HomeMy WebLinkAboutWQ0004972_Monitoring - 07-2024_20240830 (3)Monitoring Report Submittal
Permit Number#*
Name of Facility:*
Month:* July
Report Information
Type *
GW-59
WQ0004972
Forest Lake RV Park WWTP
Year:* 2024
Upload Document*
GW-59 MW Reports for July 2024.pdf
PDF Only
2.89 M B
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address: * agrenier@greenerehssolutions.com
Name of Submitter: * Amanda Grenier
Signature:
Date of submittal: 8/30/2024
This will be filled in automatically
Initial Review
Reviewer: Wanda.Gerald
Is the project number correct?* WQ0004972
Is the monitoring report accepted?* Yes No
Regional Office* Winston-Salem
Reviewer: _anonymous
Review Date: 9/17/2024
Docusign Envelope ID: 9EDCDCEA-6FA3-4BAF-AD82-56E3FDA54B3A
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: 919-356-6509
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 1
Date sample collected: 7/9/2024
FIELD ANALYSES:
WAS
Well Depth: 90.7 ft.
Well Diameter: 2 in.
pH 00400: 5.96 units Temp. 000lo: 19.1 °C
DRY at
Depth to Water Level 82546: 67.6 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. 00094: 63 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
4.5
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: ❑ YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 7/9/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NOz) as N 00615
mg/L Pb - Lead olo51 ug/L
Coliform: MF Fecal 31616 16
/100mL
Nitrate (NO3) as N 00620 0.15
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 <0.05
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al -Aluminum oilo5
mg/L
pH (Lab) 00403 6.0
units
Ba - Barium 01007
ug/L
TOC 00680 2.3
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 2.2
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo6lo <0.10
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
8/29/2024
GW-59 Rev.06-07-2018
Docusign Envelope ID: 9EDCDCEA-6FA3-4BAF-AD82-56E3FDA54B3A
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: 919-356-6509
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 2
Date sample collected: 7/9/2024
FIELD ANALYSES:
WAS
Well Depth: 46 ft.
Well Diameter: 2 in.
pH 00400: 5.69 units Temp. 000lo: 18.7 oC
DRY at
Depth to Water Level 82546:38.5 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. 00094: 51.7 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
3.5
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: ❑ YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 7/9/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NOz) as N 00615
mg/L Pb - Lead olo51 ug/L
Coliform: MF Fecal 31616 1.0
/100mL
Nitrate (NO3) as N 00620 0.44
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.062
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al -Aluminum oilo5
mg/L
pH (Lab) 00403 5.9
units
Ba - Barium 01007
ug/L
TOC 00680 <1
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 2.9
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo6lo <0.10
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018
Docusign Envelope ID: 9EDCDCEA-6FA3-4BAF-AD82-56E3FDA54B3A
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: 919-356-6509
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 3
Date sample collected: 7/9/2024
FIELD ANALYSES:
WAS
Well Depth: 20.3 ft.
Well Diameter: 2 in.
pH 00400: 4.72 units Temp. 000lo: 19.4 oC
DRY at
Depth to Water Level 82546: 11.7 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. 00094: 233 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
3
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: —]YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 7/9/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NOz) as N 00615
mg/L Pb - Lead olo51 ug/L
Coliform: MF Fecal 31616 580
/100mL
Nitrate (NO3) as N 00620 16.6
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.15
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al -Aluminum oilo5
mg/L
pH (Lab) 00403 4.8
units
Ba - Barium 01007
ug/L
TOC 00680 <1
mg/L
Ca - Calcium 00916
mg/L
Chloride 0094o 29.0
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo6lo <0.1
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018
Docusign Envelope ID: 9EDCDCEA-6FA3-4BAF-AD82-56E3FDA54B3A
SUBMIT FORM ON YELLOW PAPER ONLY
• •
DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV. OF WATER RESOURCES
GROUNDWATER QUALITY MONITORING:
INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: Expiration Date: 10/31/2027
Facility Name: Forest Lake RV WWTP
Non -Discharge WQ0004972 UIC
Permit Name (if different):
NPDES Other
Facility Address: 192 Thousand Trails Dr.
TYPE OF PERMITTED OPERATION BEING MONITORED
Advance NC
27006
County Davie
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑■ Spray Field ❑ Remediation:
Contact Person: Amanda Grenier
Telephone#: 919-356-6509
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name: Forest Lake RV Spray Irrigation Field
No. of wells to be sampled: 4
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): 4
Date sample collected: 7/9/2024
FIELD ANALYSES:
WAS
Well Depth: 39 ft.
Well Diameter: 2 in.
pH 00400: 5.58 units Temp. 000lo: 18.1 °C
DRY at
Depth to Water Level 82546: 29.2 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. 00094: 154.3 µMhos
time of
sampling,
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
check
Volume of water pumped/bailed before sampling:
1.5
gallons
Appearance Clear
here:❑
Samples for metals were collected unfiltered: ❑ YES
❑■ NO and field acidified: —]YES ❑■ NO
LABORATORY INFORMATION
Date sample analyzed: 7/9/2024
Laboratory Name: Pace Analytical
Certification No. 12
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NOz) as N 00615
mg/L Pb - Lead olo51 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 7.3
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus: Total as P 00665 0.12
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300
mg/L
Al -Aluminum oilo5
mg/L
pH (Lab) 00403 5.6
units
Ba - Barium 01007
ug/L
TOC 00680 <1
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 11.2
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 7873 method #
Total Ammonia oo6lo <0.1
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese olo55
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
George Gudgeon, Sr. Vice President
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.06-07-2018
Docusign Envelope ID: 9EDCy'A DCEA- 3� SBA iAD8, b�6�E3�FDA�5�4B3AqL-�,� �FORM Permit # WQ0004972
(Submit one each monitoring period with GW 59 forms,)
1
Enter date monitoring results were due. (8/30/24 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question I or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
X
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance.
X
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is "NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
MW #2 field pH was 5.7, lab pH 5.9. MW #3 field pH was 4.7, lab pH 4.8 and nitrate was 16.6 mg/
I. MW #4 field pH was 5.6, lab pH 5.6.
X
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
Yes, DEQ is aware and have expressed concerns about the well. 2 more test wells
were sampled and the results were sent to DEQ.
X
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells maybe improperly
located, contact the Regional Office.
X
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days, an evaluation may be
required to determine the impact the waste disposal system is havinq at the review and compliance
boundaries surroundinq this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/or penalties.
2 more test wells were dug and sampled. The results were submitted to DEQ for
review.
X
8
The person completing this portion (GIN--59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information ''submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
8/29/24
Signature of Permittee (or Authorized Agent) Date
GW-59A 12/8/2003
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
July 24, 2024
Amanda D. Grenier
Greener EHS Solutions
21 Selby Ct.
Holly Springs, NC 27540
RE: Project: Forest Lake- MW's July
Pace Project No.: 92740754
Dear Amanda Grenier:
Enclosed are the analytical results for sample(s) received by the laboratory on July 09, 2024. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
matthew.brainard@pacelabs.com
704-977-0942
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23
ace
Pace Analytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
(704)875-9092
Project: Forest Lake- MW's July
Pace Project No.: 92740754
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification M 37712
North Carolina Wastewater Certification #: 40
CERTIFICATIONS
South Carolina Certification M 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification M E87627
Kentucky UST Certification M 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification M 460221
South Carolina Laboratory ID: 99030
South Carolina Certification M 99030001
Virginia/VELAP Certification M 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Forest Lake- MW's July
92740754
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92740754001
MW #1
SM 9222D-2015
CHC
1
PASI-C
EPA 9040C
SMS
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92740754002
MW #2
SM 9222D-2015
CHC
1
PASI-C
EPA 9040C
SMS
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92740754003
MW #3
SM 9222D-2015
KDF
1
PASI-C
EPA 9040C
SMS
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
92740754004
MW #4
SM 9222D-2015
CHC
1
PASI-C
EPA 9040C
SMS
1
PASI-A
EPA 350.1 Rev 2.0 1993
NCF
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 365.1 Rev 2.0 1993
Zip
1
PASI-A
SM 4500-CI-E-2011
Zip
1
PASI-A
SM 531OB-2014
MJP
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23
ANALYTICAL RESULTS
Project: Forest Lake- MW's July
Pace Project No.: 92740754
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MW #1 Lab ID: 92740754001 Collected: 07/09/24 08:35 Received: 07/09/24 15:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
16.0 CFU/100 mL 1.0
1
07/09/24 16:06 07/10/24 14:09
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
6.0 Std. Units 0.10
1
07/19/24 15:08
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
07/18/24 16:31
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.15 mg/L 0.020
1
07/10/24 01:40
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
ND mg/L 0.050
1
07/18/2412:56 07/19/2412:03
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
2.2 mg/L 1.0
1
07/17/2410:38
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
2.3 mg/L 1.0
1
07/21/24 18:38
7440-44-0
Date: 07/24/2024 12:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 4 of 23
ANALYTICAL RESULTS
Project: Forest Lake- MW's July
Pace Project No.: 92740754
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MW #2 Lab ID: 92740754002 Collected: 07/09/24 09:30 Received: 07/09/24 15:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
1.0 CFU/100 mL 1.0
1
07/09/24 16:06 07/10/24 14:09
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.9 Std. Units 0.10
1
07/19/24 15:15
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
07/18/24 16:51
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
0.44 mg/L 0.020
1
07/10/24 01:42
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.062 mg/L 0.050
1
07/18/2412:56 07/19/2412:05
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
2.9 mg/L 1.0
1
07/17/2410:39
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
07/21/24 19:30
7440-44-0
Date: 07/24/2024 12:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23
ANALYTICAL RESULTS
Project: Forest Lake- MW's July
Pace Project No.: 92740754
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MW #3 Lab ID: 92740754003 Collected: 07/09/24 10:30 Received: 07/09/24 15:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
580 CFU/100 mL 1.0
1
07/09/24 17:48 07/10/24 15:48
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
4.8 Std. Units 0.10
1
07/19/24 14:13
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
07/18/24 16:53
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
16.6 mg/L 0.10
5
07/11/24 00:45
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.15 mg/L 0.050
1
07/18/2412:56 07/19/2412:06
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
29.0 mg/L 1.0
1
07/22/2411:24
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
07/21/24 19:47
7440-44-0
Date: 07/24/2024 12:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 23
ANALYTICAL RESULTS
Project: Forest Lake- MW's July
Pace Project No.: 92740754
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Sample: MW #4 Lab ID: 92740754004 Collected: 07/09/24 09:55 Received: 07/09/24 15:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Charlotte
Fecal Coliforms
ND CFU/100 mL 1.0
1
07/09/24 16:06 07/10/24 14:09
9040 pH
Analytical Method: EPA 9040C
Pace Analytical Services -Asheville
pH at 25 Degrees C
5.6 Std. Units 0.10
1
07/19/24 14:03
H3
350.1 Ammonia
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Ammonia
ND mg/L 0.10
1
07/18/24 16:35
7664-41-7
353.2 Nitrogen, NO2/NO3 unpres
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
Nitrogen, Nitrate
7.3 mg/L 0.10
5
07/10/24 01:59
14797-55-8
365.1 Phosphorus, Total
Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993
Pace Analytical Services -Asheville
Phosphorus
0.12 mg/L 0.050
1
07/18/2412:56 07/19/2412:11
7723-14-0
4500 Chloride
Analytical Method: SM 4500-CI-E-2011
Pace Analytical Services -Asheville
Chloride
11.2 mg/L 1.0
1
07/22/2411:26
16887-00-6
5310B TOC
Analytical Method: SM 531OB-2014
Pace Analytical Services -Asheville
Total Organic Carbon
ND mg/L 1.0
1
07/21/24 20:07
7440-44-0
Date: 07/24/2024 12:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 23
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 867115 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92740754001, 92740754002, 92740754004
METHOD BLANK: 4469324 Matrix: Water
Associated Lab Samples: 92740754001, 92740754002, 92740754004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 07/10/24 14:09
SAMPLE DUPLICATE: 4469325
Parameter
Fecal Coliforms
92740754002 Dup
Units Result Result RPD Qualifiers
CFU/100 mL 1.0 ND
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 8 of 23
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 867617 Analysis Method: SM 9222D-2015
QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92740754003
METHOD BLANK: 4472176 Matrix: Water
Associated Lab Samples: 92740754003
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fecal Coliforms CFU/100 mL ND 1.0 07/10/24 15:48
SAMPLE DUPLICATE: 4472177
Parameter
Fecal Coliforms
92740630001 Dup
Units Result Result RPD Qualifiers
CFU/100 mL 5.0 10.0 67 D6
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 9 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 869360 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754003, 92740754004
SAMPLE DUPLICATE: 4480888
92741795001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.2 8.2 0 H3
SAMPLE DUPLICATE: 4480889
92741795002 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 8.2 8.2 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 869545 Analysis Method: EPA 9040C
QC Batch Method: EPA 9040C Analysis Description: 9040 pH
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754001, 92740754002
SAMPLE DUPLICATE: 4481569
92740754001 Dup
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 6.0 6.0 0 H3
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 869256 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754001, 92740754002, 92740754003, 92740754004
METHOD BLANK: 4480143
Matrix:
Water
Associated Lab Samples: 92740754001, 92740754002, 92740754003, 92740754004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Ammonia
mg/L
ND
0.10
07/18/24 15:52
LABORATORY CONTROL SAMPLE:
4480144
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Ammonia
mg/L
5
5.1
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4480145 4480146
MS MSD
92740483002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 15.1 5 5 16.5 14.9 29 -3 90-110 10 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4480147 4480148
MS MSD
92742485001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 0.50 5 5 5.6 5.7 103 103 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 867030 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754001, 92740754002, 92740754004
METHOD BLANK: 4469077
Matrix:
Water
Associated Lab Samples: 92740754001, 92740754002, 92740754004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND
0.020
07/10/24 01:17
LABORATORY CONTROL SAMPLE:
4469078
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Nitrogen, Nitrate
mg/L
1.5
1.5
102 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4469079 4469080
MS MSD
92740417001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 0.35 1.5 1.5 1.9 1.9 105 105 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4469081 4469082
MS MSD
92740453005 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L 0.16 1.5 1.5 1.6 1.6 98 97 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 23
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 867371 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754003
METHOD BLANK: 4471016
Associated Lab Samples: 92740754003
Parameter Units
Nitrogen, Nitrate mg/L
LABORATORY CONTROL SAMPLE: 4471017
Parameter Units
Nitrogen, Nitrate mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.020 07/10/24 23:53
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1.5 1.6 104 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4471020 4471021
MS MSD
92740823010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L <0.0039 1.5 1.5 1.5 1.5 100 100 90-110 1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4471030 4471031
MS MSD
92740823007 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Nitrate mg/L <0.0039 1.5 1.5 1.2 1.2 79 79 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 868849 Analysis Method: EPA 365.1 Rev 2.0 1993
QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754001, 92740754002, 92740754003, 92740754004
METHOD BLANK: 4477962
Matrix:
Water
Associated Lab Samples: 92740754001, 92740754002, 92740754003, 92740754004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Phosphorus
mg/L
ND
0.050
07/19/2411:41
LABORATORY CONTROL SAMPLE:
4477963
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Phosphorus
mg/L
2.5
2.5
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4477964 4477965
MS MSD
92740735022 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 0.19 2.5 2.5 2.6 2.6 97 96 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4477966 4477967
MS MSD
92740737001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/L 13.0 2.5 2.5 14.6 14.8 61 70 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 15 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 868542 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754001, 92740754002
METHOD BLANK: 4476488
Matrix:
Water
Associated Lab Samples: 92740754001, 92740754002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
mg/L
ND
1.0
07/17/2410:07
LABORATORY CONTROL SAMPLE:
4476489
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
mg/L
20
20.7
103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4476490 4476491
MS MSD
92739646002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 6.2 10 10 17.0 16.9 108 107 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4476492 4476493
MS MSD
92739646003 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 8.0 10 10 17.6 18.4 96 104 90-110 4
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 16 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 869556 Analysis Method: SM 4500-CI-E-2011
QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754003, 92740754004
METHOD BLANK: 4481599
Matrix:
Water
Associated Lab Samples: 92740754003, 92740754004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Chloride
mg/L
ND
1.0
07/22/2411:21
LABORATORY CONTROL SAMPLE:
4481600
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Chloride
mg/L
20
21.0
105 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4481601 4481602
MS MSD
92741604001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 24.0 10 10 34.1 34.2 101 103 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 17 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: Forest Lake- MW's July
Pace Project No.: 92740754
QC Batch: 869883 Analysis Method: SM 531 OB-2014
QC Batch Method: SM 531 OB-2014 Analysis Description: 5310E TOC
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92740754001, 92740754002, 92740754003, 92740754004
METHOD BLANK: 4483431
Matrix:
Water
Associated Lab Samples: 92740754001, 92740754002, 92740754003, 92740754004
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Organic Carbon
mg/L
ND
1.0
07/21/24 15:55
LABORATORY CONTROL SAMPLE:
4483432
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Organic Carbon
mg/L
25
24.0
96 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4483433 4483434
MS MSD
92740735022 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 6.9 25 25 31.6 31.1 99 97 90-110 2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4483435 4483436
MS MSD
92740751001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 4.3 25 25 27.1 27.4 91 92 90-110 1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC.
Page 18 of 23
Pace Analytical Services, LLC
Face9800 Kincey Ave. Suite 100
(-�Huntersville, NC 28078
(704)875-9092
QUALIFIERS
Project: Forest Lake- MW's July
Pace Project No.: 92740754
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 07/24/2024 12:55 PM without the written consent of Pace Analytical Services, LLC. Page 19 of 23
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project:
Pace Project No.:
Forest Lake- MW's July
92740754
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92740754001
MW #1
SM 9222D-2015
867115
SM 9222D-2015
867116
92740754002
MW #2
SM 9222D-2015
867115
SM 9222D-2015
867116
92740754003
MW #3
SM 9222D-2015
867617
SM 9222D-2015
867618
92740754004
MW #4
SM 9222D-2015
867115
SM 9222D-2015
867116
92740754001
MW #1
EPA 9040C
869545
92740754002
MW #2
EPA 9040C
869545
92740754003
MW #3
EPA 9040C
869360
92740754004
MW #4
EPA 9040C
869360
92740754001
MW #1
EPA 350.1 Rev 2.0 1993
869256
92740754002
MW #2
EPA 350.1 Rev 2.0 1993
869256
92740754003
MW #3
EPA 350.1 Rev 2.0 1993
869256
92740754004
MW #4
EPA 350.1 Rev 2.0 1993
869256
92740754001
MW #1
EPA 353.2 Rev 2.0 1993
867030
92740754002
MW #2
EPA 353.2 Rev 2.0 1993
867030
92740754003
MW #3
EPA 353.2 Rev 2.0 1993
867371
92740754004
MW #4
EPA 353.2 Rev 2.0 1993
867030
92740754001
MW #1
EPA 365.1 Rev 2.0 1993
868849
EPA 365.1 Rev 2.0 1993
869261
92740754002
MW #2
EPA 365.1 Rev 2.0 1993
868849
EPA 365.1 Rev 2.0 1993
869261
92740754003
MW #3
EPA 365.1 Rev 2.0 1993
868849
EPA 365.1 Rev 2.0 1993
869261
92740754004
MW #4
EPA 365.1 Rev 2.0 1993
868849
EPA 365.1 Rev 2.0 1993
869261
92740754001
MW #1
SM 4500-CI-E-2011
868542
92740754002
MW #2
SM 4500-CI-E-2011
868542
92740754003
MW #3
SM 4500-CI-E-2011
869556
92740754004
MW #4
SM 4500-CI-E-2011
869556
92740754001
MW #1
SM 5310B-2014
869883
92740754002
MW #2
SM 5310B-2014
869883
92740754003
MW #3
SM 5310B-2014
869883
92740754004
MW #4
SM 5310B-2014
869883
Date: 07/24/2024 12:55 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 20 of 23
i DC# Title: ENV-FRM-HUN1-0083 v05 Sample Condition Upon Receipt
ace
Effective Date: 05/24/2024
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersvi lie � Raleigh❑ Mechanicsville❑ AtlantaF— KernercviliPl-1
SampleClient Name: WO# : 92740754
Upon ;
C.-i��I'A Y :PLC 0 I��-�10��Project #: �
Courier: [:]Fed -Ex [-]UPS ❑USPS ❑Client
❑ Commercial Pace❑Other:
92740754
I
Custody Seal Present? Dyes No Seals Intact? Yes ❑No [-]N/A
Date/Initials Person Examining Contents-/y /
Packing Material: ❑Bubble Wrap []Bubble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: / []Yes ❑NOO/ N/A
❑ IR Gun ID: ` ICI G Type of Ice: I/ IWet yp 7_ ❑Blue ❑None
Correction Factor -
Cooler Temp: Add/Subtract ("C) Temp should be above freezing to I 6'C
�� ❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): . -, 5 has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC Did samoles originate from n fnreinn anurre (internatinnally
jcheck maps)? UYes UNo
including Hawaii and Puerto Rico)? ❑Yes ❑No
Comments/Discrepancy:
Chain of Custody Present?
EfYes
❑No
(—]N/A I
I.
Samples Arrived within Hold Time?
Yes
❑No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
❑Yes 2�o
❑N/A
3.
Rush Turn Around Time Requested?
[--]Yes
No
[]N/A
4.
Sufficient Volume?
Ayes
[:]No
❑N/A
5.
Correct Containers Used?
10yes
❑No
❑N/A
6.
-Pace Containers Used?
]yes
❑No
❑N/A
7.
Containers Intact? Qr]Yes [—]No (—]N/A
Dissolved analysis: Samples Field Filtered?
❑Yes
dNo
[:]N/A
8.
9.
Sample Labels Match COC? Dyes ❑No ❑N/A
-Includes Date/Time/ID/Analysis Matrix: W1
Headspace in VOA Vials (>5-6mm)?
❑Yes
❑No
El N/A
110.
Trip Blank Present?
❑Yes
[:]No
N/A
11.
Trip Blank Custody Seals Present?
❑Yes
[:]No
CJN/A
COMMENTS/SAMPLE DISCREPANCY
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Lot ID of split containers:
Date/Time:
Date:
Date:
Field Data Required? ❑Yes [:]No
Qualtrax ID: 69614 Page 1 of 2 Page 21 of 23
Vace
DC#_Title: ENV-FRM-HUN1-0083 v05_Sample Condition Upon Receipt
Effective Date: 05/24/2024
'Check mark top half of box if pH and/or dechlorination is verified and within the WO# 92740754
acceptance range for preservation samples. Project # PM: MWB Due Date: 07/24/24
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg CLIENT • 92-Greener
—Bottom half of box is to list number of bottles
"'Check all unpreserved Nitrates for chlorine
Laboratory Receiving Location: Asheville ❑ Eden❑ Greenwood ❑ Huntersville [f Raleigh[] Mechanicsville[] Atlanta[—] Kernersville❑
Client 6re,� t Profile/(Circle one)3 (33o7Z Notes
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
11
Time preservation
adjusted
Amount of Preservative
added
Lot #
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers.
Qualtrax ID: 69614 Page 2 of 2 Page 22 of 23
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