WQ0003698_Monitoring - 11-2016_20161207

1
November, 30, 2016
CITY OF MARION
P.O. Drawer 700
Marion, North Carolina 28752
NC Department of Environment & Natural Resources
Division of Water Quality — Information Processing Unit
1617 Mail Service Center, Raleigh NC 27669-1617
RE: Marion WWTP
NPDES Permit No. WQ0003698
Attached is a copy of the Permit Groundwater Monitoring sampling event conducted on
November,7,2016 for the City of Marion WWTP. If you have any further questions or
require additional information, please let us know.
Sincerely,
Larry Carver, WWTP Superintendent
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OFFICE OF THE
WASTE TREATMENT
PLANT SUPERVISOR

>? Environmental Testing Solutions, Inc.
Project name: City of Marion
Collection date:
Date received:
7 -Nov -16
7 -Nov -16
Sample identification: .MW # 1 - Grab
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 161107.503
Sample number: 142371
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
_
Solids, Total Suspended
SM 2540 D
20
5.0
mg/L
9 -Nov -16
KEK
Solids, Total Dissolved
SM 2540 C
28
10
mg/L
9 -Nov -16
KEK
Total Coliform
SM 9221 B
<1.1
1.1
mg/L
7 -Nov -16
KEK
Phenolics
420.1
<0.005
0.005
mg/L
16 -Nov -16
EDH
I
Arsenic
200.8
<0.010
0.010
mg/L
14 -Nov -16
DER
1
Cadmium
200.8
<0.001
0.001
mg/L
14 -Nov -16
DER
1
Iron
200.7
0.60
0.050
mg/L
10 -Nov -16
MER
1
Lead
200.8
<0.005
0.005
mg/L
14 -Nov -16
DER
1
Total Organic Carbon
SM 5310 C
<1.00
1.00
mg/L
16 -Nov -16
LCB
1
6230 D
6230 D
See attached sheets
11 -Nov -16
JM1
2
Sample identification: MW # 2 Grab
Sample number:
142372
Parameter
Method
Result
RL
Units .
Date
Analyst
Footnotes
Analyzed
_
Solids, Total Suspended
SM 2540 D
870
5.0
mg/L
9 -Nov -16
KEK
Solids, Total Dissolved
SM 2540 C
100
10
mg/L
9 -Nov -16
KEK
Total Coliform
SM 9221 B
<1.1
1.1
mg/L
7 -Nov -16
KEK
Phenolics
420.1
<0.005
0.005
mg/L
16 -Nov -16
EDH
1
Arsenic
200.8
<0.010
0.010
mg/L
14 -Nov -16
DER
1
Cadmium
200.8
<0.001
0.001
mg/L
14 -Nov -16
DER
1
Iron
200.7
48
5.0
mg/L
11 -Nov -16
MER
1
Lead
200.8
0.013
0.005
mg/L,
14 -Nov -16
DER
1
Total Organic Carbon
SM 5310 C
1.71
1.00
mg/L
16 -Nov -16
LCB
1
6230D
6230D
See attached sheets
11 -Nov -16
JM1
2
Sample identification: MW # 3 - Grab
Sample number:
142373
Parameter
Method
Result
RL
Units
Date
Analyst
Footnotes
Analyzed
Solids, Total Suspended
SM 2540 D
250
5.0
mg/L
9 -Nov -16
KEI<
Solids, Total Dissolved
SM 2540 C
340
10
mg/L
9 -Nov -16
KEI<
Total Coliform
SM 9221 B
<1.1
1.1
mg/L
7 -Nov -16
KEK
Phenolics
420.1
<0.005
0.005
mg/L
16 -Nov -16
EDH
I
Arsenic
200.8
<0.010
0.010
mg/L
14 -Nov -16
DER
1
Cadmium
200.8
0.003
0.001
mg/L
14 -Nov -16
DER
1
Iron
200.7
6.6
0.50
mg/L
11 -Nov -16
MEC
I
Lead
200.8
0.012
0.005
mg/L
14 -Nov -16
DER
1
Total Organic Carbon
SM 5310 C
1.61
1.00
mg/L
16 -Nov -16
LCB
1
6230 D
6230 D
See attached sheet's
11 -Nov -16
JM1
2
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

1D) � }T
°AA
* Environmental Testing Solutions, Inc.
Project name: City of Marion
Collection date:
Date received:
7 -Nov -16
7 -Nov -16
Sample identification: MW 44 - Grab
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 161107.503
Sample number: 142374
Parameter
Method
Result
RL
Units
Date
Analyzed
Analyst
Footnotes
Solids, Total Suspended
SM 2540 D
86
5.0
mg/L
9 -Nov -16
KEK
Solids, Total Dissolved
SM 2540 C
39
10
mg/L
9 -Nov -16
KEK
Total Coliform
SM 9221 B
<l.l
1.1
mg/L
7 -Nov -16
KEK
Phenolics
420.1
<0.005
0.005
mg/L
16 -Nov -16
EDH
1
Arsenic
200.8
<0.010
0.010
mg/L
14 -Nov -16
DER
1
Cadmium
200.8
<0.001
0.001
mg/L
14 -Nov -16
DER
1
Iron
200.7
0.93
0.050
mg/L
10 -Nov -16
MEC
1
Lead
200.8
<0.005
0.005
mg/L
14 -Nov -16
DER
1
Total Organic Carbon
SM 5310 C
1.01
1.00
mg/L
16 -Nov -16
LCB
1
6230 D
6230 D
See attached sheets
11 -Nov -16
JMl
2
Footnotes:
RL = Reporting Limit. Values are reported down to the Reporting Limit only.
1. Sample analyzed by Rogers & Callcott Environmental.
2. Sample analyzed by Shealy Environmental, Inc.
Date reviewed: ('14, k(0
Data reviewed by: Kelley E. Keenan
Signature:
L.
NC Certification Number: 600
SC Certification Number: 99053
NC Drinking Water Certification Number: 37786
This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.

SM 6230D List + IPE & MTBE
Client: Environmental Testing Solutions, Inc. Laboratory ID: RK10008-001
Description: MW 1 Matrix: Aqueous
Date Sampled:11/07/2016 0904
Date Received: 11/10/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 50308 82608 1 11/11/20161128 JM1 26582
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 5 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
ND
0.50
ug/L
1
Bromobenzene
108-86-1
8260B
ND
0.50
ug/L
1
Bromochloromethane
74-97-5
8260B
ND
0.50
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
0.50
ug/L
1
Bromoform
75-25-2
82606
ND
0.50
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
0.50
ug/L
1
n-Butylbenzene
104-51-8
8260B
ND
0.50
ug/L
1
sec-Butylbenzene
135-98-8
8260B
ND
0.50
ug/L
1
tert-Butylbenzene
98-06-6
8260B
ND
0.50
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
0.50
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
0.50
ug/L
1
Chloroethane
75-00-3
8260B
ND
0.50
ug/L
1
Chloroform
67-66-3
8260B
ND
0.50
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
0.50
ug/L
1
2-Chlorotoluene
95-49-8
8260B
ND
0.50
ug/L
1
4-Chlorotoluene
106 43-4
8260B
ND
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
0.50
ug/L
1
Dibromochloromethane
124-48-1
8260B
ND
0.50
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
0.50
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
8260B
ND
0.50
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
0.50
ug/L
1
1,3 -Dichlorobenzene
541-73-1
8260B
ND
0.50
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
0.50
ug/L
1
Dichlorodifluoromethane
75-71-8
82608
ND
0.50
ug/L
1
1,1-Dichloroethane
75-34-3
82608
ND
0.50
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
0.50
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
0.50
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
0.50
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
0.50
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
0.50
ug/L
1
1,3-Dichloropropane
142-28-9
82608
ND
0.50
ug/L
1
2,2-Dichloropropane
594-20-7
8260B
ND
0.50
ug/L
1
1,1-Dichloropropene
563-58-6
8260B
ND
0.50
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
0.50
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8260B
ND
0.50
ug/L
1
Isopropylbenzene
98-82-8
8260B
ND
0.50
ug/L
1
p-Isopropyltoluene
99-87-6
8260B
ND
0.50
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
0.50
ug/L
1
Methylene chloride
75-09-2
8260B
ND
0.50
ug/L
1
Naphthalene
91-20-3
8260B
ND
0.50
ug/L
1
n-Propylbenzene
103-65-1
8260B
ND
0.50
ug/L
1
Styrene
100-42-5
8260B
ND
0.50
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
0.50
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 5 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SM 6230D List + IPE & MTBE
Client: Environmental Testing Solutions, Inc. Laboratory ID: RK10008-001
Description: MW 1 Matrix: Aqueous
Date Sampled:11/07/2016 0904
Date Received: 11/10/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 826OB 1 11/11/2016 1128 JM1 26582
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
CAS Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
0.50
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
0.50
ug/L
1
Toluene
108-88-3
8260B
ND
0.50
ug/L
1
1,2,3-Trichlorobenzene
87-61-6
826OB
ND
0.50
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
82608
ND
0.50
ug/L
1
1,1,1 -Trichloroethane
71-55-6
826OB
ND
0.50
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
0.50
ug/L
1
Trichloroethene
79-01-6
82608
ND
0.50
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
0.50
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
0.50
ug/L
1
1,2,4-Trimethylbenzene
95-63-6
826OB
ND
0.50
ug/L
1
1,3,5-Trimethylbenzene
108-67-8
8260B
ND
0.50
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
0.50
ug/L
1
m+p - Xylenes
179601-23-1
8260B
ND
0.50
ug/L
1
o - Xylenes
95-47-6
8260B
ND
0.50
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
104 70-130
Bromofluorobenzene
104 70-130
Toluene -d8
106 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 6 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SM 6230D List +IPE & MTBE
Client: Environmental Testing Solutions, Inc. Laboratory ID: RK10008-002
Description: MW 2 Matrix: Aqueous
Date Sampled: 1110712016 0935
Date Received: 11 /1 01201 6
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 11/11/20161152 JM1 26582
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 7 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
CAS
Analytical
Parameter
-Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
ND
0.50
ug/L
1
Bromobenzene
108-86-1
8260B
ND
0.50
ug/L
1
Bromochloromethane
74-97-5
82608
ND
0.50
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
0.50
ug/L
1
Bromoform
75-25-2
8260B
ND
0.50
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
0.50
ug/L
1
n-Butylbenzene
104-51-8
8260B
ND
0.50
ug/L
1
sec-Butylbenzene
135-98-8
8260B
ND
0.50
ug/L
1
tert-Butyl benzene
98-06-6
8260B
ND
0.50
ug/L
1
Carbon tetrachloride
56-23-5
82608
ND
0.50
ug/L
1
Chlorobenzene
108-90-7
8260B
ND
0.50
ug/L
1
Chloroethane
75-00-3
8260B
ND
0.50
ug/L
1
Chloroform
67-66-3
8260B
ND
0.50
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
0.50
ug/L
1
2-Chlorotoluene
95-49-8
82608
ND
0.50
ug/L
1
4-Chlorotoluene
106-43-4
82608
ND
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
82608
ND
0.50
ug/L
1
Dibromochloromethane
124-48-1
82608
ND
0.50
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
82608
ND
0.50
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
82608
ND
0.50
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
0.50
ug/L
1
1,3 -Dichlorobenzene
541-73-1
8260B
ND
0.50
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
0.50
ug/L
1
Dichlorodifluoromethane
75-71-8
8260B
ND
0.50
ug/L
1
1,1-Dichloroethane
75-34-3
82608
ND
0.50
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
0.50
ug/L
1
1,1-Dichloroethene
75-35-4
8260B
ND
0.50
ug/L
1
cis- 1,2-Dichloroethene
156-59-2
8260B
ND
0.50
ug/L
1
trans-1,2-Dichloroethene
156-60-5
8260B
ND
0.50
ug/L
1
1,2-Dichloropropane
78-87-5
8260B
ND
0.50
ug/L
1
1,3-Dichloropropane
142-28-9
8260B
ND
0.50
ug/L
1
2,2-Dichloropropane
594-20-7
8260B
ND
0.50
ug/L
1
1,1-Dichloropropene
563-58-6
8260B
ND
0.50
ug/L
1
Diisopropyl ether (IPE)
108-20-3
82608
ND
0.50
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
82608
ND
0.50
ug/L
1
Isopropylbenzene
98-82-8
8260B
ND
0.50
ug/L
1
p-Isopropyltoluene
99-87-6
8260B
ND
0.50
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
82608
ND
0.50
ug/L
1
Methylene chloride
75-09-2
8260B
ND
0.50
ug/L
1
Naphthalene
91-20-3
8260B
ND
0.50
ug/L
1
n-Propylbenzene
103-65-1
8260B
ND
0.50
ug/L
1
Styrene
100-42-5
8260B
ND
0.50
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
0.50
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 7 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SM 6230D List + IPE & MTBE
Client: Environmental Testing Solutions, Inc. Laboratory ID: RK10008-002
Description: MW 2 Matrix: Aqueous
Date Sampled: 1110712016 0935
Date Received: 11/10/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 11/11/20161152 JM1 26582
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation -of compound exceeded the calibration range H = Oul of holding time
ND = Not detected at or above the PQL J = Estimated result - PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 8 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
CAS Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
0.50
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
0.50
ug/L
1
Toluene
108-88-3
8260B
ND
0.50
ug/L
1
1,2,3-Trichlorobenzene
87-61-6
8260B
ND
0.50
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260B
ND
0.50
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND
0.50
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
0.50
ug/L
1
Trichloroethene
79-01-6
82606
ND
0.50
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
0.50
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
0.50
Llg/L
1
1,2,4-Trimethylbenzene
95-63-6
8260B
ND
0.50
ug/L
1
1,3,5 -Trim ethyl benzene
108-67-8
8260B
ND
0.50
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
0.50
ug/L
1
m+p - Xylenes
179601-23-1
8266B
ND
0.50
ug/L
1
o - Xylenes
95-47-6
8260B
ND
0.50
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
102 70-130
Bromofluorobenzene
102 70-130
Toluene -d8
105 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation -of compound exceeded the calibration range H = Oul of holding time
ND = Not detected at or above the PQL J = Estimated result - PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W'
Shealy Environmental Services, Inc. Page: 8 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SM 6230D List + IPE & MTBE
Client: Environmental Testing Solutions, Inc. Laboratory ID: RK10008-003
Description: MW 3 Matrix: Aqueous
Date Sampled:1110712016 1021
Date Received: 11/10/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 11/11/20161215 JM1 26582
PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 Of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax[phone] www.shealylab.com
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
ND
0.50
ug/L
1
Bromobenzene
108-86-1
8260B
ND
0.50
ug/L
1
Bromochloromethane
74-97-5
82608
ND
0.50
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
0.50
ug/L
1
Bromoform
75-25-2
8260B
ND
0.50
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
0.50
ug/L
1
n-Butylbenzene
104-51-8
8260B
ND
0.50
ug/L
1
sec-Butylbenzene
135-98-8
8260B
ND
0.50
ug/L
1
tert-Butyl benzene
98-06-6
82608
ND
0.50
ug/1-
1
Carbon tetrachloride
56-23-5
82608
ND
0.50
ug/L
1
Chlorobenzene
108-90-7
82608
ND
0.50
ug/L
1
Chloroethane
75-00-3
82608
ND
0.50
ug/L
1
Chloroform
67-66-3
8260B
ND
0.50
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
8260B
ND
0.50
ug/L
1
2-Chlorotoluene
95-49-8
82608
ND
0.50
ug/L
1
4-Chlorotoluene
106-43-4
8260B
ND
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
8260B
ND
0.50
ug/L
1
Dibromochloromethane
124-48-1
82608
ND
0.50
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
0.50
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
82608
ND
0.50
ug/L
1
1,2 -Dichlorobenzene
95-50-1
8260B
ND
0.50
ug/L
1
1,3 -Dichlorobenzene
541-73-1
8260B
ND
0.50
ug/L
1
1,4 -Dichlorobenzene
106-46-7
8260B
ND
0.50
ug/L
1
Dichlorodifluoromethane
75-71-8
8260B
ND
0.50
ug/L
1
1,1-Dichloroethane
75-34-3
82608
ND
0.50
ug/L
1
1,2-Dichloroethane
107-06-2
8260B
ND
0.50
ug/L
1
1,1-Dichloroethene
75-35-4
82608
ND
0.50
ug/L
1
cis-1,2-Dichloroethene
156-59-2
82608
ND
0.50
ug/L
1
trans-1,2-Dichloroethene
156-60-5
82608
ND
0.50
ug/L
1
1,2-Dichloropropane
78-87-5
82608
ND
0.50
ug/L
1
1,3-Dichloropropane
142-28-9
8260B
ND
0.50
ug/L
1
2,2-Dichloropropane
594-20-7
82608
ND
0.50
ug/L
1
1,1-Dichloropropene
563-58-6
8260B
ND
0.50
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
0.50
ug/L
1
Ethylbenzene
100-41-4
8260B
ND
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8260B
ND
0.50
ug/L
1
Isopropylbenzene
98-82-8
8260B
ND
0.50
ug/L
1
p-Isopropyltoluene
99-87-6
8260B
ND
0.50
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
82608
ND
0.50
ug/L
1
Methylene chloride
75-09-2
8260B
ND
0.50
ug/L
1
Naphthalene j
91-20-3
8260B
ND
0.50
ug/L
1
n-Propylbenzene
103-65-1
8260B
ND
0.50
ug/L
1
Styrene
100-42-5
8260B
ND
0.50
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
0.50
ug/L
1
PQL = Practical quantitation limit 8 = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 9 Of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax[phone] www.shealylab.com

SM 62300 List + IPE & MTBE
Client: Environmental Testing Solutions_, Inc. Laboratory ID: RK'10008-003
Description: MW 3 Matrix: Aqueous
Date Sampled:11/0712016 1021
Date Received: 11/1012016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 5030B 8260B 1 11/11/20161215 JM1 26582
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
CAS Analytical
Parameter
Number Method
Result Q
PQL
Units
Run
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
0.50
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
0.50
ug/L
1
Toluene
108-88-3
8260B
ND
0.50
ug/L
1
1,2,3-Trichlorobenzene
87-61-6
8260B
ND
0.50
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
82608
ND
0.50
ug/L
1
1,1,1 -Trichloroethane
71-55-6
8260B
ND.
0.50
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
0.50
ug/L
1
Trichloroethene
79-01-6
8260B
ND
0.50
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
0.50
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
0.50
ug/L
1
1,2,4-Trimethylbenzene
95-63-6
8260B
ND
0.50
ug/L
1
1,3,5-Trimethylbenzene
108-67-8
8260B
ND
0.50
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
0.50
ug/L
1
m+p- Xylenes
179601-23-1
8260B
ND
0.50
ug/L
1
o - Xylenes
95-47-6
8260B
ND
0.50
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
102 70-130
Bromofluorobenzene
106 70-130
Toluene -d8
109 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 10 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

SM 6230D List + IPE & MTBE
Client: Environmental Testing Solutions, Inc. Laboratory ID: RK10008-004
Description: MW 4 Matrix: Aqueous
Date Sampled:11/07/2016 0832
Date Received: 11/10/2016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 50308 8260B 1 11/11/20161239 JM1 26582
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc." Page: 11 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
CAS
Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
Benzene
71-43-2
8260B
ND
0.50
ug/L
1
Bromobenzene
108-86-1
82608
ND
0.50
ug/L
1
Bromochloromethane
74-97-5
82608
ND
0.50
ug/L
1
Bromodichloromethane
75-27-4
8260B
ND
0.50
ug/L
1
Bromoform
75-25-2
82608
ND
0.50
ug/L
1
Bromomethane (Methyl bromide)
74-83-9
8260B
ND
0.50
ug/L
1
n-Butylbenzene
104-51-8
8260B
ND
0.50
ug/L
1
sec-Butylbenzene
135-98-8
8260B
ND
0.50
ug/L
1
tert-Butylbenzene
98-06-6.
82608
ND
0.50
ug/L
1
Carbon tetrachloride
56-23-5
8260B
ND
0.50
ug/L
1
Chlorobenzene
108-90-7
82608
ND
0.50
ug/L
1
Chloroethane
75-00-3
82608
ND
0.50
ug/L
1
Chloroform
67-66-3
8260B
ND
0.50
ug/L
1
Chloromethane (Methyl chloride)
74-87-3
82608
ND
0.50
ug/L
1
2-Chlorotoluene
95-49-8
82608
ND
0.50
ug/L
1
4-Chlorotoluene
106-43-4
8260B
ND
0.50
ug/L
1
1,2-Dibromo-3-chloropropane (DBCP)
96-12-8
82608
ND
0.50
ug/L
1
Dibromochloromethane
124-48-1
82608
ND
0.50
ug/L
1
1,2-Dibromoethane (EDB)
106-93-4
8260B
ND
0.50
ug/L
1
Dibromomethane (Methylene bromide)
74-95-3
82608
ND
0.50
ug/L
1
1,2 -Dichlorobenzene
95-50-1
82608
ND
0.50
ug/L
1
1,3 -Dichlorobenzene
541-73-1
82608
ND
0.50
ug/L
1
1,4 -Dichlorobenzene
106-46-7
82608
ND
0.50
ug/L
1
Dichlorodifluoromethane
75-71-8
8260B
ND
0.50
ug/L
1
1,1-Dichloroethane
75-34-3
8260B
ND
0.50
ug/L
1
1,2-Dichloroethane
107-06-2
82608
ND
0.50
ug/L
1
1,1-Dichloroethene
75-35-4
82608
ND
0.50
ug/L
1
cis-1,2-Dichloroethene
156-59-2
8260B
ND
0.50
ug/L
1
trans-1,2-Dichloroethene
156-60-5
82608
ND
0.50
ug/L
1
1,2-Dichloropropane
78-87-5
82608
ND
0.50
ug/L
1
1,3-Dichloro propane
142-28-9
82608
ND
0.50
ug/L
1
2,2-Dichloropropane
594-20-7
8260B
ND
0.50
ug/L
1
1,1-Dichloropropene
563-58-6
82608
ND
0.50
ug/L
1
Diisopropyl ether (IPE)
108-20-3
8260B
ND
0.50
ug/1-
1
Ethylbenzene
100-41-4
82608
ND
0.50
ug/L
1
Hexachlorobutadiene
87-68-3
8260B
ND
0.50
ug/L
1
Isopropylbenzene
98-82-8
8260B
ND
0.50
ug/L
1
p-Isopropyltoluene
99-87-6
8260B
ND
0.50
ug/L
1
Methyl tertiary butyl ether (MTBE)
1634-04-4
8260B
ND
0.50
ug/L
1
Methylene chloride
75-09-2
82606
ND
0.50
ug/L
1
Naphthalene
91-20-3
8260B
ND
0.50
ug/L
1
n-Propylbenzene
103-65-1
8260B
ND
0.50
ug/L
1
Styrene
100-42-5
8260B
ND
0.50
ug/L
1
1,1,1,2 -Tetrachloroethane
630-20-6
8260B
ND
0.50
ug/L
1
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc." Page: 11 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com

• SM 6230D List + IPE & MTBE
Client: Environmental Testing Solutions, Inc. Laboratory ID:RKI0008-004
Description: MW 4 Matrix: Aqueous
Date Sampled: 1110712016 0832
Date Received: 11/1012016
Run Prep Method Analytical Method Dilution Analysis Date Analyst Prep Date Batch
1 503OB 8260B 1 . 11/11/20161239 JM1 26582
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com
CAS Analytical
Parameter
Number
Method
Result Q
PQL
Units
Run
1,1,2,2 -Tetrachloroethane
79-34-5
8260B
ND
0.50
ug/L
1
Tetrachloroethene
127-18-4
8260B
ND
0.50
ug/L
1
Toluene
108-88-3
8260B
ND
0.50
ug/L
1
1,2,3-Trichlorobenzene
87-61-6
8260B
ND
0.50
ug/L
1
1,2,4-Trichlorobenzene
120-82-1
8260B
ND
0.50
ug/L
1
1,1,1 -Trichloroethane
71-55-6
82608
ND
0.50
ug/L
1
1,1,2 -Trichloroethane
79-00-5
8260B
ND
0.50
ug/L
1
Trichloroethene
79-01-6
82608
ND
0.50
ug/L
1
Trichlorofluoromethane
75-69-4
8260B
ND
0.50
ug/L
1
1,2,3-Trichloropropane
96-18-4
8260B
ND
0.50
ug/L
1
1,2,4-Trimethylbenzene
95-63-6
8260B
ND
0.50
ug/L
1
1,3,5-Trimethylbenzene
108-67-8
8260B
ND
0.50
ug/L
1
Vinyl chloride
75-01-4
8260B
ND
0.50
ug/L
1
m+p- Xylenes
179601-23-1
8260B
ND
0.50
ug/L
1
o - Xylenes
95-47-6
8260B
ND
0.50
ug/L
1
Run 1 Acceptance
Surrogate
Q % Recovery Limits
1,2-Dichloroethane-d4
104 70-130
Bromofluorobenzene
104 70-130
Toluene -d8
109 70-130
PQL = Practical quantitation limit B = Detected in the method blank E = Quantitation of compound exceeded the calibration range H = Out of holding time
ND = Not detected at or above the PQL J = Estimated result < PQL and > MDL P = The RPD between two GC columns exceeds 40% N = Recovery is out of criteria
Where applicable, all soil sample analysis are reported on a dry weight basis unless flagged with a "W"
Shealy Environmental Services, Inc. Page: 12 of 17
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.shealylab.com