NCGNE0502_COMPLETE FILE - HISTORICAL_20090413

- - - - STORMWATER DIVISION CODING SHEET -
RESCISSIONS .
PERMIT NO. MC b Os OD�
DOC TYPE ❑ COMPLETE FILE - HISTORICAL
DATE OF ❑
RESCISSION YYYYMMDD

MODE R
North Carolina Department of Environment and Natural Resources
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins Dee Freeman
Governor Director Secretary
April 13, 2009
Mr. Michael Gill
Arvato Digital Services l-LC
108 Monticello Road
Weaverville, NC 28787
Subject: No-Exposure Certification NCGNE0502
Arvato Digital Services LLC
108 Monticello Rd. Weaverville, NC 28787
Buncombe County
Dear Mr. Gill:
The Division has reviewed your submittal of the No-Exposure Certification for Exclusion from NPDES Stormwater
Permitting form. Based on your submittal and signed certification of no exposure at the above referenced facility, the
Division is granting your conditional exclusion from permitting as provided for under 40 CFR 126.22(g), which is
incorporated by reference in North Carolina regulations.
Please note that by our acceptance of your no-exposure certification, you are obligated to maintain no-exposure
conditions at your facility. If conditions change such that your facility can no longer qualify for a no-exposure exclusion,
you are obligated to immediately obtain NPDES permit coverage for your stormwater discharge. Otherwise, the
discharge becomes subject to enforcement as an un-permitted discharge. Your conditional no-exposure exclusion
expires in five years (April 30, 2014). At that time you must re-certify with the Division, or obtain NPDES permit
coverage for any stormwater discharges from your facility.
Your conditional exclusion from permitting does not affect your facility's legal requirements to obtain environmental
permits that may be required under other federal, state, or local regulations or ordinances.
If you have any questions or need further information, please contact Brian Lowther at [phone], or at
[e-mail].
Sincerely,
ORIGINAL SIGNED BY
KEN PICKLE
for Coleen H. Sullins
cc: Asheville Regional Office
Stormwater Permitting Unit - No Exposure Files
Wetlands and Stormwater Branch One�1, 1
1617 Mail Service Center,Raleigh,North Carolina 27699-1617 No>Lt jCarotilla
Location:512 N.Salisbury St.Raleigh,North Carolina 27604
Phone:[phone] FAX:91 M07-64941 Customer Service:1-877-623-6748 !�/a�liral`f
Inlernet:www,ncwaterquality.org L� i!
An Frniar nnnndoniO AffirmMi A Art'lm Fmn1.w

b v��
FOR AGENCY USE ONLY
' e Division of Water Quality Y/Surface Water Protection pate Reccive�
1 ear Month I Day
National Pollutant Discharge Elimination System Certificate ofCoverage
NC®ENR z
rianr.�xa,w t rnrnu 0r NO EXPOSURE CERTIFICATION for Exclusion
--N��RR- NCGNE0000
NO EXPOSURE CERTIFICATION
National Pollutant Discharge Elimination System application for exclusion from a Stor r Permit Q
based on NO EXPOSURE: %
Eft
fr
Submission of this No Exposure Certification constitutes notice that your facility does no re P-0i ni
authorization for its storm water discharges associated with industrial activity in the State o
Carolina because it qualifies for a no exposure exclusion.A condition of no exposure at an i i
facility means all industrial materials and activities are protected by a storm resistant shelter( som
exceptions)to prevent exposure to rain, snow, snowmelt,and/or runoff.
Industrial materials or activities include, but are not limited to: material handling equipment or activities,
industrial machinery, raw materials, intermediate products, by-products, final products, or waste
products. Material handling activities include the storage, loading and unloading, transportation, or
conveyance of any raw material, intermediate product, final product or waste product. A storm resistant
shelter is not required for the following industrial materials and activities:drums, barrels, tanks, and
similar containers that are tightly sealed,provided those containers are not deteriorated and do not leak.
"Sealed"means banded or otherwise secured and with locked or non-operational taps or valves;
adequately maintained vehicles used in material handling;and final products, other than products that
would be mobilized in stormwater discharges(e.g., rock salt).
A No Exposure Certification must be provided for each facility qualifying for the no exposure exclusion.
In addition, the exclusion from NPDES permitting is available on a facility-wide basis only—not for
individual outfalls_ if any industrial activities or materials are, or will be, exposed to precipitation, the
facility is not eligible for the no exposure exclusion. By signing and submitting this No Exposure
Certification form, you certify that a condition of no exposure exists at this facility or site and are
obligated to comply with the terms and conditions of 40 CFR 122.26(g).
You are required to reapply for the No Exposure Exclusion once every five (5) years.
For questions,please contact the DWO Regional Office for your area. (See page 5)
(Please print or type)
1) Mailing address of owner/operator(address to which all certification correspondence will be mailed):
Name Arvarn Digital Services LLC;_
Street Address ins Mnnri raj 1 n RngCj
City Weavervi 1 l a State NC ZIP Code 2g7g7
Telephone No. (828) 698=6296 Fax: rsz� 659_201
2) Location of facility producing discharge:
Facility Name
Facility Contact Michael Gill
Street Address 108 Monticello Road
City Weaverville State NC ZIP Code 28787
County Buncombe
Telephone No. (828) 658-2000 Fax: (828) 658-2014
Page 1 of 5
SWU-NE-110607 Last revised 11/06/07
- 71,
rx�jy �iQ4 !'�J�aXSE

NCGNE0000 No Exposure Certification
3) Physical location information:
Please provide a narrative description of how to get to the facility(use street names, state road numbers, and
distance and direction from a roadway intersection)Go I-26A(to 25/70take marshall exit, turn right at
the second traffic light, then right at second driveway.
(A copy of a map with the facility clearly located on it should be included with the certification application.)
4) Is the facility located on Native American Lands? ❑ Yes KI No
5) Is this a Federal facility? ❑ Yes N No
6) Latitude 35" 42' Longitude 082' 34' (deg, min, sec)
7) This NPDES Permit Application applies to which of the following:
❑ New or Proposed Facility Date operation is to begin
❑ Existing Date operation began 07/01/1988
8) Was this facility or site ever covered under an NPDES Stormwater Permit? 6 Yes ❑ No
If yes,what is the NPDES Permit Number? NCG03000
9) Standard Industrial Classification:
Provide the 4 digit Standard Industrial Classification Code (SIC Code) that describes the primary industrial
activity at this facility
SIC Code: 3 6 5 7
10) Provide a brief description of the types of industrial activities and products produced at this facility:
Manufacture of CD11Wrn ai4d�rt�a�e
11) Does this facility have any Non-Discharge permits(ex: recycle permits)?
* No
❑ Yes
If yes, list the permit numbers for all current Non-Discharge permits for this facility:
Exposure Checklists(12. - 14.)
12) Are any of the following materials or activities exposed to precipitation, now or in the foreseeable
future? (Please check either "Yes" or "No.") If you answer "Yes"to any of these items, you are not
eligible for the no exposure exclusion.
a. Using, storing, or cleaning industrial machinery or equipment, and areas where ❑ Yes M No
residuals from using, storing or cleaning industrial machinery or equipment remain
and are exposed to stormwater
b. Materials or residuals on the ground or in stormwater inlets from spills/leaks ❑ Yes ] No
c. Materials or products from past industrial activity ❑ Yes 11 No
d. Material handling equipment (except adequately maintained vehicles) ❑ Yes M No
e. Materials or products during loadinglunloading or transporting activities ❑ Yes 11 No
f. Materials or products stored outdoors (except final products intended for outside ❑ Yes KI No
use[e.g., new cars]where exposure to stormwater does not result in the discharge
of pollutants)
Page 2 of 5
5WU-NE-110607 Last revised 11/06/07

NCGNE0000 No Exposure Certification
g. Materials contained in open, deteriorated or leaking storage drums, barrels, tanks, ❑ Yes 1�1 No
and similar containers
h. Materials or products handled/stored on roads or railways owned or maintained by ❑ Yes K] No
the discharger
i. Waste material (except waste in covered, non-leaking containers [e.g., dumpsters]) ❑ Yes Kl No
j. Application or disposal of process wastewater(unless otherwise permitted) ❑ Yes K] No
k. Particulate matter or visible deposits of residuals from roof stacks and/or vents not ❑ Yes 1] No
otherwise regulated (i.e., under an air quality control permit) and evident in the
stormwater outflow
I. Empty containers that previously contained materials that are not properly stored ❑ Yes Kl No
(i.e., not closed and stored upside down to prevent precipitation accumulation)
m. For any exterior ASTs, as well as drums, barrels, tanks, and similar containers ❑ Yes jo No
stored outside, has the facility had any releases in the past three (3) years?
13) Above Ground Storage Tanks(ASTs): If you answer "No" to any of the following items, you are not
eligible for the no exposure exclusion.
a. Are exterior ASTs or piping free of rust, damaged or weathered coating, pits, or M Yes ❑ No
deterioration, or evidence of leaks?
b. Is secondary containment provided for all exterior ASTs? If so, is it free of any X7 Yes ❑ No
cracks, holes, or evidence of leaks, and are drain valves maintained locked shut?
14) Secondary Containment: If you answer"No" to any of the following items, you are not eligible for the
no exposure exclusion.
a. Is secondary containment provided for single above ground storage containers Kl Yes ❑ No
(including drums, barrels, etc.) with a capacity of more than 660-gallons?
b. Is secondary containment provided for above ground storage containers stored Yes ❑ No
in close proximity to each other with a combined capacity of more than 1,320-
gallons?
c. Is secondary containment provided for any amount of Title III Section 313 Yes ❑ No
Superfund Amendments and Reauthorization Act(SARA)water priority
chemicals?
d. Is secondary containment provided for any amount of hazardous substances? It) Yes ❑ No
e. Are release valves on all secondary containment structures locked? 7�1 Yes ❑ No
Page 3 of 5
SWU-NE-110607 Last revised 11/06/07

NCGNE0000 No Exposure Certification
15) Hazardous Waste:
a. Is this facility a Hazardous Waste Treatment, Storage, or Disposal Facility? ❑ Yes )] No
b. Is this facility a Small Quantity Generator (less than 1000 kg. of hazardous waste ❑ Yes )] No
generated per month) of hazardous waste?
c. Is this facility a Large Quantity Generator (1000 kg. or more of hazardous waste 11 Yes ❑ No
generated per month) of hazardous waste?
If you answered yes to questions b. or c., please provide the following information:
Type(s) ofwaste:npC)I D009'D007,DO09,1)035,1)040,UO77,U!54-11-59,FO93,FG06 ee Attachment
How is material stored:Fnid raumenrally rrontr-olled T.,1;; eheuse
Where is material stored: rhpm;ral Str,r-agn grog
How many disposal shipments per year: 4
Name of transport/disposal vendor: Ash I and Inc
Vendor address:
16) Certification:
certify under penalty of law that I have read and understand the eligibility requirements for claiming a condition of"no
exposure"and obtaining an exclusion from NPDES stormwater permitting.
I certify under penalty of law that there are no discharges of stormwater contaminated by exposure to industrial activities
or materials from the industrial facility or site identified in this document(except as allowed under 40 CFR 122.26(g)(2)).
I understand that I am obligated to submit a no exposure certification form once every five 5 ears to the North Carolina
Division of Water Quality and, if requested,to the operator of the local municipal separate storm sewer system (MS4) into
which the facility discharges(where applicable). I understand that I must allow the North Carolina Division of Water
Quality,or MS4 operator where the discharge is into the local MS4,to perform inspections to confirm the condition of no
exposure and to make such inspection reports publicly available upon request.
In the event that the site no longer qualifies for a No Exposure Exclusion, I understand that I must obtain coverage under
an NPDES permit prior to any point source discharge of stormwater from the facility. Additionally, I certify under penalty
of law that this document and all attachments were prepared under my direction or supervision in accordance with a
system designed to assure that qualified personnel properly gathered and evaluated the information submitted. Based
on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the
information,the information submitted is to the best of my knowledge and belief true, accurate and complete. I am aware
that there are significant penalties for submiffing false information, including the possibility of fine and imprisonment for
knowing violations.
I certify that I am familiar with the information contained in this application and that to the best of my knowledge and
belief such information is true, complete,and accurate.
Printed Name of Person Signing: C�.4 e.l
Title:
(Sig lure of Applicant) ( ate Signed)
Page 4 of 5
SWU-NE-110607 Last revised 11/06/07

NCGNE0000 No Exposure Certification
Please note: This application for the No Exposure Exclusion is subject to approval by the
NCDENR Regional Office prior to issuance. The Regional Office may inspect your facility for
compliance with no exposure conditions prior to that approval. The Regional Office may also
inspect your facility at any time in the future for compliance with the No Exposure Exclusion.
North Carolina General Statute 143-215.6 B(i) provides that:
Any person who knowingly makes any false statement,representation,or certification in any application,record,report,plan,or other
document filed or required to be maintained under this Article or a rule implementing this Article;or who knowingly makes a false
statement of a material fact in a rulemaking proceeding or contested case under this Article;or who falsifies,tampers with,or knowingly
renders inaccurate any recording or monitoring device or method required to be operated or maintained under this Article or rules of the
[Environmental Management]Commission implementing this Article shall be guilty of a Class 2 misdemeanor which may include a fine
not to exceed ten thousand dollars($10,000).
There is currently no fee for a No Exposure Exclusion.
Final Checklist
This application should include the following items:
/This completed application and all supporting documentation.
CX A map with the location of the facility clearly marked.
Mail the entire package to:
Stormwater Permitting Unit
Division of Water Quality
1617 Mail Service Center
Raleigh, North Carolina 27699-1617
Note
The submission of this document does not guarantee the issuance of a No Exposure Exclusion.
For questions, please contact the DINO Regional Office for your area.
DWO Regional Office Contact Information:
I Win6ron!$alcm g� `
Asheville Office ...... [phone] -
Fayetteville Office ... [phone] lz�`i�yh/^ ��Y � -1Raloigh ,
Mooresville Office ... [phone]
Raleigh Office ........ [phone] jAsrtiCVille A",QSV lie
Washington Office ...(252) 946-648.1 - ,
Wilmington Office ... [phone] -- —Nrtly tri viltC
Winston-Salem ...... [phone] j
Central Office .........[phone] �
r'WilmLngfon
Page 5 of 5
SWU-NE-110607 Last revised 11/06/07

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/LSHtI\Np pISTRIBUT10fV
Ashland Distribution Waste Profile Sheet
NAICS Code: (the NAICS code is available on the government ASH 88_4649
website at http://www.census.gov/epedtwww/naics.htmo
Form Code: W 219
Source Code: G 13 Site: 20
Technology: Fuels
Generator Information
Generator Name: SONOPRESS, LLC. Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: Dan Bassett
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center,attention ES Customer Service Manager.
® Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
❑ Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
Properties.and Composition.
Orocess Generating: Acetone Used to Flush the Laquer from Machines
Haste Name: Acetone w/laquer
Hazardous Waste (40CFR Part 261) Yes® No❑ Wastewater(40CFR 268.2 (0) Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: D001, F003
State Waste Codes:
Physical State @ 70OF: Solid❑ Liquid® Both❑ Sludge❑ Compressed Gas❑ Aerosols❑
Single Layer® Multilayer❑ Free Liquids 100 to 100% pH Range 3 to 9 or N/A❑
Odor. Detailed Description Varies Color: Varies
Liquid Flash Point <73°F❑ 73-99OF® 100-1390F❑ 140-199OF❑ > 200OF❑ NIA❑
Chemical Composition: List ALL constituents present in any concentration and forward available ana"is.
Constituents Range/Units Constituents Range/Units
Acetone 5%
Laquer 6%
Alcohol 90%
TOTAL COMPOSITION MUST EQUAL OR EXCEED 100%
FRM-000027 (rev 07/05) k Page 1 of 2

Shipping Information
Packaging: DM-Drum Metal Size: 30 pal Waste Profile Number: 88-4649
Anticipated Volume: 1 Per Month Shipping Frequency: Per Month
,,ampling & Other Infonmation
Is a sample required? Yes❑ No® (Chain of custody required for all samples.)
Analytical data attached? Yes❑ No® MSDS attached? Yes ❑ No® (Check yes for all virgin products)
Liquid Specific Gravity? 008 to 1 OR actual UHC Yes❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transportation Information
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: WASTE FLAMMABLE LIQUIDS, N.O.S.
ACETONE, ALCOHOL
Hazard Clasr, 3{FWrrrcrMe Ligvid) SLb§JaiyHazard Gass TWA ID#UN 1993 Paddng Group: PGI I
Additional Description:
CERCLA Reportable Quantity(RQ): RQ=D001 RQ Units (lb/kg): 110 LB ERG# 128
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
Generator's Certification
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 -Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disposer to obtain a sample from any waste shipment for purposes of recertification. If the waste stream or
-rotes ting th ste changes, I will notify Ashland Distribution prior to shipment of the waste.
i
;0//R
ig ture Printed (or typed) name an title Date
TSDF CERTIFICATION STATEMENT
WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b), WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
..: �. �. - r _, - � ..� . - < � r z- m � •.tom
. ,�. .<. ^' ^'.' ,4.,.,-i n� .n'.��.R.a„ -fir-..pia;.€�.•'a�..�c'�h? •-- .�-,�.-_.. �'�..tia.. .,-.'-'?Fn r.'.r;--..�._;=,.i£,-. ._-r. .� #!.N �-�t _r`�+k.,M4�'_:, s
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Ed Meyer, CHMM Date: 6114107
Customer Service has submitted vendor approval to the Ashland Part 6 facility Date:
All codes have been verified with Ashland Transfer Facility Permit. Initials: Date:
FRM-000027 (rev 07105) Page 2 of 2

ASHLAND DISTRIBUTION
Ashland Distribution Waste Profile Sheet
NAICS Code: 3852 (the NAICS code is available on the government ASH 85-4741
website at http://www.r-ensus.gov/epcdAvww/naiGs.htmo
Form Code: W 119 JM 2-13-04
Source Code: G 09 Site: 02
Technology: WWT
Generator Information
Generator Name: SONOPRESS LLC Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center,attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
Properties and Composition
Drocess Generating: SOLUTION FROM MOLD SHOP
Waste Name: MOLD TANK SOLUTION
Hazardous Waste (40CFR Part 261) Yes® No❑ Wastewater(40CFR 268.2 (0) Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: D002
State Waste Codes:
Physical State @ 70°F: Solid❑ Liquid® Both❑ Sludge❑ Compressed Gas ❑ Aerosols❑
Single Layer® Multilayer❑ Free Liquids 100 to 100% pH Range 12 to 14 or WA❑
Odor. Detailed Description NONE Color: CLEAR
Liquid Flash Point <73°F❑ 73-99'F❑ 100-139`F❑ 140-199OF❑ > 200OF® NIA❑
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
CHROMIUM [1.5PPM DILUTED SODIUM 3%
HYDROXIDE
BRANSON MC-1 5%
WATER BALANCE
'OTAL COMPOSITION MUST EQUAL OR EXCEED 100%
J
FRM-000027 (rev 07/05) Page 1 of 2

Shipping Information
Packaging: DF-Drum Fiber/Poly Size: 30 GAL Waste Profile Number. 85-4741
Anticipated Volume: 1 Per Quarter Shipping Frequency: Per Month
.,ampling & Other Information
Is a sample required? Yes❑ No® (Chain of custody required for all samples.)
Analytical data attached? Yes ❑ No ®. MSDS attached? Yes ® No ❑ (Check yes for all virgin products)
Liquid Specific Gravity? .5 to 1_5 OR actual UHC Yes ❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transportation Information
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: WASTE SODIUM HYDROXIDE SOLUTION
Hazard Class 8(Connsive) SdAciary Hazard Clams f4A ID#UN1824 Padfg Group. PG I I I
Additional Description:
CERCLA Reportable Quantity(RQ): RQ=NA RQ Units(Ibfkg): 1000+ LB ERG# 154
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
Generator's Certification
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 --Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disposer t tain a sample from any waste shipment for purposes of recertification. If the waste stream or
-rocess generating ste changes, I will notify Ashland Distribution prior to shipment of the waste.
—/.7
rgnature Printed (or typed) name d title ate
TSDF CERTIFICATION STATEMENT
FOR WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b),WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit. Initials: Date:
1
FRM-000027 (rev 07/05) Page 2 of 2

ASHL^Nf> 01STRIBUTIC>N
Ashland Distribution Waste Profile Sheet
'4AICS Code: 3852 (the NAICS code is available on the government ASH 85-4730- DIRECT
website at http://www.census.gov/epcd/www/naies.htmo
Form Code: W 119 JM 1-5-07
Source Code: G 11 Site: 10
Technology: WWT
Generator Information
Generator Name: SONOPRESS LLC Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center, attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
Properties-and Composition
Process Generating: OBSOLETE MATERIAL
Vaste Name: BUFFERED OXIDE ETCH
`Hazardous Waste (40CFR Part 261) Yes® No❑ Wastewater(40CFR 268.2 (0) Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: D002
State Waste Codes:
Physical State @ 70°F: Solid❑ Liquid® Both❑ Sludge❑ Compressed Gas❑ Aerosols❑
Single Layer® Multilayer❑ Free Liquids 100 to 100% pH Range<1 to or WA❑
Odor. Detailed Description NONE Color: COLORLESS
Liquid Flash Point <73°F❑ 73-99'F❑ 100-1390F❑ 140-199`F❑ > 200OF® WA❑
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
BUFFERED OXIDE ETCH 100%
contains:
Ammonium Fluoride 30-50
Hydrogen Fluoride 0.5-10
water 40-70
TOTAL COMPOSITION MUST EQUAL OR EXCEED 1000/9
j
FRM-000027 (rev 07/05) Page 1 of 2

Shipping Information
Packaging: DF-Drum Fiber/Poly Size: 5 GAL Waste Profile Number. 85-4730
Anticipated Volume: 1 One Time Only Shipping Frequency: Per Month
ampling &-Other Information
Is a sample required? Yes❑ No® (Chain of custody required for all samples.)
Analytical data attached? Yes❑ No® MSDS attached? Yes® No❑ (Check yes for all virgin products)
Liquid Specific Gravity? .5 to 1.55 OR actual UHC Yes❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transportation Information
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: WASTE CORROSIVE LIQUIDS,TOXIC, NOS
(HYDROFLUORIC ACID,AMMONIUM FLUORIDE)
Hazard Class: 8(Corrosive) SulAdary Hazad Clasp 6.1(Non4H Hazard) ID#UN29M PacWV Group: PG I I
Additional Description:
CERCLA Reportable Quantity(RQ): RQ=NA RQ Units(lb/kg): 1000+ LB T ERG# 154
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
Generator`s Certification
hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 —Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disposer to obt ' ple from any waste shipment for purposes of recertification. If the waste stream or
pro nerating the a angel, I will notify Ashland Distribution prior to shipment of the waste.
Sig ature Printed (or typed) name and title Date
TSDF CERTIFICATION STATEMENT
R WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
HE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b),WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
T 7 x .",-e" sS^3 .i'gE' z -... '- i M;y`r .r^sa. - Yak-w.}'- I, +. T.--.Y —'3'4• ' ; ?- :=.c
"'���" --:+.�:�;�"£,,: s..a 1S
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit, Initials: Date:
i
FRM-000027 (rev 07105) Page 2 of 2

AS"LAND DISTRIBUTION
Ashland Distribution Waste Profile Sheet
.4AICS Code: 3652 (the NAICS code is available at www.naiGs_coM) ASH 854ffl-5- q(A4
Form Code: W 319 JM 3-21-06
Source Code: G 11 Site: 10
Technology: STAB
ratoc
Generator Name: SONOPRESS LLC_ Email. [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State I D#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center, attention ES Customer Service Manager.
n Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
10 Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
ropertiesAdd-Cdmpbtffid '�
Process Generating: USEDIUNUSED OFF-SPEC TAPE
Waste Name: CHROME AUDIO TAPE
.azardous Waste (40CFR Part 261) Yes[g No ❑ Wastewater(40CFR 268.2 (f)) Yes[I No
Identify ALL USEPA listed and characteristic waste code numbers: D007
State Waste Codes:
Physical State @ 70OF: Solid 0 Liquid 0 Both [:1 Sludge[I Compressed Gas L] Aerosols El
Single Layer[0 Muffilayer Ej Free Liquids to 0% pH Range to or N/A
Odor: Detailed Description NONE Color VARIES
Liquid Flash Point <730FE] 73-99*F[j 100-1 39OF El 140-199OF 0 212000FE] N/A El
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
POLYESTER FILM - 90% CHROMIUM DIXOIDE <5%
NITROCELLULOSE RESIN <5% POLYMERIC RESIN <5%
DISPERSANT <5% CARBOXILIC ACID <0.005%
W)TAL COMPOSITION MUST EQUAL OR EXCEED 100%
FRM000027 (rev 03/05) Page 1 of 2

;Shippinglnformatiori3:
Packaging DM-Drum Metal Size: 30 GAL Waste Profile Number. 85-4634
Anticipated Volume: 10 Per Month Shipping Frequency: _ Per Month
aampl!ng & Other Information _ :
r •- �s.
Is a sample required? Yes❑ No ® (Chain of custody required for all samples.) H
Analytical data attached? Yes❑ No ® MSDS attached? Yes ❑ No® (Check yes for all virgin products)
Liquid Specific Gravity? to OR actual NA UHC ❑ Yes❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transpotation=lnformatiori c '
rr
Is this a DOT Hazardous Material? Yes® No ❑
Proper Shipping Name: HAZARDOUS WASTE, SOLID NOS
(D007)
Hazard Clams 9(s%) Subddilwy Harmed Clam [WA ID#NA3077 Padfg Group; PG I I I
Additional Description:
CERCLA Reportable Quantity(RQ): RQ=D007 RQ Units (lb/kg): 10 LB ERG# 171
SPECIAL HANDLING INFORMATION: 8am-4pm p/u hours
Additional Pages Attached ❑
:w'""f--s?.- r a^r=' - k._�`"`e rs�r ram- . R'^at, '"F" ^^t--• cw •--.,r ^^�R�r-'-c• r`-`.+},...'.� i .��'__ ""`" s ? � r
Generator's Certification x :� ;, ` = Yv , f. Y .._ '' ;
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 —Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disposer to obtain a sample from any waste shipment for purposes of recertification. If the waste stream or
cess gen:rwaste changes, I will notify Ashland Distribution prior to shipment of the waste.
Sig ture Printed (or typed) n e and title Date
TSDF CERTIFICATION STATEMENT
FOR WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b), WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
1..ti y; { �-. �� ��z" cis+-_. _T—
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit. Initials: Date:
FRM000027 (rev 03/05) Page 2 of 2

ASHLAND ENSTR18UTIC3N
Ashland Distribution Waste Profile Sheet
,AICS Code: 3652 (the NAICS code is available at www.naics.com) ASH 85-4640
Form Code: W W119 JM 3-21-06
Source Code: G 19 Site: 10
Technology: RETORT
—.^.�s-'�", „'"'-x �v-�zs.�_.....,. �=...ram to �?F '€"�:'. -.E,._ ---v --r -s ...^-�--,-•r- -
Generator;Informatlon
Generator Name: SONOPRESS LLC Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCO982131476
WEAVERViLLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center, attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
.SY.
Process Generating: FACILITY CLEANUP
.1tiaste Name: CRUSHED FLUORESCENT BULBS
zardous Waste (40CFR Part 261) Yes® No❑ Wastewater(40CFR 268.2 {f)).Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: - D009
State Waste Codes:
Physical State @ 70'F: Solid ® Liquid ❑ Both ❑ Sludge ❑ Compressed Gas❑ Aerosols❑
Single Layer❑ Multilayer® Free Liquids 0 to 0% pH Range to or N/A
Odor: Detailed Description VARIES Color VARIES
Liquid Flash Point <73"F❑ _ 73-99°F ❑ 100-139OF ❑ 140-199OF ❑ > 200`F❑ NIA
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
CRUSHED BULBS 100%
TOTAL COMPOSITION MUST EQUAL OR EXCEED 100%
FRM000027 (rev 03f05) Page 1 of 2

Sh�^«-y..... - ,-"".- _v..P�r .r'- '..,.,..Y. '"""."Yc =r,.`".u` -".-.z rt .r=- -.r7 .•-.._,,,,, --� 77
fi d Information:
z:
Packaging DM-Drum Metal Size: 55 GAL Waste Profile Number: 85-4640
Anticipated Volume: 5 Semi-annually Shipping Frequency: Semi-annually
ramp mg 8Other lnforrnati0n
Is a sample required? Yes❑ No® (Chain of custody required for all samples.)
Analytical data attached? Yes❑ No® MSDS attached? Yes❑ No® (Check yes for all virgin products)
Liquid Specific Gravity? _to_OR actual NA UHC ElYes ElNo® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Tra"nsportatlon Information - :, - � . _ - _ -Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: WASTE MERCURY
Hazard Clasp 8(CorraosK e) SulJwliaryHamdClasst N/A iD#UNM9 Pact ft Group: PG 111
Additional Description:
CERCLA Reportable Quantity (RQ): RQ=D009 RQ Units (Ibfkg): 1 LB ERG# 172
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
:k t'q„":4'",,�-s"-'€.."-"� a^-....s1' a-"��„`.�."`�'-�;�. '-�"' r ;•M'�^.-- e-"•r•-'—.� -- .enerator's Certification" °
._.-."-
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 —Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disposer YLabtpin a sample from any waste shipment for purposes of recertification. If the waste stream or
?cess generatin e w e changes, I will notify Ashland Distribution prior to shipment of the waste.
S n ur Printed r typed) n me and title Date
TSDF CERTIFICATION STATEMENT
FOR WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b), WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit_ Initials: Date:
FRM000027 (rev 03/05) Page 2 of 2

GLS�-ILLV+Ia �715TFi1BUT10N
Ashland Distribution Waste Profile Sheet
NAICS Code: 3852 (the NAICS code is available on the govemment ASH 85-4732
website at http://www.census.gov/epcd/www/naics.htmo
Form Code: W 219 JM 1-23-07
Source Code: G 11 Site: 27
Technology: FUELS
Generator.Information
Generator Name: SONOPRESS LLC Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address: -
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center, attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
Properties and .Composition
IProcess Generating: OBSOLETE MATERIAL
Naste Name: DICHLOROETHANE
Hazardous Waste (40CFR Part 261) Yes ® No❑ Wastewater(40CFR 268.2 Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: U077, D001
State Waste Codes:
Physical State @ 70*F: Solid❑ Liquid ® Both❑ Sludge❑ Compressed Gas ❑ Aerosols ❑
Single Layer® Multilayer❑ Free Liquids 100 to 100% pH Range 3 to 9 or NIA❑
Odor: Detailed Description NONE Color: COLORLESS
Liquid Flash Point <73°F® 73-99OF❑ 100-139'F❑ 140-199OF ❑ >200°F❑ NIA❑
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
1,2 DICHLOROETHANE 100%
cas# 107-06-2
TOTAL COMPOSITION MUST EQUAL OR EXCEED 100%
FRM-000027 (rev 07/05) Page 1 of 2

Shipping Information
Packaging: DM-Drum Metal Size: 5 GAL Waste Profile Number: 85-4732
Anticipated Volume: 1 One Time Only Shipping Frequency: Per Month
amplingA Other Inforamation
Is a sample required? Yes❑ No® (Chain of custody required for all samples.) W
Analytical data attached? Yes❑ No® MSDS attached? Yes® No❑ (Check yes for all virgin products)
Liquid Specific Gravity? .5 to 1_5 OR actual UHC Yes❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transportation Information
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: WASTE ETHYLENE DICHLORIDE
Hazard Class 3(F1ammable Liquid) Subsidiary Hazard Class 6.1"xi-IH Hazard) ID#UN1184 Pad!ft Group: PG I l
Additional Description:
CERCLA Reportable Quantity (RQ): RQ=ETHYLENE RQ Units (lb(kg): 100 LB ERG# 131
DICHLORIDE
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
Generator's Certification
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 —Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I -
authorize the disposerj9_gAtain
a sample from any waste shipment for purposes of recertification. If the waste stream or
9ces nerati e w e changes, I will notify Ashland Distribution prior to shipment of the waste.
12-J?Za7
Si nature Printed (or typed) name and title( D e
7
TSDF CERTIFICATION STATEMENT
FOR WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b), WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
�r.:'±, V
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit. Initials: Date:
J
FRM-000027 (rev 07/05) Page 2 of 2

ASHLAND
ASI-LAND a1ST121BUT10N
Ashland Distribution Waste Profile Sheet
NAICS Code: 3852 {the NAILS code is available on the government ASH 85-4734
website at http://www.census.gov/epod/www/naics.htmD
Form Code: W 219 JM 1-29-07
Source Code: G 11 Site: 27
Technology: FUELS
Generator Information
Generator Name: SONOPRESS LLC Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center, attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
Properties and Composition
1 rocess Generating: OBSOLETE MATERIAL
JVaste Name: METHANOL
Hazardous Waste (40CFR Part 261) Yes® No❑ Wastewater(40CFR 268.2 (0) Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: U154, D001
State Waste Codes:
Physical State t@ 70OF: Solid❑ Liquid® Both❑ Sludge❑ Compressed Gas❑ Aerosols❑
Single Layer® Multilayer❑ Free Liquids 100 to 100% pH Range 3 to 9 or N/A❑
Odor. Detailed Description NONE Color: COLORLESS
Liquid Flash Point <730F® 73-99°F❑ 100-139OF❑ 140-199OF❑ � 200OF❑ WA❑
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
METHYL ALCOHOL 100%
TOTAL COMPOSITION MUST EQUAL OR EXCEED 100%
FRM-000027 (rev 07/05) > , rr Page 1 of 2

Shipping Information
Packaging: DM-Drum Metal Size: 5 GAL Waste Profile Number: 85-4734
Anticipated Volume: 1 One Time Only Shipping Frequency: Per Month
.,ampling & Other Information
Is a sample required? Yes❑ No® (Chain of custody required for all samples.)
Analytical data attached? Yes❑ No® MSDS attached? Yes® No❑ (Check yes for all virgin products)
Liquid Specific Gravity? .5 to 1_5 OR actual UHC Yes❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transportation Information
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: WASTE METHANOL
Hazard Class 3 Flammable Liquid) SubsidraryHazard Class; NIA ID#UN1230 Pad ft Group: PG I I
Additional Description:
CERCLA Reportable Quantity(RQ): RQ=NA RQ Units(lb/kg): 1000+ LB ERG# 131
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
Generator's Certification
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 —Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disp o obtain a sample from any waste shipment for purposes of recertification. If the waste stream or
^race gene a waste changes, I will notify Ashland Distribution prior to shipment of the waste.
AK, / /
ign ur Printed (or typed) name arid title Date
TSDF CERTIFICATION STATEMENT
FOR WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
.THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b), WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland.Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit. Initials: Date:
f
FRM-000027 (rev 07/05) Page 2 of 2

Ashland Distribution Waste Profile Sheet
NAICS Code: 3852 (the NAICS code is available on the government ASH 85-4739
website at http://www.census.gov/epcd/wwwlnaics.htmD
Form Code: W 219 - JM 2-12-07
Source Code: G 11 Site: 27
Technology: FUELS
Generator Information
Generator Name: SONOPRESS LLC Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales. TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center, attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
Properties and Composition
Process Generating: UNUSED METHYL ETHYL KETONE
Vaste Name: MEK
Hazardous Waste (40CFR Part 261) Yes® No❑ Wastewater(40CFR 268.2 (0) Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: U159, D001
State Waste Codes:
Physical State @ 70°F: Solid❑ Liquid® Both❑ Sludge ❑ Compressed Gas ❑ Aerosols ❑
Single Layer® Multilayer❑ Free Liquids 100 to 100% pH Range 3 to 9 or NIA❑
Odor. Detailed Description SOLVENT Color: VARIES
Liquid Flash Point <730F® 73-99OF❑ 100-139°F❑ 140-199°F❑ > 200OF❑ N/A❑
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
MEK 100%
TOTAL COMPOSITION MUST EQUAL OR EXCEED 100%
i
FRM-000027 (rev 07/05) Page 1 of 2

Shipping information
Packaging: DM-Drum Metal Size: 5 GAL Waste Profile Number: 85-4739
Anticipated Volume: 1 One Time Only Shipping Frequency: Per Month
,ampling &.Other Information
Is a sample required? Yes❑ No® (Chain of custody required for all samples.)
Analytical data attached? Yes ❑ No® MSDS attached? Yes❑ No® (Check yes for all virgin products)
Liquid Specific Gravity? .5 to 1.5 OR actual UHC Yes❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transportation Information
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: WASTE METHYL ETHYL KETONE
Hazard Class 3 fa<nmabie I quid) SaddiaryHazard Class WA ID#UN1193 PaddM Group: PGII
Additional Description:
CERCLA Reportable Quantity(RQ): RQ=NA RQ Units (lb/kg): 1000+ LB ERG# 127
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
Generator's Certification
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 —Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disposer too tain a sample from any waste shipment for purposes of recertification. If the waste stream or
process enerating t ste changes, I will notify Ashland Distribution prior to shipment of the waste.
i ature Printed (or typed) name apfi title ate
TSDF CERTIFICATION STATEMENT
FOR WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b), WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
-Pr
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit. Initials: Date:
FRM-000027 (rev 07105) Page 2 of 2

American NAME OF WASTE STREAM MATERIAL PROFILE NO.
Environmental
Services,Inc. mdl 20227
724-933-4100
724-933-4110 FAX
New
0 Amendment
A. GENERATOR INFORMATION Technical Contact //174;
Generator Name Telephone Ext.
Facility Address FAX
Billing Name
Billing Address
City/County
State Zip Codej City _L�r',IKIT State jk' Zip Code
USEPAID# lilh�l IX Attention
STATE ID# Telephone AGV.�27 Y 7'77 Ext.
B. DOT F. PHYSICAL CHARACTERISTICS AT 70OF
Shipping Name 1. Infectious or Biological Waste? D Yes Z No
2. NRC Regulated Radioactive? El Yes L21 No
3. Reactivity 0 None 0 Water Reactive
Hazard Class J� UN/NA No. L1 Pyrophoric El Shock Sensitive
Packing Group - 2// RQ 0 Cyanides 0 DOT Explosive
D Sulfides El Other
RCRA 0 Gas (Cylinder) LJ Solid
ACRA Non Hazardous/Exempt LJ Yes 21 No 0 Aerosol 0 Sludges %
Process Generating U Lab Pack Z Free Liquids %
El Dust %
State Waste Codes Layers
EPA Waste Codes (Attach addl. sheet if necessary) 2f Single Layered El Bi-Layered El Multi-Layered
Viscosity
2f Low 0 Medium L-J High
Odor
FJ None 0 Mild Strong
D. ANNUAL REPORT CODES Describe:
SIC Code
Source Code
Form Code Color/Appearance
Origin Code
System Type
E- OTHERCOMPONENTS Weight
No Yes Total ppm Density ­5 —lbs./gal. (US, liq)
PCB's Z F-1 Ibs./cu. foot
Cyanides ❑ Dry Weight 0 < 1.0% 0 5-20%
,ulfides Z F1 0 1-5% 0 20-100%
Pesticides JZ F-1
Phenolics '21 -1 PH [_J >=12.5
Dioxins 4 71 LJ < 2 0 4.1-10 0 NA -
Halogens X) F1 % 0 2.1-4 0 10.1-12.4 Exact
version 2105

American
Environmental PAGE 2 of 2 MATERIAL PROFILE NO.
Services, Inc. MGT 20227
724-933-4100
724-933-4110 FAX
Flash Point (liquid only) Boiling Point 5. Is this waste stored in vented drums? ❑ Yes-El-No
/❑ < 73eF (23eC) ❑ < 95eF (35°C) 6. Is this waste pumpable? .El�'Yes Cl No
❑ 730- 1401F (23eC - 60eC) 2f > 95°F (35eC) 7. Is this waste polymerizable? ❑ Yes 2rNo
❑ 1420- 200°F (61eC - 93°C) ❑ N/A 8. Is waste stream subject to the National Emission
❑ > 200OF (93eC)
❑ NIA Standards for Benzene Waste Operations
(40 CFR 61 Subpart FF)? ❑ Yes ErNo
BTU/Lb. 9. Is this waste regulated as an ozone depleting
� Goa
substance (40 CFR part 82)? ❑ Yes EJ'No
Dermal Toxicity LD$o (Mg/Kg) 10.Does this waste contain scrap metal pieces
❑ < = 40 ❑ > 200, < = 1000 greater than 2 inches in size? ❑ Yes dNo
❑ > 40, < = 200 2f > 1000 11. Does this waste contain>100 ppm VOC's? 1/ ijr= ❑
4. Material poisonous by inhalation? ❑ Yes No Yes ❑ No
Oral Toxicity LD50 (Mg/Kg) H. PHYSICAL/CHEMICAL CONSTITUENTS
i/
❑ < = 5 _ ❑ > 5, < = 50 lr;I<; , ��-,. :,-. , , `61
Solids: ❑ > 50, < = 200 ❑�> 200 ! %
Liquids: ❑ > 50, < = 500 > 500 %
G. METALS %
NONE ❑ TCLP (MG/L) ❑ TOTAL (PPM) %
Reg. Limit Below Above Range %
Arsenic 5 mg/L ❑ ❑ %
Barium 100 mg/L ❑ ❑ %
Cadmium 1 mg/L ❑ ❑ (Attach All MSDS, Sample Analysis and Additional Info.)
Chromium 5 mg/L ❑ ❑ I. ANTICIPATED VOLUME
Copper ❑ ❑ Qty Container QQt Container
Lead 5 mg/L ❑ ❑ ;Zf 2- 5 gl. pail ❑ Cubic Yard Box*
Mercury 0.2 mg/L ❑ ❑ ❑ 15 gl. carboy ❑ Super Sack*
Nickel 134 mg/L ❑ ❑ ❑ 30 gl. drum ❑ Rolloff/Dump Trailer*
Selenium 1 mglL ❑ ❑ ❑ 55 gl. drum ❑ Tanker*
Silver 5 mg/L ❑ ❑ ❑ 85 gl. drum ❑ Other
Zinc ❑ ❑ Per X 1 Time ❑ Week ❑ Month
Others: ❑ Year ❑ Other
(') Is this waste regulated as a Marine Pollutant
(49 CFR 171.8)? ❑ Yes ❑ No
Comments:
Generator's Certification:
I hereby certify that the above and attached description is complete and accurate to the best of my knowledge and ability to determine that no deVberate or willful omissions of composition
properties exist and that all known or suspected hazards have been closed.I certify that the materials tested are representative of all materials described by this profile. f
Generator's Authorized Signature: Dated ; ) ,
WHITE: AE$/ ' YELLOW. Safes Office Copy PINK: Customer Copy

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tt51-ILl�Nd C715rRIBU7'ION
Ashland Distribution Waste Profile Sheet
NAICS Code. 3652 (the NAICS code is available at www.naics.com) ASH 85-4627
Form Code: W 319 JM 3-21-06
Source Code: G 03 Site: 10
Technology: STAB/LF
.Gen`erator[nfomna#,on° �� •,• ,��� � w5� �-
Generator Name: SO_NOPRESS LLC Email.,' _ [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: ^859-357-3877 �
All invoices should be mailed to the appropriate customer service center,attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E. First St, Ste 700, Santa Ana, CA 92705
a vt-we �"9r�"ZF:'��arYl:'r.q•`�,v-'`ET.�CF"-cY+?fR�:�. �"" �'' ... �-u e r a't �`q.?'LX u�y .xt'-e.� �a`+fi ;'T^�-"` �c;a '� -}
Process Generating: PLATING LIQUID FILTERS
Waste Name: CARBON FILTERS
jazardous Waste (40CFR Part 261) Yes® No ❑ Wastewater(40CFR 268.2 (f)} Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: F006
State Waste Codes:
Physical State @ 70°F: Solid ® Liquid ❑ Both ❑ Sludge ❑ Compressed Gas❑ Aerosols ❑
Single Layer❑ Multilayer❑ Free Liquids 0 to 0% pH Range to or WA
Odor. Detailed Description VARIES Color VARIES
Liquid Flash Point <730F ❑ 73-99°F❑ 100-139°F ❑ 140-199°F ❑ 21200oF ❑ WA
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
CARBON FILTER MEDIA 95-99%
CARBON 1_5%
TOTAL COMPOSITION MUST EQUAL OR EXCEED 100%
i
FRM000027 (rev 03/05) Page 1 of 2

S�y ''"csi'...x-',M_71rct. �' Ki ya:c z ;'�„-'tip S+ r ".r^ z ��
i�� �� '111��„iC������ir ,' «� a i i T f ti K 3 x nKr t r n4 rl(. 7' 6 X
Packaging DM-Drum Metal Size: 55 GAL Waste Profile Number: 854627
Anticipated Volume: 5 Per Month Shipping Frequency: Per Month
rA K" aS 'vim -si �,rfa�� ��
.� � .�.. _ FiT{_�;:�ui..w _4^�ri�'..,,t-�.,f•:.::w fi3 }'�� n�~i�i`a'.9G5'eN'!kt'j...'.�AS��.�.r��."-T{S:�i,� .Fl� � �P. �t-l..0 _ { -rF
Is a sample required? Yes ❑ No® (Chain ofcustody required for all samples.)
Analytical data attached? Yes❑ No ® MSDS attached? Yes❑ No ® (Check yes for all virgin products)
Liquid Specific Gravity? to_OR actual NA UHC ElYes ElNo® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No ® If yes, attach Benzene NESHAP certification.
_Transporfatton,lnforlmat�on
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: HAZARDOUS WASTE SOLID, NOS
(F006)
Hazard Clasp 3(MiSca Subsidiary Hazard Clasp NA 1D#NA3M Pada-rg Group: PG I I I
Additional Description:
CERCLA Reportable Quantity (RQ): RQ=F006 RQ Units (lb/kg): 10 LB ERG # 171
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
_�:
Generator's
__..._. ._.._, � _ -...:�-_� �.��s'w.�c�.-�-.,•�,T-�s-��..,.�r'k.- aF�,�t..;h�_�'.-.,,.. ?' t h'r",�,.�" c�€�caPr.:�!:� �s..��._`i.. �`s�r,..�r..-^.M�, .� ���.c-,
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 --Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the dispo r to obtain a sample from any waste shipment for purposes of recertification. If the waste stream or
-ocess gene the waste changes, I will notify Ashla`n'd_yDistribution prior to shipment of the waste.
gnature Printed (or typed) na and title Date
TSDF CERTIFICATION STATEMENT
FOR WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b), WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.
i
i ..ti..- •r ., :.a'A� .a_��C:,45",.�: ,wfi'.,t.,€_.
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit. Initials: Date:
FRM000027 (rev 03/05) Page 2 of 2

ASI-ILAN€] E3ISTRIBUTION
Ashland Distribution Waste Profile Sheet
NAICS Code: 3$52 (the NAICS code is available on the government ASH 85-4667
website at http://www.census.gov/epcd/www/naics.htmo
Form Code: W 119 JM 6-16-06
Source Code: G 03 Site: 10
Technology: STAB/LF
Generator Information
Generator Name: SONOPRESS LLC Email: [e-mail]
Pick Up Address: 108 MONTICELLO ROAD USEPA ID#: NCD982131476
WEAVERVILLE, NC 28787 State ID#:
Mailing Address:
Technical Contact: OLENA HICKS Ashland Sales: TRACY HALE
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
All invoices should be mailed to the appropriate customer service center,attention ES Customer Service Manager.
❑ Ashland Distribution, 5200 Blazer Parkway, Dublin, OH. 43017
® Ashland Distribution, 3930 Glenwood Drive, Charlotte, NC. 28208
❑ Ashland Distribution, 1850 E_ First St, Ste 700, Santa Ana, CA 92705
.Properties and Composition _
Process Generating: PLATING PROCESS
Maste Name: NICKEL BATH SOLUTION
Hazardous Waste (40CFR Part 261) Yes® No❑ Wastewater(40CFR 268.2 (0) Yes❑ No
Identify ALL USEPA listed and characteristic waste code numbers: F006
State Waste Codes:
Physical State @ 70OF: Solid❑ Liquid® Both❑ Sludge❑ Compressed Gas ❑ Aerosols❑
Single Layer® Multilayer❑ Free Liquids 100 to 100% pH Range 3 to 9 or N/A❑
Odor: Detailed Description MILD Color: GREEN
Liquid Flash Point <730F❑ 73-99OF❑ 100-139OF❑ 140-199OF❑ > 200°F® N/A❑
Chemical Composition: List ALL constituents present in any concentration and forward available analysis.
Constituents Range/Units Constituents Range/Units
F006 SLUDGE (NICKEL 100%
SULFAMATE, NICKEL
SALTS)
3TAL COMPOSITION MUST EQUAL OR EXCEED 100%
FRM-000027 (rev 07/05) (-� Page 1 of 2
F

Shipping Information
Packaging: DM-Drum Metal Size: 55 GAL Waste Profile Number: 85-4667
Anticipated Volume: 2 Semi-annually Shipping Frequency: Per Month
-ampling & Other Information
Is a sample required? Yes❑ No® (Chain of custody required for all samples.)
Analytical data attached? Yes❑ No® MSDS attached? Yes® No❑ (Check yes for all virgin products)
Liquid Specific Gravity? .5 to 1_5 OR actual UHC Yes❑ No® If yes, attach UHC Listing
Benzene NESHAP Yes❑ No® If yes, attach Benzene NESHAP certification.
Transportation Information =
Is this a DOT Hazardous Material? Yes® No❑
Proper Shipping Name: HAZARDOUS WASTE LIQUID, NOS
(F006)
Hazard Class: 9 W Sulmdary Hazard Class: N/A ID#NA3082 PadftGDw PG I I I
Additional Description:
CERCLA Reportable Quantity(RQ): RQ=F006 RQ Units(Ibfkg): 10 LB ERG # 171
SPECIAL HANDLING INFORMATION:
Additional Pages Attached ❑
Generator's Certification
I hereby certify that all information submitted in this form and all attached documents contain true and accurate descriptions of
this waste. Any sample submitted is representative as defined in 40 CFR 261 —Appendix I or by using an equivalent method.
All relevant information regarding known or suspected hazards in the possession of the generator has been disclosed. I
authorize the disposer to obtain a sample from any waste shipment for purposes of recertification. If the waste stream or
process genrth `waste changes, I will notify Ashland Distribution prior to shipment of the waste.
Si ature Printed (or typed) nam and title �� D to
TSDF CERTIFICATION STATEMENT
F R WASTE STREAMS WHICH WILL BE MANIFESTED TO ASHLAND DISTRIBUTION FACILITIES: AS REQUIRED BY
THE FEDERAL REGULATIONS SET FORTH IN 40 CFR264.12(b),WE ARE HEREBY NOTIFYING YOU THAT OUR
FACILITY HAS THE APPROPRIATE HAZARDOUS WASTE MANAGEMENT PERMITS AND CAN ACCEPT THE ABOVE
WASTE STREAM GENERATED BY YOUR COMPANY.,�
OFFICE USE ONLY ❑ Check here if this is a recertification
Profile reviewed by Ashland Employee Date:
Customer Service has submitted vendor approval to the Ashland Part B facility Date:
All codes have been verified with Ashland Charlotte, NC Permit. Initials: Date:
FRM-000027 (rev 07/05) Page 2 of 2