HomeMy WebLinkAboutNC0080853_Remission (Request)_20240411 AECOM AECOM 919.461.1100 tel
5438 Wade Park Boulevard,Suite 200
Raleigh, NC 27607
April 11, 2024
Central Files
Division of Water Quality
1621 Mail Service Center
Raleigh, NC 27699-1621
Subject: Remission Request Revision 1 1 Assessment of Civil Penalty
NPDES Permit No. NCO080853/001
Nokia of America Corporation
Case No. TX-2023-0003
3370 Lexington Road,Winston-Salem, NC
To Whom It May Concern:
On behalf of Nokia of America Corporation (Nokia), AECOM Technical Services of North Carolina, Inc. is
submitting this remission request in response to the Assessment of Civil Penalty dated October 13, 2023,
from the North Carolina Department of Environmental Quality (DEQ) regarding the Salem Park facility's
toxicity self-monitoring data from the months of December 2022 and February 2023. Revision 1 is
prepared to provide an estimate of costs incurred investigating and addressing toxicity issues, as
requested by DEQ via email on April 1, 2024. For the reasons outlined below, Nokia respectfully requests
a remission for violation costs.
On March 31, 2023, on behalf of Nokia, AECOM submitted the results of the February 2023 multiple-
concentration chronic toxicity testing for NPDES Permit No. NC0080853. Within the cover letter, in
addition to notifying DEQ of the test failure, AECOM proposed several action items to further evaluate the
recent toxicity failures at the facility. Following submission of the February 2023 toxicity report, AECOM,
on behalf of Nokia, promptly implemented the following actions to better understand the source of chronic
toxicity in the system effluent:
1. Evaluate Potential Source of Toxicity—
a. Extraction well EW-16 is historically the source of the highest concentrations of
chlorinated volatile organic compounds (CVOCs) in the groundwater treatment system
influent. Additionally, annual well cleanings at EW-16 provide evidence of biological
fouling of the well screen. Based on these observations, AECOM proposed to evaluate
EW-16 as a potential source of chronic toxicity in the effluent. Approximately four hours
prior to collecting the regular March 2023 quarterly toxicity sample, AECOM shut down
extraction well EW-16. As described above, the March 2023 samples still failed the
chronic toxicity test. EW-16 was subsequently returned to operation.
b. The Toxicity Reduction Evaluation Guidance for Municipal Wastewater Treatment Plants,
published by the United States Environmental Protection Agency (USEPA) in August
1999, describes several commonly identified potential sources of toxicity for Publicly
Owned Treatment Works (POTW) effluents. Elevated metals concentrations in effluent
are listed among the commonly identified potential sources of toxicity. Specifically, zinc is
understood to have a negative impact upon reproduction in aquatic organisms at
concentrations near 25-50 pg/L and higher. See the discussions below regarding system
analytical results.
AECOM 2
To evaluate the source and concentration of metals in the system effluent, AECOM
collected a series of samples for laboratory analysis in April, May, June, July, and August
2023. At various times these samples were collected from individual wells, influent lines
for well Networks A and B, the effluent stream from the treatment system, and permit
monitoring point FE-151. The related laboratory analytical reports are presented in
Attachment A. Since metals analyses is not normally required under this permit, all
metals testing was performed above and beyond the requirements of the permit.
Additional analytical testing for metals is discussed below.
2. Expand Analytical Dataset During Toxicity Testing—To improve understanding of constituents
present in groundwater treatment system effluent, AECOM collected additional samples from
system effluent for laboratory analysis by EPA Method 8260 (VOC full list)and EPA Method
200.7 (priority pollutant metals) during toxicity testing in April, May, and June 2023. A summary of
results for key metals are presented in the Table 1, with the related laboratory analytical reports
presented in Attachment A. Below is a brief discussion of analytical results per month:
a. April 2023: VOC results from effluent samples were consistent with historical data, and
metals results were consistent with the effluent sample collected on April 5, 2023. In
addition, water quality parameters collected in April were within acceptable ranges. It was
noted that metals testing indicated zinc levels above 50 ug/L in all AS Effluent and FE-
151 samples collected. The April test toxicity test did not pass.
b. May 2023: As presented in Table 1, extraction well EW-6 was the only Network A well
with detectable concentrations of zinc during the May sampling at a detection limit of 20
pg/L. Accordingly, EW-6 was shut off prior to toxicity testing in May 2023 to evaluate the
effects on chronic toxicity. Effluent samples collected during toxicity sampling indicated
that VOC results were consistent with historical data, and that zinc concentrations
declined to non-detect values after EW-6 was shut down, and the May toxicity test
passed.
c. June 2023: In June, metals analyses was performed on both toxicity test water samples.
Although recovery well EW-6 remained shut down, the metals analysis for the initial
sample collected indicated elevated zinc. However, zinc was again less than 20 pg/L for
the second toxicity test sample. This evidently resulted in minimal impact to
reproductivity, and the June toxicity test achieved a passing result. Since zinc
concentrations were elevated in one total effluent sample without EW-6 operating,
AECOM initiated of all extraction wells to identify other extraction wells that may have
been contributing zinc. Concurrently, AECOM restored operation of EW-6, but at a lower
flow rate than previously (approximately 7 gpm instead of 11 gpm).
3. Isolate Zinc Sources—On August 29, 2023, AECOM collected water samples from all active
extraction wells, and sent them to the Pace Analytical laboratory in Minneapolis, MN to achieve a
lower detection limit for zinc than provided by the Pace Analytical laboratory in Asheville, NC (5
pg/L instead of the 10 or 20 pg/L achieved previously). Results of the individual well sampling are
presented in Table 1, with the related laboratory analytical reports presented in Attachment A.
Implementation of the above actions has identified zinc as the most probable cause of toxicity test failures
under this permit in 2022-23. Although EW-6 has been identified as a primary source, zinc also appears
in other extraction wells, but with significant variability. AECOM will continue regular zinc analyses in
individual wells, working to balance the zinc intake into the system while achieving remedial objectives.
Operation of individual recovery wells will continue to be evaluated as additional information is gathered
and hopefully patterns determined. The flow rate in extraction wells identified to frequently contain
dissolved zinc in their effluent may be reduced to mitigate metals concentrations in the combined effluent,
and therefore reduce the chance of a negative chronic toxicity test result.
AECOM 3
Most notably, following the passing test in May 2023, the toxicity sampling has now incurred a passing
result for three consecutive quarters (June, September, and December 2023), as documented in the
toxicity reports submitted to DEQ on July 21, 2023, October 30, 2023, and January 23, 2024.
It is estimated the above-described actions to investigate and address toxicity issues have incurred
approximately$13,500 in additional cost to Nokia. With each future quarterly toxicity test, it is estimated
that Nokia will incur approximately$1,500 additional cost to continue efforts to assess and balance zinc
concentrations from individual extraction wells until a reliable equilibrium is achieved.
After identifying and mitigating the most probable cause of the toxicity failures, which has resulted in four
consecutive passing tests, Nokia contends that the civil penalty qualifies for remission in accordance with
Factor(2) presented in the Civil Penalty Assessment: "the violator promptly abated continuing
environmental damage resulting from the violation."Accordingly, Nokia respectfully requests that DEQ
remit the assessed civil penalty violation costs.
Nokia greatly appreciates DEQ's willingness to consider Nokia's actions in the events following the
violation, as well as the measures that Nokia is taking to ensure compliance with the NPDES Permit and
the requirements of DEQ in the future.
If you have any questions or would like to discuss this further, please contact Conan Fitzgerald at 919-
461-1260.
Sincerely,
Cristin Dolan Conan Fitzgerald, PE
Staff Engineer Project Manager, AVP Engineering
Attachments
a. Justification for Remission Request
b. Table 1 Summary of Metals Analytical Results
c. Table 2 Summary of Costs
d. Laboratory Reports
cc: G. John Galasso, Nokia of America Corporation
J. Wakeman, AECOM
DocuSign Envelope ID:90E20F45-DC74-4117-9502-B5FFE1DC5266
JUSTIFICATION FOR REMISSION REQUEST
Case Number: TX-2023-0003 County: Forsyth
Assessed Party: Salem Business Park remediation site
Permit No. (if applicable): NCO080853 Amount Assessed: $ 2,069.48
Please use this form when requesting remission of this civil penalty.You must also complete
the 'Request For Remission, Waiver of Right to an Administrative Hearing, and Stipulation of
Facts"form to request remission of this civil penalty. You should attach any documents that
you believe support your request and are necessary for the Director to consider in evaluating
your request for remission. Please be aware that a request for remission is limited to
consideration of the five factors listed below as they may relate to the reasonableness of the
amount of the civil penalty assessed. Requesting remission is not the proper procedure for
contesting whether the violation(s) occurred or the accuracy of any of the factual statements
contained in the civil penalty assessment document. Pursuant to N.C.G.S. § 143B-282.1(c),
remission of a civil penalty may be granted only when one or more of the following five
factors applies. Please check each factor that you believe applies to your case and provide a
detailed explanation, including copies of supporting documents, as to why the factor applies
(attach additional pages as needed).
(a) one or more of the civil penalty assessment factors in N.C.G.S. 143B-282.1(b).
were wrongfully applied to the detriment of the petitioner (the assessment factors are
listed in the civil penalty assessment document);
x (b) the violator promptly abated continuing environmental damage resulting
from the violation (i.e., explain the steps that you took to correct the violation and
prevent future occurrences);
(c) the violation was inadvertent or a result of an accident (i.e., explain why the
violation was unavoidable or something you could not prevent or prepare for);
(d) the violator had not been assessed civil penalties for any previous violations;
(e) payment of the civil penalty will prevent payment for the remaining necessary
remedial actions (i.e., explain how payment of the civil penalty will prevent you from
performing the activities necessary to achieve compliance).
EXPLANATION:
Please see the attached Remissions Request letter for detailed
information.
D E Q�� North Carolina Department of Environmental Quality I Division of Water Resources I Bio Lab
4401 Reedy Creek Road I 1621 Mail Service Center I Raleigh,North Carolina 27699-1621
NORTH CAROLINA _
op.n,,,M m E,,,i.n via,i� /✓ 919.743.8400
DocuSign Envelope ID:90E20F4&DC74-4117-9502-B5FFE1DC5266
STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY
COUNTY OF FORSYTH
IN THE MATTER OF ASSESSMENT WAIVER OF RIGHT TO AN
OF CIVIL PENALTIES AGAINST ADMINISTRATIVE HEARING
AND STIPULATION OF FACTS
Salem Business Park remediation site
NPDES PERMIT NO. NCO080853 CASE NO. TX-2023-0003
Having been assessed civil penalties totaling$2,069.48 for violation(s) as set forth in the assessment
document of the Director of the Division of Water Resources dated October 13 2023 the undersigned,
desiring to seek remission of the civil penalties, does hereby waive the right to an administrative hearing
in the above-stated matter and does stipulate that the facts are as alleged in the assessment document. The
undersigned further understands that all evidence presented in support of remission of this civil penalty
must be submitted to the Director of the Division of Water Resources within 30 days of receipt of the
notice of assessment. No new evidence in support of a remission request will be allowed after 30 days
from the receipt of the notice of assessment.
This the �—� day f o c 23 .
, 20
AD SS SIGNATURE
C
TELEPHONE
D E Q North Carolina Department of Environmental Quality I Division of Water Resources Bio Lab
®®® 4401 Reedy Creek Road 1 1621 Mail Service Center Raleigh,North Carolina 27699-1 62 1
919.743.8400
Tables
AECOM
Sample Location
Analyte Sample Date Network A Network B AS
DT-1 EW-4 EW-5 EW-6 EW-12 EW-14 EW-16 EW-17 EW-18 EW-19 EW-21 EW-22 FE-151
Influent Influent Effluent
4/5/2023
4/25/2023
5/2/2023
Zinc 5/18/2023
(pg/L) 5/23/2023
6/22/2023
6/27/2023
7/26/2023
8/29(2023—®1 ®1 ®1 �®�,
4/5/2023
4/25/2023
5/2/2023
Barium 5/18/2023
5/23/2023
(Vg/L)
6/22/2023
6/27/2023
7/26/2023
8/29/2023
4/5/2023
4/25/2023
5/2/2023
Manganese 5/18/2023
(pg/L) 5/23/2023
6/22/2023
6/27/2023
7/26/2023
8/29/2023
Table 2
Summary of Costs to Identify Causes of Outfall Toxicity
NPDES Permit No. NCO080853/2023-2024
Month/Year Activity Hours Rate Cost
Laboratory Analysis for Metals -- -- $ 666.00
Field Technician Labor(sampling,water quality
3 $ 110.00 $ 330.00
April2023 screening)
Engineer III (Data Analysis/DMR/AT3) 3 $ 120.00 $ 360.00
Project Director IV(Opts assess) 6 1 $ 190.00 $ 1,140.00
Subtotal $ 2,496.00
Laboratory Analysis for Metals -- -- $ 378.00
May 2023 Field Technician Labor 6 $ 55.00 $ 330.00
Engineer III (Data Analysis/DMR/AT3) 2 $ 120.00 $ 240.00
Project Dir. IV(Team directives) 4 $ 190.00 $ 760.00
Subtotal $ 1,708.00
Laboratory Analysis for Metals -- -- $ 106.00
June 2023 Field Technician Labor 2 $ 110.00 $ 220.00
Engineer III (Data Analysis/DMR) 1.5 $ 120.00 $ 180.00
Project Dir. IV(Team directives) 6 $ 190.00 $ 1,140.00
Subtotal $ 1,646.00
Laboratory Analysis for Metals -- -- $ 462.00
July 2023 Field Technician Labor 4 $ 110.00 $ 440.00
Engineer III (Data Analysis/DMR) 2 $ 120.00 $ 240.00
Subtotal $ 1,142.00
Laboratory Analysis for Metals -- -- $ 498.00
August 2023 Field Technician Labor 4 $ 110.00 $ 440.00
Engineer III (Data Analysis/DMR) 2 $ 120.00 $ 240.00
Subtotal $ 1,178.00
Engineer III (Field Suport, Generate Remissions
10 $ 120.00 $ 1,200.00
October 2023 Request Letter)
Project Dir. IV(Team directives) 5 $ 190.00 $ 950.00
Subtotal $ 2,150.00
Laboratory Analysis for Metals -- -- $ 375.00
November 2023 Field Technician Labor 4 $ 110.00 $ 440.00
Engineer III (Data Analysis/DMR/Field Support) 10 $ 120.00 $ 1,200.00
Subtotal $ 2,015.00
Laboratory Analysis for Metals -- -- $ 81.00
December 2023 Field Technician Labor 1 $ 110.00 $ 110.00
Engineer III (Data Analysis/DMR/Field Support) 10 $ 120.00 $ 1,200.00
Subtotal $ 1,391.00
Laboratory Analysis for Metals -- -- $ 888.00
February 2024 Field Technician Labor 5 $ 110.00 $ 550.00
Engineer III (Data Ana lysis/DMR/Investigate 4 $ 120.00 $ 480.00
potential zinc treatment)
Subtotal $ 1,918.00
Totall $ 13,494.00
Notes:
Technician labor is calculated using 1 hr for system samples and 4 hrs for sampling all the extraction wells.
Office labor is calculated using a minimum of 30 min.to track and analyze each lab report and an extra 30 min.
per DMR.
\\na.aecomnet.com\LFS\AMER\Raleigh-USRAL3\DCS\Projects\L-AECOM\Jobs\L\Alcatel-Lucent-04364\Winston-Salem\60649441-2021 0&1V1\500-De1iverab1es\501-NPDES Reporting\Toxicity
Remission Requests\Calculation\Remission Request Costs.xlsx
Attachment A
Laboratory Analytical Reports
AECOM
Pace Analytical Services,LLC
(�IaceAnalyfical@ 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
April 25, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA
Pace Project No.: 92661129
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on April 06, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-4jGlAA ,
Bonnie Vang V
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
John Moran,AECOM
Jon Wakeman,AECOM Environment
f.Y�P
2" REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 19
e
Pace Analytical Services,LLC
te 100
laceAnalytical
9800HuIntesvlle,NC128078
wwwww..paclabs.com
(704)875-9092
CERTIFICATIONS
Project: NOKIA
Pace Project No.: 92661129
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
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(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
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078
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SAMPLE ANALYTE COUNT
Project: NOKIA
Pace Project No.: 92661129
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92661129001 FE-151 EPA 1664E REL 1 PASI-C
EPA 200.7 Rev 4.4 1994 D661 11 PASI-A
EPA 7470A BM 1 PASI-A
EPA 8260D LMB 4 PASI-C
SM 2540D-2015 JMH1 1 PASI-A
SM 3500-Cr B-2011 JMH 1 PASI-A
92661129002 AS EFFLUENT EPA 200.7 Rev 4.4 1994 D661 11 PASI-A
EPA 7470A BM 1 PASI-A
SM 3500-Cr B-2011 JMH 1 PASI-A
92661129003 INF A EPA 200.7 Rev 4.4 1994 D661 11 PASI-A
EPA 7470A BM 1 PASI-A
SM 3500-Cr B-2011 JMH 1 PASI-A
92661129004 INF B EPA 200.7 Rev 4.4 1994 D661 11 PASI-A
EPA 7470A BM 1 PASI-A
SM 3500-Cr B-2011 JMH 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
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(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
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078
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ANALYTICAL RESULTS
Project: NOKIA
Pace Project No.: 92661129
Sample: FE-151 Lab ID: 92661129001 Collected: 04/05/23 15:15 Received: 04/06/23 14:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method: EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease ND mg/L 4.9 1 04/14/23 16:53
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:30 7440-38-2
Barium 31.6 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-39-3
Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:30 7440-43-9
Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-47-3
Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-50-8
Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:30 7439-89-6
Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7439-92-1
Manganese 964 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7439-96-5
Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:30 7782-49-2
Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-22-4
Zinc 50.7 ug/L 10.0 1 04/10/23 09:13 04/24/23 15:30 7440-66-6
7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:18 7439-97-6
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services-Charlotte
Tetrachloroethene ND ug/L 1.0 1 04/13/23 22:23 127-18-4
Surrogates
4-Bromofluorobenzene(S) 97 % 70-130 1 04/13/23 22:23 460-00-4
1,2-Dichloroethane-d4(S) 109 % 70-130 1 04/13/23 22:23 17060-07-0
Toluene-d8(S) 101 % 70-130 1 04/13/23 22:23 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 254OD-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 04/11/23 12:18
Chromium, Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011
Pace Analytical Services-Asheville
Chromium, Hexavalent ND mg/L 0.010 1 04/07/23 15:46 18540-29-9
REPORT OF LABORATORY ANALYSIS
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Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 19
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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ANALYTICAL RESULTS
Project: NOKIA
Pace Project No.: 92661129
Sample: AS EFFLUENT Lab ID: 92661129002 Collected: 04/05/23 15:10 Received: 04/06/23 14:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:33 7440-38-2
Barium 31.9 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-39-3
Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:33 7440-43-9
Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-47-3
Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-50-8
Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:33 7439-89-6
Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7439-92-1
Manganese 994 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7439-96-5
Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:33 7782-49-2
Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-22-4
Zinc 56.8 ug/L 10.0 1 04/10/23 09:13 04/24/23 15:33 7440-66-6
7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:20 7439-97-6
Chromium,Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011
Pace Analytical Services-Asheville
Chromium, Hexavalent ND mg/L 0.010 1 04/07/23 15:46 18540-29-9
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA
Pace Project No.: 92661129
Sample: INF A Lab ID: 92661129003 Collected: 04/05/23 15:00 Received: 04/06/23 14:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:36 7440-38-2
Barium 38.0 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-39-3
Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:36 7440-43-9
Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-47-3
Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-50-8
Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:36 7439-89-6
Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7439-92-1
Manganese 1290 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7439-96-5
Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:36 7782-49-2
Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-22-4
Zinc 67.5 ug/L 10.0 1 04/10/23 09:13 04/24/23 15:36 7440-66-6
7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:22 7439-97-6
Chromium,Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011
Pace Analytical Services-Asheville
Chromium, Hexavalent ND mg/L 0.010 1 04/07/23 15:46 18540-29-9
REPORT OF LABORATORY ANALYSIS
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Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 19
Pace Analytical Services,LLC
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Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA
Pace Project No.: 92661129
Sample: INF B Lab ID: 92661129004 Collected: 04/05/23 15:05 Received: 04/06/23 14:20 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:39 7440-38-2
Barium 16.6 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-39-3
Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:39 7440-43-9
Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-47-3
Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-50-8
Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:39 7439-89-6
Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7439-92-1
Manganese ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7439-96-5
Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:39 7782-49-2
Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-22-4
Zinc ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:39 7440-66-6
7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A
Pace Analytical Services-Asheville
Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:25 7439-97-6
Chromium,Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011
Pace Analytical Services-Asheville
Chromium, Hexavalent 0.014 mg/L 0.010 1 04/07/23 15:47 18540-29-9
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92661129
QC Batch: 768204 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92661129001
METHOD BLANK: 3988481 Matrix: Water
Associated Lab Samples: 92661129001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 04/14/23 16:53
LABORATORY CONTROL SAMPLE: 3988482
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 41.1 103 78-114
MATRIX SPIKE SAMPLE: 3988483
35789915002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 1 AJ 40 34.6 83 78-114
SAMPLE DUPLICATE: 3988484
92660477006 Dup
Parameter Units Result Result RPD Qualifiers
Oil and Grease mg/L ND ND
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92661129
QC Batch: 767747 Analysis Method: EPA 7470A
QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004
METHOD BLANK: 3986252 Matrix: Water
Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.20 04/14/2313:09
LABORATORY CONTROL SAMPLE: 3986253
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury ug/L 2.5 2.9 115 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3986254 3986255
MS MSD
92660002001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 2.5 2.5 2.8 2.7 113 109 75-125 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92661129
QC Batch: 767001 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004
METHOD BLANK: 3982453 Matrix: Water
Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Arsenic ug/L ND 10.0 04/24/2314:55
Barium ug/L ND 5.0 04/24/2314:55
Cadmium ug/L ND 1.0 04/24/2314:55
Chromium ug/L ND 5.0 04/24/2314:55
Copper ug/L ND 5.0 04/24/2314:55
Iron ug/L ND 50.0 04/24/2314:55
Lead ug/L ND 5.0 04/24/2314:55
Manganese ug/L ND 5.0 04/24/2314:55
Selenium ug/L ND 10.0 04/24/2314:55
Silver ug/L ND 5.0 04/24/2314:55
Zinc ug/L ND 10.0 04/24/2314:55
LABORATORY CONTROL SAMPLE: 3982454
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Arsenic ug/L 500 480 96 85-115
Barium ug/L 500 490 98 85-115
Cadmium ug/L 500 486 97 85-115
Chromium ug/L 500 486 97 85-115
Copper ug/L 500 485 97 85-115
Iron ug/L 5000 4850 97 85-115
Lead ug/L 500 486 97 85-115
Manganese ug/L 500 493 99 85-115
Selenium ug/L 500 474 95 85-115
Silver ug/L 250 240 96 85-115
Zinc ug/L 500 482 96 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3982455 3982456
MS MSD
92660310001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Arsenic ug/L ND 500 500 539 532 107 106 70-130 1
Barium ug/L 0.021 500 500 534 528 102 101 70-130 1
mg/L
Cadmium ug/L ND 500 500 480 471 96 94 70-130 2
Chromium ug/L 0.022 500 500 518 511 99 98 70-130 1
mg/L
Copper ug/L ND 500 500 581 572 116 114 70-130 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92661129
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3982455 3982456
MS MSD
92660310001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Iron ug/L 0.52 5000 5000 5530 5490 100 99 70-130 1
mg/L
Lead ug/L 0.011 500 500 506 500 99 98 70-130 1
mg/L
Manganese ug/L 0.18 500 500 687 677 101 99 70-130 1
mg/L
Selenium ug/L ND 500 500 523 515 105 103 70-130 2
Silver ug/L ND 250 250 277 272 111 109 70-130 2
Zinc ug/L ND 500 500 479 473 94 93 70-130 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3982457 3982458
MS MSD
92661171001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Arsenic ug/L ND 500 500 503 506 101 101 70-130 0
Barium ug/L 8.4 500 500 506 512 100 101 70-130 1
Cadmium ug/L ND 500 500 490 497 98 99 70-130 1
Chromium ug/L ND 500 500 500 504 100 101 70-130 1
Copper ug/L ND 500 500 506 507 101 101 70-130 0
Iron ug/L 94.2 5000 5000 5130 5160 101 101 70-130 0
Lead ug/L ND 500 500 492 496 98 99 70-130 1
Manganese ug/L 38.6 500 500 541 546 100 101 70-130 1
Selenium ug/L ND 500 500 514 517 103 103 70-130 1
Silver ug/L ND 250 250 247 248 99 99 70-130 0
Zinc ug/L 116 500 500 611 614 99 100 70-130 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92661129
QC Batch: 767946 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92661129001
METHOD BLANK: 3987374 Matrix: Water
Associated Lab Samples: 92661129001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Tetrachloroethene ug/L ND 1.0 04/13/23 14:14
1,2-Dichloroethane-d4(S) % 108 70-130 04/13/23 14:14
4-Bromofluorobenzene(S) % 98 70-130 04/13/23 14:14
Toluene-d8(S) % 99 70-130 04/13/23 14:14
LABORATORY CONTROL SAMPLE: 3987375
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Tetrachloroethene ug/L 20 21.9 110 70-130
1,2-Dichloroethane-d4(S) % 103 70-130
4-Bromofluorobenzene(S) % 103 70-130
Toluene-d8(S) % 101 70-130
MATRIX SPIKE SAMPLE: 3987377
92660170002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Tetrachloroethene ug/L 1.1 20 25.4 122 70-145
1,2-Dichloroethane-d4(S) % 103 70-130
4-Bromofluorobenzene(S) % 99 70-130
Toluene-d8(S) % 98 70-130
SAMPLE DUPLICATE: 3987376
92660170001 Dup
Parameter Units Result Result RPD Qualifiers
Tetrachloroethene ug/L ND ND
1,2-Dichloroethane-d4(S) % 109 105
4-Bromofluorobenzene(S) % 97 98
Toluene-d8(S) % 101 99
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92661129
QC Batch: 767255 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92661129001
METHOD BLANK: 3983720 Matrix: Water
Associated Lab Samples: 92661129001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 04/11/23 12:17
LABORATORY CONTROL SAMPLE: 3983721
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 238 95 90-110
SAMPLE DUPLICATE: 3983986
92660578001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 27.5 34.0 21
SAMPLE DUPLICATE: 3983987
92661365001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 126 124 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 19
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92661129
QC Batch: 766684 Analysis Method: SM 3500-Cr B-2011
QC Batch Method: SM 3500-Cr B-2011 Analysis Description: Chromium,Hexavalent by SM3500-Cr B-2011
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004
METHOD BLANK: 3981067 Matrix: Water
Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chromium, Hexavalent mg/L ND 0.010 04/07/23 15:42
LABORATORY CONTROL SAMPLE: 3981068
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chromium, Hexavalent mg/L 0.25 0.26 102 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3981069 3981070
MS MSD
92661128001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chromium, Hexavalent mg/L 0.010 0.25 0.25 0.27 0.27 102 105 90-110 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 19
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: NOKIA
Pace Project No.: 92661129
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 19
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA
Pace Project No.: 92661129
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92661129001 FE-151 EPA1664B 768204
92661129001 FE-151 EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134
92661129002 AS EFFLUENT EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134
92661129003 INF A EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134
92661129004 INF B EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134
92661129001 FE-151 EPA 7470A 767747 EPA 7470A 768057
92661129002 AS EFFLUENT EPA 7470A 767747 EPA 7470A 768057
92661129003 INF A EPA 7470A 767747 EPA 7470A 768057
92661129004 INF B EPA 7470A 767747 EPA 7470A 768057
92661129001 FE-151 EPA 8260D 767946
92661129001 FE-151 SM 2540D-2015 767255
92661129001 FE-151 SM 3500-CrB-2011 766684
92661129002 AS EFFLUENT SM 3500-Cr B-2011 766684
92661129003 INF A SM 3500-CrB-2011 766684
92661129004 INF B SM 3500-CrB-2011 766684
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 19
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon recelpt Date preservatlon adjusted Time preservatlon Amount of Preservative Lot R
adjusted added
Note: Wheneverthere Is a discrepancy affecdL,g North Carolina compltarce samples,a cofrr of this formwi II be sent to the NorthCarolira DENR Certificatlon Office(i.e.
Out cl hold,incorrect preservative,out of temp,incoreect containers, Page 18 of 19
Hexavalent Chromium pH Adjustment
7199 WH 9.0-9.5
218.6 WH 9.3-9.7 �D✓"`
Project number: No ��' " L°-7p I S 5
Initial Adjusted
Volume
Sample ID Initial pH Date/Time Date/Time Adjusted pH Acld/Base Used
(Drops)
Fe - is "6- A -5 ,35 �
Page 19 of 19
Pace Analytical Services,LLC
9800 Kin
aceAnalytical® ey Ave. Suite 100
Huntersville,NC 28078078
www.pacelabs.com (704)875-9092
May 08, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Blvd
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA WS
Pace Project No.: 92664610
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on April 26, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace National-Mt.Juliet
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-�)GlAA ,
Bonnie Vang V
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
f.Y�P
2" REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 1 of 13
e
Pace Analytical Services,LLC
te 100
laceAnalytical
9800HuIntesvlle,NC128078
wwwww..paclabs.com
(704)875-9092
CERTIFICATIONS
Project: NOKIA WS
Pace Project No.: 92664610
Pace Analytical Services National
12065 Lebanon Road,Mt.Juliet,TN 37122 Nevada Certification#:TN-03-2002-34
Alabama Certification#:40660 New Hampshire Certification#: 2975
Alaska Certification 17-026 New Jersey Certification#:TNO02
Arizona Certification#:AZ0612 New Mexico DW Certification
Arkansas Certification#:88-0469 New York Certification#: 11742
California Certification#:2932 North Carolina Aquatic Toxicity Certification#:41
Canada Certification#: 1461.01 North Carolina Drinking Water Certification#:21704
Colorado Certification#:TN00003 North Carolina Environmental Certificate#:375
Connecticut Certification#:PH-0197 North Dakota Certification#:R-140
DOD Certification:#1461.01 Ohio VAP Certification#:CL0069
EPA#TN00003 Oklahoma Certification#:9915
Florida Certification#: E87487 Oregon Certification#:TN200002
Georgia DW Certification#:923 Pennsylvania Certification#:68-02979
Georgia Certification:NELAP Rhode Island Certification#:LA000356
Idaho Certification#:TN00003 South Carolina Certification#:84004
Illinois Certification#:200008 South Dakota Certification
Indiana Certification#:C-TN-01 Tennessee DW/Chem/Micro Certification#: 2006
Iowa Certification#:364 Texas Certification#:T 104704245-17-14
Kansas Certification#:E-10277 Texas Mold Certification#:LAB0152
Kentucky UST Certification#: 16 USDA Soil Permit#: P330-15-00234
Kentucky Certification#:90010 Utah Certification#:TN00003
Louisiana Certification#:A130792 Virginia Certification#:VT2006
Louisiana DW Certification#:LA180010 Vermont Dept.of Health: ID#VT-2006
Maine Certification#:TN0002 Virginia Certification#:460132
Maryland Certification#:324 Washington Certification#:C847
Massachusetts Certification#:M-TNO03 West Virginia Certification#:233
Michigan Certification#:9958 Wisconsin Certification#:998093910
Minnesota Certification#:047-999-395 Wyoming UST Certification#:via A21LA 2926.01
Mississippi Certification#:TN00003 A2LA-ISO 17025 Certification#: 1461.01
Missouri Certification#:340 A2LA-ISO 17025 Certification#: 1461.02
Montana Certification#:CERT0086 AIHA-LAP/LLC EMLAP Certification#:100789
Nebraska Certification#:NE-OS-15-05
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project: NOKIA WS
Pace Project No.: 92664610
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92664610001 AS EFFLUENT EPA200.7 ZSA 11 PAN
EPA 245.1 LAS 1 PAN
EPA 8260D TMH 4 PASI-C
SM 3500-Cr B-2011 JMH 1 PASI-A
PAN=Pace National-Mt.Juliet
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92664610
Sample: AS EFFLUENT Lab ID: 92664610001 Collected: 04/25/23 10:20 Received: 04/26/23 17:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Metals(ICP)200.7 Analytical Method: EPA 200.7 Preparation Method:200.7
Pace National-Mt.Juliet
Arsenic ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7440-38-2
Barium 32.5 ug/L 5.00 1 05/07/23 09:50 05/07/23 16:36 7440-39-3
Cadmium ND ug/L 2.00 1 05/07/23 09:50 05/07/23 16:36 7440-43-9
Chromium ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7440-47-3
Copper ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7440-50-8
Iron ND ug/L 50.0 1 05/07/23 09:50 05/07/23 16:36 7439-89-6
Lead ND ug/L 5.00 1 05/07/23 09:50 05/07/23 16:36 7439-92-1
Manganese 1020 ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7439-96-5
Selenium ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7782-49-2
Silver ND ug/L 5.00 1 05/07/23 09:50 05/07/23 16:36 7440-22-4
Zinc 55.2 ug/L 50.0 1 05/07/23 09:50 05/07/23 16:36 7440-66-6
Mercury 245.1 Analytical Method: EPA 245.1 Preparation Method:245.1
Pace National-Mt.Juliet
Mercury ND ug/L 0.200 1 04/30/23 22:14 05/01/23 13:33 7439-97-6
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services-Charlotte
Tetrachloroethene 3.7 ug/L 1.0 1 04/30/23 09:13 127-18-4
Surrogates
4-Bromofluorobenzene(S) 101 % 70-130 1 04/30/23 09:13 460-00-4
1,2-Dichloroethane-d4(S) 106 % 70-130 1 04/30/23 09:13 17060-07-0
Toluene-d8(S) 106 % 70-130 1 04/30/23 09:13 2037-26-5
Chromium, Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011
Pace Analytical Services-Asheville
Chromium, Hexavalent ND mg/L 0.010 1 04/29/23 16:12 18540-29-9
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WS
Pace Project No.: 92664610
QC Batch: 2055073 Analysis Method: EPA 200.7
QC Batch Method: 200.7 Analysis Description: Metals(ICP)200.7
Laboratory: Pace National-Mt.Juliet
Associated Lab Samples: 92664610001
METHOD BLANK: R3921853-1 Matrix: Water
Associated Lab Samples: 92664610001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Arsenic ug/L ND 10.0 05/07/2315:55
Barium ug/L ND 5.00 05/07/2315:55
Cadmium ug/L ND 2.00 05/07/2315:55
Chromium ug/L ND 10.0 05/07/2315:55
Copper ug/L ND 10.0 05/07/2315:55
Iron ug/L ND 50.0 05/07/2315:55
Lead ug/L ND 5.00 05/07/2315:55
Manganese ug/L ND 10.0 05/07/2315:55
Selenium ug/L ND 10.0 05/07/2315:55
Silver ug/L ND 5.00 05/07/2315:55
Zinc ug/L ND 50.0 05/07/2315:55
LABORATORY CONTROL SAMPLE: R3921853-2
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Arsenic ug/L 1000 977 97.7 85.0-115
Barium ug/L 1000 990 99.0 85.0-115
Cadmium ug/L 1000 987 98.7 85.0-115
Chromium ug/L 1000 953 95.3 85.0-115
Copper ug/L 1000 976 97.6 85.0-115
Iron ug/L 10000 9680 96.8 85.0-115
Lead ug/L 1000 980 98.0 85.0-115
Manganese ug/L 1000 921 92.1 85.0-115
Selenium ug/L 1000 1040 104 85.0-115
Silver ug/L 200 193 96.7 85.0-115
Zinc ug/L 1000 982 98.2 85.0-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3921853-4 R3921853-5
MS MSD
L1611232-01 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Arsenic ug/L ND 1000 1000 1080 1070 108 107 70.0-130 1.44
Barium ug/L 158 1000 1000 1210 1180 105 103 70.0-130 1.80
Cadmium ug/L ND 1000 1000 1090 1060 109 106 70.0-130 2.04
Chromium ug/L 1.94 1000 1000 1030 1020 103 101 70.0-130 1.64
Copper ug/L ND 1000 1000 1050 1030 105 103 70.0-130 1.45
Iron ug/L 153 10000 10000 10400 10300 103 102 70.0-130 1.34
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville,NC 28078
078
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QUALITY CONTROL DATA
Project: NOKIA WS
Pace Project No.: 92664610
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3921853-4 R3921853-5
MS MSD
L1611232-01 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Lead ug/L ND 1000 1000 1070 1050 107 105 70.0-130 2.17
Manganese ug/L 2.26 1000 1000 994 972 99.2 97.0 70.0-130 2.25
Selenium ug/L ND 1000 1000 1160 1150 116 115 70.0-130 1.09
Silver ug/L ND 200 200 210 206 105 103 70.0-130 1.84
Zinc ug/L 49.5 1000 1000 1070 1050 103 100 70.0-130 2.10
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3921853-6 R3921853-7
MS MSD
L1612317-08 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Arsenic ug/L ND 1000 1000 1070 1100 107 110 70.0-130 2.93
Barium ug/L 15.4 1000 1000 1040 1050 102 104 70.0-130 1.23
Cadmium ug/L ND 1000 1000 1060 1090 106 109 70.0-130 2.65
Chromium ug/L ND 1000 1000 994 1020 99.4 102 70.0-130 2.36
Copper ug/L 4.87 1000 1000 1050 1080 104 107 70.0-130 2.51
Iron ug/L 383 10000 10000 10300 10500 99.5 102 70.0-130 2.05
Lead ug/L ND 1000 1000 1040 1080 104 108 70.0-130 3.18
Manganese ug/L 58.9 1000 1000 1000 1030 94.3 96.8 70.0-130 2.48
Selenium ug/L ND 1000 1000 1130 1190 113 119 70.0-130 4.62
Silver ug/L ND 200 200 187 193 93.3 96.4 70.0-130 3.21
Zinc ug/L 33.1 1000 1000 1050 1090 102 105 70.0-130 3.10
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WS
Pace Project No.: 92664610
QC Batch: 2051541 Analysis Method: EPA 245.1
QC Batch Method: 245.1 Analysis Description: Mercury 245.1
Laboratory: Pace National-Mt.Juliet
Associated Lab Samples: 92664610001
METHOD BLANK: R3919487-1 Matrix: Water
Associated Lab Samples: 92664610001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L ND 0.200 05/01/2312:41
LABORATORY CONTROL SAMPLE: R3919487-2
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Mercury ug/L 3.00 3.20 107 85.0-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3919487-3 R3919487-4
MS MSD
L1609306-01 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 3.00 3.00 3.23 3.17 108 106 70.0-130 1.99
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3919487-5 R3919487-6
MS MSD
L1609589-01 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Mercury ug/L ND 3.00 3.00 3.35 3.25 112 108 70.0-130 2.81
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WS
Pace Project No.: 92664610
QC Batch: 771354 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92664610001
METHOD BLANK: 4004348 Matrix: Water
Associated Lab Samples: 92664610001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Tetrachloroethene ug/L ND 1.0 04/30/23 03:03
1,2-Dichloroethane-d4(S) % 108 70-130 04/30/23 03:03
4-Bromofluorobenzene(S) % 105 70-130 04/30/23 03:03
Toluene-d8(S) % 102 70-130 04/30/23 03:03
LABORATORY CONTROL SAMPLE: 4004349
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Tetrachloroethene ug/L 20 18.2 91 70-130
1,2-Dichloroethane-d4(S) % 104 70-130
4-Bromofluorobenzene(S) % 98 70-130
Toluene-d8(S) % 101 70-130
MATRIX SPIKE SAMPLE: 4004351
92664150011 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Tetrachloroethene ug/L 20 19.8 99 70-145
1,2-Dichloroethane-d4(S) % 100 70-130
4-Bromofluorobenzene(S) % 101 70-130
Toluene-d8(S) % 102 70-130
SAMPLE DUPLICATE: 4004350
92664150009 Dup
Parameter Units Result Result RPD Qualifiers
Tetrachloroethene ug/L ND
1,2-Dichloroethane-d4(S) % 105 91
4-Bromofluorobenzene(S) % 95 96
Toluene-d8(S) % 101 99
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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QUALITY CONTROL DATA
Project: NOKIA WS
Pace Project No.: 92664610
QC Batch: 771294 Analysis Method: SM 3500-Cr B-2011
QC Batch Method: SM 3500-Cr B-2011 Analysis Description: Chromium,Hexavalent by SM3500-Cr B-2011
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92664610001
METHOD BLANK: 4004162 Matrix: Water
Associated Lab Samples: 92664610001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chromium, Hexavalent mg/L ND 0.010 04/29/23 16:12
LABORATORY CONTROL SAMPLE: 4004163
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chromium, Hexavalent mg/L 0.25 0.25 100 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4004164 4004165
MS MSD
92664610001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chromium, Hexavalent mg/L ND 0.25 0.25 0.26 0.25 102 96 90-110 6
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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Huntersville,NC 28078
078
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QUALIFIERS
Project: NOKIA WS
Pace Project No.: 92664610
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA WS
Pace Project No.: 92664610
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92664610001 AS EFFLUENT 200.7 2055073 EPA200.7 2055073
92664610001 AS EFFLUENT 245.1 2051541 EPA245.1 2051541
92664610001 AS EFFLUENT EPA8260D 771354
92664610001 AS EFFLUENT SM 3500-Cr B-2011 771294
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 13
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ce' QC#_Tlfle: ENV-FRM-HUN1.008$v02_Sample Conditlon Upon Receipt
a
Effectivo Date: 11/14/2022.8:1830 AM
*Check mark top half of box If pH and/or dechlorination Is verified and Project h WO# : 92664610
within the acceptance range for preservation samples, PM: BV Due Date: 05/08/23
Exceptions:VOA,Conform;TpC,OII and Grease,DRO/8015(water)ROC, LLHg CLIENT: 92—AECOM—RAL
*"Bottom half of box is o list number of bottles
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pH Adjustment Log for Preserved Samples
Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time,preservation Amount of Preservative Lot It
adjusted added
Note: Whenever there Is adisereparcyaffe:tirgNorthCaro!:na compliance samples,acopyofthisformwill besen't to the NorthCaroliraDENR Certification Office fi.e.
Out of hold, Incorrect preservative, cut of temp,incorrect containers.
Page 13 of 13
Pace Analytical Services,LLC
9800 Kin
aceAnalytical® ey Ave. Suite 100
Huntersville,NC 28078078
www.pacelabs.com (704)875-9092
May 30, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on May 19, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
• Pace Analytical Services-Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-�)GlAA ,
Bonnie Vang V
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
Cristin Dolan,AECOM
Teresa Amentt Jennings,AECOM
Jon Wakeman,AECOM Environment
2� REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 1 of 12
e
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078
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CERTIFICATIONS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
Pace Analytical Services Ormond Beach
8 East Tower Circle,Ormond Beach, FL 32174 Missouri Certification#:236
Alaska DEC-CS/UST/LUST Montana Certification#:Cert 0074
Alabama Certification#:41320 Nebraska Certification: NE-OS-28-14
Colorado Certification: FL NELAC Reciprocity New Hampshire Certification#:2958
Connecticut Certification#: PH-0216 New Jersey Certification#: FL022
Delaware Certification: FL NELAC Reciprocity New York Certification#: 11608
DoD-ANAB#:ADE-3199 North Carolina Environmental Certificate#:667
Florida Certification#: E83079 North Carolina Certification#: 12710
Georgia Certification#:955 North Dakota Certification#:R-216
Guam Certification: FL NELAC Reciprocity Ohio DEP 87780
Hawaii Certification:FL NELAC Reciprocity Oklahoma Certification#: D9947
Illinois Certification#:200068 Pennsylvania Certification#:68-00547
Indiana Certification: FL NELAC Reciprocity Puerto Rico Certification#: FLO1264
Kansas Certification#:E-10383 South Carolina Certification:#96042001
Kentucky Certification#:90050 Tennessee Certification#:TN02974
Louisiana Certification#: FL NELAC Reciprocity Texas Certification:FL NELAC Reciprocity
Louisiana Environmental Certificate#:05007 US Virgin Islands Certification:FL NELAC Reciprocity
Maine Certification#: FLO1264 Virginia Environmental Certification#:460165
Maryland Certification:#346 West Virginia Certification#:9962C
Massachusetts Certification#:M-FL1264 Wisconsin Certification#:399079670
Michigan Certification#:9911 Wyoming(EPA Region 8): FL NELAC Reciprocity
Mississippi Certification:FL NELAC Reciprocity
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100, Huntersville, NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#: LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 2 of 12
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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SAMPLE ANALYTE COUNT
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92668464001 FE-151 EPA 1664E REL 1 PASI-C
EPA 200.7 KC2 3 PASI-O
EPA 8260D LMB 4 PASI-C
SM 2540D-2015 JMH1 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
PASI-O=Pace Analytical Services-Ormond Beach
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 3 of 12
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
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078
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ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
Sample: FE-151 Lab ID: 92668464001 Collected: 05/18/23 13:00 Received: 05/19/23 09:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
HEM,Oil and Grease Analytical Method: EPA 1664E
Pace Analytical Services-Charlotte
Oil and Grease 7.9 mg/L 4.9 1 05/23/23 05:06
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 28.8 ug/L 10.0 1 05/24/23 16:29 05/27/23 07:11 7440-39-3
Manganese 10.3 ug/L 5.0 1 05/24/23 16:29 05/27/23 07:11 7439-96-5
Zinc ND ug/L 20.0 1 05/24/23 16:29 05/27/23 07:11 7440-66-6
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services-Charlotte
Tetrachloroethene 2.1 ug/L 1.0 1 05/24/23 04:16 127-18-4
Surrogates
4-Bromofluorobenzene(S) 102 % 70-130 1 05/24/23 04:16 460-00-4
1,2-Dichloroethane-d4(S) 96 % 70-130 1 05/24/23 04:16 17060-07-0
Toluene-d8(S) 103 % 70-130 1 05/24/23 04:16 2037-26-5
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 05/24/23 11:20
REPORT OF LABORATORY ANALYSIS
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Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 12
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
QC Batch: 776097 Analysis Method: EPA 1664B
QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92668464001
METHOD BLANK: 4026843 Matrix: Water
Associated Lab Samples: 92668464001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Oil and Grease mg/L ND 5.0 05/23/23 05:06
LABORATORY CONTROL SAMPLE: 4026844
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L 40 32.5 81 78-114
MATRIX SPIKE SAMPLE: 4026845
92668256002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Oil and Grease mg/L ND 38.5 35.0 91 78-114
SAMPLE DUPLICATE: 4026846
92668288002 Dup
Parameter Units Result Result RPD Qualifiers
Oil and Grease mg/L ND ND
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
QC Batch: 920601 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Ormond Beach
Associated Lab Samples: 92668464001
METHOD BLANK: 5061930 Matrix: Water
Associated Lab Samples: 92668464001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 10.0 05/27/23 05:19
Manganese ug/L ND 5.0 05/27/23 05:19
Zinc ug/L ND 20.0 05/27/23 05:19
LABORATORY CONTROL SAMPLE: 5061931
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 250 259 104 85-115
Manganese ug/L 250 262 105 85-115
Zinc ug/L 1250 1340 107 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5061932 5061933
MS MSD
35801496001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 71.4 250 250 330 335 103 106 70-130 2
Manganese ug/L 83.3 250 250 334 340 100 103 70-130 2
Zinc ug/L 662 1250 1250 1890 1930 98 101 70-130 2
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5061934 5061935
MS MSD
92667772006 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 173 250 250 440 427 107 101 70-130 3
Manganese ug/L 559 250 250 826 804 107 98 70-130 3
Zinc ug/L ND 1250 1250 1360 1330 108 106 70-130 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Huntersville,NC 28078
078
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QUALITY CONTROL DATA
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
QC Batch: 776373 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92668464001
METHOD BLANK: 4027995 Matrix: Water
Associated Lab Samples: 92668464001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Tetrachloroethene ug/L ND 1.0 05/23/23 22:55
1,2-Dichloroethane-d4(S) % 95 70-130 05/23/23 22:55
4-Bromofluorobenzene(S) % 104 70-130 05/23/23 22:55
Toluene-d8(S) % 103 70-130 05/23/23 22:55
LABORATORY CONTROL SAMPLE: 4027996
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Tetrachloroethene ug/L 20 18.0 90 70-130
1,2-Dichloroethane-d4(S) % 102 70-130
4-Bromofluorobenzene(S) % 101 70-130
Toluene-d8(S) % 99 70-130
MATRIX SPIKE SAMPLE: 4027998
92668464001 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Tetrachloroethene ug/L 2.1 20 24.6 113 70-145
1,2-Dichloroethane-d4(S) % 97 70-130
4-Bromofluorobenzene(S) % 101 70-130
Toluene-d8(S) % 100 70-130
SAMPLE DUPLICATE: 4027997
92668421001 Dup
Parameter Units Result Result RPD Qualifiers
Tetrachloroethene ug/L ND ND
1,2-Dichloroethane-d4(S) % 99 93
4-Bromofluorobenzene(S) % 105 101
Toluene-d8(S) % 102 103
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
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Huntersville,NC 28078
078
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QUALITY CONTROL DATA
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
QC Batch: 776583 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92668464001
METHOD BLANK: 4028873 Matrix: Water
Associated Lab Samples: 92668464001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 05/24/23 11:17
LABORATORY CONTROL SAMPLE: 4028874
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 246 98 90-110
SAMPLE DUPLICATE: 4029014
92668450001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 4020 4140 3
SAMPLE DUPLICATE: 4029015
92668629001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 222 232 4
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 12
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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QUALIFIERS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA WINSTON SALEM
Pace Project No.: 92668464
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92668464001 FE-151 EPA1664B 776097
92668464001 FE-151 EPA 200.7 920601 EPA 200.7 920640
92668464001 FE-151 EPA 8260D 776373
92668464001 FE-151 SM 254OD-2015 776583
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 12
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Pace Analytical Services,LLC
9800 Kin
aceAnalytical® ey Ave. Suite 100
Huntersville,NC 28078078
www.pacelabs.com (704)875-9092
June 02, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA
Pace Project No.: 92669092
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on May 24, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,Q - aAAa,
Bonnie Vang
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
Cristin Dolan,AECOM
Teresa Amentt Jennings,AECOM
Jon Wakeman,AECOM Environment
z REPORT OF LABORATORY ANALYSIS
N This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 9
6
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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CERTIFICATIONS
Project: NOKIA
Pace Project No.: 92669092
Pace Analytical Services Ormond Beach
8 East Tower Circle,Ormond Beach, FL 32174 Missouri Certification#:236
Alaska DEC-CS/UST/LUST Montana Certification#:Cert 0074
Alabama Certification#:41320 Nebraska Certification: NE-OS-28-14
Colorado Certification: FL NELAC Reciprocity New Hampshire Certification#:2958
Connecticut Certification#: PH-0216 New Jersey Certification#: FL022
Delaware Certification: FL NELAC Reciprocity New York Certification#: 11608
DoD-ANAB#:ADE-3199 North Carolina Environmental Certificate#:667
Florida Certification#: E83079 North Carolina Certification#: 12710
Georgia Certification#:955 North Dakota Certification#:R-216
Guam Certification: FL NELAC Reciprocity Ohio DEP 87780
Hawaii Certification:FL NELAC Reciprocity Oklahoma Certification#: D9947
Illinois Certification#:200068 Pennsylvania Certification#:68-00547
Indiana Certification: FL NELAC Reciprocity Puerto Rico Certification#: FLO1264
Kansas Certification#:E-10383 South Carolina Certification:#96042001
Kentucky Certification#:90050 Tennessee Certification#:TN02974
Louisiana Certification#: FL NELAC Reciprocity Texas Certification:FL NELAC Reciprocity
Louisiana Environmental Certificate#:05007 US Virgin Islands Certification:FL NELAC Reciprocity
Maine Certification#: FLO1264 Virginia Environmental Certification#:460165
Maryland Certification:#346 West Virginia Certification#:9962C
Massachusetts Certification#:M-FL1264 Wisconsin Certification#:399079670
Michigan Certification#:9911 Wyoming(EPA Region 8): FL NELAC Reciprocity
Mississippi Certification:FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 2 of 9
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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SAMPLE ANALYTE COUNT
Project: NOKIA
Pace Project No.: 92669092
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92669092001 FE-151 EPA 200.7 KPP 3 PASI-O
PASI-O=Pace Analytical Services-Ormond Beach
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 3 of 9
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
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ANALYTICAL RESULTS
Project: NOKIA
Pace Project No.: 92669092
Sample: FE-151 Lab ID: 92669092001 Collected: 05/23/23 12:00 Received: 05/24/23 12:15 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 31.5 ug/L 10.0 1 05/30/2315:45 06/01/2317:25 7440-39-3
Manganese 9.6 ug/L 5.0 1 05/30/2315:45 06/01/2317:25 7439-96-5
Zinc ND ug/L 20.0 1 05/30/2315:45 06/01/2317:25 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA
Pace Project No.: 92669092
QC Batch: 921841 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Ormond Beach
Associated Lab Samples: 92669092001
METHOD BLANK: 5067534 Matrix: Water
Associated Lab Samples: 92669092001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 10.0 06/01/2316:37
Manganese ug/L ND 5.0 06/01/2316:37
Zinc ug/L ND 20.0 06/01/2316:37
LABORATORY CONTROL SAMPLE: 5067535
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 250 278 111 85-115
Manganese ug/L 250 263 105 85-115
Zinc ug/L 1250 1280 102 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5067536 5067537
MS MSD
92669071001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 41.5 250 250 309 303 107 105 70-130 2
Manganese ug/L 712 250 250 971 951 104 96 70-130 2
Zinc ug/L 0.22 1250 1250 1530 1520 104 104 70-130 1
mg/L
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: NOKIA
Pace Project No.: 92669092
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/02/2023 11:30 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 9
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA
Pace Project No.: 92669092
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92669092001 FE-151 EPA 200.7 921841 EPA 200.7 921884
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:06/02/2023 11:30 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 9
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Pace Analytical Services,LLC
9800 Kin
aceAnalytical® ey Ave. Suite 100
Huntersville,NC 28078078
www.pacelabs.com (704)875-9092
May 09, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA WS
Pace Project No.: 92665668
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on May 03, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Ormond Beach
If you have any questions concerning this report, please feel free to contact me.
Sincerely,Q - aAAa,
Bonnie Vang
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
Cristin Dolan,AECOM
Jon Wakeman,AECOM Environment
fJ pP__
2" REPORT OF LABORATORY ANALYSIS
N This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 15
6
Pace Analytical Services,LLC
te 100
laceAnalytical
9800HuIntesvlle,NC128078
wwwww..paclabs.com
(704)875-9092
CERTIFICATIONS
Project: NOKIA WS
Pace Project No.: 92665668
Pace Analytical Services Ormond Beach
8 East Tower Circle,Ormond Beach,FL 32174 Missouri Certification#:236
Alaska DEC-CS/UST/LUST Montana Certification#:Cert 0074
Alabama Certification#:41320 Nebraska Certification:NE-OS-28-14
Colorado Certification:FL NELAC Reciprocity New Hampshire Certification#:2958
Connecticut Certification#:PH-0216 New Jersey Certification#:FL022
Delaware Certification:FL NELAC Reciprocity New York Certification#: 11608
Florida Certification#: E83079 North Carolina Environmental Certificate#:667
Georgia Certification#:955 North Carolina Certification#: 12710
Guam Certification:FL NELAC Reciprocity North Dakota Certification#:R-216
Hawaii Certification:FL NELAC Reciprocity Ohio DEP 87780
Illinois Certification#:200068 Oklahoma Certification#: D9947
Indiana Certification:FL NELAC Reciprocity Pennsylvania Certification#:68-00547
Kansas Certification#:E-10383 Puerto Rico Certification#:FLO1264
Kentucky Certification#:90050 South Carolina Certification:#96042001
Louisiana Certification#: FL NELAC Reciprocity Tennessee Certification#:TN02974
Louisiana Environmental Certificate#:05007 Texas Certification:FL NELAC Reciprocity
Maine Certification#: FL01264 US Virgin Islands Certification:FL NELAC Reciprocity
Maryland Certification:#346 Virginia Environmental Certification#:460165
Massachusetts Certification#:M-FL1264 West Virginia Certification#:9962C
Michigan Certification#:9911 Wisconsin Certification#:399079670
Mississippi Certification:FL NELAC Reciprocity Wyoming(EPA Region 8):FL NELAC Reciprocity
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 2 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
SAMPLE ANALYTE COUNT
Project: NOKIA WS
Pace Project No.: 92665668
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92665668001 EW-5 EPA200.7 AAM1 3 PASI-O
92665668002 EW-6 EPA200.7 AAM1, KPP 3 PASI-O
92665668003 EW-12 EPA200.7 AAM1 3 PASI-O
92665668004 EW-14 EPA200.7 AAM1 3 PASI-O
92665668005 EW-16 EPA200.7 AAM1 3 PASI-O
92665668006 EW-21 EPA200.7 AAM1 3 PASI-O
92665668007 NETWORKA EPA200.7 AAM1, KPP 3 PASI-O
PASI-O=Pace Analytical Services-Ormond Beach
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92665668
Sample: EW-5 Lab ID: 92665668001 Collected: 05/02/23 11:35 Received: 05/03/23 16:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 26.6 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:34 7440-39-3
Manganese ND ug/L 5.0 1 05/06/23 00:43 05/08/23 15:34 7439-96-5
Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:34 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92665668
Sample: EW-6 Lab ID: 92665668002 Collected: 05/02/23 11:40 Received: 05/03/23 16:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 38.4 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:37 7440-39-3
Manganese 2930 ug/L 50.0 10 05/06/23 00:43 05/09/23 01:48 7439-96-5
Zinc 128 ug/L 20.0 1 05/06/23 00:43 05/08/23 15:37 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92665668
Sample: EW-12 Lab ID: 92665668003 Collected: 05/02/23 11:45 Received: 05/03/23 16:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 44.4 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:41 7440-39-3
Manganese 8.9 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:41 7439-96-5
Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:41 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92665668
Sample: EW-14 Lab ID: 92665668004 Collected: 05/02/23 11:50 Received: 05/03/23 16:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 169 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:44 7440-39-3
Manganese 57.9 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:44 7439-96-5
Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:44 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92665668
Sample: EW-16 Lab ID: 92665668005 Collected: 05/02/23 11:30 Received: 05/03/23 16:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 26.1 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:48 7440-39-3
Manganese 12.8 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:48 7439-96-5
Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:48 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92665668
Sample: EW-21 Lab ID: 92665668006 Collected: 05/02/23 11:25 Received: 05/03/23 16:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 167 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:51 7440-39-3
Manganese 16.7 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:51 7439-96-5
Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:51 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WS
Pace Project No.: 92665668
Sample: NETWORK A Lab ID: 92665668007 Collected: 05/02/23 12:00 Received: 05/03/23 16:25 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Pace Analytical Services-Ormond Beach
Barium 39.7 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:54 7440-39-3
Manganese 2090 ug/L 25.0 5 05/06/23 00:43 05/09/23 01:51 7439-96-5
Zinc 96.6 ug/L 20.0 1 05/06/23 00:43 05/08/23 15:54 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WS
Pace Project No.: 92665668
QC Batch: 915271 Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Ormond Beach
Associated Lab Samples: 92665668001,92665668002,92665668003,92665668004,92665668005,92665668006,92665668007
METHOD BLANK: 5032684 Matrix: Water
Associated Lab Samples: 92665668001,92665668002,92665668003,92665668004,92665668005,92665668006,92665668007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 10.0 05/08/2314:49
Manganese ug/L ND 5.0 05/08/2314:49
Zinc ug/L ND 20.0 05/08/2314:49
LABORATORY CONTROL SAMPLE: 5032685
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 250 279 112 85-115
Manganese ug/L 250 268 107 85-115
Zinc ug/L 1250 1320 106 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5032686 5032687
MS MSD
35795734001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 12.1 250 250 262 236 100 89 70-130 10
Manganese ug/L 36.7 250 250 291 266 102 92 70-130 9
Zinc ug/L 199 1250 1250 1400 1310 96 89 70-130 7
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5032688 5032689
MS MSD
35796422001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 0.0063J 250 250 277 282 108 110 70-130 2
mg/L
Manganese ug/L 0.027 250 250 288 293 104 106 70-130 2
mg/L
Zinc ug/L 1.2 1250 1250 2470 2490 99 101 70-130 1
mg/L
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: NOKIA WS
Pace Project No.: 92665668
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 12 of 15
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA WS
Pace Project No.: 92665668
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92665668001 EW-5 EPA 200.7 915271 EPA 200.7 915285
92665668002 EW-6 EPA 200.7 915271 EPA 200.7 915285
92665668003 EW-12 EPA 200.7 915271 EPA 200.7 915285
92665668004 EW-14 EPA 200.7 915271 EPA 200.7 915285
92665668005 EW-16 EPA 200.7 915271 EPA 200.7 915285
92665668006 EW-21 EPA 200.7 915271 EPA 200.7 915285
92665668007 NETWORK A EPA 200.7 915271 EPA 200.7 915285
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 13 of 15
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Page 15 of 15
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
July 06, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA WINSTON-SALEM
Pace Project No.: 92674970
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on June 28, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,Q _ aAAa,
Bonnie Vang
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
Cristin Dolan,AECOM
Teresa Amentt Jennings,AECOM
Jon Wakeman,AECOM Environment
z REPORT OF LABORATORY ANALYSIS
N This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 9
6
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
CERTIFICATIONS
Project: NOKIA WINSTON-SALEM
Pace Project No.: 92674970
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 9
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: NOKIA WINSTON-SALEM
Pace Project No.: 92674970
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92674970001 AS EFFLUENT EPA 200.7 Rev 4.4 1994 D661 3 PASI-A
PASI-A=Pace Analytical Services-Asheville
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 9
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON-SALEM
Pace Project No.: 92674970
Sample: AS EFFLUENT Lab ID: 92674970001 Collected: 06/27/23 10:00 Received: 06/28/23 14:50 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Barium 32.3 ug/L 5.0 1 06/29/2317:29 06/30/2313:41 7440-39-3
Manganese 8.5 ug/L 5.0 1 06/29/2317:29 06/30/2313:41 7439-96-5
Zinc 14.3 ug/L 10.0 1 06/29/2317:29 06/30/2313:41 7440-66-6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 9
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WINSTON-SALEM
Pace Project No.: 92674970
QC Batch: 783949 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92674970001
METHOD BLANK: 4065875 Matrix: Water
Associated Lab Samples: 92674970001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 5.0 06/30/2313:23
Manganese ug/L ND 5.0 06/30/2313:23
Zinc ug/L ND 10.0 06/30/2313:23
LABORATORY CONTROL SAMPLE: 4065876
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 500 510 102 85-115
Manganese ug/L 500 512 102 85-115
Zinc ug/L 500 497 99 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4065877 4065878
MS MSD
92674970001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 32.3 500 500 550 538 104 101 70-130 2
Manganese ug/L 8.5 500 500 529 516 104 102 70-130 2
Zinc ug/L 14.3 500 500 524 510 102 99 70-130 3
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 9
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALIFIERS
Project: NOKIA WINSTON-SALEM
Pace Project No.: 92674970
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 9
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA WINSTON-SALEM
Pace Project No.: 92674970
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92674970001 AS EFFLUENT EPA 200.7 Rev 4.4 1994 783949 EPA 200.7 Rev 4.4 1994 784006
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 9
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1 Page or•'f9
_
Pace Analytical Services,LLC
(�IaceAnalyfical@ 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
July 03, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: LUCENT NOKIA
Pace Project No.: 92674332
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on June 23, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
-4jGlAA ,
Bonnie Vang V
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
Cristin Dolan,AECOM
Teresa Amentt Jennings,AECOM
Jon Wakeman,AECOM Environment
f.Y�P
2" REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 18
e
Pace Analytical Services,LLC
te 100
laceAnalytical
9800HuIntesvlle,NC128078
wwwww..paclabs.com
(704)875-9092
CERTIFICATIONS
Project: LUCENT NOKIA
Pace Project No.: 92674332
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 18
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
SAMPLE ANALYTE COUNT
Project: LUCENT NOKIA
Pace Project No.: 92674332
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92674332001 AS INFLUENT EPA 8260D JJK 63 PASI-C
92674332002 AS EFFLUENT EPA200.7 Rev4.4 1994 D13131 3 PASI-A
EPA 8260D JJK 63 PASI-C
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 18
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
ANALYTICAL RESULTS
Project: LUCENT NOKIA
Pace Project No.: 92674332
Sample: AS INFLUENT Lab ID: 92674332001 Collected: 06/22/23 15:45 Received: 06/23/23 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services-Charlotte
Acetone ND ug/L 125 5 06/26/23 00:34 67-64-1
Benzene ND ug/L 5.0 5 06/26/23 00:34 71-43-2
Bromobenzene ND ug/L 5.0 5 06/26/23 00:34 108-86-1
Bromochloromethane ND ug/L 5.0 5 06/26/23 00:34 74-97-5
Bromodichloromethane ND ug/L 5.0 5 06/26/23 00:34 75-27-4
Bromoform ND ug/L 5.0 5 06/26/23 00:34 75-25-2
Bromomethane ND ug/L 10.0 5 06/26/23 00:34 74-83-9
2-Butanone(MEK) ND ug/L 25.0 5 06/26/23 00:34 78-93-3
Carbon tetrachloride ND ug/L 5.0 5 06/26/23 00:34 56-23-5
Chlorobenzene ND ug/L 5.0 5 06/26/23 00:34 108-90-7
Chloroethane ND ug/L 5.0 5 06/26/23 00:34 75-00-3
Chloroform ND ug/L 5.0 5 06/26/23 00:34 67-66-3
Chloromethane ND ug/L 5.0 5 06/26/23 00:34 74-87-3
2-Chlorotoluene ND ug/L 5.0 5 06/26/23 00:34 95-49-8
4-Chlorotoluene ND ug/L 5.0 5 06/26/23 00:34 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 10.0 5 06/26/23 00:34 96-12-8
Dibromochloromethane ND ug/L 5.0 5 06/26/23 00:34 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 5.0 5 06/26/23 00:34 106-93-4
Dibromomethane ND ug/L 5.0 5 06/26/23 00:34 74-95-3
1,2-Dichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 95-50-1
1,3-Dichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 541-73-1
1,4-Dichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 106-46-7
Dichlorodifluoromethane ND ug/L 5.0 5 06/26/23 00:34 75-71-8
1,1-Dichloroethane ND ug/L 5.0 5 06/26/23 00:34 75-34-3
1,2-Dichloroethane ND ug/L 5.0 5 06/26/23 00:34 107-06-2
1,1-Dichloroethene ND ug/L 5.0 5 06/26/23 00:34 75-35-4
cis-1,2-Dichloroethene 190 ug/L 5.0 5 06/26/23 00:34 156-59-2
trans-1,2-Dichloroethene ND ug/L 5.0 5 06/26/23 00:34 156-60-5
1,2-Dichloropropane ND ug/L 5.0 5 06/26/23 00:34 78-87-5
1,3-Dichloropropane ND ug/L 5.0 5 06/26/23 00:34 142-28-9
2,2-Dichloropropane ND ug/L 5.0 5 06/26/23 00:34 594-20-7
1,1-Dichloropropene ND ug/L 5.0 5 06/26/23 00:34 563-58-6
cis-1,3-Dichloropropene ND ug/L 5.0 5 06/26/23 00:34 10061-01-5
trans-1,3-Dichloropropene ND ug/L 5.0 5 06/26/23 00:34 10061-02-6
Diisopropyl ether ND ug/L 5.0 5 06/26/23 00:34 108-20-3
Ethylbenzene ND ug/L 5.0 5 06/26/23 00:34 100-41-4
Hexachloro-1,3-butadiene ND ug/L 10.0 5 06/26/23 00:34 87-68-3
2-Hexanone ND ug/L 25.0 5 06/26/23 00:34 591-78-6
p-Isopropyltoluene ND ug/L 5.0 5 06/26/23 00:34 99-87-6
Methylene Chloride ND ug/L 25.0 5 06/26/23 00:34 75-09-2
4-Methyl-2-pentanone(MIBK) ND ug/L 25.0 5 06/26/23 00:34 108-10-1
Methyl-tert-butyl ether ND ug/L 5.0 5 06/26/23 00:34 1634-04-4
Naphthalene ND ug/L 5.0 5 06/26/23 00:34 91-20-3
Styrene ND ug/L 5.0 5 06/26/23 00:34 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 5.0 5 06/26/23 00:34 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 06/26/23 00:34 79-34-5
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: LUCENT NOKIA
Pace Project No.: 92674332
Sample: AS INFLUENT Lab ID: 92674332001 Collected: 06/22/23 15:45 Received: 06/23/23 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services-Charlotte
Tetrachloroethene 891 ug/L 5.0 5 06/26/23 00:34 127-18-4
Toluene ND ug/L 5.0 5 06/26/23 00:34 108-88-3
1,2,3-Trichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 87-61-6
1,2,4-Trichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 120-82-1
1,1,1-Trichloroethane ND ug/L 5.0 5 06/26/23 00:34 71-55-6
1,1,2-Trichloroethane ND ug/L 5.0 5 06/26/23 00:34 79-00-5
Trichloroethene 132 ug/L 5.0 5 06/26/23 00:34 79-01-6
Trichlorofluoromethane ND ug/L 5.0 5 06/26/23 00:34 75-69-4
1,2,3-Trichloropropane ND ug/L 5.0 5 06/26/23 00:34 96-18-4
Vinyl acetate ND ug/L 10.0 5 06/26/23 00:34 108-05-4
Vinyl chloride ND ug/L 5.0 5 06/26/23 00:34 75-01-4
Xylene(Total) ND ug/L 5.0 5 06/26/23 00:34 1330-20-7
m&p-Xylene ND ug/L 10.0 5 06/26/23 00:34 179601-23-1
o-Xylene ND ug/L 5.0 5 06/26/23 00:34 95-47-6
Surrogates
4-Bromofluorobenzene(S) 95 % 70-130 5 06/26/23 00:34 460-00-4
1,2-Dichloroethane-d4(S) 97 % 70-130 5 06/26/23 00:34 17060-07-0
Toluene-d8(S) 98 % 70-130 5 06/26/23 00:34 2037-26-5
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: LUCENT NOKIA
Pace Project No.: 92674332
Sample: AS EFFLUENT Lab ID: 92674332002 Collected: 06/22/23 15:40 Received: 06/23/23 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Barium 34.7 ug/L 5.0 1 06/27/2311:47 06/28/2319:30 7440-39-3
Manganese 47.5 ug/L 5.0 1 06/27/2311:47 06/28/2319:30 7439-96-5
Zinc 64.4 ug/L 10.0 1 06/27/2311:47 06/28/2319:30 7440-66-6
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services-Charlotte
Acetone ND ug/L 25.0 1 06/25/23 23:21 67-64-1
Benzene ND ug/L 1.0 1 06/25/23 23:21 71-43-2
Bromobenzene ND ug/L 1.0 1 06/25/23 23:21 108-86-1
Bromochloromethane ND ug/L 1.0 1 06/25/23 23:21 74-97-5
Bromodichloromethane ND ug/L 1.0 1 06/25/23 23:21 75-27-4
Bromoform ND ug/L 1.0 1 06/25/23 23:21 75-25-2
Bromomethane ND ug/L 2.0 1 06/25/23 23:21 74-83-9
2-Butanone(MEK) ND ug/L 5.0 1 06/25/23 23:21 78-93-3
Carbon tetrachloride ND ug/L 1.0 1 06/25/23 23:21 56-23-5
Chlorobenzene ND ug/L 1.0 1 06/25/23 23:21 108-90-7
Chloroethane ND ug/L 1.0 1 06/25/23 23:21 75-00-3
Chloroform ND ug/L 1.0 1 06/25/23 23:21 67-66-3
Chloromethane ND ug/L 1.0 1 06/25/23 23:21 74-87-3
2-Chlorotoluene ND ug/L 1.0 1 06/25/23 23:21 95-49-8
4-Chlorotoluene ND ug/L 1.0 1 06/25/23 23:21 106-43-4
1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 06/25/23 23:21 96-12-8
Dibromochloromethane ND ug/L 1.0 1 06/25/23 23:21 124-48-1
1,2-Dibromoethane(EDB) ND ug/L 1.0 1 06/25/23 23:21 106-93-4
Dibromomethane ND ug/L 1.0 1 06/25/23 23:21 74-95-3
1,2-Dichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 95-50-1
1,3-Dichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 541-73-1
1,4-Dichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 106-46-7
Dichlorodifluoromethane ND ug/L 1.0 1 06/25/23 23:21 75-71-8
1,1-Dichloroethane ND ug/L 1.0 1 06/25/23 23:21 75-34-3
1,2-Dichloroethane ND ug/L 1.0 1 06/25/23 23:21 107-06-2
1,1-Dichloroethene ND ug/L 1.0 1 06/25/23 23:21 75-35-4
cis-1,2-Dichloroethene ND ug/L 1.0 1 06/25/23 23:21 156-59-2
trans-1,2-Dichloroethene ND ug/L 1.0 1 06/25/23 23:21 156-60-5
1,2-Dichloropropane ND ug/L 1.0 1 06/25/23 23:21 78-87-5
1,3-Dichloropropane ND ug/L 1.0 1 06/25/23 23:21 142-28-9
2,2-Dichloropropane ND ug/L 1.0 1 06/25/23 23:21 594-20-7
1,1-Dichloropropene ND ug/L 1.0 1 06/25/23 23:21 563-58-6
cis-1,3-Dichloropropene ND ug/L 1.0 1 06/25/23 23:21 10061-01-5
trans-1,3-Dichloropropene ND ug/L 1.0 1 06/25/23 23:21 10061-02-6
Diisopropyl ether ND ug/L 1.0 1 06/25/23 23:21 108-20-3
Ethylbenzene ND ug/L 1.0 1 06/25/23 23:21 100-41-4
Hexachloro-1,3-butadiene ND ug/L 2.0 1 06/25/23 23:21 87-68-3
2-Hexanone ND ug/L 5.0 1 06/25/23 23:21 591-78-6
p-Isopropyltoluene ND ug/L 1.0 1 06/25/23 23:21 99-87-6
Methylene Chloride ND ug/L 5.0 1 06/25/23 23:21 75-09-2
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: LUCENT NOKIA
Pace Project No.: 92674332
Sample: AS EFFLUENT Lab ID: 92674332002 Collected: 06/22/23 15:40 Received: 06/23/23 12:40 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
8260D MSV Low Level Analytical Method: EPA 8260D
Pace Analytical Services-Charlotte
4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 1 06/25/23 23:21 108-10-1
Methyl-tert-butyl ether ND ug/L 1.0 1 06/25/23 23:21 1634-04-4
Naphthalene ND ug/L 1.0 1 06/25/23 23:21 91-20-3
Styrene ND ug/L 1.0 1 06/25/23 23:21 100-42-5
1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/25/23 23:21 630-20-6
1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/25/23 23:21 79-34-5
Tetrachloroethene 2.2 ug/L 1.0 1 06/25/23 23:21 127-18-4
Toluene ND ug/L 1.0 1 06/25/23 23:21 108-88-3
1,2,3-Trichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 87-61-6
1,2,4-Trichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 120-82-1
1,1,1-Trichloroethane ND ug/L 1.0 1 06/25/23 23:21 71-55-6
1,1,2-Trichloroethane ND ug/L 1.0 1 06/25/23 23:21 79-00-5
Trichloroethene ND ug/L 1.0 1 06/25/23 23:21 79-01-6
Trichlorofluoromethane ND ug/L 1.0 1 06/25/23 23:21 75-69-4
1,2,3-Trichloropropane ND ug/L 1.0 1 06/25/23 23:21 96-18-4
Vinyl acetate ND ug/L 2.0 1 06/25/23 23:21 108-05-4
Vinyl chloride ND ug/L 1.0 1 06/25/23 23:21 75-01-4
Xylene(Total) ND ug/L 1.0 1 06/25/23 23:21 1330-20-7
m&p-Xylene ND ug/L 2.0 1 06/25/23 23:21 179601-23-1
o-Xylene ND ug/L 1.0 1 06/25/23 23:21 95-47-6
Surrogates
4-Bromofluorobenzene(S) 97 % 70-130 1 06/25/23 23:21 460-00-4
1,2-Dichloroethane-d4(S) 98 % 70-130 1 06/25/23 23:21 17060-07-0
Toluene-d8(S) 100 % 70-130 1 06/25/23 23:21 2037-26-5
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: LUCENT NOKIA
Pace Project No.: 92674332
QC Batch: 783218 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92674332002
METHOD BLANK: 4062072 Matrix: Water
Associated Lab Samples: 92674332002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 5.0 06/28/2318:09
Manganese ug/L ND 5.0 06/28/2318:09
Zinc ug/L ND 10.0 06/28/2318:09
LABORATORY CONTROL SAMPLE: 4062073
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 500 504 101 85-115
Manganese ug/L 500 508 102 85-115
Zinc ug/L 500 486 97 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4062074 4062075
MS MSD
92673583001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 7.0 500 500 520 525 103 104 70-130 1
Manganese ug/L 264 500 500 780 782 103 104 70-130 0
Zinc ug/L ND 500 500 500 503 100 101 70-130 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4062076 4062077
MS MSD
92673706001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 41.1 500 500 566 560 105 104 70-130 1
Manganese ug/L 107 500 500 628 619 104 102 70-130 1
Zinc ug/L ND 500 500 514 505 102 100 70-130 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: LUCENT NOKIA
Pace Project No.: 92674332
QC Batch: 782877 Analysis Method: EPA 8260D
QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92674332001,92674332002
METHOD BLANK: 4060901 Matrix: Water
Associated Lab Samples: 92674332001,92674332002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/25/23 16:05
1,1,1-Trichloroethane ug/L ND 1.0 06/25/23 16:05
1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/25/23 16:05
1,1,2-Trichloroethane ug/L ND 1.0 06/25/23 16:05
1,1-Dichloroethane ug/L ND 1.0 06/25/23 16:05
1,1-Dichloroethene ug/L ND 1.0 06/25/23 16:05
1,1-Dichloropropene ug/L ND 1.0 06/25/23 16:05
1,2,3-Trichlorobenzene ug/L ND 1.0 06/25/23 16:05
1,2,3-Trichloropropane ug/L ND 1.0 06/25/23 16:05
1,2,4-Trichlorobenzene ug/L ND 1.0 06/25/23 16:05
1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/25/23 16:05
1,2-Dibromoethane(EDB) ug/L ND 1.0 06/25/23 16:05
1,2-Dichlorobenzene ug/L ND 1.0 06/25/23 16:05
1,2-Dichloroethane ug/L ND 1.0 06/25/23 16:05
1,2-Dichloropropane ug/L ND 1.0 06/25/23 16:05
1,3-Dichlorobenzene ug/L ND 1.0 06/25/23 16:05
1,3-Dichloropropane ug/L ND 1.0 06/25/23 16:05
1,4-Dichlorobenzene ug/L ND 1.0 06/25/23 16:05
2,2-Dichloropropane ug/L ND 1.0 06/25/23 16:05
2-Butanone(MEK) ug/L ND 5.0 06/25/23 16:05
2-Chlorotoluene ug/L ND 1.0 06/25/23 16:05
2-Hexanone ug/L ND 5.0 06/25/23 16:05
4-Chlorotoluene ug/L ND 1.0 06/25/23 16:05
4-Methyl-2-pentanone(MIBK) ug/L ND 5.0 06/25/23 16:05
Acetone ug/L ND 25.0 06/25/23 16:05
Benzene ug/L ND 1.0 06/25/23 16:05
Bromobenzene ug/L ND 1.0 06/25/23 16:05
Bromochloromethane ug/L ND 1.0 06/25/23 16:05
Bromodichloromethane ug/L ND 1.0 06/25/23 16:05
Bromoform ug/L ND 1.0 06/25/23 16:05
Bromomethane ug/L ND 2.0 06/25/23 16:05
Carbon tetrachloride ug/L ND 1.0 06/25/23 16:05
Chlorobenzene ug/L ND 1.0 06/25/23 16:05
Chloroethane ug/L ND 1.0 06/25/23 16:05
Chloroform ug/L ND 1.0 06/25/23 16:05
Chloromethane ug/L ND 1.0 06/25/23 16:05
cis-1,2-Dichloroethene ug/L ND 1.0 06/25/23 16:05
cis-1,3-Dichloropropene ug/L ND 1.0 06/25/23 16:05
Dibromochloromethane ug/L ND 1.0 06/25/23 16:05
Dibromomethane ug/L ND 1.0 06/25/23 16:05
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: LUCENT NOKIA
Pace Project No.: 92674332
METHOD BLANK: 4060901 Matrix: Water
Associated Lab Samples: 92674332001,92674332002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Dichlorodifluoromethane ug/L ND 1.0 06/25/23 16:05
Diisopropyl ether ug/L ND 1.0 06/25/23 16:05
Ethylbenzene ug/L ND 1.0 06/25/23 16:05
Hexachloro-1,3-butadiene ug/L ND 2.0 06/25/23 16:05
m&p-Xylene ug/L ND 2.0 06/25/23 16:05
Methyl-tert-butyl ether ug/L ND 1.0 06/25/23 16:05
Methylene Chloride ug/L ND 5.0 06/25/23 16:05
Naphthalene ug/L ND 1.0 06/25/23 16:05
o-Xylene ug/L ND 1.0 06/25/23 16:05
p-Isopropyltoluene ug/L ND 1.0 06/25/23 16:05
Styrene ug/L ND 1.0 06/25/23 16:05
Tetrachloroethene ug/L ND 1.0 06/25/23 16:05
Toluene ug/L ND 1.0 06/25/23 16:05
trans-1,2-Dichloroethene ug/L ND 1.0 06/25/23 16:05
trans-1,3-Dichloropropene ug/L ND 1.0 06/25/23 16:05
Trichloroethene ug/L ND 1.0 06/25/23 16:05
Trichlorofluoromethane ug/L ND 1.0 06/25/23 16:05
Vinyl acetate ug/L ND 2.0 06/25/23 16:05
Vinyl chloride ug/L ND 1.0 06/25/23 16:05
Xylene(Total) ug/L ND 1.0 06/25/23 16:05
1,2-Dichloroethane-d4(S) % 98 70-130 06/25/23 16:05
4-Bromofluorobenzene(S) % 98 70-130 06/25/23 16:05
Toluene-d8(S) % 99 70-130 06/25/23 16:05
LABORATORY CONTROL SAMPLE: 4060902
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane ug/L 20 21.2 106 70-130
1,1,1-Trichloroethane ug/L 20 21.6 108 70-130
1,1,2,2-Tetrachloroethane ug/L 20 20.7 104 70-130
1,1,2-Trichloroethane ug/L 20 20.5 103 70-130
1,1-Dichloroethane ug/L 20 20.9 105 70-130
1,1-Dichloroethene ug/L 20 21.6 108 70-130
1,1-Dichloropropene ug/L 20 22.5 113 70-130
1,2,3-Trichlorobenzene ug/L 20 20.3 102 70-130
1,2,3-Trichloropropane ug/L 20 19.4 97 70-130
1,2,4-Trichlorobenzene ug/L 20 20.0 100 70-130
1,2-Dibromo-3-chloropropane ug/L 20 18.9 94 70-131
1,2-Dibromoethane(EDB) ug/L 20 20.7 103 70-130
1,2-Dichlorobenzene ug/L 20 20.0 100 70-130
1,2-Dichloroethane ug/L 20 19.0 95 70-130
1,2-Dichloropropane ug/L 20 21.0 105 70-130
1,3-Dichlorobenzene ug/L 20 20.3 101 70-130
1,3-Dichloropropane ug/L 20 19.7 98 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: LUCENT NOKIA
Pace Project No.: 92674332
LABORATORY CONTROL SAMPLE: 4060902
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
1,4-Dichlorobenzene ug/L 20 20.2 101 70-130
2,2-Dichloropropane ug/L 20 21.9 109 68-135
2-Butanone(MEK) ug/L 40 40.6 101 70-134
2-Chlorotoluene ug/L 20 20.6 103 70-130
2-Hexanone ug/L 40 40.2 101 70-131
4-Chlorotoluene ug/L 20 20.3 101 70-130
4-Methyl-2-pentanone(MIBK) ug/L 40 37.6 94 70-130
Acetone ug/L 40 42.6 107 70-133
Benzene ug/L 20 21.5 108 70-130
Bromobenzene ug/L 20 20.4 102 70-130
Bromochloromethane ug/L 20 20.8 104 70-130
Bromodichloromethane ug/L 20 20.1 101 70-130
Bromoform ug/L 20 20.5 102 70-130
Bromomethane ug/L 20 18.6 93 45-151
Carbon tetrachloride ug/L 20 22.3 111 70-130
Chlorobenzene ug/L 20 21.3 106 70-130
Chloroethane ug/L 20 20.9 105 39-152
Chloroform ug/L 20 19.9 100 70-130
Chloromethane ug/L 20 26.0 130 58-130
cis-1,2-Dichloroethene ug/L 20 20.5 102 70-130
cis-1,3-Dichloropropene ug/L 20 20.2 101 70-130
Dibromochloromethane ug/L 20 20.5 102 70-130
Dibromomethane ug/L 20 20.3 101 70-130
Dichlorodifluoromethane ug/L 20 25.5 127 54-133
Diisopropyl ether ug/L 20 18.8 94 70-130
Ethylbenzene ug/L 20 21.1 105 70-130
Hexachloro-1,3-butadiene ug/L 20 22.8 114 70-135
m&p-Xylene ug/L 40 42.5 106 70-130
Methyl-tert-butyl ether ug/L 20 18.3 92 70-130
Methylene Chloride ug/L 20 20.2 101 66-130
Naphthalene ug/L 20 20.1 100 70-130
o-Xylene ug/L 20 21.0 105 70-130
p-Isopropyltoluene ug/L 20 21.4 107 70-130
Styrene ug/L 20 21.3 107 70-130
Tetrachloroethene ug/L 20 21.6 108 70-130
Toluene ug/L 20 20.9 105 70-130
trans-1,2-Dichloroethene ug/L 20 22.0 110 70-130
trans-1,3-Dichloropropene ug/L 20 19.8 99 70-130
Trichloroethene ug/L 20 21.4 107 70-130
Trichlorofluoromethane ug/L 20 21.2 106 62-130
Vinyl acetate ug/L 40 37.8 95 70-144
Vinyl chloride ug/L 20 19.3 96 62-130
Xylene(Total) ug/L 60 63.5 106 70-130
1,2-Dichloroethane-d4(S) % 96 70-130
4-Bromofluorobenzene(S) % 99 70-130
Toluene-d8(S) % 101 70-130
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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QUALITY CONTROL DATA
Project: LUCENT NOKIA
Pace Project No.: 92674332
MATRIX SPIKE SAMPLE: 4060904
92673055009 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND 20 22.7 114 70-141
1,1,1-Trichloroethane ug/L ND 20 23.9 120 70-150
1,1,2,2-Tetrachloroethane ug/L ND 20 21.3 106 69-142
1,1,2-Trichloroethane ug/L ND 20 21.5 108 70-138
1,1-Dichloroethane ug/L ND 20 22.8 114 70-150
1,1-Dichloroethene ug/L ND 20 25.1 126 70-156
1,1-Dichloropropene ug/L ND 20 25.2 126 70-150
1,2,3-Trichlorobenzene ug/L ND 20 19.8 99 70-148
1,2,3-Trichloropropane ug/L ND 20 20.3 101 70-140
1,2,4-Trichlorobenzene ug/L ND 20 19.9 99 70-146
1,2-Dibromo-3-chloropropane ug/L ND 20 19.3 97 68-146
1,2-Dibromoethane(EDB) ug/L ND 20 21.5 108 70-138
1,2-Dichlorobenzene ug/L ND 20 20.8 104 70-141
1,2-Dichloroethane ug/L ND 20 20.6 103 69-143
1,2-Dichloropropane ug/L ND 20 22.0 110 68-156
1,3-Dichlorobenzene ug/L ND 20 21.3 106 70-143
1,3-Dichloropropane ug/L ND 20 20.7 104 70-138
1,4-Dichlorobenzene ug/L ND 20 21.1 105 70-142
2,2-Dichloropropane ug/L ND 20 24.2 121 52-170
2-Butanone(MEK) ug/L ND 40 38.3 96 60-157
2-Chlorotoluene ug/L ND 20 21.8 109 70-147
2-Hexanone ug/L ND 40 39.1 98 68-146
4-Chlorotoluene ug/L ND 20 21.3 106 70-142
4-Methyl-2-pentanone(MIBK) ug/L ND 40 38.6 97 70-141
Acetone ug/L ND 40 38.5 95 58-157
Benzene ug/L ND 20 22.9 115 70-142
Bromobenzene ug/L ND 20 21.2 106 70-143
Bromochloromethane ug/L ND 20 22.9 114 70-146
Bromodichloromethane ug/L ND 20 21.4 107 70-139
Bromoform ug/L ND 20 21.2 106 64-140
Bromomethane ug/L ND 20 20.1 100 28-192
Carbon tetrachloride ug/L ND 20 24.7 123 70-148
Chlorobenzene ug/L ND 20 22.8 114 70-141
Chloroethane ug/L ND 20 23.8 119 58-191
Chloroform ug/L ND 20 21.5 107 70-148
Chloromethane ug/L ND 20 28.6 143 43-162
cis-1,2-Dichloroethene ug/L ND 20 22.3 111 68-151
cis-1,3-Dichloropropene ug/L ND 20 21.0 105 70-139
Dibromochloromethane ug/L ND 20 21.5 107 70-144
Dibromomethane ug/L ND 20 21.4 107 70-139
Dichlorodifluoromethane ug/L ND 20 32.3 162 39-171
Diisopropyl ether ug/L ND 20 20.1 101 67-142
Ethylbenzene ug/L ND 20 22.7 113 70-143
Hexachloro-1,3-butadiene ug/L ND 20 24.4 122 64-163
m&p-Xylene ug/L ND 40 45.7 114 70-144
Methyl-tert-butyl ether ug/L ND 20 19.5 97 65-143
Methylene Chloride ug/L ND 20 21.0 103 62-149
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 12 of 18
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: LUCENT NOKIA
Pace Project No.: 92674332
MATRIX SPIKE SAMPLE: 4060904
92673055009 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Naphthalene ug/L ND 20 18.6 93 67-147
o-Xylene ug/L ND 20 22.3 112 70-145
p-Isopropyltoluene ug/L ND 20 22.8 114 70-147
Styrene ug/L ND 20 22.2 111 70-143
Tetrachloroethene ug/L ND 20 23.9 119 70-145
Toluene ug/L ND 20 22.4 112 70-142
trans-1,2-Dichloroethene ug/L ND 20 24.0 120 70-151
trans-1,3-Dichloropropene ug/L ND 20 20.8 104 70-139
Trichloroethene ug/L ND 20 23.4 117 62-146
Trichlorofluoromethane ug/L ND 20 26.1 130 63-153
Vinyl acetate ug/L ND 40 39.1 98 61-162
Vinyl chloride ug/L ND 20 21.7 108 61-163
Xylene(Total) ug/L ND 60 68.1 113 70-143
1,2-Dichloroethane-d4(S) % 97 70-130
4-Bromofluorobenzene(S) % 97 70-130
Toluene-d8(S) % 99 70-130
SAMPLE DUPLICATE: 4060903
92673055008 Dup
Parameter Units Result Result RPD Qualifiers
1,1,1,2-Tetrachloroethane ug/L ND ND
1,1,1-Trichloroethane ug/L ND ND
1,1,2,2-Tetrachloroethane ug/L ND ND
1,1,2-Trichloroethane ug/L ND ND
1,1-Dichloroethane ug/L ND ND
1,1-Dichloroethene ug/L ND ND
1,1-Dichloropropene ug/L ND ND
1,2,3-Trichlorobenzene ug/L ND ND
1,2,3-Trichloropropane ug/L ND ND
1,2,4-Trichlorobenzene ug/L ND ND
1,2-Dibromo-3-chloropropane ug/L ND ND
1,2-Dibromoethane(EDB) ug/L ND ND
1,2-Dichlorobenzene ug/L ND ND
1,2-Dichloroethane ug/L ND ND
1,2-Dichloropropane ug/L ND ND
1,3-Dichlorobenzene ug/L ND ND
1,3-Dichloropropane ug/L ND ND
1,4-Dichlorobenzene ug/L ND ND
2,2-Dichloropropane ug/L ND ND
2-Butanone(MEK) ug/L ND ND
2-Chlorotoluene ug/L ND ND
2-Hexanone ug/L ND ND
4-Chlorotoluene ug/L ND ND
4-Methyl-2-pentanone(MIBK) ug/L ND ND
Acetone ug/L ND ND
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 13 of 18
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA
Project: LUCENT NOKIA
Pace Project No.: 92674332
SAMPLE DUPLICATE: 4060903
92673055008 Dup
Parameter Units Result Result RPD Qualifiers
Benzene ug/L ND ND
Bromobenzene ug/L ND ND
Bromochloromethane ug/L ND ND
Bromodichloromethane ug/L ND ND
Bromoform ug/L ND ND
Bromomethane ug/L ND ND
Carbon tetrachloride ug/L ND ND
Chlorobenzene ug/L ND ND
Chloroethane ug/L ND ND
Chloroform ug/L ND ND
Chloromethane ug/L ND ND
cis-1,2-Dichloroethene ug/L ND ND
cis-1,3-Dichloropropene ug/L ND ND
Dibromochloromethane ug/L ND ND
Dibromomethane ug/L ND ND
Dichlorodifluoromethane ug/L ND ND
Diisopropyl ether ug/L ND ND
Ethylbenzene ug/L ND ND
Hexachloro-1,3-butadiene ug/L ND ND
m&p-Xylene ug/L ND ND
Methyl-tert-butyl ether ug/L ND ND
Methylene Chloride ug/L ND ND
Naphthalene ug/L ND ND
o-Xylene ug/L ND ND
p-Isopropyltoluene ug/L ND ND
Styrene ug/L ND ND
Tetrachloroethene ug/L ND ND
Toluene ug/L ND ND
trans-1,2-Dichloroethene ug/L ND ND
trans-1,3-Dichloropropene ug/L ND ND
Trichloroethene ug/L ND ND
Trichlorofluoromethane ug/L ND ND
Vinyl acetate ug/L ND ND
Vinyl chloride ug/L ND ND
Xylene(Total) ug/L ND ND
1,2-Dichloroethane-d4(S) % 98 97
4-Bromofluorobenzene(S) % 97 97
Toluene-d8(S) % 100 100
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 14 of 18
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALIFIERS
Project: LUCENT NOKIA
Pace Project No.: 92674332
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 15 of 18
Pace Analytical Services,LLC
(�IaceAnalyficalo 9800 Kiney Ave. Suite 100
Huntersville,NC 28078
078
www.pacelabs.com (704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: LUCENT NOKIA
Pace Project No.: 92674332
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92674332002 AS EFFLUENT EPA 200.7 Rev 4.4 1994 783218 EPA 200.7 Rev 4.4 1994 783273
92674332001 AS INFLUENT EPA 8260D 782877
92674332002 AS EFFLUENT EPA8260D 782877
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 16 of 18
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Page 18 of 18
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
August 09, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on July 28, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,Q - aAAa,
Bonnie Vang
bonnie.vang@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
Cristin Dolan,AECOM
Teresa Amentt Jennings,AECOM
Jon Wakeman,AECOM Environment
z REPORT OF LABORATORY ANALYSIS
N This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 23
6
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
CERTIFICATIONS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 2 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92679831001 DT-1 EPA 6020E KRL 3 PASI-A
92679831002 EW-4 EPA 6020E KRL 3 PASI-A
92679831003 EW-5 EPA 6020E KRL 3 PASI-A
92679831004 EW-6 EPA 6020E KRL 3 PASI-A
92679831005 EW-12 EPA 6020E KRL 3 PASI-A
92679831006 EW-14 EPA 6020E KRL 3 PASI-A
92679831007 EW-16 EPA 6020E KRL 3 PASI-A
92679831008 EW-17 EPA 6020E KRL 3 PASI-A
92679831009 EW-19 EPA 6020E KRL 3 PASI-A
92679831010 EW-21 EPA 6020E KRL 3 PASI-A
92679831011 EW-22 EPA 6020E KRL 3 PASI-A
92679831012 AS EFFLUENT EPA6020B KRL 3 PASI-A
PASI-A=Pace Analytical Services-Asheville
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC. Page 3 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: DT-1 Lab ID: 92679831001 Collected: 07/26/23 14:00 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 47.3 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:12 7440-39-3
Manganese 30.1 ug/L 2.0 1 08/03/23 16:17 08/08/23 03:12 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:12 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-4 Lab ID: 92679831002 Collected: 07/26/23 13:20 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 10.5 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:27 7440-39-3
Manganese 2.5 ug/L 2.0 1 08/03/23 16:17 08/08/23 03:27 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:27 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-5 Lab ID: 92679831003 Collected: 07/26/23 13:25 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 18.7 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:32 7440-39-3
Manganese ND ug/L 2.0 1 08/03/23 16:17 08/08/23 03:32 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:32 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-6 Lab ID: 92679831004 Collected: 07/26/23 13:30 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 29.3 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:37 7440-39-3
Manganese 1060 ug/L 20.0 10 08/03/23 16:17 08/09/23 02:38 7439-96-5
Zinc 37.6 ug/L 10.0 1 08/03/23 16:17 08/08/23 03:37 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-12 Lab ID: 92679831005 Collected: 07/26/23 13:10 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 35.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:42 7440-39-3
Manganese ND ug/L 2.0 1 08/03/23 16:17 08/08/23 03:42 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:42 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-14 Lab ID: 92679831006 Collected: 07/26/23 13:15 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 94.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:47 7440-39-3
Manganese 22.4 ug/L 2.0 1 08/03/23 16:17 08/08/23 03:47 7439-96-5
Zinc 214 ug/L 20.0 2 08/03/23 16:17 08/09/23 02:43 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-16 Lab ID: 92679831007 Collected: 07/26/23 13:35 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 17.3 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:52 7440-39-3
Manganese 345 ug/L 6.0 3 08/03/23 16:17 08/09/23 02:48 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:52 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 23
Pace Analytical Services,LLC
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ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-17 Lab ID: 92679831008 Collected: 07/26/23 13:40 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 14.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 04:47 7440-39-3
Manganese 20.6 ug/L 2.0 1 08/03/23 16:17 08/08/23 04:47 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 04:47 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 23
Pace Analytical Services,LLC
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ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-19 Lab ID: 92679831009 Collected: 07/26/23 13:45 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 45.6 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:12 7440-39-3
Manganese 10.2 ug/L 2.0 1 08/03/23 16:17 08/08/23 05:12 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 05:12 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 23
Pace Analytical Services,LLC
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ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-21 Lab ID: 92679831010 Collected: 07/26/23 13:55 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 138 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:17 7440-39-3
Manganese 10.7 ug/L 2.0 1 08/03/23 16:17 08/08/23 05:17 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 05:17 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: EW-22 Lab ID: 92679831011 Collected: 07/26/23 13:50 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 13.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:22 7440-39-3
Manganese ND ug/L 2.0 1 08/03/23 16:17 08/08/23 05:22 7439-96-5
Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 05:22 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Sample: AS EFFLUENT Lab ID: 92679831012 Collected: 07/26/23 16:30 Received: 07/28/23 16:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A
Pace Analytical Services-Asheville
Barium 27.6 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:37 7440-39-3
Manganese 425 ug/L 6.0 3 08/03/23 16:17 08/09/23 03:28 7439-96-5
Zinc 20.5 ug/L 10.0 1 08/03/23 16:17 08/08/23 05:37 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
QC Batch: 791234 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92679831001,92679831002,92679831003,92679831004,92679831005,92679831006,92679831007
METHOD BLANK: 4100550 Matrix: Water
Associated Lab Samples: 92679831001,92679831002,92679831003,92679831004,92679831005,92679831006,92679831007
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 1.0 08/08/23 01:42
Manganese ug/L ND 2.0 08/08/23 01:42
Zinc ug/L ND 10.0 08/08/23 01:42
LABORATORY CONTROL SAMPLE: 4100551
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 50 50.7 101 80-120
Manganese ug/L 50 51.2 102 80-120
Zinc ug/L 50 52.0 104 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4100552 4100553
MS MSD
92679152001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 566 50 50 606 610 79 88 75-125 1
Manganese ug/L 9830 50 50 9800 9530 -56 -593 75-125 3 M1
Zinc ug/L 33.7 50 50 83.5 82.6 100 98 75-125 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
QC Batch: 791237 Analysis Method: EPA 6020B
QC Batch Method: EPA 3010A Analysis Description: 6020 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92679831008,92679831009,92679831010,92679831011,92679831012
METHOD BLANK: 4100561 Matrix: Water
Associated Lab Samples: 92679831008,92679831009,92679831010,92679831011,92679831012
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 1.0 08/08/23 04:37
Manganese ug/L ND 2.0 08/08/23 04:37
Zinc ug/L ND 10.0 08/08/23 04:37
LABORATORY CONTROL SAMPLE: 4100562
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 50 47.4 95 80-120
Manganese ug/L 50 51.4 103 80-120
Zinc ug/L 50 52.1 104 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4100563 4100564
MS MSD
92679831008 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 14.1 50 50 61.0 60.9 94 94 75-125 0
Manganese ug/L 20.6 50 50 71.9 70.7 103 100 75-125 2
Zinc ug/L ND 50 50 53.6 53.9 101 102 75-125 1
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
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QUALIFIERS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA WINSTON SALEM
Pace Project No.: 92679831
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92679831001 DT-1 EPA 3010A 791234 EPA 6020B 791317
92679831002 EW-4 EPA 3010A 791234 EPA 6020B 791317
92679831003 EW-5 EPA 3010A 791234 EPA 6020B 791317
92679831004 EW-6 EPA 3010A 791234 EPA 6020B 791317
92679831005 EW-12 EPA 3010A 791234 EPA 6020B 791317
92679831006 EW-14 EPA 3010A 791234 EPA 6020B 791317
92679831007 EW-16 EPA 3010A 791234 EPA 6020B 791317
92679831008 EW-17 EPA 3010A 791237 EPA 6020B 791320
92679831009 EW-19 EPA 3010A 791237 EPA 6020B 791320
92679831010 EW-21 EPA 3010A 791237 EPA 6020B 791320
92679831011 EW-22 EPA 3010A 791237 EPA 6020B 791320
92679831012 AS EFFLUENT EPA 3010A 791237 EPA 6020B 791320
REPORT OF LABORATORY ANALYSIS
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Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 23
DC#_Title: ENV-FRM-HUN1.0083 02-
sample Condition Upon Receipt
ace.
ae1�i4�HAYGti
Effective Date: 11/14/2022 8:18:30 AM
Laboratory receiving samples:
Asheville m Eden❑ Greenwood❑ Huntersville❑ Raleigh[] Mechanicsville❑ Atlanta[] Kernersville❑
Sample Condition Client Name:Upon Receipt Project K WO# : 92679831
Iq t6 �Dllei 2A
Courier: LJ Fed Ex L.JLJPs TQuS PYCflent II I II' I II II III II II I III
❑ Commercial 20 Pace ❑Other:
92679831
Custody Seal Present? ❑Yes XNo Seals Intact? ❑Yes Ili No
Date/Initials Person Examining Contents��
Packing Material; ❑Bubble Wrap ❑Bubble Bags X None ❑ Other Biological Tissue Frozen?
Thermometer: ❑Yes ❑No I N/A
14IR Gun ID: 73Tq Type of Ice: RjWet 061up ❑None
—��'
6 Correction Factor:
Cooler Temp: Add/Subtract(°CJ Q Temp should be ahove freezing to 6'C
❑5amples out of temp criteria.Samples on Ite,cooling process
Cooler Temp Corrected (°C): has begun
USDA Regulated Soll(4 N/A,water sample)
Did samples originate In a quarantine z❑ne within the United Slates:CA,NY,or SC Did samplesoriginate from a foreign source(internationally,
(check maps)?El Yes X No including Hawaii and Puerto Rlco)?❑Yes 1�1No
Comments/Discrepancy:
Chain of Custody Present? jTQYes El No ]N/A t.
Samples Arrived withinHold7lme? DYes ❑No El N/A 2.
Short Hold Time Analysis(c72'li ❑Yes $)No El N/A 3_
Rush Turn Around Time Requested? DYes 1ZNo DN/A 4.
Sufficient Volume? Z Yes ❑No ❑N/A 5.
Correct Containers Used? PgYes ❑No ❑N/A 6,
-Pace Containers Used? IRYcs ❑No ❑NIA
Containers Intact? Yes ❑No ❑N/A 7,
Dissolved analysis:Samples Field Filtered? ❑Yes. ❑No I3(1N/A a.
Sample Labels Match COC7 ry—IQYes [I No El N/A 9.
-includes Uate/Time/ID/Anal sis Matrix:___JI
Headspace In VOA Vials(>5-6mm)? ❑Yes ❑No N/A 10,
Trip Blank Present? ❑Yes ❑No N/A 11,
Trip Blank Custody Seals Present? DYes ❑No WA
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
ni,itraY trl•RQR1A porn 1 of 7
Page 20 of 23
DC#_Title: ENV-FRM-HUN1.0083 02 Sample Condition Upon Receipt
cetrlgtf,ry�t
Effective Date:11/14/20,22 8t18t30 AM WQ# : 92679831
PM: BV Due Date: 08/09/23
*Check mark top half of box if pH and/or dechlorination is verified and Project tJ CLIENT: 92—AECOM—RAL
within the acceptance range for preservation samples.
Exceptions:VOIA,Cbliform,TOC,011 and Grease,DRO/8015(water)DOC,.LLHg
**Bottom half of box Is to list number of bottles
***Check all unpreserved Nitrates for chlorine
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Page 23 of 23
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
September 19, 2023
Conan Fitzgerald
AECOM
5438 Wade Park Boulevard
Suite 200
Raleigh, NC 27607
RE: Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Dear Conan Fitzgerald:
Enclosed are the analytical results for sample(s)received by the laboratory on August 30, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Minneapolis
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
,&—r-;,-
Adam Phillips
adam.phillips@pacelabs.com
(704)875-9092
Project Manager
Enclosures
cc: Shelley Acheson,AECOM
Cristin Dolan,AECOM
Teresa Amentt Jennings,AECOM
Jon Wakeman,AECOM Environment
z REPORT OF LABORATORY ANALYSIS
N This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 1 of 24
6
Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
CERTIFICATIONS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Pace Analytical Services,LLC-Minneapolis MN
1700 Elm Street SE, Minneapolis, MN 55414 Mississippi Certification#: MN00064
A21-A Certification#:2926.01 Missouri Certification#: 10100
Alabama Certification#:40770 Montana Certification#:CERT0092
Alaska Contaminated Sites Certification#: 17-009 Nebraska Certification#: NE-OS-18-06
Alaska DW Certification#: MN00064 Nevada Certification#: MN00064
Arizona Certification#:AZ0014 New Hampshire Certification#:2081
Arkansas DW Certification#: MN00064 New Jersey Certification#: MN002
Arkansas WW Certification#:88-0680 New York Certification#: 11647
California Certification#:2929 North Carolina DW Certification#:27700
Colorado Certification#:MN00064 North Carolina WW Certification#:530
Connecticut Certification#: PH-0256 North Dakota Certification(A2LA)#:R-036
EPA Region 8 Tribal Water Systems+Wyoming DW North Dakota Certification(MN)#: R-036
Certification#:via MN 027-053-137 Ohio DW Certification#:41244
Florida Certification#: E87605 Ohio VAP Certification(1700)#:CL101
Georgia Certification#:959 Oklahoma Certification#:9507
GMP+Certification#:GMP050884 Oregon Primary Certification#:MN300001
Hawaii Certification#: MN00064 Oregon Secondary Certification#: MN200001
Idaho Certification#:MN00064 Pennsylvania Certification#:68-00563
Illinois Certification#:200011 Puerto Rico Certification#: MN00064
Indiana Certification#:C-MN-01 South Carolina Certification#:74003001
Iowa Certification#:368 Tennessee Certification#:TN02818
Kansas Certification#:E-10167 Texas Certification#:T104704192
Kentucky DW Certification#:90062 Utah Certification#:MN00064
Kentucky WW Certification#:90062 Vermont Certification#:VT-027053137
Louisiana DEQ Certification#:AI-03086 Virginia Certification#:460163
Louisiana DW Certification#:MN00064 Washington Certification#:C486
Maine Certification#: MN00064 West Virginia DEP Certification#:382
Maryland Certification#:322 West Virginia DW Certification M 9952 C
Michigan Certification#:9909 Wisconsin Certification#:999407970
Minnesota Certification#:027-053-137 Wyoming UST Certification#:via A21-A 2926.01
Minnesota Dept of Ag Approval:via MN 027-053-137 USDA Permit#: P330-19-00208
Minnesota Petrofund Registration#: 1240
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
SAMPLE ANALYTE COUNT
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92685386001 DT-1 EPA 6020E NN2 3 PASI-M
92685386002 EW-4 EPA 6020E NN2 3 PASI-M
92685386003 EW-5 EPA 6020E NN2 3 PASI-M
92685386004 EW-6 EPA 6020E NN2 3 PASI-M
92685386005 EW-12 EPA 6020E NN2 3 PASI-M
92685386006 EW-14 EPA 6020E NN2 3 PASI-M
92685386007 EW-16 EPA 6020E NN2 3 PASI-M
92685386008 EW-17 EPA 6020E NN2 3 PASI-M
92685386009 EW-18 EPA 6020E NN2 3 PASI-M
92685386010 EW-19 EPA 6020E NN2 3 PASI-M
92685386011 EW-21 EPA 6020E NN2 3 PASI-M
92685386012 EW-22 EPA 6020E NN2 3 PASI-M
92685386013 AS EFF EPA 6020E NN2 3 PASI-M
PASI-M=Pace Analytical Services-Minneapolis
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: DT-1 Lab ID: 92685386001 Collected: 08/29/23 10:40 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 49.4 ug/L 0.30 1 09/18/23 05:30 09/18/23 17:51 7440-39-3
Manganese 27.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 17:51 7439-96-5
Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 17:51 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-4 Lab ID: 92685386002 Collected: 08/29/23 11:15 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 8.8 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:25 7440-39-3
Manganese ND ug/L 0.50 1 09/18/23 05:30 09/18/23 18:25 7439-96-5
Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 18:25 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-5 Lab ID: 92685386003 Collected: 08/29/23 11:20 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 19.6 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:32 7440-39-3
Manganese 1.7 ug/L 0.50 1 09/18/23 05:30 09/18/23 18:32 7439-96-5
Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 18:32 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-6 Lab ID: 92685386004 Collected: 08/29/23 11:25 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 48.7 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:39 7440-39-3
Manganese 3210 ug/L 10.0 20 09/18/23 05:30 09/18/23 18:42 7439-96-5
Zinc 197 ug/L 5.0 1 09/18/23 05:30 09/18/23 18:39 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-12 Lab ID: 92685386005 Collected: 08/29/23 11:40 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 125 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:45 7440-39-3
Manganese 736 ug/L 10.0 20 09/18/23 05:30 09/18/23 18:49 7439-96-5
Zinc 32.7 ug/L 5.0 1 09/18/23 05:30 09/18/23 18:45 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-14 Lab ID: 92685386006 Collected: 08/29/23 11:30 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 112 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:52 7440-39-3
Manganese 22.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 18:52 7439-96-5
Zinc 24.8 ug/L 5.0 1 09/18/23 05:30 09/18/23 18:52 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-16 Lab ID: 92685386007 Collected: 08/29/23 11:10 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 24.0 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:06 7440-39-3
Manganese 11.8 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:06 7439-96-5
Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:06 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-17 Lab ID: 92685386008 Collected: 08/29/23 11:05 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 16.6 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:13 7440-39-3
Manganese 57.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:13 7439-96-5
Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:13 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-18 Lab ID: 92685386009 Collected: 08/29/23 10:45 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 74.1 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:20 7440-39-3
Manganese 113 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:20 7439-96-5
Zinc 6.3 ug/L 5.0 1 09/18/23 05:30 09/18/23 19:20 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-19 Lab ID: 92685386010 Collected: 08/29/23 10:55 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 46.9 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:27 7440-39-3
Manganese 6.7 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:27 7439-96-5
Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:27 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-21 Lab ID: 92685386011 Collected: 08/29/23 11:00 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 151 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:34 7440-39-3
Manganese 39.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:34 7439-96-5
Zinc 5.4 ug/L 5.0 1 09/18/23 05:30 09/18/23 19:34 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: EW-22 Lab ID: 92685386012 Collected: 08/29/23 10:50 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 13.8 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:47 7440-39-3
Manganese 0.89 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:47 7439-96-5
Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:47 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
ANALYTICAL RESULTS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Sample: AS EFF Lab ID: 92685386013 Collected: 08/29/23 11:45 Received: 08/30/23 09:31 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A
Pace Analytical Services-Minneapolis
Barium 34.5 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:54 7440-39-3
Manganese 841 ug/L 10.0 20 09/18/23 05:30 09/18/23 19:58 7439-96-5
Zinc 68.7 ug/L 5.0 1 09/18/23 05:30 09/18/23 19:54 7440-66-6
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
QC Batch: 906302 Analysis Method: EPA 6020B
QC Batch Method: EPA 3020A Analysis Description: 6020E Water UPD5
Laboratory: Pace Analytical Services-Minneapolis
Associated Lab Samples: 92685386001,92685386002,92685386003,92685386004,92685386005,92685386006,92685386007,
92685386008,92685386009,92685386010,92685386011,92685386012,92685386013
METHOD BLANK: 4772899 Matrix: Water
Associated Lab Samples: 92685386001,92685386002,92685386003,92685386004,92685386005,92685386006,92685386007,
92685386008,92685386009,92685386010,92685386011,92685386012,92685386013
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Barium ug/L ND 0.30 09/18/2317:44
Manganese ug/L ND 0.50 09/18/2317:44
Zinc ug/L ND 5.0 09/18/2317:44
LABORATORY CONTROL SAMPLE: 4772900
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Barium ug/L 100 106 106 80-120
Manganese ug/L 100 105 105 80-120
Zinc ug/L 100 108 108 80-120
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4772901 4772902
MS MSD
92685386001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Barium ug/L 49.4 100 100 152 158 103 108 75-125 3
Manganese ug/L 27.0 100 100 128 130 101 102 75-125 1
Zinc ug/L ND 100 100 106 108 104 106 75-125 2
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALIFIERS
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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Pace Analytical Services,LLC
Face 9800 Kincey Ave. Suite 100
(-� Huntersville,NC 28078
(704)875-9092
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: NOKIA WINSTON SALEM
Pace Project No.: 92685386
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92685386001 DT-1 EPA 3020A 906302 EPA 6020B 906507
92685386002 EW-4 EPA 3020A 906302 EPA 6020B 906507
92685386003 EW-5 EPA 3020A 906302 EPA 6020B 906507
92685386004 EW-6 EPA 3020A 906302 EPA 6020B 906507
92685386005 EW-12 EPA 3020A 906302 EPA 6020B 906507
92685386006 EW-14 EPA 3020A 906302 EPA 6020B 906507
92685386007 EW-16 EPA 3020A 906302 EPA 6020B 906507
92685386008 EW-17 EPA 3020A 906302 EPA 6020B 906507
92685386009 EW-18 EPA 3020A 906302 EPA 6020B 906507
92685386010 EW-19 EPA 3020A 906302 EPA 6020B 906507
92685386011 EW-21 EPA 3020A 906302 EPA 6020B 906507
92685386012 EW-22 EPA 3020A 906302 EPA 6020B 906507
92685386013 AS EFF EPA 3020A 906302 EPA 6020B 906507
REPORT OF LABORATORY ANALYSIS
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DC#_Title: ENV-FRM-HUN1.0083 02 Sample Condition Upon Receipt
ace,
aMr:nuura�xrs
Effective Date: 11/W2022 8:18:30 AM
Laboratory receiving samples:
Asheville Eden❑ Greenwood❑ Htlntersvllle❑ Ralelgh❑ Mechanicsville❑ Atlanta[] Kernersville❑
Sample Condition I Client Name: f Project#: WO# : 92685386
Courier: UFed Ex LJ UPS USPS UClient 11111111
IIII�IIIIII III
❑ Commercial mace ❑Other: 92685386
Custody Seal Present? El Yes WNo Seals intact? ❑Yes Ida
Data/InitialsPerson Examin)ng. r,6ntent
Packing Material: ElBubble Wrap ❑ cc Bubble Bags �1 None ❑ Other Biological Tissu Frozen?
Thermometer: ❑Yes ❑No [RN/A
❑ IR*6urr1D:
Type of Ice: Wet Blue Nane
Correction Factor:
Cooler Temp: �— Add/Subtract (-C) Temp should be above freezing to 6'C
❑Samplesoutof temp criteria.Samples on Ice,couling process
Cooler Temp Corrected f°C : h,c begun
USDA Regulated Soil(2316NIA,water sample)
Did samples originate in a quarantine zone Within the United States:CA, NY,or SC Did samples originate from a foreign source(Internationally,
(check maps)?❑Yes ONO intluding Hawaii and Puerto Rico)?Oyes ❑No
Comments/Discrepancy-
Chain of Custody Present? 4Kes ❑No DN/A 1.
Samples Arrtved within Hold Time? R�ns ❑No ❑N/A Z.
Short Hold Time Analysis(c72 hr.)? ❑Yes &No ❑N/A 3.
Rush Turn Around Time Requested? Dyes IJKo ❑N/A A.
Sufficient Volume? ayes ❑No ❑N/A S.
Correct Containers Used? —kYes ❑No ❑N/A 6.
-Pace Containers Used? Ycs ❑No ❑N/A
Cantainers Intact? R" Yes ❑No ❑WA 7.
Dissolved analysis:Samples field Filtered? El Yes ❑No &wA 8.
Sample Labels Match COC? 'jNkes ❑No DVA 9.
-Includes DateMme/ID/Anal si.s Marrlx:
Heads ace in VOA Vials(>S-6mm)? ❑Yes ❑No N/A 10.
Trlp Blank Present? ❑Yes ❑No /A 11.
Trip Blank Custody Seals Present? ❑Yes ❑No ®_N/A
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑ND
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Page 20 of 24
DC# Title: ENV-FRM-HUN1-0083 02-Sample Conditlon Upon Receipt
r.�t.vtusu44Ys
Effective Date: 11/14/2022 8:18:30 AM
*Check mark top half of box If pH and/or dechlorination Is verified and Project# WO# : 92685386
within the acceptance range for preservation samples. PM: ABP Due Date: 09/11/23
Exceptions:VOA,Conform,TOC,Oil and Grease, DRO/8015(water)DOC,Mig CLIENT: 92—AECOM—RAL
**Bottom half of box Is to list number of Bottles
***'Checkall unpreserved Nitrates for chlorine L
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pH Adjustment Log for Preserved Samples
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adjusted added
Note: Whenever there 15 a d1 screpancy affecting North Carolina compGancesampl es,a copy of this form will besent to the North Carolina DFNR Certification Office(I,e.
Out of hold,incorrect preservative,out of temp,incorrect containers,
Page 21 of 24
DC#_Title: ENV-FRM-HUN1-0083 02_Sampie Condition Upon Receipt
ace'
rF,.uws,nr:
Effective Dater 11/14/2022 8118.30 AM
*Check mark top half of box if pH and/or dechlorination Is verified and Project#
within the acceptance range for preservation samples. .
Exceptions:VOA, Coliform,TOC,Oil and Grease, DR0/8DI5{water)DOC, LLHg
;"Bottom half of box Is to list number of bottles-
***Check all unpreserved Nitrates for chlorine
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pH Adjustment Log for Preserved Samples
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Note: Whenevertherais,a discrepancy affecting North Carolina complIance samples,a copy of this formwill besent to the North Carolina DFNR Certification Office (i.e.
Out of hold,incorrect preservative,out of temp, Incorrect containers.
Page 22 of 24
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