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HomeMy WebLinkAboutWQ0002560_Monitoring - 09-2024_20241009Monitoring Report Submittal Permit Number#* Name of Facility:* Month: * September Report Information Type * GW-59 WQ0002665 Jordan Lake SRA- Parkers Creek Year:* 2024 Upload Document* Parkers Creek MW Analysis Sept. 2024.pdf PDF Only 1.15MB Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * william.baker@ncparks.gov Name of Submitter: * William Baker III Signature: ,gker /// Date of submittal: 10/9/2024 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* WQ0002665 Is the monitoring report accepted?* Yes No Regional Office* Raleigh Reviewer: _anonymous Review Date: 10/28/2024 GW-59A COMPLIANCE REPORT FORM Permit #WQ. (LOZ&Z (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. ( C _ Will this monitoring report (GW,59 and GW-59A) YES NO be submitted after the established due date? ✓ 2 Was any required information missing on the GW-59 report forms? YES NQ- VV iF the answer to question 1 or 2 is 'YES", list in the space provided below the well identification number(s) and Pxntain the nrob/ems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes ", contact the Regional Office for guidance. >/ 4 I Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., /V N W W 2: i-U % 52o msl I log ms/� 5 1 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? / V If the answer to question 5 is NO", skip to section 8. If the answer to question 5 is "YES". list in the space provided below, each well with constituents) exceeding standards, concentratfon(s) reported, and sample collection date for each occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NQ If the answer is "YES". a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? i// if the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is havinq at the review and compliance boundaries surroundinq this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. 1 �t &Oe-- !YbR% TOf� ng g The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. i hereby acknowledge that the above information was evaluated and the information submitted in this report (Corn Hance Report GW.59Q) is true and complete to the best of my knowledge. o o 4 la Signature of Perm ittee (or Authorized Agent) Date GW-59A 12/8/2003 SUBMIT FORM ON YELLOW PAPER ONLY • • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0002665 Expiration Date: 1/1/2027 Facility Name: Jordan Lake State Recreational Area Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED Apex t8treen NC 27523 y ty Chatham Count ❑Lagoon ❑Remediation: Infiltration Gallery 'City; (state) (z,p) ® Spray Field ❑ Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Parkers Creek No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW #1 Date sample collected: 9/10/2024 FIELD ANALYSES: WAS Well Depth: 39.5 ft. Well Diameter: 3 in. pH 0040o: 7.82 units Temp. 000lo: eC DRY at Depth to Water Level 82546: ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: gallons Appearance here:❑ Samples for metals were collected unfiltered: El YES NO and field acidified: ❑ YES ® NO LABORATORY INFORMATION Date sample analyzed: 9/10/2024 Laboratory Name: Statesville Analytical Holdings LLC Certification No. #440 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 0o615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 000m µMhos K - Potassium 00937 mg/L VOC 7873 method # Total Ammonia 00610 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3asN; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only Total • _ • • I certify that to the best of my knowledge and belief. the information submitted in this report is true, accurate, and complete, and that the laboratory analytical data was produced using approved methods of analysis by a DWR-certified laboratory. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. William Baker III ORC/Authorized Agent . nt) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. •.Permittee (or Authorized • . -] SUBMIT FORM ON YELLOW PAPER ONLY ROUNDWATER QUALITY MONITORING: OMPLIANCE REPORT FORM Please Print Clearly or Type Name: Jordan Lake State Recreational Area Name (if different): Address: 280 State Parks Road ibtre 0 NC .City Contact Person: William Baker Well Location/Site Name: Parkers Creek (Siatel 27523 County Chatham (Zip) Telephone#: 919-362-0586 No. of wells to be sampled: 4 DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 :RMIT Number: W00002665 Expiration Date: 1/1/2027 �n-Discharge UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery 0 Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW #3 Date sample collected: 9/10/2024 FIELD ANALYSES: WAS Well Depth: 54.0 ft. Well Diameter: 2 in. pH 00400: 6.92 units Temp. 00010: °C DRY at Depth to Water Level 82546:18.4 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: check Volume of water pumped/bailed before sampling: 6.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: El YES IN NO and field acidified: El YES N NO Date sample analyzed: 9/10/2024 Laboratory Name: Statesville Analytical Holdings LLC Certification No. #440 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.45 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): ,issolved Solids:Total 703oo 526 mg/L Al -Aluminum of im mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 1.28 mg/L Ca - Calcium 00916 mg/L Chloride 00940 66.9 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method M ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? A Yes (1) ❑ No (0) specific Conductance 000m µMhos K - Potassium 00937 mg/L VOC 7873 method # 8260 Total Ammonia oo6lo <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% William Raker III 0RC/Authnri7PrH 1 Anent Signature of tuatet GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0002665 Expiration Date: 1/1/2027 Facility Name: Jordan Lake State Recreational Area Non -Discharge UIC Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED El Lagoon ❑Remediation: Infiltration Gallery Apex 11feet1 NC 27523 County Chatham ,City) (:hate) (Zip) A Spray Field ❑Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Parkers Creek No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW #4 Date sample collected: 9/10/2024 FIELD ANALYSES: WAS Well Depth: 51.5 ft. Well Diameter: 2 in. pH 00400: 7.40 units Temp. 00010: °C DRY at Depth to Water Level 82546:17.3 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. 00094: µMhos time of sampling, Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. Odor 00085: check Volume of water pumped/bailed before sampling: 6.0 gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑ YES Al NO and field acidified: ❑ YES A NO LABORATORY INFORMATION Date sample analyzed: 9/10/2024 Laboratory Name: Statesville Analytical Holdings LLC Certification No. #440 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NOZ) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.45 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): Dissolved Solids:Total 7030o 390 mg/L Al - Aluminum o11o5 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOC 00680 <1.0 mg/L Ca - Calcium 00916 mg/L Chloride 0094o 46.9 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method A ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? 01 Yes (1) ❑ No (0) Specific Conductance 000m µMhos K - Potassium 00937 mg/L VOC 7873 method # 8260 Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH. as N; Ammonia Nitrogen, Total) Mn - Manganese oiom ug/L method # TKN as N 00626 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 SUBMIT FORM ON YELLOW PAPER ONLY • DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: WQ0002665 Expiration Date: 1/1/2027 Facility Name: Jordan Lake State Recreational Area Non -Discharge _ UIC Permit Name (if different): NPDES Other Facility Address: 280 State Parks Road TYPE OF PERMITTED OPERATION BEING MONITORED g Gallery ❑ Lagoon ❑Remediation: Infiltration Apex 'Stfeet, NC 27523 County Chatham 'City( (State) (zip A7 Spray Field ❑ Remediation: Contact Person: William Baker Telephone#: 919-362-0586 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Parkers Creek No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: tfrom Permit! SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW #5 Date sample collected: 9/10/2024 FIELD ANALYSES: WAS Well Depth: 51.5 ft. Well Diameter: 2 in. pH 00400: 6.87 units Temp. 00010: °C DRY at Depth to Water Level 82546: 35.2 ft. below measuring point Screened Interval: ft. to _ft. Spec. Cond. 00094: µMhos time ofsampling, Measuring Point is 4.0 ft. above land surface Relative M.P. Elevation: ft. Odor 000m: check Volume of water pumped/bailed before sampling: 3 gallons Appearance here: El Samples for metals were collected unfiltered: ElYES [FBI NO and field acidified: ❑ YES 141 NO LABORATORY INFORMATION Date sample analyzed: 9/10/2024 Laboratory Name: Statesville Analytical Holdings LLC Certification No. #440 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 mg/L Pb - Lead o1o51 ug/L Coliform: MF Fecal 31616 <1 /100mL Nitrate (NO3) as N 00620 <0.1 mg/L Zn - Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 0.3 mg/L (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): 7issolved Solids:Total 703oo 708 mg/L Al - Aluminum 01105 mg/L pH (Lab) 00403 units Ba - Barium 01007 ug/L TOG 00680 1.59 mg/L Ca - Calcium 00916 mg/L Chloride oo94o 160 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ICI Yes (1) ❑ No (0) pecific Conductance 00095 µMhos K - Potassium 00937 mg/L VOC 7873 method # 8260 Total Ammonia 00610 <0.1 mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total) Mn - Manganese o1o55 ug/L , method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% GW-59 Rev.06-07-2018 Analytical Results Parkers Creek- Jordan Lake Rec Area Budget Office 1615 Mail Service Center Raleigh, NC 27699 Receive Date: 09/10/2024 Reported: 09/26/2024 For: Monitoring Wells Comments: Depth to H2O 1# N/A 3# 18'4" 4# 17'3" 5# 35'2" i TATESVILLE ANALYTICAL Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 240910-14-01 pH MW#1 7.82 Std. Units SM4500H+B-2021 09/10/2024 RR 240910-14-02 8260 Volatile MW#3 See Attached 8260 09/18/2024 MT 240910-14-02 Ammonia Nitrogen MW#3 <0.1 mg/L SM4500NH3C-2021 09/18/2024 LM 240910-14-02 Chloride MW#3 66.9 mg/L SM4500CIC-2021 09/11/2024 MD 240910-14-02 Fecal Coliforms MW#3 <1 CFU100 MIL SM9222D-2015 09/10/2024 MD 240910-14-02 Nitrate MW#3 <0.1 mg/L (NO3+ M450 09/16/2024 CL 019) SM4500-NO3-F2019 240910-14-02 pH MW#3 6.92 Std. Units SM4500H+B.2021 09/10/2024 RR 240910-14-02 T. Phosphorous MW#3 0.45 mg/L SM4500PE-2021 09/16/2024 CL 240910-14-02 TOC MW#3 1.28 mg/L SM5310B 09/18/2024 MT 240910-14-02 Total Dissolved MW#3 526 mg/L SM2540C-2020 09/11/2024 MD Solids 240910-14-03 8260 Volatile MW#4 See Attached 6260 09/18/2024 MT 240910-14-03 Ammonia Nitrogen MW#4 <0.1 mg/L SM45DONH3C-2021 09/18/2024 LM 240910-14-03 Chloride MW#4 46.9 mg/L SM4500CIC-2021 09/11/2024 MD 240910-14-03 Fecal Coliforms MW#4 <1 CFU100 MIL SM9222 D-2015 09/10/2024 MD 240910-14-03 Nitrate MW#4 <0.1 mg/L 03-IN0 2 SM45 09/16/2024 C N NO200- 2 SM4500-NO3-F2019 240910-14-03 pH MW#4 7.40 Std. Units SM4500H+B-2021 09/10/2024 RR 240910-14-03 T. Phosphorous MW#4 0.45 mg/L SM4500FE-2021 09/16/2024 CL 240910-14-03 TOC MW#4 <1.0 mg/L SM531OB 09/18/2024 MT 240910-14-03 Total Dissolved MW#4 390 mg/L SM2540C-2020 09/11/2024 MD Solids 240910-14-04 Chloride MW#5 160 mg/L SM4500CIC-2021 09/11/2024 MD 240910-14-04 Fecal Coliforms MW#5 <1 CFU100 MIL SM9222D-2015 09/10/2024 MD 240910-14-04 TOC MW#5 1.59 mg/L SM5310B 09/18/2024 MT PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 11 Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 240910-14-04 8260 Volatile MW#5 See Attached 8260 09/18/2024 MT 240910-14-04 Ammonia Nitrogen MW#5 <0.1 mg/L SM4500NH3C.2021 09/18/2024 LM 240910-14-04 Nitrate MW#5 <0.1 mg/L (N 450 09/16/2024 CL F+NO2 SM4500-NO3-F2019 240910-14-04 pH MW#5 6.87 Std. Units SM4500H+B-2021 09/10/2024 RR 240910-14-04 T. Phosphorous MW#5 0.3 mg/L SM450OPE-2021 09/16/2024 CL 240910-14-04 Total Dissolved MW#5 708 mg/L SM2540C-2020 09/11/2024 MD Solids Respectfully submitted, 1 Melissa Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 11 Condition of Receipt Sample Number 240910-14-01 Temp on Arrival: 1.5 Parameter Schedule: pH Received on Ice Sample Number 240910-14-02 Temp on Arrival: 1.5 Parameter Schedule: Total Dissolved Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Parameter Schedule: pH Received on Ice pH on Arrival: <2 Parameter Schedule: Hydrochloric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Nitrate Received on Ice Parameter Schedule: Chloride Received on Ice pH on Arrival: <2 Parameter Schedule: TOC Phosphoric Acid Received on Ice Chemicals in containers, lab Sample Number 240910-14-03 Temp on Arrival: 1.5 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 11 pH on Arrival: <2 Parameter Schedule: Total Dissolved Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Chemicals in containers, lab Parameter Schedule: pH Received on Ice Parameter Schedule: Hydrochloric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Chloride Received on Ice Parameter Schedule: Nitrate Received on Ice pH on Arrival: <2 Parameter Schedule: TOC Phosphoric Acid Received on Ice Chemicals in containers, lab Sample Number 240910-14-04 Temp on Arrival: 1.5 Parameter Schedule: Total Dissolved Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Parameter Schedule: pH Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 4 of 11 pH on Arrival: <2 Parameter Schedule: Hydrochloric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: Ammonia Nitrogen Sulfuric Acid Received on Ice Chemicals in containers, lab pH on Arrival: <2 Parameter Schedule: T. Phosphorous Sulfuric Acid Received on Ice Chemicals in containers, lab Parameter Schedule: Chloride Received on Ice Parameter Schedule: Nitrate Received on Ice pH on Arrival: <2 Parameter Schedule: TOC Phosphoric Acid Received on Ice Chemicals in containers, lab PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 5 of 11 t. q4 � _ --i--�---•- EI � I e Q Q lcz� n E n 3 a E $ O W n r 0) S o. E m E � F`- S U N_ _ P v y v v 5 o 0 o 0 Ea a a Q, E m m CD E E E E F- p i r N G LO I_ z I U IY f0 E o t�" °w,M'Qa'po+ 0 A#1 i n k ii I D m O tj E E E E a a a at l E EIn I I N � N N 0 � C v C m v E E E o E E PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 6 of 11 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: C. Little Report Date: 9/23/2024 Client: Statesville Analytical 122 Court St Project: Parkers Creek Statesville, NC 28677 Date Sample Rcvd: 9/11/2024 Meritech Work Order # 091124131 Parameters results Sample: 250910-14-02 Grab Analysis Date Reporting Limit 9/10/24 TOC 1.28 mg/L 9/18/24 1.00 mg/L Metho SM 5310C 8260 Attached 9/18/24 - 8260 Meritech Work Order # 091124132 Parameters Results Sample: 250910-14-03 Grab Analysis Date Reporting Limit 9/10/24 TOC <1.00 mg/L 9/18/24 1.00 mg/L Method SM 5310C 8260 Attached 9/18/24 - 8260 Meritech Work Order # 091124133 Parameters Results Sample: 250910-14-04 Grab Analysis Date Reporting Limit 9/10/24 Method TOC 1.59 mg/L 9/18/24 1.00 mg/L SM 5310C 8260 Attached 9/18/24 - 8260 1 hereby certify that 1 have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 www.meritechiabs.com PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 7 of 11 >MER1 CH. INC. Environmental Laboratories Laboratory Certification #165 Client: Statesville Analytical Holdings LLC Meritech lD#: 091124131 Project: Parkers Creek Analysis: 09/18/24 Client Sample 1D- 250910-14.02 Analyst: KD Sample Collection: 09/10/24 Dilution Fac(or: 10 Report Date: 09/19/24 SW-846-8260D VOLATILE ORGANICS - Water Acetone 50.0 ug/l, cis- i,3-Dichloropropene 5.00 ug/L Benzene t 5.00 ug/l trans-1,3-Dichloropropene 5,00 ug/L Bromobenzene < 5.00 ug/L Ethanol 500 ug/L Bromodichloromethane < 5.00 ug/l- Ethyl benzene 5.00 ug/l. Bromochloromethane < 5.00 ug11. Hex achlorobutadiene 5.00 ugll. Bromoform - 5.00 ugtl 2-Hexanone 10.0 ug/l. Bromomeihane < 5.00 ug/l.- lsopropylbenzene 5.00 ug/L 2-Butanone i MEK► t 50.0 ug/l, p-isopropyltoluene 5.00 ug/l. n-Butylbenzene < 5.00 ug/l_ Methylene chloride 5.00 ug/L see- ButyIbenzene < 5.00 ug/L Methly Isobulyl Ketone (M1BK) • 5.00 ug/l. tert-Butylbenzene < 5.00 ug/1. Naphthalene 5.00 ug/L Carbon Tetrachloride < 5.00 ug/1. n-Propylbenzene 5.00 ug/l, Chlorobenzene < 5.00 ug/1_ Styrene 5.00 ug/1. C'hlorocthane <: 5.00 ug/L 1.1.1,2-Tetrachloroethane 5.00 ug/1_ Chloroform -5.00 ugll- 1,1.2.2-Torachloroelhane 5,00 ug/L Chloromethanc t 5.00 ugit_ Tetrachloroethene WCE) 5.00 ug/l. 2-Chlorotoluene < 5.00 ug/1 Toluene •. 5.00 ug/L 4-Chlorotoluene < 5.00 ug/1 1,1,1-1'richloroethane 5.00 ug/L Dibromochloromethane 5.00 ug/1. 1,1,2-Trichloroethane 5.00 ugil 1?-t)ihromn-3-chloropropane < 5.00 ug/L fichloroethene (TCF) 5.00 ug/L 1,2-Dibromoethane(FDB) <5.00 ug/l. 1,2,3-1'richlorobenzene • 5.00 ug/l Dibromomethane < 5.00 uglL 1,2,4-Trichlorobenzene 5.00 ug/l, Dichlomdifluoromethane 5.00 ug/l. 1,2,3-Trichloropropane 5.00 ug/I. 1.1-Dichloroethenc S.Ou ug/l. 'I'richlorotluoromethane 5.00 ug/l. 1,2-Dichloroethene 5.00 ug/L 1,2,4-Trintethylbenzene 5.00 ug/L 1,4•Dichlorobenzene 5.00 ug/L 13.5-1rimethylbenzene 5.00 ug/L 1,2-Dichlorobenzene < 5.00 ug/1. Vinyl acetate 10,0 ug/L. 1.3-Dichlorobcnzene - 5.00 ug/l, Vinyl chloride 5.00 ug/l, 1,1-Dichloroethene -.5.00 ug/l, m/p-Xylenes 10.0 ug/L cis-1.2-Dichloroethenc 5.00 ug/L o-Xylene 5.00 ug/l. trans-I.2-Dichloroethene 5.00 ug/L 1,2-Dichloropropane 5.00 ug/L Additional Comuounds 1,3-Dichloropropane 5.00 ug/L Me(byl-tert-butyl ether IMTBE) 5.00 uglL 2,2-Dichloropropane 5.00 LIS/L Isopropyl ether(IPEi) • 5.00 11811 1.1-Dichloropropene 5.00 ug/1. 1,2-I)ichloropropene <5.00 ug/L / I hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road ' Reidsville, NC 27320 (336) 342-4748 Ph " info@meritechlabs.com PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 8 of 11 .M. ERI TE. C.H. INC. Environmental Laboratories Laboratory Certification #165 Client: Statesville Analytical Holdings LLC Meritech IDN: 091 124132 Project: Parkers Creek Analysis: 09/18/24 Client Sample ID: 250910-14-03 Analyst: KD Sample Collection: 09/10/24 Dilution Factor: 10 Report Date: 09/19/24 SW-846-8260D VOLATILE ORGANICS -Water Acetone < 50.0 ug/L cis-1,3-Dichloropropane < 5.00 ug/L Benzene <5.00 ug/L trans-1,3-Dichloropropene <5.00 ug/L Bromobenzene < 5.00 ugfL Ethanol < 500 ug/L Bromodichloromethane < 5.00 ttg/L Ethyl benzene < 5.00 ug/L Bromochloromethane 5.00 ug/l. Hexachlorobutadiene < 5.00 ug/L Bromoform 5.00 ug/L 2-Hexanone < 10.0 ug/1_ Bromomethane 5,00 ug/L Isopropylbenzene < 5.00 U&II, 2-Butanone (MEK) 50.0 ug/L p-Isopropyltoluene < 5.00 ug/1_ n-Butylbenzene 5.00 ug/L Methylene chloride < 5.00 ug/L sec-Butylbenzene 5.00 ug/l. Methly Isobutyl Ketone (MIBK) < 5.00 ug/1_ tert-Butylbenzene 5.00 ug/I. Naphthalene < 5,00 ug/L Carbon Tetrachloride 5.00 ug/L n-Propylbenzene -5.00 ug/L Chlorobenzene < 5.00 ug/L Styrene < 5.00 ug/L Chloroethane 5.00 ug/l. 1, 1. 1,2-Tetrachloroethane < 5.00 ug/L Chloroform 5.00 ug/l. 1, 1 .2,2-Tetrachloroethane < 5.00 ug/L C'hloromethane 5.00 ug/L Tetrachloroethene (PCE) < 5.00 ug/L 2-Chlorotoluene 5.00 ug/L Toluene < 5.00 ug/L 4-Chlorotoluene 5.00 ug/l. I,I,1-Trichloroethane < 5.00 ug/l. Dibromochloromethane 5.00 ug/L 1,1,2-Trichloroethane < 5.00 ug/L 1,2-Dibromo-3-chloropropane 5.00 ug/L Trichloroethene (TCE) < 5.00 ug/L 1,2-Dibromoethane(EDB) 5.00 ug/L 1,2,3-Trichlorobenzene <5.00 ug/L Dibromomethane 5.00 ug/L 1,2,4-Trichlorobenzene < 5.00 ug/L Dichlorodifluoromethane 5.00 ug/L 1,2,3-1'richloropropane <5.00 ug/l'. l,l-Dichloroethane <5.00 ug/l, rrichlorofluoromethane <5.00 ug/L 1,2-Dichloroethane 5.00 ug/L 1,2,4-Trimethylbenzene < 5.00 ug/1. I A-Dichlorobenzene 5.00 ug/L 1,3,5-1 rimethylbenzene < 5.00 ug/L 1,2-Dichlorobenzene 5.00 ug/L Vinyl acetate < 10.0 ug/L 1,3-Dichlorobenzene 5.00 ug/l. Vinyl chloride < 5.00 ug/L I,1-Dichloroethene 5.00 ug/L m/p-Xylenes < 10.0 ug/l. cis-1,2-Dichloroethene 5.00 ug/L o-Xylene < 5.00 ug/L trans- l,2- Diehl oroethene 5.00 ug/L 1.2-Dichloropropane 5.00 ug/L Additional Comuounds 1,3-Dichloropropane 5.00 ug/L Methyl-tert-butyl ether(MTBE) <5.00 ug/I- 2,2-Dichloropropane 5.00 ug/L Isopropyl ether (IPE) < 5.00 ug/L I,I-Dichloropropene 5.00 ug/L 1,2-Dichloropropene < 5.00 ug/L 1 hereby certify that I have reviewed and approve these data. Laboratory Representative 642 Tamco Road * Reidsville, NC 27320 (336) 342-4748 Ph * info@meritechlabs.com PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 9 of 11 MERITEC14 INC Environmental Laboratories ,... Laboratory Certification #165 Client: Statesville Analytical Holdings LLC Meritech ID#: 091 124133 Project: Parkers Creek Analysis: 09/18/24 Client Sample ID: 250910-14-04 Analyst: KD Sample Collection: 09/10/24 Dilution Factor: 10 Report Date: 091I1)/24 SW-846-8260D VOLATILE ORGANICS - Water Acetone " 50.0 ug/I. cis-1.3-Dichloropropene 5.00 ug/l. Benzene 5.00 ug/L trans-1,3-Dichloropropene 5.00 ug/l. Bromobenzene C 5.00 ug/L Ethanol 500 ug/l. Bromodichloromcthane 5.00 ug/l, Fthvl benzene 5.00 ugIL Bromochloromethane 5.00 ug/I lfexachlorobutadiene 5.00 ug/L Bromuform -5.00 ug/L 2-HCXanone 10.0 ug/L Bromomethane 5.00 ug/l. Isopropylbenzene 5.00 ug/L 2-13utanone(MEK) 50.0ug/1_ p-lsopropylioluene <5.00ug/l, n-Butylbenzene -5.00 ug/I. Methylene chloride < 5.00 u 1_ sec-Butylbenzene 5.00 ug/1_ Methly lsobutyl Ketone (MIBK) < 5.00 ugtl. tert-Butylbenzene 5.00 ug/l. Naphthalene 5.00 ugrL Carbon Tetrachloride 5.00 ug/L n-Propylbenzene 5.00 ug/l. L hlorobenzene 5.00 ug/L Styrene < 5.00 ugrl. Chlorocthane 5.00 ug/I. 1,1,1,2-Tetrachloroethane < 5.00 ug/L Chlorolonn 5.00 ug/l_ 1,1.2.2-Teirachloroethane 5.00 ugrL C'hluromethane 5.00 ug/L TetrachloroelheneiPCE) 5.00 ug/l. 2-C•hlorotoluene 5.00 ug/L Toluene 5.00 ug/l. 4-C'hlormoluene 5.00 ug/L I.1.1-Trichloroethane 5.00 ug/L DibromochIoromethan(. 5.00 ug/L 1,1,2-TrichIoroethane 5.00 ug/l. 1.2-Dibromo-3-chloropropane 5.00 ug/L Trichluroethene MT) 5.00 ug/l. 1.2-Dibromoethane(ED13) 5.00 ug/l. 1,2,3-1richlorobenzene - 5.00 ug/L Dibromomethane 5.00 ug/l, 1,2,4-1'richlorobenzene 5.00 ug/L Dichlorodifluoromethane 5.00 ug/l. 1,2,3-I'richloropropane 5.00 ug/l, I.I-Dichloroethene 5.00 ug/1_ Trichlornfluoromethane 5.00 ug/L 1,2-Dichlomethane 500 uyll_ 1,2,4-Trimethylbenzene 5 00 ug/l, 1,4-Dichloroben4ene 5.00 ug/l. 1,3,5-TrimethyIbenzene 5.00 ug/l, 1,2-Dichloroben7enc 5.00 ug/L Vinyl acetate 10.0 ug/l. 1,3-Diehlorobenzene 5.00 uu/1_ Vinyl chloride 5.00 ug/l_ 1,1-Dichloroethene 5.00 ugil, m/p-Xy►enes 10.0 ug,'L cis-1.2-Dichloroethene 5.00 ug/l, o-Xylene 5.00 ug/L trans-1,2-Dichloroethene 5.00 ug/L 1.2-Dichloropropane 5.00 ug/L Additional Compounds 1,3-Dichloropropane 5.00 ug/1_ Methyl -tent -butyl ether (MTBE) 5.00 ugil_ 2.2-Dichloropropane 5.00 ug/l, Isopropyl ether (IPE) 5.00 ug/l. I.1-Dichloropropene 5.00 u1:/1_ I,_2-Dichloropropane 5.00 ug/L I hereby certify that I have reviewed and approve these data. 111111 abbbbbnuratary Representative 642 Tamco Road'' Reidsville, NC 27320 (336) 342.4748 Ph' info@meritechiabs.com PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 10 of 11 L L do L L abed L69b/ZL8/bOL • L898Z ON 'a!!!nsajejS • 8ZZ XO8 Od r N 0 c r W m Gl a( F = -� E a �; F3 L � y � L �) sis� Q n. dLL o 2 O d Z w J 7i. bt O EA C 4-J T a 11 LLA O •C y T - 'o 19 � ` U U! C t� H U Z E v N ,1 _ +�•. r � 13 T W e o F- a C �-Ulf oM 0 o �:�.0 ui � u m a O y Q w � U R • Z i. Z. = E I geq w o •� W t� `Ofu C C f O � � E 2Im E � ro A ti 3 i O o a _ 4.1 C L cn ,°