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HomeMy WebLinkAboutWQ0004972_Monitoring - 06-2024_20240730Monitoring Report Submittal Permit Number#* WQ0004972 Name of Facility:* Forest Lake RV Park WWTP Month:* June Report Information Type * Revised - NDMR, NDAR-1, NDAR-2, NDMLR Year:* 2024 Upload Document* 2024_June_Forest_Lake_WQ0004972_Monthly 1.84MB Report Complete Rev 1.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address: * agrenier@greenerehssolutions.com Name of Submitter: * Amanda Grenier Signature: 6VIO'W ada e*Aw t Date of submittal: 7/30/2024 This will be filled in automatically Initial Review Reviewer: Wanda.Gerald Is the project number correct?* WQ0004972 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 8/6/2024 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E NON -DISCHARGE APPLICATION REPORT (NDAR-1) Page of Permit No.: WQ0004972 Facility Name: Forest Lake County: Davie Month: June Year: 2024 Did irrigation Field Name: 1 Field Name: Field Name: Field Name: occur Area (acres): 6 Area (acres): Area (acres): Area (acres): at this facility? Cover Crop:Grass/Trees Cover Crop: p� Cover Crop: p� Cover Crop: p: Hourly Rate (in): 0.11 Hourly Rate (in): Hourly Rate (in): Hourly Rate (in): Yes Annual Rate (in): 46.8 Annual Rate (in): Annual Rate (in): Annual Rate (in): Weather Freeboard Field Irrigated? Yes Field Irrigated? Field Irrigated? Field Irrigated? >' @ U L (4 Q Q R „ Q- E d ~ g ate. Q y L a a� `0 O cn N D .2 >' O_ Q � m -o E .2 O Q iQ 'o a7 E R H •� a� T C 0 J E T M O_ C E v x O C�=J a) -o E .2 O Q iQ 'o a7 E R H •� a� �. C v J E 0 3_ C E 3 x O M Cfo2J a, a E N _� O C i Q a N .d, E H 0 a� T C 0 R J E T M O_ C E v x O 1062J a) -o E 2 O Q iQ o y E R .T a� T C R J E� a) 3_ C E 3 Cfo2J °F in ft ft gal min in in gal min in in gal min in in gal min in in 1 CL 77 0 2 CL 76 0 3 CL 83 0 3.2 43,013 240 0.26 0.07 4 CL 84 0 4 5 CL 85 0 3.9 6 1 CL 1 83 0 3.7 7 PC 85 0.25 3.9 8 C 85 0 9 CL 83 0 10 PC 81 0 3.1 11 CL 80 0 2.6 38,544 300 0.24 0.05 121 CL 1 82 0 1 3.4 13 PC 86 0 3.2 14 PC 91 0 3 15 PC 87 0 16 CL 82 0 17 CL 87 0 2.3 48,602 300 0.30 0.06 181 CL 1 86 0 1 3.2 19 CL 85 0 3 20 PC 87 0 2.8 44,861 300 0.28 0.06 21 C 90 0 3.2 22 C 90 0 23 C 93 0 241 C 1 92 0 1 3 25 C 91 0 2.6 26 C 95 0 2.3 52,643 300 0.32 0.06 27 CL 86 0 3.4 28 C 90 0 3.2 29 PC 91 0 301 PC 1 90 1 0 311 PC Monthly Loading: 227,663 1.40 0 0.00 0 0.00 0 0.00 12 Month Floating Total (in): 22.69 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E NON -DISCHARGE APPLICATION REPORT (NDAR-1) Did the application rates exceed the limits in Attachment B of your permit? Page of El Compliant ❑ Non -Compliant Were adequate measures taken to prevent effluent ponding in or runoff from the sites? O Compliant ❑ Non -Compliant Was a suitable vegetative cover maintained on all sites as specified in your permit? O Compliant ❑ Non -Compliant Were all setbacks listed in your permit maintained for every application to each permitted site? ❑ Compliant ❑ Non -Compliant Were all freeboards maintained in accordance with the specified freeboard heights in your permit? O Compliant ❑ Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective taken. Httacn aaamonal sneers IT Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Sam Perry Permittee: MHC TT, LP Certification No.: 1014038 Signing Official: George Gudgeon Grade: SI Phone Number: 919-548-2381 Signing Official's Title: Sr. Vice President Has the ORC changed since the previous NDAR-1? Phone Number: 312-279-1400 Permit Exp.: 10/31/27 7/30/2024 7/29/2024 Sam Perry (Ju130, 2024 :28 EDT) --- Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 L:21 p2np. of Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E NON -DISCHARGE MONITORING REPORT NDMR Permit No.: WQ0004972 Facility Name: Forest Lake Preserve ELS County: Davie Month: June Year: 2024 PPI: 001 Flow Measuring Point: Parameter Monitoring Point: Parameter Code 50050 00400 50060 70300 00530 00310 31616 00600 00610 00625 00630 00620 00615 00665 00940 : O d �O O _ xU m N W °° E p ;rn o Z m C o Q �d o Yz w � s O o NolLL a 24-hr I hrs GPD su I mg/L mg/L mg/L I mg/L #/100 mL mg/L mg/L mg/L mg/L I mg/L mg/L mg/L I mg/L 1 29,857 2 30,657 3 08:00 5 36,048 6.65 0.4 4 08:00 5 26,740 6.37 0.7 5 08:00 5 27,552 6.32 0.6 6 08:00 5 36,239 6.31 0.6 7 8:00 5 42,086 6.86 1.1 8 29,824 9 27,584 10 08:00 5 42,172 6.2570.4 0.2 11 08:00 5 30,713 6.26 360 142 32.4 64 34.8 0.64 13.7 21.1 21.1 <0.02 12.7 65.6 12 08:00 5 23,703 6.39 1.2 13 08:00 5 29,576 6.32 1.1 141 08:00 5 36,104 6.52 1.2 15 38,899 16 34,277 17 08:00 5 36,750 6.73 0.2 18 08:00 5 38,386 6.62 0.8 19 08:00 5 43,512 6.6 1.2 201 08:00 5 40,989 6.63 0.8 21 08:45 5 41,909 6.59 1.2 22 45,213 23 49,731 24 08:00 5 50,596 6.27 0.3 25 08:00 5 44,654 6.63 0.8 261 08:00 5 37,027 6.75 0.7 27 08:00 5 42,701 6.61 0.8 28 08:00 5 37,479 6.31 0.7 29 21,455 30 27,532 31 Average: 35,999 0.75 360.00 142.00 32.40 64.00 34.80 0.64 13.70 21.10 21.10 0.00 12.70 65.60 Daily Maximum: 50,596 6.86 1.20 360.00 142.00 32.40 64.00 34.80 0.64 13.70 21.10 21.10 0.02 12.70 65.60 Daily Minimum: 21,455 6.25 0.20 360.00 142.00 32.40 64.00 34.80 0.64 13.70 21.10 21.10 0.02 12.70 65.60 Sampling Type: Monthly Avg. Limit: Daily Limit: Sample Frequency: Continuous 5x/Week 5X/Week Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly Monthly 3X/year Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Sampling Person(s) Certified Laboratories Name: Sam Perry 11 Name: Greener EHS Solutions, LLC Name: Name: Pace Analytical Does all monitoring data and sampling frequencies meet the requirements in Attachment A of your permit? ❑ Compliant El Non -Compliant If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. The Monthly average flow exceeded the permitted flow of 24,400 gpd. The permitted application rate was not exceeded. The flow meter was calibrated on June 27, 2023 and the meter was reading significantly low before the calibration. This was noted on the June 2023 NDMR. The plant is in the process of an upgrade to increase the capacity as well as investigating extraneous flow for 1/1 and leaking fixtures. Lab Qualifiers, 6/11/2024, BOD, 5-Day, B3 - The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L and Total Phosphorus, M1 - Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Operator in Responsible Charge (ORC) Certification Permittee Certification ORC: Sam Perry Permittee: MHC TT, LP Certification No.: 1014038 Signing Official: George Gudgeon Grade: SI Phone Number: 919-548-2381 Signing Official's Title: Sr. Vice President Has the ORC changed since the previous NDMR? ❑ Yes F11 No Phone Number: 312-279-1400 Permit Expiration: 10/31 /2027 r� 7/30/2024 LL 7/29/2024 Sam Perry (Jut 30, 2024 :28 EDT) -- Signature Date Signature Date By this signature, I certify that this report is accurrate and complete to the best of my knowledge. I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that all qualified personnel properly gathered and evaluated the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Mail Original and Two Copies to: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 L:21 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E ace Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 June 25, 2024 Amanda D. Grenier Greener EHS Solutions 21 Selby Ct. Holly Springs, NC 27540 RE: Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 Dear Amanda Grenier: Enclosed are the analytical results for sample(s) received by the laboratory on June 11, 2024. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Matthew Brainard matthew.brainard@pacelabs.com 704-977-0942 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E ace Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 CERTIFICATIONS South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 VirginiaNELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92735831001 GREENER EHS/EFFLUENT SM 9222D-2015 KDF 1 PASI-C SM 2540C-2015 AGM 1 PASI-A SM 2540D-2015 JMH1 1 PASI-A SM 521OB-2016 MDM 1 PASI-A TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 MFO 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A SM 4500-CI-E-2011 Zip 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E ace Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 Sample: GREENER EHS/EFFLUENT Lab ID: 92735831001 Collected: 06/11/24 10:30 Received: 06/11/24 13:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual MBIO 9222D Fecal Coliform CHT Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Charlotte Fecal Coliforms 64.0 CFU/100 mL 1.0 1 06/11/24 16:17 06/12/24 14:36 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services -Asheville Total Dissolved Solids 360 mg/L 25.0 1 06/14/24 17:02 2540D Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services -Asheville Total Suspended Solids 142 mg/L 69.4 1 06/15/24 11:41 5210B BOD, 5 day Analytical Method: SM 521OB-2016 Pace Analytical Services -Asheville BOD, 5 day 32.4 mg/L 2.0 1 06/13/24 06:07 06/18/24 02:53 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 34.8 mg/L 0.040 1 06/25/24 09:45 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Ammonia 0.64 mg/L 0.10 1 06/24/24 18:50 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 13.7 mg/L 0.50 1 06/24/24 20:09 06/25/24 05:53 7727-37-9 353.2 Nitrogen, NO2/NO3 unpres Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Nitrate 21.1 mg/L 0.10 5 06/12/24 03:25 14797-55-8 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 12.7 mg/L 0.25 5 06/24/2418:47 06/25/2413:03 7723-14-0 4500 Chloride Analytical Method: SM 4500-CI-E-2011 Pace Analytical Services -Asheville Chloride 65.6 mg/L 2.0 2 06/19/2412:39 16887-00-6 Date: 06/25/2024 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. B3 Page 4 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 860669 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF) - CHT Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92735831001 METHOD BLANK: 4438973 Matrix: Water Associated Lab Samples: 92735831001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 06/12/24 14:36 SAMPLE DUPLICATE: 4438974 Parameter Fecal Coliforms 92735847001 Dup Units Result Result RPD Qualifiers CFU/100 mL 2.0 ND Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 861436 Analysis Method: SM 2540C-2015 QC Batch Method: SM 2540C-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4442834 Associated Lab Samples: 92735831001 Parameter Units Total Dissolved Solids mg/L LABORATORY CONTROL SAMPLE: 4442835 Parameter Units Total Dissolved Solids mg/L SAMPLE DUPLICATE: 4442836 Parameter Units Total Dissolved Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 25.0 06/14/2416:53 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 252 101 90-110 92735539001 Dup Result Result RPD Qualifiers 51.0 47.0 8 SAMPLE DUPLICATE: 4442837 92736283007 Dup Parameter Units Result Result Total Dissolved Solids mg/L 727 745 RPD Qualifiers 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 861737 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4444431 Associated Lab Samples: 92735831001 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 4444432 Parameter Units Total Suspended Solids mg/L SAMPLE DUPLICATE: 4444484 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 06/15/2411:38 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 252 101 90-110 92735817003 Dup Result Result RPD Qualifiers 267 249 7 SAMPLE DUPLICATE: 4444485 92735823001 Dup Parameter Units Result Result Total Suspended Solids mg/L 262 246 RPD Qualifiers 6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 861051 Analysis Method: SM 521 OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4440994 Associated Lab Samples: 92735831001 Parameter Units BOD, 5 day mg/L LABORATORY CONTROL SAMPLE: 4440996 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 06/18/24 02:15 B3 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 198 226 114 84.6-115 SAMPLE DUPLICATE: 4440997 92736232001 Dup Parameter Units Result Result BOD, 5 day mg/L 554 478 RPD Qualifiers 15 B3 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 862898 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4449439 Associated Lab Samples: 92735831001 Parameter Units Nitrogen, Ammonia mg/L LABORATORY CONTROL SAMPLE: 4449440 Parameter Units Nitrogen, Ammonia mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 06/24/24 18:08 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 5 5.1 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4449441 4449442 MS MSD 92735606001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.2 5.1 103 103 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4449443 4449444 MS MSD 92735606002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.20 5 5 5.3 5.3 103 103 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 863544 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4452435 Associated Lab Samples: 92735831001 Parameter Units Nitrogen, Kjeldahl, Total mg/L LABORATORY CONTROL SAMPLE: 4452436 Parameter Units Nitrogen, Kjeldahl, Total mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.50 06/25/24 05:35 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 10 10.3 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4452437 4452438 MS MSD 92735679001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 10.3 10 10 19.4 19.3 92 91 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4453442 4453443 MS MSD 92735819001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.1 10 10 11.8 11.8 107 107 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 860734 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4439299 Associated Lab Samples: 92735831001 Parameter Units Nitrogen, Nitrate mg/L LABORATORY CONTROL SAMPLE: 4439300 Parameter Units Nitrogen, Nitrate mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.020 06/12/24 02:44 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 1.5 1.6 106 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4439301 4439302 MS MSD 92735710006 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Nitrate mg/L ND 1.5 1.5 1.5 1.5 102 101 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 863563 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4452497 Associated Lab Samples: 92735831001 Parameter Units Phosphorus mg/L LABORATORY CONTROL SAMPLE: 4452498 Parameter Units Phosphorus mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 06/25/24 09:45 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 2.5 2.6 103 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4452499 4452500 MS MSD 92735900001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.28 2.5 2.5 1.2 1.1 35 34 90-110 1 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4452501 4452502 MS MSD 92735920002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 3.7 2.5 2.5 5.9 5.8 87 84 90-110 1 M1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E Pace Analytical Services, LLC �ace� 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 QC Batch: 862257 Analysis Method: SM 4500-CI-E-2011 QC Batch Method: SM 4500-CI-E-2011 Analysis Description: 4500 Chloride Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92735831001 METHOD BLANK: 4446448 Associated Lab Samples: 92735831001 Parameter Units Chloride mg/L LABORATORY CONTROL SAMPLE: 4446449 Parameter Units Chloride mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 1.0 06/19/2412:24 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 20 20.3 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4446450 4446451 MS MSD 92735928003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 16.9 10 10 27.0 26.9 101 100 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4446452 4446453 MS MSD 92735928004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Chloride mg/L 15.3 10 10 25.0 24.9 97 96 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 13 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E ace Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: FOREST LAKE -QUARTERLY Pace Project No.: 92735831 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS B3 The dissolved oxygen depletion of the dilution water blank exceeded 0.2 mg/L. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 06/25/2024 02:35 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E ace Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: FOREST LAKE -QUARTERLY 92735831 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92735831001 GREENER EHS/EFFLUENT SM 9222D-2015 860669 SM 9222D-2015 860670 92735831001 GREENER EHS/EFFLUENT SM 254OC-2015 861436 92735831001 GREENER EHS/EFFLUENT SM 2540D-2015 861737 92735831001 GREENER EHS/EFFLUENT SM 521OB-2016 861051 SM 521OB-2016 861101 92735831001 GREENER EHS/EFFLUENT TKN+NO3+NO2 863852 Calculation 92735831001 GREENER EHS/EFFLUENT EPA 350.1 Rev 2.0 1993 862898 92735831001 GREENER EHS/EFFLUENT EPA 351.2 Rev 2.0 1993 863544 EPA 351.2 Rev 2.0 1993 863774 92735831001 GREENER EHS/EFFLUENT EPA 353.2 Rev 2.0 1993 860734 92735831001 GREENER EHS/EFFLUENT EPA 365.1 Rev 2.0 1993 863563 EPA 365.1 Rev 2.0 1993 863808 92735831001 GREENER EHS/EFFLUENT SM 4500-CI-E-2011 862257 Date: 06/25/2024 02:35 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 15 of 19 me%"& P'\1\/ 'm a ft `A wwww - .w Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E t_Sample Condition Upon Receipt race � Effective Date: 4/26/202-4 10:14:05 AM Laboratory receiving samples: Asheville ❑ Eden[:] Greenwood ❑ Huntersville ❑' Raleigh❑ Mechanicsville❑ Atlanta)-lSample Condition ke-...---• -r' Upon Receipt Client Name: Project #: WO# : 92735831 El Courier: � PFed Ex UPS USPS Client IIIIII 1111111111111111 ❑ Commercial ace ❑ Other. 92735831 Custody Seal Present? El Yes ON Seals Intact? ❑Yes ❑No [3-N/A -✓1� Packing Material: ❑ Bubble Wrap ❑ Bubble Bags None ❑ Other Thermometer✓ ❑ rk Gun ID: �� Type of Ice: L1 Wet ❑ Blue Correction Factor: Cooler Temp: ? Add/Subtract (°C) Cooler Temp Corrected ("C > > USDA Regulated Soil ( L1 N/A water sample) Did samples originate in a quarantine zone within the United States: CA, NY, or SC frhPrk mancl? F l Ypc 17 NJ. Date/Initials Person Examining Contents: Biological Tissue Frozen? [Dyes ❑ No ❑"N/A ❑ None Temp should be above freezing to VC ❑ Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a foreign source (internationally, ;-11..A:- u-...-:: -J n , M- I"1. Comments/Discrepancy: Chain of Custody Present? Dles, ❑ No ] N/A 1. Samples Arrived within Hold Time? Qfes ❑ No ❑ N/A Z, Short Hold Time Analysis (<72 hr.)? Yes ❑ No ❑ N/A 3. Rush Turn Around Time Requested? ❑ Yes -0-ko ❑ N/A 4- Sufficient Volume? Yes ❑No ❑N/A S. Correct Containers Used? -Pace Containers Used? Ef'yes tJ res ElNo ❑ No ❑ N/A ❑ N/A 6. Containers Intact? 13Yes [I No ❑N/A 7. Dissolved analysis: Samples Field Filtered? ❑Yes ❑No EJN/w 8, Sample Labels Match COC? -Includes Datelrime/ID/Analysis Matrix: ❑Yes ❑ No ❑ N/A 9. Headspace in VOA Vials (>5-6mm)? ❑ Yes ❑ No -EJi/A 10. Trip Blank Present? Trip Blank Custody Seals Present? ❑Yes ❑ Yes ❑No EltJ No Eal /A N/A 11. COMMENTS/SAMPLE DISCREPANCY CLIENT NOTIFICATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers: Date/Time: Date: Date: Field Data Required? U Yes LJ No Qualtrax ID: 69614 Paae 1 of 2 Page 16 of 19 Docusign Envelope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E 4—Sample Condition Upon Receipt race Effective Date: 4/26/2024 10:14:05 AM *Check mark top half of box if pH and/or dechlorination is verified and within the WOu : 92735831 acceptance range for preservation samples. Project # Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg pM: MWB Due Date: 06/25/24 `Bottom half of box is to list number of bottles CLIENT: 92-Greener Check all unpreserved Nitrates for chlorine i Laboratory Receiving Location: Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ mechanicsvilleLJ Atlanta❑ Kernersville❑ Client Profile Number Notes n a. O�_ z O ¢ z r n n ry Z %, Cp 4 E r S E o m c E m a E a _ a E m n E o a E m d E m o E =+ V' 3 c <` a E .= a F. E a 4 to a Q a E < o O > o O > O� > O > Of � O > T o d N $ m n (D > .' N Vl N m m F O e < O1 o CC i I 2 3 n 6 F7s 3 9 N, 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot d - - --•�•,��•- -ram •.ram � .—Ei ..�—tU—'Ji— --?ICJJ1UC leLuFryUill ucarmwn1 De senttothe North (.aroh na D EN R Ce rtificat ion Office (i.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Qualtrax ID: 69614 Pace 2 of 2 Page 17 of 19 Docusign Enveljjope ID: C34575CF-57FB-4E38-AD04-AAOD90ED823E lArFraceAnalytical Sample Receiving Non -Conformance Form (NCF) Date: Evaluated by: AffiWO# : 92735831 e Client: _ W - PM: MWB Due Date: 06/25/24 I CLIENT: 92-Greener 1. If Chain -of -Custody (COC) is not received: contact client and if necessary, fill out a COC and indicate that it was filled out by lab personnel. Note issues on this NCF. 2. If COC is incomnlete_ check annlicahle issues helow and add details where annrnnriate- J' Collection dale/time missing or Analyses or analytes: missing or Samples listed on COC do not match samples incorrect clarification needed received (missing, additional, etc. Sample IDs on COC do not match sample labels Required trip blanks were not received Required signatures are missing GommentslDetails/Other Issues not listed above: 3. SamDle intearitv issues: check annlicable issues below and add details where annrnnrinte- Samples: Condition needs to be brought to Samples: Past holding time lab ersonnel's attention details below Preservation: Improper Temperature: not within acceptance criteria (typically Samples: Not field filtered Containers: Broken or compromised 0-6C Samples: Insufficient volume received Containers: Incorrect Temperature: Samples arrived frozen Samples: Cooler damaged or Custody Seals: Missing or compromised on compromised sam les, trip blanks or coolers Vials received with improper heads ace Samples: contain chlorine or sulfides Packin Mat erial:Insufficient/Im proper Other: Comments/Details: 4. If Samples not Dreserved Droperly and SamDle Receivina adiusts nH. add details helnw- Sam le ID: Date/Time: Amount/type pres added: Preserved by: Initial and Final H: Lot # of pres added: Sample ID: Date/Time: Amount/typa res added: Preserved by: Initial and Final H: Lot # of pres added: Sample ID: Date/Time: I Amount/type pres added: Preserved by: Initial and Final H: I Lot # of pres added: 5. Client Contact: If client is contacted for any issue listed above, fill in details below: Client: Contactedper: PM Initials: Date/Time: Client Comments/Instructions: F-ALL-C-011-rev.00, 05Jul2018 Page 18 of 19 Docusign i z T �1 n A 0 0 10 N 0 N Envelope nID: 34575CF-57FB-4E38-AD04-AAOD90ED823E °' 3 o 0 _ = o a� - - n a c > a i _ o o � O m - n ^ v ' a- 3 3 3 o 3 m z 9. o iz n n n o m d m D o T x w o n O cn o rt n 0 O 3 o v a 0 a � O j R ,p m CL < O- p — �j f _ � p �' '�° 9 n W R O V m twit z N o n � v 3 1 9 3 � 13 o "o _ a?' a A= 'e D 4 N o a w v N m g o y = a u z o W g �V i C VV c a m 3 a O o a ° o D to " a a O v D 0 n' m O = 3 3 = f5 ( t ` O O a O a jn ■ a O z O 3 Z n v � f — A d _ _ 0 0 N O r; = oz PF M M 9 — _ a 3 a N , m a _ n R � N c 0 Ammonia/ T. Phos 3 3 BOD 5-day ❑■'li[A� ■❑ Chloride � y�- ,J � c Fecal Coliform MF, M-FC n r� •��1 r� o v v O 3 0 o f. .�, ■ 3 3 )3 = v c Nitrate D — r r _a 0 m a TDS y O a a 5 C (n m o 2 2 L O/ o �-- ° TSS a m f0 z 1 = a A 0 D o 2 a a Total Nitrogen 8 TKN m x to O 2 a v 00 0 0 3 3 00 Lab Use Onl 3 ti _ en co Fr K y a� _ co o, -- V Cn 0 00 3 c—' 3 3 o 3— sV8 ja 0 ? a nD 0 D � Preservation nonconformance Identified for - -Pf, s - Page 19 of 19