NC0040711_Permit Application Addendum_20161102

Tom Belnick
Permitting Supervisor
Division of Water Resources
WQ Permitting Section - NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617
Subject: NPDES Permit Application Addendum
Arauco Panels USA, LLC
Moncure, Chatham County, North Carolina
Dear Mr. Belnick:
985 Corinth Road
Moncure, North Carolina 27559
Tel: [phone]
Toll Free: 855-427-2826
Fax: [phone]
October 26, 2016
R E: CE I VED/N C DiEUDWR
NOV 0 2 2016
V+=ater Ouality
Permitting Section
Please find attached the requested addendum to our NPDES Permit application currently being
processed by your office. EPA Form 1 and 2C (original and 2 copies) are included with this
submittal, as well as the required supporting documentation. If you have any questions related
to this notification, please contact me, Todd Phillips, Moncure's Environmental Manager at 919-
545-5849 or John Bird, Arauco's Corporate Environmental Manager at 919-642-6658.
Sincerely,
(:;ZQ
Todd Phillips
Site Environmental Manager

Please nrint nr tvne in the unshaded areas only
Form Approved. OMB No. 2040-0086.
FORM
U.S. ENVIRONMENTAL PROTECTION AGENCY
I. EPA I.D. NUMBER
s TrA
1
GENERAL INFORMATION
��iEFyA Consolidated Permits Program
F D
GENERAL
(Read tire "General Instructions " btforc starling.)
2 131 14 1 15
GENERAL INSTRUCTIONS
LABEL ITEMS
If a preprinted label has been provided, affix It in the
designated space Review the Information carefully, if any of it
is Incorrect, cross through It and enter the correct data in the
I. EPA I.D. NUMBER
appropriate fill-in area below. Also, If any of the preprinted data
is absent (the area to the left of the label space lists the
III. FACILITY NAME
PLEASE PLACE LABEL IN THIS SPACE
information that should appear), please provide it In the proper
fill-in area(s) below. If the label is complete and correct, you
need not complete Items I, III, V, and VI (except VI -B which
V. FACILITY MAILING
must be completed regardless). Complete all items if no label
ADDRESS
has been provided. Refer to the Instructions for detailed item
for the legal authorizations under which this
VI. FACILITY LOCATION
data ollected
ns collected
II. POLLUTANT CHARACTERISTICS
INSTRUCTIONS: Complete A through J to determine whether you need to submit any permit application forms to the EPA. If you answer "yes" to any questions, you must
submit this form and the supplemental form listed in the parenthesis following the question Mark "X" in the box in the third column if the supplemental form is attached If
you answer "no" to each question, you need not submit any of these forms. You may answer "no" if your activity Is excluded from permit requirements; see Section C of the
instructions. See also, Section D of the Instructions for definitions of bold-faced terms.
Mark
W
Mark
W
SPECIFIC QUESTIONS
YES
NO
FORMFORM
ATTACHED
SPECIFIC QUESTIONS
YES
NO
ATTACHED
A. Is this facility a publicly owned treatment works which
B. Does or will this facility (either existing or proposed)
results in a discharge to waters of the U.S.? (FORM 2A)
X
include a concentrated animal feeding operation or
X
aquatic animal production facility which results in a
16
17
16
19
20
21
discharge to waters of the U.S.? (FORM 2B)
C. Is this a facility which currently results in discharges to�/
X
D. Is this a proposed facility (other than those described in A
X
waters of the U.S. other than those described in A or B
or B above) which will result in a discharge to waters of
above (FORM 2C)
the U.S.? (FORM 2D)
22
23
24
25
28
2]
E. Does or will this facility treat, store, or dispose of
F. Do you or will you inject at this facility industrial or
hazardous wastes? (FORM 3)
X
municipal effluent below the lowermost stratum
X
containing, within one quarter mile of the well bore,
26
29
3o
underground sources of drinking water? (FORM 4)
31
32
33
G Do you or will you inject at this facility any produced water
H. Do you or will you inject at this facility fluids for special
or other fluids which are brought to the surface in
processes such as mining of sulfur by the Frasch process,
connection with conventional oil or natural gas production,
X
solution mining of minerals, in situ combustion of fossil
X
Inject fluids used for enhanced recovery of oil or natural
fuel, or recovery of geothermal energy? (FORM 4)
gas, or inject fluids for storage of liquid hydrocarbons?
(FORM 4)
34
35
36
37
36
39
I. Is this facility a proposed stationary source which is one
J. Is this facility a proposed stationary source which is
of the 28 Industrial categories listed in the Instructions andX
NOT one of the 28 industrial categories listed in the
�/
X
which will potentially emit 100 tons per year of any air
instructions and which will potentially emit 250 tons per
pollutant regulated under the Clean Air Act and may affect
year of any air pollutant regulated under the Clean Air Act
46
41
42
43
d4
45
or be located in an attainment area? (FORM 5)
and may affect or be located In an attainment area?
(FORM 5)
III. NAME OF FACILITY
1 SKIP Arauco Panels USA LLC
Ica
15 16 - 29 30
69
IV. FACILITY CONTACT
A NAME & TITLE (last, first, & title)
B. PHONE (area code & no.)
Quesenberry, AR & NC Regiona Manufacturing
Director ( 1 ) 642-6629
NTom
16
45 a d6 49 51 1 52- 55
V. FACILTY MAILING ADDRESS
A. STREET OR P O. BOX
J3c 985 Corinth Road
15 16
d5
B. CITY OR TOWN
C. STATE D. ZIP CODE
J4 Moncure
15 16
C 24_5 9
40 41 42 47 51
VI. FACILITY LOCATION
A. STREET, ROUTE NO. OR OTHER SPECIFIC IDENTIFIER
c
5 9 5 Corinth Road
15 18
45
B. COUNTY NAME
Chatham
46
]0
C CITY OR TOWN
D. STATE E. ZIP CODE F. COUNTY CODE (rfknotrn)
s
M n lire 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1
1 1 1
C
24_5 9 1
3
15
16
40
d1 d2
47 51
52 -54
EPA Form 3510-1 (8-90) CONTINUE ON REVERSE

MNTINI irn FRnM THF FRr1NT
EPA Form 3510-1 (8-90)
VII. SIC CODES (4-ftit in order ofpriori
A. FIRST B. SECOND
c
(sped) Reconstituted wood Products 7
(specify)7
15
2493
16 19
15
16 19
C. THIRD D. FOURTH
°
(spec fY ) 7 7(speC�)
7
15 16 19
15
16 19
VIII. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
o also the owner'?
8VIII-A
© YES ❑ NO
15 ,6 55 66
C. STATUS OF OPERATOR (Finer the appropriate letter into the answer box- 1j "Other, "specify.)
D. PHONE (area code R- no.)
F = FEDERAL
M=PUBLIC rthaujederalorstate)
P
`
A [phone]
O =OTHER (specify)(speai5)
S=STATE
P =PRIVATE
56
15 6 - 18 19 2, 22 26
E. STREET OR P.O. BOX
9151 Corinth Road
26 55
F. CITY OR TOWN
G STATE
I H. ZIP CODE IX. INDIAN LAND
Is the facility located on Indian lands?
Moncure
JB
NC
27559 ❑ YES O NO
52
d] - 51
15 18 d0
d1 42
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDESDischar es to Surface Water D. PSD Air Fnussions from Pro osed Sources
C I T
c T
9 N NCO040711 g p
15 i6 i] 18 30 15 18 17 16 30
er ui,7dl ec1rnofFill E. OTHER s eci
B. UIC Undro
c T I
c T
03449 45
(specljj) NESHAPS
s U
9
15 16 i]
18 30 151 16 1] 18
30
C. RCRAHazardous Naves) E. OTHER (spec?61
C T I
c i t (SpeCji) Non -Discharge Irrigation Permit
9 R
NCD982076135 9 WQ0003396
15116 17
18 30 15 i6 1 17 18 30
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must show the outline of the facility, the
location of each of its existing and proposed intake and discharge structures, each of its hazardous waste treatment, storage, or disposal facilities, and each well where it
injects fluids underground. Include all springs, rivers, and other surface water bodies in the map area. See instructions for precise requirements.
XII. NATURE OF BUSINESS (provide a brief description)
Manufacture of particleboard and medium density fiberboard for use in building construction from raw materials.
XIII. CERTIFICATION (see instructions)
I certify under penalty of law that 1 have personally examined and am familiar with the information submitted in this application and all attachments and that based on my
inquiry of those persons immediately responsible for obtaining the information contained in the application, I believe that the information is true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fine and imprisonment.
A. NAME & OFFICIAL TITLE (tyre f% ,•print)
B. SIGNATURE
C. DATE SIGNED
COMMENTS FOR OFFICIAL USE ONLY
1C
1s ,6 u
EPA Form 3510-1 (8-90)

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LEGEND:
-) WASTEWATER
> WATER
I
I
I
I
I
1
1
I
200,000 gal/day
I
Haw River
I.
ARAUCO PANELS USA LLC
PROCESS SCHEMATIC
1676008.00
FIGURE 2

EPA I.D. NUMBER (copyfrominem 1 of Form 1) Form Approved.
OMB No. 2040-0086.
Please Drint or tvoe In the unshaded areas oniv. �NCO040711 Approval expires 3-31-98.
FORM
2C
NPDES
U.S. ENVIRONMENTAL PROTECTION AGENCY
FOR PERMIT TO DISCHARGE WASTEWATER
�""'�EPA EXISTING MANUFACTURING,APPLICATIOJCOMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consohdated Permits Program
I OUTFALL LOCATION
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water
A OUTFALL NUMBER
(USI)
B. LATITUDE C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG
2. MIN.
3. SEC 1. DEG.
2 MIN.
3 SEC
001
35.00
36.00
2.50 79.00
3.00
0.68
Haw River
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions In Item B Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and outfalls If a water balance cannot be determined (e g, for certain mining activities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation, and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW 3. TREATMENT
FALL
NO. (hsn)
b. AVERAGE FLOW b LIST CODES FROM
a OPERATION (list) (include mins) a. DESCRIPTION TABLE 2C-1
001
Sanitary Activated Sludge Treatment, Drainfield
0 3-A 5-T
Utility Water 0 Activated Sludge Treatment, Drainfield 3-A 5-T
Stormwater 4,000 gallons per day Settling Pond, MBR 3-G 1-0
Keller Scrubber APCD Blowdown 5,000 gallons per day Settling Pond, MBR 3-G 1-Q
00 1
Wet Scrubber APCD Slowdown Settling Pond, MBR
15,000 gallons per day 3-G 1-0
Biofilter Condensate (future) 4,000 gallons per day Settling Pond, MBR 3-G 1-Q
Squeeze Water 55,000 gallons per day Settling Pond, MBR 3-G 1-0
Steam Generator Purge 8,000 gallons per day Settling Pond, MBA 3-G 1-0
001
Sumps & oil/water Separator 5,000 gallons per day Settling Pond, MBR 3-G 1-Q
WESP Blowdown 4,000 gallons per day Settling Pond, MBR 3-G 1-Q
Final Effluent 100,000 gallons per day Surface Water Dis & Reuse 4-A 4-C
OFFICIAL USE ONLY (cf/luenrgandeluiessub-categories)
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINIIFn FROM THF FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal?
❑ YES (complete the following table) 0 NO (go to Section Ili
3. FREQUENCY
4. FLOW
a DAYS PER
B. TOTAL VOLUME
2 OPERATION(s)
WEEK
b MONTHS
a. FLOW RATE (uimgd)
(specifywmh mets)
1. LONG TERM
2. MAXIMUM
1 LONGTERM
2. MAXIMUM
C. DURATION
1 OUTFALL
CONTRIBUTING FLOW
(speciJ,
PER YEAR
NUMBER(bst)
(hst)
aremge)
(specify are, age)
AVERAGE
DAILY
AVERAGE
DAILY
(m days)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
© YES (complete Item 111-B) ❑ NO (go to Section 117
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)?
❑ YES (complete Item III -C) ® NO (go to Section IV)
C. If you answered 'yes" to Item III -B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the
applicable effluent guideline, and indicate the affected outfalls
1. AVERAGE DAILY PRODUCTION
2. AFFECTED OUTFALLS
(list outfall numbers)
a. QUANTITY PER DAY
b UNITS OF MEASURE
c. OPERATION, PRODUCT, MATERIAL, ETC.
(specify)
IV. IMPROVEMENTS
A Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to,
permit conditions, administrative or enforcement orders, enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
❑ YES (complete the following table) © NO (go to Item IV -B)
1. IDENTIFICATION OF CONDITION,
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
AGREEMENT, ETC.
a. NO
b. SOURCE OF DISCHARGE
a. REQUIRED
b. PROJECTED
B. OPTIONAL You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK "X" IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D. NUMBER (copyfromltem I ofFonn 1)
r:nNTINI1Fn FROM PAC F 2 NC0040711
EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE
V. INTAKE AND EFFLUENT CHARACTERISTICS
A, B, & C See Instructions before proceeding — Complete one set of tables for each outfall — Annotate the outfall number In the space provided.
NOTE: Tables V-A, V -B, and V -C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged
from any outfall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession
1.POLLUTANT
2. SOURCE
1.POLLUTANT
2. SOURCE
VI. POTENTIAL DISCHARGES NOT COVERED
BY ANALYSIS
or a component of a substance which you
below) ❑✓
currently use or manufacture as an intermediate
NO (go to Item VIA
or final product or byproduct?
Is any pollutant listed in Item V -C a substance
❑ YES (hst all such pollutants
EPA Form 3510-2C (8-90) PAGE 3 of 4 CONTINUE ON REVERSE

CONTINIJFD FROM THE FRONT
EPA Form 3510-2CT8-90) PAGE 4 of 4
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
ElYES (alenuO, the tests) and describe therrpunposes below) © NO (go to Section VIII)
VIII. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
❑ YES (hst the name, address, and telephone number of, and pollutants analyzed by, NO (go to Section L11
each such laboratory orfirm below)
A. NAME
B. ADDRESS
C. TELEPHONE
(area code d no.)
D. POLLUTANTS ANALYZED
(list)
IX. CERTIFICATION
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. NAME & OFFICIAL TITLE (type or print)
B. PHONE NO. (area code &))o.)
Tom Quesenberry, AR & NC Carolina Regional Manufacturing Dir.
[phone]
C. SIGNATU E
/�2
D. DATE SIGNED
/O a.t-j�0/6
EPA Form 3510-2CT8-90) PAGE 4 of 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some oral] of this information EPA I.D. NUMBER (copvfroni Rein I of Form 1)
on separate sheets (use the same format) instead of completing these pages. NCO 04 0711
SEE INSTRUCTIONS.
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued from page 3 of Form 2-C)
PART A—You must provide the results of at least one analysis for every pollutant in this table. Complete one table for each outfall. See instructions for additional details.
3. UNITS
4. INTAKE
2. EFFLUENT
(specifyifblank)
(oplmnal)
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM DAILY VALUE
(favadable)
(ifavailable)
AVERAGE VALUE
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Biochemical Oxygen
379
50
Demand (BOD)
b. Chemical Oxygen
3450
4
Demand (('OI))
c. Total Organic Carbon
(TOO
d. Total Suspended
Solids (7SS)
126
50
e. Ammonia (arA0
67
50
VALUE
VALUE
VALUE
VALUE
f. Flow
100,000 gal/day
Est.
g. Temperature
VALUE
VALUE
VALUE
"C
VALUE
(winter)
49.5
h. Temperature
VALUE
VALUE
VALUE
"C
VALUE
(sunnier)
76.5
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
a-,
i. pH
6.71
8 . 9
;i'
50
STANDARD UNITS
x= ,„ :�
,.:
"? -
vim. _.��d,._`"''",,, e .
"
PART B — Mark "X" in column 2-a for each pollutant you know or have reason to believe is present. Mark "X" in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (opOonal)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a
b.
a. MAXIMUM DAILY VALUE
(javarlable)
(ifovaAable)
VALUE
CAS NO.
BELIEVED
BELIEVED(1)
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(rfaventable)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
mg / L
<0.50
1
(24959-67-9)
b. Chlorine, Total
\/
X
Residual
c. Color
X
C.U.
4,200
1
d. Fecal Coliform
X
Cfu/100
>195, 122
1
e. Fluoride
mg / L
<0.50
1
(16984-48-8)
f. Nitrate Nitrite
X
mg/L
0.43
1
(as M
EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITr=NA \/-R r r1NTINi ip:n FR(1M FR(1NT
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (optional)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONGTERM AVRG. VALUE
a. LONG TERM
AND
a
b,
a. MAXIMUM DAILY VALUE
(/jarailahle)
((faradahle)
AVERAGE VALUE
CAS NO.
BELIEVED
BELIEVED(1)
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(�favadahle)
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
g. Nitrogen,
Total Organic (acX
mg/L
194
1
M
h Oil and
mg/L
21.2
1
Grease
1. Phosphorus
\ /
(as P), Total
X
mg/L
12.0
1
(7723-14-0)
j Radioactivity
(1) Alpha, Total
x
pCi/L
0.344 +/-
9.81
1
(2) Beta, Total
x
pCi/L
1,146 +/-
8.26
1
(3) Radium,
x
pCi/L
0.392 +/-
0.642
1
Total
(4) Radium 226,
X
pCi/L
-0.191 +/-
0.872
1
Total
k. Sulfate
(
x(14808-79-8)
I. Sulfide\/
x
mg/L
0.15
1
(as S)
m. Sulfite
X
(14265-45-3)
n. Surfactants
x
mg/L
<20
1
o. Aluminum,
Total
x
ug/L
1,660
1
(7429-90-5)
p. Barium, Total
X
ug / L
332
1
(7440-39-3)
q. Boron, Total
X
ug / L
1000
1
(7440-42-8)
r. Cobalt, Total�/
x
ug/L
<0.25
1
(7440-48-4)
s. Iron, TotalX
ug/L
3,900
1
(7439-89-6)
t. Magnesium,
Totalx
ug/L
18,900
1
(7439-95-4)
u. Molybdenum,
Total
X
ug/L
40
1
(7439-98-7)
v. Manganese,
TotalX
ug/L
3540
1
(7439-96-5)
w. Tin, Total\/
x
ug/L
32.8
1
(7440-31-5)
x. Titanium,
TotalX
ug/L
<25
1
(7440-32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

EPA I.D. NUMBER (copvfnmllem I of Form 1) OUTFALL NUMBER
CONTINUED FROM PAGE 3 OF FORM 2-C N00040711 001
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2o-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark "X" in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outfalls, and nonrequired GC/MS
fractions), mark "X" in column 2-b for each pollutant you know or have reason to believe is present. Mark "X" in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 2b for any pollutant, you must provide the results of at least one analysis for that pollutant if you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acrolein, acrylonitrile, 2,4 dinitrophenol, or 2 -methyl -4, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that there are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK "X"
3, EFFLUENT
4. UNITS
5. INTAKE (oprionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
c.
a. MAXIMUM DAILY VALUE
(ifavadable)
VALUE (ifavadable)
AVERAGE VALUE
CASNUMBER
=ab
ED
BELIEVED
NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)d.
(�fmvmlable)
NT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1 M. Antimony, Total
ug / L
<25
1
(7440-36-0)
2M. Arsenic, Total
X
�/
X
ug/L
<50
1
(7440-38-2)
(7440-38-2)
3M. Beryllium, Total\/
X
ug/L
<5
1
(7440-41-7)
4M. Cadmium, Total
X
ug/ L
8.3
1
(7440-43-9)
5M. Chromium,
ug/L
29.6
1
Total (7440-47-3)
6M. Copper, Total\/
X
ug / L
424
1
(7440-50-8)
7M. Lead, Total
X
�/
X
llg / L
33.8
1
(7439-92-1)
(7439-92-1)
8M. Mercury, Total\/
X
ug / L
<0.20
1
(7439-97-6)
9M. Nickel, Total
X
�/
X
ug/L
37.1
1
(7440-02-0)
(7440-02-0)
10M. Selenium,
Ug/L
<50
1
Total (7782-49-2)
11 M. Silver, Total
ug / L
<50
1
(7440-22-4)
12M. Thallium,
ug/L
<50
1
Total (7440-28-0)
13M. Zinc, Total
ug/ L
1290
1
(7440-66-6)
14M. Cyanide,
X
X
mg/L
0.017
1
Total (57-12-5)
15M. Phenols,\/
X
X \/
mg/L
2.8
1
Total
DIOXIN
2,3,7,8 -Tetra-
DESCRIBE RESULTS
chlorodibenzo-P-
Dioxin (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (opfioual
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a
b.
c
a. MAXIMUM DAILY VALUE
(rfavmlahle)
VALUE (javarlable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailahle)
REQUIRED
PRESENT
ABSENTCONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS
IV. Accrolein\/
x
ug/L
<25
1
(107-02-8)
2V. Acrylonitrile\/
X
x
ug/L
<250
1
(107-13-1)
3V. Benzene\/
x
ug/L
<10
1
(71-43-2)
4V. Bis (
\
uierhyQ Ether
(542-88-1)
/X\
5V. Bromoform
ug / L
<10
1
(75-25-2)
Carbon
Tet
TetrachlorideX
ug/L
<10
1
(56-23-5)
7V. Chlorobenzene\/
x
x �/
ug/L
<10
1
(108-90-7)
8V. Chlorodi-
bromomethane
\ /
x
\ /
x
ug/L
<10
1
(124-48-1)
/ `
, \
9V Chloroethane\/
x
�/
x
ug/L
<10
1
(75-00-3)
ro-
1OV. lvinyl the
elhylvinyl Ether
ug/L
<25
1
(110-75-8)
11 V. Chloroforml
x
ug/L
<10
1
(67-66-3)
12V. Dichloro-
bromomelhane
ug/L
<10
1
(75-27-4)
13V. Dichloro-
difluoromethaneX
ug/L
<10
1
(75-71-8)
14V.1,1-Dichloro-\/
x
ug/L
<10
1
ethane (75-34-3)
15V. 1,2-Dichloro-
ug/L
<10
1
ethane (107-06-2)
16V.1,1-Dichloro-\/
x
�/
ug/L
<10
1
ethylene (75-35-4)
^
17V.1,2-Dichloro-\/
x
ug/L
<10
1
propane (78-87-5)
18V.1,3-Dichloro-
propylene
\ /
X
\ /
X
ug/L
<10
1
(542-75-6)
19V.Ethylbenzene
ug / L
<10
1
(100-41-4)
20V. Methyl
ug/L
<10
1
Bromide (74-83-9)
21V. Methyly
x
y
x
ug/L
<10
1
Chloride (74-87-3)
EPA Form 3510-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5

r`r)KITIAII IFr) FRr)hA PAr,F V_A
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (opnonan
1. POLLUTANT
c.LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
ea.MAXIMUM
DAILY VALUE
�b.AXIMUM30DAYVALUE
(rfarailable)
VALUE (rjaruiluble)
AVERAGEVALUE
CAS NUMBER
TESTINGBELIEVED
BELIEVED
NO. OF
a. CONCEN-
b. NO.OF
(1)
(1)(1)d.
(1)
(favarlable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS (connnuero
22V. Methylene�/
ug/L
<10
1
Chloride (75-09-2)
x\
23V. 1,1,2,2-
Tetrachloroethane
X
X
ug/L
<10
1
79-34-5
24V. Tetrachloro-�/
ug/L
<10
1
ethylene (127-18-4)
^
25V. Toluene�/
ug/L
41.5
1
(108-88-3)
x\
26V.1,2-Trans-
DichloroethyleneX
X
ug/L
<10
1
156-60-5
27V.1,1,1-Trichloro-
X
ug/L
<10
1
ethane (71-55-6)
28V.1,1,2-Trichloro-
X
ug/L
<10
1
ethane (79-00-5)
29V Trichloro-
ug/L
<10
1
ethylene (79-01-6)
30V. Trichloro-
fluoromethane
x
x
ug/L
<10
1
75-69-4
/ `
31V. Vinyl Chloride
ug/L
<10
1
(75-01-4)
GC/MS FRACTION—ACID COMPOUNDS
1A.2 -Chlorophenol
ug/ L
<500
1
(95-57-8)
2A. 2,4-Dichloro-�/
x
ug/L
<500
1
phenol(120-83-2)
3A.2,4 -Dimethyl-
ug / L
<1000
1
phenol (105-67-9)
4A.4,6-Dlnitro-0-�/
ug/L
<2000
1
Cresol (534-52-1)
�\
5A.2,4-Dlnitro-
ug / L
<5000
1
phenol (51-28-5)
6A.2-Nitrophenol
ug / L
<500
1
(88-75-5)
7A. 4-Nitrophenol�/
x
X
u L
g/
< 5 0 0 0
1
(100-02-7)
/ \
8A. P-Chloro-M-�/
x
ug/L
<500
1
Cresol (59-50-7)
9A. Pentachloro-
ug/L
<1000
1
phenol (87-86-5)
10A. Phenol
ug/L
2.8
1
(108-95-2)
11 A. 2,4,6-Tnchloro-
X
ug/L
<10
1
phenol (88-05-2)
EPA Form 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

R0NTIN11Fr) FROM THF FRnNT
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7
2. MARK "X"
3. EFFLUENT 4. UNITS
5. INTAKE (opunoan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b
C.
a. MAXIMUM DAILY VALUE
(farailahle)
VALUE (ifavailahle)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(favailahle)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS
1B Acenaphthene
ug/ L
<500
1
(83-32-9)
2B. Acenaphtylene
ug/L
<500
1
(208-96.8)
3B. Anthracene
�/
�/
x
ug/L
<500
1
(120-12-7)
/�
4B. Benzidine�/
�/
ug/L
<5, 000
(92-87-5)
/�
/�
5B. Benzo (a)
AnthraceneX
ug/L
<500
1
(56-55-3)
6B. Benzo (a)
ug/L
<500
1
Pyrene (50-32-6)
76.3,4-Benzo-
fluoranthene
ug/ L
<500
1
(205-99-2)
8B. Benzo (l;/u)ug/L
�/
�/
<500
1
Perylene (191-24-2)
/�
^
9B. Benzo (k)
Fluoranthene
ug / L
<500
1
(207-08-9)
10B. Bis (2-Chloro-
erlrosy) Methane
ug/L
<1000
1
(111-91-1)
11 B. Bis (2-0?fivo-
er/rrl Ether
ug/L
<500
1
(111-44-4)
12B. Bis (2-
ClrlaroisoprapyO�/
x
x
ug/L
<500
1
Ether (102-80-1)
13B. Bis (2-Gllrr(-
hexyn Phthalate
ug/L
<500
1
(117-81-7)
14B. 4-Bromophenyl
Phenyl Etheru
ug/L
<500
1
(101-55-3)
15B. Butyl Benzyl
ug/L
<500
1
Phthalate (85-68-7)
16B. 2-Chloro-
naphthaleneu
u
ug/L
<500
1
(91-58-7)
17B. 4 -Chloro -
phenyl Phenyl Ether
x
�/
x
ug / L
<500
1
(7005-72-3)
(7005-72-3)
16B.Chrysene�/
x
�/
x
ug/L
<500
1
(218-01-9)
19B. Dlbenzo (a.h)
Anthracene
ug/L
<500
1
(53-70-3)
20B.1,2-Dichloro-�/
x
�/
x
ug/L
<10
1
(95-50-1)
-benzene
218.1,3 -Di -chloro-
ug/L
<10
1
benzene (541-73 1)
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

r`MITH,11 IFr) FPC hA PGr,F \/-A
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (oplionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
C.
a. MAXIMUM DAILY VALUE
(Itava/lahle) I
VALUE (favarlahle)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. Col
b. NO. OF
(1)
(1)
(1)
(1)
(favarlahle)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (conlrnnerl)
226.1,4-Dichloro-
ug/L
<10
1
benzene (106-46-7)
23B.3,3-Dichloro-
ug/ L
<2500
1
benzidine (91-94-1)
24B. Diethyl
ug / L
<500
1
Phthalate (84-66-2)
25B.Dimethyl
Phthalate
ug/L
<500
1
(131-11-3)
26B. Di -N -Butyl
ug/L
<500
1
Phthalate (84-74-2)
27B.2,4-Dinitro-\/
ug/L
<500
1
toluene (121-14-2)
/\
286.2,6-Dinitro-
ug/L
<500
1
toluene (606-20-2)
29B.Di-N-Octyl�/
x\/
ug/L
<500
1
Phthalate (117-84-0)
^
B. yl -
30drazin
(as Azo-
hydrazine (as Azo-
u L
g/
<500
1
benzene) (122-66-7)
31B. Fluoranthene\/
x
�/
ug/L
<500
1
(206-44-0)
^
32B. Fluorenev
ug/L
<500
1
(86-737)
^
33B. Hexachloro-
ug/L
<500
1
benzene (118-74-1)
34B. Hexachloro-
ug/L
<500
1
butadiene (87-68-3)
Hexachloro-
cyclopentadiene
cycl
ug/L
<1000
1
(77-47-4)
36B Hexachloro-v
ug/L
<500
1
ethane (67-72-1)
378. Indeno
(1,2,3 -cd) Pyrene
Ug/L
<500
1
(193-39-5)
38B.Isophorone
ug/L
<1000
1
(78-59-1)
39B. Naphthalene\/
x
�/
ug/L
<500
1
(91-20-3)
40B. Nitrobenzene
ug / L
<500
1
(98-95-3)
41 B. o-
sodimethylethylamine
ug / L
< 5 0 0
1
(62-75-9)
42B. N-Nitrosodi-
N-Propylamine
ug/ L
< 5 0 0
1
(621-64-7)
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9
2. MARK "X"
3. EFFLUENT
4. UNITS
5. INTAKE (oplhanan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
c
a. MAXIMUM DAILY VALUE
(rfavarlable)
VALUE (ifavailable)
AVERAGEVALUE
CAS NUMBER
=TESTINGBEL17�VED
BELIEVED
NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)d.
(javar/able)
NT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION - BASE/NEUTRAL COMPOUNDS (continued)
43B. N-Nitro-
sodiphenylamine
ug/L
<1000
1
(86-30-6)
44B. Phenanthrene
ug/L
<500
1
(85-01-8)
45B. Pyrene
X
x
ug/L
<500
1
(129-00-0)
46B. 1,2,4-Tri-
-Tug
chbrobe1)
�/
<500
1
(120-82-1)
/\
GC/MS FRACTION - PESTICIDES
1P. Aldrin
ug/L
<0.50
1
(309-00-2)
2P. a -BHC\/
x
�/
ug/L
<0.50
1
(319-84-6)
^
3P. (3 -BHC\/
x
�/
ug/L
<0.50
1
(319-85-7)
^
4P. y -BHC
ug /L
<0.50
1
(58-89-9)
5P. 8-BHC
ug/L
<0.50
1
(319-86-8)
(319-86-8)
^
6P. Chlordane\/
ug/L
<5
1
(57-749)
�\
7P.4,4' -DDT
ug/L
<0.50
1
(50-29-3)
8P.4,4' -DDE
ug/L
<0.50
1
(72-55-9)
9P.4,4' -DDD
ug / L
<0.50
1
(72-548)
10P. Dieldrinv
ug/L
<0.50
1
(60-57-1)
11 P. a-Enosulfan\/
x
ug/L
<0.50
1
(115-29.7)
12P. (3-Endosulfan
x
ug/L
<0.50
1
(115-29-7)
Endosulfan
Sulfate
ug/I,
<0.50
1
(1031-07-8)
14P. Endrin�/
�/
ug/L
<0.50
1
(72-20-8)
^
^
15P.Endrin
Aldeide hyde
ug / L
<0.50
1
(7421-93-4)
16P. Heptachlor�/
^
�/
x
ug/L
<0.50
1
(76-44-8)
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

EPA 1. D. NUMBER (copyfi•ow Uew l ofForni 1) OUTFALL NUMBER
CONTINUED FROM PAGE V-8 I
NCO040711 001
EPA Form 3510-2C (8-90) PAGE V-9
2. MARK"X"
3. EFFLUENT
4. UNITS
5. INTAKE(optionaQ
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
c.a.
MAXIMUM DAILY VALUE
(ifavailable)
VALUE (ifavailable)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(ifavailable)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
GC/MS FRACTION — PESTICIDES (conOnaea)
17P. Heptachlor
Epoxide
` ,
X
` ,
X
ug / L
<0.50
1
(1024-57-3)
18P. PCB -1242\/
x
x\/
ug/L
<5
1
(53469-21-9)
19P. PCB -1254
ug/L
<5
1
(11097-69-1)
20P. PCB -1221
ug / L
<5
1
(11104-28-2)
21 P. PCB -1232
ug / L
<5
1
(11141-16-5)
22P. PCB -1248
x
X
ug / L
<s
1
(12672-29-6)
23P. PCB -1260
X
X
ug/L
<5
1
(11096-82-5)
24P. PCB -1016
X
X
ug/L
<5
1
(12674-11-2)
25P. Toxaphene
x
X
ug/L
<5
1
(8001-35-2)
EPA Form 3510-2C (8-90) PAGE V-9

I_:::1
0 1 2
APPROXIMATE SCALE IN MILES
4.2
BUCKHORN DAM
Kennedy/Jenks Consultants
Arauco Panels USA, LLC
Engineering Alternatives Analysis
1676008.10
Moncure Area Plan with Outfall Location
Figure 1

(�55'neAnalyfical"
www.pacelabs.com
October 25, 2016
Todd Phillips
Arauco
985 Corinth Road
Moncure, NC 27559
RE: Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Dear Todd Phillips:
Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2016.
The results relate only to the samples included in this report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Clayton McCrickard for
Terri. Page
[e-mail]
Project Manager
Enclosures
cc: Todd Phillips, Arauco Phillips
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Pennsylvania Certification IDs
1638 Roseytown Rd Suites 2,3&4, Greensburg, PA 15601
L -A -B DOD-ELAP Accreditation #: L2417
Alabama Certification #: 41590
Arizona Certification #: AZ0734
Arkansas Certification
California Certification #: 04222CA
Colorado Certification
Connecticut Certification M PH -0694
Delaware Certification
Florida/TNI Certification #: E87683
Georgia Certification M C040
Guam Certification
Hawaii Certification
Idaho Certification
Illinois Certification
Indiana Certification
Iowa Certification #: 391
Kansas/TNI Certification M E-10358
Kentucky Certification #: 90133
Louisiana DHH/TNI Certification #: LA140008
Louisiana DEQ/TNI Certification M 4086
Maine Certification #: PA00091
Maryland Certification #: 308
Massachusetts Certification #: M-PA1457
Michigan/PADEP Certification
Missouri Certification #: 235
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH -0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification M 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification M E-10383
Louisiana Certification M FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification M 236
Montana Certification #: Cert 0074
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification M 5342
CERTIFICATIONS
Montana Certification #: Cert 0082
Nebraska Certification #: NE -05-29-14
Nevada Certification #: PA014572015-1
New Hampshire/TNI Certification #: 2976
New Jersey/TNI Certification M PA 051
New Mexico Certification #: PA01457
New York/TNI Certification #: 10888
North Carolina Certification M 42706
North Dakota Certification #: R-190
Oregon/TNI Certification #: PA200002
PennsylvaniafTNI Certification M 65-00282
Puerto Rico Certification #: PA01457
Rhode Island Certification #: 65-00282
South Dakota Certification
Tennessee Certification #: TN2867
Texas/TNI Certification #: T104704188-14-8
Utah/TNI Certification #: PA014572015-5
USDA Soil Permit #: P330-14-00213
Vermont Dept. of Health: ID# VT -0282
Virgin Island/PADEP Certification
Virginia/VELAP Certification M 460198
Washington Certification #: C868
West Virginia DEP Certification M 143
West Virginia DHHR Certification #: 9964C
Wisconsin Certification
Wyoming Certification M 8TMS-L
Nebraska Certification: NE -OS -28-14
Nevada Certification: FL NELAC Reciprocity
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Oklahoma Certification #: D9947
Pennsylvania Certification M 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Wyoming Certification: FL NELAC Reciprocity
West Virginia Certification #: 9962C
Wisconsin Certification M 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
North Carolina Wastewater Certification #: 12
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
REPORT OF LABORATORY ANALYSIS
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Project: WATER TEST
Pace Project No.: 92314764
Charlotte Certification IDs
Kentucky UST Certification #: 84
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification IDs
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project:
Pace Project No.:
WATER TEST
92314764
Analytes .
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92314764001
51)
SM 2120E ColorADMI
DWJ
4
PASI-E
EPA 1664B
JMS
1
PASI-C
EPA 608
SWB
27
PASI-C
EPA 200.7
SH1
22
PASI-A
EPA 7470
WAB
1
PASI-A
EPA 625
BPJ
60
PASI-C
EPA 624
GAW
38
PASI-C
EPA 900.0
NEG
2
PASI-PA
EPA 903.0
LAL
1
PASI-PA
EPA 903.1
WRR
1
PASI-PA
SM 4500-S21D
EWS
1
PASI-A
SM 5540C
TK1
2
PASI-O
TKN-NH3 Calculation
EWS
1
PASI-A
EPA 300.0
AES2
2
PASI-A
EPA 300.0
CMB
1
PASI-O
EPA 350.1 1993 Rev 2.0
DMN
1
PASI-A
EPA 351.2
BRJ
1
PASI-A
EPA 353.2
WRC
1
PASI-A
EPA 365.1
BRJ
1
PASI-A
EPA 420.4
DMN
1
PASI-A
SM 4500 -CN -E
DMN
1
PASI-A
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Project: WATER TEST
Pace Project No.: 92314764
Sample: 5D
Parameters
2120E Color ADMI
Color, ADMI
Adjusted Color, ADMI
pH
Adjusted pH, ADMI
Field Data Raleigh
Collected By
Collected Date
Collected Time
Field pH
Field Temperature
HEM, Oil and Grease
Oil and Grease
608 GCS Pesticides and PCBs
Aldrin
alpha -BHC
beta -BHC
delta -BHC
gamma -BHC (Lindane)
Chlordane (Technical)
4,4' -DDD
4,4' -DDE
4,4' -DDT
Dieldrin
Endosulfan I
Endosulfan II
Endosulfan sulfate
Endrin
Endrin aldehyde
Heptachlor
Heptachlor epoxide
PCB -1016 (Aroclor 1016)
PCB -1221 (Aroclor 1221)
PCB -1232 (Aroclor 1232)
PCB -1242 (Aroclor 1242)
PCB -1248 (Aroclor 1248)
PCB -1254 (Aroclor 1254)
PCB -1260 (Aroclor 1260)
Toxaphene
Surrogates
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
Date: 10/25/2016 03:50 PM
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
ANALYTICAL RESULTS
Lab ID: 92314764001 Collected: 10/04/16 14:00 Received: 10/04/16 15:26 Matrix: Water
Results
Upits
Report Limit
DF
Prepared
Analyzed
CAS No. Qual
Analytical Method: SM 2120E Color ADMI
3400
units
1250
50
10/06/16 08:45
4200
units
1250
50
10/06/16 08:45
7.4
units
1.0
1
10/06/16 08:45
7.6
units
1.0
1
10/06/16 08:45
Analytical Method:
MATT
1
10/04/16 14:00
HUBER
10042016
1
10/04/16 14:00
1400
1
10/04/16 14:00
7.4
Std. Units
0.10
1
10/04/16 14:00
25.3
deg C
0.50
1
10/04/16 14:00
Analytical Method: EPA 1664B
21.2
mg/L
5.0
1
10/13/16 08:45
Analytical Method: EPA 608 Preparation Method: EPA 3510
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
309-00-2
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
319-84-6
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
319-85-7
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
319-86-8
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
58-89-9
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
57-74-9
ND'
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
72-54-8
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
72-55-9
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
50-29-3
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
60-57-1
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
959-98-8
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
33213-65-9
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
1031-07-8
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
72-20-8
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
7421-93-4
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
76-44-8
ND
ug/L
0.50
1
10/06/16 09:48
10/07/16 23:49
1024-57-3
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
12674-11-2
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
11104-28-2
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
11141-16-5
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
53469-21-9
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
12672-29-6
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
11097-69-1
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
11096-82-5
ND
ug/L
5.0
1
10/06/16 09:48
10/07/16 23:49
8001-35-2
14
%
20-110
1
10/06/16 09:48
10/07/16 23:49
877-09-8 S2
92
%
20-138
1
10/06/16 09:48
10/07/16 23:49
2051-24-3
REPORT OF LABORATORY ANALYSIS
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full,
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5ac
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eAnalyfical
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ANALYTICAL RESULTS
Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: 5D
Parameters
Lab ID: 92314764001
Results Units
Collected: 10/04/16 14:00
Report Limit DF
Received: 10/04/16 15:26 Matrix: Water
Prepared Analyzed CAS No.
Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Aluminum
1660
ug/L
500
5
10/10/16 21:55
10/13/16 16:37
7429-90-5
Antimony
ND
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-36-0
D3
Arsenic
ND
ug/L
50.0
5
10/10/16 21:55
10/13/16 16:37
7440-38-2
D3
Barium
332
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-39-3
Beryllium
ND
ug/L
5.0
5
10/10/16 21:55
10/13/16 16:37
7440-41-7
D3
Boron
1000
ug/L
250
5
10/10/16 21:55
10/13/16 16:37
7440-42-8
Cadmium
8.3
ug/L
5.0
5
10/10/16 21:55
10/13/16 16:37
7440-43-9
Chromium
29.6
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-47-3
Cobalt
ND
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-48-4
D3
Copper
424
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-50-8
Iron
3900
ug/L
250
5
10/10/16 21:55
10/13/16 16:37
7439-89-6
Lead
33.8
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7439-92-1
Magnesium
18900
ug/L
500
5
10/10/16 21:55
10/13/16 16:37
7439-95-4
Manganese
3540
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7439-96-5
Molybdenum
40.0
ug/L
25.0
5
10/10/16 21:55
10/14/16 15:27
7439-98-7
Nickel
37.1
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-02-0
Selenium
ND
ug/L
50.0
5
10/10/16 21:55
10/13/16 16:37
7782-49-2
D3
Silver
ND
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-22-4
D3
Thallium
ND
ug/L
50.0
5
10/10/16 21:55
10/13/16 16:37
7440-28-0
D3
Tin
32.8
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-31-5
Titanium
ND
ug/L
25.0
5
10/10/16 21:55
10/13/16 16:37
7440-32-6
D3
Zinc
1290
ug/L
50.0
5
10/10/16 21:55
10/13/16 16:37
7440-66-6
7470 Mercury
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Mercury
ND
ug/L
0.20
1
10/11/1614:10
10/12/1610:13
7439-97-6
625 MSSV
Analytical Method: EPA625 Preparation Method: EPA625
Acenaphthene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
83-32-9
Acenaphthylene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
208-96-8
Anthracene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
120-12-7
Benzidine
ND
ug/L
5000
10
10/10/16 13:52
10/14/16 20:15
92-87-5
Benzo(a)anthracene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
56-55-3
Benzo(a)pyrene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
50-32-8
Benzo(b)fluoranthene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
205-99-2
Benzo(g,h,i)perylene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
191-24-2
Benzo(k)fluoranthene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20.15
207-08-9
4-Bromophenylphenyl ether
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
101-55-3
Butylbenzylphthalate
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
85-68-7
4-Chloro-3-methylphenol
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
59-50-7
bis(2-Chloroethoxy)methane
ND
ug/L
1000
10
10/10/16 13:52
10/14/16 20:15
111-91-1
bis(2-Chloroethyl) ether
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
111-44-4
2-Chloronaphthalene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
91-58-7
2 -Chlorophenol
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
95-57-8
4-Chlorophenylphenyl ether
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
7005-72-3
Chrysene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
218-01-9
Dibenz(a,h)anthracene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
53-70-3
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: WATER TEST
Pace Project No.: 92314764
Sample: 5D Lab ID: 92314764001 Collected: 10/04/16 14:00 Received: 10/04/16 15:26 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
625 MSSV Analytical Method: EPA 625 Preparation Method: EPA 625
3,3'-Dichlorobenzidine
ND
ug/L
2500
10
10/10/16 13:52
10/14/16 20:15
91-94-1
2,4-Dichlorophenol
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
120-83-2
Diethylphthalate
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
84-66-2
2,4 -Dimethylphenol
ND
ug/L
1000
10
10/10/16 13:52
10/14/16 20:15
105-67-9
Dimethylphthalate
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
131-11-3
Di-n-butylphthalate
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
2000
10
10/10/16 13:52
10/14/16 20:15
534-52-1
2,4-Dinitrophenol
ND
ug/L
5000
10
10/10/16 13:52
10/14/16 20:15
51-28-5
2,4-Dinitrotoluene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
121-14-2
2,6-Dinitrotoluene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
606-20-2
Di-n-octylphthalate
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
117-84-0
1,2-Diphenylhydrazine
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
122-66-7
bis(2-Ethylhexyl)phthalate
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
117-81-7
Fluoranthene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
206-44-0
Fluorene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
86-73-7
Hexachloro-1,3-butadiene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
87-68-3
Hexachlorobenzene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
118-74-1
Hexachlorocyclopentadiene
ND
ug/L
1000
10
10/10/16 13:52
10/14/16 20:15
77-47-4
Hexachloroethane
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
67-72-1
Indeno(1,2,3-cd)pyrene
ND
ug/L
500
10
10/10/1613:52
10/14/1620:15
193-39-5
Isophorone
ND
ug/L
1000
10
10/10/16 13:52
10/14/16 20:15
78-59-1
Naphthalene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
91-20-3
Nitrobenzene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
98-95-3
2-Nitrophenol
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
88-75-5
4-Nitrophenol
ND
ug/L
5000
10
10/10/16 13:52
10/14/16 20:15
100-02-7
N-Nitrosodimethylamine
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
62-75-9
N-Nitroso-di-n-propylamine
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
621-64-7
N-Nitrosodiphenylamine
ND
ug/L
1000
10
10/10/16 13:52
10/14/16 20:15
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
108-60-1
Pentachlorophenol
ND
ug/L
1000
10
10/10/16 13:52
10/14/16 20:15
87-86-5
Phenanthrene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
85-01-8
Phenol
1090
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
Pyrene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
129-00-0
1,2,4-Trichlorobenzene
ND
ug/L
500
10
10/10/16 13:52
10/14/16 20:15
120-82-1
2,4,6 -Trichlorophenol
ND
ug/L
1000
10
10/10/16 13:52
10/14/16 20:15
88-06-2
Surrogates
Nitrobenzene -d5 (S)
0
%
10-120
10
10/10/16 13:52
10/14/16 20:15
4165-60-0
D3,S4
2-Fluorobiphenyl (S)
0
%
15-120
10
10/10/16 13:52
10/14/16 20:15
321-60-8
S4
Terphenyl-d14 (S)
0
%
11-131
10
10/10/16 13:52
10/14/16 20:15
1718-51-0
S4
Phenol-d6(S)
0
%
10-120
10
10/10/16 13:52
10/14/16 20:15
13127-88-3
S4
2-Fluorophenol (S)
0
%
10-120
10
10/10/16 13:52
10/14/16 20:15
367-12-4
S4
2,4,6-Tribromophenol (S)
0
%
10-137
10
10/10/16 13:52
10/14/16 20:15
118-79-6
S4
624 Volatile Organics
Analytical Method: EPA 624
Acrolein
ND
ug/L
25.0
5
10/10/16 21:56
107-02-8
Acrylonitrile
ND
ug/L
250
5
10/10/16 21:56
107-13-1
Benzene
ND
ug/L
10.0
5
10/10/16 21:56
71-43-2
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: WATER TEST
Pace Project No.: 92314764
Sample: 5D Lab ID: 92314764001 Collected: 10/04/16 14:00 Received: 10/04/16 15:26 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua]
624 Volatile Organics Analytical Method: EPA 624
Bromodichloromethane
ND
ug/L
10.0
5
10/10/16 21:56
75-27-4
Bromoform
ND
ug/L
10.0
5
10/10/16 21:56
75-25-2
Bromomethane
ND
ug/L
10.0
5
10/10/16 21:56
74-83-9
Carbon tetrachloride
ND
ug/L
10.0
5
10/10/16 21:56
56-23-5
Chlorobenzene
ND
ug/L
10.0
5
10/10/16 21:56
108-90-7
Chloroethane
ND
ug/L
10.0
5
10/10/16 21:56
75-00-3
2-Chloroethylvinyl ether
ND
ug/L
25.0
5
10/10/16 21:56
110-75-8
c2
Chloroform
ND
ug/L
10.0
5
10/10/16 21:56
67-66-3
Chloromethane
ND
ug/L
10.0
5
10/10/16 21:56
74-87-3
Dibromochlorom ethane
ND
ug/L
10.0
5
10/10/16 21:56
124-48-1
1,2 -Dichlorobenzene
ND
ug/L
10.0
5
10/10/16 21:56
95-50-1
1,3 -Dichlorobenzene
ND
ug/L
10.0
5
10/10/16 21:56
541-73-1
1,4 -Dichlorobenzene
ND
ug/L
10.0
5
10/10/1621:56
106-46-7
Dichlorodifluoromethane
ND
ug/L
10.0
5
10/10/16 21:56
75-71-8
1,1-Dichloroethane
ND
ug/L
10.0
5
10/10/16 21:56
75-34-3
1,2-Dichloroethane
ND
ug/L
10.0
5
10/10/16 21:56
107-06-2
1,1-Dichloroethene
ND
ug/L
10.0
5
10/10/16 21:56
75-35-4
cis- 1,2-Dichloroethene
ND
ug/L
10.0
5
10/10/16 21:56
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
10.0
5
10/10/16 21:56
156-60-5
1,2-Dichloropropane
ND
ug/L
10.0
5
10/10/16 21:56
78-87-5
cis- 1,3-Dichloropropene
ND
ug/L
10.0
5
10/10/16 21:56
10061-01-5
trans- 1,3-Dichloropropene
ND
ug/L
10.0
5
10/10/16 21:56
10061-02-6
Ethylbenzene
ND
ug/L
10.0
5
10/10/16 21:56
100-41-4
Methylene Chloride
ND
ug/L
10.0
5
10/10/16 21:56
75-09-2
1,1,2,2 -Tetrachloroethane
ND
ug/L
10.0
5
10/10/16 21:56
79-34-5
Tetrachloroethene
ND
ug/L
10.0
5
10/10/16 21:56
127-18-4
Toluene
41.5
ug/L
10.0
5
10/10/16 21:56
108-88-3
1,1,1 -Trichloroethane
ND
ug/L
10.0
5
10/10/16 21:56
71-55-6
1,1,2 -Trichloroethane
ND
ug/L
10.0
5
10/10/1621:56
79-00-5
Trichloroethene
ND
ug/L
10.0
5
10/10/16 21:56
79-01-6
Trichlorofluoromethane
ND
ug/L
10.0
5
10/10/16 21:56
75-69-4
Vinyl chloride
ND
ug/L
10.0
5
10/10/16 21:56
75-01-4
Surrogates
4-Bromofluorobenzene (S)
99
%
70-130
5
10/10/16 21:56
460-00-4
D3
Toluene -d8 (S)
112
%
70-130
5
10/10/16 21:56
2037-26-5
1,2-Dichloroethane-d4 (S)
87
%
70-130
5
10/10/16 21:56
17060-07-0
4500S2D Sulfide Water
Analytical Method: SM 4500-S2D
Sulfide
0.15
mg/L
0.10
1
10/07/1611:00
18496-25-8
5540C MBAS Surfactants
Analytical Method: SM 5540C
LAS Molecular Weight, g/mol
320
100
10/06/16 07:41
MBAS, Calculated as LAS
ND
mg/L
20.0
100
10/06/16 07:41
D3
Total Organic Nitrogen Calc.
Analytical Method: TKN-NH3 Calculation
Total Organic Nitrogen
194
mg/L
0.50
1
10/17/16 17:18
REPORT OF LABORATORY ANALYSIS
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reproduced,
except in full,
Date: 10/25/2016 03:50 PM
without
the written consent of Pace Analytical
Services, LLC.
Page 8 of 51

Pace Analytical Services, LLC
® 670
aceAnalytical Raleigh, NC 27607
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: WATER TEST
Pace Project No.: 92314764
Sample: 5D Lab ID: 92314764001 Collected: 10/04/16 14:00 Received: 10/04/16 15:26 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Bromide
ND mg/L
0.50
5
10/12/16 07:44
24959-67-9 D3
Fluoride
ND mg/L
0.50
1
10/08/16 01:34
16984-48-8
Sulfate
2.8 mg/L
2.0
1
10/08/16 01:34
14808-79-8
350.1 Ammonia
Analytical Method: EPA 350.1 1993 Rev 2.0
Nitrogen, Ammonia
77.5 mg/L
5.0
50
10/17/16 14:46
7664-41-7
351.2 Total Kjeldahl Nitrogen
Analytical Method: EPA 351.2
Nitrogen, Kjeldahl, Total
271 mg/L
10.0
20
10/12/16 21:31
7727-37-9
353.2 Nitrogen, NO2/NO3 pres.
Analytical Method: EPA 353.2
Nitrogen, NO2 plus NO3
0.043 mg/L
0.020
1
10/14/16 22:17
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
12.0 mg/L
0.25
5
10/12/16 00:52
7723-14-0
420.4 Phenolics, Total
Analytical Method: EPA 420.4
Phenol
2.8 mg/L
0.30
30
10/13/1614:22
450OCNE Cyanide, Total
Analytical Method: SM 4500 -CN -E
Cyanide
0.017 mg/L
0.0080
1
10/07/1614:31
57-12-5 P4
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 51

(�IacleAnalytical"
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Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332074
QC Batch Method: SM 2120E ColorADMI
Associated Lab Samples: 92314764001
METHOD BLANK: 1839927
Associated Lab Samples: 92314764001
Parameter
Color, ADMI
QUALITY CONTROL DATA
Analysis Method: SM 2120E ColorADMI
Analysis Description: 2120E ColorADMI
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
units ND 25.0 10/06/16 08:25
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1839928
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Color, ADM] units 125 126 101 90-110
SAMPLE DUPLICATE: 1839929
92314599001 Dup
Parameter Units Result Result RPD Qualifiers
Color, ADMI units 28.0 28.0 0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 51

(�IaceAnalyficalo
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Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332939
QC Batch Method: EPA 1664B
Associated Lab Samples: 92314764001
METHOD BLANK: 1845063
Associated Lab Samples: 92314764001
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664B
Analysis Description: 1664 HEM, Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 5.0 10/13/16 08:45
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
1845064
Spike LCS
LCS
% Rec
Parameter
Units
Cone. Result
% Rec
Limits
Qualifiers
Oil and Grease
mg/L
40 35.2
88
78-114
MATRIX SPIKE SAMPLE:
1845065
92314704001 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rec
Limits Qualifiers
Oil and Grease
mg/L
1 AJ 40
35.4
85
78-114
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332563 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 92314764001
METHOD BLANK: 1843065 Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 10/12/16 08:54
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1843066
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.6 103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1843067 1843068
MS MSD
92314296021 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.5 2.4 99 96 75-125 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
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aceAnalytical
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QUALITY CONTROL DATA
Project- WATER TEST
Pace Project No.: 92314764
QC Batch: 332390 Analysis Method: EPA 200.7
QC Batch Method: EPA200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 92314764001
METHOD BLANK: 1842160
Associated Lab Samples: 92314764001
Parameter Units
Aluminum
ug/L
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Boron
ug/L
Cadmium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Iron
ug/L
Lead
ug/L
Magnesium
ug/L
Manganese
ug/L
Molybdenum
ug/L
Nickel
ug/L
Selenium
ug/L
Silver
ug/L
Thallium
ug/L
Tin
ug/L
Titanium
ug/L
Zinc
ug/L
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
100
10/13/1615:53
ND
5.0
10/13/1615:53
ND
10.0
10/14/1615:21
ND
5.0
10/13/1615:53
ND
1.0
10/13/1615:53
NO
50.0
10/13/1615:53
ND
1.0
10/13/1615:53
ND
5.0
10/13/1615:53
ND
5.0
10/13/1615:53
ND
5.0
10/13/1615:53
ND
50.0
10/13/1615:53
ND
5.0
10/13/1615:53
ND
100
10/13/1615:53
ND
5.0
10/13/1615:53
ND
5.0
10/14/1615:21
ND
5.0
10/13/1615:53
ND
10.0
10/13/1615:53
ND
5.0
10/13/1615:53
ND
10.0
10/13/1615:53
ND
5.0
10/13/1615:53
ND
5.0
10/13/1615:53
ND
10.0
10/13/1615:53
Qualifiers
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1842161
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
ug/L
5000
4960
99
85-115
Antimony
ug/L
500
502
100
85-115
Arsenic
ug/L
500
492
98
85-115
Barium
ug/L
500
502
100
85-115
Beryllium
ug/L
500
504
101
85-115
Boron
ug/L
500
496
99
85-115
Cadmium
ug/L
500
501
100
85-115
Chromium
ug/L
500
504
101
85-115
Cobalt
ug/L
500
507
101
85-115
Copper
ug/L
500
514
103
85-115
Iron
ug/L
5000
4960
99
85-115
Lead
ug/L
500
497
99
85-115
Magnesium
ug/L
5000
4970
99
85-115
Manganese
ug/L
500
507
101
85-115
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 51

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1842161
Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Molybdenum
ug/L
500
519
104
85-115
Nickel
ug/L
500
495
99
85-115
Selenium
ug/L
500
507
101
85-115
Silver
ug/L
250
252
101
85-115
Thallium
ug/L
500
509
102
85-115
Tin
ug/L
500
504
101
85-115
Titanium
ug/L
500
501
100
85-115
Zinc
ug/L
500
515
103
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1842162
1842163
MS
MSD
92314604001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Cone.
Cone.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Aluminum
ug/L
ND
5000
5000
5000
4980
100
99
70-130
0
Antimony
ug/L
ND
500
500
508
506
101
101
70-130
0
Arsenic
ug/L
ND
500
500
498
496
99
98
70-130
1
Barium
ug/L
0.0086
500
500
512
511
101
100
70-130
0
mg/L
Beryllium
ug/L
ND
500
500
510
508
102
102
70-130
0
Boron
ug/L
0.20
500
500
703
708
100
101
70-130
1
mg/L
Cadmium
ug/L
ND
500
500
503
501
101
100
70-130
0
Chromium
ug/L
ND
500
500
497
501
99
100
70-130
1
Cobalt
ug/L
ND
500
500
502
499
100
100
70-130
1
Copper
ug/L
0.0062
500
500
524
523
103
103
70-130
0
mg/L
Iron
ug/L
0.60
5000
5000
5560
5560
99
99
70-130
0
mg/L
Lead
ug/L
ND
500
500
491
488
98
97
70-130
1
Magnesium
ug/L
2.1
5000
5000
6880
6940
96
98
70-130
1
mg/L
Manganese
ug/L
0.069
500
500
566
568
99
100
70-130
0
mg/L
Molybdenum
ug/L
0.011
500
500
536
534
105
105
70-130
0
mg/L
Nickel
ug/L
0.011
500
500
499
498
98
97
70-130
0
mg/L
Selenium
ug/L
ND
500
500
513
510
102
102
70-130
1
Silver
ug/L
ND
250
250
250
251
100
100
70-130
0
Thallium
ug/L
ND
500
500
500
496
99
99
70-130
1
Tin
ug/L
ND
500
500
500
504
100
100
70-130
1
Titanium
ug/L
ND
500
500
504
504
101
101
70-130
0
Zinc
ug/L
0.011
500
500
518
518
101
101
70-130
0
mg/L
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 51

(�15'cieAnalytical"
www.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: WATER TEST
Pace Project No.: 92314764
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1842164
1842165
MS
MSD
92314779001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter
Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Aluminum
ug/L
253
5000
5000
5270
5270
100
100
70-130
0
Antimony
ug/L
384
500
500
880
883
99
100
70-130
0
Arsenic
ug/L
ND
500
500
489
489
97
97
70-130
0
Barium
ug/L
6.8
500
500
513
512
101
101
70-130
0
Beryllium
ug/L
ND
500
500
507
506
101
101
70-130
0
Boron
ug/L
ND
500
500
506
510
99
100
70-130
1
Cadmium
ug/L
ND
500
500
498
499
100
100
70-130
0
Chromium
ug/L
12.9
500
500
508
508
99
99
70-130
0
Cobalt
ug/L
ND
500
500
498
497
100
99
70-130
0
Copper
ug/L
17.3
500
500
531
530
103
103
70-130
0
Iron
ug/L
223
5000
5000
5170
5160
99
99
70-130
0
Lead
ug/L
ND
500
500
485
486
97
97
70-130
0
Magnesium
ug/L
2160
5000
5000
7030
7060
97
98
70-130
0
Manganese
ug/L
7.4
500
500
504
504
99
99
70-130
0
Molybdenum
ug/L
ND
500
500
519
524
104
105
70-130
1
Nickel
ug/L
ND
500
500
485
486
97
97
70-130
0
Selenium
ug/L
ND
500
500
503
504
100
101
70-130
0
Silver
ug/L
ND
250
250
250
249
100
100
70-130
0
Thallium
ug/L
ND
500
500
497
494
99
99
70-130
1
Tin
ug/L
13.1
500
500
509
511
99
100
70-130
0
Titanium
ug/L
5.6
500
500
506
505
100
100
70-130
0
Zinc
ug/L
19.8
500
500
517
515
99
99
70-130
0
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 51

aceAnalytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332528 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92314764001
METHOD BLANK: 1842838
Associated Lab Samples: 92314764001
Parameter Units
1,1,1 -Trichloroethane
ug/L
1,1,2,2 -Tetrachloroethane
ug/L
1,1,2 -Trichloroethane
ug/L
1,1-Dichloroethane
ug/L
1,1-Dichloroethene
ug/L
1,2 -Dichlorobenzene
ug/L
1,2-Dichloroethane
ug/L
1,2-Dichloropropane
ug/L
1,3 -Dichlorobenzene
ug/L
1,4 -Dichlorobenzene
ug/L
2-Chloroethylvinyl ether
ug/L
Acrolein
ug/L
Acrylonitrile
ug/L
Benzene
ug/L
Bromodichloromethane
ug/L
Bromoform
ug/L
Bromomethane
ug/L
Carbon tetrachloride
ug/L
Chlorobenzene
ug/L
Chloroethane
ug/L
Chloroform
ug/L
Chloromethane
ug/L
cis- 1,2-Dichloroethene
ug/L
cis- 1,3-Dichloropropene
ug/L
Dibromochlorom ethane
ug/L
Ethylbenzene
ug/L
Methylene Chloride
ug/L
Tetrachloroethene
ug/L
Toluene
ug/L
trans-1,2-Dichloroethene
ug/L
trans-1,3-Dichloropropene
ug/L
Trichloroethene
ug/L
Trichlorofluoromethane
ug/L
Vinyl chloride
ug/L
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
Toluene -d8 (S)
%
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
5.0
10/10/1612:33
ND
5.0
10/10/1612:33
ND
50.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
ND
2.0
10/10/1612:33
93
70-130
10/10/1612:33
91
70-130
10/10/16 12:33
105
70-130
10/10/1612:33
Qualifiers
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
LABORATORY CONTROL SAMPLE: 1842839
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 51
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,1 -Trichloroethane
ug/L
20
20.4
102
52-162
1,1,2,2 -Tetrachloroethane
ug/L
20
17.6
88
46-157
1,1,2 -Trichloroethane
ug/L
20
18.2
91
52-150
1,1-Dichloroethane
ug/L
20
20.1
100
59-155
1,1-Dichloroethene
ug/L
20
22.2
111
1-234
1,2 -Dichlorobenzene
ug/L
20
19.2
96
18-190
1,2-Dichloroethane
ug/L
20
18.6
93
49-155
1,2-Dichloropropane
ug/L
20
18.7
93
1-210
1,3 -Dichlorobenzene
ug/L
20
17.7
89
59-156
1,4 -Dichlorobenzene
ug/L
20
18.1
90
18-190
2-Chloroethylvinyl ether
ug/L
40
36.7
92
1-305
Acrolein
ug/L
100
109
109
15-152
Acrylonitrile
ug/L
100
105
105
75-132
Benzene
ug/L
20
20.2
101
37-151
Bromodichloromethane
ug/L
20
19.8
99
35-155
Bromoform
ug/L
20
19.8
99
45-169
Bromomethane
ug/L
20
34.5
172
1-242
Carbon tetrachloride
ug/L
20
21.2
106
70-140
Chlorobenzene
ug/L
20
19.0
95
37-160
Chloroethane
ug/L
20
20.5
102
14-230
Chloroform
ug/L
20
19.9
100
51-138
Chloromethane
ug/L
20
28.5
143
1-273
cis-1,2-Dichloroethene
ug/L
20
21.0
105
68-146
cis- 1,3-Dichloropropene
ug/L
20
19.4
97
1-227
Dibromochloromethane
ug/L
20
19.8
99
53-149
Ethylbenzene
ug/L
20
18.5
93
37-162
Methylene Chloride
ug/L
20
19.7
98
1-221
Tetrachloroethene
ug/L
20
18.3
92
64-148
Toluene
ug/L
20
19.1
95
47-150
trans-1,2-Dichloroethene
ug/L
20
21.1
105
54-156
trans- 1,3-Dichloropropene
ug/L
20
18.5
93
17-183
Trichloroethene
ug/L
20
21.1
106
71-157
Trichlorofluoromethane
ug/L
20
23.5
118
17-181
Vinyl chloride
ug/L
20
22.5
113
1-251
1,2-Dichloroethane-d4 (S)
%
102
70-130
4-Bromofluorobenzene (S)
%
101
70-130
Toluene -d8 (S)
%
98
70-130
MATRIX SPIKE SAMPLE:
1842841
92315108002
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1 -Trichloroethane
ug/L
ND
20
22.2
111
46-171
1,1,2,2 -Tetrachloroethane
ug/L
ND
20
19.5
97
73-159
1,1,2 -Trichloroethane
ug/L
ND
20
19.8
99
64-152
1,1-Dichloroethane
ug/L
ND
20
20.7
103
43-172
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 51

laneAnalyficalo
www.pacelabs.com
QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
MATRIX SPIKE SAMPLE:
Parameter
1842841
Units
92315108002
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/L
ND
20
17.9
89
48-189
1,2 -Dichlorobenzene
ug/L
ND
20
21.5
107
54-154
1,2-Dichloroethane
ug/L
ND
20
20.8
104
42-171
1,2-Dichloropropane
ug/L
ND
20
21.5
107
55-157
1,3 -Dichlorobenzene
ug/L
ND
20
20.0
100
57-148
1,4 -Dichlorobenzene
ug/L
ND
20
20.1
100
58-149
2-Chloroethylvinyl ether
ug/L
ND
40
ND
0
70-130 P5
Acrolein
ug/L
ND
100
96.1
96
70-130
Acrylonitrile
ug/L
ND
100
107
107
70-130
Benzene
ug/L
ND
20
21.8
109
54-163
Bromodichloromethane
ug/L
ND
20
22.9
115
56-152
Bromoform
ug/L
ND
20
22.3
111
53-151
Bromomethane
ug/L
ND
20
10.6
53
10-200
Carbon tetrachloride
ug/L
ND
20
22.1
110
41-175
Chlorobenzene
ug/L
ND
20
21.6
108
67-152
Chloroethane
ug/L
ND
20
11.2
56
23-200
Chloroform
ug/L
ND
20
21.6
108
51-166
Chloromethane
ug/L
ND
20
3.1
15
40-175 M1
cis- 1,2-Dichloroethene
ug/L
ND
20
21.8
109
45-174
cis- 1,3-Dichloropropene
ug/L
ND
20
20.0
100
38-146
Dibromochloromethane
ug/L
ND
20
21.1
105
65-144
Ethylbenzene
ug/L
ND
20
21.0
105
57-152
Methylene Chloride
ug/L
ND
20
19.8
99
40-167
Tetrachloroethene
ug/L
ND
20
20.3
102
59-155
Toluene
ug/L
ND
20
22.3
112
47-162
trans-1,2-Dichloroethene
ug/L
ND
20
21.1
105
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
19.7
99
39-148
Trichloroethene
ug/L
ND
20
21.0
105
60-153
Trichlorofluoromethane
ug/L
ND
20
15.6
78
42-199
Vinyl chloride
ug/L
ND
20
4.4
22
46-176 M1
1,2-Dichloroethane-d4 (S)
%
100
70-130
4-Bromofluorobenzene (S)
%
99
70-130
Toluene -d8 (S)
%
101
70-130
SAMPLE DUPLICATE: 1842840
Parameter
Units
92315108001
Result
Dup
Result RPD Qualifiers
1,1,1 -Trichloroethane
ug/L
ND
ND
1,1,2,2 -Tetrachloroethane
ug/L
ND
ND
1,1,2 -Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2 -Dichlorobenzene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 51

aceAnalytical
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
SAMPLE DUPLICATE: 1842840
Parameter
Units
92315108001
Result
Dup
Result
1,3 -Dichlorobenzene
ug/L
ND
ND
1,4 -Dichlorobenzene
ug/L
ND
ND
2-Chloroethylvinyl ether
ug/L
ND
ND
Acrolein
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis- 1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans-1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
94
91
4-Bromofluorobenzene (S)
%
92
93
Toluene -d8 (S)
%
105
106
RPD Qualifiers
3
2
1
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 51

lacieAnalyfical"
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Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332077
QC Batch Method: EPA 3510
Associated Lab Samples: 92314764001
METHOD BLANK: 1839937
Associated Lab Samples: 92314764001
Parameter Units
4,4' -DDD
ug/L
4,4' -DDE
ug/L
4,4' -DDT
ug/L
Aldrin
ug/L
alpha -BHC
ug/L
beta -BHC
ug/L
Chlordane (Technical)
ug/L
delta -BHC
ug/L
Dieldrin
ug/L
Endosulfan I
ug/L
Endosulfan II
ug/L
Endosulfan sulfate
ug/L
Endrin
ug/L
Endrin aldehyde
ug/L
gamma -BHC (Lindane)
ug/L
Heptachlor
ug/L
Heptachlor epoxide
ug/L
PCB -1016 (Aroclor 1016)
ug/L
PCB -1221 (Aroclor 1221)
ug/L
PCB -1232 (Aroclor 1232)
ug/L
PCB -1242 (Aroclor 1242)
ug/L
PCB -1248 (Aroclor 1248)
ug/L
PCB -1254 (Aroclor 1254)
ug/L
PCB -1260 (Aroclor 1260)
ug/L
Toxaphene
ug/L
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
QUALITY CONTROL DATA
Analysis Method:
Analysis Description
Matrix: Water
EPA 608
608 GCS Pest PCB
Blank
Result
Reporting
Limit
Analyzed
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.050
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.50
10/08/16 00:25
ND
0.50
10/08/16 00:25
78
20-138
10/08/16 00:25
77
20-110
10/08/16 00:25
Qualifiers
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
1839938
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
4,4' -DDD
ug/L
.25
0.23
94
31-141
4,4' -DDE
ug/L
.25
0.23
93
30-145
4,4' -DDT
ug/L
.25
0.22
88
25-160
Aldrin
ug/L
.25
0.21
83
42-122
alpha -BHC
ug/L
.25
0.24
98
37-134
beta -BHC
ug/L
.25
0.23
95
17-147
delta -BHC
ug/L
.25
0.27
107
19-140
Dieldrin
ug/L
.25
0.22
89
36-146
Endosulfan I
ug/L
.25
0.23
93
45-153
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 20 of 51

lacieAnalj6cal"
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
LABORATORY CONTROL SAMPLE: 1839938
Parameter
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Endosulfan II
ug/L
.25
0.24
98
1-202
Endosulfan sulfate
ug/L
.25
0.25
101
26-144
Endrin
ug/L
.25
0.25
102
30-147
Endrin aldehyde
ug/L
.25
0.22
88
50-150
gamma -BHC (Lindane)
ug/L
.25
0.25
103
32-127
Heptachlor
ug/L
.25
0.23
92
34-111
Heptachlor epoxide
ug/L
.25
0.24
96
41-126
Decachlorobiphenyl (S)
%
93
20-138
Tetrachloro-m-xylene (S)
%
103
20-110
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 21 of 51

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332504 Analysis Method: EPA 625
QC Batch Method: EPA 625 Analysis Description: 625 MSS
Associated Lab Samples: 92314764001
METHOD BLANK: 1842701
Associated Lab Samples: 92314764001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
1,2,4-Trichlorobenzene
ug/L
ND
5.0
10/11/1618:04
1,2-Diphenylhydrazine
ug/L
ND
5.0
10/11/1618:04
2,2'-Oxybis(1-chloropropane)
ug/L
ND
5.0
10/11/1618:04
2,4,6 -Trichlorophenol
ug/L
ND
10.0
10/11/1618:04
2,4-Dichlorophenol
ug/L
ND
5.0
10/11/1618:04
2,4 -Dimethylphenol
ug/L
ND
10.0
10/11/1618:04
2,4-Dinitrophenol
ug/L
ND
50.0
10/11/1618:04
2,4-Dinitrotoluene
ug/L
ND
5.0
10/11/1618:04
2,6-Dinitrotoluene
ug/L
ND
5.0
10/11/1618:04
2-Chloronaphthalene
ug/L
ND
5.0
10/11/1618:04
2 -Chlorophenol
ug/L
ND
5.0
10/11/1618:04
2-Nitrophenol
ug/L
ND
5.0
10/11/1618:04
3,3'-Dichlorobenzidine
ug/L
ND
25.0
10/11/1618:04
4,6-Dinitro-2-methylphenol
ug/L
ND
20.0
10/11/1618:04
4-Bromophenylphenyl ether
ug/L
ND
5.0
10/11/16 18:04
4-Chloro-3-methylphenol
ug/L
ND
5.0
10/11/1618:04
4-Chlorophenylphenyl ether
ug/L
ND
5.0
10/11/16 18:04
4-Nitrophenol
ug/L
ND
50.0
10/11/1618:04
Acenaphthene
ug/L
ND
5.0
10/11/1618:04
Acenaphthylene
ug/L
ND
5.0
10/11/1618:04
Anthracene
ug/L
ND
5.0
10/11/1618:04
Benzidine
ug/L
ND
50.0
10/11/1618:04
Benzo(a)anthracene
ug/L
ND
5.0
10/11/1618:04
Benzo(a)pyrene
ug/L
ND
5.0
10/11/1618:04
Benzo(b)fluoranthene
ug/L
ND
5.0
10/11/1618:04
Benzo(g,h,i)perylene
ug/L
ND
5.0
10/11/1618:04
Benzo(k)fluoranthene
ug/L
ND
5.0
10/11/1618:04
bis(2-Chloroethoxy)methane
ug/L
ND
10.0
10/11/1618:04
bis(2-Chloroethyl) ether
ug/L
ND
5.0
10/11/16 18:04
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
10/11/1618:04
Butylbenzylphthalate
ug/L
ND
5.0
10/11/1618:04
Chrysene
ug/L
ND
5.0
10/11/1618:04
Di-n-butylphthalate
ug/L
ND
5.0
10/11/1618:04
Di-n-octylphthalate
ug/L
ND
5.0
10/11/1618:04
Dibenz(a,h)anthracene
ug/L
ND
5.0
10/11/1618:04
Diethylphthalate
ug/L
ND
5.0
10/11/1618:04
Dimethylphthalate
ug/L
ND
5.0
10/11/1618:04
Fluoranthene
ug/L
ND
5.0
10/11/1618:04
Fluorene
ug/L
ND
5.0
10/11/1618:04
Hexachloro-1,3-butadiene
ug/L
ND
5.0
10/11/1618:04
Hexachlorobenzene
ug/L
ND
5.0
10/11/1618:04
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 22 of 51

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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
METHOD BLANK: 1842701
Associated Lab Samples: 92314764001
Parameter
Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed
Hexachlorocyclopentadiene
ug/L
ND
10.0
10/11/1618:04
Hexachloroethane
ug/L
ND
5.0
10/11/1618:04
Indeno(1,2,3-cd)pyrene
ug/L
ND
5.0
10/11/1618:04
Isophorone
ug/L
ND
10.0
10/11/1618:04
N-Nitroso-di-n-propylamine
ug/L
ND
5.0
10/11/1618:04
N-Nitrosodimethylamine
ug/L
ND
5.0
10/11/1618:04
N-Nitrosodiphenylamine
ug/L
ND
10.0
10/11/1618:04
Naphthalene
ug/L
ND
5.0
10/11/1618:04
Nitrobenzene
ug/L
ND
5.0
10/11/1618:04
Pentachlorophenol
ug/L
ND
10.0
10/11/1618:04
Phenanthrene
ug/L
ND
5.0
10/11/1618:04
Phenol
ug/L
ND
5.0
10/11/1618:04
Pyrene
ug/L
ND
5.0
10/11/1618:04
2,4,6-Tribromophenol (S)
%
64
10-137
10/11/16 18:04
2-Fluorobiphenyl (S)
%
59
15-120
10/11/16 18:04
2-Fluorophenol (S)
%
39
10-120
10/11/16 18:04
Nitrobenzene -d5 (S)
%
66
10-120
10/11/16 18:04
Phenol-d6(S)
%
25
10-120
10/11/16 18:04
Terphenyl-d14 (S)
%
85
11-131
10/11/16 18:04
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1842702
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
1,2,4-Trichlorobenzene
ug/L
50
41.1
82
44-142
1,2-Diphenylhydrazine
ug/L
50
42.1
84
25-150
2,2'-Oxybis(1-chloropropane)
ug/L
50
49.4
99
36-166
2,4,6 -Trichlorophenol
ug/L
50
45.4
91
37-144
2,4-Dichlorophenol
ug/L
50
53.0
106
1-191
2,4 -Dimethylphenol
ug/L
50
53.8
108
32-119
2,4-Dinitrophenol
ug/L
250
135
54
1-181
2,4-Dinitrotoluene
ug/L
50
47.0
94
39-139
2,6-Dinitrotoluene
ug/L
50
48.1
96
50-158
2-Chloronaphthalene
ug/L
50
37.8
76
60-118
2 -Chlorophenol
ug/L
50
40.3
81
23-134
2-Nitrophenol
ug/L
50
50.8
102
29-182
3,3'-Dichlorobenzidine
ug/L
100
94.7
95
1-262
4,6-Dinitro-2-methylphenol
ug/L
100
93.0
93
1-181
4-Bromophenylphenyl ether
ug/L
50
53.2
106
53-127
4-Chloro-3-methylphenol
ug/L
100
88.3
88
22-147
4-Chlorophenylphenyl ether
ug/L
50
46.7
93
25-158
4-Nitrophenol
ug/L
250
84.7
34
1-132
Acenaphthene
ug/L
50
39.0
78
47-145
Acenaphthylene
ug/L
50
39.2
78
33-145
Anthracene
ug/L
50
47.2
94
1-166
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
LABORATORY CONTROL SAMPLE:
Parameter
1842702
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Benzidine
ug/L
100
34J
34
25-150
Benzo(a)anthracene
ug/L
50
46.0
92
33-143
Benzo(a)pyrene
ug/L
50
44.5
89
17-163
Benzo(b)fluoranthene
ug/L
50
43.1
86
24-159
Benzo(k)fluoranthene
ug/L
50
46.3
93
11-162
bis(2-Chloroethoxy)methane
ug/L
50
50.1
100
33-184
bis(2-Chloroethyl) ether
ug/L
50
45.0
90
12-158
bis(2-Ethylhexyl)phthalate
ug/L
50
49.2
98
8-158
Butylbenzylphthalate
ug/L
50
46.5
93
1-152
Chrysene
ug/L
50
46.7
93
17-168
Di-n-butylphthalate
ug/L
50
51.2
102
1-118
Di-n-octylphthalate
ug/L
50
50.2
100
4-146
Dibenz(a,h)anthracene
ug/L
50
51.3
103
1-227
Diethylphtha late
ug/L
50
43.1
86
1-114
Dimethylphthalate
ug/L
50
40.7
81
1-112
Fluoranthene
ug/L
50
48.4
97
26-137
Fluorene
ug/L
50
39.8
80
59-121
Hexachloro-1,3-butadiene
ug/L
50
38.2
76
24-116
Hexachlorobenzene
ug/L
50
49.1
98
1-152
Hexachlorocyclopentadiene
ug/L
50
38.3
77
25-150
Hexachloroethane
ug/L
50
32.3,
65
40-113
Indeno(1,2,3-cd)pyrene
ug/L
50
47.4
95
1-171
Isophorone
ug/L
50
52.6
105
21-196
N-Nitroso-di-n-propylamine
ug/L
50
46.8
94
1-230
N-Nitrosodimethylamine
ug/L
50
24.1
48
25-150
N-Nitrosodiphenylamine
ug/L
50
44.5
89
25-150
Naphthalene
ug/L
50
37.1
74
21-133
Nitrobenzene
ug/L
50
47.8
96
35-180
Pentachlorophenol
ug/L
100
99.6
100
14-176
Phenanthrene
ug/L
50
46.3
93
54-120
Phenol
ug/L
50
23.9
48
5-112
Pyrene
ug/L
50
44.3
89
52-115
2,4,6-Tribromophenol (S)
%
102
10-137
2-Fluorobiphenyl (S)
%
73
15-120
2-Fluorophenol (S)
%
48
10-120
Nitrobenzene -d5 (S)
%
83
10-120
Phenol -d6 (S)
%
37
10-120
Terphenyl-d14 (S)
%
95
11-131
SAMPLE DUPLICATE: 1842704
92315395006 Dup
Parameter Units Result Result RPD Qualifiers
1,2,4-Trichlorobenzene ug/L ND ND
1,2-Diphenylhydrazine ug/L ND ND
2,2'-Oxybis(1-chloropropane) ug/L ND ND
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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(�IacieAnalyficalo
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
SAMPLE DUPLICATE: 1842704
Parameter
Units
92315395006
Result
Dup
Result
2,4,6 -Trichlorophenol
ug/L
ND
ND
2,4-Dichlorophenol
ug/L
ND
ND
2,4 -Dimethylphenol
ug/L
ND
ND
2,4-Dinitrophenol
ug/L
ND
ND
2,4-Dinitrotoluene
ug/L
ND
ND
2,6-Dinitrotoluene
ug/L
ND
ND
2-Chloronaphthalene
ug/L
ND
ND
2 -Chlorophenol
ug/L
ND
ND
2-Nitrophenol
ug/L
ND
ND
3,3'-Dichlorobenzidine
ug/L
ND
ND
4,6-Dinitro-2-methylphenol
ug/L
ND
ND
4-Bromophenylphenyl ether
ug/L
ND
ND
4 -Chloro -3 -methyl phenol
ug/L
ND
ND
4-Chlorophenylphenyl ether
ug/L
ND
ND
4-Nitrophenol
ug/L
ND
ND
Acenaphthene
ug/L
ND
ND
Acenaphthylene
ug/L
ND
ND
Anthracene
ug/L
ND
ND
Benzidine
ug/L
ND
ND
Benzo(a)anthracene
ug/L
ND
ND
Benzo(a)pyrene
ug/L
ND
ND
Benzo(b)fluoranthene
ug/L
ND
ND
Benzo(g,h,i)perylene
ug/L
ND
ND
Benzo(k)fluoranthene
ug/L
ND
ND
bis(2-Chloroethoxy)methane
ug/L
ND
ND
bis(2-Chloroethyl) ether
ug/L
ND
ND
bis(2-Ethylhexyl)phthalate
ug/L
ND
ND
Butylbenzylphthalate
ug/L
ND
ND
Chrysene
ug/L
ND
ND
Di-n-butylphthalate
ug/L
ND
ND
Di-n-octylphthalate
ug/L
ND
ND
Dibenz(a,h)anthracene
ug/L
ND
ND
Diethylphthalate
ug/L
ND
ND
Dimethylphthalate
ug/L
ND
ND
Fluoranthene
ug/L
ND
ND
Fluorene
ug/L
ND
ND
Hexachloro-1,3-butadiene
ug/L
ND
ND
Hexachlorobenzene
ug/L
ND
ND
Hexachlorocyclopentadiene
ug/L
ND
ND
Hexachloroethane
ug/L
ND
ND
Indeno(1,2,3-cd)pyrene
ug/L
ND
ND
Isophorone
ug/L
ND
ND
N-Nitroso-di-n-propylamine
ug/L
ND
ND
N-Nitrosodimethylamine
ug/L
ND
ND
N-Nitrosodiphenylamine
ug/L
ND
ND
Naphthalene
ug/L
ND
ND
Nitrobenzene
ug/L
ND
ND
RPD Qualifiers
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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aceAnalydcal
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
SAMPLE DUPLICATE: 1842704
Parameter
Units
92315395006
Result
Dup
Result
Pentachlorophenol
ug/L
ND
ND
Phenanthrene
ug/L
ND
ND
Phenol
ug/L
ND
ND
Pyrene
ug/L
ND
ND
2,4,6-Tribromophenol (S)
%
95
78
2-Fluorobiphenyl (S)
%
71
62
2-Fluorophenol (S)
%
41
32
Nitrobenzene -d5 (S)
%
75
66
Phenol -d6 (S)
%
27
22
Terphenyl-d14 (S)
%
86
94
RPD Qualifiers
19
14
23
14
20
9
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332179 Analysis Method: SM 4500-S2D
QC Batch Method: SM 4500-S2D Analysis Description: 4500S2D Sulfide Water
Associated Lab Samples: 92314764001
METHOD BLANK: 1840719 Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Sulfide mg/L ND 0.10 10/07/1611:00
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1840720
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Sulfide mg/L .5 0.50 100 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1840721 1840722
MS MSD
92314716004 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Sulfide mg/L ND .5 .5 0.51 0.51 103 102 80-120 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1840723 1840724
MS MSD
92314698002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/L NO .5 .5 0.51 0.51 103 102 80-120 1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 51

laceAnalyficalo
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QC Batch: 324645
Analysis Method:
SM 5540C
QC Batch Method: SM 5540C
Analysis Description:
5540C MBAS Surfactants
Associated Lab Samples: 92314764001
METHOD BLANK: 1731315
Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
LAS Molecular Weight, g/mol
320
10/06/16 07:41
MBAS, Calculated as LAS
mg/L
ND 0.20 10/06/16 07:41
LABORATORY CONTROL SAMPLE: 1731316
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
LAS Molecular Weight, g/mol
320
MBAS, Calculated as LAS
mg/L
.3 0.30
100 90-110
MATRIX SPIKE SAMPLE: 1731318
35268980001 Spike
MS MS % Rec
Parameter
Units
Result Conc.
Result % Rec Limits Qualifiers
LAS Molecular Weight, g/mol
320
320
MBAS, Calculated as LAS
mg/L
<0.074 .3
0.30 90 90-110
SAMPLE DUPLICATE: 1731317
35268980001 Dup
Parameter Units Result Result
LAS Molecular Weight, g/mol 320 320
MBAS, Calculated as LAS mg/L <0.074 ND
RPD Qualifiers
0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332319 Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92314764001
METHOD BLANK: 1841497 Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fluoride mg/L ND 0.50 10/07/1619:04
Sulfate mg/L ND 2.0 10/07/1619:04
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1841498
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Fluoride mg/L 2.5 2.4 97 90-110
Sulfate mg/L 20 19.0 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1841499
1841500
MS
MSD
92314888001 Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec
% Rec Limits RPD Qual
Fluoride mg/L <0.50 2.5
2.5
2.3
2.4 85
86 90-110 1 M1
Sulfate mg/L 28.0 20
20
45.7
44.0 89
80 90-110 4 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1841501
1841502
MS
MSD
92314972003 Spike
Spike
MS
MSD
MS MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result
% Rec % Rec Limits RPD Qual
Fluoride mg/L 0.30J 2.5
2.5
2.9
2.9
104 104 90-110 0
Sulfate mg/L 38.6 20
20
53.6
53.4
75 74 90-110 0 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 51

(�5a'&eAnalytical"
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 324916 Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92314764001
METHOD BLANK: 1733455 Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Bromide mg/L ND 0.10 10/11/16 07:05
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1733456
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Bromide mg/L 10 9.5 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1733457 1733458
MS MSD
35268870001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Bromide mg/L 0.0691-1 10 10 9.4 9.4 94 94 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1733459 1733460
MS MSD
35269294001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Bromide mg/L 0.069U 10 10 9.4 9.2 94 92 90-110 2
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
Page 30 of 51

(�IaveAnalyfica(
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Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 333364
QC Batch Method: EPA 350.1 1993 Rev 2.0
Associated Lab Samples: 92314764001
METHOD BLANK: 1847383
Associated Lab Samples: 92314764001
Parameter Units
Nitrogen, Ammonia mg/L
LABORATORY CONTROL SAMPLE: 1847384
Parameter Units
Nitrogen, Ammonia mg/L
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 1993 Rev 2.0
Analysis Description: 350.1 Ammonia
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 10/17/1614:18
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
5 5.0 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1847385 1847386
MS MSD
92314724002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qua]
Nitrogen, Ammonia mg/L ND 5 5 4.8 4.8 97 97 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1847387 1847388
MS MSD
92314724003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L ND 5 5 4.8 4.8 96 97 90-110 0
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332579 Analysis Method: EPA 351.2
QC Batch Method: EPA 351.2 Analysis Description: 351.2 TKN
Associated Lab Samples: 92314764001
METHOD BLANK: 1843127 Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/12/16 21:20
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1843128
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L 10 10.9 109 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1843129 1843130
MS MSD
92315377001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Kjeldahl, Total mg/L ND 10 10 10.3 10 100 96 90-110 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QC Batch: 332982
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92314764001
METHOD BLANK: 1845266
Matrix: Water
Associated Lab Samples: 92314764001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L
ND 0.020
10/14/16 22:03
LABORATORY CONTROL SAMPLE: 1845267
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L
2.5
2.4
97 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1845268
1845269
MS
MSD
92313532004
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.037
2.5
2.5 2.4
2.4 95 95
75-125
0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1845270
1845271
MS
MSD
92315221001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Nitrogen, NO2 plus NO3 mg/L 0.88
2.5
2.5 3.3
3.3 96 96
75-125
0
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QC Batch: 332559
Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1
Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92314764001
METHOD BLANK: 1843047
Matrix: Water
Associated Lab Samples: 92314764001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Phosphorus mg/L
ND 0.050
10/12/16 00:07
LABORATORY CONTROL SAMPLE: 1843048
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus mg/L
2.5
2.6
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1843049
1843050
MS
MSD
92314720001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qua[
Phosphorus mg/L 3.3
2.5
2.5 5.5
5.6 87 91
90-110
1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1843051
1843052
MS
MSD
92314898002
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Phosphorus mg/L 39.0
2.5
2.5 43.8
41.7 193 108
90-110
5 M6
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332847 Analysis Method: EPA 420.4
QC Batch Method: EPA 420.4 Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92314764001
METHOD BLANK: 1844475 Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phenol mg/L ND 0.010 10/13/1613:51
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1844476
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phenol mg/L .05 0.052 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1844477 1844478
MS MSD
92314691001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua]
Phenol mg/L 0.040 .05 .05 0.072 0.072 63 64 90-110 1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1844479 1844480
MS MSD
92315037002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phenol mg/L 0.064 .05 .05 0.085 0.084 42 39 90-110 2 M1
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC.
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(�55'ce A nalyfical
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QUALITY CONTROL DATA
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 332109 Analysis Method: SM 4500 -CN -E
QC Batch Method: SM 4500 -CN -E Analysis Description: 450OCNE Cyanide, Total
Associated Lab Samples: 92314764001
METHOD BLANK: 1840086 Matrix: Water
Associated Lab Samples: 92314764001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Cyanide mg/L ND 0.0080 10/07/1614:11
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
LABORATORY CONTROL SAMPLE: 1840087
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Cyanide mg/L .1 0.10 103 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1840088
1840089
MS
MSD
92314777002 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qual
Cyanide mg/L ND .1
.1
0.11
0.10
103
99
75-125
3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1840090
1840091
MS
MSD
92314840006 Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units Result Conc.
Conc.
Result
Result
% Rec
% Rec
Limits
RPD Qua[
Cyanide mg/L ND .1
.1
0.10
0.10
99
100
75-125
1
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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laneAnalyfical"
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ANALYTICAL RESULTS - RADIOCHEMISTRY
Project: WATER TEST
Pace Project No.: 92314764
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Sample: 5D
Lab ID: 92314764001 Collected: 10/04/16 14:00
Received:
10/04/16 15:26 Matrix: Water
PWS:
Site ID:
Sample Type:
Parameters
Method
Act ± Unc (MDC) Carr Trac
Units
Analyzed
CAS No. Qual
Gross Alpha
EPA 900.0
0.344 ± 9.81 (19.2)
pCi/L
10/20/16 18:41
12587-46-1
C:NA T. -NA
Gross Beta
EPA 900.0
1,146±206 (8.26)
pCi/L
10/20/1618:41
12587-47-2
C:NA T:NA
Total Alpha Radium
EPA 903.0
0.392:1: 0.365 (0.642)
pCi/L
10/23/16 14:19
C:84% T:NA
Radium -226
EPA 903.1
-0.191 ± 0.872 (1.77)
pCi/L
10/25/16 10:07
13982-63-3
C:NA T:41%
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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(�IaceAnalyfical"
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QUALITY CONTROL - RADIOCHEMISTRY
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 237220 Analysis Method: EPA 903.0
QC Batch Method: EPA 903.0 Analysis Description: 903.0 Total Alpha Radium
Associated Lab Samples: 92314764001
METHOD BLANK: 1165801 Matrix: Water
Associated Lab Samples: 92314764001
Parameter Act ± Unc (MDC) Carr Trac
Total Alpha Radium 0.149±0.152 (0.273) C:96% TTNA
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Units Analyzed Qualifiers
pCi/L 10/23/1614:19
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL - RADIOCHEMISTRY
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 237267 Analysis Method: EPA 900.0
QC Batch Method: EPA 900.0 Analysis Description: 900.0 Gross Alpha/Beta
Associated Lab Samples: 92314764001
METHOD BLANK: 1166126 Matrix: Water
Associated Lab Samples: 92314764001
Parameter Act ± Unc (MDC) Carr Trac Units Analyzed Qualifiers
Gross Alpha -0.863±0.902 (2.95) C:NA TTNA pCi/L 10/20/16 16:16
Gross Beta 4.16±2.22 (3.94)C:NAT:NA pCi/L 10/20/1616:16 1g
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, LLC.
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QUALITY CONTROL - RADIOCHEMISTRY
Project: WATER TEST
Pace Project No.: 92314764
QC Batch: 237293 Analysis Method: EPA 903.1
QC Batch Method: EPA 903.1 Analysis Description: 903.1 Radium -226
Associated Lab Samples: 92314764001
METHOD BLANK: 1166215 Matrix: Water
Associated Lab Samples: 92314764001
Parameter Act ± Unc (MDC) Carr Trac
Radium -226 0.0880 ± 0.402 (0.238) C:NAT:88%
Units Analyzed
pCi/L 10/25/1610:07
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALIFIERS
Project: WATER TEST
Pace Project No.: 92314764
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Act - Activity
Unc - Uncertainty: SDWA = 1.96 sigma count uncertainty, all other matrices = Expanded Uncertainty (95% confidence interval).
Gamma Spec = Expanded Uncertainty (95.4% Confidence Interval)
(MDC) - Minimum Detectable Concentration
Trac - Tracer Recovery (%)
Carr - Carrier Recovery (%)
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
PASI-O Pace Analytical Services - Ormond Beach
PASI-PA Pace Analytical Services - Greensburg
SAMPLE QUALIFIERS
Sample: 92314764001
[1] Upon receipt at the laboratory, 3 mis of nitric acid were added to the samples to meet the sample preservation
requirement of pH <2 for radiological analyses.
ANALYTE QUALIFIERS
1g The Gross Beta MB associated with samples 30198509001, 2043589001, 2043590001 in this analytical project was
greater than the associated MDC and required analysis RL. Data is reportable w/narration.
D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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Date: 10/25/2016 03:50 PM without the written consent of Pace Analytical Services, LLC. Page 41 of 51

Pace Analytical Services, LLC
(�5a'neAnalyficalo 6701 Conference Drive
Raleigh, NC 27607
www.pacelab&com [phone]
QUALIFIERS
Project: WATER TEST
Pace Project No.: 92314764
ANALYTE QUALIFIERS
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
P4 Sample field preservation does not meet EPA or method recommendations for this analysis.
P5 The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
S2 Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample
re -analysis).
S4 Surrogate recovery not evaluated against control limits due to sample dilution.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether.
REPORT OF LABORATORY ANALYSIS
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aceAnalytical
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Project: WATER TEST
Pace Project No.: 92314764
Lab ID
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
92314764001
Sample ID
51)
51)
51)
5D
51)
5D
51)
51)
51)
5D
51)
5D
51)
51)
5D
51)
51)
51)
51)
51)
5D
51)
Date: 10/25/2016 03:50 PM
Pace Analytical Services, LLC
6701 Conference Drive
Raleigh, NC 27607
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
QC Batch Method
QC Batch
Analytical Method
SM 2120E Color ADMI
332074
EPA1664B
332939
EPA 3510
332077
EPA 608
EPA 200.7
332390
EPA 200.7
EPA 7470
332563
EPA 7470
EPA 625
332504
EPA 625
EPA 624
332528
EPA 900.0
237267
EPA 903.0
237220
EPA 903.1
237293
SM 4500-S2D
332179
SM 5540C
324645
TKN-NH3 Calculation
333461
EPA 300.0
324916
EPA 300.0
332319
EPA 350.1 1993 Rev 2.0
333364
EPA 351.2
332579
EPA 353.2
332982
EPA 365.1
332559
EPA 420.4
332847
SM 4500 -CN -E
332109
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Analytical
Batch
332248
332584
332698
332797
Page 43 of 51

CLIENT NOTIFICATION/RESOLUTION
Person Contacted: Date/Time.,
Comments/Sample
Discrepancy:
Field Data Required? (]Yes []No
Project Manager SCURF Review: lV , / Date: 10 I cfl I be
Project Manager SRF Review: Date:
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copyof this form will besent tc the North Carolina DEHNRCerdficatlon Office (Le.
Out of hold, incorrect preservative, out of temp, Incorrect containers)
i
Page 44—of-51
{ aC8Atla�yb'Cc7i
Document Name:
Sample Condition Upon Recei tiSCUR)
Document Kevlsed: May 24, 2010
Page 1 of 2
Chain of Custody Present?
Document No.:
Issuing Authority:
[]N/A
'
Samples Arrived within Hold Time?
Yes
F•RAL-CS-001-Rev.04
Pace Raleigh Quality Office
2.
Short Hold Time Analysis (42 hr.)?
Yes
[]No
2 of 2 for Internal Use ONLY_
moo=
Name;
`Page
WOW 9231.4764
No
,Cplieri4
r IY A'ris,�
l j
NI& \ 1 `�S Pro ect
-9402%g_2014701'14
i
MYes
Q No
❑UPS ❑Client
II I III' II; Ili'lll',I I I II �II
❑ Commercial
�Pacex
[]Other:
[]N/A
6.
-Pace Containers Used?
Yes
923147,64
Custody Seal Present?
Des ONo
Seats intact? Oyes ONO
Date/Initlak Person Examining Contents:
Packing Material:
[]Bubble Wrap
❑Bubble Bags [None ❑Other:
Samples Field Filtered?
Thermometer:
T1505
Type of Ice: OWet ❑Blue []None 05amples on ice, cooling process has begun
r/
Correction Factor: 0,01C Cooler Temp Corrected ('Cl: Biological Tissue Frozen? []Yes ❑No N/A
Temp should be-abovekeezing
to 6°C
[]No
ON/A
USDA Regulated Soil (P]
N/A, water sample)
Did sample�6riginate In
1—IYnc Nn
a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a forelgn source (Inter atonally,
includIna Hawall and Puerto Hirai? MYes IANo
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: Date/Time.,
Comments/Sample
Discrepancy:
Field Data Required? (]Yes []No
Project Manager SCURF Review: lV , / Date: 10 I cfl I be
Project Manager SRF Review: Date:
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copyof this form will besent tc the North Carolina DEHNRCerdficatlon Office (Le.
Out of hold, incorrect preservative, out of temp, Incorrect containers)
i
Page 44—of-51
Comments/Discrepancy:
Chain of Custody Present?
yes
[No
[]N/A
1.
Samples Arrived within Hold Time?
Yes
[]No
[]N/A
2.
Short Hold Time Analysis (42 hr.)?
Yes
[]No
❑N/A
S.
Rush Tum Around Time Requested?
DYes
No
❑N/A
4.
Sufficient Volume?
MYes
Q No
N/A
5:
Correct Containers Used?
Yes
///
[]No
[]N/A
6.
-Pace Containers Used?
Yes
No
N/A
Containers intact?
1AY.
JJNo
N/A
7.
Samples Field Filtered?
QYes
QNo
N/A
8., Note V sediment is visible in the dissolved container
Sample Labels Match COC?
Aes
[]No
ON/A
,e
9. u'9A ( "y V_ I`��,. CA .o
` y �1U�
V�1U� Ailf S(}tl�l/�vt, { mow+ �v• �1 -i Y vt
-includes Date/TIme/ID/Analysis Matrix
All containers needing add/base preservation have en
10, mores
checked?(
es
❑No
[]N/A
All containers needing preservation are found to be in
ii
"op'"'
compllance with EPA recommendation?
InSOi rrH7
{HNO3, H2SO4, HCI -Q, NaOH >9 Sulfide, NaOH>12 Cyanide)
s
❑No
QN/A
e.a"gou
Exceptions: VOA, Coliform, TOC, Olt and Grease,
yyyts
DRO/8015 (water) DOC;LLH
❑No
N/A
"s°'r'Oq`p1D0
Samples checked for dechlorinatlon?
es
[]No
(]N/A
11.
Heads ace in VOA Vials (>S•6mtn)7
Yes
No
/A
12.
Trip Blank Present?
[Yes
[]No
/A
13.
Trip Blank Custody Seals Present?
[]Yes
[]No
YN/A
PaceTrip Blank lot# (ifpurchased),_
CLIENT NOTIFICATION/RESOLUTION
Person Contacted: Date/Time.,
Comments/Sample
Discrepancy:
Field Data Required? (]Yes []No
Project Manager SCURF Review: lV , / Date: 10 I cfl I be
Project Manager SRF Review: Date:
Note: Wheneverthere is a discrepancy affecting North Carolina compliance samples, a copyof this form will besent tc the North Carolina DEHNRCerdficatlon Office (Le.
Out of hold, incorrect preservative, out of temp, Incorrect containers)
i
Page 44—of-51

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October 06, 2016
Terri Paize
Pace Analytical Services, Inc.
205 East Meadow Rd Suite A
Eden NC 27288
TEL: [phone]
FAX: [phone]
RE: 92314764
Dear Terri Page:
MALY7XCAL ENVIRONMENTAL S►ERVICESj INC.
Order No: 1610251
Analytical Environmental Services, Inc. received 1 samples on 10/5/2016.10:25:00 AM
for the analyses presented in following report.
No problems were encountered during the analyses. Additionally, all results for the associated
Quality Control samples were within EPA and/or AES established limits. Any discrepancies
associated with the analyses contained herein will be noted and submitted in the form of a
project Case Narrative.
AES's accreditations are as follows:
-NELAC/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid &
Chemical Materials; -and Drinking Water Microbiology, effective 07/01/16-06/30/17.
-NELAC/Louisiana Agency Interest No. 100818 for or analysis of Non -Potable Water'and Solid
& Chemical Materials, effective 07/01/16-06/30/17.
-NELAC/Texas Certificate No. T104704509-16-6 for or analysis of Non -Potable Water and
Solid & Chemical Materials, effective 03/01/16-02/28/17.
-AIHA-LAP, LLC Laboratory ID: 100671 for Industrial Hygiene samples (Organics, Metals,
PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and
Environmental Microbiology (Fungal) Direct Examination, effective until 09/01/17.
Tara Westervelt
Project Manager
SosoPYesid'enikial"]]rive -A#land+,:Eieaz�ia3i33s�U,•Tel:7'$Q:a 57.$ '11� ' l a '770i4i5'�181$8'' o��. �oe."$00.972:�k$$�
" •ti artiv.aesata®rita.canl •
1 of 6
Page 48 of 51

Analytical Environmental Services, Inc '
Date: - 6 -Oct -16
Client: Pace Analytical Services, Inc. Client Sample ID: 51)
Project Name: 923144764 Collection Date: 10/4/2016 2:00:00 PM
Lab ID: 1610251-001 Matrix: Aqueous
Analyses Result Reporting Qual Units BatchID MotionDate Analyzed Analyst
Limit Factor
Carbonyl Compoulnds.by .B[PLC' SW8315A
Formaldehyde 650 500 ng/L 230490 1 10/05/201616:55 RF
Qualifiers: 0 Value exceeds maximum ccntaminaat level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
3 of 6
H Estimated (value above quantitation range)
S Spike Recovery outside limits duo to matrix
Narr See case narrative
NC Not confirmed
< Less than Resultvalue
7 Estimated value detected below Reporting Limit
Page 49 of 51

m
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Analytical Environmental Services, Inc
Data: 10-0ct-16
Client: Pace Analytical Services, Inc.
Project Name: 92314764 Dates Report
Lab Order. 1610251
Lab Sample ID . Client Sample ID Collection Date Matrix Test Name TCLP Date Prep Date Analysis Date
1610251-001A 51) • . . • • • 1014/2016 2:00:OO17M Aqueous • Carbonyl Compounds by HPLC SW8315 10/5/2016 11:30:OOAM 10/05/2016
5of6

Analytical Environmental Services, Inc Date: 6 -Oct -16
Ctienf. ':Pace Analytical Services, Inc. ANALYTICAL QC SUM IARY REPORT
Project Name: 92314764
Workorde:: 1610251 BatchID: 230490
Sample ID: MB -230490
Client ID: ..
Units: ug/L
Prep Date: 10/0412016
Run No: 326762
SampleType: MBLK
TestCode: •. Carbonyl Compouttds by HPLC SW8315A
BatchID: 230490
Analysis Date: 10/05/2016
Seq No: 7081284
Analyte
Result RPT Limit SPK value SPK Ref Val
%REC - Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Formaldehyde
BRL 50
Sample ID: LCS-230490
Client ID:
Units: ug(L
Prep Date: • 10/04/2016
Run No: 326762
SampleType: LCS
TestCode: Carbonyl Compounds by HPLC SW8315A
BatchID: 230490
Analysis Date: 10/05/2016
Seq No: 7081285
Analyte
Result RPT Limit SPK value SPK Ref Val
o/aREC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Formaldehyde .
1123 50 1000
112 70 130
Sample ID: 1610172-001AMS
Client ID: _
Units: ug/L
Prep Date: 10/04/2016
Run No: 326762
SampleType: MS
TestCode: CarboaylCompotmdsbyHPLC SW8315A
BatchID: 230490
Analysis Date: 10/05/2016
Sell No: 7081708
Analyte
Result RPT Limit SPK value SPK Ref Val
• %REC Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Formaldehyde 1039 50 1000, 45.30 99.3 44.7 135
Sample ID: 1610172-OOIANISD
Client ID:
Units: ug/L
Prep Date: 10/04/2016
Run No: 326762
SampleType: MSD
TestCode: Carbonyl compounds by HPLC SW8315A
BatchID: 230490
Analysis Date: 10/05/2016
Sell No: 7081709
Analyte
Result RPT Limit • SPK value SPK Ref Val
%REC - Low Limit
High Limit RPD Ref Val %RPD
RPD Limit Qual
Formaldehyde 1290
Qualifiers- > Greater than Result value
BRL Belo -reporting limit
1 Estimated value detected below Reporting Limit
Rpt Lim Reporting Limit
6of6
50 1000 45.30 124 44.7 135 1039 21.6 27.3
< Less than Result value
E Estimated (value above quantitation range)
N Analyte notNELAC conified
S Spike Recovery outside limits due to matrix
B Analyte detected in the associated method blank
H Holding times for preparation or analysis exceeded
R RPD outside limits due to matrix