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HomeMy WebLinkAboutNC0080853_Remission (Request)_20240411 AECOM AECOM 919.461.1100 tel 5438 Wade Park Boulevard,Suite 200 Raleigh, NC 27607 April 11, 2024 Central Files Division of Water Quality 1621 Mail Service Center Raleigh, NC 27699-1621 Subject: Remission Request Revision 1 1 Assessment of Civil Penalty NPDES Permit No. NCO080853/001 Nokia of America Corporation Case No. TX-2023-0003 3370 Lexington Road,Winston-Salem, NC To Whom It May Concern: On behalf of Nokia of America Corporation (Nokia), AECOM Technical Services of North Carolina, Inc. is submitting this remission request in response to the Assessment of Civil Penalty dated October 13, 2023, from the North Carolina Department of Environmental Quality (DEQ) regarding the Salem Park facility's toxicity self-monitoring data from the months of December 2022 and February 2023. Revision 1 is prepared to provide an estimate of costs incurred investigating and addressing toxicity issues, as requested by DEQ via email on April 1, 2024. For the reasons outlined below, Nokia respectfully requests a remission for violation costs. On March 31, 2023, on behalf of Nokia, AECOM submitted the results of the February 2023 multiple- concentration chronic toxicity testing for NPDES Permit No. NC0080853. Within the cover letter, in addition to notifying DEQ of the test failure, AECOM proposed several action items to further evaluate the recent toxicity failures at the facility. Following submission of the February 2023 toxicity report, AECOM, on behalf of Nokia, promptly implemented the following actions to better understand the source of chronic toxicity in the system effluent: 1. Evaluate Potential Source of Toxicity— a. Extraction well EW-16 is historically the source of the highest concentrations of chlorinated volatile organic compounds (CVOCs) in the groundwater treatment system influent. Additionally, annual well cleanings at EW-16 provide evidence of biological fouling of the well screen. Based on these observations, AECOM proposed to evaluate EW-16 as a potential source of chronic toxicity in the effluent. Approximately four hours prior to collecting the regular March 2023 quarterly toxicity sample, AECOM shut down extraction well EW-16. As described above, the March 2023 samples still failed the chronic toxicity test. EW-16 was subsequently returned to operation. b. The Toxicity Reduction Evaluation Guidance for Municipal Wastewater Treatment Plants, published by the United States Environmental Protection Agency (USEPA) in August 1999, describes several commonly identified potential sources of toxicity for Publicly Owned Treatment Works (POTW) effluents. Elevated metals concentrations in effluent are listed among the commonly identified potential sources of toxicity. Specifically, zinc is understood to have a negative impact upon reproduction in aquatic organisms at concentrations near 25-50 pg/L and higher. See the discussions below regarding system analytical results. AECOM 2 To evaluate the source and concentration of metals in the system effluent, AECOM collected a series of samples for laboratory analysis in April, May, June, July, and August 2023. At various times these samples were collected from individual wells, influent lines for well Networks A and B, the effluent stream from the treatment system, and permit monitoring point FE-151. The related laboratory analytical reports are presented in Attachment A. Since metals analyses is not normally required under this permit, all metals testing was performed above and beyond the requirements of the permit. Additional analytical testing for metals is discussed below. 2. Expand Analytical Dataset During Toxicity Testing—To improve understanding of constituents present in groundwater treatment system effluent, AECOM collected additional samples from system effluent for laboratory analysis by EPA Method 8260 (VOC full list)and EPA Method 200.7 (priority pollutant metals) during toxicity testing in April, May, and June 2023. A summary of results for key metals are presented in the Table 1, with the related laboratory analytical reports presented in Attachment A. Below is a brief discussion of analytical results per month: a. April 2023: VOC results from effluent samples were consistent with historical data, and metals results were consistent with the effluent sample collected on April 5, 2023. In addition, water quality parameters collected in April were within acceptable ranges. It was noted that metals testing indicated zinc levels above 50 ug/L in all AS Effluent and FE- 151 samples collected. The April test toxicity test did not pass. b. May 2023: As presented in Table 1, extraction well EW-6 was the only Network A well with detectable concentrations of zinc during the May sampling at a detection limit of 20 pg/L. Accordingly, EW-6 was shut off prior to toxicity testing in May 2023 to evaluate the effects on chronic toxicity. Effluent samples collected during toxicity sampling indicated that VOC results were consistent with historical data, and that zinc concentrations declined to non-detect values after EW-6 was shut down, and the May toxicity test passed. c. June 2023: In June, metals analyses was performed on both toxicity test water samples. Although recovery well EW-6 remained shut down, the metals analysis for the initial sample collected indicated elevated zinc. However, zinc was again less than 20 pg/L for the second toxicity test sample. This evidently resulted in minimal impact to reproductivity, and the June toxicity test achieved a passing result. Since zinc concentrations were elevated in one total effluent sample without EW-6 operating, AECOM initiated of all extraction wells to identify other extraction wells that may have been contributing zinc. Concurrently, AECOM restored operation of EW-6, but at a lower flow rate than previously (approximately 7 gpm instead of 11 gpm). 3. Isolate Zinc Sources—On August 29, 2023, AECOM collected water samples from all active extraction wells, and sent them to the Pace Analytical laboratory in Minneapolis, MN to achieve a lower detection limit for zinc than provided by the Pace Analytical laboratory in Asheville, NC (5 pg/L instead of the 10 or 20 pg/L achieved previously). Results of the individual well sampling are presented in Table 1, with the related laboratory analytical reports presented in Attachment A. Implementation of the above actions has identified zinc as the most probable cause of toxicity test failures under this permit in 2022-23. Although EW-6 has been identified as a primary source, zinc also appears in other extraction wells, but with significant variability. AECOM will continue regular zinc analyses in individual wells, working to balance the zinc intake into the system while achieving remedial objectives. Operation of individual recovery wells will continue to be evaluated as additional information is gathered and hopefully patterns determined. The flow rate in extraction wells identified to frequently contain dissolved zinc in their effluent may be reduced to mitigate metals concentrations in the combined effluent, and therefore reduce the chance of a negative chronic toxicity test result. AECOM 3 Most notably, following the passing test in May 2023, the toxicity sampling has now incurred a passing result for three consecutive quarters (June, September, and December 2023), as documented in the toxicity reports submitted to DEQ on July 21, 2023, October 30, 2023, and January 23, 2024. It is estimated the above-described actions to investigate and address toxicity issues have incurred approximately$13,500 in additional cost to Nokia. With each future quarterly toxicity test, it is estimated that Nokia will incur approximately$1,500 additional cost to continue efforts to assess and balance zinc concentrations from individual extraction wells until a reliable equilibrium is achieved. After identifying and mitigating the most probable cause of the toxicity failures, which has resulted in four consecutive passing tests, Nokia contends that the civil penalty qualifies for remission in accordance with Factor(2) presented in the Civil Penalty Assessment: "the violator promptly abated continuing environmental damage resulting from the violation."Accordingly, Nokia respectfully requests that DEQ remit the assessed civil penalty violation costs. Nokia greatly appreciates DEQ's willingness to consider Nokia's actions in the events following the violation, as well as the measures that Nokia is taking to ensure compliance with the NPDES Permit and the requirements of DEQ in the future. If you have any questions or would like to discuss this further, please contact Conan Fitzgerald at 919- 461-1260. Sincerely, Cristin Dolan Conan Fitzgerald, PE Staff Engineer Project Manager, AVP Engineering Attachments a. Justification for Remission Request b. Table 1 Summary of Metals Analytical Results c. Table 2 Summary of Costs d. Laboratory Reports cc: G. John Galasso, Nokia of America Corporation J. Wakeman, AECOM DocuSign Envelope ID:90E20F45-DC74-4117-9502-B5FFE1DC5266 JUSTIFICATION FOR REMISSION REQUEST Case Number: TX-2023-0003 County: Forsyth Assessed Party: Salem Business Park remediation site Permit No. (if applicable): NCO080853 Amount Assessed: $ 2,069.48 Please use this form when requesting remission of this civil penalty.You must also complete the 'Request For Remission, Waiver of Right to an Administrative Hearing, and Stipulation of Facts"form to request remission of this civil penalty. You should attach any documents that you believe support your request and are necessary for the Director to consider in evaluating your request for remission. Please be aware that a request for remission is limited to consideration of the five factors listed below as they may relate to the reasonableness of the amount of the civil penalty assessed. Requesting remission is not the proper procedure for contesting whether the violation(s) occurred or the accuracy of any of the factual statements contained in the civil penalty assessment document. Pursuant to N.C.G.S. § 143B-282.1(c), remission of a civil penalty may be granted only when one or more of the following five factors applies. Please check each factor that you believe applies to your case and provide a detailed explanation, including copies of supporting documents, as to why the factor applies (attach additional pages as needed). (a) one or more of the civil penalty assessment factors in N.C.G.S. 143B-282.1(b). were wrongfully applied to the detriment of the petitioner (the assessment factors are listed in the civil penalty assessment document); x (b) the violator promptly abated continuing environmental damage resulting from the violation (i.e., explain the steps that you took to correct the violation and prevent future occurrences); (c) the violation was inadvertent or a result of an accident (i.e., explain why the violation was unavoidable or something you could not prevent or prepare for); (d) the violator had not been assessed civil penalties for any previous violations; (e) payment of the civil penalty will prevent payment for the remaining necessary remedial actions (i.e., explain how payment of the civil penalty will prevent you from performing the activities necessary to achieve compliance). EXPLANATION: Please see the attached Remissions Request letter for detailed information. D E Q�� North Carolina Department of Environmental Quality I Division of Water Resources I Bio Lab 4401 Reedy Creek Road I 1621 Mail Service Center I Raleigh,North Carolina 27699-1621 NORTH CAROLINA _ op.n,,,M m E,,,i.n via,i� /✓ 919.743.8400 DocuSign Envelope ID:90E20F4&DC74-4117-9502-B5FFE1DC5266 STATE OF NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY COUNTY OF FORSYTH IN THE MATTER OF ASSESSMENT WAIVER OF RIGHT TO AN OF CIVIL PENALTIES AGAINST ADMINISTRATIVE HEARING AND STIPULATION OF FACTS Salem Business Park remediation site NPDES PERMIT NO. NCO080853 CASE NO. TX-2023-0003 Having been assessed civil penalties totaling$2,069.48 for violation(s) as set forth in the assessment document of the Director of the Division of Water Resources dated October 13 2023 the undersigned, desiring to seek remission of the civil penalties, does hereby waive the right to an administrative hearing in the above-stated matter and does stipulate that the facts are as alleged in the assessment document. The undersigned further understands that all evidence presented in support of remission of this civil penalty must be submitted to the Director of the Division of Water Resources within 30 days of receipt of the notice of assessment. No new evidence in support of a remission request will be allowed after 30 days from the receipt of the notice of assessment. This the �—� day f o c 23 . , 20 AD SS SIGNATURE C TELEPHONE D E Q North Carolina Department of Environmental Quality I Division of Water Resources Bio Lab ®®® 4401 Reedy Creek Road 1 1621 Mail Service Center Raleigh,North Carolina 27699-1 62 1 919.743.8400 Tables AECOM Sample Location Analyte Sample Date Network A Network B AS DT-1 EW-4 EW-5 EW-6 EW-12 EW-14 EW-16 EW-17 EW-18 EW-19 EW-21 EW-22 FE-151 Influent Influent Effluent 4/5/2023 4/25/2023 5/2/2023 Zinc 5/18/2023 (pg/L) 5/23/2023 6/22/2023 6/27/2023 7/26/2023 8/29(2023—®1 ®1 ®1 �®�, 4/5/2023 4/25/2023 5/2/2023 Barium 5/18/2023 5/23/2023 (Vg/L) 6/22/2023 6/27/2023 7/26/2023 8/29/2023 4/5/2023 4/25/2023 5/2/2023 Manganese 5/18/2023 (pg/L) 5/23/2023 6/22/2023 6/27/2023 7/26/2023 8/29/2023 Table 2 Summary of Costs to Identify Causes of Outfall Toxicity NPDES Permit No. NCO080853/2023-2024 Month/Year Activity Hours Rate Cost Laboratory Analysis for Metals -- -- $ 666.00 Field Technician Labor(sampling,water quality 3 $ 110.00 $ 330.00 April2023 screening) Engineer III (Data Analysis/DMR/AT3) 3 $ 120.00 $ 360.00 Project Director IV(Opts assess) 6 1 $ 190.00 $ 1,140.00 Subtotal $ 2,496.00 Laboratory Analysis for Metals -- -- $ 378.00 May 2023 Field Technician Labor 6 $ 55.00 $ 330.00 Engineer III (Data Analysis/DMR/AT3) 2 $ 120.00 $ 240.00 Project Dir. IV(Team directives) 4 $ 190.00 $ 760.00 Subtotal $ 1,708.00 Laboratory Analysis for Metals -- -- $ 106.00 June 2023 Field Technician Labor 2 $ 110.00 $ 220.00 Engineer III (Data Analysis/DMR) 1.5 $ 120.00 $ 180.00 Project Dir. IV(Team directives) 6 $ 190.00 $ 1,140.00 Subtotal $ 1,646.00 Laboratory Analysis for Metals -- -- $ 462.00 July 2023 Field Technician Labor 4 $ 110.00 $ 440.00 Engineer III (Data Analysis/DMR) 2 $ 120.00 $ 240.00 Subtotal $ 1,142.00 Laboratory Analysis for Metals -- -- $ 498.00 August 2023 Field Technician Labor 4 $ 110.00 $ 440.00 Engineer III (Data Analysis/DMR) 2 $ 120.00 $ 240.00 Subtotal $ 1,178.00 Engineer III (Field Suport, Generate Remissions 10 $ 120.00 $ 1,200.00 October 2023 Request Letter) Project Dir. IV(Team directives) 5 $ 190.00 $ 950.00 Subtotal $ 2,150.00 Laboratory Analysis for Metals -- -- $ 375.00 November 2023 Field Technician Labor 4 $ 110.00 $ 440.00 Engineer III (Data Analysis/DMR/Field Support) 10 $ 120.00 $ 1,200.00 Subtotal $ 2,015.00 Laboratory Analysis for Metals -- -- $ 81.00 December 2023 Field Technician Labor 1 $ 110.00 $ 110.00 Engineer III (Data Analysis/DMR/Field Support) 10 $ 120.00 $ 1,200.00 Subtotal $ 1,391.00 Laboratory Analysis for Metals -- -- $ 888.00 February 2024 Field Technician Labor 5 $ 110.00 $ 550.00 Engineer III (Data Ana lysis/DMR/Investigate 4 $ 120.00 $ 480.00 potential zinc treatment) Subtotal $ 1,918.00 Totall $ 13,494.00 Notes: Technician labor is calculated using 1 hr for system samples and 4 hrs for sampling all the extraction wells. Office labor is calculated using a minimum of 30 min.to track and analyze each lab report and an extra 30 min. per DMR. \\na.aecomnet.com\LFS\AMER\Raleigh-USRAL3\DCS\Projects\L-AECOM\Jobs\L\Alcatel-Lucent-04364\Winston-Salem\60649441-2021 0&1V1\500-De1iverab1es\501-NPDES Reporting\Toxicity Remission Requests\Calculation\Remission Request Costs.xlsx Attachment A Laboratory Analytical Reports AECOM Pace Analytical Services,LLC (�IaceAnalyfical@ 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 April 25, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: NOKIA Pace Project No.: 92661129 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on April 06, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, -4jGlAA , Bonnie Vang V bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM John Moran,AECOM Jon Wakeman,AECOM Environment f.Y�P 2" REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 19 e Pace Analytical Services,LLC te 100 laceAnalytical 9800HuIntesvlle,NC128078 wwwww..paclabs.com (704)875-9092 CERTIFICATIONS Project: NOKIA Pace Project No.: 92661129 Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA Pace Project No.: 92661129 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92661129001 FE-151 EPA 1664E REL 1 PASI-C EPA 200.7 Rev 4.4 1994 D661 11 PASI-A EPA 7470A BM 1 PASI-A EPA 8260D LMB 4 PASI-C SM 2540D-2015 JMH1 1 PASI-A SM 3500-Cr B-2011 JMH 1 PASI-A 92661129002 AS EFFLUENT EPA 200.7 Rev 4.4 1994 D661 11 PASI-A EPA 7470A BM 1 PASI-A SM 3500-Cr B-2011 JMH 1 PASI-A 92661129003 INF A EPA 200.7 Rev 4.4 1994 D661 11 PASI-A EPA 7470A BM 1 PASI-A SM 3500-Cr B-2011 JMH 1 PASI-A 92661129004 INF B EPA 200.7 Rev 4.4 1994 D661 11 PASI-A EPA 7470A BM 1 PASI-A SM 3500-Cr B-2011 JMH 1 PASI-A PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA Pace Project No.: 92661129 Sample: FE-151 Lab ID: 92661129001 Collected: 04/05/23 15:15 Received: 04/06/23 14:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services-Charlotte Oil and Grease ND mg/L 4.9 1 04/14/23 16:53 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:30 7440-38-2 Barium 31.6 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-39-3 Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:30 7440-43-9 Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-47-3 Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-50-8 Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:30 7439-89-6 Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7439-92-1 Manganese 964 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7439-96-5 Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:30 7782-49-2 Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:30 7440-22-4 Zinc 50.7 ug/L 10.0 1 04/10/23 09:13 04/24/23 15:30 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services-Asheville Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:18 7439-97-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Tetrachloroethene ND ug/L 1.0 1 04/13/23 22:23 127-18-4 Surrogates 4-Bromofluorobenzene(S) 97 % 70-130 1 04/13/23 22:23 460-00-4 1,2-Dichloroethane-d4(S) 109 % 70-130 1 04/13/23 22:23 17060-07-0 Toluene-d8(S) 101 % 70-130 1 04/13/23 22:23 2037-26-5 2540D Total Suspended Solids Analytical Method:SM 254OD-2015 Pace Analytical Services-Asheville Total Suspended Solids ND mg/L 2.5 1 04/11/23 12:18 Chromium, Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011 Pace Analytical Services-Asheville Chromium, Hexavalent ND mg/L 0.010 1 04/07/23 15:46 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA Pace Project No.: 92661129 Sample: AS EFFLUENT Lab ID: 92661129002 Collected: 04/05/23 15:10 Received: 04/06/23 14:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:33 7440-38-2 Barium 31.9 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-39-3 Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:33 7440-43-9 Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-47-3 Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-50-8 Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:33 7439-89-6 Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7439-92-1 Manganese 994 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7439-96-5 Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:33 7782-49-2 Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:33 7440-22-4 Zinc 56.8 ug/L 10.0 1 04/10/23 09:13 04/24/23 15:33 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services-Asheville Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:20 7439-97-6 Chromium,Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011 Pace Analytical Services-Asheville Chromium, Hexavalent ND mg/L 0.010 1 04/07/23 15:46 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA Pace Project No.: 92661129 Sample: INF A Lab ID: 92661129003 Collected: 04/05/23 15:00 Received: 04/06/23 14:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:36 7440-38-2 Barium 38.0 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-39-3 Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:36 7440-43-9 Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-47-3 Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-50-8 Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:36 7439-89-6 Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7439-92-1 Manganese 1290 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7439-96-5 Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:36 7782-49-2 Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:36 7440-22-4 Zinc 67.5 ug/L 10.0 1 04/10/23 09:13 04/24/23 15:36 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services-Asheville Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:22 7439-97-6 Chromium,Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011 Pace Analytical Services-Asheville Chromium, Hexavalent ND mg/L 0.010 1 04/07/23 15:46 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA Pace Project No.: 92661129 Sample: INF B Lab ID: 92661129004 Collected: 04/05/23 15:05 Received: 04/06/23 14:20 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Arsenic ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:39 7440-38-2 Barium 16.6 ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-39-3 Cadmium ND ug/L 1.0 1 04/10/23 09:13 04/24/23 15:39 7440-43-9 Chromium ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-47-3 Copper ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-50-8 Iron ND ug/L 50.0 1 04/10/23 09:13 04/24/23 15:39 7439-89-6 Lead ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7439-92-1 Manganese ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7439-96-5 Selenium ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:39 7782-49-2 Silver ND ug/L 5.0 1 04/10/23 09:13 04/24/23 15:39 7440-22-4 Zinc ND ug/L 10.0 1 04/10/23 09:13 04/24/23 15:39 7440-66-6 7470 Mercury Analytical Method: EPA 7470A Preparation Method: EPA 7470A Pace Analytical Services-Asheville Mercury ND ug/L 0.20 1 04/13/2315:08 04/14/2314:25 7439-97-6 Chromium,Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011 Pace Analytical Services-Asheville Chromium, Hexavalent 0.014 mg/L 0.010 1 04/07/23 15:47 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92661129 QC Batch: 768204 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92661129001 METHOD BLANK: 3988481 Matrix: Water Associated Lab Samples: 92661129001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 04/14/23 16:53 LABORATORY CONTROL SAMPLE: 3988482 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 40 41.1 103 78-114 MATRIX SPIKE SAMPLE: 3988483 35789915002 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 1 AJ 40 34.6 83 78-114 SAMPLE DUPLICATE: 3988484 92660477006 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L ND ND Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92661129 QC Batch: 767747 Analysis Method: EPA 7470A QC Batch Method: EPA 7470A Analysis Description: 7470 Mercury Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004 METHOD BLANK: 3986252 Matrix: Water Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.20 04/14/2313:09 LABORATORY CONTROL SAMPLE: 3986253 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Mercury ug/L 2.5 2.9 115 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3986254 3986255 MS MSD 92660002001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L ND 2.5 2.5 2.8 2.7 113 109 75-125 3 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92661129 QC Batch: 767001 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004 METHOD BLANK: 3982453 Matrix: Water Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic ug/L ND 10.0 04/24/2314:55 Barium ug/L ND 5.0 04/24/2314:55 Cadmium ug/L ND 1.0 04/24/2314:55 Chromium ug/L ND 5.0 04/24/2314:55 Copper ug/L ND 5.0 04/24/2314:55 Iron ug/L ND 50.0 04/24/2314:55 Lead ug/L ND 5.0 04/24/2314:55 Manganese ug/L ND 5.0 04/24/2314:55 Selenium ug/L ND 10.0 04/24/2314:55 Silver ug/L ND 5.0 04/24/2314:55 Zinc ug/L ND 10.0 04/24/2314:55 LABORATORY CONTROL SAMPLE: 3982454 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Arsenic ug/L 500 480 96 85-115 Barium ug/L 500 490 98 85-115 Cadmium ug/L 500 486 97 85-115 Chromium ug/L 500 486 97 85-115 Copper ug/L 500 485 97 85-115 Iron ug/L 5000 4850 97 85-115 Lead ug/L 500 486 97 85-115 Manganese ug/L 500 493 99 85-115 Selenium ug/L 500 474 95 85-115 Silver ug/L 250 240 96 85-115 Zinc ug/L 500 482 96 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3982455 3982456 MS MSD 92660310001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Arsenic ug/L ND 500 500 539 532 107 106 70-130 1 Barium ug/L 0.021 500 500 534 528 102 101 70-130 1 mg/L Cadmium ug/L ND 500 500 480 471 96 94 70-130 2 Chromium ug/L 0.022 500 500 518 511 99 98 70-130 1 mg/L Copper ug/L ND 500 500 581 572 116 114 70-130 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92661129 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3982455 3982456 MS MSD 92660310001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Iron ug/L 0.52 5000 5000 5530 5490 100 99 70-130 1 mg/L Lead ug/L 0.011 500 500 506 500 99 98 70-130 1 mg/L Manganese ug/L 0.18 500 500 687 677 101 99 70-130 1 mg/L Selenium ug/L ND 500 500 523 515 105 103 70-130 2 Silver ug/L ND 250 250 277 272 111 109 70-130 2 Zinc ug/L ND 500 500 479 473 94 93 70-130 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3982457 3982458 MS MSD 92661171001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Arsenic ug/L ND 500 500 503 506 101 101 70-130 0 Barium ug/L 8.4 500 500 506 512 100 101 70-130 1 Cadmium ug/L ND 500 500 490 497 98 99 70-130 1 Chromium ug/L ND 500 500 500 504 100 101 70-130 1 Copper ug/L ND 500 500 506 507 101 101 70-130 0 Iron ug/L 94.2 5000 5000 5130 5160 101 101 70-130 0 Lead ug/L ND 500 500 492 496 98 99 70-130 1 Manganese ug/L 38.6 500 500 541 546 100 101 70-130 1 Selenium ug/L ND 500 500 514 517 103 103 70-130 1 Silver ug/L ND 250 250 247 248 99 99 70-130 0 Zinc ug/L 116 500 500 611 614 99 100 70-130 1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92661129 QC Batch: 767946 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92661129001 METHOD BLANK: 3987374 Matrix: Water Associated Lab Samples: 92661129001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Tetrachloroethene ug/L ND 1.0 04/13/23 14:14 1,2-Dichloroethane-d4(S) % 108 70-130 04/13/23 14:14 4-Bromofluorobenzene(S) % 98 70-130 04/13/23 14:14 Toluene-d8(S) % 99 70-130 04/13/23 14:14 LABORATORY CONTROL SAMPLE: 3987375 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Tetrachloroethene ug/L 20 21.9 110 70-130 1,2-Dichloroethane-d4(S) % 103 70-130 4-Bromofluorobenzene(S) % 103 70-130 Toluene-d8(S) % 101 70-130 MATRIX SPIKE SAMPLE: 3987377 92660170002 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Tetrachloroethene ug/L 1.1 20 25.4 122 70-145 1,2-Dichloroethane-d4(S) % 103 70-130 4-Bromofluorobenzene(S) % 99 70-130 Toluene-d8(S) % 98 70-130 SAMPLE DUPLICATE: 3987376 92660170001 Dup Parameter Units Result Result RPD Qualifiers Tetrachloroethene ug/L ND ND 1,2-Dichloroethane-d4(S) % 109 105 4-Bromofluorobenzene(S) % 97 98 Toluene-d8(S) % 101 99 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92661129 QC Batch: 767255 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92661129001 METHOD BLANK: 3983720 Matrix: Water Associated Lab Samples: 92661129001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 04/11/23 12:17 LABORATORY CONTROL SAMPLE: 3983721 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 238 95 90-110 SAMPLE DUPLICATE: 3983986 92660578001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 27.5 34.0 21 SAMPLE DUPLICATE: 3983987 92661365001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 126 124 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92661129 QC Batch: 766684 Analysis Method: SM 3500-Cr B-2011 QC Batch Method: SM 3500-Cr B-2011 Analysis Description: Chromium,Hexavalent by SM3500-Cr B-2011 Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004 METHOD BLANK: 3981067 Matrix: Water Associated Lab Samples: 92661129001,92661129002,92661129003,92661129004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chromium, Hexavalent mg/L ND 0.010 04/07/23 15:42 LABORATORY CONTROL SAMPLE: 3981068 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Chromium, Hexavalent mg/L 0.25 0.26 102 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3981069 3981070 MS MSD 92661128001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chromium, Hexavalent mg/L 0.010 0.25 0.25 0.27 0.27 102 105 90-110 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: NOKIA Pace Project No.: 92661129 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 19 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA Pace Project No.: 92661129 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92661129001 FE-151 EPA1664B 768204 92661129001 FE-151 EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134 92661129002 AS EFFLUENT EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134 92661129003 INF A EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134 92661129004 INF B EPA 200.7 Rev 4.4 1994 767001 EPA 200.7 Rev 4.4 1994 767134 92661129001 FE-151 EPA 7470A 767747 EPA 7470A 768057 92661129002 AS EFFLUENT EPA 7470A 767747 EPA 7470A 768057 92661129003 INF A EPA 7470A 767747 EPA 7470A 768057 92661129004 INF B EPA 7470A 767747 EPA 7470A 768057 92661129001 FE-151 EPA 8260D 767946 92661129001 FE-151 SM 2540D-2015 767255 92661129001 FE-151 SM 3500-CrB-2011 766684 92661129002 AS EFFLUENT SM 3500-Cr B-2011 766684 92661129003 INF A SM 3500-CrB-2011 766684 92661129004 INF B SM 3500-CrB-2011 766684 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:04/25/2023 04:09 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 19 z z �xzzzzt�s zzz z- z `I ^�-M z O c o `' Y a G m M a o Lad. •�' QY C' m' ''� ` 2 i .K LL CEl C co 4 C. �r'.pPIi -J1 QI !I 1 J u •) U c E U u E Y E w 'Qt C p _ 'z ci u c > ' G' a. u o + .� EE .a mo.'r 4, E ,. E c �` ,,' _ p k- 1-' V v u U. mw:4r+maa J .H: mw4,C) M.m' .•I;nti-pry a u a'-'.�4:� - . [ I] o� � N �.OU.J1lU`i�.Ui.l a.Oi Vll�f�{� •1�-. CO.l.�� - dm �/ EL cm .0 uuu ucvcrP❑m(ku:lnav! a izN � ■ O J /. I 3 Z. CD to M Q V N :� t s ,O vs 14 Ql c 14 r+ n PI a > 777 E v 77g40 7,7 r7�� Ate, rr E O E •r9 O .� d - - ze c c in ME f0vto 1 • 1 SL gJ U 1= U u °' cu f o 3 >- 0 aE a o o y u 01 y v C/ E c 3 0 .L a 3 1 E N a a 1 o u e E v 3 na u v y; L m — � > 3 W- 6 C V F c 'o � N o ou Q W - Y 0 V Zva U E y Z u a fy y u n 0 to w in of -o ,-,._. O s H a.. ..a t �l v LL O U en � y a/ a � ` MI I U m I {�� .ni � d LO ^• 7i U � C U - O Gl N r 1 1i7 a. d J 9 cz •X V J J b v v 9 Z ® - -` ciCL L C c V \ v p n Q)i E E a '- CL d 19 E a a E c c c u a i°J u a u v s n -^ u - rmt a a DC# 'Title: ENV-FRM-HUN1-0083 02_Sample Condition Upon Receipt ace a»cauacu Effoctive Date: 11/14/2022 8:18:36 AM f "Check mark top half of box if pH and/or dechlorination Is verified and Proj_ect_I# WO# : 92661 129 Withln the acceptance rAnge for preservation samples. FM: BV Due Date: 04/18/23 .'4teptlons:VOA,Coliforni, 0C,Oil and Grease, DRO/80.15(water)DOC,LLHg ,,,,: CLIENT: 92—AECOM—RAL (3ottom half of box`isr'to Ilst number of bottles ***Check all unpreserl/ed Nitrates for chlorine Z Q Q p _ Z 2 ` V Q Z Y l = v � v '� = u z z i i °' a > -5 n ro n ° v v a Z Q ¢ ry z v v g� ccyy ro n FL n dl O p ¢ p ' Z Ln _ 7iJ a j N i Z g a a` T a o n c y 2 c ? Z u N m a n u rd N E Q 2 2 0. - 0. ., : d O - '' Q O b Q a to J .J J .d ..J J: J J z J .:� J 7 > ? > [L C in to .l E E E': E E E E E E F E E E E E E J -' y� N D t1tiA — N p se• �^ OLA V N N U1 N'r Uh J v x > o nG, G - �r rn. a l7- 0 q r :S[ on m t-rCr. m.: ,m•: t/�:z. .,.�:r _T. .,�:... £. Q • o ? 7.. C �x<: ,.d'r.u�i v; �' _T, : 7' p ).s 1 A � t i 3\X\1\1 t z � 3 ti t � JI \N NN\N \N 6 7 8 9 I 10 11 12 N�w pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon recelpt Date preservatlon adjusted Time preservatlon Amount of Preservative Lot R adjusted added Note: Wheneverthere Is a discrepancy affecdL,g North Carolina compltarce samples,a cofrr of this formwi II be sent to the NorthCarolira DENR Certificatlon Office(i.e. Out cl hold,incorrect preservative,out of temp,incoreect containers, Page 18 of 19 Hexavalent Chromium pH Adjustment 7199 WH 9.0-9.5 218.6 WH 9.3-9.7 �D✓"` Project number: No ��' " L°-7p I S 5 Initial Adjusted Volume Sample ID Initial pH Date/Time Date/Time Adjusted pH Acld/Base Used (Drops) Fe - is "6- A -5 ,35 � Page 19 of 19 Pace Analytical Services,LLC 9800 Kin aceAnalytical® ey Ave. Suite 100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 May 08, 2023 Conan Fitzgerald AECOM 5438 Wade Park Blvd Suite 200 Raleigh, NC 27607 RE: Project: NOKIA WS Pace Project No.: 92664610 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on April 26, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace National-Mt.Juliet • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, -�)GlAA , Bonnie Vang V bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures f.Y�P 2" REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 13 e Pace Analytical Services,LLC te 100 laceAnalytical 9800HuIntesvlle,NC128078 wwwww..paclabs.com (704)875-9092 CERTIFICATIONS Project: NOKIA WS Pace Project No.: 92664610 Pace Analytical Services National 12065 Lebanon Road,Mt.Juliet,TN 37122 Nevada Certification#:TN-03-2002-34 Alabama Certification#:40660 New Hampshire Certification#: 2975 Alaska Certification 17-026 New Jersey Certification#:TNO02 Arizona Certification#:AZ0612 New Mexico DW Certification Arkansas Certification#:88-0469 New York Certification#: 11742 California Certification#:2932 North Carolina Aquatic Toxicity Certification#:41 Canada Certification#: 1461.01 North Carolina Drinking Water Certification#:21704 Colorado Certification#:TN00003 North Carolina Environmental Certificate#:375 Connecticut Certification#:PH-0197 North Dakota Certification#:R-140 DOD Certification:#1461.01 Ohio VAP Certification#:CL0069 EPA#TN00003 Oklahoma Certification#:9915 Florida Certification#: E87487 Oregon Certification#:TN200002 Georgia DW Certification#:923 Pennsylvania Certification#:68-02979 Georgia Certification:NELAP Rhode Island Certification#:LA000356 Idaho Certification#:TN00003 South Carolina Certification#:84004 Illinois Certification#:200008 South Dakota Certification Indiana Certification#:C-TN-01 Tennessee DW/Chem/Micro Certification#: 2006 Iowa Certification#:364 Texas Certification#:T 104704245-17-14 Kansas Certification#:E-10277 Texas Mold Certification#:LAB0152 Kentucky UST Certification#: 16 USDA Soil Permit#: P330-15-00234 Kentucky Certification#:90010 Utah Certification#:TN00003 Louisiana Certification#:A130792 Virginia Certification#:VT2006 Louisiana DW Certification#:LA180010 Vermont Dept.of Health: ID#VT-2006 Maine Certification#:TN0002 Virginia Certification#:460132 Maryland Certification#:324 Washington Certification#:C847 Massachusetts Certification#:M-TNO03 West Virginia Certification#:233 Michigan Certification#:9958 Wisconsin Certification#:998093910 Minnesota Certification#:047-999-395 Wyoming UST Certification#:via A21LA 2926.01 Mississippi Certification#:TN00003 A2LA-ISO 17025 Certification#: 1461.01 Missouri Certification#:340 A2LA-ISO 17025 Certification#: 1461.02 Montana Certification#:CERT0086 AIHA-LAP/LLC EMLAP Certification#:100789 Nebraska Certification#:NE-OS-15-05 Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA WS Pace Project No.: 92664610 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92664610001 AS EFFLUENT EPA200.7 ZSA 11 PAN EPA 245.1 LAS 1 PAN EPA 8260D TMH 4 PASI-C SM 3500-Cr B-2011 JMH 1 PASI-A PAN=Pace National-Mt.Juliet PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92664610 Sample: AS EFFLUENT Lab ID: 92664610001 Collected: 04/25/23 10:20 Received: 04/26/23 17:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual Metals(ICP)200.7 Analytical Method: EPA 200.7 Preparation Method:200.7 Pace National-Mt.Juliet Arsenic ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7440-38-2 Barium 32.5 ug/L 5.00 1 05/07/23 09:50 05/07/23 16:36 7440-39-3 Cadmium ND ug/L 2.00 1 05/07/23 09:50 05/07/23 16:36 7440-43-9 Chromium ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7440-47-3 Copper ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7440-50-8 Iron ND ug/L 50.0 1 05/07/23 09:50 05/07/23 16:36 7439-89-6 Lead ND ug/L 5.00 1 05/07/23 09:50 05/07/23 16:36 7439-92-1 Manganese 1020 ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7439-96-5 Selenium ND ug/L 10.0 1 05/07/23 09:50 05/07/23 16:36 7782-49-2 Silver ND ug/L 5.00 1 05/07/23 09:50 05/07/23 16:36 7440-22-4 Zinc 55.2 ug/L 50.0 1 05/07/23 09:50 05/07/23 16:36 7440-66-6 Mercury 245.1 Analytical Method: EPA 245.1 Preparation Method:245.1 Pace National-Mt.Juliet Mercury ND ug/L 0.200 1 04/30/23 22:14 05/01/23 13:33 7439-97-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Tetrachloroethene 3.7 ug/L 1.0 1 04/30/23 09:13 127-18-4 Surrogates 4-Bromofluorobenzene(S) 101 % 70-130 1 04/30/23 09:13 460-00-4 1,2-Dichloroethane-d4(S) 106 % 70-130 1 04/30/23 09:13 17060-07-0 Toluene-d8(S) 106 % 70-130 1 04/30/23 09:13 2037-26-5 Chromium, Hexavalent,28 Day Analytical Method:SM 3500-Cr B-2011 Pace Analytical Services-Asheville Chromium, Hexavalent ND mg/L 0.010 1 04/29/23 16:12 18540-29-9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WS Pace Project No.: 92664610 QC Batch: 2055073 Analysis Method: EPA 200.7 QC Batch Method: 200.7 Analysis Description: Metals(ICP)200.7 Laboratory: Pace National-Mt.Juliet Associated Lab Samples: 92664610001 METHOD BLANK: R3921853-1 Matrix: Water Associated Lab Samples: 92664610001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Arsenic ug/L ND 10.0 05/07/2315:55 Barium ug/L ND 5.00 05/07/2315:55 Cadmium ug/L ND 2.00 05/07/2315:55 Chromium ug/L ND 10.0 05/07/2315:55 Copper ug/L ND 10.0 05/07/2315:55 Iron ug/L ND 50.0 05/07/2315:55 Lead ug/L ND 5.00 05/07/2315:55 Manganese ug/L ND 10.0 05/07/2315:55 Selenium ug/L ND 10.0 05/07/2315:55 Silver ug/L ND 5.00 05/07/2315:55 Zinc ug/L ND 50.0 05/07/2315:55 LABORATORY CONTROL SAMPLE: R3921853-2 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Arsenic ug/L 1000 977 97.7 85.0-115 Barium ug/L 1000 990 99.0 85.0-115 Cadmium ug/L 1000 987 98.7 85.0-115 Chromium ug/L 1000 953 95.3 85.0-115 Copper ug/L 1000 976 97.6 85.0-115 Iron ug/L 10000 9680 96.8 85.0-115 Lead ug/L 1000 980 98.0 85.0-115 Manganese ug/L 1000 921 92.1 85.0-115 Selenium ug/L 1000 1040 104 85.0-115 Silver ug/L 200 193 96.7 85.0-115 Zinc ug/L 1000 982 98.2 85.0-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3921853-4 R3921853-5 MS MSD L1611232-01 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Arsenic ug/L ND 1000 1000 1080 1070 108 107 70.0-130 1.44 Barium ug/L 158 1000 1000 1210 1180 105 103 70.0-130 1.80 Cadmium ug/L ND 1000 1000 1090 1060 109 106 70.0-130 2.04 Chromium ug/L 1.94 1000 1000 1030 1020 103 101 70.0-130 1.64 Copper ug/L ND 1000 1000 1050 1030 105 103 70.0-130 1.45 Iron ug/L 153 10000 10000 10400 10300 103 102 70.0-130 1.34 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WS Pace Project No.: 92664610 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3921853-4 R3921853-5 MS MSD L1611232-01 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Lead ug/L ND 1000 1000 1070 1050 107 105 70.0-130 2.17 Manganese ug/L 2.26 1000 1000 994 972 99.2 97.0 70.0-130 2.25 Selenium ug/L ND 1000 1000 1160 1150 116 115 70.0-130 1.09 Silver ug/L ND 200 200 210 206 105 103 70.0-130 1.84 Zinc ug/L 49.5 1000 1000 1070 1050 103 100 70.0-130 2.10 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3921853-6 R3921853-7 MS MSD L1612317-08 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Arsenic ug/L ND 1000 1000 1070 1100 107 110 70.0-130 2.93 Barium ug/L 15.4 1000 1000 1040 1050 102 104 70.0-130 1.23 Cadmium ug/L ND 1000 1000 1060 1090 106 109 70.0-130 2.65 Chromium ug/L ND 1000 1000 994 1020 99.4 102 70.0-130 2.36 Copper ug/L 4.87 1000 1000 1050 1080 104 107 70.0-130 2.51 Iron ug/L 383 10000 10000 10300 10500 99.5 102 70.0-130 2.05 Lead ug/L ND 1000 1000 1040 1080 104 108 70.0-130 3.18 Manganese ug/L 58.9 1000 1000 1000 1030 94.3 96.8 70.0-130 2.48 Selenium ug/L ND 1000 1000 1130 1190 113 119 70.0-130 4.62 Silver ug/L ND 200 200 187 193 93.3 96.4 70.0-130 3.21 Zinc ug/L 33.1 1000 1000 1050 1090 102 105 70.0-130 3.10 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WS Pace Project No.: 92664610 QC Batch: 2051541 Analysis Method: EPA 245.1 QC Batch Method: 245.1 Analysis Description: Mercury 245.1 Laboratory: Pace National-Mt.Juliet Associated Lab Samples: 92664610001 METHOD BLANK: R3919487-1 Matrix: Water Associated Lab Samples: 92664610001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury ug/L ND 0.200 05/01/2312:41 LABORATORY CONTROL SAMPLE: R3919487-2 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Mercury ug/L 3.00 3.20 107 85.0-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3919487-3 R3919487-4 MS MSD L1609306-01 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L ND 3.00 3.00 3.23 3.17 108 106 70.0-130 1.99 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: R3919487-5 R3919487-6 MS MSD L1609589-01 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Mercury ug/L ND 3.00 3.00 3.35 3.25 112 108 70.0-130 2.81 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WS Pace Project No.: 92664610 QC Batch: 771354 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92664610001 METHOD BLANK: 4004348 Matrix: Water Associated Lab Samples: 92664610001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Tetrachloroethene ug/L ND 1.0 04/30/23 03:03 1,2-Dichloroethane-d4(S) % 108 70-130 04/30/23 03:03 4-Bromofluorobenzene(S) % 105 70-130 04/30/23 03:03 Toluene-d8(S) % 102 70-130 04/30/23 03:03 LABORATORY CONTROL SAMPLE: 4004349 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Tetrachloroethene ug/L 20 18.2 91 70-130 1,2-Dichloroethane-d4(S) % 104 70-130 4-Bromofluorobenzene(S) % 98 70-130 Toluene-d8(S) % 101 70-130 MATRIX SPIKE SAMPLE: 4004351 92664150011 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Tetrachloroethene ug/L 20 19.8 99 70-145 1,2-Dichloroethane-d4(S) % 100 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 102 70-130 SAMPLE DUPLICATE: 4004350 92664150009 Dup Parameter Units Result Result RPD Qualifiers Tetrachloroethene ug/L ND 1,2-Dichloroethane-d4(S) % 105 91 4-Bromofluorobenzene(S) % 95 96 Toluene-d8(S) % 101 99 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WS Pace Project No.: 92664610 QC Batch: 771294 Analysis Method: SM 3500-Cr B-2011 QC Batch Method: SM 3500-Cr B-2011 Analysis Description: Chromium,Hexavalent by SM3500-Cr B-2011 Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92664610001 METHOD BLANK: 4004162 Matrix: Water Associated Lab Samples: 92664610001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chromium, Hexavalent mg/L ND 0.010 04/29/23 16:12 LABORATORY CONTROL SAMPLE: 4004163 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Chromium, Hexavalent mg/L 0.25 0.25 100 90-110 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4004164 4004165 MS MSD 92664610001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Chromium, Hexavalent mg/L ND 0.25 0.25 0.26 0.25 102 96 90-110 6 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: NOKIA WS Pace Project No.: 92664610 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 13 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA WS Pace Project No.: 92664610 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92664610001 AS EFFLUENT 200.7 2055073 EPA200.7 2055073 92664610001 AS EFFLUENT 245.1 2051541 EPA245.1 2051541 92664610001 AS EFFLUENT EPA8260D 771354 92664610001 AS EFFLUENT SM 3500-Cr B-2011 771294 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/08/2023 10:25 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 13 v n c r) n � > a ro n vc�v� c `- a o o b c K 3 s C1 o r' v �+ 7Ll v R n '• in in v� �, \ `�• co / as :o on O rho t`' cr ; a r v clo c n o ^ o q N L y o a Z n 3 71 d � o yw p a �. 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O y-1+• e�1"tl a t�'r <.r~- '��'-�a N pC ro 3 r�* o• ¢ .,� m ro: .9 a o c:m 4 r•o r n u n m 3 9 v �� dim HNane nn� - It rt 3 rD d S n o r :roa � ,o oar n :� Qtz.. 2 a zzxryyzy� �zxat��, , Page 12 of_13 ce' QC#_Tlfle: ENV-FRM-HUN1.008$v02_Sample Conditlon Upon Receipt a Effectivo Date: 11/14/2022.8:1830 AM *Check mark top half of box If pH and/or dechlorination Is verified and Project h WO# : 92664610 within the acceptance range for preservation samples, PM: BV Due Date: 05/08/23 Exceptions:VOA,Conform;TpC,OII and Grease,DRO/8015(water)ROC, LLHg CLIENT: 92—AECOM—RAL *"Bottom half of box is o list number of bottles ""*Chock all unpreserved Nitrates for chlorine J z z 2 2 a Y O� _ � a z _ � m � Z N z N a z N c� Z 2 n, rJ . x a a Lq O = ^� x O U Q cry a� s u u. > '1 L':: c¢# c c M. =N Z Z lJ a c O N a Z O ai '7 a ^ Z o Q N Z �p N 2 Z R Off" 6 4�. C M = i+ /1 Ol u , rya :i'1 U. _ .R ^ N 7 A .O .o �+ u 2 Z 7 Z .� 't. .p ." rrr6 _ a F E a E Ag ¢ Q a ^ b "CL a a ¢ °� d d J 1 d j O O a 4 N *4CL E E E b: E E E E b b E E _r a ' n _. E E 1 n a o T u1 a n N _ _ o _ o E E E E E E o, E E Hr tOtt .Ji N}�+ n H ,Ny r•� ri N cT M Uj ❑ 7 7 ;Vf f !� a5 _ O u5 - V Si 1- 5 ,?M Q{7 7 9 7r p M 7 Yv ; M m Ln N a ;i x > {n O3, J ljO71 {n. m Q > o 1 2 3 I\ \1 \N\1 n s 6 7 8 9 I 10 11 1Z pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time,preservation Amount of Preservative Lot It adjusted added Note: Whenever there Is adisereparcyaffe:tirgNorthCaro!:na compliance samples,acopyofthisformwill besen't to the NorthCaroliraDENR Certification Office fi.e. Out of hold, Incorrect preservative, cut of temp,incorrect containers. Page 13 of 13 Pace Analytical Services,LLC 9800 Kin aceAnalytical® ey Ave. Suite 100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 May 30, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on May 19, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte • Pace Analytical Services-Ormond Beach If you have any questions concerning this report, please feel free to contact me. Sincerely, -�)GlAA , Bonnie Vang V bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM Cristin Dolan,AECOM Teresa Amentt Jennings,AECOM Jon Wakeman,AECOM Environment 2� REPORT OF LABORATORY ANALYSIS r This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 12 e Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kincey Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 CERTIFICATIONS Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 Pace Analytical Services Ormond Beach 8 East Tower Circle,Ormond Beach, FL 32174 Missouri Certification#:236 Alaska DEC-CS/UST/LUST Montana Certification#:Cert 0074 Alabama Certification#:41320 Nebraska Certification: NE-OS-28-14 Colorado Certification: FL NELAC Reciprocity New Hampshire Certification#:2958 Connecticut Certification#: PH-0216 New Jersey Certification#: FL022 Delaware Certification: FL NELAC Reciprocity New York Certification#: 11608 DoD-ANAB#:ADE-3199 North Carolina Environmental Certificate#:667 Florida Certification#: E83079 North Carolina Certification#: 12710 Georgia Certification#:955 North Dakota Certification#:R-216 Guam Certification: FL NELAC Reciprocity Ohio DEP 87780 Hawaii Certification:FL NELAC Reciprocity Oklahoma Certification#: D9947 Illinois Certification#:200068 Pennsylvania Certification#:68-00547 Indiana Certification: FL NELAC Reciprocity Puerto Rico Certification#: FLO1264 Kansas Certification#:E-10383 South Carolina Certification:#96042001 Kentucky Certification#:90050 Tennessee Certification#:TN02974 Louisiana Certification#: FL NELAC Reciprocity Texas Certification:FL NELAC Reciprocity Louisiana Environmental Certificate#:05007 US Virgin Islands Certification:FL NELAC Reciprocity Maine Certification#: FLO1264 Virginia Environmental Certification#:460165 Maryland Certification:#346 West Virginia Certification#:9962C Massachusetts Certification#:M-FL1264 Wisconsin Certification#:399079670 Michigan Certification#:9911 Wyoming(EPA Region 8): FL NELAC Reciprocity Mississippi Certification:FL NELAC Reciprocity Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100, Huntersville, NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#: LA029 South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92668464001 FE-151 EPA 1664E REL 1 PASI-C EPA 200.7 KC2 3 PASI-O EPA 8260D LMB 4 PASI-C SM 2540D-2015 JMH1 1 PASI-A PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte PASI-O=Pace Analytical Services-Ormond Beach REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 Sample: FE-151 Lab ID: 92668464001 Collected: 05/18/23 13:00 Received: 05/19/23 09:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual HEM,Oil and Grease Analytical Method: EPA 1664E Pace Analytical Services-Charlotte Oil and Grease 7.9 mg/L 4.9 1 05/23/23 05:06 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 28.8 ug/L 10.0 1 05/24/23 16:29 05/27/23 07:11 7440-39-3 Manganese 10.3 ug/L 5.0 1 05/24/23 16:29 05/27/23 07:11 7439-96-5 Zinc ND ug/L 20.0 1 05/24/23 16:29 05/27/23 07:11 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Tetrachloroethene 2.1 ug/L 1.0 1 05/24/23 04:16 127-18-4 Surrogates 4-Bromofluorobenzene(S) 102 % 70-130 1 05/24/23 04:16 460-00-4 1,2-Dichloroethane-d4(S) 96 % 70-130 1 05/24/23 04:16 17060-07-0 Toluene-d8(S) 103 % 70-130 1 05/24/23 04:16 2037-26-5 2540D Total Suspended Solids Analytical Method:SM 2540D-2015 Pace Analytical Services-Asheville Total Suspended Solids ND mg/L 2.5 1 05/24/23 11:20 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 QC Batch: 776097 Analysis Method: EPA 1664B QC Batch Method: EPA 1664E Analysis Description: 1664 HEM,Oil and Grease Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92668464001 METHOD BLANK: 4026843 Matrix: Water Associated Lab Samples: 92668464001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Oil and Grease mg/L ND 5.0 05/23/23 05:06 LABORATORY CONTROL SAMPLE: 4026844 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L 40 32.5 81 78-114 MATRIX SPIKE SAMPLE: 4026845 92668256002 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Oil and Grease mg/L ND 38.5 35.0 91 78-114 SAMPLE DUPLICATE: 4026846 92668288002 Dup Parameter Units Result Result RPD Qualifiers Oil and Grease mg/L ND ND Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 QC Batch: 920601 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Ormond Beach Associated Lab Samples: 92668464001 METHOD BLANK: 5061930 Matrix: Water Associated Lab Samples: 92668464001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 10.0 05/27/23 05:19 Manganese ug/L ND 5.0 05/27/23 05:19 Zinc ug/L ND 20.0 05/27/23 05:19 LABORATORY CONTROL SAMPLE: 5061931 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 250 259 104 85-115 Manganese ug/L 250 262 105 85-115 Zinc ug/L 1250 1340 107 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5061932 5061933 MS MSD 35801496001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 71.4 250 250 330 335 103 106 70-130 2 Manganese ug/L 83.3 250 250 334 340 100 103 70-130 2 Zinc ug/L 662 1250 1250 1890 1930 98 101 70-130 2 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5061934 5061935 MS MSD 92667772006 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 173 250 250 440 427 107 101 70-130 3 Manganese ug/L 559 250 250 826 804 107 98 70-130 3 Zinc ug/L ND 1250 1250 1360 1330 108 106 70-130 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 QC Batch: 776373 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92668464001 METHOD BLANK: 4027995 Matrix: Water Associated Lab Samples: 92668464001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Tetrachloroethene ug/L ND 1.0 05/23/23 22:55 1,2-Dichloroethane-d4(S) % 95 70-130 05/23/23 22:55 4-Bromofluorobenzene(S) % 104 70-130 05/23/23 22:55 Toluene-d8(S) % 103 70-130 05/23/23 22:55 LABORATORY CONTROL SAMPLE: 4027996 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Tetrachloroethene ug/L 20 18.0 90 70-130 1,2-Dichloroethane-d4(S) % 102 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 99 70-130 MATRIX SPIKE SAMPLE: 4027998 92668464001 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Tetrachloroethene ug/L 2.1 20 24.6 113 70-145 1,2-Dichloroethane-d4(S) % 97 70-130 4-Bromofluorobenzene(S) % 101 70-130 Toluene-d8(S) % 100 70-130 SAMPLE DUPLICATE: 4027997 92668421001 Dup Parameter Units Result Result RPD Qualifiers Tetrachloroethene ug/L ND ND 1,2-Dichloroethane-d4(S) % 99 93 4-Bromofluorobenzene(S) % 105 101 Toluene-d8(S) % 102 103 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 QC Batch: 776583 Analysis Method: SM 2540D-2015 QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92668464001 METHOD BLANK: 4028873 Matrix: Water Associated Lab Samples: 92668464001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 05/24/23 11:17 LABORATORY CONTROL SAMPLE: 4028874 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Total Suspended Solids mg/L 250 246 98 90-110 SAMPLE DUPLICATE: 4029014 92668450001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 4020 4140 3 SAMPLE DUPLICATE: 4029015 92668629001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 222 232 4 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 12 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA WINSTON SALEM Pace Project No.: 92668464 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92668464001 FE-151 EPA1664B 776097 92668464001 FE-151 EPA 200.7 920601 EPA 200.7 920640 92668464001 FE-151 EPA 8260D 776373 92668464001 FE-151 SM 254OD-2015 776583 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/30/2023 02:52 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 12 U Li .o cl tQ N v j ' 7 } t O F( C N 17. � C d�i ro >' a O U 4 t f _ c H V : M N �WL.� 71•. t S E40 61 l'H W.-. V y� "f yK'� fi ° ( �S�'Y£� r r "�:f) t U �•� 'D -- O N` W W g ;�i!�W,.'r,ML l � 'L ', ��+ �y^+.� .�E � Sr .•� ,� .� p ai G W t � W.:. N to N iry _..� •n E .� M (!.V E � 4. I�. 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Ns It — - -N\ .Lia I N7 i N\\- \N . p .f k.AOl1 le. dip. �'� 43 B ilu g n to I--,—. _ .. .. �l_1�a�P{4�1o�,:�a�et3lN�aivasi�ady�ij�•- Js�s JUM-W003U-Z6 A3I10 �Hll. QO0*40VO#tiWOOR116 tUQ'l&WOObtyis 1 £Z/t£/50 :a180 ama Ag :Wd 4!�► tlaf0ad pu paWiral►1.sltlt�31�9]• ? p�:xdlh�i -Fi1 aq 4 ? /loy+0 #J+r ti9�899Z6 � #ors 101 >,.e uodn.uoliIPuoa Id 3� °C900 NRO +'p� �, Pag'o.. of 12 Pace Analytical Services,LLC 9800 Kin aceAnalytical® ey Ave. Suite 100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 June 02, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: NOKIA Pace Project No.: 92669092 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on May 24, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Ormond Beach If you have any questions concerning this report, please feel free to contact me. Sincerely,Q - aAAa, Bonnie Vang bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM Cristin Dolan,AECOM Teresa Amentt Jennings,AECOM Jon Wakeman,AECOM Environment z REPORT OF LABORATORY ANALYSIS N This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 9 6 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 CERTIFICATIONS Project: NOKIA Pace Project No.: 92669092 Pace Analytical Services Ormond Beach 8 East Tower Circle,Ormond Beach, FL 32174 Missouri Certification#:236 Alaska DEC-CS/UST/LUST Montana Certification#:Cert 0074 Alabama Certification#:41320 Nebraska Certification: NE-OS-28-14 Colorado Certification: FL NELAC Reciprocity New Hampshire Certification#:2958 Connecticut Certification#: PH-0216 New Jersey Certification#: FL022 Delaware Certification: FL NELAC Reciprocity New York Certification#: 11608 DoD-ANAB#:ADE-3199 North Carolina Environmental Certificate#:667 Florida Certification#: E83079 North Carolina Certification#: 12710 Georgia Certification#:955 North Dakota Certification#:R-216 Guam Certification: FL NELAC Reciprocity Ohio DEP 87780 Hawaii Certification:FL NELAC Reciprocity Oklahoma Certification#: D9947 Illinois Certification#:200068 Pennsylvania Certification#:68-00547 Indiana Certification: FL NELAC Reciprocity Puerto Rico Certification#: FLO1264 Kansas Certification#:E-10383 South Carolina Certification:#96042001 Kentucky Certification#:90050 Tennessee Certification#:TN02974 Louisiana Certification#: FL NELAC Reciprocity Texas Certification:FL NELAC Reciprocity Louisiana Environmental Certificate#:05007 US Virgin Islands Certification:FL NELAC Reciprocity Maine Certification#: FLO1264 Virginia Environmental Certification#:460165 Maryland Certification:#346 West Virginia Certification#:9962C Massachusetts Certification#:M-FL1264 Wisconsin Certification#:399079670 Michigan Certification#:9911 Wyoming(EPA Region 8): FL NELAC Reciprocity Mississippi Certification:FL NELAC Reciprocity REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 9 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA Pace Project No.: 92669092 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92669092001 FE-151 EPA 200.7 KPP 3 PASI-O PASI-O=Pace Analytical Services-Ormond Beach REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 9 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA Pace Project No.: 92669092 Sample: FE-151 Lab ID: 92669092001 Collected: 05/23/23 12:00 Received: 05/24/23 12:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 31.5 ug/L 10.0 1 05/30/2315:45 06/01/2317:25 7440-39-3 Manganese 9.6 ug/L 5.0 1 05/30/2315:45 06/01/2317:25 7439-96-5 Zinc ND ug/L 20.0 1 05/30/2315:45 06/01/2317:25 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:06/02/2023 11:30 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 9 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA Pace Project No.: 92669092 QC Batch: 921841 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Ormond Beach Associated Lab Samples: 92669092001 METHOD BLANK: 5067534 Matrix: Water Associated Lab Samples: 92669092001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 10.0 06/01/2316:37 Manganese ug/L ND 5.0 06/01/2316:37 Zinc ug/L ND 20.0 06/01/2316:37 LABORATORY CONTROL SAMPLE: 5067535 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 250 278 111 85-115 Manganese ug/L 250 263 105 85-115 Zinc ug/L 1250 1280 102 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5067536 5067537 MS MSD 92669071001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 41.5 250 250 309 303 107 105 70-130 2 Manganese ug/L 712 250 250 971 951 104 96 70-130 2 Zinc ug/L 0.22 1250 1250 1530 1520 104 104 70-130 1 mg/L Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:06/02/2023 11:30 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 9 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: NOKIA Pace Project No.: 92669092 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:06/02/2023 11:30 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 9 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA Pace Project No.: 92669092 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92669092001 FE-151 EPA 200.7 921841 EPA 200.7 921884 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:06/02/2023 11:30 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 9 �, - ` o _� 3_- o a o — n 0 a v o v ro m (�fro 6 o < o n in' N )rru rD r� D vl w ° \ Q• rD G Z- n H `G � cr o 9 ( rn o O L'I -t - }� 3 0 w d C 7 n z K < v c _ (a, c �•O [�['� W � p Q �. 3 �1 � t N ti N a Q x r� m 5 .... - _A y.A r� LO o m 1.1 Y7 v Doi CD O • A N L Y n N O. Q 2 � ocl o a o n n Oj Da ., a ro � N •• - _ -- rD O O a p [ e Z N ° e rD m rD 3 2: o o 'c" o n v �. o'. g C _ R cv 3 r"o O m o c \ a tt ? 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K7 •. unn1 r z N N. tt rD 1 fD Z (7 n (ND. _ rt.�.n W il z .�2:Z 'ZI .91:�t n P&g 8 9 :YN rK �[.[i.i.^JT[L]111T ^ r.1+L+.1.'L`t_.r4K' • l' -1Kin. [[%A lL"1 1A1ri`.i{IR1R�.iGhVWVI1F'ASArLT.iFA[12�5".,�[Kt1riCAfr_\'1[A11t5?3!191Yif.5 liL'Ai1i 2i�i3':1X�133".I-/1.+ bowl. ltlet,EW-FRM-HUN`1•0083 V62.AMplO-:Jd-Onditl&'-Upon Receipt tiecttve b.OV�,�1/1q�. $� 4 ',AI1� . '+Chq.'-A n0k.tgp[0I1FOfb K:itpH00/04ichis;!rMOon 19 Ved(fedand proj��# WO# : 92669092 witbin th. a pt dl 'a :.p p priteervatloll f0 l�s:. 6xceptloICVQq,0I 0M.TQC JgltAiXPrOO'e,DRGj8.416�Nlate'r).q�IC;tt;l♦� PM: BV Due Date: 06/05/23 **Bottom half of box-alto Ust:nlumbel of battles CLIENT: 92-AECOM-RAL '�•*Check:aff uripro~i its; � i. fkr ieh103fjne R�{ p _ Z. c n1 Q Z Z ro _ ro SC g: g Yo• p '° za ° q a a� r; u. m a - Z ci. jii u u i a�( ;� �r 5 z b z '' a m a, n; E E E E la re E E. J. o 8 ui. i :l D: E E E: e E 6 E Pt c' g 26 y �: a m a { m ,m Q y p 4 - -- _ \1 f 5 - - i - c — 1 a 'OH`A,djustmient.tog for Preserved Samples Simple ICE Type of Pr..e;ervatNO F --- _ PH Ppoq re�ejpt pate _resarvatlori adlusted Time preservation Aritount:of:PrrasCv�tiVe. Lot# adjusted added' [ypte: Whenever there is a discrepancy�ffkdling oorthCarollnatompAancesarnples,acopyofthtsforriitivill bet nCtoth*&mktiCaroliiiaDENaC.erlificationOFfice{i.e. Dt talFold,Ineorrect'preservatiVe,au.tof temp,Incorrect cogminers, Page 9 of 9 Pace Analytical Services,LLC 9800 Kin aceAnalytical® ey Ave. Suite 100 Huntersville,NC 28078078 www.pacelabs.com (704)875-9092 May 09, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: NOKIA WS Pace Project No.: 92665668 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on May 03, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Ormond Beach If you have any questions concerning this report, please feel free to contact me. Sincerely,Q - aAAa, Bonnie Vang bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM Cristin Dolan,AECOM Jon Wakeman,AECOM Environment fJ pP__ 2" REPORT OF LABORATORY ANALYSIS N This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 15 6 Pace Analytical Services,LLC te 100 laceAnalytical 9800HuIntesvlle,NC128078 wwwww..paclabs.com (704)875-9092 CERTIFICATIONS Project: NOKIA WS Pace Project No.: 92665668 Pace Analytical Services Ormond Beach 8 East Tower Circle,Ormond Beach,FL 32174 Missouri Certification#:236 Alaska DEC-CS/UST/LUST Montana Certification#:Cert 0074 Alabama Certification#:41320 Nebraska Certification:NE-OS-28-14 Colorado Certification:FL NELAC Reciprocity New Hampshire Certification#:2958 Connecticut Certification#:PH-0216 New Jersey Certification#:FL022 Delaware Certification:FL NELAC Reciprocity New York Certification#: 11608 Florida Certification#: E83079 North Carolina Environmental Certificate#:667 Georgia Certification#:955 North Carolina Certification#: 12710 Guam Certification:FL NELAC Reciprocity North Dakota Certification#:R-216 Hawaii Certification:FL NELAC Reciprocity Ohio DEP 87780 Illinois Certification#:200068 Oklahoma Certification#: D9947 Indiana Certification:FL NELAC Reciprocity Pennsylvania Certification#:68-00547 Kansas Certification#:E-10383 Puerto Rico Certification#:FLO1264 Kentucky Certification#:90050 South Carolina Certification:#96042001 Louisiana Certification#: FL NELAC Reciprocity Tennessee Certification#:TN02974 Louisiana Environmental Certificate#:05007 Texas Certification:FL NELAC Reciprocity Maine Certification#: FL01264 US Virgin Islands Certification:FL NELAC Reciprocity Maryland Certification:#346 Virginia Environmental Certification#:460165 Massachusetts Certification#:M-FL1264 West Virginia Certification#:9962C Michigan Certification#:9911 Wisconsin Certification#:399079670 Mississippi Certification:FL NELAC Reciprocity Wyoming(EPA Region 8):FL NELAC Reciprocity REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA WS Pace Project No.: 92665668 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92665668001 EW-5 EPA200.7 AAM1 3 PASI-O 92665668002 EW-6 EPA200.7 AAM1, KPP 3 PASI-O 92665668003 EW-12 EPA200.7 AAM1 3 PASI-O 92665668004 EW-14 EPA200.7 AAM1 3 PASI-O 92665668005 EW-16 EPA200.7 AAM1 3 PASI-O 92665668006 EW-21 EPA200.7 AAM1 3 PASI-O 92665668007 NETWORKA EPA200.7 AAM1, KPP 3 PASI-O PASI-O=Pace Analytical Services-Ormond Beach REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92665668 Sample: EW-5 Lab ID: 92665668001 Collected: 05/02/23 11:35 Received: 05/03/23 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 26.6 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:34 7440-39-3 Manganese ND ug/L 5.0 1 05/06/23 00:43 05/08/23 15:34 7439-96-5 Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:34 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92665668 Sample: EW-6 Lab ID: 92665668002 Collected: 05/02/23 11:40 Received: 05/03/23 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 38.4 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:37 7440-39-3 Manganese 2930 ug/L 50.0 10 05/06/23 00:43 05/09/23 01:48 7439-96-5 Zinc 128 ug/L 20.0 1 05/06/23 00:43 05/08/23 15:37 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92665668 Sample: EW-12 Lab ID: 92665668003 Collected: 05/02/23 11:45 Received: 05/03/23 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 44.4 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:41 7440-39-3 Manganese 8.9 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:41 7439-96-5 Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:41 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92665668 Sample: EW-14 Lab ID: 92665668004 Collected: 05/02/23 11:50 Received: 05/03/23 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 169 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:44 7440-39-3 Manganese 57.9 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:44 7439-96-5 Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:44 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92665668 Sample: EW-16 Lab ID: 92665668005 Collected: 05/02/23 11:30 Received: 05/03/23 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 26.1 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:48 7440-39-3 Manganese 12.8 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:48 7439-96-5 Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:48 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92665668 Sample: EW-21 Lab ID: 92665668006 Collected: 05/02/23 11:25 Received: 05/03/23 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 167 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:51 7440-39-3 Manganese 16.7 ug/L 5.0 1 05/06/23 00:43 05/08/23 15:51 7439-96-5 Zinc ND ug/L 20.0 1 05/06/23 00:43 05/08/23 15:51 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WS Pace Project No.: 92665668 Sample: NETWORK A Lab ID: 92665668007 Collected: 05/02/23 12:00 Received: 05/03/23 16:25 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7 Pace Analytical Services-Ormond Beach Barium 39.7 ug/L 10.0 1 05/06/23 00:43 05/08/23 15:54 7440-39-3 Manganese 2090 ug/L 25.0 5 05/06/23 00:43 05/09/23 01:51 7439-96-5 Zinc 96.6 ug/L 20.0 1 05/06/23 00:43 05/08/23 15:54 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WS Pace Project No.: 92665668 QC Batch: 915271 Analysis Method: EPA 200.7 QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Ormond Beach Associated Lab Samples: 92665668001,92665668002,92665668003,92665668004,92665668005,92665668006,92665668007 METHOD BLANK: 5032684 Matrix: Water Associated Lab Samples: 92665668001,92665668002,92665668003,92665668004,92665668005,92665668006,92665668007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 10.0 05/08/2314:49 Manganese ug/L ND 5.0 05/08/2314:49 Zinc ug/L ND 20.0 05/08/2314:49 LABORATORY CONTROL SAMPLE: 5032685 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 250 279 112 85-115 Manganese ug/L 250 268 107 85-115 Zinc ug/L 1250 1320 106 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5032686 5032687 MS MSD 35795734001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 12.1 250 250 262 236 100 89 70-130 10 Manganese ug/L 36.7 250 250 291 266 102 92 70-130 9 Zinc ug/L 199 1250 1250 1400 1310 96 89 70-130 7 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 5032688 5032689 MS MSD 35796422001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 0.0063J 250 250 277 282 108 110 70-130 2 mg/L Manganese ug/L 0.027 250 250 288 293 104 106 70-130 2 mg/L Zinc ug/L 1.2 1250 1250 2470 2490 99 101 70-130 1 mg/L Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: NOKIA WS Pace Project No.: 92665668 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 12 of 15 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA WS Pace Project No.: 92665668 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92665668001 EW-5 EPA 200.7 915271 EPA 200.7 915285 92665668002 EW-6 EPA 200.7 915271 EPA 200.7 915285 92665668003 EW-12 EPA 200.7 915271 EPA 200.7 915285 92665668004 EW-14 EPA 200.7 915271 EPA 200.7 915285 92665668005 EW-16 EPA 200.7 915271 EPA 200.7 915285 92665668006 EW-21 EPA 200.7 915271 EPA 200.7 915285 92665668007 NETWORK A EPA 200.7 915271 EPA 200.7 915285 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:05/09/2023 09:20 AM without the written consent of Pace Analytical Services,LLC. Page 13 of 15 ID rD ' 5 cl v {- V _ ° ID o � x o P a ° C C C CLn ry c, ._ � � C O •� T S Z n " 3 R. 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C r I.� j{^ { + .A�F+��p rl:ry•y r n ♦� i+ n b'.n a n Sr(n H e o V J Z,u _O•fp O S ry. .-t i ¢ rf'°.a:y;•7A•13 - q O O ��pqp U..^ _�. a .co_.,_ m �1t :'.•: {,' !y +'tihri ,� .hlt 'p. .a r0 rF.`:tl•rt _ 6 n m v, x� '3, l:•.;.; .�� i,,r ) ! 1�,(� �� Nm n y n b � M '` 0.• n• a / i �' -ii A t. it.f t :�• r _F+ Mai j,• ''•o ��$�. .� .,n 3 x W (+-ii -a-I � O. ��. � _ jF,1•+ { c1. rN3 t 1?! 17 ;1.7 M'il.� I.1 � art 3 n o. z z"z . Page 14 of 15 .� ..-.0:•rytvl� 'a'1)23!1J0 uolaejUpPaJ UN90 cugo,ID41JON 24304 luasaq fllMtu� a, 's7aujwuoa JaajlajyJ ftal jo ano'anpen�esa�d'�ya��oaui °! 4�jokioae.sajdtuesapue.gdWoaeupolejylJoNguih e.Awedansrpt:slaw »anaualo4ja�n� 4 4A1 :aloN Pappp passnlPY it lal anlleniasaJd Jo lunoutb 101RAiasaad.aW sajd- [L pa3sn(pp ub(ie7il�eada�'rb adla�al�odn Nd weS,panjasa.ld.�o} &jljuasar,jjWd';&; al'31du,es fit/ Hd Ii Q.t ' s . 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N C- a 3 N C n ri ', C 13 10 H Z uu y. a Z 2 n A' �t a: c y m f0 a�u(ao14a�u,,Este;e�.ilfH_p�n�asa�dun 1�.���45�� �b2i—W003ti—Z6 seJuaq>So`aegwnu =If Q;,sl xo o e £Z/QO/SO :a1 eQ an0 '1N3I�0 9� !� 4 uioaao"� �H11%JW.11a;9 gt!ip A9 :Wd 1 STgB/0�a aseaa�pue I , 1 !n a.bon�suQj��$5ii� i 0 �il tu a 1.#ajdwes uo(3enietsaid 1 ad � ` 0000e30e eyul44W899999Z6 . # PUjraas) llbpeulaol asp /p d►1 xoq 0--jilt 4 d07'4jew qjay0,, Wit'dg.:8z�a:zz�z/e�c t �e�ed��►�l�ej►a ;dieaea:dad uo -- --- n hlpu :ai�w�s-Zan.VeOaLNnN-WNJ-A 3 :01;1.L #:)a ' Page 15 of 15 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 July 06, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: NOKIA WINSTON-SALEM Pace Project No.: 92674970 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on June 28, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville If you have any questions concerning this report, please feel free to contact me. Sincerely,Q _ aAAa, Bonnie Vang bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM Cristin Dolan,AECOM Teresa Amentt Jennings,AECOM Jon Wakeman,AECOM Environment z REPORT OF LABORATORY ANALYSIS N This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 9 6 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 CERTIFICATIONS Project: NOKIA WINSTON-SALEM Pace Project No.: 92674970 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 9 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA WINSTON-SALEM Pace Project No.: 92674970 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92674970001 AS EFFLUENT EPA 200.7 Rev 4.4 1994 D661 3 PASI-A PASI-A=Pace Analytical Services-Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 9 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON-SALEM Pace Project No.: 92674970 Sample: AS EFFLUENT Lab ID: 92674970001 Collected: 06/27/23 10:00 Received: 06/28/23 14:50 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Barium 32.3 ug/L 5.0 1 06/29/2317:29 06/30/2313:41 7440-39-3 Manganese 8.5 ug/L 5.0 1 06/29/2317:29 06/30/2313:41 7439-96-5 Zinc 14.3 ug/L 10.0 1 06/29/2317:29 06/30/2313:41 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 9 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON-SALEM Pace Project No.: 92674970 QC Batch: 783949 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92674970001 METHOD BLANK: 4065875 Matrix: Water Associated Lab Samples: 92674970001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 5.0 06/30/2313:23 Manganese ug/L ND 5.0 06/30/2313:23 Zinc ug/L ND 10.0 06/30/2313:23 LABORATORY CONTROL SAMPLE: 4065876 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 500 510 102 85-115 Manganese ug/L 500 512 102 85-115 Zinc ug/L 500 497 99 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4065877 4065878 MS MSD 92674970001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 32.3 500 500 550 538 104 101 70-130 2 Manganese ug/L 8.5 500 500 529 516 104 102 70-130 2 Zinc ug/L 14.3 500 500 524 510 102 99 70-130 3 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 9 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALIFIERS Project: NOKIA WINSTON-SALEM Pace Project No.: 92674970 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 9 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA WINSTON-SALEM Pace Project No.: 92674970 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92674970001 AS EFFLUENT EPA 200.7 Rev 4.4 1994 783949 EPA 200.7 Rev 4.4 1994 784006 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/06/2023 05:45 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 9 Si 0 CI 0 5 �. �. (_ ✓.t `_ .o a s a o 3 m o v a a 3 m Q• n 0 m' ❑ O < ❑ ❑ 3 3 C u 2 n rD N 3 Dy N D D `a x � 3 0 a r C a m R � s N � ❑ rD 3 3 0 \ 1 o 3 3 o p c w v� a a ? P3 v � z r M � C 1 w c o_ 5. .rCT r. T ......__---. w A ..•N r \ C C C C l x < m Q a O 2 z n r a i A � irs ,r w w ❑ < � � � � Urb ID rn o 3 a � IDa d p ID a -- �' 3 C rp ro o b $ is Z 0 y_ < G fD } m Cjryp O w —. rD 3 L O S N a K q O N n' ,3j C. 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I v 001Jo143 Jot SOle zKhanJasaJdun salligq 10 Jagwnu isill 01.51 xd4 jo410,4 ui014o0#w. lU8-W003U-Z6 :1N3I l3 £Z/I I/LO ajep anQ "ll'�Cfa:•(Ja;em}STbQ6aa'oseaa9:PUe 1!0'�pl'wJQ1IjQ7 b0/1 sud!3d�6iq; A9 :Wd t'aldwe, :uoj;enaasajd.to}'a�ueJ a�u e»e 41.ulN l A 016ti19Z6 • #OM : #:Pa(oad pue paUflan s1 UOIIUUIJ01438p J'o)pue Kd}j xoq;o'Jjeq dolJOUS potty«. :VtJ ;d;aaaM uodn uowpuo3 ajdWUt ZOA £800.6Nn-H-W)l -AN'3 :albI__#�a 1 Page or•'f9 _ Pace Analytical Services,LLC (�IaceAnalyfical@ 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 July 03, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: LUCENT NOKIA Pace Project No.: 92674332 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on June 23, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville • Pace Analytical Services-Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, -4jGlAA , Bonnie Vang V bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM Cristin Dolan,AECOM Teresa Amentt Jennings,AECOM Jon Wakeman,AECOM Environment f.Y�P 2" REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 18 e Pace Analytical Services,LLC te 100 laceAnalytical 9800HuIntesvlle,NC128078 wwwww..paclabs.com (704)875-9092 CERTIFICATIONS Project: LUCENT NOKIA Pace Project No.: 92674332 Pace Analytical Services Charlotte South Carolina Laboratory ID:99006 South Carolina Certification#:99006001 9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003 North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#: E87627 North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84 North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029 South Carolina Laboratory ID:99006 Virginia/VELAP Certification#:460221 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 SAMPLE ANALYTE COUNT Project: LUCENT NOKIA Pace Project No.: 92674332 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92674332001 AS INFLUENT EPA 8260D JJK 63 PASI-C 92674332002 AS EFFLUENT EPA200.7 Rev4.4 1994 D13131 3 PASI-A EPA 8260D JJK 63 PASI-C PASI-A=Pace Analytical Services-Asheville PASI-C=Pace Analytical Services-Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: LUCENT NOKIA Pace Project No.: 92674332 Sample: AS INFLUENT Lab ID: 92674332001 Collected: 06/22/23 15:45 Received: 06/23/23 12:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone ND ug/L 125 5 06/26/23 00:34 67-64-1 Benzene ND ug/L 5.0 5 06/26/23 00:34 71-43-2 Bromobenzene ND ug/L 5.0 5 06/26/23 00:34 108-86-1 Bromochloromethane ND ug/L 5.0 5 06/26/23 00:34 74-97-5 Bromodichloromethane ND ug/L 5.0 5 06/26/23 00:34 75-27-4 Bromoform ND ug/L 5.0 5 06/26/23 00:34 75-25-2 Bromomethane ND ug/L 10.0 5 06/26/23 00:34 74-83-9 2-Butanone(MEK) ND ug/L 25.0 5 06/26/23 00:34 78-93-3 Carbon tetrachloride ND ug/L 5.0 5 06/26/23 00:34 56-23-5 Chlorobenzene ND ug/L 5.0 5 06/26/23 00:34 108-90-7 Chloroethane ND ug/L 5.0 5 06/26/23 00:34 75-00-3 Chloroform ND ug/L 5.0 5 06/26/23 00:34 67-66-3 Chloromethane ND ug/L 5.0 5 06/26/23 00:34 74-87-3 2-Chlorotoluene ND ug/L 5.0 5 06/26/23 00:34 95-49-8 4-Chlorotoluene ND ug/L 5.0 5 06/26/23 00:34 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 10.0 5 06/26/23 00:34 96-12-8 Dibromochloromethane ND ug/L 5.0 5 06/26/23 00:34 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 5.0 5 06/26/23 00:34 106-93-4 Dibromomethane ND ug/L 5.0 5 06/26/23 00:34 74-95-3 1,2-Dichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 95-50-1 1,3-Dichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 541-73-1 1,4-Dichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 106-46-7 Dichlorodifluoromethane ND ug/L 5.0 5 06/26/23 00:34 75-71-8 1,1-Dichloroethane ND ug/L 5.0 5 06/26/23 00:34 75-34-3 1,2-Dichloroethane ND ug/L 5.0 5 06/26/23 00:34 107-06-2 1,1-Dichloroethene ND ug/L 5.0 5 06/26/23 00:34 75-35-4 cis-1,2-Dichloroethene 190 ug/L 5.0 5 06/26/23 00:34 156-59-2 trans-1,2-Dichloroethene ND ug/L 5.0 5 06/26/23 00:34 156-60-5 1,2-Dichloropropane ND ug/L 5.0 5 06/26/23 00:34 78-87-5 1,3-Dichloropropane ND ug/L 5.0 5 06/26/23 00:34 142-28-9 2,2-Dichloropropane ND ug/L 5.0 5 06/26/23 00:34 594-20-7 1,1-Dichloropropene ND ug/L 5.0 5 06/26/23 00:34 563-58-6 cis-1,3-Dichloropropene ND ug/L 5.0 5 06/26/23 00:34 10061-01-5 trans-1,3-Dichloropropene ND ug/L 5.0 5 06/26/23 00:34 10061-02-6 Diisopropyl ether ND ug/L 5.0 5 06/26/23 00:34 108-20-3 Ethylbenzene ND ug/L 5.0 5 06/26/23 00:34 100-41-4 Hexachloro-1,3-butadiene ND ug/L 10.0 5 06/26/23 00:34 87-68-3 2-Hexanone ND ug/L 25.0 5 06/26/23 00:34 591-78-6 p-Isopropyltoluene ND ug/L 5.0 5 06/26/23 00:34 99-87-6 Methylene Chloride ND ug/L 25.0 5 06/26/23 00:34 75-09-2 4-Methyl-2-pentanone(MIBK) ND ug/L 25.0 5 06/26/23 00:34 108-10-1 Methyl-tert-butyl ether ND ug/L 5.0 5 06/26/23 00:34 1634-04-4 Naphthalene ND ug/L 5.0 5 06/26/23 00:34 91-20-3 Styrene ND ug/L 5.0 5 06/26/23 00:34 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 5.0 5 06/26/23 00:34 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 5.0 5 06/26/23 00:34 79-34-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: LUCENT NOKIA Pace Project No.: 92674332 Sample: AS INFLUENT Lab ID: 92674332001 Collected: 06/22/23 15:45 Received: 06/23/23 12:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Tetrachloroethene 891 ug/L 5.0 5 06/26/23 00:34 127-18-4 Toluene ND ug/L 5.0 5 06/26/23 00:34 108-88-3 1,2,3-Trichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 87-61-6 1,2,4-Trichlorobenzene ND ug/L 5.0 5 06/26/23 00:34 120-82-1 1,1,1-Trichloroethane ND ug/L 5.0 5 06/26/23 00:34 71-55-6 1,1,2-Trichloroethane ND ug/L 5.0 5 06/26/23 00:34 79-00-5 Trichloroethene 132 ug/L 5.0 5 06/26/23 00:34 79-01-6 Trichlorofluoromethane ND ug/L 5.0 5 06/26/23 00:34 75-69-4 1,2,3-Trichloropropane ND ug/L 5.0 5 06/26/23 00:34 96-18-4 Vinyl acetate ND ug/L 10.0 5 06/26/23 00:34 108-05-4 Vinyl chloride ND ug/L 5.0 5 06/26/23 00:34 75-01-4 Xylene(Total) ND ug/L 5.0 5 06/26/23 00:34 1330-20-7 m&p-Xylene ND ug/L 10.0 5 06/26/23 00:34 179601-23-1 o-Xylene ND ug/L 5.0 5 06/26/23 00:34 95-47-6 Surrogates 4-Bromofluorobenzene(S) 95 % 70-130 5 06/26/23 00:34 460-00-4 1,2-Dichloroethane-d4(S) 97 % 70-130 5 06/26/23 00:34 17060-07-0 Toluene-d8(S) 98 % 70-130 5 06/26/23 00:34 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: LUCENT NOKIA Pace Project No.: 92674332 Sample: AS EFFLUENT Lab ID: 92674332002 Collected: 06/22/23 15:40 Received: 06/23/23 12:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994 Pace Analytical Services-Asheville Barium 34.7 ug/L 5.0 1 06/27/2311:47 06/28/2319:30 7440-39-3 Manganese 47.5 ug/L 5.0 1 06/27/2311:47 06/28/2319:30 7439-96-5 Zinc 64.4 ug/L 10.0 1 06/27/2311:47 06/28/2319:30 7440-66-6 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte Acetone ND ug/L 25.0 1 06/25/23 23:21 67-64-1 Benzene ND ug/L 1.0 1 06/25/23 23:21 71-43-2 Bromobenzene ND ug/L 1.0 1 06/25/23 23:21 108-86-1 Bromochloromethane ND ug/L 1.0 1 06/25/23 23:21 74-97-5 Bromodichloromethane ND ug/L 1.0 1 06/25/23 23:21 75-27-4 Bromoform ND ug/L 1.0 1 06/25/23 23:21 75-25-2 Bromomethane ND ug/L 2.0 1 06/25/23 23:21 74-83-9 2-Butanone(MEK) ND ug/L 5.0 1 06/25/23 23:21 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 06/25/23 23:21 56-23-5 Chlorobenzene ND ug/L 1.0 1 06/25/23 23:21 108-90-7 Chloroethane ND ug/L 1.0 1 06/25/23 23:21 75-00-3 Chloroform ND ug/L 1.0 1 06/25/23 23:21 67-66-3 Chloromethane ND ug/L 1.0 1 06/25/23 23:21 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 06/25/23 23:21 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 06/25/23 23:21 106-43-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 06/25/23 23:21 96-12-8 Dibromochloromethane ND ug/L 1.0 1 06/25/23 23:21 124-48-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 06/25/23 23:21 106-93-4 Dibromomethane ND ug/L 1.0 1 06/25/23 23:21 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 106-46-7 Dichlorodifluoromethane ND ug/L 1.0 1 06/25/23 23:21 75-71-8 1,1-Dichloroethane ND ug/L 1.0 1 06/25/23 23:21 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 06/25/23 23:21 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 06/25/23 23:21 75-35-4 cis-1,2-Dichloroethene ND ug/L 1.0 1 06/25/23 23:21 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 06/25/23 23:21 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 06/25/23 23:21 78-87-5 1,3-Dichloropropane ND ug/L 1.0 1 06/25/23 23:21 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 06/25/23 23:21 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 06/25/23 23:21 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 06/25/23 23:21 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 06/25/23 23:21 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 06/25/23 23:21 108-20-3 Ethylbenzene ND ug/L 1.0 1 06/25/23 23:21 100-41-4 Hexachloro-1,3-butadiene ND ug/L 2.0 1 06/25/23 23:21 87-68-3 2-Hexanone ND ug/L 5.0 1 06/25/23 23:21 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 06/25/23 23:21 99-87-6 Methylene Chloride ND ug/L 5.0 1 06/25/23 23:21 75-09-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 ANALYTICAL RESULTS Project: LUCENT NOKIA Pace Project No.: 92674332 Sample: AS EFFLUENT Lab ID: 92674332002 Collected: 06/22/23 15:40 Received: 06/23/23 12:40 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services-Charlotte 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 1 06/25/23 23:21 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 06/25/23 23:21 1634-04-4 Naphthalene ND ug/L 1.0 1 06/25/23 23:21 91-20-3 Styrene ND ug/L 1.0 1 06/25/23 23:21 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 06/25/23 23:21 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 06/25/23 23:21 79-34-5 Tetrachloroethene 2.2 ug/L 1.0 1 06/25/23 23:21 127-18-4 Toluene ND ug/L 1.0 1 06/25/23 23:21 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 06/25/23 23:21 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 06/25/23 23:21 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 06/25/23 23:21 79-00-5 Trichloroethene ND ug/L 1.0 1 06/25/23 23:21 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 06/25/23 23:21 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 06/25/23 23:21 96-18-4 Vinyl acetate ND ug/L 2.0 1 06/25/23 23:21 108-05-4 Vinyl chloride ND ug/L 1.0 1 06/25/23 23:21 75-01-4 Xylene(Total) ND ug/L 1.0 1 06/25/23 23:21 1330-20-7 m&p-Xylene ND ug/L 2.0 1 06/25/23 23:21 179601-23-1 o-Xylene ND ug/L 1.0 1 06/25/23 23:21 95-47-6 Surrogates 4-Bromofluorobenzene(S) 97 % 70-130 1 06/25/23 23:21 460-00-4 1,2-Dichloroethane-d4(S) 98 % 70-130 1 06/25/23 23:21 17060-07-0 Toluene-d8(S) 100 % 70-130 1 06/25/23 23:21 2037-26-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: LUCENT NOKIA Pace Project No.: 92674332 QC Batch: 783218 Analysis Method: EPA 200.7 Rev 4.4 1994 QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92674332002 METHOD BLANK: 4062072 Matrix: Water Associated Lab Samples: 92674332002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 5.0 06/28/2318:09 Manganese ug/L ND 5.0 06/28/2318:09 Zinc ug/L ND 10.0 06/28/2318:09 LABORATORY CONTROL SAMPLE: 4062073 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 500 504 101 85-115 Manganese ug/L 500 508 102 85-115 Zinc ug/L 500 486 97 85-115 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4062074 4062075 MS MSD 92673583001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 7.0 500 500 520 525 103 104 70-130 1 Manganese ug/L 264 500 500 780 782 103 104 70-130 0 Zinc ug/L ND 500 500 500 503 100 101 70-130 1 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4062076 4062077 MS MSD 92673706001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 41.1 500 500 566 560 105 104 70-130 1 Manganese ug/L 107 500 500 628 619 104 102 70-130 1 Zinc ug/L ND 500 500 514 505 102 100 70-130 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: LUCENT NOKIA Pace Project No.: 92674332 QC Batch: 782877 Analysis Method: EPA 8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services-Charlotte Associated Lab Samples: 92674332001,92674332002 METHOD BLANK: 4060901 Matrix: Water Associated Lab Samples: 92674332001,92674332002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 1.0 06/25/23 16:05 1,1,1-Trichloroethane ug/L ND 1.0 06/25/23 16:05 1,1,2,2-Tetrachloroethane ug/L ND 1.0 06/25/23 16:05 1,1,2-Trichloroethane ug/L ND 1.0 06/25/23 16:05 1,1-Dichloroethane ug/L ND 1.0 06/25/23 16:05 1,1-Dichloroethene ug/L ND 1.0 06/25/23 16:05 1,1-Dichloropropene ug/L ND 1.0 06/25/23 16:05 1,2,3-Trichlorobenzene ug/L ND 1.0 06/25/23 16:05 1,2,3-Trichloropropane ug/L ND 1.0 06/25/23 16:05 1,2,4-Trichlorobenzene ug/L ND 1.0 06/25/23 16:05 1,2-Dibromo-3-chloropropane ug/L ND 2.0 06/25/23 16:05 1,2-Dibromoethane(EDB) ug/L ND 1.0 06/25/23 16:05 1,2-Dichlorobenzene ug/L ND 1.0 06/25/23 16:05 1,2-Dichloroethane ug/L ND 1.0 06/25/23 16:05 1,2-Dichloropropane ug/L ND 1.0 06/25/23 16:05 1,3-Dichlorobenzene ug/L ND 1.0 06/25/23 16:05 1,3-Dichloropropane ug/L ND 1.0 06/25/23 16:05 1,4-Dichlorobenzene ug/L ND 1.0 06/25/23 16:05 2,2-Dichloropropane ug/L ND 1.0 06/25/23 16:05 2-Butanone(MEK) ug/L ND 5.0 06/25/23 16:05 2-Chlorotoluene ug/L ND 1.0 06/25/23 16:05 2-Hexanone ug/L ND 5.0 06/25/23 16:05 4-Chlorotoluene ug/L ND 1.0 06/25/23 16:05 4-Methyl-2-pentanone(MIBK) ug/L ND 5.0 06/25/23 16:05 Acetone ug/L ND 25.0 06/25/23 16:05 Benzene ug/L ND 1.0 06/25/23 16:05 Bromobenzene ug/L ND 1.0 06/25/23 16:05 Bromochloromethane ug/L ND 1.0 06/25/23 16:05 Bromodichloromethane ug/L ND 1.0 06/25/23 16:05 Bromoform ug/L ND 1.0 06/25/23 16:05 Bromomethane ug/L ND 2.0 06/25/23 16:05 Carbon tetrachloride ug/L ND 1.0 06/25/23 16:05 Chlorobenzene ug/L ND 1.0 06/25/23 16:05 Chloroethane ug/L ND 1.0 06/25/23 16:05 Chloroform ug/L ND 1.0 06/25/23 16:05 Chloromethane ug/L ND 1.0 06/25/23 16:05 cis-1,2-Dichloroethene ug/L ND 1.0 06/25/23 16:05 cis-1,3-Dichloropropene ug/L ND 1.0 06/25/23 16:05 Dibromochloromethane ug/L ND 1.0 06/25/23 16:05 Dibromomethane ug/L ND 1.0 06/25/23 16:05 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: LUCENT NOKIA Pace Project No.: 92674332 METHOD BLANK: 4060901 Matrix: Water Associated Lab Samples: 92674332001,92674332002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Dichlorodifluoromethane ug/L ND 1.0 06/25/23 16:05 Diisopropyl ether ug/L ND 1.0 06/25/23 16:05 Ethylbenzene ug/L ND 1.0 06/25/23 16:05 Hexachloro-1,3-butadiene ug/L ND 2.0 06/25/23 16:05 m&p-Xylene ug/L ND 2.0 06/25/23 16:05 Methyl-tert-butyl ether ug/L ND 1.0 06/25/23 16:05 Methylene Chloride ug/L ND 5.0 06/25/23 16:05 Naphthalene ug/L ND 1.0 06/25/23 16:05 o-Xylene ug/L ND 1.0 06/25/23 16:05 p-Isopropyltoluene ug/L ND 1.0 06/25/23 16:05 Styrene ug/L ND 1.0 06/25/23 16:05 Tetrachloroethene ug/L ND 1.0 06/25/23 16:05 Toluene ug/L ND 1.0 06/25/23 16:05 trans-1,2-Dichloroethene ug/L ND 1.0 06/25/23 16:05 trans-1,3-Dichloropropene ug/L ND 1.0 06/25/23 16:05 Trichloroethene ug/L ND 1.0 06/25/23 16:05 Trichlorofluoromethane ug/L ND 1.0 06/25/23 16:05 Vinyl acetate ug/L ND 2.0 06/25/23 16:05 Vinyl chloride ug/L ND 1.0 06/25/23 16:05 Xylene(Total) ug/L ND 1.0 06/25/23 16:05 1,2-Dichloroethane-d4(S) % 98 70-130 06/25/23 16:05 4-Bromofluorobenzene(S) % 98 70-130 06/25/23 16:05 Toluene-d8(S) % 99 70-130 06/25/23 16:05 LABORATORY CONTROL SAMPLE: 4060902 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L 20 21.2 106 70-130 1,1,1-Trichloroethane ug/L 20 21.6 108 70-130 1,1,2,2-Tetrachloroethane ug/L 20 20.7 104 70-130 1,1,2-Trichloroethane ug/L 20 20.5 103 70-130 1,1-Dichloroethane ug/L 20 20.9 105 70-130 1,1-Dichloroethene ug/L 20 21.6 108 70-130 1,1-Dichloropropene ug/L 20 22.5 113 70-130 1,2,3-Trichlorobenzene ug/L 20 20.3 102 70-130 1,2,3-Trichloropropane ug/L 20 19.4 97 70-130 1,2,4-Trichlorobenzene ug/L 20 20.0 100 70-130 1,2-Dibromo-3-chloropropane ug/L 20 18.9 94 70-131 1,2-Dibromoethane(EDB) ug/L 20 20.7 103 70-130 1,2-Dichlorobenzene ug/L 20 20.0 100 70-130 1,2-Dichloroethane ug/L 20 19.0 95 70-130 1,2-Dichloropropane ug/L 20 21.0 105 70-130 1,3-Dichlorobenzene ug/L 20 20.3 101 70-130 1,3-Dichloropropane ug/L 20 19.7 98 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: LUCENT NOKIA Pace Project No.: 92674332 LABORATORY CONTROL SAMPLE: 4060902 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 20 20.2 101 70-130 2,2-Dichloropropane ug/L 20 21.9 109 68-135 2-Butanone(MEK) ug/L 40 40.6 101 70-134 2-Chlorotoluene ug/L 20 20.6 103 70-130 2-Hexanone ug/L 40 40.2 101 70-131 4-Chlorotoluene ug/L 20 20.3 101 70-130 4-Methyl-2-pentanone(MIBK) ug/L 40 37.6 94 70-130 Acetone ug/L 40 42.6 107 70-133 Benzene ug/L 20 21.5 108 70-130 Bromobenzene ug/L 20 20.4 102 70-130 Bromochloromethane ug/L 20 20.8 104 70-130 Bromodichloromethane ug/L 20 20.1 101 70-130 Bromoform ug/L 20 20.5 102 70-130 Bromomethane ug/L 20 18.6 93 45-151 Carbon tetrachloride ug/L 20 22.3 111 70-130 Chlorobenzene ug/L 20 21.3 106 70-130 Chloroethane ug/L 20 20.9 105 39-152 Chloroform ug/L 20 19.9 100 70-130 Chloromethane ug/L 20 26.0 130 58-130 cis-1,2-Dichloroethene ug/L 20 20.5 102 70-130 cis-1,3-Dichloropropene ug/L 20 20.2 101 70-130 Dibromochloromethane ug/L 20 20.5 102 70-130 Dibromomethane ug/L 20 20.3 101 70-130 Dichlorodifluoromethane ug/L 20 25.5 127 54-133 Diisopropyl ether ug/L 20 18.8 94 70-130 Ethylbenzene ug/L 20 21.1 105 70-130 Hexachloro-1,3-butadiene ug/L 20 22.8 114 70-135 m&p-Xylene ug/L 40 42.5 106 70-130 Methyl-tert-butyl ether ug/L 20 18.3 92 70-130 Methylene Chloride ug/L 20 20.2 101 66-130 Naphthalene ug/L 20 20.1 100 70-130 o-Xylene ug/L 20 21.0 105 70-130 p-Isopropyltoluene ug/L 20 21.4 107 70-130 Styrene ug/L 20 21.3 107 70-130 Tetrachloroethene ug/L 20 21.6 108 70-130 Toluene ug/L 20 20.9 105 70-130 trans-1,2-Dichloroethene ug/L 20 22.0 110 70-130 trans-1,3-Dichloropropene ug/L 20 19.8 99 70-130 Trichloroethene ug/L 20 21.4 107 70-130 Trichlorofluoromethane ug/L 20 21.2 106 62-130 Vinyl acetate ug/L 40 37.8 95 70-144 Vinyl chloride ug/L 20 19.3 96 62-130 Xylene(Total) ug/L 60 63.5 106 70-130 1,2-Dichloroethane-d4(S) % 96 70-130 4-Bromofluorobenzene(S) % 99 70-130 Toluene-d8(S) % 101 70-130 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: LUCENT NOKIA Pace Project No.: 92674332 MATRIX SPIKE SAMPLE: 4060904 92673055009 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND 20 22.7 114 70-141 1,1,1-Trichloroethane ug/L ND 20 23.9 120 70-150 1,1,2,2-Tetrachloroethane ug/L ND 20 21.3 106 69-142 1,1,2-Trichloroethane ug/L ND 20 21.5 108 70-138 1,1-Dichloroethane ug/L ND 20 22.8 114 70-150 1,1-Dichloroethene ug/L ND 20 25.1 126 70-156 1,1-Dichloropropene ug/L ND 20 25.2 126 70-150 1,2,3-Trichlorobenzene ug/L ND 20 19.8 99 70-148 1,2,3-Trichloropropane ug/L ND 20 20.3 101 70-140 1,2,4-Trichlorobenzene ug/L ND 20 19.9 99 70-146 1,2-Dibromo-3-chloropropane ug/L ND 20 19.3 97 68-146 1,2-Dibromoethane(EDB) ug/L ND 20 21.5 108 70-138 1,2-Dichlorobenzene ug/L ND 20 20.8 104 70-141 1,2-Dichloroethane ug/L ND 20 20.6 103 69-143 1,2-Dichloropropane ug/L ND 20 22.0 110 68-156 1,3-Dichlorobenzene ug/L ND 20 21.3 106 70-143 1,3-Dichloropropane ug/L ND 20 20.7 104 70-138 1,4-Dichlorobenzene ug/L ND 20 21.1 105 70-142 2,2-Dichloropropane ug/L ND 20 24.2 121 52-170 2-Butanone(MEK) ug/L ND 40 38.3 96 60-157 2-Chlorotoluene ug/L ND 20 21.8 109 70-147 2-Hexanone ug/L ND 40 39.1 98 68-146 4-Chlorotoluene ug/L ND 20 21.3 106 70-142 4-Methyl-2-pentanone(MIBK) ug/L ND 40 38.6 97 70-141 Acetone ug/L ND 40 38.5 95 58-157 Benzene ug/L ND 20 22.9 115 70-142 Bromobenzene ug/L ND 20 21.2 106 70-143 Bromochloromethane ug/L ND 20 22.9 114 70-146 Bromodichloromethane ug/L ND 20 21.4 107 70-139 Bromoform ug/L ND 20 21.2 106 64-140 Bromomethane ug/L ND 20 20.1 100 28-192 Carbon tetrachloride ug/L ND 20 24.7 123 70-148 Chlorobenzene ug/L ND 20 22.8 114 70-141 Chloroethane ug/L ND 20 23.8 119 58-191 Chloroform ug/L ND 20 21.5 107 70-148 Chloromethane ug/L ND 20 28.6 143 43-162 cis-1,2-Dichloroethene ug/L ND 20 22.3 111 68-151 cis-1,3-Dichloropropene ug/L ND 20 21.0 105 70-139 Dibromochloromethane ug/L ND 20 21.5 107 70-144 Dibromomethane ug/L ND 20 21.4 107 70-139 Dichlorodifluoromethane ug/L ND 20 32.3 162 39-171 Diisopropyl ether ug/L ND 20 20.1 101 67-142 Ethylbenzene ug/L ND 20 22.7 113 70-143 Hexachloro-1,3-butadiene ug/L ND 20 24.4 122 64-163 m&p-Xylene ug/L ND 40 45.7 114 70-144 Methyl-tert-butyl ether ug/L ND 20 19.5 97 65-143 Methylene Chloride ug/L ND 20 21.0 103 62-149 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 12 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: LUCENT NOKIA Pace Project No.: 92674332 MATRIX SPIKE SAMPLE: 4060904 92673055009 Spike MS MS %Rec Parameter Units Result Conc. Result %Rec Limits Qualifiers Naphthalene ug/L ND 20 18.6 93 67-147 o-Xylene ug/L ND 20 22.3 112 70-145 p-Isopropyltoluene ug/L ND 20 22.8 114 70-147 Styrene ug/L ND 20 22.2 111 70-143 Tetrachloroethene ug/L ND 20 23.9 119 70-145 Toluene ug/L ND 20 22.4 112 70-142 trans-1,2-Dichloroethene ug/L ND 20 24.0 120 70-151 trans-1,3-Dichloropropene ug/L ND 20 20.8 104 70-139 Trichloroethene ug/L ND 20 23.4 117 62-146 Trichlorofluoromethane ug/L ND 20 26.1 130 63-153 Vinyl acetate ug/L ND 40 39.1 98 61-162 Vinyl chloride ug/L ND 20 21.7 108 61-163 Xylene(Total) ug/L ND 60 68.1 113 70-143 1,2-Dichloroethane-d4(S) % 97 70-130 4-Bromofluorobenzene(S) % 97 70-130 Toluene-d8(S) % 99 70-130 SAMPLE DUPLICATE: 4060903 92673055008 Dup Parameter Units Result Result RPD Qualifiers 1,1,1,2-Tetrachloroethane ug/L ND ND 1,1,1-Trichloroethane ug/L ND ND 1,1,2,2-Tetrachloroethane ug/L ND ND 1,1,2-Trichloroethane ug/L ND ND 1,1-Dichloroethane ug/L ND ND 1,1-Dichloroethene ug/L ND ND 1,1-Dichloropropene ug/L ND ND 1,2,3-Trichlorobenzene ug/L ND ND 1,2,3-Trichloropropane ug/L ND ND 1,2,4-Trichlorobenzene ug/L ND ND 1,2-Dibromo-3-chloropropane ug/L ND ND 1,2-Dibromoethane(EDB) ug/L ND ND 1,2-Dichlorobenzene ug/L ND ND 1,2-Dichloroethane ug/L ND ND 1,2-Dichloropropane ug/L ND ND 1,3-Dichlorobenzene ug/L ND ND 1,3-Dichloropropane ug/L ND ND 1,4-Dichlorobenzene ug/L ND ND 2,2-Dichloropropane ug/L ND ND 2-Butanone(MEK) ug/L ND ND 2-Chlorotoluene ug/L ND ND 2-Hexanone ug/L ND ND 4-Chlorotoluene ug/L ND ND 4-Methyl-2-pentanone(MIBK) ug/L ND ND Acetone ug/L ND ND Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 13 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA Project: LUCENT NOKIA Pace Project No.: 92674332 SAMPLE DUPLICATE: 4060903 92673055008 Dup Parameter Units Result Result RPD Qualifiers Benzene ug/L ND ND Bromobenzene ug/L ND ND Bromochloromethane ug/L ND ND Bromodichloromethane ug/L ND ND Bromoform ug/L ND ND Bromomethane ug/L ND ND Carbon tetrachloride ug/L ND ND Chlorobenzene ug/L ND ND Chloroethane ug/L ND ND Chloroform ug/L ND ND Chloromethane ug/L ND ND cis-1,2-Dichloroethene ug/L ND ND cis-1,3-Dichloropropene ug/L ND ND Dibromochloromethane ug/L ND ND Dibromomethane ug/L ND ND Dichlorodifluoromethane ug/L ND ND Diisopropyl ether ug/L ND ND Ethylbenzene ug/L ND ND Hexachloro-1,3-butadiene ug/L ND ND m&p-Xylene ug/L ND ND Methyl-tert-butyl ether ug/L ND ND Methylene Chloride ug/L ND ND Naphthalene ug/L ND ND o-Xylene ug/L ND ND p-Isopropyltoluene ug/L ND ND Styrene ug/L ND ND Tetrachloroethene ug/L ND ND Toluene ug/L ND ND trans-1,2-Dichloroethene ug/L ND ND trans-1,3-Dichloropropene ug/L ND ND Trichloroethene ug/L ND ND Trichlorofluoromethane ug/L ND ND Vinyl acetate ug/L ND ND Vinyl chloride ug/L ND ND Xylene(Total) ug/L ND ND 1,2-Dichloroethane-d4(S) % 98 97 4-Bromofluorobenzene(S) % 97 97 Toluene-d8(S) % 100 100 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 14 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALIFIERS Project: LUCENT NOKIA Pace Project No.: 92674332 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 15 of 18 Pace Analytical Services,LLC (�IaceAnalyficalo 9800 Kiney Ave. Suite 100 Huntersville,NC 28078 078 www.pacelabs.com (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: LUCENT NOKIA Pace Project No.: 92674332 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92674332002 AS EFFLUENT EPA 200.7 Rev 4.4 1994 783218 EPA 200.7 Rev 4.4 1994 783273 92674332001 AS INFLUENT EPA 8260D 782877 92674332002 AS EFFLUENT EPA8260D 782877 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:07/03/2023 11:36 AM without the written consent of Pace Analytical Services,LLC. Page 16 of 18 a a 3 A 8 n u 3 0 n v fD 0 5 ro ro CO d a °a n c 3 \ c c cITS C Er v o 3 a O < j D < < ry aCL O a _ a r) ■ n o A yr w a a B a a J ° + ro ' a a d ^ v` Q ., ofb 3: y ro 00 $ ro �. 67 - - 0 � o. n' w g ran .N N � (D t c rD w ro o ? On 3 G ¢ G1 n cIlk.8 � ty m n! �o ��p:. o g� o— 3 Oj o e CI ID Cr 3 •� ro M _ �r 4 a p u O = ID "a v v 3' 3 a O a ° w R ro a o c o ' o o a a. n n �. A g p in (A LA i :'2 c � r1 3 m et rl n io ro 9 Container Type;Plastic(?) or Glass(G) " ;IOL � � �■� � r 1 ro aq nF o Ir ` •w ro 3 rq i D ,a:a.r emr..� ac•�r >SRp- wa• Tr.: -M n Vf/8 f y �:A.rWM N.•"O.y v G H r t N 6U r M H rt N•fi rt'- •p a t. N O --N• N rr p.V••. .I.N W O H A O N O �r fP:- 'Z ��• 5Og O-O O r?•N - d N �b R0. .1� M rf-'L N.V N f1 0 N n C].��to O A O� G W"rG I-f~0 a•0 N ro [�1 fD r�V••�J F' Y G A W l0 G•R N 0. ,C. IE o. O, Ib ',1` _� nnHH w3 m wii •• ` m W.�'HP m C E. ...,� R. of v' w r� t••r d w rr y ��?1 u R n.N.��py y vw ra •rt it •• r- w to u a a N• o wnt6 M t~n �rpp m"�. .C SE •nH H•+ Y. A' a ` ..w 2 JD 7J -7 '1 .H n �, M ¢..a. d:r O n O x r rry ro �' +►1" �o 'n� � c � '°ro 3 .I �17 j� r■•70' 0 9,� 3 'a •y t0 N•(�� O- � H N�N rr O - . �•' .rt N S N ."tl. ten h O. b V. C... . : a 1�{{ 1�pp c �f 'ar' ny 3 N z 2 •IA.•Oa H H rd P..� f0 tt�N Z a; z z x z, z x' P, I4! _cs..:r eu.+zcYa�w+u d11'tCYIYTI•fiiRAi'1tFlJA_'tSr. Y_t GA;•;I'�Y. HrCYYIIGttii.,iiHMi•SSl4R4IR1f71Ml.YI.'+1R'A{L.IftiNNl'..RRYAMif+tlJlAi51]'1:3." '!!NIIW aw �v.K Dh#�Titli�:,E-N-V-FRPM-HUNI.0083 v02 Sample Condition Upon Receipt ' i�kneueinus 9 6.&a -ate 1;1/.14/2022`$18t30 AM k Project t 33 0hp-0 ntarlC.aap.half df, ox Ef pH and/or dechlorinax!on Is verified and t1: h� --� +i�T01hthi.-.a�eptagto,.tiaingofct.dresetvatlonsamples, Due Date: 07/05/23 biCeotlops: p/Ai'toll(girnr 11RC,PPsnd:ii .ala,QRO/8015(water)DOC, LLHg CLIENT: 92-PECOM-RAL "[ pttot aiklfof box into 11' notabar.aif bottlit J "-�Che6lf:;��tfn�reservei"�:�Nitiate�'fo�ctifp�'l.�i'e. Z v y U L. c•. e c a. 2 �, q c �.. O n z f� z �. c x�. j c US x s c. j id Z. � t. 4 t! V 7 y }iJ, fy. 3 �. 3 F �i �7. 'r' C M a a V. �: 0. FI a G' EF E E, ''' ' fQ. E :E 1. �: 1 �.1 �. J E J rA £ uu}} yy►► `Q�� LA �. ky u�j tt M 4. r!. at. V t9 i7 t7 0{.. i ch ,(e; Qi -$ "m m: .A 2 — — — - t. •3 F.. t 4 Ki 3 i 7 10 1 12 pH Adjustment Log.,forpreservedi Sampits Sainple;ID. ]ypa-Mpt40mrvative pH upon receipt Date preservation dd)ust+ed Ifinw,preseivaticn Amount..tif Preservative Ibt q adjusted added, NOW.Whenevertherelsadiscrepancy,affecting North CarolinacompliaAcesamples;acopy.ofthis dr-MWlll besentt6the North Carolina DENR:CerilAcation Office(i.e. Out of 1;04t;Incorrect preservative,out of tonp,Incorrect enntalners. Page 18 of 18 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 August 09, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on July 28, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Asheville If you have any questions concerning this report, please feel free to contact me. Sincerely,Q - aAAa, Bonnie Vang bonnie.vang@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM Cristin Dolan,AECOM Teresa Amentt Jennings,AECOM Jon Wakeman,AECOM Environment z REPORT OF LABORATORY ANALYSIS N This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 23 6 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 CERTIFICATIONS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Pace Analytical Services Asheville 2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030 Florida/NELAP Certification#: E87648 South Carolina Certification#:99030001 North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222 North Carolina Wastewater Certification#:40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92679831001 DT-1 EPA 6020E KRL 3 PASI-A 92679831002 EW-4 EPA 6020E KRL 3 PASI-A 92679831003 EW-5 EPA 6020E KRL 3 PASI-A 92679831004 EW-6 EPA 6020E KRL 3 PASI-A 92679831005 EW-12 EPA 6020E KRL 3 PASI-A 92679831006 EW-14 EPA 6020E KRL 3 PASI-A 92679831007 EW-16 EPA 6020E KRL 3 PASI-A 92679831008 EW-17 EPA 6020E KRL 3 PASI-A 92679831009 EW-19 EPA 6020E KRL 3 PASI-A 92679831010 EW-21 EPA 6020E KRL 3 PASI-A 92679831011 EW-22 EPA 6020E KRL 3 PASI-A 92679831012 AS EFFLUENT EPA6020B KRL 3 PASI-A PASI-A=Pace Analytical Services-Asheville REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: DT-1 Lab ID: 92679831001 Collected: 07/26/23 14:00 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 47.3 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:12 7440-39-3 Manganese 30.1 ug/L 2.0 1 08/03/23 16:17 08/08/23 03:12 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:12 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-4 Lab ID: 92679831002 Collected: 07/26/23 13:20 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 10.5 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:27 7440-39-3 Manganese 2.5 ug/L 2.0 1 08/03/23 16:17 08/08/23 03:27 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:27 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-5 Lab ID: 92679831003 Collected: 07/26/23 13:25 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 18.7 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:32 7440-39-3 Manganese ND ug/L 2.0 1 08/03/23 16:17 08/08/23 03:32 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:32 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-6 Lab ID: 92679831004 Collected: 07/26/23 13:30 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 29.3 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:37 7440-39-3 Manganese 1060 ug/L 20.0 10 08/03/23 16:17 08/09/23 02:38 7439-96-5 Zinc 37.6 ug/L 10.0 1 08/03/23 16:17 08/08/23 03:37 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-12 Lab ID: 92679831005 Collected: 07/26/23 13:10 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 35.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:42 7440-39-3 Manganese ND ug/L 2.0 1 08/03/23 16:17 08/08/23 03:42 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:42 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-14 Lab ID: 92679831006 Collected: 07/26/23 13:15 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 94.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:47 7440-39-3 Manganese 22.4 ug/L 2.0 1 08/03/23 16:17 08/08/23 03:47 7439-96-5 Zinc 214 ug/L 20.0 2 08/03/23 16:17 08/09/23 02:43 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-16 Lab ID: 92679831007 Collected: 07/26/23 13:35 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 17.3 ug/L 1.0 1 08/03/23 16:17 08/08/23 03:52 7440-39-3 Manganese 345 ug/L 6.0 3 08/03/23 16:17 08/09/23 02:48 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 03:52 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-17 Lab ID: 92679831008 Collected: 07/26/23 13:40 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 14.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 04:47 7440-39-3 Manganese 20.6 ug/L 2.0 1 08/03/23 16:17 08/08/23 04:47 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 04:47 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 11 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-19 Lab ID: 92679831009 Collected: 07/26/23 13:45 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 45.6 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:12 7440-39-3 Manganese 10.2 ug/L 2.0 1 08/03/23 16:17 08/08/23 05:12 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 05:12 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 12 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-21 Lab ID: 92679831010 Collected: 07/26/23 13:55 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 138 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:17 7440-39-3 Manganese 10.7 ug/L 2.0 1 08/03/23 16:17 08/08/23 05:17 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 05:17 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 13 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: EW-22 Lab ID: 92679831011 Collected: 07/26/23 13:50 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 13.1 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:22 7440-39-3 Manganese ND ug/L 2.0 1 08/03/23 16:17 08/08/23 05:22 7439-96-5 Zinc ND ug/L 10.0 1 08/03/23 16:17 08/08/23 05:22 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 14 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Sample: AS EFFLUENT Lab ID: 92679831012 Collected: 07/26/23 16:30 Received: 07/28/23 16:00 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020 MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3010A Pace Analytical Services-Asheville Barium 27.6 ug/L 1.0 1 08/03/23 16:17 08/08/23 05:37 7440-39-3 Manganese 425 ug/L 6.0 3 08/03/23 16:17 08/09/23 03:28 7439-96-5 Zinc 20.5 ug/L 10.0 1 08/03/23 16:17 08/08/23 05:37 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 15 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 QC Batch: 791234 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92679831001,92679831002,92679831003,92679831004,92679831005,92679831006,92679831007 METHOD BLANK: 4100550 Matrix: Water Associated Lab Samples: 92679831001,92679831002,92679831003,92679831004,92679831005,92679831006,92679831007 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 1.0 08/08/23 01:42 Manganese ug/L ND 2.0 08/08/23 01:42 Zinc ug/L ND 10.0 08/08/23 01:42 LABORATORY CONTROL SAMPLE: 4100551 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 50 50.7 101 80-120 Manganese ug/L 50 51.2 102 80-120 Zinc ug/L 50 52.0 104 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4100552 4100553 MS MSD 92679152001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 566 50 50 606 610 79 88 75-125 1 Manganese ug/L 9830 50 50 9800 9530 -56 -593 75-125 3 M1 Zinc ug/L 33.7 50 50 83.5 82.6 100 98 75-125 1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 16 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 QC Batch: 791237 Analysis Method: EPA 6020B QC Batch Method: EPA 3010A Analysis Description: 6020 MET Laboratory: Pace Analytical Services-Asheville Associated Lab Samples: 92679831008,92679831009,92679831010,92679831011,92679831012 METHOD BLANK: 4100561 Matrix: Water Associated Lab Samples: 92679831008,92679831009,92679831010,92679831011,92679831012 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 1.0 08/08/23 04:37 Manganese ug/L ND 2.0 08/08/23 04:37 Zinc ug/L ND 10.0 08/08/23 04:37 LABORATORY CONTROL SAMPLE: 4100562 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 50 47.4 95 80-120 Manganese ug/L 50 51.4 103 80-120 Zinc ug/L 50 52.1 104 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4100563 4100564 MS MSD 92679831008 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 14.1 50 50 61.0 60.9 94 94 75-125 0 Manganese ug/L 20.6 50 50 71.9 70.7 103 100 75-125 2 Zinc ug/L ND 50 50 53.6 53.9 101 102 75-125 1 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 17 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALIFIERS Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 18 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA WINSTON SALEM Pace Project No.: 92679831 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92679831001 DT-1 EPA 3010A 791234 EPA 6020B 791317 92679831002 EW-4 EPA 3010A 791234 EPA 6020B 791317 92679831003 EW-5 EPA 3010A 791234 EPA 6020B 791317 92679831004 EW-6 EPA 3010A 791234 EPA 6020B 791317 92679831005 EW-12 EPA 3010A 791234 EPA 6020B 791317 92679831006 EW-14 EPA 3010A 791234 EPA 6020B 791317 92679831007 EW-16 EPA 3010A 791234 EPA 6020B 791317 92679831008 EW-17 EPA 3010A 791237 EPA 6020B 791320 92679831009 EW-19 EPA 3010A 791237 EPA 6020B 791320 92679831010 EW-21 EPA 3010A 791237 EPA 6020B 791320 92679831011 EW-22 EPA 3010A 791237 EPA 6020B 791320 92679831012 AS EFFLUENT EPA 3010A 791237 EPA 6020B 791320 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:08/09/2023 03:28 PM without the written consent of Pace Analytical Services,LLC. Page 19 of 23 DC#_Title: ENV-FRM-HUN1.0083 02- sample Condition Upon Receipt ace. ae1�i4�HAYGti Effective Date: 11/14/2022 8:18:30 AM Laboratory receiving samples: Asheville m Eden❑ Greenwood❑ Huntersville❑ Raleigh[] Mechanicsville❑ Atlanta[] Kernersville❑ Sample Condition Client Name:Upon Receipt Project K WO# : 92679831 Iq t6 �Dllei 2A Courier: LJ Fed Ex L.JLJPs TQuS PYCflent II I II' I II II III II II I III ❑ Commercial 20 Pace ❑Other: 92679831 Custody Seal Present? ❑Yes XNo Seals Intact? ❑Yes Ili No Date/Initials Person Examining Contents�� Packing Material; ❑Bubble Wrap ❑Bubble Bags X None ❑ Other Biological Tissue Frozen? Thermometer: ❑Yes ❑No I N/A 14IR Gun ID: 73Tq Type of Ice: RjWet 061up ❑None —��' 6 Correction Factor: Cooler Temp: Add/Subtract(°CJ Q Temp should be ahove freezing to 6'C ❑5amples out of temp criteria.Samples on Ite,cooling process Cooler Temp Corrected (°C): has begun USDA Regulated Soll(4 N/A,water sample) Did samples originate In a quarantine z❑ne within the United Slates:CA,NY,or SC Did samplesoriginate from a foreign source(internationally, (check maps)?El Yes X No including Hawaii and Puerto Rlco)?❑Yes 1�1No Comments/Discrepancy: Chain of Custody Present? jTQYes El No ]N/A t. Samples Arrived withinHold7lme? DYes ❑No El N/A 2. Short Hold Time Analysis(c72'li ❑Yes $)No El N/A 3_ Rush Turn Around Time Requested? DYes 1ZNo DN/A 4. Sufficient Volume? Z Yes ❑No ❑N/A 5. Correct Containers Used? PgYes ❑No ❑N/A 6, -Pace Containers Used? IRYcs ❑No ❑NIA Containers Intact? Yes ❑No ❑N/A 7, Dissolved analysis:Samples Field Filtered? ❑Yes. ❑No I3(1N/A a. Sample Labels Match COC7 ry—IQYes [I No El N/A 9. -includes Uate/Time/ID/Anal sis Matrix:___JI Headspace In VOA Vials(>5-6mm)? ❑Yes ❑No N/A 10, Trip Blank Present? ❑Yes ❑No N/A 11, Trip Blank Custody Seals Present? DYes ❑No WA COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: ni,itraY trl•RQR1A porn 1 of 7 Page 20 of 23 DC#_Title: ENV-FRM-HUN1.0083 02 Sample Condition Upon Receipt cetrlgtf,ry�t Effective Date:11/14/20,22 8t18t30 AM WQ# : 92679831 PM: BV Due Date: 08/09/23 *Check mark top half of box if pH and/or dechlorination is verified and Project tJ CLIENT: 92—AECOM—RAL within the acceptance range for preservation samples. Exceptions:VOIA,Cbliform,TOC,011 and Grease,DRO/8015(water)DOC,.LLHg **Bottom half of box Is to list number of bottles ***Check all unpreserved Nitrates for chlorine S U _ n. Z Q e Q Q ch h z Z 2 N N Z O. a b3 a ° "' n D v a 3 z z 9 ¢ Y ¢ . �>' a a a n o R L a Q u a a 9 = N a YI u v u iy u ,., 7 T � 7 Z V N o, Q. a a > n ^ fi' A d .2 .0 or _°' u — n`7 EE EE { v a dr a a a a a d d ¢ O p O d E E E Q. E E .E J J J 7 J J a U1 V1 VI J E C E Ea a�; r E n o g o m ~ ~ o o E E E E E E � E E E o E E N v1 = Vl N ry y ul '—J in O O: p O O O N O O O d p E N u z n~ chi 7C 3 h e = Fv ' " rrq j 3 3 a r s rl. N_ m m rn 0) r, 0 0 of m m m ao m co m m Q Q q Q Q q O 7 > O Y ? 0 Ln to Q >I N .q 1 2 - Ni'/\N 3 N N , \\ \ I X/\\ I N X\\ 6 Xl\,\ \X, \N \ -\\ I \K\N N \P '/\N 8 9 1D \ X\N 11 1 12 1 pH Adjustment Log for Preserved Samples Sample ID Type of Pre servalIw pit upon receipt Date preservatlon adjusted Tlrne preservation Amount of Preservative Lot p adjusted added Note: Whenever there Is a d1screpancy affect!nk,North Carolina compliance sample5,a copy of this form be sent to the North Carolina DENR'IertificationOfficL (i.e. Out of hold, Incorrect preservative,out of temp,incorrect containers. rliraltrav In. AQR14 Donn 9 of J Page 21 of 23 n 0 0 m •c n x n en — - � � � 3 o g a ° x n A v 3 d cu IIN tO O O 3 0 2 1 C y 3 vl d a. r'�o ♦♦ \' Q �. 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N (YrN) v A Page 23 of 23 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 September 19, 2023 Conan Fitzgerald AECOM 5438 Wade Park Boulevard Suite 200 Raleigh, NC 27607 RE: Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Dear Conan Fitzgerald: Enclosed are the analytical results for sample(s)received by the laboratory on August 30, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services-Minneapolis If you have any questions concerning this report, please feel free to contact me. Sincerely, ,&—r-;,- Adam Phillips adam.phillips@pacelabs.com (704)875-9092 Project Manager Enclosures cc: Shelley Acheson,AECOM Cristin Dolan,AECOM Teresa Amentt Jennings,AECOM Jon Wakeman,AECOM Environment z REPORT OF LABORATORY ANALYSIS N This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 1 of 24 6 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 CERTIFICATIONS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Pace Analytical Services,LLC-Minneapolis MN 1700 Elm Street SE, Minneapolis, MN 55414 Mississippi Certification#: MN00064 A21-A Certification#:2926.01 Missouri Certification#: 10100 Alabama Certification#:40770 Montana Certification#:CERT0092 Alaska Contaminated Sites Certification#: 17-009 Nebraska Certification#: NE-OS-18-06 Alaska DW Certification#: MN00064 Nevada Certification#: MN00064 Arizona Certification#:AZ0014 New Hampshire Certification#:2081 Arkansas DW Certification#: MN00064 New Jersey Certification#: MN002 Arkansas WW Certification#:88-0680 New York Certification#: 11647 California Certification#:2929 North Carolina DW Certification#:27700 Colorado Certification#:MN00064 North Carolina WW Certification#:530 Connecticut Certification#: PH-0256 North Dakota Certification(A2LA)#:R-036 EPA Region 8 Tribal Water Systems+Wyoming DW North Dakota Certification(MN)#: R-036 Certification#:via MN 027-053-137 Ohio DW Certification#:41244 Florida Certification#: E87605 Ohio VAP Certification(1700)#:CL101 Georgia Certification#:959 Oklahoma Certification#:9507 GMP+Certification#:GMP050884 Oregon Primary Certification#:MN300001 Hawaii Certification#: MN00064 Oregon Secondary Certification#: MN200001 Idaho Certification#:MN00064 Pennsylvania Certification#:68-00563 Illinois Certification#:200011 Puerto Rico Certification#: MN00064 Indiana Certification#:C-MN-01 South Carolina Certification#:74003001 Iowa Certification#:368 Tennessee Certification#:TN02818 Kansas Certification#:E-10167 Texas Certification#:T104704192 Kentucky DW Certification#:90062 Utah Certification#:MN00064 Kentucky WW Certification#:90062 Vermont Certification#:VT-027053137 Louisiana DEQ Certification#:AI-03086 Virginia Certification#:460163 Louisiana DW Certification#:MN00064 Washington Certification#:C486 Maine Certification#: MN00064 West Virginia DEP Certification#:382 Maryland Certification#:322 West Virginia DW Certification M 9952 C Michigan Certification#:9909 Wisconsin Certification#:999407970 Minnesota Certification#:027-053-137 Wyoming UST Certification#:via A21-A 2926.01 Minnesota Dept of Ag Approval:via MN 027-053-137 USDA Permit#: P330-19-00208 Minnesota Petrofund Registration#: 1240 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 2 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 SAMPLE ANALYTE COUNT Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 92685386001 DT-1 EPA 6020E NN2 3 PASI-M 92685386002 EW-4 EPA 6020E NN2 3 PASI-M 92685386003 EW-5 EPA 6020E NN2 3 PASI-M 92685386004 EW-6 EPA 6020E NN2 3 PASI-M 92685386005 EW-12 EPA 6020E NN2 3 PASI-M 92685386006 EW-14 EPA 6020E NN2 3 PASI-M 92685386007 EW-16 EPA 6020E NN2 3 PASI-M 92685386008 EW-17 EPA 6020E NN2 3 PASI-M 92685386009 EW-18 EPA 6020E NN2 3 PASI-M 92685386010 EW-19 EPA 6020E NN2 3 PASI-M 92685386011 EW-21 EPA 6020E NN2 3 PASI-M 92685386012 EW-22 EPA 6020E NN2 3 PASI-M 92685386013 AS EFF EPA 6020E NN2 3 PASI-M PASI-M=Pace Analytical Services-Minneapolis REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, without the written consent of Pace Analytical Services,LLC. Page 3 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: DT-1 Lab ID: 92685386001 Collected: 08/29/23 10:40 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 49.4 ug/L 0.30 1 09/18/23 05:30 09/18/23 17:51 7440-39-3 Manganese 27.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 17:51 7439-96-5 Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 17:51 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 4 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-4 Lab ID: 92685386002 Collected: 08/29/23 11:15 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 8.8 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:25 7440-39-3 Manganese ND ug/L 0.50 1 09/18/23 05:30 09/18/23 18:25 7439-96-5 Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 18:25 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 5 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-5 Lab ID: 92685386003 Collected: 08/29/23 11:20 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 19.6 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:32 7440-39-3 Manganese 1.7 ug/L 0.50 1 09/18/23 05:30 09/18/23 18:32 7439-96-5 Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 18:32 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 6 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-6 Lab ID: 92685386004 Collected: 08/29/23 11:25 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 48.7 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:39 7440-39-3 Manganese 3210 ug/L 10.0 20 09/18/23 05:30 09/18/23 18:42 7439-96-5 Zinc 197 ug/L 5.0 1 09/18/23 05:30 09/18/23 18:39 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 7 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-12 Lab ID: 92685386005 Collected: 08/29/23 11:40 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 125 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:45 7440-39-3 Manganese 736 ug/L 10.0 20 09/18/23 05:30 09/18/23 18:49 7439-96-5 Zinc 32.7 ug/L 5.0 1 09/18/23 05:30 09/18/23 18:45 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 8 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-14 Lab ID: 92685386006 Collected: 08/29/23 11:30 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 112 ug/L 0.30 1 09/18/23 05:30 09/18/23 18:52 7440-39-3 Manganese 22.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 18:52 7439-96-5 Zinc 24.8 ug/L 5.0 1 09/18/23 05:30 09/18/23 18:52 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 9 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-16 Lab ID: 92685386007 Collected: 08/29/23 11:10 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 24.0 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:06 7440-39-3 Manganese 11.8 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:06 7439-96-5 Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:06 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 10 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-17 Lab ID: 92685386008 Collected: 08/29/23 11:05 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 16.6 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:13 7440-39-3 Manganese 57.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:13 7439-96-5 Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:13 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 11 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-18 Lab ID: 92685386009 Collected: 08/29/23 10:45 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 74.1 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:20 7440-39-3 Manganese 113 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:20 7439-96-5 Zinc 6.3 ug/L 5.0 1 09/18/23 05:30 09/18/23 19:20 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 12 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-19 Lab ID: 92685386010 Collected: 08/29/23 10:55 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 46.9 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:27 7440-39-3 Manganese 6.7 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:27 7439-96-5 Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:27 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 13 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-21 Lab ID: 92685386011 Collected: 08/29/23 11:00 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 151 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:34 7440-39-3 Manganese 39.0 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:34 7439-96-5 Zinc 5.4 ug/L 5.0 1 09/18/23 05:30 09/18/23 19:34 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 14 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: EW-22 Lab ID: 92685386012 Collected: 08/29/23 10:50 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 13.8 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:47 7440-39-3 Manganese 0.89 ug/L 0.50 1 09/18/23 05:30 09/18/23 19:47 7439-96-5 Zinc ND ug/L 5.0 1 09/18/23 05:30 09/18/23 19:47 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 15 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Sample: AS EFF Lab ID: 92685386013 Collected: 08/29/23 11:45 Received: 08/30/23 09:31 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6020B MET ICPMS Analytical Method: EPA 6020E Preparation Method: EPA 3020A Pace Analytical Services-Minneapolis Barium 34.5 ug/L 0.30 1 09/18/23 05:30 09/18/23 19:54 7440-39-3 Manganese 841 ug/L 10.0 20 09/18/23 05:30 09/18/23 19:58 7439-96-5 Zinc 68.7 ug/L 5.0 1 09/18/23 05:30 09/18/23 19:54 7440-66-6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 16 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 QC Batch: 906302 Analysis Method: EPA 6020B QC Batch Method: EPA 3020A Analysis Description: 6020E Water UPD5 Laboratory: Pace Analytical Services-Minneapolis Associated Lab Samples: 92685386001,92685386002,92685386003,92685386004,92685386005,92685386006,92685386007, 92685386008,92685386009,92685386010,92685386011,92685386012,92685386013 METHOD BLANK: 4772899 Matrix: Water Associated Lab Samples: 92685386001,92685386002,92685386003,92685386004,92685386005,92685386006,92685386007, 92685386008,92685386009,92685386010,92685386011,92685386012,92685386013 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Barium ug/L ND 0.30 09/18/2317:44 Manganese ug/L ND 0.50 09/18/2317:44 Zinc ug/L ND 5.0 09/18/2317:44 LABORATORY CONTROL SAMPLE: 4772900 Spike LCS LCS %Rec Parameter Units Conc. Result %Rec Limits Qualifiers Barium ug/L 100 106 106 80-120 Manganese ug/L 100 105 105 80-120 Zinc ug/L 100 108 108 80-120 MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 4772901 4772902 MS MSD 92685386001 Spike Spike MS MSD MS MSD %Rec Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual Barium ug/L 49.4 100 100 152 158 103 108 75-125 3 Manganese ug/L 27.0 100 100 128 130 101 102 75-125 1 Zinc ug/L ND 100 100 106 108 104 106 75-125 2 Results presented on this page are in the units indicated by the"Units"column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 17 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALIFIERS Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 DEFINITIONS DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot. ND-Not Detected at or above adjusted reporting limit. TNTC-Too Numerous To Count J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL-Adjusted Method Detection Limit. PQL-Practical Quantitation Limit. RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S-Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is a combined concentration. Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values. LCS(D)-Laboratory Control Sample(Duplicate) MS(D)-Matrix Spike(Duplicate) DUP-Sample Duplicate RPD-Relative Percent Difference NC-Not Calculable. SG-Silica Gel-Clean-Up U-Indicates the compound was analyzed for,but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as "Total"may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 18 of 24 Pace Analytical Services,LLC Face 9800 Kincey Ave. Suite 100 (-� Huntersville,NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: NOKIA WINSTON SALEM Pace Project No.: 92685386 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92685386001 DT-1 EPA 3020A 906302 EPA 6020B 906507 92685386002 EW-4 EPA 3020A 906302 EPA 6020B 906507 92685386003 EW-5 EPA 3020A 906302 EPA 6020B 906507 92685386004 EW-6 EPA 3020A 906302 EPA 6020B 906507 92685386005 EW-12 EPA 3020A 906302 EPA 6020B 906507 92685386006 EW-14 EPA 3020A 906302 EPA 6020B 906507 92685386007 EW-16 EPA 3020A 906302 EPA 6020B 906507 92685386008 EW-17 EPA 3020A 906302 EPA 6020B 906507 92685386009 EW-18 EPA 3020A 906302 EPA 6020B 906507 92685386010 EW-19 EPA 3020A 906302 EPA 6020B 906507 92685386011 EW-21 EPA 3020A 906302 EPA 6020B 906507 92685386012 EW-22 EPA 3020A 906302 EPA 6020B 906507 92685386013 AS EFF EPA 3020A 906302 EPA 6020B 906507 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced,except in full, Date:09/19/2023 11:51 AM without the written consent of Pace Analytical Services,LLC. Page 19 of 24 DC#_Title: ENV-FRM-HUN1.0083 02 Sample Condition Upon Receipt ace, aMr:nuura�xrs Effective Date: 11/W2022 8:18:30 AM Laboratory receiving samples: Asheville Eden❑ Greenwood❑ Htlntersvllle❑ Ralelgh❑ Mechanicsville❑ Atlanta[] Kernersville❑ Sample Condition I Client Name: f Project#: WO# : 92685386 Courier: UFed Ex LJ UPS USPS UClient 11111111 IIII�IIIIII III ❑ Commercial mace ❑Other: 92685386 Custody Seal Present? El Yes WNo Seals intact? ❑Yes Ida Data/InitialsPerson Examin)ng. r,6ntent Packing Material: ElBubble Wrap ❑ cc Bubble Bags �1 None ❑ Other Biological Tissu Frozen? Thermometer: ❑Yes ❑No [RN/A ❑ IR*6urr1D: Type of Ice: Wet Blue Nane Correction Factor: Cooler Temp: �— Add/Subtract (-C) Temp should be above freezing to 6'C ❑Samplesoutof temp criteria.Samples on Ice,couling process Cooler Temp Corrected f°C : h,c begun USDA Regulated Soil(2316NIA,water sample) Did samples originate in a quarantine zone Within the United States:CA, NY,or SC Did samples originate from a foreign source(Internationally, (check maps)?❑Yes ONO intluding Hawaii and Puerto Rico)?Oyes ❑No Comments/Discrepancy- Chain of Custody Present? 4Kes ❑No DN/A 1. Samples Arrtved within Hold Time? R�ns ❑No ❑N/A Z. Short Hold Time Analysis(c72 hr.)? ❑Yes &No ❑N/A 3. Rush Turn Around Time Requested? Dyes IJKo ❑N/A A. Sufficient Volume? ayes ❑No ❑N/A S. Correct Containers Used? —kYes ❑No ❑N/A 6. -Pace Containers Used? Ycs ❑No ❑N/A Cantainers Intact? R" Yes ❑No ❑WA 7. Dissolved analysis:Samples field Filtered? El Yes ❑No &wA 8. Sample Labels Match COC? 'jNkes ❑No DVA 9. -Includes DateMme/ID/Anal si.s Marrlx: Heads ace in VOA Vials(>S-6mm)? ❑Yes ❑No N/A 10. Trlp Blank Present? ❑Yes ❑No /A 11. Trip Blank Custody Seals Present? ❑Yes ❑No ®_N/A COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑ND Lot ID of split containers: CLIENT NOTIFICATION/RESOLUTION Person contacted: Date/Time: Project Manager SCURF Review: Date: Project Manager SRF Review: Date: Page 20 of 24 DC# Title: ENV-FRM-HUN1-0083 02-Sample Conditlon Upon Receipt r.�t.vtusu44Ys Effective Date: 11/14/2022 8:18:30 AM *Check mark top half of box If pH and/or dechlorination Is verified and Project# WO# : 92685386 within the acceptance range for preservation samples. PM: ABP Due Date: 09/11/23 Exceptions:VOA,Conform,TOC,Oil and Grease, DRO/8015(water)DOC,Mig CLIENT: 92—AECOM—RAL **Bottom half of box Is to list number of Bottles ***'Checkall unpreserved Nitrates for chlorine L v Iu Z Z 9Z Z N N Z N a Z z _ N Q � z N m m 2 Q iv } it a n 2 v = a ` Q Q Y d = N —a Cu——uC_ dr� z— z-— O V —� rn —>T u Tu a n — O m O z ct 0CCL Z � C Q 2 p Z D u � — Y a` e� n a = z ev ro f„ J � S .a E a 0.J 0 Q. m E dJ Vu1 ,-1 N .-, eN-I N N .N-1 �--! '-1 N ,..I N O O O O. O M N N in O O O O a 3 J x N rb 3 3 (hn a = > x 1.' a~c > > aa nm qN '0.0.1 a ' `qqr 0. t�7 U�' MU' i9 C7 t�J U0' l9 0 (a a a nN a cm7 i t7 r m m Cfl m m m tD [0 Q Q Q Q Q O O > > O x > 1A kn m Q > LS 1 N\N 2 l 3 4 5 6 \1 7 8 9 IN \1 N 10 11 IN \, v�\ N N\N N\1 1Z pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot d adjusted added Note: Whenever there 15 a d1 screpancy affecting North Carolina compGancesampl es,a copy of this form will besent to the North Carolina DFNR Certification Office(I,e. Out of hold,incorrect preservative,out of temp,incorrect containers, Page 21 of 24 DC#_Title: ENV-FRM-HUN1-0083 02_Sampie Condition Upon Receipt ace' rF,.uws,nr: Effective Dater 11/14/2022 8118.30 AM *Check mark top half of box if pH and/or dechlorination Is verified and Project# within the acceptance range for preservation samples. . Exceptions:VOA, Coliform,TOC,Oil and Grease, DR0/8DI5{water)DOC, LLHg ;"Bottom half of box Is to list number of bottles- ***Check all unpreserved Nitrates for chlorine a a a c Ci � v Q• 4 — - � a e; a Z Z ? v N Z 8 v v W n j X a q a O _rof- q Q q $_ _a__m_ °- Z N Q - c c c a 2 b C7 a v ry Z rOrV a a T c p a u �i- 2 Z = Z n�i a 4 j ,may .-1. d ? � j 2 Y T ro ro o rEE� aEE ly E �FF ¢ q Q Q Y C E °� nJ a. a E d d J d O. �j � in o o o ° :t = o �.°'.. E E E E E E ?d E E E o E E �. OO{} o O P P O E N rl m H O1 01 O� 01 U" ' w 0. a 0. ~ a 6 6 0. l7 r9 ,7 (7 y tL l7 Ih l9 m m m I'd m m m m 3 ¢ Q ¢ ¢ a on > > o Y >` f„ v, m a a o 1 2 3 L\\N N N\N N N 6 7 8 9 10 it 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation Amount of Preservative Lot q adjusted added Note: Whenevertherais,a discrepancy affecting North Carolina complIance samples,a copy of this formwill besent to the North Carolina DFNR Certification Office (i.e. Out of hold,incorrect preservative,out of temp, Incorrect containers. Page 22 of 24 u n n n 3 rL {{ a CO CD CL Z. XS� R3— ° o 13 0 0 0. w N a = 0 Cr 3 7 7 ] Cr C_ � a q• O � C v 3 m a C m z a v � N C G C (D K c O C7 N c ;i m "\ KY � � a � a n D �1n 3 d G'r O p � V, w .•� S ry�ry � w nY 9 o C fl N QzCD h ei ET a' h v_I m Z• _ a n 'u a E� 2 d ` n Q O .26, Er o e w cam, r. a' n Q 'Ii :i1. 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