WQ0031712_2023 Residual Annual Report (Corrected)_20240610

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR)* WQ0031712
Applicant/Permittee Davidson Water, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
..................................................................................................................................................................................................................................................................................... ... ... ... ... ... .. ... ... ... ... ..
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0031712
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 969, Welcome, NC 27374
Facility Name*
Davidson Water Class A Residuals Program
Please provide comments/notes on your current submittal below.
Re -submitting corrected report due to a minor rounding error.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Davidson Water Annual Report - WQ0031712.pdf 5.77MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 6/10/2024

--Resources, Inc.
Davidson Water, Inc.
2023 Annual Report
Residuals Land Application
Permit No. WQ0031712
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville RD — Mocksville, NC 27028

February 27, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report — Davidson Water, Inc.
Treatment and Land Application of Residuals
Permit No. WQ0031712
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 257.7 dry tons of wastewater residuals to
29.01 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Brent Collins
Director of Technical Services
brent.collinsa,emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0031712 FACILITY NAME: Davidson Water, Inc.
PHONE: [phone] COUNTY: Davidson OPERATOR: Davidson Water, Inc.
FACILITY TYPE (please check one): ❑ Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
B Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes ❑ No 10 If No skip parts A, B, C and certify form below
Part A*: Part B*:
Sources s ( include NPDES # if Volume (dry tons) Recipient Information
Month Amendment/
applicable) Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s)
January
February
March
April Davidson Water 87.35
May Davidson Water 173.81
June
July
August
September
October
November
December
87.35 Roger Spillman 87.35 soil amendment
173.81 Roger Spillman 173.81 soil amendment
Total from FORM DMSDF (sup) 0 0 0 0
Totals: Annual (dry tons): 0 261.16 261.16 261.16
Amendment(s) used: I Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)0 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit © Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No — 0 If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
On lyl�f 02/27/21 fCDoh 02/27/2,
Ron Sink (Feb 27, 202410:45 EST) Craig Koontflreb 27, 202409:33 EST)
Signature of Permittee Date Signature of Preparer* * Date
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0031712
Davidson Water, Inc.
PWS#0229025
Davidson Water, Inc.
Laboratory: 1)
2)
3)
4)
5)
Waypoint Analytical
Conc.
Sample or Composite Date
Parameter
Limit
(mg/kg)
(mg/kg)a
1/9/23
4/12/23
5/15/23
Percent Solids (%)
NA
22.9
4.24
29.4
Arsenic
75
1.05
5.22
9.56
Cadmium
85
10.5
1.41
6.94
Copper
4,300
26.4
23
51
Chromium
NA
26.7
38
27.3
Lead
840
13.9
18.5
15
Mercury
57
0.0274
0.472
0.103
Molybdenum
75
5.07
6.54
6.26
Nickel
420
12.3
16
27.4
Selenium
100
7.69
18.8
21.8
Zinc
7,500
51.1
68.9
46.9
Total Phosphorus
NA
2920
3000
2400
TKN
NA
12000
61300
11700
Ammonia -Nitrogen
NA
267
3390
531
Nitrate and Nitrite
NA
20.9
21.7
44.9
a For surface disposal facilities
the ceiling
concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ckvlG koodf 02/27/24
Craig KooAs (Feb 27, 2024 09:33 EST)
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0031712
Facility Name:
Davidson Water, Inc.
Residual Source
PWS#0229025
NPDES # or WQ#:
WWTP Name:
Davidson Water WTP
Residual Analysis Data
Parameter
(mg/kg)
1/9/23
4/12/23
5/15/23
Aluminum
21000
33300
26000
Calcium
2480
1360
850
Magnesium
847
1180
1020
pH
5.2
6.1
5.9
Potassium
699
1130
850
Sodium
178
380
263
SAR
0.38
0.37
0.78
PAN
1328
7508
1427
Laboratory: 1)
2)
3)
4)
5)
Sample or Composite Date
Waypoint Analytical
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
C-aia kood r 02/27/24
Craig 27, 2024 J9:33 EST)
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davidson Water, Inc. Total Dry Tons Applied (Annual): 182.53
Permit #: WQ0031712 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series: WeC
Acres Used: 22.98 Acres Permitted: 22.98 Site #: DV8 Field #: 10
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
1
J J J
5 6
J
J
J
10
11
12
Com-
Davidson
Piedmont
Water
Water
posite
4/12/23
4/5/23
Date
% Solids
4.24
20.7
Arsenic
5.22
5.69
Cadmium
1.41
4.1
Copper
23
71.6
Chromiwn
38
13.8
Lead
18.5
4.27
Mercury
0.472
0.102
Molyb-
6.54
13.6
denum
Nickel
16
16.3
Selenium
18.8
7.58
Zinc
68.9
19.2
Total
Phos-
3000
1210
phorus
Annual Heavy Metal Field Loadings (Calculated
in lbs/acre):
Total
1
2 3 4
5 6
7
10 J
Ll_j
12
_.2j
DT/Ac./
App.
14
Event
3.80
4.14
Arsenic
0.040
0.047 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.087
Cadmium
0.011
0.034 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.045
Copper
0.175
0.593 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.768
Chromiun 1
0.289
0.114 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.403
Lead
0.141
0.035 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.176
Mercury
0.004
0.001 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.004
Molyb-
0.050
0.113 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.162
denum
Nickel
0.122
0.135 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.257
Selenium
0.143
0.063 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.206
Zinc
0.524
0.159 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.683
Total
Phos-
22.806
10.024 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
32.830
phorus
'tI certify,
under
penalty of law, that this document was prepared under my cirection
or supervision
in accordance with
a system designed to assure that qualified personnel properly
gathered and evaluated
the information submitted. I am
aware that there
are significant penalties for submitting false information, including
the possibility of
fines and
imprisonment for knowing violations".
zl-z
2/18/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davidson Water, Inc
WQ Permit #:
WQ0031712 Field #: 10 Acres Utilized:
22.98
Land Owner: Roger Spillman
Annual Dry Tons Applied:
182.53
Site #: DV8 Acres Permitted:
22.98
Operator: Roger Spillman
Predominant Soil Series:
WeC Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay
Crop 1 Max. PAN:
106
Crop 2 Name: Crop 2 Max. PAN:
Volume applied Volume
Residual Sources Soil
Precip. a
o 4 Z Nitrate
Name of Crop Type
(enter one) Solids/ % Applied per
(NPDES #, WQ#, Cond.
past 24 '5
w w w `; TKN o 5 and PAN Applied
Receiving Residual
Liquid Solids Acre
Fert., Animal (may'
Firs. w
oa o ( lbs/acre)
* N CD CD Nitrite
Application
Q
Wet,
Waste, etc)
*o'
*�
Cu. Yds Gallons (Dry Tons/Ac)
Moist)
inches
0 0 mg/kg mg/kg mg/kg Crop 1 Crop 2
Crop 1 Crop 2
4/13 78000 4.24 0.600
Davidson Water Dry
<.5" S
0.5 0.1 61300 3390 21.7 9.011 NA
Fescue
4/17 58500 4.24 0.450
Davidson Water Dry
<.5" S
0.5 0.1 61300 3390 21.7 6.758 NA
Fescue
4/18 110500 4.24 0.850
Davidson Water Dry
<.5" S
0.5 0.1 61300 3390 21.7 12.766 NA
Fescue
4/19 123500 4.24 0.950
Davidson Water Dry
<.5" S
0.5 0.1 61300 3390 21.7 14.268 NA
Fescue
4/20 123500 4.24 0.950
Davidson Water Dry
<.5" S
0.5 0.1 61300 3390 21.7 14.268 NA
Fescue
5/9 351 20.7 2.663
Piedmont Water Dry
<.5" S
0.5 0.4 11400 882 4.74 24.779 NA
Fescue
5/11 117 20.7 0.888
Piedmont Water Dry
<.5" S
0.5 0.4 11400 882 4.74 8.260 NA
Fescue
5/12 78 20.7 0.592
Piedmont Water Dry
<.5" S
0.5 0.4 11400 882 4.74 5.506 NA
Fescue
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0 0 0.000
Residuals Applications totals
on FORM FSF
supp ( attach FORM FSF supp to this form): 0.000 0.000
TOTALS:
546 494000 As
Cd Cu Cr
Pb Hg
Mo Ni Se Zn P 95.616 0.000
Lime Applied
Annuallbs/acre 0.087
0.045 0.768 0.403
0.176 0.004
0.162 0.257 0.206 0.683 32.830
Date lbs/ac
Prior Years Cumulative lbs/ac 0
0 0 0
0 0
0 0 0 0
Current Cumulative lbs/ac 0.087
0.045 0.768 0.403
0.176 0.004
0.162 0.257 0.206 0.683
Permitted C. P. L. R.**** 36
34 1338
267 15
374 89 2498
Permit PAN Limit Ist/2nd Crop
1 106
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that
qualified personnel properly gathered and evaluated
the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines
and imprisonment for
knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
2/18/2024
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested
-0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Davidson Water, Inc. Total Dry Tons Applied (Annual): 207.81
Permit #: WQ0031712 Cation Exchange Capacity (non 503 only):
Operator: Roger Spillman Owner: Roger Spillman Predominant Soil Series: RnC
Acres Used: 6.03 Acres Permitted: 6.03 Site #: DV8 Field #: 11
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
t
21 31 41
5 6
J
J
J
10
Lid
12
Com-
Davidson
Piedmont
Water
Water
posite
4/12/23
4/5/23
Date
% Solids
4.24
20.7
Arsenic
5.22
5.69
Cadmium
1.41
4.1
Copper
23
71.6
Chromiwn
38
13.8
Lead
18.5
4.27
Mercury
0.472
0.102
Molyb-
6.54
13.6
denum
Nickel
16
16.3
Selenium
18.8
7.58
Zinc
68.9
19.2
Total
Phos-
3000
1210
phorus
Annual Heavy Metal Field Loadings (Calculated
in lbs/acre):
Total
1
2 3 4
5 6
7
10 J
Ll_j
12
_.2j
DT/Ac./
App.
Event
28.83
5.64
14
Arsenic
0.301
0.064 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.365
Cadmium
0.081
0.046 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.128
Copper
1.326
0.807 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.133
Chromiun 1
2.191
0.156 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.346
Lead
1.067
0.048 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.115
Mercury
0.027
0.001 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Molyb-
0.377
0.153 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.530
denum
Nickel
0.922
0.184 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.106
Selenium
1.084
0.085 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.169
Zinc
3.972
0.216 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
4.189
Total
Phos-
172.950
13.644 0.000 0.000
0.000 0.000
0.000
0.000
0.000
0.000
0.000
0.000
186.594
phorus
'tI certify,
under
penalty of law, that this document was prepared under my cirection
or supervision
in accordance with
a system designed to assure that qualified personnel properly
gathered and evaluated
the information submitted.
I am
aware that there
are significant penalties for submitting false information, including
the possibility of
fines and
imprisonment for knowing violations".
zl-z
2/18/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Davidson Water, Inc
WQ Permit #: WQ0031712 Field #: 11 Acres Utilized: 6.03
Land Owner: Roger Spillman
Annual Dry Tons Applied: 207.81
Site #: DV8 Acres Permitted: 6.03
Operator: Roger Spillman
Predominant Soil Series:
RnC Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay
Crop 1 Max. PAN: 141
Crop 2 Name: Crop 2 Max. PAN:
Volume applied Volume
Residual Sources Soil Precip. a
o 4 Z Nitrate Name of Crop Type
(enter one) Solids/ % Applied per
(NPDES #, WQ#, Cond. past 24 '5
w w w `; TKN 8 5 and PAN Applied Receiving Residual
Liquid Solids Acre
Fert., Animal (may' Iks. w
oa o ( lbs/acre)
* N CD CD Nitrite Application
Q
Wet, *o'
Waste, etc)
*�
Cu. Yds Gallons (Dry Tons/Ac)
Moist) inches
0 0 mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2
5/9 312 29.4 12.811
Davidson Water Dry <.5" S
0.5 0.1 11700 531 44.9 36.571 NA Fescue
5110 390 29.4 16.014
Davidson Water Dry <.5" S
0.5 0.1 11700 531 44.9 45.713 NA Fescue
5111 195 20.7 5.638
Piedmont Water Dry <.5" S
0.5 0.4 11400 882 4.74 52.462 NA Fescue
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0.000
0.000 0.000
0 0 0.000
Residuals Applications totals on FORM FSF
supp ( attach FORM FSF supp to this form): 0.000 0.000
TOTALS:
897 0 As
Cd Cu Cr Pb Hg
Mo Ni Se Zn P 134.746 o.000 Lime Applied
Annuallbs/acre 0.365
0.128 2.133 2.346 1.115 0.028
0.530 1.106 1.169 4.189 186.594 Date lbs/ac
Prior Years Cumulative lbs/ac 0
0 0 0 0 0
0 0 0 0
Current Cumulative lbs/ac 0.365
0.128 2.133 2.346 1.115 0.028
0.530 1.106 1.169 4.189
Permitted C. P. L. R.**** 36
34 1338 267 15
374 89 2498
Permit PAN Limit Ist/2nd Crop
1 141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated
the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines
and imprisonment for knowing violations."
Z-Z
*Application Method: S - Surface, IN - Injection, INC - Incorporation
4;5�0.
2/18/2024
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

1 /9/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 178 40.762 23 1.772261
Calcium 2480 567.92 20 28.396
Magnesium 847 193.963 12 16.16358
Percent Solids 22.9
SAR 0.38
SAR Na+
l2 (C,,z+ + M9z+)
1.77226
0.5( 28.396 2 + 16.16358 2 )

4/12/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 380 16.112 23 0.700522
Calcium 1360 57.664 20 2.8832
Magnesium 1180 50.032 12 4.169333
Percent Solids 4.24
SAR 0.37
SAR Na+
l2 (C,,z+ + M9z+)
0.70052
0.5( 2.8832 2 + 4.16933 2 )

5/15/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 263 77.322 23 3.361826
Calcium 850 249.9 20 12.495
Magnesium 1020 299.88 12 24.99
Percent Solids 29.4
SAR 0.78
SAR Na+
l2 (C,,z+ + M9z+)
3.36183
0.5( 12.495 2 + 24.99000 2 )

Waypointo
ANALYTICAL
1 /18/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-010-0011
Client Project Description: Davidson Water Sludge
Lexington, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/10/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypoi t
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program - NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program - NELAP
LA037
12/31/2023
Louisiana
State Program - NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
02/11/2023
Texas
State Program - NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program - NELAP
460181
09/14/2023
Page of 00001/23-010-0011
Page 2 of 9

Waypoint,
ANALYTICAL
Report Number:
Client Project Description:
Lab No Client Sample ID
91174 Davidson Water
dw 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample Summary Table
23-010-0011
Davidson Water Sludge
Lexington, INC
Matrix
Solids
Date Collected
O1/09/2023 09:15
Date Received
O1/10/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Davidson Water Sludge
Lab Report Number: 23-010-0011
Date: 1/18/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 91048 (Grab)
Analyte: Aluminum
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Calcium
QC Batch No: 1-658650/1-657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Iron
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Potassium
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 91048 (Grab)
Analyte: Magnesium
QC Batch No: 1-658650/1-657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Manganese
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 91048 (Grab)
Analyte: Sulfur
QC Batch No: L658387/L657717
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Page 4 of 9

Waypoint
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample 91191 (Annapolis Truck Chute)
Analyte: Mercury
QC Batch No: 1-658555/1-658246
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

0
Waypoi nt, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Davidson Water Sludge
Brent Collins Report Date : 01/18/2023
755 Yadkinville Rd Information : Lexington, NC Received : 01/10/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-010-0011 REPORT OFANALYSIS Project Manager
Lab No : 91174 Matrix: Solids
Sample ID : Davidson Water Sampled: 1/9/2023 9:15
Test Results Units MDL MQL DF Date / Time By Analytical
Analyzed Method
Moisture
77.1
%
1
01/12/23 16:03
FMM
SW-DRYWT
Ammonia Nitrogen
2673
mg/Kg -
dry
69.9
437
1
01/18/23 09:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<20.9
mg/Kg -
dry
20.9
20.9
1
01/17/23 13:55
ZBD
4500NO3F-2016
Organic N
117003
mg/Kg -
dry
69.87
436.7
1
01/17/23 10:45
CALCULATION
pH
5.2
S.U.
1
01/17/2315:30
SAR
9045D
Total Solids
22.9
%
0.010
0.010
1
01/12/23 16:03
FMM
254OG-2011
Total Volatile Solids
24.6
%
0.010
0.010
1
01/12/23 16:03
FMM
254OG-2011
Total Kjeldahl Nitrogen
12000
mg/Kg -
dry
43.7
1090
1
01/17/23 10:45
JPJ
>M-4500-NH3C-TKP
Phosphorus
2920
mg/Kg -
dry
12.1
21.8
1
01/12/23 22:22
TJS
6010D
Aluminum
21000
mg/Kg -
dry
20.2
21.8
1
01/12/23 22:22
TJS
6010D
Arsenic
<1.05
mg/Kg -
dry
1.05
2.18
1
01/12/23 22:22
TJS
6010D
Cadmium
10.5
mg/Kg -
dry
0.0873
0.437
1
01/12/23 22:22
TJS
6010D
Calcium
2480
mg/Kg -
dry
169
218
1
01/12/23 22:22
TJS
6010D
Chromium
26.7
mg/Kg -
dry
1.03
1.09
1
01/12/23 22:22
TJS
6010D
Copper
26.4
mg/Kg -
dry
1.35
2.18
1
01/12/23 22:22
TJS
6010D
Iron
342000
mg/Kg -
dry
742
873
20
01/13/23 20:15
TJS
6010D
Lead
13.9
mg/Kg -
dry
0.786
1.31
1
01/12/23 22:22
TJS
6010D
Magnesium
847
mg/Kg -
dry
11.3
21.8
1
01/12/23 22:22
TJS
6010D
Manganese
217
mg/Kg -
dry
1.42
2.18
1
01/12/23 22:22
TJS
6010D
Mercury
<0.0274
mg/Kg -
dry
0.0274
0.629
1
01/13/23 16:21
JTR
7471A
Molybdenum
5.07
mg/Kg -
dry
0.589
1.09
1
01/12/23 22:22
TJS
6010D
Nickel
12.3
mg/Kg -
dry
0.524
1.09
1
01/12/23 22:22
TJS
6010D
Potassium
699
mg/Kg -
dry
27.0
43.7
1
01/12/23 22:22
TJS
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 6 of 9

Waypoi nt,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Davidson Water Sludge
Brent Collins
Report Date : 01/18/2023
755 Yadkinville Rd
Information : Lexington, NC
Received : 01/10/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-010-0011
REPORT OFANALYSIS
Project Manager
Lab No : 91174
Matrix: Solids
Sample ID : Davidson Water
Sampled: 1/9/2023 9:15
Test
Results
Units MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
7.69
mg/Kg - dry 1.40
2.18 1 01/12/23 22:22 TJS 6010D
Sodium
178
mg/Kg - dry 56.8
109 1 01/12/23 22:22 TJS 6010D
Zinc
51.1
mg/Kg - dry 3.54
5.46 1 01/12/23 22:22 TJS 6010D
Sulfur
3310
mg/Kg - dry 22.6
43.7 1 01/12/23 22:22 TJS 6010D
Sodium Absorption Ratio
0.37
Ratio 0.01
0.01 1 01/12/23 22:22 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

WaypANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-010-0011
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 Other:
0 UPS 0 Client 0 Courier
Thermometer ID:
135
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
# Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
# N/A
Trip Blanks received with VOAs
0 Yes
0 No
# N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
# N/A
F_ High concentration container (48 hr)
F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
# No
Comments:
Signature: IlEmily M. Peterson
Date & Time: 101 /10/2023 08:59:11
Page 8 of 9

ro
a
(D
0
t-h
Client Name/Address
EMA Resources Inc
755 Yadkinville Rd
Mocksville, NC 27028
Project Description
Project Number
Client Project Manager/Contact Billing Information s
Brent Collins Account #46245
For Laboratory Use Only
Project/Site Location (City/State) ch
IdRUSH — Additional arges apply Met d of Shl ment
Special Detection Urrials) Fed Ex �p�_jJUPS MUSPS
Date Results Needed Courier O Client Drop Off
`i PC MS41111104 M Other
Project Manager Phone If Project Manager Email Purchase Order Number
336-399-3646 brent Collins@emaresources corn 16QV4 df0A v .4-q.-
Wa oint
ANALYTICAL
2790 Whitten Road
Memphh, TN 38133 Unless noted, all containers
[phone] per Table I I of 40 CFR Part
136.
Date Time Sample Identification
For Laboratory Use Only
Ice
Custody Lab Comments
Seals
61 N
(V/
Y
Blank oo Temp
Q.Y(-m5
�P
C
0
t13
C
,z
c1
in
i�
c a'i
c M
M
E
o
O
E
4
0
W
u
¢
c
a
O
+
Z
D
ro
(a
�
U
w
z
t°
ci
F—
U
Z
Rectuired Analysis ( Preservative
! ��►
,✓v
u11,E
Matrix Key
WW —Wastewater GW — Groundwater
DW—Drinking Water S—Soil/Solid O—Oil
P - Product M - Misc
Site/Facility ID x
A Cool < 10C Na25203 (Micro OnIyJ
0 Cool <= 6C
C H2504pH<2
D None Required
E NsOH pHn10
r HNO3 pH<2
G HCLpH<2
H H3POA pH<2
I Cool r_ 6C NA25203
Comments/Notes
Meta(s:AI,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
(IIIII IIIII Illl IIIII IIIU I II IIII I till III I IIIII I III IIII II23-010-0011
46245
0110-2023
EMA Resources Inc 09 58;39
Davidson Water Sludge
Sampled by (Name — Print) Client Remarks/Comments
Sludge Samples - Report Dry Weight
Relinquif +bid: (SIGNATURE) Date Time Received by: {SIGNATURE) Date Time
i/0 .5- .3o
Relinquished by; (SIGNATURE) Date Time Received by: [SIGNATURE) Date Time
Relinquished by: (SIGNATURE) Date Time ReNived : (SIG A U ) Da a Tillne
6—AVA A A
Y
U

Waypointo
ANALYTICAL
4/24/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-103-0011
Client Project Description: Davidson Water Sludge
Davidson, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/13/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoi t
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program - NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program - NELAP
LA037
12/31/2023
Louisiana
State Program - NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program - NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program - NELAP
460181
09/14/2023
Page 1 of 1 00001/23-103-0011
Page 2 of 8

Waypoint,
ANALYTICAL
Report Number:
Client Project Description:
Lab No Client Sample ID
95946 Davidson Water
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Sample Summary Table
23-103-0011
Davidson Water Sludge
Davidson, INC
Matrix
Solids
Date Collected
04/12/2023 09:05
www.waypointanalytical.com
Date Received
04/13/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Davidson Water Sludge
Lab Report Number: 23-103-0011
Date: 4/24/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 96083
Analyte: Aluminum
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083
Analyte: Iron
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083
Analyte: Potassium
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 96083
Analyte: Manganese
QC Batch No: 1-676414/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083
Analyte: Lead
QC Batch No: 1-676414/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

Waypoi t,
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Davidson Water Sludge
Information : Davidson, NC
Report Date : 04/24/2023
Received : 04/13/2023
Connie Cook
Report Number : 23-103-0011
REPORT OFANALYSIS
Project
Manager
Lab No : 95946
Matrix:
Solids
Sample ID : Davidson Water
Sampled:
4/12/2023
9:05
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
95.4
%
1
04/20/2316:45
JLS
SW-DRYWT
Ammonia Nitrogen
3390
mg/Kg
- dry
348
2170
1
04/21/23 13:15
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<21.7
mg/Kg
- dry
21.7
109
1
04/18/23 13:24
ZBD
4500NO3F-2016
Organic N
57910
mg/Kg
- dry
347.8
2174
1
04/21/23 13:15
CALCULATION
pH
6.1
S.U.
1
04/20/2316:20
CNB
9045D
Total Solids
4.24
%
0.010
0.010
1
04/19/23 07:49
CJR
254OG-2011
Total Kjeldahl Nitrogen
61300
mg/Kg
- dry
217
5430
1
04/24/23 10:00
CLP >M-4500-NH3C-TKP
Phosphorus
3000
mg/Kg
- dry
60.0
109
1
04/15/23 07:41
BKN
6010D
Aluminum
33300
mg/Kg
- dry
100
109
1
04/15/23 07:41
BKN
6010D
Arsenic
<5.22
mg/Kg
- dry
5.22
10.9
1
04/15/23 07:41
BKN
6010D
Cadmium
1.413
mg/Kg
- dry
0.435
2.17
1
04/15/23 07:41
BKN
6010D
Calcium
1360
mg/Kg
- dry
841
1090
1
04/15/23 07:41
BKN
6010D
Chromium
38.0
mg/Kg
- dry
5.13
5.43
1
04/15/23 07:41
BKN
6010D
Copper
23.0
mg/Kg
- dry
6.74
10.9
1
04/15/23 07:41
BKN
6010D
Iron
309000
mg/Kg
- dry
926
1090
5
04/18/23 18:55
BKN
6010D
Lead
18.5
mg/Kg
- dry
3.91
6.52
1
04/15/23 07:41
BKN
6010D
Magnesium
1180
mg/Kg
- dry
56.1
109
1
04/15/23 07:41
BKN
6010D
Manganese
337
mg/Kg
- dry
7.07
10.9
1
04/15/23 07:41
BKN
6010D
Mercury
<0.472
mg/Kg
- dry
0.472
3.91
1
04/17/23 11:13
FDS
7471A
Molybdenum
6.54
mg/Kg
- dry
2.93
5.43
1
04/15/23 07:41
BKN
6010D
Nickel
16.0
mg/Kg
- dry
2.61
5.43
1
04/15/23 07:41
BKN
6010D
Potassium
1130
mg/Kg
- dry
134
217
1
04/15/23 07:41
BKN
6010D
Selenium
18.8
mg/Kg
- dry
6.96
10.9
1
04/15/23 07:41
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 5 of 8

0
Waypoi nt, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Davidson Water Sludge
Brent Collins
Report Date : 04/24/2023
755 Yadkinville Rd
Information
: Davidson, NC
Received : 04/13/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-103-0011
REPORT OFANALYSIS
Project Manager
Lab No : 95946
Matrix:
Solids
Sample ID : Davidson Water
Sampled:
4/12/2023 9:05
Test
Results
Units MDL
MQL
DF
Date / Time
By Analytical
Analyzed
Method
Sodium
3803
mg/Kg - dry 283
543
1
04/15/23 07:41
BKN 6010D
Zinc
68.9
mg/Kg - dry 17.6
27.2
1
04/15/23 07:41
BKN 6010D
Sulfur
1760
mg/Kg - dry 113
217
1
04/15/23 07:41
BKN 6010D
Sodium Absorption Ratio
0.393
Ratio 0.01
0.01
1
04/15/23 07:41
CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 6 of 8

WaypANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-103-0011
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 Other:
0 UPS 0 Client 0 Courier
Thermometer ID:
135
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
1
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
# Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
# N/A
Trip Blanks received with VOAs
0 Yes
0 No
# N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
# N/A
F_ High concentration container (48 hr)
F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
# No
Comments:
Signature: IlEmily M. Peterson Date & Time: 104/13/2023 09:17:34 1
Page 7 of 8

ro
w
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m co
0
ra
03
Client Name/Address Client Project Manager/Contact Billing Information For Laboratory Use Only
EMA Resources Inc Brent Collins Account #46245
755 Yadklnvllle Rd
Mocksvllle, NC 27028
Project Description Project/S:te Location (City/State) i i RUSH - Additional charges apply Method of Shipment Matrix Key
(rJ-j Special Detectipn Limits) O Fed Ex SUPS �USPS WW -Wastewater GW-Groundwater
� Date Results Needed Courier Client Drop Off DW - Drinking Water S - Soil /Solid 0 - Oil
P-Product M-Mist
Other
Project Number Project Manager Phone p Project Manager Email Purchase Order Number Site/Facility ID M
336-399-3646 [e-mail] 'a�;dro,% Wa}-�
M Z N A Cool < 10C Na25203 (Micro Only)
• p y E U 6 Cool <_ 6C
Waypoint 0 NoneHZS0eq it
� N r
Y C7 0 None Required
ANALYTICAL c ° E E O (n E NaOH pH>20
2790 Whitten Road v In Q f HNO3pH<2
Memphia TN 38133 Unless noted, all containers G X. o .�+ Z r ` U G HCLpH<2
[phone] per Table II of 40 CFR Part E Z Q �/ U H Cool c=6C NA2$203
13b. n A
Date Time Sample Identification z Required Analysis / Preservative Comments/Notes
'+llz 9:05 De,, , dsd Wm; e,- I 4'bt C Metals AI,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
l + + I I II46245
—
` I IIIIII I III IIII IIIII� illl IIIII IIII IIIIIIIIII Iliil IIIII ICI IIII 0 t43-T4231
EMA Resources Inc 09 1718
Davidson Water Sludoe
W!� ■ a ■
For Laboratory Use Only Sampled by (Name - Print) Client Remarks/Comments
►�ylc/1e Custody
S aldy Lab Comments / ,�� 6fhls Sludge Samples - Report Dry Weight
V N Y No Relinquis by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date Time
1 11 3. 30
elan Coole emp Relinquished by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date Time
Z�L
Relinquished by: (SIGNATURE) Date Time Received : (SIM! -hdi't) NO me

Waypointo
ANALYTICAL
6/2/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-137-0094
Client Project Description: Davidson Water Sludge
Davidson, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 5/17/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' —'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypoi t
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program - NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program - NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program - NELAP
LA037
12/31/2023
Louisiana
State Program - NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program - NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program - NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program - NELAP
460181
09/14/2023
Page 1 of 1 00001 /23-137-0094
Page 2 of 8

Waypoint,
ANALYTICAL
Report Number:
Client Project Description:
Lab No Client Sample ID
94916 Davidson Water
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
Sample Summary Table
23-137-0094
Davidson Water Sludge
Davidson, INC
Matrix
Solids
Date Collected
05/15/2023 10:00
www.waypointanalytical.com
Date Received
05/17/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Davidson Water Sludge
Lab Report Number: 23-137-0094
Date: 6/2/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 95251
Analyte: Aluminum
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95251
Analyte: Calcium
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95251
Analyte: Potassium
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 95251
Analyte: Phosphorus
QC Batch No: 1-683237/1-682745
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94916 (Davidson Water)
Analyte: Selenium
QC Batch No: 1-683237/1-682745
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 59842
Analyte: Mercury
QC Batch No: 1-683650/1-683458
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected
Page 4 of 8

Waypoi t,
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Project Davidson Water Sludge
Information : Davidson, NC
Report Date : 06/02/2023
Received : 05/17/2023
Connie Cook
Report Number : 23-137-0094
REPORT OFANALYSIS
Project
Manager
Lab No : 94916
Matrix:
Solids
Sample ID : Davidson Water
Sampled:
5/15/2023
10:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
70.6
%
1
05/22/2317:15
JLS
SW-DRYWT
Ammonia Nitrogen
531
mg/Kg
- dry
54.4
340
1
05/25/23 14:20
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
44.9 B
mg/Kg
- dry
3.40
17.0
1
05/18/23 14:53
ZBD
4500NO3F-2016
Organic N
11170
mg/Kg
- dry
54.42
340.1
1
05/25/23 14:20
CALCULATION
pH
5.9
s•u•
1
05/23/2316:00
CNB
9045D
Total Solids
29.4
%
0.010
0.010
1
05/22/23 17:15
JLS
2540G-2011
Total Kjeldahl Nitrogen
11700
mg/Kg
- dry
34.0
850
1
06/01/23 12:00
JPJ >M-4500-NH3C-TKP
Phosphorus
2400
mg/Kg
- dry
9.39
17.0
1
05/20/23 08:03
BKN
6010D
Aluminum
26000
mg/Kg
- dry
15.7
17.0
1
05/20/23 08:03
BKN
6010D
Arsenic
9.56
mg/Kg
- dry
0.816
1.70
1
05/20/23 08:03
BKN
6010D
Cadmium
6.94
mg/Kg
- dry
0.0680
0.340
1
05/20/23 08:03
BKN
6010D
Calcium
850
mg/Kg
- dry
132
170
1
05/20/23 08:03
BKN
6010D
Chromium
27.3
mg/Kg
- dry
0.802
0.850
1
05/20/23 08:03
BKN
6010D
Copper
51.0
mg/Kg
- dry
1.05
1.70
1
05/20/23 08:03
BKN
6010D
Iron
287000
mg/Kg
- dry
578
680
20
05/22/23 21:43
BKN
6010D
Lead
15.0
mg/Kg
- dry
0.612
1.02
1
05/20/23 08:03
BKN
6010D
Magnesium
1020
mg/Kg
- dry
8.78
17.0
1
05/20/23 08:03
BKN
6010D
Manganese
309
mg/Kg
- dry
1.11
1.70
1
05/20/23 08:03
BKN
6010D
Mercury
0.1033
mg/Kg
- dry
0.0779
0.646
1
05/23/23 10:49
FDS
7471A
Molybdenum
6.26
mg/Kg
- dry
0.459
0.850
1
05/20/23 08:03
BKN
6010D
Nickel
27.4
mg/Kg
- dry
0.408
0.850
1
05/20/23 08:03
BKN
6010D
Potassium
850
mg/Kg
- dry
21.0
34.0
1
05/20/23 08:03
BKN
6010D
Selenium
<21.8
mg/Kg
- dry
21.8
34.0
20
05/22/23 21:43
BKN
6010D
Qualifiers/ B Analyte detected in blank
DF
Dilution
Factor
Definitions J Estimated value
MQL
Method Quantitation Limit
Page 5 of 8

Waypoi nt,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Davidson Water Sludge
Brent Collins
Report Date : 06/02/2023
755 Yadkinville Rd
Information : Davidson, NC
Received : 05/17/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-137-0094
REPORT OFANALYSIS
Project Manager
Lab No : 94916
Matrix: Solids
Sample ID : Davidson Water
Sampled: 5/15/2023 10:00
Test
Results
Units MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
263
mg/Kg - dry 44.2
85.0 1 05/20/23 08:03 BKN 6010D
Zinc
46.9
mg/Kg - dry 2.76
4.25 1 05/20/23 08:03 BKN 6010D
Sulfur
2160
mg/Kg - dry 17.6
34.0 1 05/20/23 08:03 BKN 6010D
Sodium Absorption Ratio
0.77
Ratio 0.01
0.01 1 05/20/23 08:03 CALCULATION
Qualifiers/ B Analyte detected in blank
DF Dilution Factor
Definitions J Estimated value
MQL Method Quantitation Limit
Page 6 of 8

WayPoint 279D Whitten Road, Memphis, 21.2440
Main 901.213.2400 'Fax [phone]
ANALYTICAL www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-137-0094
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: 136
Shipping container/cooler uncompromised? # Yes 0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
# Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
# Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
# Yes
0 No
Samples were considered acceptable as cooling
process had begun.
Water - Sample containers properly preserved
0 Yes
0 No
# N/A
Water - VOA vials free of headspace
0 Yes
0 No
# N/A
Trip Blanks received with VOAs
0 Yes
0 No
# N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
# N/A
F_ High concentration container (48 hr)
F_ Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low conc pre -weighed
vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
# No
Comments:
Signature: IMakayla Weaver I Date & Time: 05/17/2023 11:57:41
Page 7 of 8

ro
w
IQ
m
m
0
co
Client Name/Address Client Project Manager/Contact
EMA Resources Inc Brent Collins
755 Yadklnvllle Rd
Mocksville, NC 27028
Project Description Project/Site Location (City/State)
L, A J CI 50'1 U
Project Number Project Manager Phone #
336-399-3646
WaY- oint
ANALYTICAL
2790 Whilleil Road
Memphis, TN 38133 Unless noted, all containers
[phone] per Table II of 40 CFR Part
136.
Date Time ` Sample identification
S11S /0:00 6.,. d50n W.�,,
IIII I IIIII IIII IIIII I III IIII llll llllll llll IIIIIIIIII IIII IIII 464�
EMA Resources tic
Davidson Waler Sludge
For Laboratory Use Only
ee Custody Lab Comments
Seals
N
y
Blank/Cooler Temp
Billing Information
Account #46245
RUSH -Additional charges apply
Special Detection Limits)
Date Results Needed
Project Manager Email
brent.collins@emaresources corn
For Laboratory Use Only
Method of Shipment
IzFed Ex H
UPS MUSPS
CourierClient Drop Off
Other
Purchase Order Number
b ad; di -A W a}rr
Matrix Key
WW -Wastewater GW-Groundwater
DW- DnnkingWater S -Soll/Solid O - Oil
P - Product M - Misc
Site/Facility ID #
z U)A Coot < 10C Na2S203 (Micro Only)
12 d a0 C U a C004 <- (PC
at O E C H2SO4pH<2
A Y C:) E �f0nt 0 None Required
U) P E Naom PH>30
w OUJ rs D Q f HNO3pH<2
O M i •l . T ( 1 G HCL PH<2
C a O Y 0 y �/ H H3904 pH42
? ? z Q U t Cool <-- 6C WS203
z L?
Required Analysis /Preservative Comments/Notes
i 4,i7� C ✓ V- ✓ ✓ ✓ Metals:Al,As,Ca,Cd,Cr,Cu,Fe,Pb
Mn,Mg,Mo,Hg,Ni,Se,Na,P,S,K,Zn
' ttttttJ
I
Sampled by (Name - Print) Client Remarks/Comments
Sludge Samples - Report Dry Weight
Relinquished by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date Time
itf'4_ � 51/1 3.30
Relinquished by: (SIGNATURE) Date Time Received by: (SIGNATURE) Date Time
Relinquished by: (SIGNATURE) Date Time �IRe� ell blt:,� Date 7 im
/J 5/

aceAnalytical
ANALYTICAL REPORT
January 19, 2023
EMA Resources
Sample Delivery Group
Samples Received:
Project Number:
Description:
Report To:
L1574639
01/10/2023
Sludge
Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
6�m� rN&L
Cassandra Foster
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval ofthe laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
f 4 ,
Iw - . - -
<P0—
,,g,4 —
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 1 of 23

I RUN we] 3oZe7►IIiI►11601
Cp: Cover Page
1
F-CP1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
3S5
DAVIDSON WATER L1574639-01
5
FCn]
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
C
Wet Chemistry by Method D93/1010A
10
[GI
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
rAI
Volatile Organic Compounds (GC/MS) by Method 8260D
14
Chlorinated Acid Herbicides (GC) by Method 8151A
16
rscl
Pesticides (GC) by Method 8081B
17
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
18
GI: Glossary of Terms
20
Al: Accreditations & Locations
21
Sc: Sample Chain of Custody
22
ACCOUNT: PROJECT: S DG:
DATE/TIME:
PAGE:
EMA Resources L1574639
01/19/23 12:18
2 of 23

SAMPLE
SUMMARY
Collected by
Collected date/time
Received date/time
DAVIDSON WATER L1574639-01 Waste
Brent Collins
01/09/23 09:05
01/10/23 08:45
C p
Method
Batch
Dilution
Preparation
Analysis
Analyst
Location
date/time
date/time
FF
Preparation by Method 1311
WG1986135
1
01/11/2311:23
01/11/2311:23
JTM
Mt. Juliet, TN
Preparation by Method 1311
WG1986615
1
01/11/23 09:20
01/11/23 09:20
BTP
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1986823
]
01/12/2316:11
01/12/23 23:09
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1986127
i
01/13/2311:00
01/13/2319:30
AW
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1987054
1
01/12/2316:00
01/12/2318:25
KAD
Mt. Juliet, TN
Fn]
Wet Chemistry by Method D93/1010A
WG1989070
1
01/16/23 01:09
01/16/23 01:09
CRB
Mt. Juliet, TN
Mercury by Method 7470A
WG1987570
1
01/12/2310:56
01/13/23 09:26
SRT
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1987930
1
01/12/2318:48
01/12/23 23:27
ABL
Mt. Juliet, TN
Fr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1987508
1
01/12/2314:14
01/12/2314:14
ADM
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1988910
1
01/17/23 09:56
01/18/2314:42
DLH
Mt. Juliet, TN
FQ
Pesticides (GC) by Method 8081B
WG1989109
1
01/16/23 09:32
01/16/2315:18
JDJ
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1985658
1
01/13/23 05:38
01/13/2318:49
JRM
Mt. Juliet, TN
FGI
rAI
FC
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 3 of 23

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Cassandra Foster
Project Manager
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013.
RP
FC
FSS
FSr
FC
FG1
FAI
LEI
ACCOUNT: PROJECT: S DG: DATE/TIME:
EMA Resources L1574639 01/19/23 12:18
PAGE:
4 of 23

DAVIDSON WATER
SAMPLE RESULTS - 01
Collected date/time: 01/09/23 09:05
L1574639
Preparation by Method 1311
Result
Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction -
1/11/202311:23:05 AM
WG1986135
TCLP ZHE Extraction -
1/11/2023 9:20:45 AM
WG1986615
Fluid 1
1/11/202311:23:05 AM
WG1986135
Initial pH 6.64
1/11/202311:23:05 AM
WG1986135
Final pH 4.75
1/11/202311:23:05 AM
WG1986135
Wet Chemistry by Method 9012 B
Result Qualifier
RDL
Analyte
mg/kg
mg/kg
Reactive Cyanide
0.428
0.250
Wet Chemistry by
Method 9034-9030B
Result Qualifier
RDL
Analyte
mg/kg
mg/kg
Reactive Sulfide
ND
75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date/time
1 01/12/2023 23:09 WG1986823
Dilution Analysis Batch
date/time
1 01/13/202319:30 WG1986127
Result Qualifier
Dilution
Analysis
Analyte su
date /time
Corrosivity by pH 5.67 T8
1
01/12/202318:25
Sample Narrative:
L1574639-01 WG1987054: 5.67 at 19.8C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution
Analysis
Analyte Deg. F
date/time
Ignitability DNI at 170
1
01/16/2023 01:09
Mercury by Method 7470A
Result Qualifier
RDL
Limit
Analyte mgA
mgA
mg/I
Mercury ND
0.0100
0.20
Metals (ICP) by Method 6010D
Result Qualifier
RDL
Limit
Analyte mgA
mgA
mg/I
Arsenic ND
0.100
5
Barium 0.128
0.100
100
Cadmium ND
0.100
1
Chromium ND
0.100
5
Lead ND
0.100
5
Selenium ND
0.100
1
Silver ND
0.100
5
Volatile Organic Compounds (GC/MS) by Method
8260D
Result Qualifier
RDL
Limit
Analyte mgA
mgA
mg/I
Benzene ND
0.0500
0.50
Carbon tetrachloride ND
0.0500
0.50
Chlorobenzene ND
0.0500
100
Chloroform ND
0.250
6
Batch
WG1987054
Batch
WG1989070
Dilution Analysis
date / time
1 01/13/2023 09:26
Dilution Analysis
date / time
1 01/12/2023 23:27
1 01/12/2023 23:27
1 01/12/2023 23:27
1 01/12/2023 23:27
1 01/12/2023 23:27
1 01/12/2023 23:27
1 01/12/2023 23:27
Dilution Analysis
date / time
1 01/12/202314:14
1 01/12/202314:14
1 01/12/202314:14
1 01/12/202314:14
Batch
WG1987570
Batch
WG1987930
WG1987930
WG1987930
WG1987930
WG1987930
WG1987930
WG1987930
Batch
WG1987508
WG1987508
WG1987508
WG1987508
ACCOUNT: PROJECT: S DG: DATE/TIME:
EMA Resources L1574639 01/19/23 12:18
PAGE:
5 of 23

DAVIDSON WATER
SAMPLE RESULTS
- 01
Collected date/time: 01/09/23 09:05
L1574639
Volatile Organic Compounds (GC/MS) by Method 8260D
Qualifier
RDL
Limit
Dilution
Analysis
Batch
FPResult
Analyte mg/I
mg/I
mg/I
date / time
1,2-Dichloroethane ND
0.0500
0.50
1
01/12/202314:14
WG1987508
ITC]
1,1-Dichloroethene ND
0.0500
0.70
1
01/12/202314:14
WG1987508
2-Butanone (MEK) ND
0.500
200
1
01/12/202314:14
WG1987508
Tetrachloroethene ND
0.0500
0.70
1
01/12/202314:14
WG1987508
F
Trichloroethene ND
0.0500
0.50
1
01/12/202314:14
WG1987508
Vinyl chloride ND
0.0500
0.20
1
01/12/202314:14
WG1987508
FCn]
(S) Toluene-d8 ill
80.0-120
011121202314.14
WG1987508
(S)4-Bromofluorobenzene 89.8
77.0-126
011121202314.14
WG1987508
(S)12-Dichloroethane-d4 98.3
70.0-130
011121202314.14
WG1987508
Chlorinated Acid Herbicides (GC) by Method 8151A
FQ
Result Qualifier
RDL
Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date / time
FG1
2,4,5-TP (Silvex) ND
0.00200
1
1
01/18/202314:42
WG1988910
2,4-D ND
0.00200
10
1
01/18/202314:42
WG1988910
(S)2,4-Dichloropheny/AceticAcid 85.4
14.0-158
011181202314:42
WG1988910
rAl
Pesticides (GC) by Method 8081B
Fc
Result Qualifier
RDL
Limit
Dilution
Analysis
Batch
Analyte mg/I
mg/I
mg/I
date / time
Chlordane ND
0.00500
0.03
1
01/16/202315:18
WG1989109
Endrin ND
0.00500
0.02
1
01/16/202315:18
WG1989109
Heptachlor ND
0.00500
0.0080
1
01/16/202315:18
WG1989109
Heptachlor epoxide ND
0.00500
0.0080
1
01/16/202315:18
WG1989109
Lindane ND
0.00500
0.40
1
01/16/202315:18
WG1989109
Methoxychlor ND
0.00500
10
1
01/16/202315:18
WG1989109
Toxaphene ND
0.0100
0.50
1
01/16/202315:18
WG1989109
(S) Decochlorobipheny/ 60.6
10.0-128
011161202315.18
WG1989109
(S) Tetrochloro-m-xylene 72.3
10.0-127
011161202315.18
WG1989109
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
1,4-Dichlorobenzene
ND
0.100
7.50
1 01/13/202318:49
WG1985658
2,4-Dinitrotoluene
ND
0.100
0.13
1 01/13/202318:49
WG1985658
Hexachlorobenzene
ND
0.100
0.13
1 01/13/202318:49
WG1985658
Hexachloro-1,3-butadiene
ND
0.100
0.50
1 01/13/202318:49
WG1985658
Hexachloroethane
ND
0.100
3
1 01/13/202318:49
WG1985658
Nitrobenzene
ND
0.100
2
1 01/13/202318:49
WG1985658
Pyridine
ND
0.100
5
1 01/13/202318:49
WG1985658
3&4-Methyl Phenol
ND
0.100
400
1 01/13/202318:49
WG1985658
2-Methylphenol
ND
0.100
200
1 01/13/202318:49
WG1985658
Pentachlorophenol
ND
0.100
100
1 01/13/202318:49
WG1985658
2,4,5-Trichlorophenol
ND
0.100
400
1 01/13/202318:49
WG1985658
2,4,6-Trichlorophenol
ND
0.100
2
1 01/13/202318:49
WG1985658
(S) 2-Fluorophenol
36.9
10.0-120
011131202318.49
WG1985658
(S) Phenol-d5
21.5
10.0-120
011131202318.49
WG1985658
(S) Nitrobenzene-d5
69.1
10.0-127
011131202318.49
WG1985658
(S) 2-Fluorobiphenyl
73.1
10.0-130
011131202318.49
WG1985658
(S)2,4,6-Tribromophenol
76.5
10.0-155
011131202318.49
WG1985658
(S) p-Terphenyl-d14
85.1
10.0-128
011131202318.49
WG1985658
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 6 of 23

WG1986823
Wet Chemistry by Method 9012 B
Method Blank (MB)
(MB) R3880625-1 01/12/23 22:44
MB Result
Analyte mg/kg
Reactive Cyanide U
MB Qualifier MB MDL MB RDL
mg/kg mg/kg
0.0390 0.250
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1574639-01
(LCS) R3880625-2 01/12/23 22:45
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Reactive Cyanide 2.50 2.48 99.0 85.0-115
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 7 of 23

WG1986127
Wet Chemistry by Method 9034-9030B
Method Blank (MB)
(MB) R3880956-1 01/13/2319:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Sulfide U 30.0 75.0
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1574639-01
(LCS) R3880956-2 01/13/2319:30
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Reactive Sulfide 100 68.1 68.1 53.8-124
L1574192-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574192-01 01/13/2319:30 • (MS) R3880956-3 01/13/2319:30 • (MSD) R3880956-5 01/13/2319:30
Spike Amount
Original Result MS Result
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/kg
mg/kg mg/kg
mg/kg %
% %
% %
Reactive Sulfide 100
ND ND
ND 31.2
0.000 1 10.0-136
J3 J6 200 20
Sample Narrative:
MSD: Matrix spike failure due to matrix.
ACCOUNT:
PROJECT:
S DG:
DATE/TIME: PAGE:
EMA Resources
L1574639
01/19/23 12:18 8 of 23

WG1987054 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9045D L1574639-01
Laboratory Control Sample (LCS)
Fp(LCS)
R3880594-1 0111212318:25
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
2
Analyte su su % %
TC
Corrosivity by pH 10.0 9.90 99.0 99.0-101
FS
Sample Narrative:
LCS: 9.9 at 20.6C
[qn
Fr
�GI
rAl
FC
ACCOUNT: PROJECT: S DG: DATE/TIME:
PAGE:
EMA Resources L1574639 01/19/23 12:18
9 of 23

WG1989070
Wet Chemistry by Method D93/1010A
L1574641-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1574641-01 01/16/23 01:09 • (DUP) R3881156-3 01/16/23 01:09
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F %
Ignitability DNI at170 DNI at170 1 0.000
QUALITY CONTROL SUMMARY
L1574639-01
DUP Qualifier DUP RPD
Limits
o�
10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3881156-1 01/16/23 01:09 • (LCSD) R3881156-2 01/16/23 01:09
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F % % % % %
Ignitability 126 129 127 102 100 95.6-104 1.57 10
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 10 of 23

WG1987570
Mercury by Method 7470A
Method Blank (MB)
(MB) R3880748-1 01/13/23 08:59
MB Result
Analyte mg/1
Mercury U
MB Qualifier MB MDL MB RDL
mg/1 mg/1
0.00330 0.0100
Laboratory Control Sample (LCS)
I
QUALITY CONTROL SUMMARY
L1574639-01
(LCS) R3880748-2 01/13/23 09:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/1 mg/1 % %
Mercury 0.0300 0.0257 85.6 80.0-120
L1574564-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574564-01 01/13/23 09:03 • (MS) R3880748-3 01/13/23 09:05 • (MSD) R3880748-4 01/13/23 09:11
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/1 mg/1 mg/1 mg/1 % % % % %
Mercury 0.0300 NO 0.0289 0.0279 96.2 93.0 1 75.0-125 3.45 20
L1574610-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574610-01 01/13/23 09:13 • (MS) R3880748-5 01/13/23 09:15 • (MSD) R3880748-6 01/13/23 09:17
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits
Analyte mg/1 mg/1 mg/1 mg/1 % % % % %
Mercury 0.0300 NO 0.0315 0.0309 105 103 1 75.0-125 2.17 20
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 11 of 23

WG1987930
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3880644-1 01/12/23 22:33
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Arsenic
U
0.0333
0.100
Barium
U
0.0333
0.100
Cadmium
U
0.0333
0.100
Chromium
U
0.0333
0.100
Lead
U
0.0333
0.100
Selenium
U
0.0333
0.100
Silver
U
0.0333
0.100
Laboratory Control Sample (LCS)
(LCS) R3880644-2 01/12/23 22:36
QUALITY CONTROL SUMMARY
L1574639-01
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
%
%
Arsenic
10.0
8.72
87.2
80.0-120
Barium
10.0
9.22
92.2
80.0-120
Cadmium
10.0
9.13
91.3
80.0-120
Chromium
10.0
8.86
88.6
80.0-120
Lead
10.0
9.01
90.1
80.0-120
Selenium
10.0
9.78
97.8
80.0-120
Silver
2.00
1.76
88.1
80.0-120
L1573877-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1573877-01 01/12/23 22:38 • (MS) R3880644-4 01/12/23 22:44 • (MSD) R3880644-5 01/12/23 22:46
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
8.39
8.47
83.9
84.7
Barium
10.0
0.655
9.51
9.55
88.6
88.9
Cadmium
10.0
ND
8.78
8.77
87.8
87.7
Chromium
10.0
ND
8.55
8.55
85.5
85.5
Lead
10.0
3.85
12.4
12.4
85.4
85.3
Selenium
10.0
ND
9.36
9.54
93.6
95.4
Silver
2.00
ND
1.68
1.69
84.2
84.3
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
1 75.0-125
0.997
20
1 75.0-125
0.398
20
1 75.0-125
0.144
20
1 75.0-125
0.0724
20
1 75.0-125
0.0210
20
1 75.0-125
1.85
20
1 75.0-125
0.0684
20
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 12 of 23

WG1987930
Metals (ICP) by Method 6010D
QUALITY CONTROL SUMMARY
L1574639-01
L1574610-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574610-01 01/12/23 22:49 • (MS) R3880644-6 01/12/23 22:52 • (MSD) R3880644-7 01/12/23 22:54
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec. Dilution
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
8.22
8.31
81.2
82.2 1
Barium
10.0
ND
8.70
8.78
87.0
87.8 1
Cadmium
10.0
ND
8.58
8.70
85.8
87.0 1
Chromium
10.0
ND
8.39
8.53
83.4
84.8 1
Lead
10.0
ND
8.38
8.48
83.1
84.1 1
Selenium
10.0
ND
9.03
8.97
90.3
89.7 1
Silver
2.00
ND
1.65
1.66
82.3
82.9 1
Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
75.0-125
1.18
20
75.0-125
0.965
20
75.0-125
1.33
20
75.0-125
1.61
20
75.0-125
1.15
20
75.0-125
0.679
20
75.0-125
0.798
20
ACCOUNT:
EMA Resources
PROJECT: S DG: DATE/TIME: PAGE:
L1574639 01/19/23 12:18 13 of 23

WG1987508 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1574639-01
Method Blank (MB)
(MB) R3880692-3 01/12/2312:47
MB Result
MB Qualifier MB MDL
MB RDL
Analyte
mg/I
mg/I
mg/I
Benzene
U
0.0167
0.0500
Carbon tetrachloride
U
0.0167
0.0500
Chlorobenzene
U
0.0167
0.0500
Chloroform
U
0.0833
0.250
1,2-Dichloroethane
U
0.0167
0.0500
1,1-Dichloroethene
U
0.0167
0.0500
2-Butanone (MEK)
U
0.167
0.500
Tetra chloroethene
U
0.0167
0.0500
Trichloroethene
U
0.0167
0.0500
Vinyl chloride
U
0.0167
0.0500
(S) Toluene-d8
106
80.0-120
(S) 4-Bromofluorobenzene
92.1
77.0-126
(S)1,2-Dichloroethane-d4
979
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3880692-1 01/12/23 08:21 • (LCSD) R3880692-2 01/12/2312:03
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
Analyte
mg/I
mg/I
mg/I
%
%
%
Benzene
0.250
0.245
0.268
98.0
107
70.0-123
Carbon tetrachloride
0.250
0.242
0.266
96.8
106
68.0-126
Chlorobenzene
0.250
0.256
0.270
102
108
80.0-121
Chloroform
0.250
0.249
0.263
99.6
105
73.0-120
1,2-Dichloroethane
0.250
0.225
0.242
90.0
96.8
70.0-128
1,1-Dichloroethene
0.250
0.238
0.276
95.2
110
71.0-124
2-Butanone (MEK)
1.25
1.39
1.24
ill
99.2
44.0-160
Tetra chloroethene
0.250
0.276
0.304
110
122
72.0-132
Trichloroethene
0.250
0.265
0.281
106
112
78.0-124
Vinyl chloride
0.250
0.217
0.261
86.8
104
67.0-131
(S) Toluene-d8
105
104
80.0-120
(S) 4-Bromofluorobenzene
95.3
93.1
77.0-126
(S)1,2-Dichloroethane-d4
96.1
93.3
70.0-130
LCS Qualifier LCSD Qualifier RPD
RPD Limits
o�
o�
8.97
20
9.45
20
5.32
20
5.47
20
7.28
20
14.8
20
11.4
20
9.66
20
5.86
20
18.4
20
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1574639 01/19/23 12:18 14 of 23

WG1987508 QUALITY CONTROL SUMMARY
Volatile Organic Compounds (GC/MS) by Method 8260D L1574639-01
L1574860-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574860-01 01/12/2313:31 • (MS) R3880692-4 01/12/2319:00 • (MSD) R3880692-5 01/12/2319:22
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
%
%
Benzene
0.250
ND
0.182
0.265
72.8
106
1
17.0-158
J3
37.1
27
Carbon tetrachloride
0.250
ND
0.129
0.251
51.6
100
1
23.0-159
J3
64.2
28
Chlorobenzene
0.250
ND
0.202
0.278
80.8
111
1
33.0-152
J3
31.7
27
Chloroform
0.250
ND
ND
0.269
77.6
108
1
29.0-154
J3
32.4
28
1,2-Dichloroethane
0.250
ND
0.214
0.249
85.6
99.6
1
29.0-151
15.1
27
1,1-Dichloroethene
0.250
ND
0.143
0.267
57.2
107
1
11.0-160
J3
60.5
29
2-Butanone (MEK)
1.25
ND
1.45
1.31
116
105
1
10.0-160
10.1
32
Tetrachloroethene
0.250
ND
0.172
0.293
68.8
117
1
10.0-160
J3
52.0
27
Trichloroethene
0.250
ND
0.172
0.268
68.8
107
1
10.0-160
J3
43.6
25
Vinyl chloride
0.250
ND
0.115
0.235
46.0
94.0
1
10.0-160
J3
68.6
27
(S) Toluene-d8
107
107
80.0-120
(S)4-Bromofluorobenzene
92.3
92.1
77.0-126
(S)1,2-Dichloroethane-d4
98.0
97.1
70.0-130
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1574639
01/19/23 12:18
15 of 23

WG1988910
Chlorinated Acid Herbicides (GC) by Method 8151A
QUALITY CONTROL SUMMARY
L1574639-01
Method Blank (MB)
(MB) R3882451-1 01/18/2314:09
MB Result
Analyte mg/I
2,4,5-TP (Silvex) U
2,4-D U
(S) 2,4-Dichlorophenyl Acetic 82.6
Acid
MB Qualifier MB MDL
mg/I
0.000667
0.000667
Laboratory Control Sample (LCS)
(LCS) R3882451-2 01/18/2314:20
MB RDL
mg/I
0.00200
0.00200
14.0-158
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte
mg/I
mg/I
%
%
2,4,5-TP (Silvex)
0.0500
0.0467
93.4
50.0-125
2,4-D
0.0500
0.0496
99.2
50.0-120
(S) 2,4-Dichlorophenyl Acetic
80.8
14.0-158
Acid
L1575786-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1575786-01 01/18/2318:57 • (MS) R3882451-3 01/18/2319:08 • (MSD) R3882451-4 01/18/2319:19
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
2,4,5-TP (Silvex)
0.0500
ND
0.0392
0.0337
78.4
67.4
1 50.0-125
2,4-D
0.0500
ND
0.0453
0.0396
90.6
79.2
1 50.0-120
(S) 2,4-Dichlorophenyl Acetic
832
72.6
14.0-158
Acid
MS Qualifier MSD Qualifier RPD RPD Limits
15.1 20
13.4 20
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 16 of 23

WG1989109
QUALITY
CONTROL
SUMMARY
Pesticides (GC) by Method 8081B
L1574639-01
Method Blank (MB)
Fp(MB)
R3881396-1 01/16/2313:59
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/1
mg/1
mg/1
F
Chlordane U
0.00167
0.00500
Endrin U
0.00167
0.00500
FS
Heptachlor U
0.00167
0.00500
Heptachlor epoxide U
0.00167
0.00500
Gamma BHC U
0.00167
0.00500
[qn
Methoxychlor U
0.00167
0.00500
Toxaphene U
0.00333
0.0100
Fr
(S) Decachlorobipheny/ 88.7
10.0-128
(S) Tetrachloro-m-xylene 101
10.0-127
Laboratory Control Sample (LCS)
7G1
(LCS) R3881396-2 01/16/2314:08
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/1
mg/1
%
%
rAl
Endrin 0.0100
Heptachlor 0.0100
0.0100
0.0109
100
109
57.0-134
27.0-132
Fc
Heptachlor epoxide 0.0100
0.00975
97.5
57.0-130
Gamma BHC 0.0100
0.0102
102
55.0-129
Methoxychlor 0.0100
0.0104
104
54.0-155
(S) Decachlorobipheny/
51.9
10.0-128
(S) Tetrachloro-m-xylene
70.1
10.0-127
L1572732-01 Original Sample (OS) • Matrix
Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1572732-01 01/16/2314:26 • (MS) R3881396-3 01/16/2314:34 •
(MSD) R3881396-4 01/16/2314:43
Spike Amount
Original Result
MS Result
MSD Result MS Rec.
MSD Rec. Dilution Rec. Limits MS Qualifier
MSD Qualifier RPD
RPD Limits
Analyte mg/1
mg/1
mg/1
mg/1 %
%
%
%
%
Endrin 0.0100
NO
0.0100
0.00976 100
97.6 1
10.0-160
2.43
39
Heptachlor 0.0100
NO
0.0104
0.00976 104
97.6 1
16.0-136
6.35
40
Heptachlor epoxide 0.0100
NO
0.00952
0.00932 95.2
93.2 1
10.0-160
2.12
36
Gamma BHC 0.0100
NO
0.0100
0.0101 100
101 1
14.0-141
0.995
40
Methoxychlor 0.0100
NO
0.0103
0.00984 103
98.4 1
10.0-160
4.57
34
(S) Decachlorobipheny/
53.0
44.2
10.0-128
(S) Tetrachloro-m-xylene
72.4
70.0
10.0-127
ACCOUNT:
PROJECT:
S DG:
DATE/TIME:
PAGE:
EMA Resources
L1574639
01/19/23 12:18
17 of 23

WG1985658
QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds
(GC/MS) by
Method 8270E
L1574639-01
Method Blank (MB)
'
Cp
(MB) R3880808-2 01/13/2311:29
MB Result
MB Qualifier
MB MDL
MB RDL
2
Analyte mg/I
mg/I
mg/I
TC
- ]
1,4-Dichlorobenzene U
0.0333
0.100
2,4-Dinitrotoluene U
0.0333
0.100
FSS
Hexachlorobenzene U
0.0333
0.100
Hexachloro-1,3-butadiene U
0.0333
0.100
Hexachloroethane U
0.0333
0.100
[qn
Nitrobenzene U
0.0333
0.100
Pyridine U
0.0333
0.100
Fr
3&4-Methyl Phenol U
0.0333
0.100
2-Methylphenol U
0.0333
0.100
Pentachlorophenol U
0.0333
0.100
2,4,5-Trichlorophenol U
0.0333
0.100
2,4,6-Trichlorophenol U
0.0333
0.100
q
(S) 2-Fluorophenol 38.3
10.0-120
(S) Phenol-d5 22.8
10.0-120
(S) Nitrobenzene-d5 72.1
10.0-127
rAl
(S) 2-Fluorobiphenyl 72.9
10.0-130
(S) 2,4,6-Tribromophenol 72.0
10.0-155
FC
(S) p-Terphenyl-d14 85.4
10.0-128
Laboratory Control Sample (LCS)
(LCS) R3880808-1 01/13/2311:08
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
1,4-Dichlorobenzene 0.500
0.372
74.4
18.0-120
2,4-Dinitrotoluene 0.500
0.466
93.2
49.0-124
Hexachlorobenzene 0.500
0.427
85.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.362
72.4
19.0-120
Hexachloroethane 0.500
0.365
73.0
15.0-120
Nitrobenzene 0.500
0.351
70.2
27.0-120
Pyridine 0.500
0.0738
14.8
10.0-120
3&4-Methyl Phenol 0.500
0.222
44.4
31.0-120
2-Methylphenol 0.500
0.284
56.8
28.0-120
Pentachlorophenol 0.500
0.441
88.2
23.0-120
2,4,5-Trichlorophenol 0.500
0.448
89.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.433
86.6
42.0-120
(S) 2-Fluorophenol
44.9
10.0-120
(S) Phenol-d5
27.7
10.0-120
(S) Nitrobenzene-d5
70.4
10.0-127
ACCOUNT:
PROJECT: S DG: DATE/TIME:
PAGE:
EMA Resources
L1574639 01/19/23 12:18
18 of 23

WG1985658
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
Laboratory Control Sample (LCS)
(LCS) R3880808-1 01/13/2311:08
Spike Amount LCS Result LCS Rec.
Analyte mg/I mg/I %
(S) 2-Fluorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-dM
77.2
87.0
85.2
QUALITY CONTROL SUMMARY
L1574639-01
Rec. Limits
10.0-130
10.0-155
10.0-128
LCS Qualifier
L1574641-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574641-01 01/13/2319:10 • (MS) R3880808-3 01/13/2319:32 • (MSD) R3880808-4 01/13/2319:53
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
1,4-Dichlorobenzene
0.500
NO
0.356
0.376
71.2
75.2
1 17.0-120
2,4-Dinitrotoluene
0.500
NO
0.449
0.486
89.8
97.2
1 39.0-125
Hexachlorobenzene
0.500
NO
0.411
0.440
82.2
88.0
1 35.0-122
Hexachloro-1,3-butadiene
0.500
NO
0.352
0.379
70.4
75.8
1 12.0-120
Hexachloroethane
0.500
NO
0.356
0.372
71.2
74.4
1 10.0-120
Nitrobenzene
0.500
NO
0.343
0.358
68.6
71.6
1 12.0-120
Pyridine
0.500
NO
NO
NO
10.2
10.1
1 10.0-120
3&4-Methyl Phenol
0.500
NO
0.258
0.279
51.6
55.8
1 10.0-120
2-Methylphenol
0.500
NO
0.262
0.290
52.4
58.0
1 10.0-120
Pentachlorophenol
0.500
NO
0.444
0.467
88.8
93.4
1 10.0-128
2,4,5-Trichlorophenol
0.500
NO
0.432
0.464
86.4
92.8
1 33.0-120
2,4,6-Trichlorophenol
0.500
NO
0.415
0.448
83.0
89.6
1 26.0-120
(S)2-Fluoropheno/
40.8
4a6
10.0-120
(S) Phenol-d5
25.7
26.1
10.0-120
(S) Nitrobenzene-d5
68.7
70.6
10.0-127
(S) 2-Fluorobiphenyl
74.5
78.4
10.0-130
(S)2,4,6-Tribromophenol
86.5
92.0
10.0-155
(S) p-Terphenyl-dM
83.6
87.0
10.0-128
MS Qualifier MSD Qualifier RPD
RPD Limits
5.46
40
7.91
25
6.82
24
7.39
34
4.40
40
4.28
30
0.786
37
7.82
36
10.1
30
5.05
37
7.14
31
7.65
31
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 19 of 23

GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL Method Detection Limit.
ND Not detected at the Reporting Limit (or MDL where applicable).
RDL Reported Detection Limit.
Rec. Recovery.
RPD Relative Percent Difference.
SDG Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U Not detected at the Reporting Limit (or MDL where applicable).
Analyte The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
J3
J6
T8
Description
The associated batch QC was outside the established quality control range for precision.
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
EMA Resources
PROJECT: SDG: DATE/TIME: PAGE:
L1574639 01/19/23 12:18 20 of 23

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 , CP
Alabama
40660
Nebraska
NE-05-15-05
Alaska
17-026
Nevada
TN000032021-1
E
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey —NE LAP
TNO02
California
2932
New Mexico
TN00003
3
SS
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
rCn]
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
E
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
FQ
Kansas
E-10277
RhodeIsland
LA000356
Kentucky' a
KY90010
South Carolina
84004002
Kentucky'
16
South Dakota
n/a
°
FG1
Louisiana
A130792
Tennessee'
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006
Michigan
9958
Virginia
110033
FC1
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A— 150 17025
1461.01
AIHA-LAP,LLC EM LAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
' Drinking Water ' Underground Storage Tanks 3 Aquatic Toxicity ° Chemical/Microbiological 'Mold 'Wastewater n/a Accreditation not applicable
*Not all certifications held by the laboratory are applicable to the results reported in the attached report.
*Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: S DG: DATE/TIME: PAGE:
EMA Resources L1574639 01/19/23 12:18 21 of 23

Company Name/A a tgl -is 1 ntainerlo Hvp Chain of Cust ody Page _of
EMA Resources Mr. Brent Collins LPCrhks
755 Yadkinville Road
TT
755 Yadkinville Road Mocksville, NC 27028 aceAnalytical
Mocksville, NC 27028
Report to: Email To: 12065 tebanon Rd recant Rdiet. TN 77121
[e-mail]•ro whitak Submubn♦ammpkvathsdolno/wstody
Mr. Brent Collins � Y• mnstRutes acknowkdamentand aEoeDlanse onha
Pace Terms and Conditions found at:
�ro'ect Description: City/State /State w�v Please Circle: httoxannro.wutabs.com/mats/oasstand ,d
Sludge Collected: AN ` PT MT CT ET wr..Pdf
J g P � Y �P7c�A4�✓1
Phone: [phone] Client Project # Lab Project # SDG #
r 1 `�
F090
Li netted by (print): Site/Facility ID # P.O. # d
in
Acctnum: EMARES
Collected by (signature): Rush? (Lab MUST Be Notified) Quote # I Q.;, Template:T11413
00, ° ? Prelo In: P895394
Same Day _ Five Day 2 J g
_ Next Day _ 5 Day (Rad Only) Date Results Needed PM: 807 -Justin Carr �/ t1�/�/ Immediately / Two Day _ 10 Day (Rad Only) No PB.� a (� � �' /
Packed on I ce N _ Y �/ _Three Day of r .. z
[ I shipped )ia: Fe EX Ground
Sample ID Comp/Grab I Matrix' I Depth I Date Time ntrs � U Remarks Sampiell(labonly)
iiii III ? 111 U
L iz. i .s" WA-er 55 gIZj 9: OS 2 X X
f
a Matrix: :ernarks: gar+,01. R2Ft?:i•_v_ ;':tso s-t
SS, Sop AIR - Air F Filter pH Temp COC Seal Present/Intact: dNP _Y _N
GW-Groundwater B- Bioassay CDC signed/Accurate: lY ^N
WW-WasteWater Flow Other Bottles arrive intact: h N
DW - Drinkin ater Correct bottles used: �_
B Sufficient volume sent: N
Samples returned via: //1�
OT - Other Yr _ UPS _ FeclEx —Courier Tracking # / 1�7K tf O f !J� i� aonlica�g
"j (� / I VOA Zero Headspace: Y N
Preservation Correct/Checked: , �N
Relinquished by: (SSig�GTime:
naature) Date: me: 7 Received by: (Signature) Trip Blank Received: Yes/V RAD Screen <0.5 mR/hr: JYV _N
119Z3 3 J 0 TBR HCL /MeoH
Re inquished by: (Signature) Date: Time: Received by: (Signatufe) Tem Bottles Received: I breservation required by Login: Date/Time
Relinquished by c 15i n u 1 ^at . _ -A fry .nxWoks SI11-
CIA a mI��n � li�� NCF /6?

2023 Davidson Water Annual Report -
WQ0031712
Final Audit Report 2024-02-27
Created: 2024-02-19
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAAx2EL2gbV3-yiy_foOGTjpvp3wXHAFj1T
"2023 Davidson Water Annual Report - WQ0031712" History
Document created by Brent Collins ([e-mail])
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Pages from 2023 Davidson Water Annual
Report - WQ0031712
Final Audit Report 2024-02-27
Created: 2024-02-27
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAARLLDW6gU7zydlsM40eGBSA691LfpAINv
"Pages from 2023 Davidson Water Annual Report - WQ0031712
" History
Document created by Brent Collins([e-mail])
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