WQ0005555_Monitoring - 07-2024_20240828

Monitoring Report Submittal
...................................................
Permit Number#* WQ0005555
Name of Facility:* Weyerhaeuser Company
Month: * July Year: * 2024
Report Information
Type* Upload Document*
NDMR, NDAR-1, NDAR-2, NDMLR Signed Jul 2024 NDAR & NDMR Rev 1.pdf 2.87MB
PDF Only
GW-59 Signed July 2024 GW-59 rev1.pdf 8.39MB
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * [e-mail]
Name of Submitter: * Dennis R Atkinson
Signature:
a�i� rr«t ��t. �:►�Jow
Date of submittal: 8/28/2024
This will be filled in automatically
Initial Review

Reviewer: Wanda.Gerald
Is the project number correct?* WQ0005555
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 9/20/2024

FORM NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-11 Page 1 of
Permit No.: W00005555
Facility Name: Weyerhaeuser - Elkin. NC
County: Surry
Month: July
Year: 2024
Did irrigation occur
Field Name:
01
Field Name:
02
Field Name:
03
Field Name:
04
Area (acres):
2.17
Area (acres):
2 17
Area (acres):
2.17
Area (acres):
2.17
at this facility?
Cover Crop:Ha
Y
Cover Crop:
P�
Ha Y
Cover Crop:
P�
Ha Y
Cover Crop:
P�
Ha Y
YI � lU
Hourly Rate (in):
0.25
Hourly Rate (in):
0 25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Weather
Freeboard
Field Irrigated?
YES El NO
Field Irrigated?
` YI S _ : NO
Field Irrigated?
❑ YES 171 NO
Field Irrigated?
❑ YES L NO
T
v
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.
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aaE
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rn
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aa
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= JE
°F
in
ft
ft
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
in
1
0
2 443
2
C
0
2.428
3
0
2.434
4
0
2.454
5
C
98
0.15
2A62
6,912
30
0.12
0.12
6
1.22
2.442
7
0
2-578
8
003
2 685
9
0
2.705
10
0
2.709
11
0
2.732
12
0
2.863
13
0
2.876
14
C
101
0
2.992
6,802
30
0.12
0.12
151
1
0
11255
16
0
3.266
17
0
3.277
18
0.2
3.197
19
C
79
0
3.215
6.794
30
0.12
0.12
20
0.87
2.851
21
0.57
2.775
22
1.8
2 486
23
PC
85
0.1
249
11,280
60
0.19
0.19
5.640
60
0.10
0-10
24
0,16
2.747
25
1 0.34
12,742
26
0.1
2.756
27
PC
85
0.29
2.77
28
C
87
0
2 781
11.168
60
0.19
0.19
5,584
60
0.09
0 09
29
0.06
3.183
30
0.66
3.164
311
1 0.32
13167
Monthly Loading:�42.956
" ""'�'
0.73:"a
1 1 224
0 19
0
0 00
>`t�_ ;
0
000
12 Month Floating Total (in):
�,^e
-...
18.14
" ,->'
i247
.74
19 76
!.Ihd

FORM: NDAR-1 08-11 NON-DISCHARGF APPI ICATInN RFPnRT INDAR-11 Page 2 of 4
Permit No.: W00005555
Facility Name: Weyerhaeuser - Elkin, NC
County: Slurry
Month: July
Year: 2024
Did irrigation
Field Name:
05
Field Name:
06
Field Name:
07
Field Name:
08
occur
Area (acres):
2,29
Area (acres):
13
Area (acres):
2,01
Area (acres):
2 08
at this facility?
Cover Crop:
Hay
Cover Crop:
Hay
Cover Crop:
Hay
Cover Crop:
Hay
vE ,,
Hourly Rate (in):
0.25
Hourly Rate (in):
0,25
Hourly Rate (in):
0.25
Hourly Rate (in):
025
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Annual Rate (in):
20
Weather
Freeboard
Field Irrigated?
n YES f 1 NO
Field Irrigated?
❑ YES �l NO
Field Irrigated?
El YES ❑ NO
Field Irrigated?
] YES i l NO
o
2'
r
a
,t, '
E
a
�x
°
J=J
E
°
p
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Q
_
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=J
Ed
% Q
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=
EE
px°fl
J
Ern
7
T p
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=oCo > J
°F
in
ft
ft
gal I
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
in
1
0
2,443
2
0
2.428
3
0
2,434
4
0
2-454
5
C
98
0 15
2 462
6
C
99
1.22
2,442
8.652
30
0.14
1 0.14
7
C
89
0
2.578
1
1
6.640
30
0.12
0.12
8
0.03
2.685
9
0
2,705
10
0
2.709
11
C
88
0
2.732
6,957
30
1 0.13
0.13
121
0
2,863
13
C
94
0
2.876
6,104
30
0.11
0.11
14
C
100
0
2.992
8.489
30
0.14
0.14
15
0
3 255
16
1
0
13.266
17
0
3.277
18
02
3 197
19
C
81
0
3.215
8,720
30
0.14
0.14 1
6,900
30
0.13
0.13
20
0.87
2-851
21
0.57
2,775
22
1 8
12486
23
0.1
249
24
0.16
2 747
25
0,34
2 742
26
PC
85
0.1
2,756
6,884
30
0.13
0.13
27
0,29
2,77
28
C
84
0
2 781
8,641
30
0.14
0.14
29
006
13183
30
0.66
3,164
31
0 32
13 167
Monthly Loading:
34,502
=', .3_.
0.55
0.00
g
33,485
061
0
'�E."
000
12 Month Floating Total (in)
.
�
14.78
12.83
1.04
6.81

FORM. NDAR-1 08-11 NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page 3 of 4
Permit No.: WQ0005555
Facility Name: Weyerhaeuser - Elkin, NC
County: Surry
Month: July
Year: 2024
Did irrigation
Field Name:
A
Field Name:
D
Field Name:
CN
Field Name:
CS
occur
Area (acres):
2.8
Area (acres):
2 56
Area (acres):
1.96
Area (acres):
1,24
at this facility?
Cover Crop:Ha
Y
Cover Crop:
P
Ha Y
Cover Crop:
P�
Ha Y
Cover Crop:
P�
Ha Y
Yi ; No
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Hourly Rate (in):
0.25
Annual Rate (in):
31.8
Annual Rate (in):
31.8
Annual Rate (in):
31.8
Annual Rate (in):
31.8
Weather
Freeboard
Field Irrigated?
'__ YES ] NO
Field Irrigated?
❑ YES a rdo
Field Irrigated?
= YES _- NO
Field Irrigated?
LI YES OO NO
>,
o
p
vN
a�
d
to
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H
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av
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=
J
°F
in
ft
ft
gal
min
in
in
gal
min
in
in
gal
min
in
in
gal
min
in
in
1
0
2.443
2
0
2.428
3
0
2 434
4
0
2A54
5
0.15
2.462
6
1.22
2 442
7
0
2.578
8
0.03
2.685
9
0
2.705
10
0
2.709
11
0
2.732
12
0
2.863
13
0
2.876
14
0
2.992
15
0
3.255
16
0
3.266
17
0
3.277
18
0.2
3,197
19
0
3,215
20
0.87
2.851
21
0.57
2.775
22
18
2-486
23
0.1
2.49
24
0.16
2 747
25
034
2,742
261
0 1
12.756
27
0,29
2.77
28
0
2 781
29
0.06
3 183
30
0.66
3 164
31
032
3 167
Monthly Loading:
0
0.00
0
000
sr;i-;4;
0
°; :
0,00
0
0 00
12 Month Floating Total (in):
2.01
_fi„m:
043
C G'
E=` ,'`�:
¢`G .,i`
1.39
11

FORM: NDAR-1 08-11
NON -DISCHARGE APPLICATION REPORT (NDAR-1)
Page 4 of 4
Did the application rates exceed the limits in Attachment B of your permit?
Were adequate measures taken to prevent effluent ponding in or runoff from the sites?
Was a suitable vegetative cover maintained on all sites as specified in your permit?
Were all setbacks listed in your permit maintained for every application to each permitted site?
Were all freeboards maintained in accordance with the specified freeboard heights in your permit?
0 Compliant ❑ Non -Compliant
El Compliant ❑ Non -Compliant
El Compliant ❑ Non -Compliant
I] Compliant ❑ Non -Compliant
Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification
Permittee Certification
ORC: Dennis R. Atkinson
Permittee:
Weyerhaeuser Company
Certification No.: 15574
Signing Official: Steve Kobelak
Grade: SI Phone Number: 336-526-6437
Signing Officials Title: Mill Manager
Has the ORC changed since the previous NDAR-17 ❑ Yes O No
Phone Number: 336-5 Permit Exp.: 8/31/25
..✓
—-�
Signature Date
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance
with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the
information submitted is, to the best of my knowledge and belief, true, accurate, and complete. 1 am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations.
Mail Original and Two Copies to:
Division of Water Quality
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _1_ of _3_
Permit No.: WQ0005555
Facility Name: Weyerhaeuser - Elkin OSB Mill WWTF
County: Surry
Month: July
Year: 2024
PPI: 001
Flow Measuring Point: Influent ❑ Effluent ❑ No Flow generated
Parameter Monitoring Point: ❑ Influent P Effluent E]Groundwater Lowering El surface water
Parameter Code --►
50050
00310
00916
00680
00940
01034
31616
71880
00927
71900
00610
00625
00620
00600
00340
00400
o
O
c
O
E
IU c
rn°
E
4`tiaa3 .
_
_m
LL
I
gO
P
oE
vfdc
_ mcrn
•E z
0
z
~ 'zPcrn
O>, G
U
a
24-hr
hrs
GPD
mglL
mglL .
mg1L
mg/L
mg/L
#1100 mL
mglL
mglL
mglL
mglL
mglL
mglL
mglL
mg1L
su
1
08:00
4
0
7.02
2
08:00
8
5,085
3
08:00
6
7,611
4
08:00
8
5
08:00
4
0,
6
TWO,-
7
03,
8
08.00
4
0 '
6.93
9
p>
10
11
08:00
8
- '0
12
08:00
4
6,352.
13
0
14
0 .
15
08:00
4
.0
6.98
16
08:00
8
0
17
08:00
6
20,144
18
08:00
8
0
19
08:00
4
0
20
0
21
0
221
08:00
4
0
6.88
23
08:00
8
0
24
08:00
6
1,555,
310
26.5
684
130
<0.120
11.0
5.03
25.7
<0.000800
1.06
41.1
<5.00
41.1
2550
6.82
25
08:00
8
0
26
08:00
4
0
27
0.
28
0
29
08:00
4
0
7.23
30
08:00
8
0...
31
08:00
6
8,186
Average:
.1',902
310.00
26.5.0
684.00
130.00
0.00
110,00
5.03
25.70
0.00
1.06
41.10
0.00
41.10
2,550,00
Daily Maximum:
20,144
310.00
26.50;
684.00
130.0.Q
0.12
110100
5.03
25.70.
0.00
1.06
41.10
5,00
41.10
2,550:00`
7.23
Daily Minimum:
Q .,. .
310.00
2&50
684.00
130;00
0.12
110,00
5.03
25:70.
0.00
1.06
41.10
.5,00
41.10
2,550.00
6.82
Sampling Type:
Recorder
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab
Grab.
Grab
Monthly Limit:
Daily Limit:
28;800
Sample Frequency:
Continuous
3 X Year
32X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
3 X Year
Per Event

FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _2_ of _3_
Permit No.: WQ0005555
Facility Name: Weyerhaeuser - Elkin OSB Mill WWTF
County.- Surry
11
'. ■ ■1;FTFTRMrFr16reTiIN
. •. ■ 0 ■ ■
•
•
i
nor,",
1
®-®------�---

FORM: NDMR 05-16 NON -DISCHARGE MONITORING REPORT (NDMR) Page _3_ of _3_
Sampling Person(s) 11 Certified Laboratories
Name:
David Morris
Name:
WayPoint Anaylical - Cert. No. 402
Name:
Brody Edwards
Name:
PACE - Cert No. 40 & 633
Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑� Compliant ❑ Non -Compliant
If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective
action(s) taken. Attach additional sheets if necessary.
Operator in Responsible Charge (ORC) Certification 11 Permittee Certification
ORC: Dennis R. Atkinson
Certification No.: 15574
Grade: Si Phone Number:
Has the ORC changed since the previous NDMR?
Permittee: Weyerhaeuser Co.
Signing official: Steve Kobelak
336-526-6437 Signing Official's Title: Mill Manger
❑ yes 0 No Phone Number: 336-526-6456 Permit Expiration: 8/31 /2025
Signature Date
By this signature, I certify that this report is accurrate and complete to the best of my knowledge.
Signature Date
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information
submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for
gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
Mail Original and Two Copies to:
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, North Carolina 27699-1617

Waypoint
ANALYTICAL
8/7/2024
Weyerhaeuser Corporation
Dennis Atkinson
524 Pride Way
Elkin, NC, 28621
Ref: Analytical Testing
Lab Report Number: 24-206-0010
Client Project Description: EFF Wastewater
Dear Dennis Atkinson:
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/24/2024 for the analyses presented in the
following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136
Method Update Rule May 2021) unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Terri W Cole
Laboratory Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 16

Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytica I.tom
Certification Summary
Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC
State
Program
Lab ID
Expiration Date
North Carolina
State Program
37735
07/31/2025
North Carolina
State Program
402
12/31/2024
South Carolina
State Program
99012
07/31/2024
South Carolina
State Program
99012
12/31/2024
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2025
Arkansas
State Program
88-0650
02/07/2025
California
State Program
2904
06/30/2024
Florida
State Program - NELAP
E871157
06/30/2025
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2025
Kentucky
State Program
90047
12/31/2024
Kentucky
State Program
80215
06/30/2025
Kentucky
State Program
KY90047
12/31/2024
Louisiana
State Program
- NELAP
LA037
12/31/2024
Louisiana
State Program
- NELAP
04015
06/30/2025
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2025
North Carolina
State Program
415
12/31/2024
Pennsylvania
State Program
- NELAP
68-03195
05/31/2025
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2025
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00016/24-206-0010
Page 2 of 16

waypoint (D 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 24-206-0010
Client Project Description: EFF Wastewater
Lab No
Client Sample ID
Matrix
Date Collected
Date Received Method Lab ID
98623
EFF
Aqueous
07/24/2024 10:45
07/24/2024 14:10
98623
EFF
Aqueous
07/24/2024 10:45
07/24/2024 14:10 8315A WP MTN
98623
EFF
Aqueous
07/24/2024 10:45
07/24/2024 14:10 531OC-2011 WP MTN
98624
Field
Aqueous
07/24/2024 10:45
07/24/2024 14:10
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 3 of 16

Waypoint
ANALYTICAL
Client: Weyerhaeuser Corporation
Project: EFF Wastewater
Lab Report Number: 24-206-0010
Date: 8/7/2024
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
CASE NARRATIVE
Total Metals Method EPA-200.7
Sample 98183
QC Batch No: V50204/V50028
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 98623 (EFF)
QC Batch No: V50218/V50028
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 98623 (EFF)
QC Batch No: V50597/V50028
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 98183
Analyte: Calcium
QC Batch No: V50090/V50028
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 98623 (EFF)
Analyte: Chromium
QC Batch No: V50597/V50028
ICB and CCB failed high. Sample concentration BRL. Results not affected.
Sample 98623 (EFF)
Analyte: Magnesium
QC Batch No: V50218/V50028
ICB failed high. Result 1 Ox concentration. Result not affected.
Sample 98183
Analyte: Sodium
QC Batch No: V50119/V50028
CCB failed high. Result 10x concentration. Result not affected.
Metals Digestion Method EPA-200.7 (PREP)
Sample 98623 (EFF)
QC Batch No: V50028/V50028
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Mercury Method 245.1
Sample 98576
Analyte: Mercury
QC Batch No: V50079/V50046
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 4 of 16

Waypointo
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Sample 98576
Analyte: Mercury
QC Batch No: V50079/V50046
CCV failed high. Sample concentration BRL. Results not affected.
Sample 98623 (EFF)
Analyte: Mercury
QC Batch No: V50079/V50046
CCV failed high. Sample concentration BRL. Results not affected.
Mercury Method 245.1 (Prep)
Sample 98623 (EFF)
QC Batch No: V50046/V50046
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Anions by Ion Chromatography Method 300.0
Sample 98623 (EFF)
QC Batch No: V50377/V50376
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 98632
Analyte: Chloride
QC Batch No: V50377/V50376
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Sample 98632
Analyte: Nitrite-N
QC Batch No: V50377/V50376
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
TKN by Block Digestion and FIA Method EPA-351.2
Sample 98606 (INF)
Analyte: Total Kjeldahl Nitrogen
QC Batch No: V50226/V50184
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
625.1 - Base/Neutrals and Acids by GC/MS Method 625.1
Sample 98623 (EFF)
QC Batch No: V50155/V50085
The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly.
Sample 98623 (EFF)
QC Batch No: V50155/V50085
Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the
extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory
Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due
to the sample matrix.
Analyte: Phenol
Page 5 of 16

Waypoint
ANALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
QC Batch No: V50155/V50085
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Total Phosphorus Method 4500-P F-2011
Sample 98865 (PZ-10)
Analyte: Phosphorus
QC Batch No: V50514/V50214
Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the
system was in control, but the reported result could be affected by matrix interference.
Fecal Coliform MPN Method 9221E-2011
QC Batch No: V50073
Duplicate result: 170 MPN/ 100 n
Sample 98623 (EFF)
Analyte: Fecal Coliform
QC Batch No: V50073
Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits.
Volatile Organic Compounds - GC/MS Method 8260D
Analyte: 2-Butanone
QC Batch No: V50202/V50167
This target analyte was flagged for recoveries outside QC limits in the associated LCS/LCSD. Results should be
considered estimated due to the potential for a high bias.
Analyte: Bromomethane
QC Batch No: V50202/V50167
Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there
was adequate sensitivity to report this compound at the laboratory reporting limit as non -detect.
Analyte: Chloroethane
QC Batch No: V50202/V50167
Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there
was adequate sensitivity to report this compound at the laboratory reporting limit as non -detect.
Analyte: 1,2-Dibromo-3-chloropropane
QC Batch No: V50202/V50167
Target analyte did not meet calibration verification criteria. Analysis of a low level check demonstrated that there
was adequate sensitivity to report this compound at the laboratory reporting limit as non -detect.
Page 6 of 16

wavDointe
ANALYTICAL
00052
Weyerhaeuser Corporation
Dennis Atkinson
524 Pride Way
Elkin , NC 28621
Report Number : 24-206-0010
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Project EFF Wastewater
Information :
REPORT OF ANAL YSIS
Report Date : 08/07/2024
Received : 07/24/2024
Lab No : 98623
Matrix: Aqueous
Sample ID : EFF
Sampled:
7/24/2024
10:45
Test
Results
Units
MDL MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Fecal Coliform MPN/g
110
MPN/100ml-
2.0
1
07/24/24 14:33
MLW
9221E-2011
Sodium Absorption Ratio
1.00
Ratio
0.100
10
07/29/24 21:52
CALCULATION
Plant Available Nitrogen
12.5
mg/L
0.100
1
07/24/24 22:06
CALCULATION
Ammonia Nitrogen
1.06
mg/L
0.10
1
08/01/24 14:16
RLW
4500-NH3G-2011
Biochemical Oxygen Demand (5-day)
310
mg/L
2.0
1
07/24/24 09:38
MLW
521OB-2015
Chloride
130
mg/L
50.0
50
07/24/24 22:06
NDL
300.0
COD (Chemical Oxygen Demand)
2550
mg/L
90
1
07/26/24 10:00
SLO
5220D-2011
Nitrate (NO3-N)
<5.00
mg/L
5.00
50
07/24/24 22:06
NDL
300.0
Nitrite (NO2-N)
<5.00
mg/L
5.00
50
07/24/24 22:06
NDL
300.0
Nitrate+Nitrite-N
<5.00
mg/L
5.00
50
07/24/24 22:06
300.0
Total Dissolved Solids
4070
mg/L
50
1
07/25/24 14:38
GOB
2540C-2015
Total Suspended Solids
307
mg/L
55.5
1
07/26/24 10:48
GOB
2540D-2015
Total Kjeldahl Nitrogen
41.1
mg/L
5.00
10
07/30/24 10:28
RLW
EPA-351.2
Total Nitrogen
41.1
mg/L
5.00
10
07/24/24 22:06
CALCULATION
Phosphorus
3.38
mg/L
0.050
1
08/02/24 15:44
RLW
4500-P F-2011
TOC
684
mg/L
100
100
08/01/2411:37
JJT
531OC-2011
Calcium
26.5
mg/L
8.00
10
07/29/24 21:52
JKC
EPA-200.7
Chromium
<0.120
mg/L
0.120
10
08/07/24 13:54
JKC
EPA-200.7
Magnesium
25.7
mg/L
4.00
10
07/29/24 21:52
JKC
EPA-200.7
Mercury (Total)
<0.000800
mg/L
0.000800
1
07/25/24 18:10
NPC
245.1
Sodium
955
mg/L
160
100
08/02/2418:24
JKC
EPA-200.7
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 7 of 16

wavDointe
ANALYTICAL
00052
Weyerhaeuser Corporation
Dennis Atkinson
524 Pride Way
Elkin , NC 28621
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Project EFF Wastewater
Information :
Report Number : 24-206-0010 REPOR T OF A NA L YSIS
Report Date : 08/07/2024
Received : 07/24/2024
Lab No : 98623 Matrix: Aqueous
Sample ID : EFF Sampled: 7/24/2024 10:45
Analytical Method: 625.1 Prep Batch(es): V50085 07/26/24 09:41
Prep Method: 625.1 (Prep)
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Phenol
<0.200
mg/L
0.200
4
07/26/24 22:07
AMP
V50155
Surrogate: Phenol-d5
13.7
Limits:
10-63%
4 07/26/24 22:07 AMP
625.1
Surrogate: 2-Fluorophenol
19.4 *
Limits:
22-84%
4 07/26/24 22:07 AMP
V50155
Surrogate: 2,4,6-Tribromophenol
29.2 *
Limits:
31-144%
4 07/26/24 22:07 AMP
V50155
Analytical Method: 8260D
Prep Batch(es):
V50167
07/26/24 14:07
Prep Method: 5030B
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Acetone
<180
Ng/L
180
500
100
07/27/24 00:14
ENM
V50202
Acrolein
<200
pg/L
200
500
100
07/27/24 00:14
ENM
V50202
Acrylonitrile
<23.0
Ng/L
23.0
500
100
07/27/24 00:14
ENM
V50202
Benzene
<18.0
pg/L
18.0
50.0
100
07/27/24 00:14
ENM
V50202
Bromobenzene
<21.0
Ng/L
21.0
50.0
100
07/27/24 00:14
ENM
V50202
Bromochloromethane
<42.0
pg/L
42.0
100
100
07/27/24 00:14
ENM
V50202
Bromodichloromethane
<16.0
Ng/L
16.0
50.0
100
07/27/24 00:14
ENM
V50202
Bromoform
<150
pg/L
150
500
100
07/27/24 00:14
ENM
V50202
Bromomethane
<28.0
Ng/L
28.0
100
100
07/27/24 00:14
ENM
V50202
n-Butylbenzene
<18.5
pg/L
18.5
100
100
07/27/24 00:14
ENM
V50202
sec -Butyl benzene
<20.0
Ng/L
20.0
50.0
100
07/27/24 00:14
ENM
V50202
tert-Butyl benzene
<92.0
pg/L
92.0
200
100
07/27/24 00:14
ENM
V50202
Carbon Disulfide
<15.0
Ng/L
15.0
500
100
07/27/24 00:14
ENM
V50202
Carbon Tetrachloride
<18.0
pg/L
18.0
50.0
100
07/27/24 00:14
ENM
V50202
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 8 of 16

�n
W�ypOI ■ ■� . 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00052
Weyerhaeuser Corporation Project EFF Wastewater
Dennis Atkinson Report Date : 08/07/2024
524 Pride Way Information : Received : 07/24/2024
Elkin , NC 28621
Report Number : 24-206-0010 REPOR T OF A NA L YSIS
Lab No : 98623
Matrix: Aqueous
Sample ID : EFF
Sampled:
7/24/2024
10:45
Analytical Method: 8260D
Prep Batch(es):
V50167
07/26/24 14:07
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Chlorobenzene
<19.0
Ng/L
19.0
50.0
100
07/27/24 00:14
ENM
V50202
Chlorodibromomethane
<19.0
pg/L
19.0
50.0
100
07/27/24 00:14
ENM
V50202
Chloroethane
<43.0
N9/L
43.0
100
100
07/27/24 00:14
ENM
V50202
Chloroform
<22.0
pg/L
22.0
50.0
100
07/27/24 00:14
ENM
V50202
Chloromethane
<22.0
N9/L
22.0
50.0
100
07/27/24 00:14
ENM
V50202
2-Chlorotoluene
<20.0
pg/L
20.0
50.0
100
07/27/24 00:14
ENM
V50202
4-Chlorotoluene
<20.0
N9/L
20.0
50.0
100
07/27/24 00:14
ENM
V50202
Di -Isopropyl Ether (DIPE)
<96.0
pg/L
96.0
500
100
07/27/24 00:14
ENM
V50202
1,2-Dibromo-3-Chloropropane
<110
N9/L
110
200
100
07/27/24 00:14
ENM
V50202
1,2-Dibromoethane
<20.0
pg/L
20.0
50.0
100
07/27/24 00:14
ENM
V50202
Dibromomethane
<23.0
N9/L
23.0
50.0
100
07/27/24 00:14
ENM
V50202
1,2-Dichlorobenzene
<22.0
pg/L
22.0
50.0
100
07/27/24 00:14
ENM
V50202
1,3-Dichlorobenzene
<19.0
Ng/L
19.0
50.0
100
07/27/24 00:14
ENM
V50202
1,4-Dichlorobenzene
<21.0
pg/L
21.0
50.0
100
07/27/24 00:14
ENM
V50202
Dichlorodifluoromethane
<120
N9/L
120
500
100
07/27/24 00:14
ENM
V50202
1,1-Dichloroethane
<24.0
pg/L
24.0
50.0
100
07/27/24 00:14
ENM
V50202
1,2-Dichloroethane
<15.0
N9/L
15.0
50.0
100
07/27/24 00:14
ENM
V50202
1,1-Dichloroethene
<15.0
pg/L
15.0
50.0
100
07/27/24 00:14
ENM
V50202
cis-1,2-Dichloroethene
<20.0
N9/L
20.0
50.0
100
07/27/24 00:14
ENM
V50202
trans-1,2-Dichloroethene
<18.0
pg/L
18.0
50.0
100
07/27/24 00:14
ENM
V50202
1,2-Dichloropropane
<19.0
N9/L
19.0
50.0
100
07/27/24 00:14
ENM
V50202
1,3-Dichloropropane
<13.0
pg/L
13.0
50.0
100
07/27/24 00:14
ENM
V50202
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 9 of 16

�n
W�ypOI ■ ■� . 0 449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
ANALYTICAL www.waypointanalytical.com
00052
Weyerhaeuser Corporation Project EFF Wastewater
Dennis Atkinson Report Date : 08/07/2024
524 Pride Way Information : Received : 07/24/2024
Elkin , NC 28621
Report Number : 24-206-0010 REPOR T OF A NA L YSIS
Lab No : 98623
Matrix: Aqueous
Sample ID : EFF
Sampled:
7/24/2024
10:45
Analytical Method: 8260D
Prep Batch(es):
V50167
07/26/24 14:07
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
2,2-Dichloropropene
<21.0
Ng/L
21.0
200
100
07/27/24 00:14
ENM
V50202
1,1-Dichloropropene
<20.0
pg/L
20.0
50.0
100
07/27/24 00:14
ENM
V50202
cis- 1,3-Dich loropropene
<21.0
N9/L
21.0
50.0
100
07/27/24 00:14
ENM
V50202
trans-1,3-Dichloropropene
<15.0
pg/L
15.0
50.0
100
07/27/24 00:14
ENM
V50202
Ethylbenzene
<17.0
N9/L
17.0
50.0
100
07/27/24 00:14
ENM
V50202
Ethyl Tertiary Butyl Ether (ETBE)
<180
pg/L
180
1000
100
07/27/24 00:14
ENM
V50202
Hexachlorobutadiene
<35.0
N9/L
35.0
200
100
07/27/24 00:14
ENM
V50202
n-Hexane
<130
pg/L
130
1000
100
07/27/24 00:14
ENM
V50202
2-Hexanone
<38.0
N9/L
38.0
500
100
07/27/24 00:14
ENM
V50202
Isopropyl benzene
<18.0
pg/L
18.0
500
100
07/27/24 00:14
ENM
V50202
4-Isopropyl toluene
<8.90
N9/L
8.90
50.0
100
07/27/24 00:14
ENM
V50202
Methyl Ethyl Ketone (MEK)
1283
pg/L
71.0
500
100
07/27/24 00:14
ENM
V50202
Methyl tert-butyl ether (MTBE)
<14.0
Ng/L
14.0
50.0
100
07/27/24 00:14
ENM
V50202
4-Methyl-2-Pentanone
<100
pg/L
100
500
100
07/27/24 00:14
ENM
V50202
Methylene Chloride
<33.0
N9/L
33.0
100
100
07/27/24 00:14
ENM
V50202
Naphthalene
<47.0
pg/L
47.0
100
100
07/27/24 00:14
ENM
V50202
n-Propylbenzene
<19.0
N9/L
19.0
50.0
100
07/27/24 00:14
ENM
V50202
Styrene
<22.0
pg/L
22.0
50.0
100
07/27/24 00:14
ENM
V50202
1,1,1,2-Tetrachloroethane
<16.0
N9/L
16.0
50.0
100
07/27/24 00:14
ENM
V50202
1,1,2,2-Tetrachloroethane
<16.0
pg/L
16.0
50.0
100
07/27/24 00:14
ENM
V50202
Tetrachloroethene
<22.0
N9/L
22.0
50.0
100
07/27/24 00:14
ENM
V50202
Toluene
<22.0
pg/L
22.0
50.0
100
07/27/24 00:14
ENM
V50202
Qualifiers/ * Outside QC Limit
DF
Dilution Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 10 of 16

wavDointe
ANALYTICAL
00052
Weyerhaeuser Corporation
Dennis Atkinson
524 Pride Way
Elkin , NC 28621
Report Number : 24-206-0010
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Project EFF Wastewater
Information :
REPORT OF ANAL YSIS
Report Date : 08/07/2024
Received : 07/24/2024
Lab No : 98623
Sample ID : EFF
Matrix: Aqueous
Sampled: 7/24/2024 10:45
Analytical Method: 8260D
Prep Batch(es):
V50167
07/26/24 14:07
Prep Method: 5030E
Test
Results
Units
MDL
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
1,2,3-Trichlorobenzene
<38.0
Ng/L
38.0
200
100
07/27/24 00:14 ENM
V50202
1,2,4-Trichlorobenzene
<31.0
pg/L
31.0
100
100
07/27/24 00:14 ENM
V50202
1,1,1-Trichloroethane
<16.0
Ng/L
16.0
50.0
100
07/27/24 00:14 ENM
V50202
1,1,2-Trichloroethane
<9.60
pg/L
9.60
50.0
100
07/27/24 00:14 ENM
V50202
Trichloroethene
<18.0
Ng/L
18.0
50.0
100
07/27/24 00:14 ENM
V50202
Trichlorofluoromethane
<18.0
pg/L
18.0
50.0
100
07/27/24 00:14 ENM
V50202
1,2,3-Trichloropropane
<27.0
Ng/L
27.0
100
100
07/27/24 00:14 ENM
V50202
1,3,5-Trimethyl benzene
<18.0
pg/L
18.0
50.0
100
07/27/24 00:14 ENM
V50202
Vinyl Acetate
<100
Ng/L
100
200
100
07/27/24 00:14 ENM
V50202
Vinyl Chloride
<17.0
pg/L
17.0
50.0
100
07/27/24 00:14 ENM
V50202
o-Xylene
<21.0
Ng/L
21.0
50.0
100
07/27/24 00:14 ENM
V50202
m,p-Xylene
<42.0
pg/L
42.0
100
100
07/27/24 00:14 ENM
V50202
Xylene (Total)
<21
Ng/L
21.0
50.0
100
07/27/24 00:14
V50202
Surrogate: 4-Bromofluorobenzene
99.8
Limits:
70-130%
100 07/27/24 00:14 ENM
V50202
Surrogate: Dibromofluoromethane
104
Limits:
70-130%
100 07/27/24 00:14 ENM
V50202
Surrogate: 1,2-Dichloroethane - d4
102
Limits:
70-130%
100 07/27/24 00:14 ENM
V50202
Surrogate: Toluene-d8
100
Limits:
70-130%
100 07/27/24 00:14 ENM
V50202
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 11 of 16

Waypointo.
ANALYTICAL
00052
Weyerhaeuser Corporation
Project
Dennis Atkinson
524 Pride Way
Information
Elkin , NC 28621
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi nta na lytica Isom
EFF Wastewater
Report Number : 24-206-0010 REPOR T OF A NA L YSIS
Report Date : 08/07/2024
Received : 07/24/2024
Lab No : 98623 Matrix: Aqueous
Sample ID : EFF Sampled: 7/24/2024 10:45
Analytical Method: 8315A Prep Batch(es): L763751 07/25/24 14:15
Prep Method: 8315A
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Batch
Formaldehyde 5030 N9/L 500 1 07/26/24 21:34 SWB L764025
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 12 of 16

Waypointo.
ANALYTICAL
00052
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypoi nta na lytica Isom
Weyerhaeuser Corporation Project EFF Wastewater
Dennis Atkinson
524 Pride Way Information
Elkin , NC 28621
Report Number : 24-206-0010 REPOR T OF A NA L YSIS
Report Date : 08/07/2024
Received : 07/24/2024
Lab No : 98624
Sample ID : Field
Matrix: Aqueous
Sampled: 7/24/2024 10:45
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Conductivity
40100
pmhos/cm
1 1 07/24/24 10:45 FLD FIELD
pH
8.9
s.u.
1 07/24/24 10:45 FLD FIELD
Temperature
26.8
C
0.1 1 07/24/24 10:45 FLD FIELD
Qualifiers/ * Outside QC Limit
Definitions J Estimated value
DF Dilution Factor
MQL Method Quantitation Limit
Page 13 of 16

(2)
WayPAo0nt..
NALYTICAL
449 Springbrook Rd, Charlotte, NC 28217
Main 704.529.6364
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 00052
Customer Name: Weyerhaeuser Corporation
Report Number: 24-206-0010
Shipping Method
0 Fed Ex 0 US Postal U Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
IRT15 1.8C
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample Iabel(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
0 Not Present
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
* No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Angelo Norvell Date & Time: 07/24/2024 15:36:45
Page 14 of 16

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