 00665
X0.050 mg/L
hophosphate 70507
mg/L
Other (Specify
11- Aluminum 01105
mg/L
Ba - Barium 01007
ug/L
Ca - Calcium oo916
mg/L
:d - Cadmium 01027
ug/L
-omium: Total 01034
ug/L
Cu -Copper 01042
mg/L
ORGANICS:
Fe - Iron 01045
ug/L
(Specify test a
Hg - Mercury 71900
ug/L
Lab Report At
C - Potassium 00937
mg/L
VOC 78732:
- Magnesium 00927
mg/L
- Manganese 01055
ug/L
Ni - Nickel 01067
ug/L
(or
Certification No. DWQ#11_
ug/L
mg/L
Compounds and Concentration Units):
Sodium 221 mg/L
DRY at
time of
sampling,
check– ]
here: L—I
by GC, GC/MS, HPLC)
nd method #. ATTACH LAB REPORT.)
tached? p Yes (0) E❑ No (0)
method # SW8260B
method # `
method #
method #

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
PAM ITY INF0RMATI0N Please
Facility Name:
Permit Name (if i
Facility Address:
Contact Person:
Well Location/Site Name:
WELL ID NUMBER (from Permit) MW -13A
Well Depth: 1.6 ft.
Depth to Water Level 82546: 8.0 ft. below measuring point
Measuring Point is 3 ft. above land surface
Volume of water pumped/bailed before sampling: 3.9 gall
Samples for metals were collected unfiltered: X YES ❑ NO
to sample analyzed: 11/9/16 - 11/22/16
iRAMETERS NOTE: Values should reflect dissolved and
COD 00335
PERMIT Number: WQ0000485' E=xpiration nate: I J/15-1lZU Ie
mg/L
Coliform: MF Fecal 31616
<1
/100mL
Coliform: MF Total 31504
Pb - Lead 01051 ug/L
/100mL Pho:
(Note: Use MPN method for highly turbid samples)
Telephone#: [phone]
solved Solids:Total 70300
18:0
mg/L
pH (Lab) 00403
6.40
units
TOC 00660
1.91
mg/L
Chloride 00940
1.6
mg/L
Arsenic 01002
FIELD ANALYSES:
ug/L
Grease and Oils 00552 _
Well Diameter: 2 in.
mg/L
Phenol 32730
DRY at
ug/L
Sulfate 00945
9.3
mg/L
ecific Conductance 00095
Odor 000m:
uMhos
Total Ammonia oo610
<0.100
mg/L
(Ammonia Nitrogem: NH3 as N; Ammonia Nitrogen, Total)
checlt-
TKN as N 00625
= Magnesium 00927
mg/L
and Title - Please print or type
rMENT OF ENVIRONMENT & NATURAL RESOURCES'
N OF WATER RESOURCES tNFORMATION.PROCESSING`UNIT ,
lIL SERVICECENTER; RALEIGH,; NC 276994817- Phone, 919-807.6300 -
pe
PERMIT Number: WQ0000485' E=xpiration nate: I J/15-1lZU Ie
lose Hill
Non -Discharge UIC.
NPDES Other _
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon 0 Remediation: Infiltration Gallery
:e (NO2) as N 00615
County Duplin
Pb - Lead 01051 ug/L
X Spray Field
❑ Remediation;.
Telephone#: [phone]
Q Rotary Distributor
[] Land Application of,Sludge.
No. of wells to be sampled: 11
❑ Water Source Heat Pump
[] Other:
(from permit)
\I - Aluminum o1,1o5
mg/L
Sodium 3,92 m /L
Ba - Barium 01007
ug/L
If WELI
Date sample collected: 11/912016
FIELD ANALYSES:
-
WAS
Well Diameter: 2 in.
pH 00400: 6.40 units
Temp. 000lo; 20 oC
DRY at
Screened Interval' 16 ft. to 6
ft. Spec. Cond. 00094:
uMhos
time of
Relative MY. Elevation: ft.
Odor 000m:
None
samplir
s
Appearance
Brown
checlt-
and field acidified: X YES ❑ NO
Laboratory Name:
Microbac Fayetteville_ Division Certification No. DWQ#11
idal concentrations.
:e (NO2) as N 00615
mg/L
Pb - Lead 01051 ug/L
3 (NO3) as N 00620
<0.05o mg/L
Zn - Zinc 01092 mg1L
is: Total as P 00665
<0.050 mg/L.
hophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
\I - Aluminum o1,1o5
mg/L
Sodium 3,92 m /L
Ba - Barium 01007
ug/L
Chloroform 0.565 ug/L
Ca -Calcium oo9i6
mg/L
d - Cadmium 01027
'ug/L
omium: Total o1o34
ug/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury 71900
ug/L
Lab Report Attached? p Yes (0) ❑ No (0)
- Potassium 00937
mg/L
VOC 78732: method #' SW8260B
= Magnesium 00927
mg/L
method #
- Manganese o1o55
ug/L
method #
Ni - Nickel o1o67
ug/L
method #
mg/L
of Permittee (or
MAXI -M

1 DEPARTMENT :OF ENVIRONMENT & NATURAL RESOURCES
-
DEPART,
j DIVISION OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
PROCESSMG,UNIT
COMPLIANCE REPORT FORM 1617 _MAIL SERVICE, CENTER,. RALEIGH, NC 2769.946i 7 - Phone: [phone],
FACILITY INFORMATION Please Print Clea
Facility Name: Valley Proteins I
Permit Name (if different):
Facility Address: 469 Yellow
- - -. Rose Hill . NC 25458 -
Contact Person:
Well Location/Site Name
pe PLKMI I NumDeP: VVUUuuus+oo cxNuduUii vaLc.
ose Hill Non -Discharge UIC
NPDES Other
d. TYPE OF PERMITTED OPERATION BEING MONITORED
County Duplin ❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Telephone#: [phone] p Rotary Distributor ❑ Land Application of Sludge
No. of wells to be sampled: 11 ❑ Water Source Heat Pump ❑ Other:
(from Permit)
Date sample analyzed:_ 11/9/16 - 11/22/16
PARAMETERS NOTE: Values should reflect dissolved and c
COD 00335
Microbac Fayetteville Division
mg/L
Coliform; MF Fecal 31616
If WELL
FLING INFORMATION
L IDNUMBER Permit) : MW -1'4A
!
Date sample collected: 11/g/2016
FHIANALYSES:
LD
/100mL Pho
WAS
(from
De p 16ft.
Well Diameter: 2 in.
pELD
5:50 units Temp. 000tc 19 °C
778
DRY at
h to Water Level 82546: 6.6 ft, below measuring point
Screened Interval: 1`0 ft. to 2.5 ft.
Spec. Cond. 00094: uMhos
TOC 00680
time. of
curing Point is 3 ft. above land surface
, Relative M.P. Elevation: ft.
Odor 00085; None
mg/L
sampltne
Tie of water pumped/bailed before sampling: 4.60
gallons
Grease and Oils 00552
Appearance Clear
mg/L
checl
Ales for metals were collected unfiltered: X YES
NQ
and field acidified: X YES M NO
99
mg/L
here:
Date sample analyzed:_ 11/9/16 - 11/22/16
PARAMETERS NOTE: Values should reflect dissolved and c
COD 00335
Microbac Fayetteville Division
mg/L
Coliform; MF Fecal 31616
<1
/1.00mL
Coliform: MF Total 31504
Pb - Lead 01051
/100mL Pho
(Note:. Use. WN method for highly
turbid samples)
rus: Total as P 00665
)issolved Solids:Total 70300
778
mg/L
pH (Lab) 00403
5.50
units
TOC 00680
6.48
mg/L
Chloride 00940
216
mg/L
Arsenic 01002
ug/L
Grease and Oils 00552
mg/L
Phenol 32730
ug/L
Sulfate 00945
99
mg/L
Specific Conductance 0009.5
(Specify test a
ttMhos
Total Ammonia 00610
X0.100
mg/L
(Ammonia Nitrogen; N113 as N, Ammonia Nitrogen, Total)
VOC 713732:
TKN as N 00625
mg/L
mg/L
Only
IM
(or Authorized Agent) Name and Title -
Laboratory Name:
Microbac Fayetteville Division
dal concentrations.
,ite (NO2) as N oo615
mg/L
Pb - Lead 01051
Ite (NO3) as N 00620
0.54 mg/L
Zn - Zinc 01092
rus: Total as P 00665
<0.050 mg/L
rthophosphate 70507
mg/L
Other (Specify
AI -Aluminum 01105
mg/L
Ba - Barium 01007
ug/L
Ca - Calcium 00916
mg/L
Cd - Cadmium 01027
ug/L,
iromium: Total 01034
ug/L
Cu - Copper 01042
mg/L
ORGANICS: (b
Fe - Iron 01045
ug/L
(Specify test a
Hg - Mercury 71900
ug/L
Lab Report At
K - Potassium 00937
mg/L
VOC 713732:
3 - Magnesium 00927
mg/L
i - Manganese 01055
ug/L
Ni - Nickel 01067
ug/L
mg/L Effluent
(or
Certification No. DWQ#11
ug/L
mg/L
Compounds and Concentration Units):
Sodium 324 mg/L
y GC, GC/MS, HPLC)
nd method #. ATTACH LAB REPORT.)
tached? ❑Yes (0) ❑ No (0)
method # SW8260B
method #
method #
method #
mg/L VOC Removal%
LPIs r

Groundwater Monitoring Well 2 Year Exceedance History Report
pH 6.5-8.5
1
7A
8A
9
10A
11A
12B
13A
14A
Nov -16
5.4
5
5.5
6
5.5
5.6
5.2
6.4
5.5
Jul -16
4
5.5
4.2
796
5
5.1
4.6
5.9
5.3
Mar -16
6.2
5.8
822
1170
6.3
6.3
6.2
5.4
6
Nov -15
5
4.7
5.3
5.7
5.3
5
5
4.8
5.3
Jul -15
6.3
4
4
5
5.2
4.6
4.3
5
5
Mar -15
4.6
4.3
4.2
6.1
5.7
5.4
5
4.9
6
Nov -14
4.7
5.4
4.6
5.2
6.3
5
5
6.2
TDS 500
10A
11A
12B
14A
Nov -16
616
944
758
778
Jul -16
682
1070
904
1070
Mar -16
546
888
572
738
Nov -15
648
738
904
796
Jul -15
826
826
704
784
Mar -15
780
882
822
1170
Nov -14
684
760
1110
852
TOC 10
9
Nov -16
34.3
Jul -16
53
Mar -16
38.2
Nov -15
48.4
Jul -15
32.7
Mar -15
42.7
Nov -14
24.2

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
MICRO A ®
Fayetteville Division
Certificate of Analysis
Project: N Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 1, grab
K6K0371-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
<0.250
ug/L
11/22/16 15:52
TMB
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
2.76
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:05
JR
SM 9222 D-1997
Color
Clear
<0.125
11/10/16 16:01
JMO
Field Observation
Depth of Water
16.0
feet
11/09/16 11:10
JMP
Field Measurement
Depth to Water Surface
6.00
feet
11/09/16 11:10
JMP
Field Measurement
Gallons purged (by client)
4.9
gallons
11/09/16 11:10
JMP
Field
Nitrate as N
<0.0500
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
<0.200
11/10/16 16:01
JMO
Field Observation
pH, Field Test
5.4
pH Units
11/09/16 11:10
JMP
SM 4500 H+B-2000
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/22/16 15:52
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
6.87
mg/L
11/16/16 11:52
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
126
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
19
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
19
°C
11/09/16 11:10
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/22/16 15:52
TMB
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
1,1-Dichloroethene
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
1,1-Dichloropropene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/22/16 15:52
TMB
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/22/16 15:52
TMB
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/22/16 15:52
TMB
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Microbac Laboratories, Inc.
Page 1 of 40
2592 Hope Wills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 1, grab
K6K0371-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,2 -Dichlorobenzene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/22/16 15:52
TMB
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/22/16 15:52
TMB
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
2-Butanone
<2.50
ug/L
11/22/16 15:52
TMB
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/22/16 15:52
TMB
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
2-Hexanone
<2.50
ug/L
11/22/16 15:52
TMB
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/22/16 15:52
TMB
SW8260B
Acetone
<2.50
ug/L
11/22/16 15:52
TMB
SW8260B
Benzene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
Bromobenzene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
Bromochloromethane
<0.200
ug/L
11/22/16 15:52
TMB
SW8260B
Bromodichloromethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Bromoform
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
Bromomethane
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
Carbon disulfide
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Chlorobenzene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Chloroethane
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
Chloroform
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
Chloromethane
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Microbac Laboratories, Inc.
Page 2 of 40
2592 Hope Wills Road I Fayetteville, PIC 28306 910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
V IC OBAC@
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 1, grab
K6K0371-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
Dibromomethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Ethylbenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Isopropylbenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
m -,p -Xylene
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
Methylene chloride
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Naphthalene
<0.200
ug/L
11/22/16 15:52
TMB
SW8260B
n-Butylbenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
n-Propylbenzene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
o -Xylene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Styrene
<0.125
ug/L
11/22/16 15:52
TMB
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Tetrachloroethene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Toluene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/22/16 15:52
TMB
SW8260B
Trichloroethene
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Vinyl acetate
<2.50
ug/L
11/22/16 15:52
TMB
SW8260B
Vinyl chloride
<0.250
ug/L
11/22/16 15:52
TMB
SW8260B
Surrogate: 1,2-Dichloroethane-d4
93.6%
80%-120%
11/22/16 15:52
TMB
SW8260B
Surrogate: 4 BromoJluorobenzene
102%
86%-115%
11/22/16 15:52
TMB
SW8260B
Surrogate: DibromoJluoromethane
93.7%
86%-118%
11/22/16 15:52
TMB
SW8260B
Surrogate: Toluene -d8
100%
88%-110%
11/22/16 15:52
TMB
SW8260B
Total Organic Carbon
4.26
mg/L
11/21/16 12:19
DCM
E415.1
MMell 2, grab
Microbac Laboratories, Inc.
Page 3 of 40
2592 Hope Mills Road I Fayetteville, IVC 28306 910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
� iCR AC®
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
K6K0371-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
8.92
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:05
JR
SM 9222 D-1997
Color
Clear
11/10/16 16:01
JMO
Field Observation
Depth of Water
31.0
feet
11/09/16 13:20
JMP
Field Measurement
Depth to Water Surface
22.0
feet
11/09/16 13:20
JMP
Field Measurement
Gallons purged (by client)
4.4
gallons
11/09/16 13:20
JMP
Field
Nitrate as N
0.413
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
11/10/16 16:01
JMO
Field Observation
pH, Field Test
6.7
pH Units
11/09/16 13:20
JMP
SM 4500 H+B-2000
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
21.7
mg/L
11/18/16 11:36
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
346
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
3.2
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
18
°C
11/09/16 13:20
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/18/16 20:58
JDS /
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
1,1-Dichloroethene
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
1, 1 -Dichloropropene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 4 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I wwrw.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 2, grab
K6K0371-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,2-Dichloroethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/18/16 20:58
JDS /
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/18/16 20:58
JDS /
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
2-Butanone
<2.50
ug/L
11/18/16 20:58
JDS /
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/18/16 20:58
JDS /
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
2-Hexanone
<2.50
ug/L
11/18/16 20:58
JDS /
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/18/16 20:58
JDS /
SW8260B
Acetone
<2.50
ug/L
11/18/16 20:58
JDS /
SW8260B
Benzene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
Bromobenzene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
Bromochloromethane
<0.200
ug/L
11/18/16 20:58
JDS /
SW8260B
Bromodichloromethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Bromoform
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
Bromomethane
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
Carbon disulfide
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Chlorobenzene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Chloroethane
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
Chloroform
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
Chloromethane
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Dibromomethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Microbac Laboratories, Inc. Page 5 of 40
2592 Hope Mills Road I Fayetteville, PIC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 2, grab
K6K0371-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac Laboratories, Inc - Ohio Valley
Dichlorodifluoromethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Ethylbenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Isopropylbenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
m -,p -Xylene
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
Methylene chloride
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Naphthalene
<0.200
ug/L
11/18/16 20:58
JDS /
SW8260B
n-Butylbenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
n-Propylbenzene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
o -Xylene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Styrene
<0.125
ug/L
11/18/16 20:58
JDS /
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Tetrachloroethene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Toluene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/18/16 20:58
JDS /
SW8260B
Trichloroethene
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Vinyl acetate
<2.50
ug/L
11/18/16 20:58
JDS /
SW8260B
Vinyl chloride
<0.250
ug/L
11/18/16 20:58
JDS /
SW8260B
Surrogate: 1,2-Dichloroethane-d4
96.2%
80%-120%
11/18/16 20:58
JDS/
SW8260B
Surrogate: 4-Bromofluorobenzene
96.6%
86%-115%
11/18/16 20:58
JDS/
SW8260B
Surrogate: Dibromofluoromethane
97.8%
86%-118%
11/18/16 20:58
JDS/
SW8260B
Surrogate: Toluene -d8
92.8%
88%-110%
11/18/16 20:58
JDS/
SW8260B
Total Organic Carbon
6.85
mg/L
11/22/16 09:06
DCM
E415.1
M/Well 4, grab
K6K0371-03
Microbac Laboratories, Inc.
Page 6 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
(IDIRO BAC@
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
3.39
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:05
JR
SM 9222 D-1997
Color
Clear
ug/L
11/10/16 16:01
JMO
Field Observation
Depth of Water
30.0
feet
11/09/16 12:50
JMP
Field Measurement
Depth to Water Surface
6.70
feet
11/09/16 12:50
JMP
Field Measurement
Gallons purged (by client)
11
gallons
11/09/16 12:50
JMP
Field
Nitrate as N
<0.0500
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
ug/L
11/10/16 16:01
JMO
Field Observation
pH, Field Test
6.9
pH Units
11/09/16 12:50
JMP
SM 4500 H+B-2000
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
9.42
mg/L
11/16/16 11:52
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
212
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
<0.25
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
20
°C
11/09/16 12:50
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/18/16 21:30
JDS /
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
1, 1 -Dichloroethene
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
1, 1 -Dichloropropene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/18/16 21:30
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 7 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose 1HII Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
VIRBAC®
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 4, grab
K6K0371-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,3,5-Trimethylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/18/16 21:30
JDS /
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
2-Butanone
<2.50
ug/L
11/18/16 21:30
JDS /
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/18/16 21:30
JDS /
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
2-Hexanone
<2.50
ug/L
11/18/16 21:30
JDS /
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/18/16 21:30
JDS /
SW8260B
Acetone
<2.50
ug/L
11/18/16 21:30
JDS /
SW8260B
Benzene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
Bromobenzene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
Bromochloromethane
<0.200
ug/L
11/18/16 21:30
JDS /
SW8260B
Bromodichloromethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Bromoform
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
Bromomethane
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
Carbon disulfide
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Chlorobenzene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Chloroethane
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
Chloroform
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
Chloromethane
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Dibromomethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Ethylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Microbac Laboratories, Inc. Page 8 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose Hill Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 4, grab
K6K0371-03
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
Hexachlorobutadiene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Isopropylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
m -,p -Xylene
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
Methylene chloride
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Naphthalene
<0.200
ug/L
11/18/16 21:30
JDS /
SW8260B
n-Butylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
n-Propylbenzene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
o -Xylene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Styrene
<0.125
ug/L
11/18/16 21:30
JDS /
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Tetrachloroethene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Toluene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/18/16 21:30
JDS /
SW8260B
Trichloroethene
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Vinyl acetate
<2.50
ug/L
11/18/16 21:30
JDS /
SW8260B
Vinyl chloride
<0.250
ug/L
11/18/16 21:30
JDS /
SW8260B
Surrogate: 1,2-Dichloroethane-d4
967%
80%-120%
11/18/16 21:30
JDS/
SW8260B
Surrogate:4-Bromofluorobenzene
96.2%
86%-115%
11/18/1621:30
JDS/
SW8260B
Surrogate: Dibromofluoromethane
99.7%
86%-118%
11/18/16 21:30
JDS/
SW8260B
Surrogate: Toluene -d8
92.6%
88%-110%
11/18/16 21:30
JDS/
SW8260B
Total Organic Carbon
5.80
mg/L
11/21/16 12:45
DCM
E415.1
M/Well 7A, grab
K6K0371-04
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Microbac Laboratories, Inc.
Page 9 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 7A, grab
K6K0371-04
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
Chloride
33.4
Coliform, Fecal
<1.0
Color
Clear
Depth of Water
16.0
Depth to Water Surface
7.00
Gallons purged (by client)
4.4
Nitrate as N
<0.0500
Odor
None
pH, Field Test
5.0
mg/L
mg/L
per 100 mL
feet
feet
gallons
mg/L
pH Units
11/14/16 08:30
11/11/16 11:42
11/09/16 17:05
11/10/16 16:01
11/09/16 11:45
11/09/16 11:45
11/09/16 11:45
11/11/16 11:42
11/10/16 16:01
11/09/16 11:45
DSK
AC
JR
JMO
JMP
JMP
JMP
AC
JMO
JMP
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
Sodium
88.7
mg/L
11/18/16 11:36
AC
Total Dissolved Solids
386
mg/L
11/10/16 13:34
JR
Sulfate as SO4
7.6
mg/L
11/11/16 11:42
AC
Temperature, field
19
°C
11/09/16 11:45
JMP
SM 4500 NH3 C-1997
EPA 300.0, Rev. 2.1 (1993)
SM 9222 D-1997
Field Observation
Field Measurement
Field Measurement
Field
EPA 300.0, Rev. 2.1 (1993)
Field Observation
SM 4500 H+B-2000
(Aqueous)
SM 4500-P F-1999
EPA 200.7 Rev 4.4 1994
SM 2540 C-1997
EPA 300.0, Rev. 2.1 (1993)
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/18/16 22:02
JDS /
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
1, 1 -Dichloroethene
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
1, 1 -Dichloropropene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 10 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
�VI C O BAC@
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 7A, grab
K6K0371-04
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,2 -Dichlorobenzene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/18/16 22:02
JDS /
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/18/16 22:02
JDS /
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
2-Butanone
<2.50
ug/L
11/18/16 22:02
JDS /
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/18/16 22:02
JDS /
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
2-Hexanone
<2.50
ug/L
11/18/16 22:02
JDS /
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/18/16 22:02
JDS /
SW8260B
Acetone
<2.50
ug/L
11/18/16 22:02
JDS /
SW8260B
Benzene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
Bromobenzene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
Bromochloromethane
<0.200
ug/L
11/18/16 22:02
JDS /
SW8260B
Bromodichloromethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Bromoform
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
Bromomethane
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
Carbon disulfide
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Chlorobenzene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Chloroethane
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
Chloroform
0.146
ug/L
11/18/16 22:02
JDS /
SW8260B
Chloromethane
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
J
Microbac Laboratories, Inc.
Page 11 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HILI Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
OIC C@
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 7A, grab
K6K0371-04
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
Dibromomethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Ethylbenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Isopropylbenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
m -,p -Xylene
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
Methylene chloride
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Naphthalene
<0.200
ug/L
11/18/16 22:02
JDS /
SW8260B
n-Butylbenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
n-Propylbenzene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
o -Xylene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Styrene
<0.125
ug/L
11/18/16 22:02
JDS /
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Tetrachloroethene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Toluene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/18/16 22:02
JDS /
SW8260B
Trichloroethene
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Vinyl acetate
<2.50
ug/L
11/18/16 22:02
JDS /
SW8260B
Vinyl chloride
<0.250
ug/L
11/18/16 22:02
JDS /
SW8260B
Surrogate: 1,2-Dichloroethane-d4
97.8%
80%-120%
11/18/16 22:02
JDS/
SW8260B
Surrogate: 4-Bromofluorobenzene
96.9%
86%-115%
11/18/16 22:02
JDS/
SW8260B
Surrogate: Dibromofluoromethane
99.1%
86%-118%
11/18/16 22:02
JDS/
SW8260B
Surrogate: Toluene -d8
92.1%
88%-110%
11/18/16 22:02
JDS/
SW8260B
Total Organic Carbon
5.40
mg/L
11/21/16 12:58
DCM
E415.1
M/Well 8A, grab
Microbac Laboratories, Inc.
Page 12 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose Hlll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
V ICROBA °
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
K6K0371-05
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
5.60
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
6.0
per 100 mL
11/09/16 17:05
JR
SM 9222 D-1997
Color
Clear
11/10/16 16:01
JMO
Field Observation
Depth of Water
16.0
feet
11/09/16 11:55
JMP
Field Measurement
Depth to Water Surface
8.00
feet
11/09/16 11:55
JUT
Field Measurement
Gallons purged (by client)
3.9
gallons
11/09/16 11:55
JMP
Field
Nitrate as N
0.459
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
11/10/16 16:01
JMO
Field Observation
pH, Field Test
5.5
pH Units
11/09/16 11:55
JMP
SM 4500 H+B-2000
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
4.12
mg/L
11/16/16 11:52
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
118
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
35
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
19
°C
11/09/16 11:55
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/18/16 22:34
JDS /
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1, 1 -Dichloroethane
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
1, 1 -Dichloroethene
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
1, 1 -Dichloropropene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 13 of 40
2592 Hope Mills (toad I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIII Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
�r&IRAC°
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 8A, grab
K6K0371-05
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
1,2-Dichloroethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/18/16 22:34
JDS /
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/18/16 22:34
JDS /
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
2-Butanone
<2.50
ug/L
11/18/16 22:34
JDS /
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/18/16 22:34
JDS /
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
2-Hexanone
<2.50
ug/L
11/18/16 22:34
JDS /
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/18/16 22:34
JDS /
SW8260B
Acetone
<2.50
ug/L
11/18/16 22:34
JDS /
SW8260B
Benzene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
Bromobenzene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
Bromochloromethane
<0.200
ug/L
11/18/16 22:34
JDS /
SW8260B
Bromodichloromethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Bromoform
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
Bromomethane
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
Carbon disulfide
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Chlorobenzene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Chloroethane
<0.500
ug/L
11/18/16 22:34.
JDS /
SW8260B
Chloroform
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
Chloromethane
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Dibromomethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 14 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HILI Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
(SPICRC
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 8A, grab
K6K0371-05
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
Dichlorodifluoromethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Ethylbenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Isopropylbenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
m -,p -Xylene
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
Methylene chloride
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Naphthalene
<0.200
ug/L
11/18/16 22:34
JDS /
SW8260B
n-Butylbenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
n-Propylbenzene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
o -Xylene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Styrene
<0.125
ug/L
11/18/16 22:34
JDS /
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Tetrachloroethene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Toluene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/18/16 22:34
JDS /
SW8260B
Trichloroethene
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Vinyl acetate
<2.50
ug/L
11/18/16 22:34
JDS /
SW8260B
Vinyl chloride
<0.250
ug/L
11/18/16 22:34
JDS /
SW8260B
Surrogate: 1,2-Dichloroethane-d4
97.2%
80%-120%
11/18/16 22:34
JDS/
SW8260B
Surrogate: 4-Bromofluorobenzene
95.5%
86%-115%
11/18/16 22:34
JDS/
SW8260B
Surrogate: Dibromofluoromethane
98.2%
86%-118%
11/18/16 22:34
JDS/
SW8260B
Surrogate: Toluene -d8
93.3%
88%-110%
11/18/16 22:34
JDS /
SW8260B
Total Organic Carbon
2.93
mg/L
11/21/16 13:10
DCM
E415.1
M/Well 9, grab
K6K0371-06
Microbac Laboratories, Inc. Page 15 of 40
2592 Hope Wills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
(D)MiCROBAC°
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
Chloride
10.3
Coliform, Fecal
24
Color
Clear
Depth of Water
14.0
Depth to Water Surface
6.00
Gallons purged (by client)
3.9
Nitrate as N
0.449
Odor
None
pH, Field Test
6.0
mg/L
mg/L
per 100 mL
feet
feet
gallons
mg/L
pH Units
11/14/16 08:30
11/11/16 11:42
11/09/16 17:35
11/10/16 16:01
11/09/16 12:30
11/09/16 12:30
11/09/16 12:30
11/11/16 11:42
11/10/16 16:01
11/09/16 12:30
DSK
AC
JR
JMO
JMP
JMP
JMP
AC
JMO
JMP
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
Sodium
22.3
mg/L
11/18/16 11:36
AC
Total Dissolved Solids
282
mg/L
11/10/16 13:34
JR
Sulfate as SO4
11
mg/L
11/11/16 11:42
AC
Temperature, field
18
°C
11/09/16 12:30
JMP
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
SM 4500 NH3 C-1997
EPA 300.0, Rev. 2.1 (1993)
SM 9222 D-1997
Field Observation
Field Measurement
Field Measurement
Field
EPA 300.0, Rev. 2.1 (1993)
Field Observation
SM 4500 H+B-2000
(Aqueous)
SM 4500-P F-1999
EPA 200.7 Rev 4.4 1994
SM 2540 C-1997
EPA 300.0, Rev. 2.1 (1993)
SM 2550 B-2000
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/18/16 23:06
JDS /
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
1, 1 -Dichloroethene
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
1,1-Dichloropropene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 16 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 9, grab
K6K0371-06
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac Laboratories, Inc. - Ohio Valley
1,2-Dichloropropane
<0.200
ug/L
11/18/16 23:06
JDS /
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/18/16 23:06
JDS /
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
2-Butanone
<2.50
ug/L
11/18/16 23:06
JDS /
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/18/16 23:06
JDS /
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
2-Hexanone
<2.50
ug/L
11/18/16 23:06
JDS /
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/18/16 23:06
JDS /
SW8260B
Acetone
<2.50
ug/L
11/18/16 23:06
JDS /
SW8260B
Benzene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
Bromobenzene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
Bromochloromethane
<0.200
ug/L
11/18/16 23:06
JDS /
SW8260B
Bromodichloromethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Bromofonn
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
Bromometbane
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
Carbon disulfide
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Chlorobenzene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Chloroethane
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
Chloroform
0.942
ug/L
11/18/16 23:06
JDS /
SW8260B
Chloromethane
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Dibromomethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
J
Microbac Laboratories, Inc.
Page 17 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose Hlll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
�MICROBAC@
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 9, grab
K6K0371-06
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac Laboratories, Inc. - Ohio Valley
Ethylbenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Isopropylbenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
m -,p -Xylene
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
Methylene chloride
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Naphthalene
<0.200
ug/L
11/18/16 23:06
JDS /
SW8260B
n-Butylbenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
n-Propylbenzene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
o -Xylene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Styrene
<0.125
ug/L
11/18/16 23:06
JDS /
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Tetrachloroethene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Toluene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/18/16 23:06
JDS /
SW8260B
Trichloroethene
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Vinyl acetate
<2.50
ug/L
11/18/16 23:06
JDS /
SW8260B
Vinyl chloride
<0.250
ug/L
11/18/16 23:06
JDS /
SW8260B
Surrogate: 1,2-Dichloroethane-d4
96.5%
80%-120%
11/18/16 23:06
JDS/
SW8260B
Surrogate: 4-BromoJluorobenzene
97.1%
86%-115%
11/18/16 23:06
JDS /
SW8260B
Surrogate: DibromoJluoromethane
98.5%
86016-118%
11/18/16 23:06
JDS/
SW8260B
Surrogate: Toluene -d8
92.0%
88%-110%
11118116 23:06
JDS /
SW8260B
Total Organic Carbon
34.3
mg/L
11/22/16 03:44
DCM
E415.1
M/Well 10A, grab
K6K0371-07
Analyte Result Units Analyzed Analyzed By Method Qualifier
Microbac Laboratories, Inc.
Page 18 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

V t C O BAC@
Fayetteville Division
Certificate of Analysis
Valley Protein - Rose HIll Plant Date Reported: 12/27/16
Mr. Matthew Haynes Project: M/Well Samples - Nov Date Received: 11/09/16
469 Yellow Cut Road Date Sampled: 11/09/16
Rose Hill NC, 28458 Sampled By: Poythress
M/Well 10A, grab
K6K0371-07
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
0.37
mg/L
11/15/16 11:59
DSK
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
231
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:35
JR
SM 9222 D-1997
Color
Clear
19
11/10/16 16:01
JMO
Field Observation
Depth of Water
16.0
feet
11/09/16 12:10
JMP
Field Measurement
Depth to Water Surface
4.50
feet
11/09/16 12:10
JMP
Field Measurement
Gallons purged (by client)
5.6
gallons
11/09/16 12:10
JMP
Field
Nitrate as N
0.0505
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
ug/L
11/10/16 16:01
JMO
Field Observation
pH, Field Test
5.5
pH Units
11/09/16 12:10
JMP
SM 4500 H+B-2000
Microbac Laboratories, Inc.
Page 19 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com
(Aqueous)
Phosphorus, Total
0.37
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
176
mg/L.
11/18/16 11:36
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
616
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
110
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
19
°C
11/09/16 12:10
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/18/16 23:38
JDS /
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
1, 1 -Dichloroethene
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
1,1-Dichloropropene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 19 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HE Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 10A, grab
K6K0371-07
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac Laboratories, Inc. - Ohio Valley
1,2 -Dichlorobenzene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/18/16 23:38
JDS /
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/18/16 23:38
JDS /
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
2-Butanone
<2.50
ug/L
11/18/16 23:38
JDS /
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/18/16 23:38
JDS /
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
2-Hexanone
<2.50
ug/L
11/18/16 23:38
JDS /
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/18/16 23:38
JDS /
SW8260B
Acetone
<2.50
ug/L
11/18/16 23:38
JDS /
SW8260B
Benzene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
Bromobenzene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
Bromochloromethane
<0.200
ug/L
11/18/16 23:38
JDS /
SW8260B
Bromodichloromethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Bromoform
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
Bromomethane
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
Carbon disulfide
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Chlorobenzene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Chloroetbane
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
Chloroform
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
Chloromethane
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Microbac Laboratories, Inc.
Page 20 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
MfWell 10A, grab
K6K0371-07
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
Dibromomethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Ethylbenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Isopropylbenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
m -,p -Xylene
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
Methylene chloride
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Naphthalene
<0.200
ug/L
11/18/16 23:38
JDS /
SW8260B
n-Butylbenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
n-Propylbenzene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
o -Xylene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Styrene
<0.125
ug/L
11/18/16 23:38
JDS /
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Tetrachloroethene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Toluene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/18/16 23:38
JDS /
SW8260B
Trichloroethene
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Vinyl acetate
<2.50
ug/L
11/18/16 23:38
JDS /
SW8260B
Vinyl chloride
<0.250
ug/L
11/18/16 23:38
JDS /
SW8260B
Surrogate: 1,2-Dichloroethane-d4
97.9%
80%-120%
11/18/16 23:38
JDS/
SW8260B
Surrogate: 4-BromoJluorobenzene
95.8%
86%-115%
11/18/16 23:38
JDS/
SW8260B
Surrogate: Dibromofluoromethane
98.8%
86%-118%
11/18/16 23:38
JDS /
SW8260B
Surrogate: Toluene -d8
92.9%
88%-110%
11/18/16 23:38
JDS/
SW8260B
Total Organic Carbon
8.93
mg/L
11/21/16 13:37
DCM
E415.1
M/Well 11A, grab
Microbac Laboratories, Inc.
Page 21 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

VcCRO.C®
Fayetteville Division
Certificate of Analysis
Valley Protein - Rose Hlll Plant
Date Reported: 12/27/16
Mr. Matthew Haynes
Project: M/Well Samples - Nov
Date Received: 11/09/16
469 Yellow Cut Road
Date Sampled: 11/09/16
Rose Hill NC, 28458
Sampled By: Poythress
K6K0371-08
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
62.3
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:35
JR
SM 9222 D-1997
Color
Clear
11/10/16 16:01
JMO
Field Observation
Depth of Water
16.0
feet
11/09/16 10:20
JMP
Field Measurement
Depth to Water Surface
5.00
feet
11/09/16 10:20
JMP
Field Measurement
Gallons purged (by client)
5.4
gallons
11/09/16 10:20
JMP
Field
Nitrate as N
0.0715
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
11/10/16 16:01
JMO
Field Observation
pH, Field Test
5.6
pH Units
11/09/16 10:20
JMP
SM 4500 H+B-2000
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
187
mg/L
11/18/16 11:36
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
944
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
43
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
18
°C
11/09/16 10:20
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/19/16 01:44
FJB
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1, 1 -Dichloroethane
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
1,1-Dichloroethene
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
1,1-Dichloropropene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/19/16 01:44
FJB
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/19/16 01:44
FJB
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/19/16 01:44
FJB
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
Microbac Laboratories, Inc.
Page 22 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
VICROAC6
Fayetteville Division
Certificate of Analysis
Project: M1Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M[Well 11A, grab
K6K0371-08
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,2-Dichloroethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/19/16 01:44
FJB
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/19/16 01:44
FJB
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
2-Butanone
<2.50
ug/L
11/19/16 01:44
FJB
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/19/16 01:44
FJB
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
2-Hexanone
<2.50
ug/L
11/19/16 01:44
FJB
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/19/16 01:44
FJB
SW8260B
Acetone
<2.50
ug/L
11/19/16 01:44
FJB
SW8260B
Benzene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
Bromobenzene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
Bromochloromethane
<0.200
ug/L
11/19/16 01:44
FJB
SW8260B
Bromodichloromethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Bromoform
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
Bromomethane
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
Carbon disulfide
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Chlorobenzene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Chloroethane
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
Chloroform
0.278
ug/L
11/19/16 01:44
FJB
SW8260B
Chloromethane
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Dibromomethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
J
Microbac Laboratories, Inc. Page 23 of 40
2592 Hope Mills (toad I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I wwwr.microbac.com

Valley Protein - Rose Hlll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: MfWell Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 11A, grab
K6K0371-08
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mi[robac Laboratories, Inc - Ohio Valley
Dichlorodifluoromethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Ethylbenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Isopropylbenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
m -,p -Xylene
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
Methylene chloride
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Naphthalene
<0.200
ug/L
11/19/16 01:44
FJB
SW8260B
n-Butylbenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
n-Propylbenzene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
o -Xylene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Styrene
<0.125
ug/L
11/19/16 01:44
FJB
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Tetrachloroethene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Toluene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/19/16 01:44
FJB
SW8260B
Trichloroethene
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Vinyl acetate
<2.50
ug/L
11/19/16 01:44
FJB
SW8260B
Vinyl chloride
<0.250
ug/L
11/19/16 01:44
FJB
SW8260B
Surrogate: 1,2-Dichloroethane-d4
103%
80%-120%
11/19/16 01:44
FJB
SW8260B
Surrogate: 4-Bromofluorobenzene
106%
86%-115%
11/19/16 01:44
FJB
SW8260B
Surrogate: Dibromofluoromethane
102%
86%-118%
11/19/16 01:44
FJB
SW8260B
Surrogate: Toluene -d8
102%
88%-110%
11/19/16 01:44
FJB
SW8260B
Total Organic Carbon
6.26
mg/L
11/21/16 14:14
DCM
E415.1
NMell 12B, grab
K6K0371-09
Microbac Laboratories, Inc. Page 24 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville Division
Certificate of Analysis
Valley Protein - Rose Hill Plant
Date Reported: 12/27/16
Mr. Matthew Haynes
Project: M/Well Samples - Nov
Date Received: 11/09/16
469 Yellow Cut Road
Date Sampled: 11/09/16
Rose Hill NC, 28458
Sampled By: Poythress
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
51.5
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:35
JR
SM 9222 D-1997
Color
Clear
11/10/16 16:01
JMO
Field Observation
Depth of Water
20.0
feet
11/09/16 10:40
JMP
Field Measurement
Depth to Water Surface
7.00
feet
11/09/16 10:40
JMP
Field Measurement
Gallons purged (by client)
6.4
gallons
11/09/16 10:40
JMP
Field
Nitrate as N
0.103
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
11/10/16 16:01
JMO
Field Observation
pH, Field Test
5.2
pH Units
11/09/16 10:40
JMP
SM 4500 H+B-2000
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
221
mg/L
12/01/16 13:45
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
758
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
68
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
19
°C
11/09/16 10:40
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/19/16 02:12
FJB
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
1,1-Dichloroethene
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
1, 1 -Dichloropropene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/19/16 02:12
FJB
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/19/16 02:12
FJB
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/19/16 02:12
FJB
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/19/16 02:12
FJB
SW8260B
Microbac Laboratories, Inc.
Page 25 of 40
2592 Hope Mills Road I Fayetteville, NC 28306
1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/WeR 12B, grab
K6K0371-09
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
1,3,5-Trimethylbenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/19/16 02:12
FJB
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
2-Butanone
<2.50
ug/L
11/19/16 02:12
FJB
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/19/16 02:12
FJB
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
2-Hexanone
<2.50
ug/L
11/19/16 02:12
FJB
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/19/16 02:12
FJB
SW8260B
Acetone
<2.50
ug/L
11/19/16 02:12
FJB
SW8260B
Benzene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
Bromobenzene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
Bromochloromethane
<0.200
ug/L
11/19/16 02:12
FJB
SW8260B
Bromodichloromethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Bromoform
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
Bromomethane
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
Carbon disulfide
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Chlorobenzene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Chloroethane
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
Chloroform
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
Chloromethane
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Dibromomethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Ethylbenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Microbac Laboratories, Inc.
Page 26 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HILI Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
VICRO Ac°
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 12B, grab
K6K0371-09
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac Laboratories, Inc. - Ohio Valley
Hexachlorobutadiene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Isopropylbenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
m -,p -Xylene
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
Methylene chloride
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Naphthalene
<0.200
ug/L
11/19/16 02:12
FJB
SW8260B
n-Butylbenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
n-Propylbenzene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
o -Xylene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Styrene
<0.125
ug/L
11/19/16 02:12
FJB
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Tetrachloroethene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Toluene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/19/16 02:12
FJB
SW8260B
Trichloroethene
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Vinyl acetate
<2.50
ug/L
11/19/16 02:12
FJB
SW8260B
Vinyl chloride
<0.250
ug/L
11/19/16 02:12
FJB
SW8260B
Surrogate: 1,2-Dichloroethane-d4
98.3%
80%-120%
11/19/16 02:12
FJB
SW8260B
Surrogate: 4 BromoJluorobenzene
99.5%
86%-115%
11/19/16 02:12
FJB
SW8260B
Surrogate: DibromoJluoromethane
102%
86%-118%
11/19/16 02:12
FJB
SW8260B
Surrogate: Toluene -d8
99.6%
88%-110%
11/19/16 02:12
FJB
SW8260B
Total Organic Carbon
7.03
mg/L
11/21/16 14:27
DCM
E415.1
M/Well 13A, grab
K6K0371-10
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc - Fayetteville
Microbac Laboratories, Inc. Page 27 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

�VICOBAC`
Fayetteville Division
Microbac Laboratories, Inc. Page 28 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com
Certificate of Analysis
IMM
ValleyValley Protein - Rose Hlll Plant
Date Reported: 12/27/16
Mr. Matthew Haynes
Project: M/Well Samples - Nov
Date Received: 11/09/16
469 Yellow Cut Road
Date Sampled: 11/09/16
Rose Hill NC, 28458
Sampled By: Poythress
X[/Well 13A, grab
K6K0371-10
Analyte
Result
Units
Analyzed
Analyzed By
Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
1.60
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:35
JR
SM 9222 D-1997
Color
Brown
11/10/16 16:01
JMO
Field Observation
Depth of Water
16.0
feet
11/09/16 10:55
JMP
Field Measurement
Depth to Water Surface
8.00
feet
11/09/16 10:55
JMP
Field Measurement
Gallons purged (by client)
3.9
gallons
11/09/16 10:55
JMP
Field
Nitrate as N
<0.0500
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
11/10/16 16:01
JMO
Field Observation
pH, Field Test
6.4
pH Units
11/09/16 10:55
JMP
SM 4500 H+B-2000
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
3.92
mg/L
11/16/16 11:52
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
18.0
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
9.3
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
20
°C
11/09/16 10:55
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/19/16 02:41
FJB
SW8260B
1,1,2-Trichloroetbane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
1, 1 -Dichloroethene
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
1,1-Dichloropropene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/19/16 02:41
FJB
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/19/16 02:41
FJB
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/19/16 02:41
FJB
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Microbac Laboratories, Inc. Page 28 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1 910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIII Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: MIWell Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 13A, grab
K6K0371-10
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,2 -Dichlorobenzene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/19/16 02:41
FJB
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/19/16 02:41
FJB
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
2-Butanone
<2.50
ug/L
11/19/16 02:41
FJB
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/19/16 02:41
FJB
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
2-Hexanone
<2.50
ug/L
11/19/16 02:41
FJB
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/19/16 02:41
FJB
SW8260B
Acetone
<2.50
ug/L
11/19/16 02:41
FJB
SW8260B
Benzene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
Bromobenzene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
Bromochloromethane
<0.200
ug/L
11/19/16 02:41
FJB
SW8260B
Bromodichloromethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Bromoform
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
Bromomethane
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
Carbon disulfide
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Chlorobenzene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Chloroethane
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
Chloroform
0.565
ug/L
11/19/16 02:41
FJB
SW8260B
Chloromethane
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
J
Microbac Laboratories, Inc.
Page 29 of 40
2592 Hope Mills Road I Fayetteville, IAC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HILI Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 13A, grab
K6K0371-10
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
Dibromomethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Ethylbenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Isopropylbenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
m -,p -Xylene
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
Methylene chloride
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Naphthalene
<0.200
ug/L
11/19/16 02:41
FJB
SW8260B
n-Butylbenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
n-Propylbenzene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
o -Xylene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Styrene
<0.125
ug/L
11/19/16 02:41
FJB
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Tetrachloroethene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Toluene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/19/16 02:41
FJB
SW8260B
Trichloroethene
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Trichlorofluoromethane
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Vinyl acetate
<2.50
ug/L
11/19/16 02:41
FJB
SW8260B
Vinyl chloride
<0.250
ug/L
11/19/16 02:41
FJB
SW8260B
Surrogate: 1,2-Dichloroethane-d4
101%
80%-120%
11/19/16 02:41
FJB
SW8260B
Surrogate: 4-BromoJluorobenzene
104%
86%-115%
11/19/16 02:41
FJB
SW8260B
Surrogate: DibromoJluoromethane
103%
86%-118%
11/19/16 02:41
FJB
SW8260B
Surrogate: Toluene -d8
101%
88%-110%
11/19116 02:41
FJB
SW8260B
Total Organic Carbon
1.91
mg/L
11/21/16 14:40
DCM
E415.1
M/Well 14A, grab
Microbac Laboratories, Inc.
Page 30 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIll Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
&)MICROBAC@
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
K6K0371-11
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Fayetteville
Ammonia as N
<0.100
mg/L
11/14/16 08:30
DSK
SM 4500 NH3 C-1997
Chloride
216
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Coliform, Fecal
<1.0
per 100 mL
11/09/16 17:35
JR
SM 9222 D-1997
Color
Clear
11/10/16 16:01
JMO
Field Observation
Depth of Water
16.0
feet
11/09/16 11:30
JMP
Field Measurement
Depth to Water Surface
6.60
feet
11/09/16 11:30
JMP
Field Measurement
Gallons purged (by client)
4.6
gallons
11/09/16 11:30
JMP
Field
Nitrate as N
0.541
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Odor
None
11/10/16 16:01
JMO
Field Observation
pH, Field Test
5.5
pH Units
11/09/16 11:30
JMP
SM 4500 H+B-2000
(Aqueous)
Phosphorus, Total
<0.050
mg/L
11/15/16 11:59
DSK
SM 4500-P F-1999
Sodium
324
mg/L
12/01/16 13:45
AC
EPA 200.7 Rev 4.4 1994
Total Dissolved Solids
778
mg/L
11/10/16 13:34
JR
SM 2540 C-1997
Sulfate as SO4
99
mg/L
11/11/16 11:42
AC
EPA 300.0, Rev. 2.1 (1993)
Temperature, field
19
°C
11/09/16 11:30
JMP
SM 2550 B-2000
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/19/16 03:10
FJB
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
1,1-Dichloroethene
<0.500
ug/L
11/19/16 03:10
FJB
SW8260B
1,1-Dichloropropene
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,2,3-Trichlorobenzene
<0.150
ug/L
11/19/16 03:10
FJB
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/19/16 03:10
FJB
SW8260B
1,2,4-Trichlorobenzene
<0.200
ug/L
11/19/16 03:10
FJB
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/19/16 03:10
FJB
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
Al2
Al2
Microbac Laboratories, Inc.
Page 31 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose HIII Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/Well 14A, grab
K6K0371-11
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,2-Dichloroethane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/19/16 03:10
FJB
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/19/16 03:10
FJB
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
2-Butanone
<2.50
ug/L
11/19/16 03:10
FJB
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/19/16 03:10
FJB
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
2-Hexanone
<2.50
ug/L
11/19/16 03:10
FJB
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/19/16 03:10
FJB
SW8260B
Acetone
<2.50
ug/L
11/19/16 03:10
FJB
SW8260B
Benzene
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
Bromobenzene
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
Bromochloromethane
<0.200
ug/L
11/19/16 03:10
FJB
SW8260B
Bromodichloromethane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
Bromoform
<0.500
ug/L
11/19/16 03:10
FJB
SW8260B
Bromomethane
<0.500
ug/L
11/19/16 03:10
FJB
SW8260B
Carbon disulfide
<0.500
ug/L
11/19/16 03:10
FJB
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
Chlorobenzene
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
Chloroethane
<0.500
ug/L
11/19/16 03:10
FJB
SW8260B
Chloroform
<0.125
ug/L
11/19/16 03:10
FJB
SW8260B
Chloromethane
<0.500
ug/L
11/19/16 03:10
FJB
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/19/16 03:10
FJB
SW8260B
Dibromomethane
<0.250
u9/1.
11/19/16 03:10
FJB
SW8260B
Microbac Laboratories, Inc.
Page 32 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose 1HII Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
M/We1114A, grab
K6K0371-11
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac Laboratories, Inc. - Ohio Valley
Dichlorodifluoromethane
<0.250
Ethylbenzene
<0.250
Hexachlorobutadiene
<0.250
Isopropylbenzene
<0.250
m -,p -Xylene
<0.500
Methylene chloride
<0.250
Naphthalene
<0.200
n-Butylbenzene
<0.250
n-Propylbenzene
<0.125
o -Xylene
<0.250
p-Isopropyltoluene
<0.250
sec-Butylbenzene
<0.250
Styrene
<0.125
tert-Butylbenzene
<0.250
Tetrachloroethene
<0.250
Toluene
<0.250
trans-1,2-Dichloroethene
<0.250
trans-1,3-Dichloropropene
<0.500
Trichloroethene
<0.250
Trichlorofluoromethane
<0.250
Vinyl acetate
<2.50
Vinyl chloride
<0.250
Surrogate: 1,2-Dichloroethane-d4
99.7%
Surrogate: 4 BromoJluorobenzene
103%
Surrogate: DibromoJluoromethane
101%
Surrogate: Toluene -d8
99.3%
Total Organic Carbon
6.48
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
ug/L
11/19/16 03:10
FJB
SW8260B
80%-120%
11/19/16 03:10
FJB
SW8260B
86%-115%
11/19/16 03:10
FJB
SW8260B
86%-118%
11/19/16 03:10
FJB
SW8260B
88%-110%
11/19/16 03:10
FJB
SW8260B
mg/L
11/21/16 14:53
DCM
E415.1
Trip Blank
K6K0371-12
Microbac Laboratories, Inc.
Page 33 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.mlcrobac.com

Valley Protein - Rose MR Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
1,1,1,2 -Tetrachloroethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,1,1 -Trichloroethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,1,2,2 -Tetrachloroethane
<0.200
ug/L
11/18/16 22:50
FJB
SW8260B
1,1,2 -Trichloroethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,1-Dichloroethane
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B 4
1,1-Dichloroethene
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
1, 1 -Dichloropropene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,2,3-Tichlorobenzene
<0.150
ug/L
11/18/16 22:50
FJB
SW8260B
1,2,3-Trichloropropane
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
1,2,4-Tichlorobenzene
<0.200
ug/L
11/18/16 22:50
FJB
SW8260B
1,2,4-Trimethylbenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,2-Dibromo-3-chloropropane
<1.00
ug/L
11/18/16 22:50
FJB
SW8260B
1,2-Dibromoethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,2 -Dichlorobenzene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
1,2-Dichloroethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,2-Dichloropropane
<0.200
ug/L
11/18/16 22:50
FJB
SW8260B
1,3,5-Trimethylbenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,3 -Dichlorobenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
1,3-Dichloropropane
<0.200
ug/L
11/18/16 22:50
FJB
SW8260B
1,4 -Dichlorobenzene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
2,2-Dichloropropane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
2-Butanone
<2.50
ug/L
11/18/16 22:50
FJB
SW8260B
2-Chloroethyl vinyl ether
<2.00
ug/L
11/18/16 22:50
FJB
SW8260B
2-Chlorotoluene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
2-Hexanone
<2.50
ug/L
11/18/16 22:50
FJB
SW8260B
4-Chlorotoluene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
4-Methyl-2-pentanone
<2.50
ug/L
11/18/16 22:50
FJB
SW8260B
Acetone
10.2
ug/L
11/18/16 22:50
FJB
SW8260B
Benzene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
Bromobenzene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
Bromochloromethane
<0.200
ug/L
11/18/16 22:50
FJB
SW8260B
Bromodichloromethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Bromoform
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
Microbac Laboratories, Inc.
Page 34 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 910.864.1920 p 1910.864.8774 f I www.microbac.com

Valley Protein - Rose 1UII Plant
Mr. Matthew Haynes
469 Yellow Cut Road
Rose Hill NC, 28458
Fayetteville Division
Certificate of Analysis
Project: M/Well Samples - Nov
Date Reported: 12/27/16
Date Received: 11/09/16
Date Sampled: 11/09/16
Sampled By: Poythress
Trip Blank
K6K0371-12
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
Bromomethane
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
Carbon disulfide
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
Carbon tetrachloride
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Chlorobenzene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
Chlorodibromomethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Chloroethane
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
Chloroform
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
Chloromethane
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
cis-1,2-Dichloroethene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
cis-1,3-Dichloropropene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Dibromomethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Dichlorodifluoromethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Ethylbenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Hexachlorobutadiene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Isopropylbenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
m -,p -Xylene
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
Methylene chloride
0.727
ug/L
11/18/16 22:50
FJB
SW8260B
Naphthalene
<0.200
ug/L
11/18/16 22:50
FJB
SW8260B
n-Butylbenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
n-Propylbenzene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
o -Xylene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
p-Isopropyltoluene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
sec-Butylbenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Styrene
<0.125
ug/L
11/18/16 22:50
FJB
SW8260B
tert-Butylbenzene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Tetrachloroethene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Toluene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
trans-1,2-Dichloroethene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
trans-1,3-Dichloropropene
<0.500
ug/L
11/18/16 22:50
FJB
SW8260B
Trichloroethene
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
J
Microbac Laboratories, Inc.
Page 35 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

Fayetteville Division
Certificate of Analysis
Valley Protein - Rose HIIl Plant Date Reported: 12/27/16
Mr. Matthew Haynes Project: M/Well Samples - Nov Date Received: 11/09/16
469 Yellow Cut Road Date Sampled: 11/09/16
Rose Hill NC, 28458 Sampled By: Poythress
Trip Blank
K6K0371-12
Analyte
Result
Units
Analyzed
Analyzed By
Method
Qualifier
Analyzed by: Mivobac Laboratories, Inc - Ohio Valley
Trichlorofluoromethane
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Vinyl acetate
<2.50
ug/L
11/18/16 22:50
FJB
SW8260B
Vinyl chloride
<0.250
ug/L
11/18/16 22:50
FJB
SW8260B
Surrogate: 1,2-Dichloroethane-d4
99.7%
80%-120%
11/18/16 22:50
FJB
SW8260B
Surrogate: 4-Bromofluorobenzene
105%
86Yoo -115%
11/18/16 22:50
FJB
SW8260B
Surrogate: Dibromq/luoromethane
100%
86516-118%
11/18/16 22:50
FJB
SW8260B
Surrogate: Toluene -d8
99.9%
88%-110%
11/18116 22:50
FJB
SW8260B
QC Batch Run - (Microbac Laboratories, Inc - Fayetteville)
Analyte
Result
Units
Source
RPD
Limit
Sodium
1040
mg/L
K6K0732
2
200
Sodium
5.02
mg/L
0050368
0.9
200
Sodium
4.94
mg/L
0049891
2
200
Phosphorus, Total
ND
mg/L
K6K0371
10
Sodium
4.90
mg/L
0049991
2
200
Phosphorus, Total
1.7
mg/L
K6K0295
0.2
10
Phosphorus, Total
0.014
mg/L
K6K0447
42
10
Sodium
5.15
mg/L
K6K0455
12
200
Sulfate as SO4
ND
mg/L
K6K0409
10
Ammonia as N
ND
mg/L
K6K0447
20
Sulfate as SO4
20.1
mg/L
K6K0389
6
10
Sulfate as SO4
17.6
mg/L
K6K0459
8
10
Sulfate as SO4
100
mg/L
K6K0371
1
10
Sodium
11.0
mg/L
K6K0455
3
200
Sodium
1000
mg/L
K6K0732
4
200
Total Dissolved Solids
242
mg/L
K6K0327
4
5
Total Dissolved Solids
122
mg/L
K6K0327
61
5
Sodium
63.3
mg/L
K6K0447
200
Microbac Laboratories, Inc.
Page 36 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

O ICR BAS°
Fayetteville Division
Certificate of Analysis
Valley Protein - Rose Hill Plant Date Reported: 12/27/16
Mr. Matthew Haynes Project: M/Well Samples - Nov Date Received: 11/09/16
469 Yellow Cut Road Date Sampled: 11/09/16
Rose Hill NC, 28458 Sampled By: Poythress
QC Batch Run - (Microbac Laboratories, Inc. - Fayetteville)
Analyte
Result
Units
Source
RPD
Limit
Chloride
212
mg/L
K6K0371
2
10
Ammonia as N
ND
mg/L
K6K0371
20
Chloride
44.6
mg/L
K6K0389
0.4
10
Ammonia as N
ND
mg/L
K6K0470
20
Ammonia as N
ND
mg/L
K6K0389
20
Chloride
320
mg/L
K6K0409
0.1
10
Phosphorus, Total
0.042
mg/L
K6K0350
26
10
Nitrate as N
0.118
mg/L
K6K0459
34
200
Nitrate as N
ND
mg/L
K6K0409
200
Chloride
18.6
mg/L
K6K0459
2
10
Nitrate as N
1.91
mg/L
K6K0371
111
200
Nitrate as N
6.41
mg/L
K6K0389
3
200
QC Batch Run - (Microbac Laboratories, Inc - Ohio Valley)
Analyte Result Units Source RPD Limit
Report amended on December 26, 2016 for work order K6K0371 that was originally reported on December 7, 2016 to correct M/Well #4 water
measurements.
Report amended on December 27, 2016 for work order K6K0371 that was originally reported on December 7, 2016 to correct all water depth to and from
measurements.
Notes and Definitions
U Not detected at or above adjusted sample detection limit
J The analyte was positively identified, but the quantitation was below the RL
Al2 MS/MSD fail recovery, but the LCS passes criteria.
• [Undefined]
State Certifications:
NCDNR #11
NCDOH #37714
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Thank you for your business. We invite your feedback on our level ofservice to you. Please contact the Division Manager, Rob Dermer at 910-864-1920 with any
questions. You may also contact J. Trevor Boyce, President atpresident@,microbac.com
Microbac Laboratories, Inc.
Page 37 of 40
2592 Hope Mills Road I Fayetteville, NC 28306 1910.864.1920 p 1910.864.8774 f I www.microbac.com

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I Page 40 of 40