NC0003298_Dioxin Monitoring Study_20170103

INTERNATIONAL PAPER
December 29, 2016
Certified Mail: 7015 0640 0001 0270 0610
Mr. Jay Sauber
Chief, Environmental Sciences Section
NC DEQ Division of Water Quality
1621 Mail Service Center
Raleigh, NC 27699-1621
RIEGELWOOD MILL
JOHN L. RIEGEL ROAD
RIEGELWOOD, NC 28456
JAN 0 3 2017
Water Quality
Permitting Section
SUBJECT: Dioxin Monitoring Study of Fish Tissue from the Cape Fear River in the Vicinity of the
International Paper Company Mill at Riegelwood, NC — 2016 Report
NPDES Permit No. NC0003298
Dear Mr. Sauber:
Please find enclosed the 2016 annual report for fish tissue dioxin monitoring conducted on the Cape
Fear River in the vicinity of International Paper's Riegelwood Mill.
If you have questions or need additional information, please call our Environmental Engineer, Emily
Gelder, at 910/362-3476.
Sincerely,
�,�� t�✓lh�v, l�
G ry M row
Environmental, Health, Safety & Sustainability Manager
Enclosure
cc: James H. Gregson, Surface Water Protection Supervisor
NC DEQ — Wilmington Regional Office
127 Cardinal Drive Extension'
Wilmington, NC 28405
Tom Belnick, NPDES Unit Supervisor
NC DEQ Division of Water Quality
1617 Mail Service Center
Raleigh, NC 27699-1617
ehg
S:\Groups\Environmental\Wastewater\Fish Tissue\2016\Annual Fish Tissue Dioxin Report -2016.docx

December 29, 2016
Page 2 of 2
Danny Staley
NC DHHS, Division of Public Health
1931 Mail Service Center
Raleigh, NC 27699-1931
Tom Tharrington
NC DEQ — Wilmington Regional Office
127 Cardinal Drive Extension
Wilmington, NC 28405
ehg
S:\Groups\Environmental\Wastewater\Fish Tissue\2016\Annual Fish Tissue Dioxin Report -2016.docx

RECEIV DINCCENWR
JAN 0 3 2017
Water Quality
Permitting section
DIOXIN MONITORING STUDY OF FISH TISSUE
FROM THE CAPE FEAR RIVER IN THE VICINITY OF
THE INTERNATIONAL PAPER COMPANY MILL
AT RIEGELWOOD, NORTH CAROLINA
2016 REPORT
Prepared for
International Paper Company
Riegelwood Mill
John L. Riegel Road
Riegelwood, North Carolina 28456
Prepared by
CZR Incorporated
4709 College Acres Drive, Suite 2
Wilmington, North Carolina 28403
December 2016

X"
DIOXIN MONITORING STUDY OF FISH TISSUE
FROM THE CAPE FEAR RIVER IN THE VICINITY OF
THE INTERNATIONAL PAPER COMPANY MILL
AT RIEGELWOOD, NORTH CAROLINA
TABLE OF CONTENTS
Page
TABLEOF CONTENTS...................................................................................................ii
LISTOF TABLES............................................................................................................iii
LISTOF FIGURES..........................................................................................................iii
LISTOF APPENDICES................................................................................................... iii
-= 1.0 INTRODUCTION.................................................................................................. 1
2.0 METHODS............................................................................................................2
2.1 Sampling Stations........................................................... 2
. ..........................
2.2 Species Selection
2.3 Sample Collection Methodology 8
2.4 Sample Preparation aration and Shipment 11
' p p p
2.5 Chemical Analysis.................................................................................... 12
3.0 RESULTS AND DISCUSSION........................................................................... 13
3.1 Fish Collection......................................................................................... 13
3.2 Tissue Analyses....................................................................................... 13
REFERENCES.............................................................................................................. 22
ii

LIST OF TABLES
Table Page
2-1 Water quality parameters measured in Cape Fear River sampling during
2016 fish collections in association with International Paper, Riegelwood, NC .... 7
2-2 Collection dates, techniques, effort, and fish captured in Cape Fear River fish
_ collections during 2016 in association with International Paper, Riegelwood,
NC........................................................................................................................ 9
3-1 Summary of 2016 fish composites retained from three Cape Fear River
stations in the vicinity of the International Paper Company Mill at Riegelwood,
NC...................................................................................................................... 15
3-2 Fish composite data for three Cape Fear River stations in the vicinity of the
International Paper Company Mill at Riegelwood, NC, collected during 2016.... 19
3-3 Summary of analytical results from fish tissue composites collected in the
Cape Fear River near the International Paper Company Mill at Riegelwood,
NC, during 2016................................................................................................. 20
3-4 Comparison of dioxin (2,3,7,8-TCDD) concentrations among gamefish and
bottom feeder composites from the Cape Fear River from 1992 to 2016 ........... 21
LIST OF FIGURES
Figure Page
2-1 Sampling Stations'— Sites of Fish Collection on the Cape Fear River near
Riegelwood, NC.................................................................................................... 3
2-2 Sampling Station 1 -- Site of Fish Collection on the Cape Fear River near
Riegelwood, NC....................................................................................................4
2-3 Sampling Station 2 -- Site of Fish Collection on the Cape Fear River near
Riegelwood, NC.................................................................................................... 5
2-4 Sampling Station 3 -- Site of Fish Collection on the Cape Fear River near
Riegelwood, NC.................................................................................................... 6
LIST OF APPENDICES
APPENDIX A: DIOXIN MONITORING STRATEGY
APPENDIX B: NORTH CAROLINA SCIENTIFIC COLLECTION PERMITS
APPENDIX C: LETTER OF TRANSMITTAL/CHAIN OF CUSTODY
APPENDIX D: TOTAL TEQ (WHO TEFS) / SGS LEVEL 11 ANALYTICAL LAB REPORTS

1.0 INTRODUCTION
International Paper Company's (International Paper) NPDES permit (No.
NC0003298) for the Riegelwood mill requires the collection and analysis of fish tissue for
the presence of dioxins and furans. The mill is located along the Cape Fear River near
Riegelwood, Columbus County, North Carolina. The dioxin monitoring program is
administered by the North Carolina Division of Water Resources (DWR), formerly the
Division of Water Quality. International Paper contracted CZR Incorporated (CZR) to
collect fish samples during 2016. To maintain report consistency, the format and style of
this report are similar to CZR Incorporated's past monitoring reports (1993 through 2015
Dioxin Monitoring Study of Fish Tissue from the Cape Fear River in the Vicinity of the
Federal Paper Board's Mill at Riegelwood, North Carolina) which were modeled and
derived from the September 1992 report (EA Report No. 12347.01) titled "Dioxin Monitoring
Study of Fish Tissue from the Cape Fear River in the Vicinity of Federal Paper's
Riegelwood, North Carolina Mill" prepared by EA Engineering, Science, and Technology,
Inc.
Monitoring protocols were established in September 1990 to comply with the Special
Order by Consent (SOC) EMC WQ No. 84-30 AD II effective 12 July 1990. The protocols
comply with both the NPDES permit and the SOC. The following sections discuss sampling
stations, sample collection techniques, sample preparation, and analytical results.
1

2.0 METHODS
2.1 Samplinq Stations
Fish collections occurred in the sampling areas established from previous studies
(EA Engineering, Science, and Technology, Inc., 1992). Sampling stations were originally
-� selected as required by the current NPDES permit and SOC. North Carolina's current
DWR fish tissue dioxin monitoring strategy for the Riegelwood mill is provided in Appendix
A. One station was located upstream of the mill's discharge and the remaining stations
were located downstream of the mill (Figure 2-1).
Station 1 is approximately 11 miles upstream of Lock & Dam No. 1 in the vicinity of
Elwell's Ferry (SR 1730). This station is a control site located approximately 20 miles
upstream of the mill outfall and separated from the mill by a physical barrier, Lock & Dam
No. 1 (Figure 2-2). Station 2 is approximately 2 miles downstream of the mill discharge
near Green Bank Landing (Figure 2-3). Station 3 is approximately 13 miles downstream of
the mill discharge near the confluence of the Cape Fear River and the Black River (Figure
2-4).
Generally, fish habitat was sparse and varied among the three sampling stations.
The available fish habitat consisted of inundated tree roots, aquatic macrophytes,
overhanging riparian vegetation, snags, and fallen timber. Physicochemical measurements
taken in conjunction with fish collections at each sampling station are found in Table 2-1.
2

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DATE: 12/09/08 1 FILE: 1340 -SP1
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DATE: 12/09/08 1 FILE: 1340 -SP1
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Table 2-1. Water quality parameters measured in Cape Fear River sampling during 2016 fish collections in association with
International Paper, Riegelwood, NC. ,
Sampling
Temp
DO
Station
Date
Time
(°C)
DO%
(mg/L)
Cond(gS)
SpCond(µS)
Salinity(psu)
Secchi(in)
pH
1
20 -Sept -16
1120
26.6
55.7
4.42
118.2
114.4
0.05
31.50
5.48
1
21 -Sept -16
1035
25.9
51.6
4.20
110.1
108.2
0.05
23.50
5.89
2
20 -Sept -16
1530
26.4
46.9
3.77
133.6
130.1
0.06
28.25
6.04
2
21 -Sept -16
1350
26.4
50.8
4.09
129.7
126.4
0.06
27.50
6.01
2
1 -Nov -16
1145
19.1
74.6
6.90
170.0
192.0
0.09
26.50
5.79
2
2 -Nov -16
1630
19.7
84.6
7.72
111.8
125.3
0.06
24.00
5.43
2
3 -Nov -16
1430
19.9
81.5
7.41
96.0
106.4
0.05
35.50
5.37
3
1 -Nov -16
1545
19.6
56.3
5.13
100.9
112.5
0.05
25.50
5.89
3
2 -Nov -16
1330
18.7
58.8
5.49
95.1
108.2
0.05
24.00
5.51
3
3 -Nov -16
1145
19.5
74.0
6.77
123.7
138.5
0.06
21.00
5.72
3
7 -Nov -16
1645
19.0
71.1
6.58
121.2
127.9
0.06
11.00
5.68

V . 2.2 Species Selection
The goal of the fish collection effort was to obtain four composite samples at each
sampling location with each sample consisting of ten individuals of the same species and of
similar length and weight. Larger (adult) specimens were given preference. Composites at
each station were composed of gamefish and bottom feeding species fillets. Target
species listed in the state's dioxin strategy include:
• one composite sample for largemouth bass with sunfish (bluegill, redbreast,
etc.) as fallback species;
• one composite sample for bluegill with other sunfish (redbreast, redear, etc.)
as fallback species;
• one composite sample for catfish (order of preference being flathead,
channel, blue, and others) or carp;
• one composite sample for catfish (order of preference being flathead,
channel, blue, or others with fallback species as edible finfish).
2.3 Sample Collection Methodology
Various active and passive methods of fish collection were used to obtain target
species. Fish were collected under scientific fish collecting Permit Number SECP-707778
j (North Carolina Division of Marine Fisheries) and License Number 15-SFC00004 (North
Carolina Wildlife Resources Commission) (Appendix B). Gill nets (flounder nets; 5.50 -inch
mesh x 20 mesh x 50 or 100 yards and 5.75 -inch mesh x 15 mesh x 50 or 100 yards), trot
lines, and hook and line fishing were primarily used to collect fish. Descriptions of effort
and gear types used are given in Table 2-2.
1.1

Table 2-2. Collection dates, techniques, effort, and fish captured in Cape Fear River fish collections during 2016 in association with International Paper,
Riegelwood, NC. See Figures 1 through 3 for site/station locations.
Sampling
Station Date Gear Level of Effort Catch
1
20 September 2016
Hook & line
1.50 hour
10 bluegill, 1 channel catfish
Trot line
2 lines — 50 hooks
1 flathead catfish (released — too small)
Gill net
8 nets overnight — 400 yards
15 blue catfish, 1 flathead catfish, 1 channel catfish, 3 common carp
1
21 September 2016
Hook & line
1.50 hour
11 bluegill, 1 channel catfish
Trot line
2 lines — 50 hooks
1 channel catfish
Gill net
4 nets overnight — 200 yards
8 blue catfish, 3 common carp
2
20 September 2016
Hook & line
0.75 hour
4 bluegill
co 2
21 September 2016
Hook & line
0.75 hour
5 bluegill, 1 channel catfish
Trot line
2 lines — 50 hooks
1 channel catfish
Gill net
3 nets overnight — 200 yards
5 blue catfish, 6 common carp, 1 flathead catfish
2
1 November 2016
Hook & line
1.25 hour
0 fish
Trot line
2 lines — 50 hooks
2 blue catfish, 1 channel catfish
Gill net
4 nets overnight — 200 yards
4 blue catfish, 1 channel catfish, 8 common carp
2
2 November 2016
Hook & line
1.75 hour
4 bluegill
2
3 November 2016
Hook & line
1.00 hour
2 bluegill
Gill net
2 nets overnight —100 yards
2 blue catfish, 7 common carp (released)

Table 2-2. (Concluded).
Sampling
Station Date Gear Level of Effort Catch
3
31 October 2016
Hook & line
0.50 hour
0 fish
3
1 November 2016
Hook & line
1.50 hour
1 bluegill
Trot line
2 lines — 50 hooks
3 blue catfish
Gill net
4 nets overnight — 200 yards
6 blue catfish, 7 common carp, 1 grass carp (released)
3
2 November 2016
Hook & line
1.50 hour
4 bluegill
Gill net
6 nets overnight — 300 yards
7 blue catfish, 7 common carp (1 released), 1 grass carp (released)
3
3 November 2016
Hook & Line
1.25 hour
0 fish
Gill net
4 nets overnight — 200 yards
2 blue catfish, 2 common carp (released), 1 flathead catfish
3
7 November 2016
Hook & Line
1.75 hour
1 bluegill
0

2.4 Sample Preparation and Shipment
Collected fish were descaled or skinned, filleted, and preserved by CZR. SGS
Environmental Services (5500 Business Drive, Wilmington, North Carolina 28405) was
responsible for final sample preparation (i.e., homogenization) and chemical analysis. To
prevent cross -contamination between stations and composites, all equipment used to
handle fish (excluding nets) was solvent rinsed with pesticide -grade acetone and hexane
and when applicable, wrapped with aluminum foil (e.g., measuring boards and scale pans)
which was changed between composites. Fish from different stations were held in
separate coolers and disposable latex gloves were worn and frequently changed when
handling fish during each phase of sample preparation.
As fish were collected, they were placed on wet ice until processing. Fish were
filleted with knives on cutting boards wrapped with aluminum foil (dull side up). Cutting
board wraps were changed and fillet knives were solvent rinsed between composites. Fillet
samples consisted of flesh from both sides of each specimen, including the skin (for
gamefish) but not the scales. Catfish and carp specimens were skinned. Samples were
wrapped in aluminum foil (dull side toward the fish) to shield it from light and were labeled
with sample location, species, and date of collection. All labeled samples making up a
single composite were placed in individual plastic "zip -lock" bags, then all composite
sample bags were sealed inside a larger bag for each station. Samples were frozen to
await delivery to the laboratory for analysis.
On 10 November 2016, the frozen samples were hand -delivered to SGS
Environmental Services in Wilmington, North Carolina, in coolers packed with ice. A copy
of the letter of transmittal/chain of custody that accompanied samples is included in
Appendix C.
11

2.5 Chemical Analysis
SGS Environmental Services performed the chemical extraction and analyses in
accordance with EPA Method 1613B using high-resolution chromatography/high-resolution
mass spectrometry for detecting the presence of 2,3,7,8- tetrachlorodibenzo-p-dioxin
(TCDD) and 2,3,7,8-tetrach lori nated i benzofu ran (TCDF). Additionally, analyses of all 17 of
the dioxin and furan congeners that are substituted with chlorine at the 2,3,7, and 8
positions were performed.
All summary results were reported as 2,3,7,8-TCDD; 2,3,7,8-TCDF; and dioxin
toxicity equivalents (TEQs). TEQs were calculated using 17 of the 2,3,7,8 -chlorine
substituted dioxin and furan congeners using the 2005 World Health Organization (WHO)
toxicity equivalent factors (TEFs) for mammals (Total TEQ WHO TEFs) (Van den Berg et
al., 2006). Congener concentrations reported as non -detect were entered as zero in the
calculation of all TEQ values. Congeners reported as estimated maximum possible
concentrations (EMPC) were not included in calculations of total TEQs. Total extractable
lipid content was also determined for each composite sample. A composite sample of blue
catfish from Station 1 was designated for duplicate laboratory analysis. A quantity sufficient
for re -extraction of each composite sample (where available) was retained and will be held
frozen for a period of 30 days at the lab following the analysis. Duplicate samples will be
held at CZR for three months following the completion of this report.
12

3.0 RESULTS AND DISCUSSION
3.1 Fish Collection
A summary description of the 2016 fish composites is found in Table 3-1. Gamefish
and bottom feeder target species were collected from each of the three stations. Gamefish
or water -column feeding species submitted for analysis included bluegill (Lepomis
macrochirus) from Stations 1, 2, and 3. Bottom feeder species submitted for analysis
included blue catfish (lctalurus furcatus) and common carp (Cyprinus carpio) from Stations
1, 2, and 3. Sample composites with calculated average total fish lengths and weights are
found in Table 3-2.
3.2 Tissue Analyses
Dioxin (TCDD) concentrations (all reported in parts per trillion — ppt) in 2016 were
detected in only 2 of 13 composite samples, neither exceeding 0.20 ppt (Table 3-3). The
highest concentration of dioxin detected was 0.19 ppt found in common carp composite
number 4 (composite of 6 individuals) at reference Station 1. The only other concentration
detected was an estimated maximum possible concentration of 0.09 ppt found in blue
catfish composite number 10 (composite of 10 individuals), located at Station 3. No dioxin
concentrations were detected from Station 2.
Furan (TCDF) concentrations (all reported in parts per trillion — ppt) in 2016 were
also detected in 2 of 13 composite samples, neither exceeding 0.40 ppt (Table 3-3). Just
as with dioxin, the highest concentration of furan detected was 0.38 ppt found in common
carp composite number 4 (composite of 6 individuals), located at reference Station 1. The
only other concentration detected was 0.34 ppt found in common carp composite number
12 (composite of 10 individuals), located at Station 3. As with dioxin, no furan
concentrations were detected from Station 2.
13

All analytical results for fish tissue composites collected and submitted during 2016
are summarized in Table 3-3. Percent lipid contents ranged from 0.2 (bluegill at both
Stations 1 and 2) to 5.4 (blue catfish from Station 3). Reported TEQs for 2,3,7,8-TCDD/F
only are all below 0.10 ppt. Data for individual congeners (Total TEQ, WHO TEFs) and
laboratory data reports provided by SGS Environmental Services are included in Appendix
D.
The State of North Carolina currently uses a dioxin and furan concentration of 4.00
ppt in issuing an advisory (NCDENR 2013). Total dioxin and furan concentrations below
this amount are considered acceptable by the State of North Carolina. Total TEQ values
for all 17 congeners (using WHO TEFs) in 2016 ranged from 0.00 ppt in all bluegill
composites submitted from Stations 1, 2, and 3 and blue catfish composite number 3 from
Station 1 to 0.81 ppt in blue catfish composite number 7 at Station 2 (Table 3-3). Total
TEQ values for all fish composite samples collected and submitted in 2016 are well below
the state advisory level of 4.00 ppt. Average dioxin concentrations (TCDD) from game and
bottom feeding fish in the vicinity of the Riegelwood Mill have remained relatively low during
the course of annual sampling periods over the last twenty-five years and do not display
any increasing trends in TCDD concentration (Table 3-4).
14

Table 3-1. Summary of 2016 fish composites retained from three Cape Fear River stations in
the vicinity of the International Paper Company Mill at Riegelwood, North Carolina.
Station Composite Species Length
Weight (g) Fillet A (g) Ka
1
1
Bluegill
137
48
6
1.87
1
1
Bluegill
145
50
6
1.64
1
1
Bluegill
145
50
6
1.64
1
1
Bluegill
147
55
9
1.73
1
1
Bluegill
156
60
9
1.58
1
1
Bluegill
146
62
9
1.99
1
1
Bluegill
146
65
6
2.09
1
1
Bluegill
160
65
9
1.59
1
1
Bluegill
156
65
11
1.71
1
1
Bluegill
151
65
9
1.89
1
2
Bluegill
152
68
9
1.94
1
2
Bluegill
151
68
6
1.98
1
2
Bluegill
156
71
11
1.87
1
2
Bluegill
165
85
11
1.89
1
2
Bluegill
165
91
14
2.03
1
2
Bluegill
175
105
14
1.96
1
2
Bluegill
171
110
14
2.20
1
2
Bluegill
180
113
14
1.94
1
2
Bluegill
182
115
17
1.91
1
2
Bluegill
194
130
17
1.78
1
3
Blue catfish
569
2,495
275
1.35
1
3
Blue catfish
577
2,675
300
1.39
1
3
Blue catfish
604
2,800
310
1.27
1
3
Blue catfish
589
2,903
305
1.42
1
3
Blue catfish
599
3,220
340
1.50
1
3
Blue catfish
602
3,243
300
1.49
1
3
Blue catfish
599
3,265
310
1.52
1
3
Blue catfish
617
3,606
415
1.54
1
3
Blue catfish
640
4,000
450
1.53
1
3.
Blue catfish
668
4,300
515
1.44
1
4
Common carp
468
2,150
160
2.10
1
4
Common carp
600
3,719
260
1.72
1
4
Common carp
560
3,810
270
2.17
1
4
Common carp
587
3,856
305
1.91
1
4
Common carp
628
4,050
470
1.64
1
4
Common carp
610
4,100
390
1.81
1
-
Bluegill
213
205
28
2.12
1
-
Blue catfish
465
1,200
110
1.19
1
-
Blue catfish
513
1,633
110
1.21
1
-
Blue catfish
545
1,750
220
1.08
15

Table 3-1.
(continued).
Station
Composite
Species
Length
Weight (g)
Fillet A (g)
Ka
_ 1
-
Blue catfish
551
2,003
210
1.20
1
-
Blue catfish
546
2,200
190
1.35
1
-
Blue catfish
559
2,223
205
1.27
1
-
Blue catfish
681
4,310
420
1.36
1
-
Blue catfish
660
4,475
500
1.56
1
-
Blue catfish
673
4,550
490
1.49
1
-
Blue catfish
675
4,581
490
1.49
1
-
Blue catfish
690
4,650
485
1.42
1
-
Blue catfish
676
4,700
580
1.52
1
-
Blue catfish
706
5,215
570
1.48
1
-
Channel catfish
414
590
90
0.83
1
-
Channel catfish
420
750
100
1.01
1
-
Channel catfish
432
850
125
1.05
1
-
Channel catfish
506
1,170
150
0.90
1
-
Flathead catfish
545
1,995
130
1.23
2
5
Bluegill
149
55
9
1.66
2
5
Bluegill
140
60
11
2.19
2
5
Bluegill
164
74
9
1.68
2
5
Bluegill
160
85
17
2.08
2
5
Bluegill
170
100
26
2.04
2
5
Bluegill
178
116
14
2.06
2
5
Bluegill
188
120
17
1.81
2
5
Bluegill
193
147
17
2.04
2
5
Bluegill
210
150
23
1.62
2
5
Bluegill
172
150
34
2.95
2
6
Bluegill
211
165
23
1.76
2
6
Bluegill
200
180
37
2.25
2
6
Bluegill
200
195
45
2.44
2
6
Bluegill
233
240
31
1.90
2
6
Bluegill
232
250
34
2.00
2
7
Blue catfish
450
1,080
190
1.19
2
7
Blue catfish
585
2,300
255
1.15
2
7
Blue catfish
550
2,500
355
1.50
2
7
Blue catfish
560
2,510
320
1.43
2
7
Blue catfish
570
2,515
325
1.36
2
7
Blue catfish
612
2,800
350
1.22
2
7
Blue catfish
668
4,300
400
1.44
2
7
Blue catfish
650
4,500
630
1.64
2
7
Blue catfish
699
4,700
520
1.38
2
7
Blue catfish
720
4,850
725
1.30
2
8
Common carp
490
2,550
240
2.17
2
8
Common carp
560
2,700
270
1.54
2
8
Common carp
535
2,750
269
1.80
2
8
Common carp
540
3,100
270
1.97
16

Table 3-1. (continued).
Station
Composite
Species
Length
Weight (g)
Fillet A (g)
Ka
2
8
Common carp
550
3,250
445
1.95
2
8
Common carp
550
3,300
255
1.98
2
8
Common carp
634
3,900
335
1.53
2
8
Common carp
660
3,900
297
1.36
2
8
Common carp
670
4,500
625
1.50
2
8
Common carp
570
4,510
420
2.44
2
-
Blue catfish
430
580
100
0.73
2
-
Blue catfish
615
900
340
0.39
2
-
Blue catfish
470
1010
155
0.97
2
-
Channel catfish
404
675
80
1.02
2
-
Channel catfish
420
710
145
0.96
2
-
Channel catfish
492
1,400
135
1.18
2
-
Channel catfish
555
2,500
390
1.46
2
-
Common carp
515
2,300
200
1.68
2
-
Common carp
520
2,350
350
1.67
2
-
Common carp
510
2,520
350
1.90
2
-
Common carp
680
5,900
525
1.88
2
-
Flathead catfish
672
4,550
340
1.50
3
9
Bluegill
170
120
20
2.44
3
9
Bluegill
185
150
11
2.37
3
9
Bluegill
180
160
31
2.74
3
9
Bluegill
208
205
28
2.28
3
9
Bluegill
215
221
65
2.22
3
9
Bluegill
220
260
50
2.44
3
10
Blue catfish
560
2,100
195
1.20
3
10
Blue catfish
560
2,500
310
1.42
3
10
Blue catfish
590
2,520
300
1.23
3
10
Blue catfish
610
3,300
445
1.45
3
10
Blue catfish
640
3,300
553
1.26
3
10
Blue catfish
655
3,525
485
1.25
3
10
Blue catfish
715
3,850
530
1.05
3
10
Blue catfish
645
3,950
510
1.47
3
10
Blue catfish
690
4,000
630
1.22
3
10
Blue catfish
650
4,100
700
1.49
3
11
Blue catfish
695
4,400
700
1.31
3
11
Blue catfish
695
4,550
475
1.36
3
11
Blue catfish
735
5,250
770
1.32
3
11
Blue catfish
745
5,450
885
1.32
3
11
Blue catfish
800
7,910
1,260
1.54
3
12
Common carp
505
2,800
335
2.17
3
12
Common carp
505
2,950
285
2.29
3
12
Common carp
530
3,000
275
2.02
17

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Table 3-2. Fish composite data for three Cape Fear River stations in the vicinity of the International Paper
Company Mill at Riegelwood, North Carolina, collected during 2016.
Station
CompositeNumber
Type a
Species
in
Average
length
Average
Average
G
number
5
215.2
composite
)
weight (g)
weight (g)
1
1
G
Bluegill
10
148.9
58.5
8.0
1
2
G
Bluegill
10
169.1
95.6
13.0
1
3
B
Blue catfish
10
606.4
3,250.7
352 Ob
1
4
B
Common carp
6
576.0
3,614.0
309.0
2 5
G
Bluegill
10
172.4
105.7
18.0
2 6
G
Bluegill
5
215.2
206.0
34.0
2 7
B
Blue catfish
10
606.4
3,205.5
407.0
2 8
B
Common carp
10
576.0
3,446.0
343.0
3
9
G
Bluegill
6
184.7
197.7
34.0
3
10
B
Blue catfish
10
631.5
3,314.5
465.8
3
11
B
Blue catfish
5 -
734.0
5,512.0
818.0
3
12
B
Common carp
10
570.0
3,464.0
347.0
a = Gamefish/water-column feeder; B = Bottom feeder.
bReplicate samples submitted.
19

Table 3-3. Summary of analytical results from fish tissue composites collected in the Cape Fear River near the International Paper Company
Mill at Riegelwood, North Carolina, during 2016. Detailed case narratives of the laboratory results are found in Appendix D.
Notes:
a ± 5% statistical variability.
b Includes Estimated Maximum Possible Concentrations due to ion ratio failure.
C Toxic Equivalent (Total TEQ WHO TEFs) excludes Estimated Maximum Possible Concentrations per EPA Method 1613B.
d Not detected.
6
e Duplicate sample.
f Analyte not displayed on table was detected, but Total TEQ (WHO TEFs) remains less than 0.00 ppt.
9 Estimated Maximum Possible Concentration.
2,3,7,8-TCDD (ppt)
2,3,7,8-TCDF (ppt)
2,3,7,8-
TCDD/F
Total TEQ
Percent
Percent
Percent
WHO TEQ
WHO TEFs
Station
Species Composite (#)
lipid
Concentration
recovery'
Concentration
recoverya
(ppt)b
(ppt),
1
Bluegill (1)
0.2
NDd
59.3
NDd
63.3
0.00
0.00
1
Bluegill (2)
0.4
NDd
73.9
NDd
75.8
0.00
0.00
1
Blue catfish (3)
1.7
NDd
46.6
NDd
48.0
0.00
0.00
1
Common carp (4)
2.8
0.19
49.9
0.38
53.4
0.04
0.66
1
Blue catfish (13)e
1.7
NDd
49.0
NDd
50.4
0.00
0.02
2
Bluegill (5)
0.5
NDd
60.1
NDd
63.1
0.00
0.00
2
Bluegill (6)
0.2
NDd
72.8
NDd
76.9
0.00
0.001
0 2
Blue catfish (7)
2.3
NDd
55.7
NDd
59.3
0.00
0.81
2
Common carp (8)
2.8
NDd
48.3
NDd
48.3
0.00
0.13
3
Bluegill (9)
0.8
NDd
60.3
NDd
62.5
0.00
0.001
3
Blue catfish (10)
5.4
0.099
65.3
NDd
66.1
0.09
0.14
3
Blue catfish (11)
4.0
NDd
55.1
NDd
55.8
0.00
0.36
3
Common carp (12)
2.1
NDd
69.1
0.34
69.2
0.03
0.22
Notes:
a ± 5% statistical variability.
b Includes Estimated Maximum Possible Concentrations due to ion ratio failure.
C Toxic Equivalent (Total TEQ WHO TEFs) excludes Estimated Maximum Possible Concentrations per EPA Method 1613B.
d Not detected.
6
e Duplicate sample.
f Analyte not displayed on table was detected, but Total TEQ (WHO TEFs) remains less than 0.00 ppt.
9 Estimated Maximum Possible Concentration.

N
Table 3-4. Summary of analytical results from fish tissue composites collected in the Cape Fear River near the International Paper Company Mill at
Riegelwood, NC, during 2016. Detailed case narratives of the laboratory results are found in Appendix D.
ND = Not detected; detection limits were not used in calculating average concentrations of 2,3,7,8-TCDD.
aValues represent average of dioxin concentrations and estimated concentrations.
bValues represent average of estimated concentrations.
`Estimated concentration found in replicate.
2,3,7,8-TCDD average concentration (ppt)
Station 1
Station 2
Station 3
Year
Gamefish
Bottom feeder
Gamefish
Bottom feeder
Gamefish
Bottom feeder
1992
0.09
0.15
0.38
2.09
0.35
1.15
1993
0.09a
0.16
0.17b
0.59
0.33
0.38
1994
0.08
ND
0.32
0.2
0.22
0.42
1995
ND
ND
ND
0.21b
ND
ND
1996
ND
ND
ND
0.37b
ND
0.12
1997
ND
0.17b
0.20a
0.25a
ND
0.06b
1998
ND
ND
ND
ND
ND
0.31
1999
ND
0.05b
0.08b
0.17b
ND
0.31b
2000
ND
N D`
0.18b
ND
0.09b
ND
2001
ND
ND`
0.11b
0.19b
0.11b
0.08b
2002
ND
0.26b
ND
0.29b
ND
ND
2003
ND
ND
ND
0.05b
ND
0.63
2004
ND
0.25b
ND
0.14
0.26
0.1
2005
0.23
0.34a
0.12
0.43
0.20
0.26a
2006
0.07b
0.22a
ND
0.24a
ND
0.36a
2007
ND
0.33a
ND
0.15a
ND
0.07b
2008
ND
0.42a
ND
0.11
ND
0.33a
2009
0.42
0.70
0.32
1.13
0.56b
0.49
2010
ND
0.30b
ND
0.29b
0.14b
0.12b
2011
ND
0.10b
ND
0.42
ND
ND
2012
ND
0.18b
ND
0.52a
ND
0.11b
2013
ND
0.11b
ND
0.18a
ND
0.19a
2014
ND
0.12
ND
0.09a
ND
0.07b
2015
0.01b
0.12a
0.01b
0.10a
ND
0.21a
2016
ND
0.08
ND
ND
ND
0.03b
*1992 data were obtained from EA Report No. 12347.01 (EA Engineering, Science, and Technology, Inc., 1992).
ND = Not detected; detection limits were not used in calculating average concentrations of 2,3,7,8-TCDD.
aValues represent average of dioxin concentrations and estimated concentrations.
bValues represent average of estimated concentrations.
`Estimated concentration found in replicate.

REFERENCES
CZR Incorporated. 1993. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of Federal Paper Board's Mill at Riegelwood, North Carolina.
CZR Incorporated.' 1994. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of Federal Paper Board's Mill at Riegelwood, North Carolina.
CZR Incorporated. 1995. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of Federal Paper Board's Mill at Riegelwood, North Carolina.
CZR Incorporated. 1996. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 1997. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 1998. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 1999. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2000. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2001. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2002. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2003. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2004. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
,- Carolina.
CZR Incorporated. 2005. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
} River in the Vicinity of the International Paper Company Mill at Riegelwood, North
=:. Carolina.
22

CZR Incorporated. 2006. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2007. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2008. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2009. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2010. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2011. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2012. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2013. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2014. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
CZR Incorporated. 2015. Dioxin Monitoring Study of Fish Tissue from the Cape Fear
River in the Vicinity of the International Paper Company Mill at Riegelwood, North
Carolina.
EA Engineering, Science, and Technology, Inc. 1992. Dioxin Monitoring Study of Fish
Tissue from the Vicinity of Federal Paper Board Company's Riegelwood Mill.
Prepared for Federal Paper Board Company, Inc., EA Engineering, Science, and
Technology, Inc., Smyrna, Georgia. Report No. 12347.01.
National Council for Air and Stream Improvement (NCASI). 1991. A critical review of the
literature on the bioaccumulation of 2,3,7,8-tetrachlorodibenzo-p-dioxin and furan in
fish. NCASI Tech. Bull. No. 610.
23

NCDENR. 2013. Standard Operating Procedures Fish Tissue Assessments. North
Carolina Department of Environmental and Natural Resources. Division of Water
Resources, Environmental Sciences Section, Intensive Survey Branch. Version 1.2.
Taylor, K., and K. M. Rudo. 1990. Risk Assessment of Dioxin Contaminated Fish.
Division of Epidemiology, NC Department of Environment, Health, and Natural
Resources. Raleigh, North Carolina.
Van den Berg, M. et al. 1998. Toxic Equivalency Factors (TEFs) for PCBs, PCDDs,
PCDFs for Humans and Wildlife. Environmental Health Perspectives 106: 775-792.
Van den Berg, M. et al. 2006. The 2005 World Health Organization Reevaluation of
Human and Mammalian ,Toxic Equivalency Factors for Dioxins and Dioxin -Like
Compounds. Toxicological Sciences 93(2): 223-241.
24

APPENDIX A
DIOXIN MONITORING STRATEGY

Monitoring Strategy for International Paper Company at Riegelwood, North Carolina
Composite Sample Guidance
All fish samples will be composited to maximize the number of sampled individuals and the
potential of sampling contaminated fish. Composite samples will consist of single species,
ideally represented by a maximum of ten individual fish. Composites will be prepared by
combining fillet fish tissue from similar sized individual fish, with a preference for larger fish.
Individual length and weight (metric) will be recorded for each fish and the average weight
and length for composites will be calculated. Whole fish tissue analysis is not required.
Fillets will be prepared by leaving skin on and removing scales for most species, with the
exception of catfish which will be skinned. Individual fish will be identified to species. A
sufficient quantity of each (un -extracted) composite sample will be retained and archived
(frozen) for a period of three months following submission of the final report.
Sample Collections Total laboratory samples to be analyzed = 13 (12 samples and one
duplicate)
Sampling Site 1 - Cape Fear River in the vicinity of SR 1730 Bladen County
Four composite samples will be analyzed for dioxin at this station:
-one composite sample for largemouth bass with sunfish as fallback species,
-one composite sample for bluegill with other sunfish as fallback species
(redbreast, redear, etc.),
-one composite sample for catfish (flatheads, channels, blue, other) or carp,
-one composite sample for catfish (flatheads, channels, blue, other) with
other edible finfish as fallback species.
Sampling Site 2 - Cape Fear River in the vicinity of Bryant Mill Creek
Four composite samples will be analyzed for dioxin at this station:
-one composite sample for largemouth bass with sunfish as fallback species,
-one composite sample for bluegill with other sunfish as fallback species
(redbreast, redear, etc.),
-one composite sample for catfish (flatheads, channels, blue, other) or carp,
-one composite sample for catfish (flatheads, channels, blue, other) with
other edible finfish as fallback species.
Sampling Site 3 - Cape Fear River in the vicinity of confluence with Black River
i►_K

Four composite samples will be analyzed for dioxin at this station:
-one composite sample for largemouth bass with sunfish as fallback species,
-one composite sample for bluegill with other sunfish as fallback species
(redbreast, redear, etc.),
-one composite sample for catfish (flatheads, channels, blue, other) or carp,
-one composite sample for catfish (flatheads, channels, blue, other) with
other edible finfish as fallback species.
Laboratory Analysis and Reporting Procedures
Samples will be analyzed for Dioxin and Furans in accordance with analytical protocols set
out in Appendix C of USEPA/Paper Industry Cooperative Dioxin Screening Study (EPA
440/1-88-025, March 1988) or other equivalent analytical protocol approved by EPA.
Analysis will include the determination of concentrations of 2,3,7,8 TCDD and 2,3,7,8
TCDF. Dioxin analysis will be performed using high resolution Mass Spectrometry as
required by EPA Methods 624, 625, 8290, 1613 or other approved methods.
Required Analysis of Dioxins and Furans
Matrix Compound Quantitative Limits
Fish 2,3,7,8 TCDD 1 part per trillion
Fish 2,3,7,8 TCDF 1 part per trillion
Results will be reported in ppt with a minimum quantitative limit of 1 ppt. Where the
compound is detected at concentrations
estimate of the concentration will be given
noted.
Reports
less than the minimum quantitative limit, an
. If a compound is not detected it will be so
A monitoring report will be submitted that will include:
-sampling locations shown on copies of topographical maps (1:2400);
-analytical methods and procedures with name of laboratory;
-individual specimen description (species, length, weight, condition);
-composite descriptions (species, average length, average weight);
-All results will be reported as 2,3,7,8 TCDD and 2,3,7,8 TCDF in parts per trillion
(ppt).
Monitoring reports (with results) will be sent in triplicate and directed to:
Mr. Steve Tedder
Chief, Water Quality Section
Division of Environmental Management
PO Box 27687
Raleigh, North Carolina 27611
A-2

APPENDIX B
NORTH CAROLINA SCIENTIFIC COLLECTION PERMITS

NORTH
CAROUNa
` ¢csnunus
puYKSdn
Phone: [phone]
Fax: [phone]
PERMITTEE/LICENSEE
Scientific Fish Collecting License
North Carolina Wildlife Resources Commission
Division of Inland Fisheries
MSC 1721
Raleigh, NC 27699-1721
SAMUEL COOPER
CZR, INC
4709 COLLEGE ACRES DRIVE
SUITE 2
WILMINGTON; NC 28403
CZR ircoti,.•
Wilmington, N
AUTHORITY
STATUTES
113-261,113-262, & 113-272.4
PERMIT NUMBER
16SFC00004
EFFECTIVE I EXPIRES
01101/2016 12/31/2016
Conditions and, Authorizations:
Print Date: 04/26/2016
The above licensee is authorized -to, collect the species/organisms by the sampling methods as listed below without
restriction to season, size, or creel limits unless otherwise specified under Special Conditions. These species/organisms
may be collected in the River Basins/Counties listed below. Sampling in Collection -Sensitive Waters is not authorized
under this license unless specified under Special Conditions or allowed through a Commission -issued Endangered Species
Permit. Fora current list of Collection -Sensitive' Waters, see www.ncwildlife.org/Licensing/fishcollection.aspx. The take or
possession of federally or state listed'endangered, threatened, or special concern •species is not authorized under this
license except in conjunction with a valid Endangered Species Permit. The licensee is required to comply with all
requirements and laws specified by the U.S. Fish and Wildlife Service and National Marine Fisheries Service as they
pertain to federally -listed species. For a current list of federally or state listed endangered, threatened, or "Special concern
species, see www.ncNWil8life.org/Licensing/fishcollection.aspx.
SPECIES/ORGANISMS:
Amblyopsidae; Amiidae; Anguillidae; Aphredoderidae; Atherinopsidae; Catostomidae; Centrarchidae; Clupeidae;
Cottidae; Cyprinidae; Elassomatidae; Esocidae; Fundulidae; Ictaluridae; Lepisosteidae; Moronidae; Percidae;
Petromyzontidae; Poeciliidae; Salmonidae; Umbridae
RIVER BASINS/COUNTIES:
CAPE FEAR - Bladen, Brunswick, Columbus, Pender
ROANOKE - Bertie, Martin, Washington
TAR-PAMLICO - Beaufort
SAMPLING METHOD:
Electrofishing, Boat; Net, Dip; Net, Fyke; Net, Gill; Seines; Traps; Trawls; Hook and Line
ASSISTANTS:
SHERRY BANNER, JULIA BERGER; RANDALL PULLEY, LORRIE LALIBERTE BOSWELL, NICHOLAS TUDOR,
AMANDA JOHNSON, ZACH GILSTRAP, MATTHEW MICHEL, BENJAMIN BRINK, TOM FUCIGNA, MARK
WESTENDORFF, ERIC MOTE
SPECIAL CONDITIONS:
DEPUE E
M AY - 9 2016
,CZR Incorporated
Wilmington; NC
This permit/license is non -transferable and expires at midnight on the above specified expiration date.
ISSUED BY:
TITLE:
Chief
16-SFC60004

NORTH Endangered Species Permit
AUTHORITY
AUTHOn
AUTHO
GS 113-331 -113-337
MSO W&
`°""'�'°' North Carolina Wildlife Resources Commission
RULES
License Section
15A NCAC 101.0001 -.0005
Phone: (888),248-6824 1707 Mail Service Center
Fax: [phone] Raleigh, NC 27699-1700
PERMITTEE/LICENSEE
PERMIT NUMBER
16-ES00022
SAMUEL COOPER
EFFECTIVE
EXPIRES
CZR; INC
4709 COLLEGE ACRES DRIVE
01/0112016
12/31/2016
SUITE 2
COUNTY
DISTRICTWILMINGTON,
NC 28403
Type of Permit:
Possession, Survey, Take
Species Authorized:
-Fish, Freshwater
Location Where Authorized Activity May Be Conducted:
STATEWIDE
Conditions and Authorizations:
State -listed Species Only
pECE�VE
MAR 1 7 2016
CZR Incorporated
Wilmington, NC
03/0812016
Authorized for incidental take of state -listed fish species while conducting fish collection activities as a designated -agent of the NC,Wildlife Resources
Commission.
All mortalities must be reported to this office (919)-707-0050 within twenty-four (24) hours; a written report describing the mortality event must be
submitted within five (5) work days to: Division of Wildlife Management/Permits, 1722 Mail Service Center, Raleigh, NC 27699-1722; and all mortalities
must be included in the annual report.
All activities must be supervised' ON-SITE by the permittee, or by an authorized subpermittee as designated by the permit holder. All individuals
conducting activities under this permit must carry a copy of this permit and a letter of authorization while engaged in permitted activities.
Authorized subpermittees: Julia Berger, Sherry Banner, Lome Laliberte Boswell, Randall Pulley, Nicholas Tudor, Amanda Johnson, Zach Gilstrap,
Matthew Michel, Benjamin Brink, Mark Westendorff, Tom Fucigna
All specimens must be retained in the possession of the permittee unless lawfully transferred, released, or destroyed.
A fish collection license is also required from the North Carolina Wildlife Resources Commission, Division of Inland Fisheries.
Possession and transportation of dead specimens is permitted only as authorized by this permit;
Unless specifically authorized by this permit, collected voucher specimens must be deposited in the North Carolina Museum of Natural Sciences,
Raleigh.
Issuance of this permit does not constitute permission to conduct these activities on any public or private lands; Such permission must be obtained
separately from the appropriate landowner or land manager before beginning these authorized activities. This permit, neither directly nor by
Implication, grants right of trespass.
The validity of this permit is conditioned upon strict observance of all applicable local, state, and federal law.
A requested amendment to this permit must be submitted in writing by the permittee any time the permittee name, contact information, species,
location, or permit conditions change.
Failure to meet any of the conditions specified herein constitutes just cause for revocation of the permit or denial of renewal.
II A complete report is due within 15 days of the expiration of this permit. The report must be submitted through the online reporting system
(httos://ncoaws.ora/Daws/). Failure to submit the report may result in the permit not being renewed.
I This permithicense is non -transferable and expires at midnight on the above specified expiration date.
ISSUED BY: TITLE:
r644r"_ L I Permits Supervisor
16-ES00022

North Carolina -Division of Marine Fisheries
Proof of Purchase
UPDATE: Scientific or Educational Collection Permit: Permit Number 707778
j Permit Number : 107778 NC Residency : Sales Outlet: DMF Wilmington Office
1 Permit Year : 2016 Qualifying Product: Terminal Number : MJCHUFFO
Effective Date/Time : 02/18/2016 16:10 Fee : 0.00
Expiration Date/Time : 12/31/2016 23:59 Status : Active
Issue Date/Time : 02/18/2016 16:10 Status Date : 02/18/2016
Permit Holder: 730069 CZR, INC.
Business Type:
Physical Address: 4709 COLLEGE ACRES DRIVE,
Mailing Address
SUITE 2,
WILMINGTON,
NC, 28403
United States
County : New Hanover
County
'Race :
Eyes :
Weight:
Gender:
Date of Birth :
Hair;
Height:
ft. Inches
Home Phone: [phone]
Primary Residence:
NC Prior Names:
'Business Phone : [phone]
Secondary Residence
Fax : [phone]
Ids:
E -Mail : [e-mail]
Business Agent : 730085
COOPER, SAMUEL
Physical Address: 5425 ANDOVER ROAD,
Mailing Address :
WILMINGTON, NC, 28403
United States
County : New Hanover
lRace:
County
Caucasian
Eyes : Brown
Weight:
160
Gender : Male
Date of Birth 03/12/1963 Hair: Brown
Height:
5 ft. 10 inches
Home Phone: [phone]
Primary Residence :
NC Prior Names:
Business Phone, [phone]
Secondary Residence
Fax : [phone]
Ids:
E -Mail : [e-mail]
Contact Information
Contact Person
I Contact Person DOB
Contact Person Telephone #
SAMUEL COOPER
03/12/1963
[phone]
Purpose of Collection
Research
Teaching Specimens
Educational Display (Aquariums)
X� Other (specify)
SECTION 401 WQC MONITORING & DIOXIN SCANS
Collectors - -
Partiei Altid
Name_ _ _
DOB -- - _„
Contact Phone
JULIA K. BERGER�
0210211951,
[phone]
SHERRY BANNER
07/21/1943
[phone]
LORRIE LALIBERTE BOSWELL 06/29/1981
[phone]
RANDALL PULLEY
02/02/1978
[phone]
GEORGE H. CARROLL
06/03/1953
[phone]
CHELSEA MCDOUGALL
07/03/1987
[phone]
NICHOLAS TUDOR
06/23/1989
[phone]
AMANDA JOHNSON
05/02/1986
[phone]
ZACH GILSTRAP
10/07/1986
[phone]
SAM COOPER
03/12/1963
[phone]
MATTHEW J. MICHAEL
01/21/1981
[phone]
DAVID P. CONZONIERI
11/29/1992
[phone]
CHAD R. COLEY
07/24/1969
[phone]
MITCHELL A. MORTON
10/10/1974
[phone]
MATTHEW MICHEL
01/21/1981
[phone]
BENJAMIN BRINK
02/14/1990
[phone]
MARK WESTENDORFF
09/24/1964
[phone]
MARK WESTENDORFF'
09/24/1964
(91,0) 392-9253
DMF Wilmington Office, 127 Cardinal Drive, Wilmington NC., 28405 MARLA CHUF1

North Carolina Division of Marine Fisheries
Proof of Purchase
UPDATE : Scientific or Educational Collection Permit : Permit Number 707778
Permit Number :
707778 NC Residency:
Sales Outlet:
DMF Wilmington Office
Permit Year :
2016 Qualifying Product:
Terminal Number: MJCHUFFO
Effective Date/Time : 02/18/2016 16:10
Fee :
0.00
Expiration Date/Time : 12/31/201623:59 Status :
Active
Issue Date/Time :
02/18/2016 16:10 Status Date :
02/18/2016
Restriction Information
,,Restriction Type:
Gear Code----
Species Group:
Water Body:
RESTRICT TO
Gear Quantity:
Species Quantity:
Gear Units :
Species Size :
Time:
Species Units:
' Start Time:
End Time:
Comments: GEARS OR METHODS: ELECTROFISHING; GILL NETS; FYKE NETS; TROT LINES; DIP NETS; TRAWL; SEINE; HOOK AND LINE; FISH
TRAPS
_
Restriction Type:
Gear Code:
Species Group:
Water Body.
RESTRICT TO
Gear Quantity :
Species Quantity,:
Gear Units:
Species Size
rime:
Species Units
,Start Time:
End Time:
Comments: ALL EXCEPT THOSE LISTED AS ENDANGERED OR THREATENED,
_SPECIES:
.Restriction Type :
Gear Code
Species Group:
Water Body:
RESTRICT TO
Gear Quantity!
Species Quantity ;
0200000000-ALBEMAR
LE SOUND
Gear Umts ,:
Species Sin:
• rime:
Species Units:
.Start Time:
End Time:
'Comments:
Restriction Type :
Gear Code:
Species Group :
Water Body
'RESTRICT TO
Gear Quantity:
Species Quantity ;
Gear Units:
Species Size :
Time:
Species Units
Start Time:
End Time:
'Comments: WATER
BODY: PCS PROJECT AREA II
;Restriction Type :
Gear Code:
Species Group :
Water Body:
RESTRICT TO
Gear Quantity :
Species Quantity;
0535301000 -SCOTT
CREEK
Gear Units ;
Species Size
• rime:
Species Units!
Start Time:
End Time:
•Comments
Restriction Type ;
Gear Code :� "
_ Grou_�
Spccics p---:-,
Water Body:
'RESTRICT TO
Gear Quantity:
Species Quantity,:
0528070201 -BAILEY
CREEK
Gear Units::
Species Size:
rime:
Species Units:
`Start Time:
End Time:
Comments:—
—T_—~ --
• Restriction Type ;
Gear Code . a
Species Group
Water Body:
.RESTRICT TO
Gear Quantity.:
Species Quantity :
0528370000 -SOUTH
CREEK
Gear Units:
Species Size
rime:
Species Units:
-Start Time:
End Time:
Comments:
'Restriction Type ;
Gear Code :
Species Group:
Water Body:
.RESTRICT TO
Gear Quantity':
Species Quantity:
0528370100-TOOLEY
CREEK
Gear Units;
Species Size:
'Time:
Species Units:
"start Time:
End Time:
(Comments:
Type :
Gear Code :
Species Group:
Water Body
,;Restriction
"RESTRICT TO
Gear Quantity:
Species Quantity:
0528360000 -HUDDLES
GUT
Gear Units.:
Species Sin:
.Lime:
Species Units:
Start Time:
End Time:
• Comments:
- DMF Wilmington Office, I27 Cardinal Drive, Wilminglon NC„ 28405 MARLA CHUFF

North Carolina Division of Marine Fisheries
- Proof of Purchase
UPDATE : Scientific or Educational Collection Permit: Permit Number 707778
Permit Number :
707778 NC Residency:
Sales Outlet :
DMF Wilmington Office
Permit Year:
2016 Qualifying Product:
Terminal Number : MJCHUFFO
Effective Doty Time : 02/18/2016 16:10
Fee:
0.00
Expiration Datefrime
: 12/31/2016 23:59 Status : Active
Issue Datefrime :
02/18/2016 16:10 Status Date a 02/18/2016
Restriction Type :
Gear Code:
Species Group
Water Body:
RESTRICT TO
Gear Quantity:
Species Quantity.,
0528370300 -JACKS
CREEK
Gear Units :
Species Size
Time:
Species Units
Start Time:
End Time:
Comments:
,Restriction Type:
Gear Code :
Species Group :
Water Body:
RESTRICT TO
Gear Quantity :
Species Quantity:
0528370201-DRINKWA
TER CREEK
Gear Units :
Species Size
Time:
Species Units
Start Time:
End Time:
Comments;
_
Restriction Type :
Gear Code:
Species Group :
Water Body:
',RESTRICT TO
Gear Quantity:
Species Quantity:
0528370200-JACOBS
CREEK
Gear Units 'r
Species Size
Time:
Species Units:
Start Time:
End Time:
,Comments:
Restriction Type.:
Gear Code :
Species Group :
Water Body:
,RESTRICT TO
Gear Quantity:
Species Quantity :
0528350400 -PORTER
CREEK
Gear Units:
Species Size
Time:
Species Units
,Start Time:
End Time:
Comments:
Restriction Type :
_ _ _
_
Gear Code :
_
Species Group :
Water Body
RESTRICT TO
Gear Quantity :
Species Quantity :
0528063302 -SCOTT
CREEK
Gear Units :
Species Size:
Time:
Species Units
Start Time:
End Time:
Comments:
,Restriction Type :
Gear Code:
Species Group :
Water Body:
RESTRICT TO
Gear Quantity :
Species Quantity :
0528370900 -LITTLE
CREEK
Gear Units :
Species Size:
ime :
Species Units:,
Start Time:
End Time:
Comments:
_
Restriction Type :
Gear Code:
Species Group :
Water Body:
RESTRICT TO
Gear Quantity :
Species Quantity:
0528410101 -DUCK
CREEK
Gear Units :
Species Size:
Time:
Species Units
Start Time:
End Time:
Comments:
Restriction Type:
Gear Code:
Species Group :
Water Body:
RESTRICT TO
Gear Quantity :
Species Quantity :
0205010000 -MUDDY
CREEK
Gear Units :
Species Size
Time:
Species Units
Start Time:
End Timei
Comments:
Restriction Type :
—_-_ Gear Code:
Species Group :
Water Body:
RESTRICT TO
Gear Quantity ;
Species Quantity:
0208000000-CHOWAN
RIVER
Gear Units :
Species Size:
Time:
Species Units :
.Start Time:
End Time:
Comments:
DMF Wilmington Office,l27 Cardinal Drive, Wilmington NC., 28405 MARLA CHUFF

" North Carolina Division of Marine Fisheries
Proof of Purchase
UPDATE : Scientific or Educational Collection Permit : Permit Number 707778
Permit Number : 707778 NC Residency : Sales Outlet : DMF Wilmington Office
Permit Year : 2016 Qualifying Product : Terminal Number: MJCHUFFO
Effective Datefrime ; 02/18/2016 16:10 Fee : 0.00
Expiration Date/Time : 12/31/2016 23:59 Status : Active
Issue Datefrime : 02/18/2016 16:10 Status Date : 02/18/2016
estnctton ype :
Gear Code: " - -
pedes uroup .
Start Time:
RESTRICT TO
Gear Quantity:
Species Quantity:
0528000000-PAMLICO
•
'Restriction Type,*
___....._,._
Gear Code :
RIVER
',RESTRICT TO
Gear Units :
Species Size:
'
•'Time :
Species Size:
Species Units ;
.Start Time:
End Time:
End Time:
Comments:
.Restriction Type :
Gear Code :
_
Species Group :
Water Body :
RESTRICT TO
Gear Quantity :
Species Quantity:
0528010000 -LONG
Species Quantity
Gear Units ;
CREEK
--.Time:
Gear Units ;
Species Size:
!Start Time:
-Time:
Gear Code;:
Species Units
Start Time:
End Time:
Gear Units
'Comments:
_ u _ _� .------
'Restriction Type,*
___....._,._
Gear Code :
Species Group
',RESTRICT TO
Gear Quantity :
Species Quantity:
'
Gear Units t
Species Size:
Time :
Species Units
Start Time:
End Time:
Comments:
;Restriction Type,:,
Gear Code:
Sneeies Groun
Gear Quantity';
Gear Units :
•'Bine
Start Time: End Time:
-Comments: UNNAMED TRIBUTARIES TO
Restriction Type:
Gear Code;:
'ltESTRI[CT TO
Gear Quantity:
'
Gear Units
Time.:
Start Time:
End Time:
,Comments:
Species Group:
Restriction Type:
Gear Code:
.RESTRICT TO
Gear Quantity!
Gear Units ;
Cear Units' -
Species Quantity
Species Size:
Species Units:
BEAUFORT COUNTY,, NC
Spccies�.Grotlp :
Species Quantity:
Species Sizs :
Species Units
Species Group
Species Quantity
Species Size
Time:
Species Units
• Start Time:
End Time:
Comments:
'Restriction Type;:
Gear Code :
Species Group:
RESTRICT TO
Gear Quantity :
Species Quantity
Gear Units ;
Species Size:
-'Time:
Species Units
Start Time:
End Time:
• Comments:
;Restriction Type,:,
Gear Code:
Species Group:
RESTRICT TO
Gear Quantity :
Species Quantity
Gear Units ;
Species Size
--.Time:
Species Units
!Start Time:
End Time:
0528350000 -DURHAM
CREEK
Water Body:
0210020000 -WELCH
CREEK
0210000000-ROANOKE
RIVER
vvaici 13UUy .
1900000000 -CAPE
FEAR RIVER
Water Body :
1201020204-WHITEHU
RST CREEK
____ DMF Wilmington Office, 127 Cardinal Drive, Wilmington NC., 28405 MARLA CHUFF

North Carolina Division of Marine Fisheries
Proof of Purchase
UPDATE : Scientific or Educational Collection Permit : Permit Number 707778
Permit Number: 707778 NC Residency: Sales Outlet: DMF Wilmington Office
Permit Year : 2016 Qualifying Product : Terminal Number,: MJCHUFFO
Effective Date/Time: 02/18/2016 16:10 Fee : 0.00
Expiration Date/Time : 12/3112016 23:59 Status: Active
Issue Date/Time : 02/18/2016 16:10 Status Date : 02/18/2016
r—
Request To Sell?� Authorized to Sell?»�
Issued By: / Issued Date:
' p DMF Wilmington Office, 127 Cardinal Drive, Wilmington NC., 28405 n MARLA CHUFF

APPENDIX C
LETTER OF TRANSMITTAL/CHAIN OF CUSTODY

ood
aZR4709 COLLEGE ACRES DRIVE
SUITE 2
I N C O R P O RA T E D WILMINGTON, NORTH CAROLINA 28403-1725
ENVIRONMENTAL CONSULTANTS TEL [phone]
FAX [phone]
CHAIN OF CUSTODY [e-mail]
TO: SGS Environmental Services
Attn: Amy Boehm
5500 Business Drive
Wilmington, NC 28405
DATE: 10 November- 2016
RE: International Paper Company, Inc., 2016 Annual Fish Project
FROM: Randall L. Pulley
CZR Incorporated, Suite 2
4709 College Acres Drive
Wilmington, NC 28403
[e-mail]
czr-inc.com
TESTS: Analysis of fish tissues for percent lipid (extraction) and 2, 3, 7, 8 TCDD (Dioxin), 2, 3, 7, 8, TCDF
(Furan) with full screen of congeners (Polychlorinated Dibenzodioxins and Polychlorinated Dibenzofurans)
via EPA Method 1613B.
ENCLOSED ITEMS:
Thirteen (13) frozen composite fish tissue (fillets) samples, each fillet wrapped in aluminum foil (dull side toward
fish) and enclosed in labeled "zip -lock" plastic bags. Composites are identified below.
SAMPLE ID #
Composite # Site Species (number of fish fillets)
I 1 BIuegill (10 "A" fillets)
2 1 BIuegill (10 "A" fillets)
3 1 Blue Catfish (10 "A" fillets)
4 1 Common Carp (6 "A" fillets)
5 2 Bluegill (10 "A" fillets)
6 2 Bluegill (5 "A" fillets)
7 2 Blue Catfish (10 "A" fillets)
8 2 Common Carp (10 "A" fillets)
9 3 Bluegill (6 "A" fillets)
10 3 Blue Catfish (10 "A" fillets)
11 3 Blue Catfish (5 "A" fillets)
12 3 Cormrnon Carp (10 "A" fillets)
13 1 Blue Catfish - replicate (10 "B" fillets)
COMMENTS:
- Send one digital version and two hard copies of the report to Sam Cooper/CZR at the above address. We
also request permission to include the report as an appendix to CZR's report summarizing the 2016
collection efforts and results.
- Forward the invoice to International Paper -Riegelwood, Shared Services, P.O. Boz 792, Milford, OH
45150
- A detailed fish composite data table is also enclosed.
Relinquished by: ate/time
Received by.: ' - ! Date/time
CZR CP# 1340.24
2151 Aiterncite AIA South - SUITE 2000 - JUPITER, FLORIDA 33477-3902
TEL [phone] - FAX [phone] - [e-mail] - www.CZRINC.com

APPENDIX D
TOTAL TEQ (WHO TEFS) / SGS LEVEL II ANALYTICAL LAB REPORTS

Table Dl. Congener data (pg/g and TEF TEQ) by sample analyzed for 2016 study. See Figure 2-1 for sampling station locations in the Cape Fear River Values for TEFs are WHO mammalian factors from Van den Berg et al., 2006
Composite
1
2
3
4
5
6
7
8
9
Station
1
1
1
1
2
2
2
2
3
Species
WHO-
BG
BG
BC
CC
BG
BG
BC
CC
BG
Lab
TEF
SGS
SGS
SGS
SGS
SGS
SGS
SGS
SGS
SGS
Units
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
TCDD
2,3,7,8-TCDD
1.0
ND(O.10)
0.00
ND(O.13)
0.00
ND(0.88)
0.00
0.19
0.19
ND(0.23)
0.00
ND(0.19)
0.00
ND(0.29)
0.00
ND(0.37)
000
ND(0.08)
0.00
PeCDD
1,2,3,7,8-PeCDD
10
ND(0.13)
0.00
ND(0.11)
0.00
EMPC(1.06)
1.06
EMPC(0.56)
0.56
ND(O.19)
0.00
ND(0.15)
0.00
0.64
0.64
ND(0.60)
0.00
ND(O10)
0.00
HxCDD
1,2,3,4,7,8-HxCDD
0.1
ND(0.13)
0.00
ND(0.14)
0.00
ND(0 70)
0.00
EMPC(0 50)
0.05
ND(0.20)
0.00
ND(0.16)
0.00
ND(0 28)
0.00
ND(0.51)
0.00
ND(O.11)
0.00
1,2,3,6,7,8-HxCDD
0.1
ND(O.14)
0.00
ND(0.15)
000
ND(0.70)
0.00
0.89
0.09
ND(0.20)
0.00
ND(0.16)
0.00
0.45
0.05
0.75
0.08
ND(O.11)
000
1,2,3,7,8,9-HxCDD
0.1
ND(0.14)
0.00
ND(0 15)
0.00
ND(0.76)
0.00
0.48
005
ND(0 22)
0.00
ND(0.17)
0.00
0.51
0.05
ND(0.55)
0.00
EMPC(0 17)
0.02
HpCDD
1,2,3,4,6,7,8-HpCDD
0.01
ND(O.14)
0.00
ND(0.15)
000
EMPC(2 28)
0.02
4.32
0.04
ND(0.24)
000
ND(0 23)
0.00
1.27
0.01
2.33
0.02
EMPC(0.16)
0.00
OCDD
0.0003
ND(0.27)
0.00
ND(O.20)
0.00
EMPC(9.43)
000
1910
0.01
ND(0.42)
0.00
ND(0.34)
0.00
3.11
0.00
1030
000
1.21
0.00
TCDF
2,3,7,8-TCDF
0.1
ND(0.13)
0.00
ND(O.11)
0.00
ND(0.99)
0.00
0.38
004
ND(0.22)
0.00
ND(0.17)
0.00
ND(0.28)
0.00
ND(0.47)
0.00
ND(0.09)
000
PeCDF
1,2,3,7,8-PeCDF
0.03
ND(O.11)
000
ND(009)
0.00
ND(0.61)
0.00
0.58
0.02
ND(015)
000
ND(O.14)
0.00
ND(0.21)
0.00
0.99
0.03
ND(0.09)
0.00
2,3,4,7,8-PeCDF
0.3
ND(O.11)
0.00
ND(0.09)
0.00
ND(0.55)
0.00
0.53
016
ND(014)
0.00
ND(0.13)
0.00
ND(0.20)
0.00
ND(O.47)
0.00
ND(0.09)
0.00
HxCDF
1,2,3,4,7,8-HxCDF
0.1
ND(O.10)
0.00
ND(O 08)
0.00
ND(0.33)
0.00
0.26
0.03
ND(0.12)
000
ND(0 11)
0.00
0.36
0.04
ND(0.32)
0.00
ND(0.06)
0.00
1,2,3,6,7,8-HxCDF
0.1
ND(0.09)
0.00
ND(0.07)
0.00
ND(0.32)
0.00
040
0.04
ND(0.11)
0.00
ND(0.10)
0.00
0.22
0.02
ND(0.31)
0.00
ND(006)
0.00
1,2,3,7,8,9-HxCDF
0.1
ND(0.10)
0.00
ND(0.08)
0.00
ND(0.33)
0.00
EMPC(0.17)
0.02
ND(0.12)
0.00
ND(O.11)
0.00
ND(0.18)
0.00
ND(0 34)
000
ND(0.06)
0.00
2,3,4,6,7,8-HxCDF
0.1
ND(0.13)
0.00
ND(0.11)
0.00
ND(0.53)
0.00
ND(0.15)
0.00
ND(0.17)
0.00
ND(0.15)
0.00
ND(0.26)
000
ND(0 46)
0.00
ND(0.08)
0.00
HpCDF
1,2,3,4,6,7,8-HpCDF
0.01
ND(0 07)
0.00
ND(0.05)
0.00
ND(0.30)
0.00
0.41
0.00
ND(O.10)
0.00
ND(0.09)
0.00
EMPC(0.22)
0.00
EMPC(0 32)
0.00
ND(0 06)
0.00
1,2,3,4,7,8,9-HpCDF
0.01
ND(0.13)
0.00
ND(0.10)
0.00
ND(0 57)
0.00
ND(0 16)
0.00
ND(0.16)
0.00
ND(0.17)
000
ND(0.30)
0.00
ND(0.50)
0.00
ND(0.10)
0.00
OCDF
0.0003
ND(0 40)
000
ND(0.30)
0.00
ND(1.38)
0.00
0.33
000
ND(0 57)
0.00
0.49
0.00
ND(0.53)
0.00
ND(0.84)
0.00
ND(0.20)
0.00
TOTAL TEQ (EMPC = 0)
0.00
0.00
0.00
0.66
0.00
0.00
0.81
0.13
0.00
TOTAL TEQ (EMPC = EMPC)
0.00
0.00
1.08
1.29
0.00
0.00
0.81
0.13
0.02
Legend/Notes: (BC) blue catfish, (BG) bluegill sunfish, (CC) common carp; ND(Detection Limit) indicates compound not detected; EMPC(Estimated Maximum Possible Concentration) indicates estimated maximum value due to ion ratio failure; Total TEQs exclude Estimated
Maximum possible Concentrations per EPA Method 1613B.

Table Dl. (concluded)
Composite
10
11
12
13
3
3
3
1
Location
BC
BC
CC
BC -replicate
Species WHO-
Lab
TEF
SGS
SGS
SGS
SGS
Units
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
pg/g
TEQ
TCDD
2,3,7,8-TCDD
1.0
EMPC(0.09)
0.09
ND(0.15)
0.00
ND(0.20)
0.00
ND(0.64)
0.00
PeCDD
1,2,3,7,8-PeCDD
1.0
EMPC(0.12)
0.12
EMPC(1.27)
127
EMPC(0.52)
0.52
ND(069)
0.00
HxCDD
1,2,3,4,7,8-HxCDD
0.1
ND(0.16)
0.00
0.35
0.04
ND(0.27)
0.00
ND(0.63)
0.00
1,2,3,6,7,8-HxCDD
0.1
0.37
0.04
0.99
0.10
0.47
0.05
ND(0.68)
0.00
1,2,3,7,8,9-HxCDD
01
0.30
0.03
061
0.06
ND(0.30)
0.00
ND(0.61)
000
HpCDD
1,2,3,4,6,7,8-HpCDD
0.01
EMPC(I.12)
0.01
2.43
0.02
1.79
0.02
2.05
0.02
OCDD
0.0003
493
0.00
8.08
0.00
6.63
0.00
9.12
0.00
TCDF
2,3,7,8-TCDF
0.1
ND(0.12)
0.00
ND(0.19)
0.00
034
0.03
ND(0.56)
0.00
PeCDF
1,2,3,7,8-PeCDF
0.03
ND(0.13)
0.00
ND(0.20)
0.00
0.46
0.01
ND(0.73)
0.00
2,3,4,7,8-PeCDF
0.3
0.25
0.08
041
0.12
0.31
0.09
ND(0.73)
0.00
HxCDF
1,2,3,4,7,8-HxCDF
0.1
ND(0.08)
0.00
0.20
0.02
016
0.02
ND(0.31)
0.00
1,2,3,6,7,8-HxCDF
0.1
ND(0.07)
0.00
ND(0.12)
0.00
EMPC(0.27)
0.03
ND(031)
0.00
1,2,3,7,8,9-HxCDF
0.1
ND(0.07)
0.00
ND(0.13)
0.00
ND(0.14)
0.00
ND(0.32)
0.00
2,3,4,6,7,8-HxCDF
0.1
ND(0.10)
0.00
ND(0.16)
0.00
ND(0.18)
0.00
ND(0.41)
0.00
HpCDF
1,2,3,4,6,7,8-HpCDF
0.01
ND(0.07)
0.00
ND(0.15)
000
ND(0.11)
0.00
ND(0.33)
0.00
1,2,3,4,7,8,9-HpCDF
0.01
ND(O11)
0.00
ND(0.23)
0.00
ND(0.19)
0.00
ND(0.55)
0.00
OCDF
0.0003
0.50
0.00
EMPC(0.35)
0.00
ND(0.45)
0.00
ND(1.48)
000
TOTAL TEQ (EMPC = 0)
0.14
0.36
0.22
0.02
TOTAL TEQ (EMPC = EMPC)
0.36
1.63
0.77
0.02
Legend/Notes: (BC) blue catfish; (BG) bluegill sunfish; (CC) common carp; ND(Detection Limit) indicates compound not detected; EMPC(Estimated Maximum Possible Concentration) indicates estimated maximum value due to ion ratio failure; Total TEQs exclude Estimated
Maximum possible Concentrations per EPA Method 1613B

Prepared by
This report is approved by
Digitally signed by Amy Boehm
Date: 2016.12.06 14:08:18
-05'00'
-------------------
Amy Boehm
Senior Project Manager
FINAL LAB REPORT
2016 Annual Fish Project
A9421
06 -Dec -2016
Prepared for
CZR, Inc.
Sam Cooper
4709 College Acre Drive Suite 2
Wilmington, NC 28403
Phone:[phone]
Email: [e-mail]
tTocument is issue�by�Company under itsGeneral Conditions o ery c� aaccessib a at Attention isdrawn to tffeimd�o
ity,indemnification and jurisdiction issues defined therein.
remains committed to serving you in the most effective manner. Should you have any questions or need additional information and technical support, please do not hesitate to contact us
management and staff of SGS welcomes customer feedback, both positive and negative, as we continually improve our services. Please visit our web site at -,_,_and
on the 'Email Us' link or go to our survey ;. Thank you for choosing SGS.
holder of this document is advised that it is a final submission and supersedes and voids all prior reports with the same report or identification number. The information contained hereon
cts the Company's findings at the time of its intervention only and within the limits of Client's instructions, if any. The Company's sole responsibility in conducting the work herein is to its Client
does not exonerate parties to a transaction from exercising all of their rights and obligations under such applicable transaction documents. This report may be reproduced in full only The
ipany expressly disclaims any and all liability for the Client's use of or reliance upon the data contained herein. Any alteration, forgery or falsification of the content or appearance of this
iment which is not expressly authorized by the Company is unlawful and offenders may be prosecuted to the fullest extent of the law.
Its reported relate only to the items tested.
WO# A9421
Page 1 of 42

f+��l_.-1 (When applicable, see QC Annotations for details)
Client Project
2016 Annual Fish Project
SGS Project #
A9421
Analytical Protocol(s)
1613 PCDD/F
No. Samples Submitted
13 fish composites
Additional QC Sample(s)
0
No. Laboratory Method Blanks
1
No. OPRs / Batch CS3
1
Date Received
10 -Nov -16
Condition Received
Good
Temperature upon Receipt (°C)
-6.5,-11.3
Extraction within Holding Time
Yes
Analysis within Holding Time
Yes
WO# A9421 Page 2 of 42

1. Please see Appendices attached for data qualifier/attribute and lab identifier descriptions which may be contained in the
project.
tiF
r
WO# A9421
Page 3 of 42

B
The analyte was found in the method blank, at a concentration that was at least 10% of the concentration in the
sample.
C
Two or more congeners co -elute. In EDDs, C denotes the lowest IUPAC congener in a co -elution group and
additional co-eluters for the group are shown with the number of the lowest IUPAC co-eluter.
E
The reported concentration exceeds the calibration range (upper point of the calibration curve) and is an estimated
value.
EMPC
Represents an Estimated Maximum Possible Concentration. EMPCs arise in cases where the signal/noise ratio is
not sufficient for peak identification (the determined ion -abundance ratio is outside the allowed theoretical range),
or where there is a co -eluting interference.
H/h
If the standard recovery is below the method or SOP specified value "H" is assigned. If the obtained value is less
than half the specified value "h" is assigned.
J
Indicates that an analyte has a concentration below the reporting limit (lowest point of the calibration curve) and is
an estimated value.
ND
Indicates a non -detect.
NR or R
Indicates a value that is not reportable.
PR
Due to interference, the associated congener is poorly resolved.
QI
Indicates the presence of a quantitative interference.
SI
Denotes "Single Ion Mode" and is utilized for PCBs where the secondary ion trace has a significantly elevated
noise level due to background PFK. Responses for such peaks are calculated using an EMPC approach based
solely on the primary ion area(s) and may be considered estimates.
U
The analyte was not detected. The estimated detection limit (EDL) may be reported for this analyte.
V
The labeled standard recovery was found to be outside of the method control limits.
Page 4 of 6
WO# A9421 Page 4 of 42

i�
,S-GS,
T_
J
The reported result is an estimate. The value is less than the minimum calibration level but greater than the
estimated detection limit (EDL).
U
The analyte was not detected in the sample at the estimated detection limit (EDL).
E
The reported concentration is an estimate. The value exceeds the upper calibration range (upper point of the
calibration curve).
D
Dilution Data. Result was obtained from the analysis of a dilution.
B
Analyte found in the sample and associated method, blank.
C
Co -eluting congener
Cxx
Co -elutes with the indicated congener, data is reported under the lowest IUPAC congener. 'Xx' denotes the
IUPAC number with the lowest numerical designated congener.
NR
Analyte is not reportable because of problems in sample preparation or analysis.
V
Labeled standard recovery is not within method control limits.
X
Results from re-injection/repeat/second-column analysis.
EMPC
Estimated maximum possible concentration. Indicates that a peak is identified but did not meet the method
specified ion -abundance ratio.
AR
Indicates use of the archived portion of the sample extract.
CU
Indicates a sample that required additional clean-up prior to MS injection/processing.
D
Indicates a dilution of the sample extract. The number that follows the "D" indicates the dilution factor.
DE
Indicates a dilution performed with the addition of ES (extraction standard) solution.
DUP
Designation for a duplicate sample.
MS
Designation for a matrix spike.
MSD
Designation for a matrix spike duplicate.
RJ
Indicates a reinjection of the sample extract.
S
Indicates a sample split. The number that follows the "S" indicates the split factor.
Page 5 of 6
WO# A9421 Page 5 of 42

SGS
Arkansas
88-0682
California (ELAP)
ELAP Cert #2914
CLIA
34D1013708
Connecticut
PH -0258
USDA Soil Permit
P330-14-00135
DoD
2726.01
Florida (Primary NELAP)
E87634
ISO 17025/IEC
2726.01
Louisiana
4115
Maine
#2016028
Massachusetts
M-NC919
Minnesota (Primary NELAP For Method 23)
Lab #037-999-459 Cert #981125
New Jersey
NC100
New York
11685
North Carolina DWR
481
North Dakota
R-197
Oregon
NC200002
Pennsylvania
68-03675
South Carolina
Lab #99029 Cert #99029002
Texas
T104704260-16-9
US Coast Guard
16714/159.317/SGS
Virginia
Lab #460214 Cert #8722
Washington
C913
West Virginia
293
Kev. 12 -Sep -2U 1(i
r
l
Page 6 of 6 �;
WO# A9421 Page 6 of 42

A9421 - TEQ
Project ID: 2016 Annual Fish Project
Sample Summary
Method 1613B
Part 1
Method
Comp1
Comp2
Comp3
Comp 4
Comps
CompB
Comp?
Comp 8
Comp9
Comp 10
Comp 11
Comp12
Com 13
Analyte
Blank
Site 1
Site 1
Site 1 Blue
Site 1
Site 2
Site 2
Site 2 Blue
Site 2
Site 3
Site 3 Blue
Site 3 Blue
Site 3
Site 1 Blue
A9421_ 145
Bluegill
Bluegill
Catfish
Common
Bluegill
Bluegill
Catfish
Common
Bluegill
Catfish
Catfish
Common
Catfish-
atfiish -
14
14
Carp
Carp
Carp
Replicate
PgIg
Pg/g
Pg/9
PA
Pg/9
gig
Pg/9
9/9
PgIg
PgIg
PgIg
PA
g/9
PA
2,3,7,8-TCDD
(0.312)
(0.104)
(0.125)
(0.77)
0.192
(0.23)
(0.187)
(0.293)
(0.374)
(0.0844)
[0.0941]
(0.146)
(0201)
(0.637)
1,2,3,7,8-PeCDD
(0.314)
(0.133)
(0.105)
[1.06]
[0.561]
(0.191)
(0.146)
0.644
(0.601)
(0.0954)
[0.115]
[1.27]
[0.524]
(0.685)
1,2,3,4,7,8-HxCDD
(0 23)
(0.129)
(0.142)
(0.698)
[0.5]
(0.199)
(0.155)
(0.28)
(0.509)
(0.113)
(0.158)
0.345
(0.274)
(0.626)
1,2,3,6,7,8-HxCDD
(0.24)
(0.141)
(0.152)
(0.7)
0.891
(0.203)
(0.162)
0.447
0.749
(0.114)
0.371
0.99
0.47
(0.683)
1,2,3,7,8,9-HxCDD
(0.257)
(0.142)
(0.146)
(0.761)
0.475
(0.215)
(0.166)
0.507
(0553)
[0.169]
0.296
0.606
(0.297)
(0.607)
1,2,3,4,6,7,6-HpCDD
(0.339)
(0.139)
(0.151)
[2.28]
4.32
(0.24)
(0.233)
1.27
2.33
[0.162]
[1.12]
2.43
1.79
2.05
OCDD
(0.538)
(0.268)
(0.204)
[9.43]
19.1
(0.418)
(0.344)
3.11
10.3
1.21
4.93
8.08
6.63
9.12
2,3,7,8-TCDF
(0.246)
(0.125)
(0.11)
(0.987)
0.384
(0.219)
(0.173)
(0.283)
(0.473)
(0.0929)
(0.119)
(0.189)
0.343
(0.562)
1,2,3,7,8-PeCDF
(0.171)
(0.108)
(0.0917)
(0.613)
0.583
(0.151)
(0.137)
(0.21)
0.991
(0.0926)
(0.13)
(0.197)
0.46
(0.732)
2,3,4,7,8-PeCDF
(017)
(0.105)
(0.0871)
(0.55)
0.527
(0.142)
(0.127)
(0.199)
(0.471)
(0.0871)
0.246
0.405
0.31
(0.73)
1,2,3,4,7,8-HxCDF
(0.158)
(0.0963)
(0.0768)
(0.327)
0.255
(0.119)
(0.108)
0.356
(0.323)
(0.0639)
(0.0759)
0.198
0.162
(0.305)
1,2,3,6,7,8-HxCDF
(0.147)
(0.0891)
(0.0715)
(0.315)
0.399
(0.112)
(0.0977)
0.224
(0.31)
(0.0556)
(0.0682)
(0.121)
[0.27]
(0.309)
2,3,4,6,7,8-HxCDF
(0.155)
(0.0965)
(0.0773)
(0.326)
[0 172]
(0.123)
(0.106)
(0.178)
(0.335)
(0.061)
(0.0744)
(0.126)
(0137)
(0.32)
1,2,3,7,8,9-HxCDF
(0 216)
(0.126)
(0.107)
(0.529)
(0.146)
(0.17)
(0.149)
(0.255)
(0 459)
(0.0813)
(0.0997)
(0.164)
(0.18)
(0.411)
1,2,3,4,6,7,8-HpCDF
(0.16)
(0.0671)
(0.0539)
(0.301)
0.409
(0.0991)
(0.0903)
[0.223]
[0.319]
(0.0602)
(0.0668)
(0.149)
(0.111)
(0.326)
1,2,3,4,7,8,9-HpCDF
(0.298)
(0.129)
(0.101)
(0.574)
(0.156)
(0.164)
(0.167)
(0.296)
(0.498)
(0.1)
(0.106)
(0.232)
(0.186)
(0.554)
OCDF
(0.55)
(0.397)
(0.297)
(1.38)
0.333
(0.568)
0.488
(0.528)
(0 836)
(0.196)
0 503
[0.347]
(0 446)
(1.48)
WHO -2005 TEO (ND=O; EMPC=O)
0
0
0
0
0.661
0
0.000146
0.811
0.131
0.000363
0.142
0.362
0.224
0.0232
WHO -2005 TEO (ND=O; EMPC=EMPC)
0
0
0
1.08
1.29
0
0.000146
0.814
0.134
0.0189
0.362
1.63
0.775
0.0232
WHO -2005 TEO (ND=DL/2; EMPC=O)
0.428
0.185
0.175
1.16
0.754
0.305
0.246
1.04
0.841
0.141
0.283
0.554
0.486
1
WHO -2005 TEO (ND=Du2; EMPC=EMPC)
0.428
0.185
0.175
1.79
1.3
0.305
0.246
1.04
0.843
0.153
0.395
1.74
0.922
1
WHO -2005 TEO (ND=DL; EMPC=EMPC)
0.855
0.369
0.35
1 2.51
1.31
0.609
0.492
1 1.28
1 1.55
0.287
0.427
1 1.85
1.07
1 1.98
Checkcode
064-609-WZX
682-452-KJR
057-138-RZW
236-631-ZMJ
IA9421_14514DF003
680-894-RPK
860-459-GBW
348-654-SMZ
781-687-PJJ
281-592-WPG
794-649-QKR
740 -406 -GPX
565 -465 -TVR
198-325-JKC
364-936-JBB
Lab ID
--l-4-DF50-
A9421 145140F_001
A9421 14514 DF 002
A 2114514_DF �
A9421 14514 DF 005
A9421 14514 DF 008
M421 14514 DF 00I
A9421 14514_DF OOB
M421 14514DF009
A9421 14514 DF 010
A9421 14514 DF 011
A9421 14514 DF 012
A9421 14514_DF 013
() = DJVO# A9421 Page 7 of 42
[ ] = EMPC

A9421 - Totals
Project ID: 2016 Annual Fish Project
Sample Summary
Method 16136
Part 2
et o
Comp1
Comp2
Comp3
Comp 4
Comps
Compe
Comp?
Comp 8
Comp9
Comp 10
Comp 11
Comp 2
omp
Analyte
Blank
Site 1
Site 1
Site 1 Blue
Site 1
Site 2
Site 2
Site 2 Blue
Site 2
Site 3
Site 3 Blue
Site 3 Blue
Site 3
Site 1 Blue
A9421_145
Bluegill
Bluegill
Catfish
Common
Bluegill
Bluegill
CatFsh
Common
Bluegill
Catfish
Catfish
Common
Catfish -
14
Carp
Caro
Carp
Replicate
P9�9139
P9/9
Pg/g
PgIg
9/g
Pg/9
P9/9
/9
PA
/9
/9
PA
9/
Totals
TCDDs
0
0
0
0
0.192
0
0
0
0
0
0
0.197
0
0
PeCDDs
0
0
0
0
0.336
0
0
0.644
0
0
0
0.216
0
0
HxCDDs
0
0
0
0
1.37
0
0
0.954
0.749
0
0.666
1.94
0.47
0
HpCDDs
0
0
0
0
4.32
0
0
127
2.33
0.543
0
2.43
1.79
2.05
OCDD
0
0
0
0
19.1
0
0
3.11
10.3
1.21
4.93
8.08
6.63
9.12
TCDFs
0
0
0
0
0.988
0
0
0
0
0
0
0
0.343
0.954
PeCDFs
0
0
0
3.03
3.46
0
0
0.888
0.991
0
1.47
1.28
2.16
1.26
HxCDFs
0
0
0
0
1.31
0
0
0.845
0
0
0
0.406
0.162
0
HpCDFs
0
0
0
0
0.577
0
0
0
0
0
0
0
0
0
OCDF
0
0
0
0
0.333
0
0.488
0
0
0
0.503
0
0
0
Total PCDD/Fs (ND=O; EMPC=O)
0
0
0
3.03
32
0
0.488
7.71
14.4
1.75
7.57
14.5
4 x,11.6
13.4
Total PCDD/Fs (ND=O; EMPC=EMPC)
0
0
0
17.2
34.2
0
0.488
8.23
15.3
2.31
9.2
16.9
13.6
13.4
Total PCDD/Fs (2378-XND=DL;EMPC=EMPC)
- 4.5
2.39
2'.1
,..,,28.1.-.,_
34.6,:
�,e�'3.56 P
3.04',
10.8'
- .21.1
3.61
10.1 F.
_ 18.2-
15.5 A
;.22.4
Total 2378s (ND -0; EMPC=0)
0
0
0,
0
27.9
0
0.488
6.56
14.4
1.21
6.34
13
10.2
11.2
Total 23783 (ND=0.5; EMPC=0),
2.25 ,
1.2.
1.05
5.78
28.2
1.78
1.76
7.9
17.4
1.98
6.98
14
11.3
15.7
,Total 2378s (ND=1; EMPC=O)
4.5
2.39
2.1
11.6
28.6
3.58
3.04
9.24
20.4
2.75
7.82
'14.9-
12.3
20.1
Total 2378s(ND=O;EMPC-1)_
0
0
0
12.8
29.1
0
- 0.488
6.78
14.7
1.54
7.88
14.7
91"
11.2
TOtal 23783 (ND=0.5;,EMPC=1)
2.25-
1.2
_
1.05
17.2'
_
29.2
1.78
1.76
` 8.04
17.8
'2.19-
8.13
15.3
11:9
15.7 "
Total 23783 (ND=1; EMPC=1) _
4.5 '
2:39
-2.1
21.6
29.4
3.56 '
3.04 _
9.3
20.4
'2.84
8.57
16
12.8
20.1
Checkcode
064-609-WZX
682-452-KJR
057-138-RZW
236-631-ZMJ
680-894-RPK
860-459-GBW
348-654-SMZ
781-687-PJJ
281-592-WPG
794-649-QKR
740 -406 -GPX
565 -465 -TVR
198-325-J KC
364-936-JBB
Lab ID
- -4.DFSDSAJ2
A9421_14514 -DF 001
A9421 14514 DFJ02
M421 14514DF003
A9121 14514DFro40.1
M421 14514 DF 005
A9421 14514 DF 000
A9421 14514DF007
M421 14514 DF
A9421 14514 DF 009
A9421 14514nF010
M421_14514_DF_011
A9421_14514_DF 012
M421 14514 DF_013
Total 2378s = Sum of 17 2378 -substituted PCDD/PCDF congeners (SARA 313)
() = WWO# A9421 Page 8 of 42
[ ] = EMPC /

A9421 - Others
Project ID: 2016 Annual Fish Project
Sample Summary
Method 1613B
Part 3
--SG$-
MethodComp
Comp
COMP12
Comp13
Comp1
Comp2
Comp3
Comps
Comp6
Comp?
Comp9
Comp 10
Comp 11
Analyte
Blank
Site 1
Site 1
Site 1 Blue
Site 1
Site 2
Site 2
Site 2 Blue
Site 2
Site 3
Site 3 Blue
Site 3 Blue
Site 3
Site 1 Blue
A9421 145
Common
Common
Common
Catfish -
Bluegill
Bluegill
Catfish
Bluegill
Bluegill
Catfish
Bluegill
Catfish
Catfish
14
Cara
Carp
Carr)
Replicate
Pg/g
PgIg
pg/9
Pgg
pg/g
pg/g
pg/g
pg/g
PgIg
Pg/g
Pg�g
pg/g
Pg/g
PgIg
Other PCDD/Fs (ND=O, EMPC=O)
Other TCDD
0
0
0
0
0
0
0
0
0
0
0
0.197
0
0
Other PeCDD
0
0
0
0
0.336
0
0
0
0
0
0
0.216
0
0
Other HxCDD
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Other HpCDD
0
0
0
0
0
0
0
0
0
0.543
0
0
0
0
Other TCDF
0
0
0
0
0.604
0
0
0
0
0
0
0
0
0.954
Other PeCDF
0
0
0
3.03
2.35
0
0
0.888
0
0
1.22
0.873
1.39
1.26
Other HxCDF
0
0
0
0
0.658
0
0
0.265
0
0
0
0.208
0
0
Other HpCDF
0
0
0
0
0.168
0
0
0
0
0
0
0
0
0
Other PCDD/Fs (ND=O, EMPC=EMPC)
Other TCDD
0
0
0
0
0.471
0
0
0
0
0
0
0.197
0
0
Other PeCDD
0
0
0
0
0.336
0
0
0
0
0
0.155
0.216
0
0
Other HxCDD
0
0
0
0
0
0
0
0
0
0
0
0
0
0
Other HpCDD
0
0
0
0
0
0
0
0
0
0.543
0
0
0
0
OtherTCDF
0
0
0
0
0.777
0
0
0
0
0.231
0
0
1.02
0.954
Other PeCDF
0
0
0
4.48
2.74
0
0
1.18
0.616
0
1.36
1.62
1.39
1.26
Other HxCDF
0
0
0
0
0.656
0
0
0.265
0
0
0
0.208
0.271
0
Other HpCDF
0
0
0
0
0.168
0
0
0
0
0
0
0
0
0
Checkcode
064-609-WZX
682-452-KJR
057-138-RZW
236-631-ZMJ
680-894-RPK
860-459-GBW
348-654-SMZ
781-687-PJJ
281-592-WPG
794-649-QKR
740 -406 -GPX
565 -465 -TVR
198-325-JKC
364-936-JBB
Lab ID
OF 90SRQ
0.9421 14514 DF 001
A 21 14514_DF 002
A9421 1451d_DL000
A9u1 u514 Dr 004tu
A9421 14514_DF 005
A9421_1451d_OF_ONB
A9421_1451d_DF_001
0.9421 14514_OF 000
A9421 14516_DF_009
A 21 14514 OF 010
A9421 14514 OF 011
A9421 14514_DF 012
A9121_14514 -DF -013
() = DJVO# A9421 Page 9 of 42
[ ] = EMPC

A9421 - DLs
Project ID: 2016 Annual Fish Project
Sample Summary
Method 16138
Part 5 (DLs)
Method
Comp1
Comp2
Comp3
Comp
Comps
Comps
Comp?
Comp 8
Comp9
Comp 10
Comp 11
OMP12
Comp13
Blank
Site 1
Site 2
Site 3
Site 1 Blue
Analyte
Site 1
Site 1
Site 1 Blue
Site 2
Site 2
Site 2 Blue
Site 3
Site 3 Blue
Site 3 Blue
A9421 145
14
Bluegill
Bluegill
Catfish
Common
Carp
Bluegill
Bluegill
Catfish
Common
Carp
Bluegill
Catfish
Catfish
Common
Carp
Catfish -
Replicate
9�9
P
g/9
g/9
g/9
g/9
gig
PO
g/9
PO
g/9
gig
Pg/9
/g
2,3,7,8-TCDD
0.312
0.104
0.125
0.77
0.115
0.23
0.187
0.293
0.374
0.0844
0.096
0.146
0.201
0.637
1,2,3,7,8-PeCDD
0.314
0.133
0.105
0.885
0.136
0.191
0.146
0.326
0 601
0.0954
0.119
0.168
0.217
0.685
1,2,3,4,7,8-HxCDD
0.23
0.129
0.142
0.698
0.22
0.199
0.155
0.28
0.509
0.113
0.158
0.184
0.274
0.626
1,2,3,6,7,8-HxCDD
0.24
0.141
0.152
0.7
0.221
0.203
0.162
0.282
0.535
0.114
0.173
0.212
0.292
0.683
1,2,3,7,8,9-HxCDD
0.257
0.142
0.146
0.761
0 227
0.215
0.166
0.304
0.553
0.115
0.173
0.204
0.297
0.607
1,2,3,4,6,7,8-HpCDD
0.339
0.139
0.151
0.664
0.177
0.24
0.233
0.262
0.587
0.124
0.165
0.281
0 261
0.864
QCDD
0.538
0.268
0.204
1.17
0.269
0.418
0.344
0.536
0.921
0.185
0.24
0.368
0.432
1.52
2,3,7,8-TCDF
0.246
0.125
0.11
0.987
0.158
0.219
0.173
0.283
0.473
0.0929
0.119
0.189
0.196
0.562
1,2,3,7,8-PeCDF
0.171
0.108
0.0917
0.613
0.153
0.151
0.137
0.21
0.512
0.0926
0.13
0.197
0.21
0.732
2,3,4,7,8-PeCDF
0.17
0.105
0.0871
0.55
0.145
0.142
0.127
0.199
0.471
0.0871
0.127
0.19
0.186
0.73
1,2,3,4,7,8-HxCDF
0.158
0.0963
0.0768
0.327
0.115
0.119
0.108
0.176
0.323
0.0639
0.0759
0.119
0.132
0.305
1,2,3,6,7,8-HxCDF
0.147
0.0891
0.0715
0.315
0.107
0.112
0.0977
0.164
0.31
0.0556
0.0682
0.121
0.124
0.309
2,3,4,6,7,8-HxCDF
0.155
0.0965
0.0773
0.326
0.109
0.123
0.106
0.178
0.335
0.061
0.0744
0.126
0.137
0.32
1,2,3,7,6,9-HxCDF
0.216
0.126
0.107
0.529
0.146
0.17
0.149
0.255
0.459
0.0813
0.0997
0.164
0.18
0.411
1,2,3,4,6,7,8-HpCDF
0.16
0.0671
0.0539
0.301
0.0846
0.0991
0.0903
0.161
0.31
0.0602
0.0668
0.149
0.111
0.326
1,2,3,4,7,8,9-HpCDF
0.298
0.129
0.101
0.574
0.156
0.164
0.167
0.296
0.498
0.1
0.106
0.232
0.186
0.554
OCDF
0.55
0.397
0.297
1.38
1 0.234
0.568
0.392
1 0.528
0.836
1 0.196
0.219
0.331
0.446
1.48
Total TCDD
0.312
0.104
0.125
0.77
0.115
0.23
0.187
0.293
0.374
0.0844
0.096
0.146
0.201
0.637
Total PeCDD
0.314
0.133
0.105
0.885
0.136
0.191
0.146
0.326
0.601
0.0954
0.119
0.168
0.217
0.685
Total HxCDD
0.242
0.137
0.146
0.719
0.222
0.206
0.161
0.288
0.532
0.114
0.168
0.2
0.287
0.637
Total HpCDD
0.339
0.139
0.151
0.664
0.177
0.24
0.233
0.262
0.587
0.124
0.165
0.281
0.261
0.864
Total TCDF
0.246
0.125
0.11
0.987
0.158
0.219
0.173
0.283
0.473
0.0929
0.119
0.189
0.196
0.562
Total PeCDF
0.17
0.106
0.0894
0.582
0.149
0.147
0.132
0.205
0.491
0.0898
0.128
0.194
0.198
0.731
TotalH%CDF
0.165
0.1
0.0817
0.361
0.118
0 128
0.113
0.188
0.35
0.0645
0.0784
0.131
-0.141
0.332
Total HpCDF
0.214
0.0912
0.0729
0.405
0.114
0.125
0.12
0.215
0.388
0.0768
0.0836
0.185
0.142
0.418
Checkcode
064-609-WZX
682-452-KJR
057-138-RZW
236-631-ZMJ
680-894-RPK
860-459-GBW
348-654-SMZ
781-687-PJJ
281-592-WPG
794-649-QKR
740 -406 -GPX
565 -465 -TVR
198-325-JKC
364-936-JBB
Lab ID
M91_14514DF9D-2
A9421 14514_OF 001
A8421 14514 DF 002
A9421 14514 DF 003
A9421 145140E OOLRJ
0.9421 14514 DF 005
A9421 1451d_DF 009
A9421_14514 DF 001
A9421_14510 DF 008
A9421 14514_OF_ON
A9421 14514DF 010
A9421 145140E 011
A9421 14514 DF. -01 2
A9421 14514 DF 013
WO# A9421 Page 10 of 42

3
2.5
701
WHO-2005-TEQ
Project ID: 2016 Annual Fish Project
A9421
'.. ND=O; EMPC=O
ND=O; EMPC=EMPC
n ND=DL/2; EMPC=O
■ ND=DL/2; EMPC=EMPC
t ND=DL; EMPC=EMPC
1
0.5
C
NON et �s\` cQ �s\` a<Q ��\ �s�` r��s\` acQ atie
%�� 9\Jed ,011 Gad o�� 0\vel g\vel CPQ o\`C op r'S Gab 0\1 eQ\�°
`,e� `,e1 �\ve �� pe ,`�e'L \ve '00 `�e3 ,\oe lb\\,e e Q�
yS LS Ceti tiG° hS 6S `�e1' LLo 9S �e15 �e3 3C° a�4`�r,
oaf\an G°�Q Go�Q ��3g\�S`�e `o�Q Go�.Q t��1S �S�tie C°�.Q Q1�S� Q�1S� 1�S`�e\JeG
�etir Lo C°"Q Lo `°�.Q L°t�` `oc�` °�Q S\�e1
G 13
0011
WO# A9421 Page 11 of 42

35
30
25
20
on
ego
CL
15
10
5
0
Totals
Project ID: 2016 Annual Fish Project
A9421
306
.Total PCDD/Fs (ND=O; EMPC=O)
13 Total PCDD/Fs (ND=O; EMPC=EMPC)
%.'Tntml Drnn/Fc /7R7Q_Y Kir)-ni • PRADr-i:RADrI
Ob Je61, a00W Late ego ew �s�' ��� eoo' �E�s� ��s�' Gats �a�
La ot` Ga o� &3! Ga Ga op ep\�
Go�� S\;e L S�tie L �3�oe Go�ct` S`�e3 3��oe 3���e CO
\Sr Q
G°spy Go�p L p3S`�e AS�Sey Go�ph Go�p6 p� S\�e 3S\Ie� Go�p9 y�S\�e yyS`Np ti .!;p �veGa
CI`e�r GoF C.o�p CPF Loop C o�p Go�p o�9 y3S `,ey0
G
G0\
WO# A9421 Page 12 of 42

80
70
60
50
ci
cc 40
NO
0
30
20
10
0
`pp `pp `pp Gpp `pp Gpp `pp �`pQ eLp� e`pQ +GpQ �`pQ +`pF *`pQ Q`pQ Q`pF O`pQ
y
Mean Recoveries of Extraction Standards (N=14)
Project ID: 2016 Annual Fish Project .0 Mean nStd. Dev.
A9421
WO# A9421 Page 13 of 42

120
KI1II
80
Mean Recoveries of Clean -Up Standards (N=14)
Project ID: 2016 Annual Fish Project .0 Mean r] Std. Dev.
A9421
40
20
C
\�GQp Qe`Qp Q�GQQ �+GQQ �Q`QQ
WO# A9421 Page 14 of 42

R
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co
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Sample ID: Comp 1 Site 1 Bluegill Method 1613B
Client Data
Samole Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.23 g
Lab Sample ID A9421_14514_DF_001
Date Extracted: 15 -Nov -2016
Date Collected: 20 -Sep -2016
% Lipid: 0.2%
QC Batch No: 14514
Date Analyzed: 04 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 17:08:27
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
ND
0.104
ES 2378 -TCDD
59.3
12378-PeCDD
ND
0.133
ES 12378-PeCDD
51.9
123478-HxCDD
ND
0.129
ES 123478-HxCDD
63
123678-HxCDD
ND
0.141
ES 123678-HxCDD
60.3
123789-HxCDD
ND
0.142
E_S 123789-_HxCDD
6.2.1
1234678-HpCDD
ND
0.139
ES 1234678-HpCDD
61
OCDD
ND
0.268
ES OCDD
51.9
2378-TCDF
ND
0.125
ES 2378-TCDF
63.3
12378-PeCDF
ND
0.108
ES 12378-PeCDF
62.1
23478-PeCDF
ND
0.105
ES 23478-PeCDF
60.7
123478-HxCDF
ND
0.0963
ES 123478-HxCDF
70.4
123678-HxCDF
ND
0.0891
ES 123678-HxCDF
72.6
234678-HxCDF
ND
0.0965
ES 234678-HxCDF
70.5
123789-HxCDF
ND
0.126
ES 123789-HxCDF
63.7
1234678-HpCDF
ND
0.0671
ES 1234678-HpCDF
75.6
1234789_ -HpCDF
ND
0.129
ES 1234789-HpCDF
58.4
OCDF
ND
0.397
ES OCDF
50.2
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
79.8
Total TCDD
ND-
0.104
ND
CS 12347-PeCDD
82.8
- -- ---- ------ - - -
Total PeCDD
-
-- -- - - -- -- ----
ND
- --- --------- - -
0.133
- - ----- - -- --
ND
--- - - - - - — - --
--- ---------- ---
CS 12346-PeCDF
------------ ---- ---
91.8
---- —
Total HxCDD
ND
0.137
ND
CS 123469-HxCDF
109
Total HpCDD
ND
0.139
ND
CS 1234689-HpCDF
98.5
Total TCDF
ND
ND
Total PeCDF
ND
_0.125
0.106
ND
Total HxCDF
ND
0.1
ND
Total HpCDF
ND
0.0912
ND
Total PCDD/Fs
'ND
NID
WHO -2005 TEQs
5500 Business Drive
TEQ: ND_=DL/2
0_.185
0_185-----
Wilmington, NC 28405, USA
SG
_
TEQ: ND=DL
_ _ _
0.369
_ _-
0.369
-- _0_185- -
0.369
__ _ __ _ --- _
- www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WOYfefi@ddhb: 682-452-KJR SGS North Arr@aga-MFbVQ1Z8 Report Created: 06 -Dec -2016 08:12 Analyst: pw

Sample ID: Comp 2 Site 1 Bluegill Method 1613B
Client Data
Samaie Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10-Nov-2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.64 g
Lab Sample ID A9421_14514_DF_002
Date Extracted: 15-Nov-2016
Date Collected: 20-Sep-2016
% Lipid: 0.4%
QC Batch No: 14514
Date Analyzed: 04-Dec-2016
Split: -
Dilution: -
Time Analyzed: 18:00:52
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378-TCDD
ND
0.125
ES 2378-TCDD
73.9
12378-PeCDD
ND
0.105
ES 12378-PeCDD
66.1
123478-HxCDD
ND
0.142
ES 123478-HxCDD
79.3
123678-HxCDD
ND
0.152
ES 123678-HxCDD
78.4
123789-HxCDD
ND
0.146
-
ES 123789-HxCDD
77.3
1234678-HpCDD
ND
0.151
ES 1234678-HpCDD
76.5
OCDD
ND
0.204
ES OCDD '
67.6
2378-TCDF
ND
0.11
ES 2378-TCD-F-,
75.8
12378-PeCDF
ND
0.0917
ES 12378-PeCDF
77
23478-PeCDF
ND
0.0871
ES 23478-PeCDF
75.1
123478-HxCDF
ND
0.0768
ES 123478-HxCDF
88.2
123678-HxCDF
ND
0.0715
ES 123678-HxCDF
87.7
234678-HxCDF
ND
0.0773
ES 234678-HxCDF
87.9
123789-HxCDF
ND
0:107
ES 123789-HxCDF
78.7
1234678-HpCDF
ND
0.0539
ES 1234678-HpCDF
93.6
1234789-HpCDF_
ND
0.101
ES 1234789-HpCDF
75.5
OCDF
ND
0.297
ES OCDF
66.8
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
93.9
Total TCDD
ND
0.125
ND
CS 12347-PeCDD
96.1
Total PeCDD
ND
0.105
ND
CS 12346-PeCDF
104
Total HxCDD
ND
0.146
ND
CS 123469-HxCDF
119
Total HpCDD
ND
0.151
ND
CS 1234689-HpCDF
1'08
Total TCDF
ND
0.11
ND
Total PeCDF
ND
0.0894
ND
Total HxCDF
ND
0.0817
ND
Total HpCDF
ND
0.0729
ND
Total PCDD/Fs
ND
ND
WHO-2005 TEQs
�j 5500 Business Drive
TEQ: ND=O
0
0
- ---
--
TEQ: ND=DL/2
0.175
0.175
0.175
I Wilmington, NC 28405, USA
TEQ: ND=DL
0.35
0.35
0.35
u www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WO&MaMle: 057-138-RZW SGS North AmRagm 23FbV%28 Report Created: 06 -Dec -2016 08:12 Analyst: pw

Sample ID: Comp 3 Site 1 Blue Catfish Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.59 g
Lab Sample ID A9421_14514_DF_003
Date Extracted: 15 -Nov -2016
Date Collected: 20 -Sep -2016
% Lipid: 1.7%
QC Batch No: 14514
Date Analyzed: 04 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 18:53:18
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
ND
0.77
ES 2378 -TCDD
46.6
12378-PeCDD
EMPC
1.06
J
ES 12378-PeCDD
43.3
123478-HxCDD
-ND
0.698
ES 123478=HxCDD
55.2
123678-HxCDD
ND
0.7
ES 123678-HxCDD
54.1
123789-HxCDD
ND
0.761
ES 123789-HxCDD
50.2
1234678-HpCDD
EMPC
2.28
J
ES 1234678-HpCDD
55
OCDD
EMPC
9.43
ES OCDD
46.5
2378-TCDF
ND
0.987
ES 237_8-TCDF
48
12378-PeCDF
ND
0.613
ES 12378-PeCDF
51.9
23478-PeCDF
ND
0.55
ES 23478-PeCDF
50.9
123478-HxCDF
ND
0.327
ES 123478-HxCDF
63.7
123678-HxCDF
ND"
0.315
ES 123678-HxCDF
63.5
234678-HxCDF
ND
0.326
ES 234678-HxCDF
62
123789-HxCDF
ND
0.529
ES 123789-HxCDF
48.4
1234678-HpCDF
ND
0.301
ES 1234678-HpCDF
67.3
1234789-HpCDF
ND
0.574
ES 1234789-HpCDF
49.2
OCDF
ND
1.38
ES OCDF
45.4
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
80.7
Total TCDD
ND
0.77
ND
CS 12347-PeCDD
91.3
Total PeCDD
ND
-1.06
-107
CS 12346-PeCDF
Total HxCDD
ND
0.719
ND
CS 123469-HxCDF
126
Total HpCDD
ND
2.28
CS 1234689-HpCDF
112
Total TCDF
ND
0.987
ND
Total PeCDF
3.03
4.4_8
Total HxCDF
ND
Total HpCDF
ND
.___0.361-_
0.405
ND
--
- -
Total PCDD/Fs
3.03
17.2
WHO -2005 TEQs
0
1.16
1.16
1.08
1.79
TEQ: ND=O
TEQ: ND=DU2
5500 Business Drive
{ Wilmington, NC 28405, USA
TEQ: ND=DL
2.32
2.32
2.51
-U www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
Report Created: 06 -Dec -2016 08:12 Analyst: pw
WOW66842b: 236-631-ZMJ
SGS North AmPags 24FbV%28
Report Created: 06 -Dec -2016 08:12 Analyst: pw

Sample ID: Comp 4 Site 1 Common Carp. Method 16138
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.55 g
Lab Sample ID A9421_14514_DF_004-RJ
Date Extracted: 15 -Nov -2016
Date Collected: 21 -Sep -2016
% Lipid: 2.8%
QC Batch No: 14514
Date Analyzed: 05 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 12:34:08
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
0.192
J
ES 2378 -TCDD
49.9
12378-PeCDD
EMPC
0.561
J
ES 12378-PeCDD
46.6
123478-HxCDD
EMPC
0.5
J
ES 123478=HxCDD
53.8"
123678-HxCDD
0.891
J
ES 123678-HxCDD
53.3
123789-HxCDD
0.475
-J
ES 123789-HxCDD
53.4
1234678-HpCDD
4.32
ES 1234678-HpCDD
50.2
OCDD
19.1
ES OCDD
42.2
2378-TCDF
0.384
J
ES 2378-TCDF
53.4
12378-PeCDF
0.583
J
ES 12378-PeCDF
55.1
23478-PeCDF
0.527
J
ES 23478-PeCDF
53.2
123478-HxCDF
0.255
J
ES 123478-HxCDF
59.8
123678-HxCDF
0.399
J
ES 123678-HxCDF
60
234678-HxCDF
EMPC
0.172
J
ES 234678-HxCDF
59.1
123789-HxCDF
ND
0.146
ES 123789-HxCDF
52.8
1234678-HpCDF
0.409
J
ES 1234678-HpCDF
58
1234789-HpCDF
ND
0.156
ES 1234789-HpCDF
47.7
OCDF
0.333
J
ES OCDF
42.7
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
69.3
Total TCDD
0.192
0.663
CS 12347-PeCDD
75
Total PeCDD
0.336
0.897
CS 12346-PeCDF
79.8
Total HxCDD
1.37
1.86
CS 123469-HxCDF
90.7
Total HpCDD
4.32'
4.32
CS 1234689-HpCDF
79.6
Total TCDF
0.988
1.16
Total PeCDF
3.46
3.85
Total HxCDF
1.31
1.48
Total HpCDF
0.577
0.577
--- --- --- -- ----- --
--- --- ------ -
-- ----- - ---- -
Total PCDD/Fs
32
34.2
WHO -2005 TEQs
5500 Business Drive
TEQ: ND=O
0.661
1.29
TEQ: ND=DL/2
0.754
0.217
1.3
Wilmington, NC 28405, USA
-T-E--b:-N--D-
0.847
0.434
1.31
- www.us.sgs.com
_=DL
Tel: [phone]; Toll -Free 866 846-8290
WON6 : 680-894-RPK SGS North AmPEige 25FbM 8 Report Created. 06 -Dec -2016 08:18 Analyst: pw

Sample ID: Comp 5 Site 2 Bluegill Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.52 g
Lab Sample ID A9421_14514_DF_005
Date Extracted: 15 -Nov -2016
Date Collected: 20 -Sep -2016
% Lipid: 0.5%
QC Batch No: 14514
Date Analyzed: 04 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 20:38:10
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
ND
0.23ES
2378 -TCDD
60.1
12378-PeCDD
ND_
0.191
ES 12378-PeCDD
123478-HxCDD. i_ -
-_ ND �--J_
----0.199 _Y
-----v- 4---
44
_'- --
ES 123478-HxCDD
_5_5.8_
� 65.6
-------_---_._-
123678-HxCDD_
ND
--4444---2224__
ES 123678-HxCDD
66.4
123789-HxCDD°-_-
_---�ND ----
-4444--
_0.203
_ 0.2.15~--�
-
_
ES 123789-HxCDD 44-2.4442222___--
-- .
62.8
-- - 4
444-4444-- -- --
- __ --_-- ---_-_4244
1234678-HpCDD
4442_ ___4424_
ND
-- 44 44-_--2444----°---
--- --�444444
44-•4444- 4444-
-----4444--
_-------444444
ES 1234678-HpCDD
4444- 62.9_
ocDo �
ND__________
_0.24
—_ 0.41:84444-
-
Es ocDo�_--- ---
55.1
23782378-TCDF--"_---_
v---- ND '-
0.219 .4444
-�_-
'----~-ES2378-TCDF
- - --
63.1
--
-- - -
- ---- - -
12378-PeCDF
-- -- - --° --
ND
ND 2444
- - --- -
0.151
Y-0:142 :-
- -
_ ---
ES 12378-PeCDF
- --
66.3
--
23478-PeCDF --�
_--�-----�--
-
_
ES 23478-PeCDF �
-- --- ---- - - -
64.9 2222_
- =----- -
-�--
-- - ----
------ -...
123478-HxCDF
- --
- - - - - - -
0.119
- - - -
-- -
ES 123478-HxCDF
-�-_
74.1__
123678-HxCDF
_ND
__t--- ND 2.222
0.1,12 4244
�
ES 123678-HxCDF
x --
---75.8
- - - -
- ---
44236 --- - - -
234678-HxCDF
- - - --
ND
-
0.123
ES 234678-HxCDF
73.1_
123789-HxCDF
_ _
- 'ND y
_
0.17
-��s
��
ES 123789=HxCDF
_
63.2
-°-- - --- --
-- --- --_. -•--
1234678-HpCDF
0.0_991
ES 1234678-HpCDF
_
1234789-HpCDF _
_ND_
- �- N D ^ !
,0.1 64 A
-^-� —
-'
ES 1234789-HpCDF --
_78
--- 60.7 ---
_-
--
OCDF
ND
0.568
JES OCDF
54.4
Totals
Standard
CS Recoveries
CS 37 CI -2378 -TCDD
78.4
---
Total TCDD
ND
ND
CS 12347-PeCDD
86.9
-96
_
_
Total PeCDD--
_
- ND
_0.23_
0.191
ND
��-
CS 12346-PeCDF
Total HxCDD_
ND
0.206
ND
CS 123469-HxCDF___
Total HpCDD-
_
-�-ND
4444 ND
_
0.24
0.219
_
ND
-
CS 1234689-HpCDF
97.8
Total TCDF i--
�ND
ND
Total PeCDF
_
ND
0.147
ND
Total,HxCDF __ 24.22_
ND
-- -__ _4222-- __- _--P 4444 --
0.128
--- 4--__-_4422__
ND
4444 -___4444
_
� -- 4444 . __
-- - 4444- -4444-- - 4444
- - — --4444-- -- � -
-- -- - -- •-�- --
---_ _ __ - - - --_
Total HpCDF
ND
444
0.125
ND
To°tal PCDD/Fs
ND '
ND
WHO -2005 TEQs
_
------------2222..__
TEQ:- ND=O
0 _.__4222,
0
5500 Business Drive
__.-----_-24442444-2444_-2224.-22442244__
TE_Q: ND=DU2
0.305_
0.305
Wilmington, NC 28405, USA
TEQ: ND=DL —
0.609 ---------2444-____T_
0':609 ----__
- www.ussgs.com
_0.305
0.609
-------------------4444--
��- -'
Tel: [phone]; Toll -Free 866 846-8290
WOMA : 860-459-GBW SGS North Am@aga-WFbM38 Report Created: 06 -Dec -2016 08:12 Analyst: pw

Sample ID: Comp 6 Site 2 Bluegill I Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.75 g
Lab Sample ID A9421_14514_DF_006
Date Extracted: 15 -Nov -2016
Date Collected: 02 -Nov -2016
% Lipid: 0.2%
QC Batch No: 14514
Date Analyzed: 04 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 21:30:36
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
ND
0.187
ES 2378 -TCDD
72.8
12378-PeCDD
ND
0.146
ES 12378-PeCDD
65.2
123478-HxCDD
ND
0.155
ES 123478-HxCDD
77.8
123678-HxCDD
ND
0.162ES
123678-HxCDD
79.6
---- - — - -
123789-HxCDD
- - - -- -
ND
— --
0.166
- - - - -- - --
-- --- ---------
--- --
ES 123789-HxCDD
- -- -- ---
79
-- - - - - -- -
1234678-HpCDD
ND
0.233
ES 1234678-HpCDD
75.1
OCDD
ND
0.344
ES OCDD
71.8
2378-TCDF
ND
0.173
ES 2378-TCDF
76.9
12378-PeCDF
ND
0.137
ES 12378-PeCDF
79.4
23478-PeCDF
ND
0.127
ES 23478-PeCDF
78.3
123478-HxCDF
ND
0.108
ES 123478-HxCDF
88.8
123678-HxCDF
ND
0.0977
ES 123678-HxCDF
92.1
234678-HxCDF
ND
0.106
ES 234678-HxCDF
87.3
123789-HxCDF
ND
0.149
7
ES 123789-HxCDF
75.1
1234678-HpCDF
ND
0.0903
ES 1234678-HpCDF
92
1234789-HpCDF
ND
0.167
ES 1234789-HpCDF
71
OCDF
0.488
J
JES OCD F
66.5
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
86.6
Total TCDD
ND
0.187
ND
CS 12347-PeCDD
98.4
Total PeCDD
ND
0.146
ND
CS 2346- P eCDF
110
Total HxCDD
ND
0.161
ND
-11 - -
CS 12346-xCDF
123
Total HpCDD
ND
0.233
ND
CS 1234689-HpCDF
107
Total TCDF
ND
0.173
ND
Total PeCDF
ND
0.132
ND
Total HxCDF
ND
0.113
ND
Total HpCDF
ND
0.12
ND
Total PCDD/Fs
0.488
0.488
WHO -2005 T_ E_Q_s
5500 Business Drive
TEQ: ND=O
_
0.000146
0.000146
--
TEQ: ND=DL/2
0.246
0.246
0.246Olt
Wilmington, NC 28405, USA
TEQ: ND=DL
0.492
0.492
0.492
a www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WOWe@ : 348-654-SMZ SGS North ArrRaga 2l3Fob%28 Report Created: 06 -Dec -2016 08:12 Analyst: pw

Sample ID: Comp 7 Site 2 Blue Catfish Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10-Nov-2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.94 g
Lab Sample ID A9421_14514_DF_007
Date Extracted: 15-Nov-2016
Date Collected: 21-Sep-2016
% Lipid: 2.3%
QC Batch No: 14514
Date Analyzed: 05-Dec-2016
Split: -
Dilution: -
Time Analyzed: 2:05:44
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries Qualifiers
2378-TCDD
ND
0.293
ES 2378-TCDD
55.7'
12378-PeCDD
0.644
J
ES 12378-PeCDD
53.5
64.6
�.-�
123478-HxCDD
ND
0.28
ES 123478-HxCDD
123678-HxCDD
0.447J
ES 123678-HxCDD
123789-HxCDD
�-- 0.507
j_______
ES 123789-HxCDD •-�
E 1
-
_63.2
-^_ 60.5-
_ - - --
1234678-HpCDD
1.27J
-- -- -- -
ES 1234678-HpCDD
-
59.3
-----------
ocDD ----_.__
—__.-3.11
- - _- ---� ND -- ---~-
-----__-J- -
Es ocoD"�__----
--51-----
------
2378-TCDF ----
2378-TCDF
0.283
--�---
--- �—
ES 2378-TCDF �
-
—_- 59.3 . -'
-- -- - -
12378-PeCDF
- _ -
ND_
.__---, ND
-- - -
_0.21
"0.199-__
- - - - -
-___--�--
- -
- - - - -- _
ES 12378-PeCDF_
ES 23478-PeCDF ----
- - - -
23478-PeCDFv._r___
_62.5_
_-�- 59.7
123478-HxCDF
0.356
J
ES 123478-HxCDF_
72
123678-HxCDF "_-
-
0.224 -----
j ---
ES 123678-HxCDF _ -
_ -,72.1
234678-HxCDF
ND
0.178
ES 234678-HxCDF
ES 123789-HxCDF
69.1
123789-HxCDF
ND
0.255
54.8
1234678-HpCDF
EMPC
0.223
J
ES 1234678-HpCDF
73.6
0.296 _
-�---
-_--- ---
ES 1234789-HpCDF---
-_---57.9__- - -'
1234789-HpCDF �----
--- - ND---------
OCDF
ND
0.528
JES OCDF
50.7
Totals
Standard
CS Recoveries
CS 37C-1-2378-TCDD
88.6
Total TCDD
0_._293
ND
CS 12347-PeCDD
99.1
_
Total PeCDD
_ _ND_
0.644
- -
CS 12346-PeCDF
_
112xA-__
0.644
y --
Total HxCDD
0.954
CS 123469-HxCDF
124_
Total HpCDD -
_
v - 1.27
—
_0.954
1.27�
_
CS 1234689-HpCDF
_
111
Total PeCDF
0.888_1.18_
--____.__--.- _._.
_ ___-_
Total HxCDF - —
—_-_-0.845
s
—"0.845
�'•"--`-" -
._.�___.
Total HpCDF
ND
0.223
Total PCDD/Fs--
7.71
8.23 .
WHO-2005 TEQs
5500 Business Drive
TEQ: ND=DL/2
1.04
Wilmington, NC 28405, USA
TEQ: ND=DL -�
- _-i 1.28 - -
_0.443
— 0.885 . -
_1.04_
- 1:28 —
— —
www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WOWS& : 781-687-PJJ SGS North Aml9age 218Fo6&28 Report Created: 06 -Dec -2016 08:13 Analyst: pw

Sample ID: Comp 8 Site 2 Common Carp Method 16136
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.99 g
Lab Sample ID A9421_14514_DF_008
Date Extracted: 15 -Nov -2016
Date Collected: 21 -Sep -2016
% Lipid: 2.8%
QC Batch No: 14514
Date Analyzed: 05 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 2:58:09
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
. ES Recoveries
Qualifiers
2378 -TCDD
ND
0.374
ES 2378 -TCDD
48.3
12378-PeCDD
ND
0.601
ES 12378-PeCDD
42.2
123478-HxCDD
ND
0.509
ES 123478-HxCDD
50.5
123678-HxCDD
0.749
J
ES 123678-HxCDD
49.5
123789-HxCDD
ND
0.55.3
ES 123789-HxCDD
50.8
1234678-HpCDD
2.33
ES 1234678-HpCDD
47.4
OCDD
10.3
ES OCDD
40.6
2378-TCDF
ND -
0.473
ES 2378-TCDF
_48.3
12378-PeCDF
0.991
J
ES 12378-PeCDF
48
2347_8-PeCDF
ND
0.471
ES 23478-PeCDF
47.7
123478-HxCDF
ND
0.323
ES 123478-HxCDF
58
123678-HxCDF
ND
0.31
ES 123678-HxCDF
57.1
234678-HxCDF
ND
0.335
ES 234678-HxCDF
56.3
123789-HxCDF
ND
0.459
ES 123789-HxCDF -
50.6
1234678-HpCDF
EMPC
0.319
J
ES 1234678-HpCDF
56.4
1234789-HpCDF
ND
0.498
ES 1234789-HpCDF
47.5
OCDF
ND
0.836
ES OCDF
41.2
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
76.9
Total TCDD
ND
0.374
ND
CS 12347-PeCDD
83.1
Total PeCDD
ND
0.601
ND
CS 12346-PeCDF
87
Total HxCDD
0.749
0.749
CS 123469-HxCDF
105
Total HpCDD
2.33
2.33
CS 1234689-HpCDF
93.5
Total TCDF
ND
0.473
ND `
Total PeCDF
0.991
1.61
Total HxCDF
ND
0.35
ND
Total HpCDF
ND
0.319
-- - --- - - - - -- -
- --
Total PCDD/Fs
14.4
15.3
WHO-2005 TEQs
5500 Business Drive
TEQ: ND=O
0.131
0.134
TEQ: ND=DL/2
0.841
0.748
0.843
i Wilmington, NC 28405, USA
TEQ: ND=DL
1.55
1.5
1.55
i- www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WOMA : 281-592-WPG SGS North AmI3ageJMFofigi218 Report Created: 06 -Dec -2016 08:13 Analyst: pw

Sample ID: Comp 9 Site 3 Bluegill Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.33 g
Lab Sample ID A9421_14514_DF_009
Date Extracted: 15 -Nov -2016
Date Collected: 02 -Nov -2016
% Lipid: 0.8%
QC Batch No: 14514
Date Analyzed: 05 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 3:50:36
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
ND
0.0844
ES 2378 -TCDD
60.3
12378-PeCDD
ND
0.0954
ES 12378-PeCDD
54.2
123478-HxCDD
ND
0.113
ES 123478-HxCDD
61
123678-HxCDD
ND
0.114
ES 123678-HxCDD
60.7
123789-HxCDD
EMPC
0.169
J
ES 123789-HxCDD
59.5
1234678-HpCDD
EMPC
0.162
J
ES 1234678-HpCDD
57.4
OCDD
1.21
J
ES OCDD'
50.7
2378-TCDF
ND
0.0929
ES 2378-TCDF
62.5
12378-PeCDF
ND
0.0926
ES 12378-PeCDF
62.7
23478-PeCDF
ND
0.0871
ES 23478-PeCDF
62.5 _.
123478-HxCDF
ND
0.0639
ES 123478-HxCDF
66.8
123678-HxCDF
ND
0.0556
ES 123678-HxCDF,
68.2
234678-HxCDF
ND
0.061
ES 234678-HxCDF
64.8
123789-HxCDF
ND
0.0813
ES 123789-HxCDF
60.5
1234678-HpCDF
ND
0.0602
ES 1234678-H CDF
_ 67.1
1234789-HpCDF
ND
0.1
ES 1234789-HpCDF
56.6
OCDF
ND
0.196
ES OCDF
51.1
Totals
Standard
CS Recoveries
CS 37C] -2378 -TCDD
79.7
Total TCDD
ND
0.0844
ND
CS 12347-PeCDD
84.7
Total PeCDD
ND
0.0954
ND
CS 12346-PeCDF
91.3
Total HxCDD
ND
0.543
0.169
0.705
CS 123469-HxCDF
CS 1234689-HpCDF
101
$$.$
Total HpCDD
Total TCDF
ND
0.231,
Total PeCDF
ND
0.0898
ND
Total HxCDF
ND
0.0645
ND
Total HpCDF
ND
0.0768
ND
Total PCDD/Fs
1.75
2.31
WHO -2005 TEQs
5500 Business Drive
------- -
-- --0 -- 00-33
6
'_ - -- - - ..-
+
-- 0.0189
-
TEQ: N_D=_DL/2_
0.141
0.1141
0.153
Wilmington, NC 28405, USA
TEQ: ND -DL -
- 0.282
0.281
0.287
_ _
www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WO*afi@d&b: 794-649-QKR
SGS North AmlBage-3® V428 Report Created: 06 -Dec -2016 08:13 Analyst: pw

Sample ID: Comp 10 Site 3 Blue Catfish Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
WeightlVolume: 10.09 g
Lab Sample ID A9421_14514_DF_010
Date Extracted: 15 -Nov -2016
Date Collected: 01 -Nov -2016
% Lipid: 5.4%
QC Batch No: 14514
Date Analyzed: 05 -Deo -2016
Split: -
Dilution: -
Time Analyzed: 4:43:00
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
EMPC
0.0941
J
ES 2378 -TCDD
65.3
12378-PeCDD
EMPC
0.115
J
ES 12378-PeCDD
ES 123478-HxCDD-
60.5
123478-HxCDD
ND "
-0.158
65.2
123678-HxCDD
0.371_
J
ES 123678-HxCDD
63.3
123789-HxCDD
0.296
-
_ J
ES°123789-HxCDD
61.8
1234678-HpCDD
EMPC
1.12
J -
�J.
ES 1234678--HpCDD
62.9
_
ocDD -
-
4.93 _
-
,_
-
� �, "
Es ocDD
52.8_-�-
2378-TCDF
ND
0'.119
ES 2378-TCDF
66.1
_
12378-PeCDF
ND
0.13
-
ES 12378-PeCDF_
_ 6_8.3_ _
-
23478-PeCDF - -
_
~ 0.246-
-
J
ES 23478-PeCDF
67.5-
123478-HxCDF
ND
0.0759
ES 123478-HxCDF
70.8
123678-HxCDF
236
ND
0.0682
=° --
-- - - --- -
ES 123678-HxCDF_ _ -
71.2-
----- -
234678-HxCDF
- - -- - - - -
ND
<" " ND
- - ---
0.0744
- -- - -
ES 234678-HxCDF
ES 123789-HxCDF
71.6
123789-HxCDF,
0.0997
66.1- -
1234678-HpCDF
ND
0.0668
ES 1234678-HpCDF
68.7
1234789-HpCDF
ND_
�_ �
d_
ES 1234789-HpCDF -••-
- - 61.3
OCDF - - -
- 0.503
_� _ _-0.1:06_-
_:-�_
J
ES OCDF
55.9
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
85
Total TCDD
ND
0.0941
CS 12347-PeCDD
91.6
Total PeCDD
ND
0.27
CS 12346-PeCDF
95.9
Total HxCDD
0.666
0.666
CS 123469-HxCDF
103
Tota-I:HpCDD
_ ND _ =__--
94
_--_ '_ _ - . _
1.1 -_- ..._
_ _ - .--
C$,1234689-HPCDF
Total TCDF
Total PeCDF
1.47
1.61
Total HxCDF
ND
0.0784
ND
Total HpCDF
ND
0.0836
ND
Total PCDD/Fs
7.57
92
a
WHO -2005 TEQs
_ _
5500 Business Drive
TEQ: ND=O
0.142,
0.362 _
TEQ: ND=DL/2
0.283
0.177
- 0.355 -
0.395
_- 0.427
-- - --
Wilmington, NC 28405, USA
www.us.sgs.com
TEQ:_N_D=DL_
0.424 ._---
- - - -
- -•
Tel: [phone]; Toll -Free 866 846-8290
W010e604811e: 740 -406 -GPX SGS North Am@ags-MFo6gi28 Report Created: 06 -Dec -2016 08:13 Analyst: pw

Sample ID: Comp 11 Site 3 Blue Catfish Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10-Nov-2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.44 g
Lab Sample ID A9421_14514_DF_011
Date Extracted: 15-Nov-2016
Date Collected: 02-Nov-2016
% Lipid: 4.0%
QC Batch No: 14514
Date Analyzed: 05-Deo-2016
Split: -
Dilution: -
Time Analyzed: 5:35:25
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries Qualifiers
2378-TCDD
ND
0.146
ES 2378-TCDD
55.1
12378-PeCDD
EMPC
1.27
J
ES 12378-PeCDD
51
123478-HxCDD
0.345
J
ES 123478-HxCDD
57.2
123678-HxCDD
0.99
J
ES 123678-HxCDD
56.3
123789-HxCDD
0.606
J-
ES 123789-HxCDD
56.5
1234678-HpCDD
2.43
ES 1234678-HpCDD
53.9
OCDD
8.08,
ES OCDD
47.4
2378-TCDF
ND
0.189
ES 2378-TCDF
55.8
12378-PeCDF
ND
0.197
ES 12378-PeCDF
57.9
23478-PeCDF
0.405
J
ES_23478-PeCDF
55.1
123478-HxCDF
0.198
J
ES 123478-HxCDF
63.1
123678-HxCDF
ND
0.121
ES' 123678-HxCDF
63.2
234678-HxCDF
ND
0.126
ES 234678-HxCDF
61.1
127378'9"-HxCDF
ND
0.164
ES 123789-HxCDF
56.6
1234678-HpCDF
ND
0.149
ES 1234678-HpCDF
61.3
1234789-HpCDF
ND
0.232
ES 1234789-HpCDF
55.3
OCDF
EMPC
0.347
J
ES OCDF
48.6
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
86.5
Total TCDD
0.197
0.197
CS 12347-PeCDD
92.7
Total PeCDD
0.216
-
1.49 --
-
CS 12346-PeCDF
- - ---- ----- - -
98.4
- - - - -
-
-- - - -- - -
Total HxCDD
- -
1.94
- - - - -
1.94
-
- -
CS 123469-HxCDF
110
Total HpCDD
2.43
99.6
2.43
CS 1234689-HpCDF
Total TCDF
-
'ND
0.189
ND
-
- -
--
Total PeCDF
- -
1.28
2.03
-
Total HxCDF
-_
'0.406
_. --
..__
0.406
--------- -._ __-- - .
_- _-- _ __--_...-----
Total HpCDF
ND
0.185
ND
Total, PCDD/Fs
14.5
16.9
WHO-2005 TEQs
r" 5500 Business Drive
TEQ: 'ND=O
0.362
1.63
TEQ:
0.5_54_
0.25_8_1.74
Wilmington, NC 28405, USA
_ND=DL/2
TEQ: ND=DL---
-_ _ _
----0.746 __--
_ _ _ - -_ _ _ _ _ _ . _ _
- "0.516` - -
_ 1.85
-- • - - -
- -
_- `L_ www.us.sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WOMABdOb: 565 -465 -TVR SGS North Arr@ega -MFbV@28 Report Created: 06 -Dec -2016 08:15 Analyst: pw
J( tiles ��, i,• ;i )� �� ( P( i

Sample ID: Comp 12 Site 3 Common Carp Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.77 g
Lab Sample ID A9421_14514_DF_012
Date Extracted: 15 -Nov -2016
Date Collected: 02 -Nov -2016
% Lipid: 2.1 %
QC Batch No: 14514
Date Analyzed: 05 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 6:27:52
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
ND
0_.20.1_
ES 2378 -TCDD
69.1
12378-PeCDD
EMPC
0.524
J
ES 12378-PeCDD
63.2
123478-HxCDD
ND
0.274
ES 123478-HxCDD
70.7
123678-HxCDD
0.47
J
ES 123678-HxCDD
68.8
123789-HxCDD
ND
0.297
ES 123789-HxCDD
67.3
1234678-HpCDD
1.79
J
ES 1234678-HpCDD
65.7
OCDD
6.63
ES, OCDD
56.7
2378-TCDF
0.343
J
ES 2378-TCDF
69.2
12378-PeCDF
0.46
J
ES 12378-PeCDF
70.8
23478-PeCDF
0.31
J
ES 23478-PeCDF
69
123478-HxCDF
0.162
J
ES 123478-HxCDF
76.9
123678-HxCDF
EMPC
0.27
J
ES 123678-HxCDF
77.5
234678-HxCDF
ND
0.137
ES 234678-HxCDF
75.8
123789-HxCDF
ND
0.18
ES 123789-HxCDF
68.8_
1234678-HpCDF
ND
0.111
ES 1234678-HpCDF
75.1
1234789-HpCDF
ND
0.186
ES 1234789-HpCDF
66.4
OCDF
ND
0.446
JES OCDF
58.2
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
84.7
Total TCDD
ND
0.201
ND
CS 12347-PeCDD
92.6
Total PeCDD
ND
0.524
CS 12346-PeCDF
6.1
96-.1-
Total
Total HxCDD
0.47
0.47
CS 123469-HxCDF
107
Total HpCDD
1.79
1.79
CS 1234689-HpCDF
95.8
Total TCDF
0.343
1.37
Total PeCDF
2.16
2.16
Total HxCDF
0.162
0.703
Total HpCDF
ND
0.142
ND
- ----- ---- -- _ -- ---
------------- - ---
- _ _._----
Total PCDD/Fs
11.6
13.6
WHO-2005 -TEQs
( 5500 Business Drive
TEQ: ND=O
0.224
0.775
TEQ: ND=DL/2
0.486
0.325
0.922
i Wilmington, NC 28405, USA
TEQ: ND=DL
0.747
0.65
1.07
- - www. us sgs.com
Tel: [phone]; Toll -Free 866 846-8290
WOM3090b: 198-325-JKC SGS North AmREigm- 3Fo44Z8 Report Created: 06 -Dec -2016 08:16 Analyst: pw

Sample ID: Comp 13 Site 1 Blue Catfish - Replicate Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: 10 -Nov -2016
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.87 g
Lab Sample ID A9421_14514_DF_013
Date Extracted: 15 -Nov -2016
Date Collected: 20 -Sep -2016
% Lipid: 1.7%
QC Batch No: 14514
Date Analyzed: 05 -Dec -2016
Split: -
Dilution: -
Time Analyzed: 7:20:19
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378 -TCDD
ND
0.637
ES 2378 -TCDD
49
12378-PeCDD
ND
0.685
ES 12378-PeCDD
45.4
123478-HxCDD
ND
0.626
ES 123478-HxCDD
51.9
123678-HxCDD
ND
0.683
ES 123678-HxCDD
51
123789-HxCDD
ND
0.607
ES 123789-HxCDD
51.3
1234678-HpCDD
2.05
J
ES 1234678-HpCDD
49.5
OCDD
9.12
ES OCDD
41.7
2378-TCDF
ND
0.562
ES 2378-TCDF
50.4
12378-PeCDF
ND
0.732
Es 12378-PeCDF
50.6
23478-PeCDF
ND
0.73
ES 23478-PeCDF
48.7
123478-HxCDF
ND
0.305
ES 123478-HxCDF
58.7
123678-HxCDF
ND
0.309
ES 123678-HxCDF
58.3
234678-HxCDF
ND
0.32
ES 234678-HxCDF
55.9
123789-HxCDF
ND
0.411
ES 123789-HxCDF
53
1234678-HpCDF
ND
0.326
ES 1234678-HpCDF
59.6
1234789-HpCDF
ND
0.554
ES 1234789-H CDF
47.9
OCDF
ND
1.48
ES OCDF
42.5
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
78.6'
Total -TCDD
ND
0.637
ND
CS 12347-PeCDD
81.9
Total PeCDD
ND
0.685
ND
CS 12346-PeCDF
87.6
Total HxCDD
ND
0.637
ND
CS 123469-HxCDF
102
-----___---___._
Total HpCDD HpCDD
_. __- --_---- -- --
2.05
--------- ------
----____.__-_ __._
2:05
- ---- ------- --------_-___..___-._._�
-__--------------
92.9
-
CS 1234689-HpCDF
Total TCDF - -
----
0.954"
0.954
-
Total PeCDF
----- - -
1.26
1.26
��---------.-_ _
Total HxCDF
__---- -
ND
-_--
0.332
-.__. _� . ___-.----
ND
-.--- -------
------s_._-_____-._
_ __ _____.--- --------------------
Total HpCDF
ND
0.418
ND
Total PCDD/Fs '
13.4
13.4
WHO-2005 TEQs
i 5500 Business Drive
TEQ: ND=0
0.0232
0.0232
T_EQ: N_D_=DL/2
1-_
__ -- ------1.98 -- - -
0.9_82
--- 1.96
1
__ ._.1.98 _,_._
__ _ __.__ _ _
1 Wilmington, NC 28405, USA
SG i@ www.ussgs.com
TE Q: ND=DL _____
Tel: [phone]; Toll -Free 866 846-8290
WOYteOddkfle: 364-936-JBB SGS North AmRagm-MFbVQt28 Report Created: 06 -Dec -2016 08:16 Analyst: pw

Sample ID: Method Blank A942114514 Method 1613B
Client Data
Sample Data
Laboratory Data
Name: CZR, Inc.
Matrix: Tissue
Lab Project ID: A9421
Date Received: n/a
Project ID: 2016 Annual Fish Project
Weight/Volume: 10.00 g
Lab Sample ID MB1_14614_DF_SDS-RJ2
Date Extracted: 15-Nov-2016
Date Collected: n/a
% Lipid: n/a
QC Batch No: 14514
Date Analyzed: 05-Dec-2016
Split: -
Dilution: -
Time Analyzed: 13:27:16
Analyte
Conc. (pg/g)
DL (pg/g)
EMPC (pg/g)
Qualifiers
Standard
ES Recoveries
Qualifiers
2378'-TCDD
ND
0.312
ES 2378-TCDD,
46.8
12378-PeCDD
ND
0.3_1_4
ES 12378-PeCDD
_ 46
i
123478-HxCDD
_
-- ND
- 0.23
e_
ES 123478-HxCDD
54.2
123678-HxCDD
ND
0.24
ES 123678-HxCDD_
53_
123789-HxCDD -
_ _
- ND s
0.257
—�
e
ES 123789-HxCDD _
50.6--
1234678-HpCDD
ND
0.3_39
ES 1234678-HpCDD
-
50.7
- ND ---- -
0.538 —
.
�-
-T--
Es ocDD
45.5----
49.2
ocDD-__---•---
-
2378-TCDF -
ND -
w 0.246
— `
ES 2378-TCDF
12378-PeCDF
ND
0.171
ES 12378-PeCDF
53.3_
23478-PeCDF -
_ _
— ND
_
0.17 s
ES 23478-PeCDF
51.4
123478-HxCDF
ND
0.158
ES 123478-HxCDF
--
61.2
s--
-
123678-HxCDF—
- ND --
0.147 _
_-_--
ES 123678-HxCDF
62.6
234678-HxCDF
0.155
ES 234678-HxCDF
_ 59
_
123789-HxCDF _
_ND
'ND _ =-
_
0:216--
^'
ES 123789-HxCDF
49.4 ,
1234678-HpCDF
ND
0.16
ES 1234678-H CDF
63.5
1234789-HpCDF
ND
0.298
ES 1234789-HpCDF
48.6
OCDF
ND
0.55
ES OCDF
44.4
Totals
Standard
CS Recoveries
CS 37CI-2378-TCDD
84.5
Total TCDD
ND_
0.312
ND
CS 12347-PeCDD
101
_
Total PeCDD
-- ND`
0:314 —
ND
—
CS 12346-PeCDF -�
- 113
e
Total HxCDD
ND
0.242
ND
CS 123469-HxCDF
124
Total HpCDD
ND
0.339
ND-,,
CS 1234689-HpCDF
108
Total TCDF,
ND
0.246
ND
e,
Total PeCDF
ND
ND
0.17
01-165,
ND
Total HxCDF,
ND.
Total HpCDF
ND
0.214
ND
_
Total'PCDD/Fs
ND
ND
WHO-2005 TEQs
TEQs' ND=O
0
0
5500 Business Drive
TEQ: ND=DU20.428
_
__—0.428
0.855
-------------
0.428
— _ �_v
0.855-
-----------------
Wilmington, NC 28405, USA
www.us.sgs.com
--�
TEQND=DL °_-0.855
— —
_
Tel: [phone]; Toll -Free 866 846-8290
WOWe@ e: 064-609-WZX SGS North AmREigw-MFo6&2l8 Report Created: 06 -Dec -2016 08:18 Analyst: pw

METHOD 1613B
PCDD/F ONGOING PRECISION AND RECOVERY (OPR)
FORM 8A
Lab Name:
SGS North America
Initial Calibration:
ICAL: MM7 DF 12212015
01JUN2016
Instrument ID:
MM7
GC Column ID:
ZB-5ms
VER Data Filename:
161205X02
Analysis Date:
04 -DEC -2016 14:31:09
Lab ID:
OPR1 14514 DF
SPIKE
CONC.
RANGE
NATIVE ANALYTES
CONC.
FOUND
(ng/mL)
OK
2,3,7,8-TCDD
10
10.6
6.7
- 15.8
Y
1,2,3,7,8-PeCDD
50
50
35
- 71
Y
1,2,3,4,7,8-HxCDD
50
59.4
35
- 82
Y
1,2,3,6,7,8-HxCDD
50-
60.1
38
- 67
Y
1,2,3,7,8,9-HxCDD
50
57.4
32
- 81
Y
1,2,3,4,6,7,8-HpCDD
50
58.4
35
- 70
Y
OCDD
100
115
78
- 144
Y
2,3,7,8-TCDF
10
14
7.5
- 15.8
Y
1,2,3,7,8-PeCDF
50
57.6
40
- 67
Y
2,3,4,7,8-PeCDF
50
57
34
- 80
Y
1,2,3,4,7,8-HxCDF
50
52.8
36
- 67
Y
1,2,3,6,7,8-HxCDF
50
51.5
42
- 65
Y
2,3,4,6,7,8-HxCDF
50
52.7
35
- 78
Y
1,2,3,7,8,9-HxCDF
50
51.6
39
- 65
Y
1,2,3,4,6,7,8-HpCDF
50
51.8
41
- 61
Y
1,2,3,4,7,8,9-HpCDF
50
50.6
39
- 69
Y
OCDF
100
107
63
- 170
Y
Contract -required concentration limits for OPR as specified in Table 6,
Method 1613. 10/94
Processed: 06 Dec 2016 08:11 Analyst: pw
WO# A9421 Page 36 of 42
�A
l

j
METHOD 1613B
PCDD/F ONGOING PRECISION AND RECOVERY (OPR)
FORM 813
Lab Name:
SGS North America
Initial Calibration:
ICAL: MM7 DF 12212015
01JUN2016
Instrument ID:
MM7
GC Column ID:
ZB-5ms
VER Data Filename:
161205X02
Analysis Date:
04 -DEC -2016 14:31:09
Lab ID:
OPR1 14514 DF
SPIKE
CONC.
RANGE
LABELED ANALYTES
CONC.
FOUND
(ng/mL)
OK
13C -2,3,7,8-TCDD
100
54.6
20
- 175
Y
13C-1,2,3,7,8-PeCDD
100
51.4
21
- 227
Y
13C-1,2,3,4,7,8-HxCDD
100
60.9
21
- 193
Y
13C-1,2,3,6,7,8-HxCDD
100
60.6
25
- 163
Y
13C-1,2,3,7,8,9-HxCDD
100
55.6
26
- 166
Y
13C-1,2,3,4,6,7,8-HpCDD
100
64.3
26
- 166
Y
13C-OCDD
200
123
26
- 397
Y
13C-2,3,7,8-TCDF
100
55.3
22
- 152
Y
13C-1,2,3,7,8-PeCDF
100
59.5
21
- 192
Y
13C-2,3,4,7,8-PeCDF
100
58.3
13
- 328
Y
13C-1,2,3,4,7,8-HxCDF
100
71.1
19
- 202
Y
13C-1,2,3,6,7,8-HxCDF
100
73.5
21
- 159
Y
13C-2,3,4,6,7,8-HxCDF
100
69.6
22
- 176
Y
13C-1,2,3,7,8,9-HxCDF
100
57.7
17
- 205
Y
13C-1,2,3,4,6,7,8-HpCDF
100
85.5
21
- 158
Y
13C-1,2,3,4,7,8,9-HpCDF
100
62.7
20
- 186
Y
13C-OCDF
200
120
26
- 397
Y
CLEANUP STANDARD
37CI-2,3,7,8-TCDD
40
32.5
12.4
- 76.4
Y
Contract -required concentration limits for OPR as specified in Table 6,
Method 1613. 10/94
Processed: 06 Dec 2016 08:11
Analyst: pw
WO# A9421
Page 37 of 42

S-GS-
5500
Business Drive
Wilmington, NC 28405 USA
Tel: [phone]
Toll Free: 866 846-8290
Fax: [phone]
Sample Receipt Notification
Project Manager:
Amy Boehm
Receipt Date & Time:
10 -Nov -16 at 13:35
AP Project name:
'494? ;
Requested TAT:
;""' rgys
Projected due date:
28 -Nov -16
Matrix:
Tissue
Phone#:
910-794-1613
Email Address:
[e-mail]
Company Contact:
Sam Cooper
Company:
CZR, Inc.
Project Name & Site:
2026 AnnualFi,-/- Frgj,-c.f
Project PO#:
fnvoic,a /c arrternatianal Pape,;,
QAAP/Contract #:
N/A
Requested Analysis:
o• eSrte++l 16133, & % lipi6
Phone#:
9103929253
Email Address:
[e-mail]
Client Sm ID
p
WO# A9421
AP Sm ID
p
Sample Condition & Notes
p
Quantity Size
Q
Sampling
Date
Sampling Time
p g
Received Container #
Temp
Shipping #
pp g
Comp 1 Site 1 Bluegill
A9421001
`; �c�)C-)
Bluegill (10 "A" Fillets)
10 Bag
20 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 2 Site 1 Bluegill
A9421002
Bluegill (10 "A" Fillets)
10 Bag
20 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 3 Site 1 Blue Catfish
A9421003
Blue Catfish (10 "A" Fillets)
10 Bag
20 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 4 Site 1 Common Carp
A9421004
Common Carp (6 "A" Fillets)
6 Bag
21 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 5 Site 2 Bluegill
A9421_005
Bluegill (10 "A" Fillets)
10 Bag
20 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 6 Site 2 Bluegill
A9421006
Bluegill (5 "A" Fillets)
5 Bag
02 -Nov -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 7 Site 2 Blue Catfish
A9421_007
Blue Catfish (10 "A" Fillets)
10 Bag
21 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 8 Site 2 Common Carp
A9421_008
Common Carp (10 "A" Fillets)
10 Bag
21 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 9 Site 3 Bluegill
A9421_009
Bluegill (6 "A" Fillets)
6 Bag
02 -Nov -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 10 Site 3 Blue Catfish
A9421_010
Blue Catfish (10 "A" Fillets)
10 Bag
01 -Nov -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 11 Site 3 Blue Catfish
A9421011
Blue Catfish (5 "A" Fillets)
5 Bag
02 -Nov -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 12 Site 3 Common Carp A9421_012
Common Carp (10 "A" Fillets)
10 Bag
02 -Nov -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Comp 13 Site 1 Blue Catfish - Replicate A9421013
Blue Catfish - Replicate (10 "B" Fillets)
10 Bag
20 -Sep -16
00:00
-6.5,-11.3
1,2
N/A,N/A,
Preservation Type:
ample Seals:
No
Any un -extracted sample will be stored for 90 days from
reporting date. Additional storage fees may apply for any
samples stored longer than 90 days.
Notes/Comments:
Samples received intact.
Received by: Ashley Owens Logger/ in bv: Ashlev Owens
All services are rendered in accordance with the applicable SGS General Conditions of Service accessible via: http://www.sgs.com/terms and conditions.htm
Qced by: AK I I Nov 16
WO# A9421
Page 38 of 42
SGS North America
�'
AML [•"�'�,{���. ��'l i.
ll �1i ( �i��i -) )�
`; �c�)C-)
�, �)i
Il���� i� ;i C
��� )l� ;', l,_
i %- �� �,� � .

/-"Lt/— '•/ 1
nd
4709 COLLEGE ACRES DRIVE
ZRSUITE 2
INC ORPORATED WILMINGTON, NORTH CAROLINA 283-1725
TEL [phone]
ENVIRONMENTAL CONSULTANTS FAX [phone]
CHAIN OF CUSTODY czrWIm@czr-inc-com
TO: SGS Environmental Services
Attn: Amy Boehm
5500 Business Drive
Wilmington, NC 28405
DATE: 10 November 2016
RE: International Paper Company, Inc., 2016 Annual Fish Project
FROM: Randall L. Pulley
CZR Incorporated, Suite 2
4709 College Acres Drive
Wilmington, NC 28403
[e-mail]
TESTS: Analysis of fish tissues for percent lipid (extraction) and 2, 3, 7, 8 TCDD (Dioxin), 2, 3, 7, 8, TCDF
(Furan) with full screen of congeners (P61ychlorinated Dibenzodioxins and Polychlorinated Dibenzofurans)
via EPA Method 1613B.
s
ENCLOSED ITEMS:
Thirteen (13) frozen composite fish tissue (fillets) samples, each fillet wrapped in aluminum foil (dull side toward
fish) and enclosed in labeled "zip -lock' plastic bags. Composites are identified below.
SAMPLE ID #
Composite # Site
Species (number of fish fillets)
I I
Bluegill (10 "A" fillets)
i 2 1
Bluegill (10 "A" fillets)
3 1
Blue Catfish (10 "A" fillets)
4 1
Common Carp (6 "A" fillets)
5 2
Bluegill (10 "A" fillets)
6 2
Bluegill (5 "A" fillets)
7 2
Blue Catfish (10 "A" fillets)
8 2
Common Carp (10 "A" fillets)
9 ;
Bluegill (6 "A" fillets)
10 3
Blue Catfish (10 "A"fillets)
11 3
Blue Catfish (5 "A" fillets)
,w 12 3
Common Carp (10 "A" fillets)
e -13 1
Blue Catfish - replicate (10 "B" fillets)
COMMENTS:
- Send one digital version and two hard copies of the report to Sam Cooper/CZR at the above address. We
also request permission to include the report as an appendix
to CZR's report summarizing the 2016
collection efforts and results.
- - Forward the invoice to International Paper -Riegelwood, Shared Services, P.O. Box 792, Milford, OH
45150
- - A detailed fish composite data table is also enclosed.
(11(o to,
Q2:_Relinquished by: ate/time
1 _ L9•50
-- 1 � din I •! � .
` Received by: Date/time �1t
CZR CP# 40.4 •`' •
WO# A9421 Page AQ ^f AO
-3902
2151 Aitemate AIA South • SUITE 2000 • JUPITER, FLORIDA 33477

Site 1- 2016
International Paper - Cape Fear River
Label foil with "Site 2, Bluegill (1), date caught, 'A' or'B"' Put same species from same site in zip -lock by A or B fillet. A = left fillet
M M, M171
Date Caught
By:
Date Filleted
By
Site
Species (#)
Total Length (mm) Total Weight (g)
Fillet A Weight (g)
Fillet B Weight (g)
Composite #
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Catfish (9)
569
2495
275
f
3
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Catfish (12)
577
2675
9/21/2016
RP/MW
9/22/2016
RP
1
Blue Catfish (22)
604
2800
310
_
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Catfish (14)-
589
2903
305
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Catfish (15)
599
3220
340
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Catfish (7)
602
3243
300
`
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Catfish (11)
599
3265
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Catfish (5)
617
3606
415
31
9/21/2016
RP/MW
9/22/2016
RP
1
Blue Catfish (23)
640
4000
450
2
9/21/2016
RP/MW
9/22/2016
RP
1
Blue Catfish (17)
668
4300
515
,9/20/2016
RP/MW
9/21/2016
SC
1
Bluegill(8)
137
48
6
6
1
9/21/2016
RP/MW
9/22/2016
RP
1
Bluegill(20)
145
50
6
6
9/21/2016
RP/MW
9/22/2016
RP
1
Bluegill(21)
145
50
6
6
9/21/2016
RP/MW
9/22/2016
RP
1
Bluegill(17)
147
55
9
9
9/21/2016
RP/MW
9/22/2016
RP
1
Bluegill(12)
156
60
9
9
9/20/2016
RP/MW
9/21/2016
SC
1
Bluegill(4)
146
62
9
9
9/20/2016
RP/MW
9/21/2016
SC
1
Bluegill(9)
146
65
6
3
9/21/2016
RP/MW
9/22/2016
RP
1
Bluegill(13)
160
65
9
9
9/21/2016
RP/MW
9/22/2016
RP
1
Bluegill(16)
156
65
11
9
9/21/2016
RP/MW
9/22/2016
RP
1
eluegill(18)
151
65
9
9
9/20/2016
RP/MW
9/21/2016
SC
1
Blue Illi(2)
1_52
64
9 _
9 I
2
9/20/2016
RP/MW
9/21/2016
SC
1
Bl III(3)
151
_ 68 _
_ 6
_ 9
9/20/2016
AP/MW
9/21/2016
SC
1
B1Pe ,ill (1}
156
_ 31
_ _ 11
9
9/20/2016
RP1MW
9121/2016
SC
Y
elue tll(7)
165
$S
_ 11 _
11
9/2012016
RP/MW
9/21/2016
SC
1
Blue ill(5)
165
91
14
14
9/20/2016
RP/MW
9/21/2016
SC
1
Blue 01(10) i
175
105
14 _
11 _
9/2112016
RP/MW
_9/22/2016_
RP _ _
1
8i 111IIS)
171
110
14
17
9/2012016
RP/MW
1 9/21/2016
SC
1
Bluevil (6)
180
113 _
14 _
_ 11 _
9/21%2016
RP/MW
1 9/12/2016
RP
1
Blue&19(14)
182
115
17 _
17 _
9/21/2016
RP/MW
9/22/2016
RP
1
BIue8n) 19i
194_
130
17 _
17
-w tit —
„ "• `"i. _°zlra`, ..` `s.:ai
=$fir :�. -'�,';: - _k, .:fix
_ *r; °'.-
_: t:- yn'= '.4,�w i' .�J_
=.a
9/21/2016
RP/MW
9/22/2016
RP
1
Common Carp (5)
468
2150
160
160
4
9/20/2016
RP/MW
9/21/2016
SC
1
Common Carp (1)
600
3719
260
335
9/20/2016
RP/MW
9/21/2016
SC
1
Common Carp (3)
560
3810
270
310
9/20/2016
RP/MW
9/21/2016
SC,
1
Common Carp (2)
587
3856
305
345
9/21/2016
RP/MW
9/22/2016
RP
1
Common Carp (6)
628
4050
470
365
9/21/2016
RP/MW
9/22/2016
RP
1
CommonCarp'(4)
610
4100
390
340
WO# A9421
Page 40 of 42

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Site 3 - 2016]
Site 3
Bluegill
6
1,2,3,4,5,6 - A fillets - - - I
International Paper - Cape Fear River
Site 3
Blue catfish
10
1,2,4,6,9,10,11,13,15,18 -A fillets
Composite 11
Site 3
Mue catf3t
S5,7,8,12,17-A
fillets
[Composite 12,
Site 3,,
mon
�,omcar
__. _
_P-
10,
Label foil with "Site 2, Bluegill (1), date caught, 'A' or'B"' Put same species from same site in zip -lack by A or B fillet. A = left fillet
IF -
Date Caught
By:
Date Filleted
By
Site
Species (#)
Total Length (mm)
Total Weight (g)
Fillet A Weight (g)
Fillet B Weight (g)
Composite #
W I
,
-
11/1/2016
ZG/MW
11/3/2016
CM
3
Blue Catfish (11)
560
2100
195
250
10
11/1/2016
ZG/MW
11/3/2016
LLB
3
Blue Catfish (13)
560
2500
310
275
11/1/2016
ZG/MW
11/3/2016
CM
3
Blue Catfish (4) -
590
2520
300
290
11/1/2016
ZG/MW
11/3/2016
LLB
3
Blue Catfish (2)
610
3300
445
410
11/1/2016
ZG/MW
11/3/2016
CM
3
Blue Catfish (18)
640
3300
553
520
11/1/2016
ZG/MW
11/3/2016
CM
3
Blue Catfish (10)
655
3525
485
420
11/2/2016
ZG/MW
11/3/2016
CM
3
Blue Catfish (15)
715
3850
530
495
11/2/2016
ZG/MW
11/3/2016
CM
3
Blue Catfish (6)
645
3950
510
425
11/2/2016
ZG/MW
11/3/2016
SC
3
Blue Catfish (9)
690
4000
630
570
11/2/2016
ZG/MW
11/3/2016
SC
3
Blue Catfish (1)
650
4100
1 700
705
11/2/2016
ZG/MW
11/3/2016
CM
3
Blue Catfish (S)
695
4400
700
735
11
11/2/2016
ZG/MW
11/3/2016
Sc
3
—Blue Catfish f12)
695
4550
475
430
11/2/2016
ZG/MW
1 11/3/2016
SIC
3
Blue Catfish (17)
735
5250
770
700
11/3/1016
ZG/MW
11/4/2016
NT
3
Blue CatfM (8)
745
5450
ass
900
11/312016
ZG/MW
1114/2016
CM
3
Blue Catfish (7)
800
7910
1260
1200
U
41,
11/2/2016
ZG/MW
11/4/2016
CM
3
Bluegill (5)
185
ISO
11
14
9
11/2/2016
ZG/MW
11/4/2016
NT
3
Bluegill (4)
120
170
20
20
11/2/2016
ZG/MW
11/4/2016
NT
3
Bluegill (2)
160
180
31
28
11/7/2016
RP/LLB
11/8/2016
RP
3
Bluegill (6)
208
205
28
28
11/2/2016
ZG/MW
11/4/2016
CM
3
Bluegill (3)
215
221
65
57
11/1/2016
ZG/MW
11/3/2016
LLB
3
Bluegill (1)
220
260
so
47
'AW,41" _-, `7 - . �,
, I ,
I __ :,
, ,
1, , R
11/2/2016
ZG/MW
11/4/2016
SC
3
Common Carp (9)
505
2800
335
290
'12
11/2/2016,
ZG/MW
11/4/2016
CM
3,
Common Carp (11)
505
2950
285
280
11/2/2016
ZG/MW
11/4/2016
CM
3
Common Carp (10)
530
3000
275
240
°11/1/2016
ZG/MW
CM
3
Common Carp (1)
530
3150
345
315
11/2/2016
ZG/MW
_11/3/2016
11/4/2016
NT
3
Common Carp (13)
585
3150
258
280
11/2/2016
'ZG/MW
11/4/2016
CM
3
Common Carp (12)
550
3200
323,,,
270
11/1/2016
ZG/MW
11/3/2016
LLB
3
Common Carp (2)
540
3350
290
340
11/1/2016
ZG/MW
11/3/2016
CM
3
Common Carp (6)
620
3535
370
350
11/2/2016
ZG/MW
11/4/2016
SC
3
common Carp (8)
615
4300
420
380
7MM,
ZG MW11/3/2016
SC
3
1 Common Carp (7)
715
5200
570
'590
_,gomposite 9
Site 3
Bluegill
6
1,2,3,4,5,6 - A fillets - - - I
Composite 10
Site 3
Blue catfish
10
1,2,4,6,9,10,11,13,15,18 -A fillets
Composite 11
Site 3
Mue catf3t
S5,7,8,12,17-A
fillets
[Composite 12,
Site 3,,
mon
�,omcar
__. _
_P-
10,
1, 3 , &fll
WO# A9421
Page 42 of 42