WQ0036561_Corrected 2023 Residual Annual Report_20240514

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0036561
Applicant/Permittee City of Danville
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0036561
Has Current Existing permit number
Applicant/Permittee Address*
279 Park Avenue, Danville, VA 24541
Facility Name*
City of Danville Class B Residuals Program
Please provide comments/notes on your current submittal below.
Submitting with corrected 5/1/23 pathogen/vector form. The wrong dates were initially used.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Danville Annual Report - WQ0036561.pdf 16.25MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 5/14/2024

--Resources, Inc.
City of Danville
2023 Annual Report
Residuals Land Application
Permit No. WQ0036561
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

February 27, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report — City of Danville, VA
Treatment and Land Application of Residuals
Permit No. WQ0036561
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 454.22 dry tons of wastewater residuals
to 220.48 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Brent Collins
Director of Technical Services
brent.collins&emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0036561 County: Pittsylvania County, VA Year:
2023
Facility Name (as shown on permit):
Land Application Operator:
City of Danville, Northside WWTP
EMA Resources Inc.
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
❑d Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the permit:1
26
Total number of fields utilized for land application during the year:
7
Total amount of dry tons applied during the year for all application sites:
454.22
Total number of acres utilizes for land application during the year:
220.48
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. El Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
1) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Alan Johnson - Division Director of Water & Wastewater Treatment
Permittee Name and Title (type or print)
26/01 /2024
Ala 6, 202412:35 EST)
Akii ,Zo�ns01? 29/01 /2024
Alan Johnson (Jan 29, 202415:24 EST)
Signature of Permittee L
�z
Date
1 /21 /2024
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DEN FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WWTP Name:
Residual Analysis Data
WQ0036561
City of Danville
VA0060593
Northside WWTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
(m g)a
Sample or Composite Date
4/3/23
4/18/23
5/l/23
5/15/23
Average
Percent Solids (%)
NA
3.97
4.01
4.02
3.91
3.98
Arsenic
75
12.5
12.5
12.5
12.8
12.58
Cadmium
85
2.5
2.5
2.5
2.56
2.52
Copper
4,300
440
348
450
405
410.75
Chromium
NA
43.3
36
43
39
40.33
Lead
840
48.5
1 38.8
54.3
51
48.15
Mercury
57
4.7
4.53
4.48
4.31
4.51
Molybdenum
75
9.78
7.5
10.9
9.54
9.43
Nickel
420
55
44.8
1 56
53.8
52.40
Selenium
100
12.5
12.5
12.5
12.8
12.58
Zinc
7,500
2390
1930
2350
2120
2197.5
Total Phosphorus
NA
22500
19200
23700
22200
21900
TKN
NA
71000
79000
115000
52600
79400
Ammonia -Nitrogen
NA
22400
12000
9550
11700
13913
Nitrate and Nitrite
NA
125
125
125
128
125.75
'For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Alan Gould ,
Signature of Preparer
26/01 /2024
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0036561
Facility Name: City of Danville
Residual Source
NPDES # or WQ#:
WWTP Name:
Residual Analysis Data
VA0060593
Northside WWTP
Laboratory:
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Sam le or Com osite Date
4/3/23
4/18/23
5/1/23
5/15/23
Average
Aluminum
29300
23500
31800
27700
28075
Calcium
16500
13600
15900
14900
15225
Magnesium
3550
3000
3650
3490
3422.5
pH
7.3
7.4
7.6
7.5
7.45
Potassium
3980
3650
4000
3970
3900
Sodium
17700
17100
16700
16600
17025
PAN
25905
26225
36535
18248
26728
SAR
6.48
6.9
6.21
6.27
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Man Gard(Ja 6.2Q412:3 Ei-1
Signature of Preparer
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
26/01 /2024
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 50.70
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: James Blackwell Owner: Nettie Blackwell Predominant Soil Series: FbB2
Acres Used: 20.33 Acres Permitted: 20.33 Site #: CS06 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
7j
8j
9j
10
11
12
DT/Ac./
App.
.fir
Event
2.49
Arsenic
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
2.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.049
Chromium
0.201
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.201
Lead
0.240
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.240
Mercury
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.022
Molyb-
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
denum
Nickel
0.261
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.261
Selenium
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Zinc
10.961
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
10.961
Total
Phos-
109.237
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
109.237
horus
1
1
1
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
z: f z 4; 5 1 114-
Signature of Land Applier
1/21/2024
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
Nettie Blackwell
Operator: James Blackwell
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 50.70 Site #:
Predominant Soil Series: FbB2
Crop 1 Max. PAN:
141
Crop 2 Name:
Acres Utilized:
CS06 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
20.33
20.33
0
o �
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
�a
F
w
*o•
o
,•d
�,
#
w •,
* N
*�
TKN
mg/kg
Z
;
o
oa o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/18
188500
3.98
1.539
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
82.261
NA
Fescue
7/19
117000
3.98
0.955
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
51.059
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
305500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
133.319
0.000
Lime Applied
Annuallbs/acre
0.063
0.013
2.049
0.201
0.240
0.022
0.047
0.261
0.063
10.961
109.237
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.055
0.01
1.446
0.385
0.264
0.006
0.073
0.218
0.016
5.367
Current Cumulative lbs/ac
0.118
0.023
3.495
0.586
0.504
0.028
0.120
0.479
0.079
16.328
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
2498
Permit PAN Limit lst/2nd Crop
141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation
vv''t���'^�-- 1/21/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 119.77
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: James Blackwell Owner: Nettie Blackwell Predominant Soil Series: FbB2
Acres Used: 45.87 Acres Permitted: 45.87 Site #: CS06 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
7j
8j
9j
10
11
12
DT/Ac./
App.
.fir
Event
2.61
Arsenic
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
2.145
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.145
Chromium
0.211
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.211
Lead
0.251
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.251
Mercury
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Molyb-
0.049
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.049
denum
Nickel
0.274
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.274
Selenium
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Zinc
11.475
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.475
Total
Phos-
114.362
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
114.362
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z:f z 4;��4e-
Signature of Land Applier
1/21/2024
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
Nettie Blackwell
Operator: James Blackwell
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 119.77 Site #:
Predominant Soil Series: FbB2
Crop 1 Max. PAN:
141
Crop 2 Name:
Acres Utilized:
CS06 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
45.87
45.87
0
o �
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
�a
F
w
*o•
o
,•d
�,
#
w •,
* N
*�
TKN
mg/kg
Z
;
o
oa o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/12
52000
3.98
0.188
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
10.058
NA
Fescue
7/13
266500
3.98
0.964
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
51.545
NA
Fescue
7/14
201500
3.98
0.729
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
38.973
NA
Fescue
7/17
201500
3.98
0.729
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
38.973
NA
Fescue
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
721500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
139.549
0.000
Lime Applied
Annuallbs/acre
0.066
0.013
2.145
0.211
0.251
0.024
0.049
0.274
0.066
11.475
114.362
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.533
0.127
63.467
4.292
2.837
0.061
0.631
2.578
0.213
70.971
Current Cumulative lbs/ac
0.599
0.140
65.612
4.503
3.088
0.085
0.680
2.852
0.279
82.446
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
2498
Permit PAN Limit lst/2nd Crop
i
F 141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation
vv''t���'^�-- 1/21/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 69.05
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: James Blackwell Owner: Nettie Blackwell Predominant Soil Series: FbB2
Acres Used: 26.89 Acres Permitted: 26.89 Site #: CS06 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
7j
8j
9j
10
11
12
DT/Ac./
App.
.fir
Event
2.57
Arsenic
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
2.110
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.110
Chromium
0.207
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.207
Lead
0.247
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.247
Mercury
0.023
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.023
Molyb-
0.048
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.048
denum
Nickel
0.269
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.269
Selenium
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Zinc
11.286
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
11.286
Total
Phos-
112.478
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
112.478
horus
1
1
1
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
z: f z 4; 5 1 114-
Signature of Land Applier
1/21/2024
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
Nettie Blackwell
Operator: James Blackwell
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 69.05 Site #:
Predominant Soil Series: FbB2
Crop 1 Max. PAN:
141
Crop 2 Name:
Acres Utilized:
CS06 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
26.89
26.89
0
o �
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
�a
F
w
*o•
o
,•d
�,
#
w •,
* N
*�
TKN
mg/kg
Z
;
o
oa o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/19
117000
3.98
0.722
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
38.602
NA
Fescue
7/20
266500
3.98
1.645
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
87.928
NA
Fescue
7/21
32500
3.98
0.201
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
10.723
NA
Fescue
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
416000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
137.253
0.000
Lime Applied
Annuallbs/acre
0.065
0.013
2.110
0.207
0.247
0.023
0.048
0.269
0.065
11.286
112.478
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.065
0.013
2.110
0.207
0.247
0.023
0.048
0.269
0.065
11.286
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
2498
Permit PAN Limit lst/2nd Crop
i
F 141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation
vv''t���'^�-- 1/21/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual):
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: Margaret Hatchett Owner: Margaret Hatchett Predominant Soil Series:
Acres Used: 27.76 Acres Permitted: 27.76 Site #: CS12 Field #:
16.18
ToC
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
7j
8j
9j
10
11
12
DT/Ac./
App.
.fir
Event
0.58
Arsenic
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Cadmium
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Copper
0.479
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.479
Chromium
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Lead
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Mercury
0.005
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.005
Molyb-
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
denum
Nickel
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.061
Selenium
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.015
Zinc
2.562
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.562
Total
Phos-
25.535
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
25.535
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
z: f z 4; 5 1 114-
1/21/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
Margaret Hatchett
Operator: Margaret Hatchett
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 16.18 Site #:
Predominant Soil Series: ToC
Crop 1 Max. PAN:
90.75 Crop 2 Name:
2
CS12
Acres Utilized:
Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
27.76
27.76
0
o �
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu_ Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
�a
F
w
*o•
o
,•d
�,
#
w •,
* N
*�
TKN
mg/kg
Z
;
o
oa o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/24
97500
3.98
0.583
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
31.161
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
97500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
31.161
0.000
Lime Applied
Annuallbs/acre
0.015
0.003
0.479
0.047
0.056
0.005
0.011
0.061
0.015
2.562
25.535
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.092
0.017
2.904
0.537
0.389
0.011
0.088
0.437
0.034
12.326
Current Cumulative lbs/ac
0.107
0.020
3.383
0.584
0.445
0.016
0.099
0.498
0.049
14.888
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
2498
Permit PAN Limit 1st/2nd Crop
F 9-0.75
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation
vv''t���'^�-- 1/21/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 36.69
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: William Hatchett Owner: W.H. Hatchett Predominant Soil Series: FbB2
Acres Used: 17.47 Acres Permitted: 17.47 Site #: CS12 Field #: 5
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
7j
8j
9j
10
11
12
DT/Ac./
App.
.fir
Event
2.10
Arsenic
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Cadmium
0.011
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.011
Copper
1.725
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.725
Chromium
0.169
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.169
Lead
0.202
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.202
Mercury
0.019
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.019
Molyb-
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
denum
Nickel
0.220
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.220
Selenium
0.053
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.053
Zinc
9.230
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
9.230
Total
Phos-
91.980
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
91.980
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z:f z 4;��4e-
Signature of Land Applier
1/21/2024
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
W.H. Hatchett
Operator: William Hatchett
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 36.69 Site #:
Predominant Soil Series: FbB2
Crop 1 Max. PAN:
188
Crop 2 Name:
Acres Utilized:
CS 12 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
17.47
17.47
0
o �
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
�a
F
w
*o•
o
,•d
�,
#
w •,
* N
*�
TKN
mg/kg
Z
;
o
oa o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/21
91000
3.98
0.865
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
46.213
NA
Fescue
7/24
130000
3.98
1.235
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
66.019
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
221000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
112.233
0.000
Lime Applied
Annuallbs/acre
0.053
0.011
1.725
0.169
0.202
0.019
0.040
0.220
0.053
9.230
91.980
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.302
0.071
13.232
2.596
1.577
0.034
0.314
1.847
0.196
44.9
Current Cumulative lbs/ac
0.355
0.082
14.957
2.765
1.779
0.053
0.354
2.067
0.249
54.130
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
2498
Permit PAN Limit lst/2nd Crop
188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation
vv''t���'^�-- 1/21/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 141.33
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: David Sartin Owner: David Sartin Predominant Soil Series: ToB
Acres Used: 75.78 Acres Permitted: 75.78 Site #: CS14 Field #: 1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
7j
8j
9j
10
11
12
DT/Ac./
App.
.fir
Event
1.87
Arsenic
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Cadmium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
1.532
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.532
Chromium
0.150
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.150
Lead
0.180
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.180
Mercury
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Molyb-
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
denum
Nickel
0.195
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.195
Selenium
0.047
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.047
Zinc
8.197
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
8.197
Total
Phos-
81.687
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
81.687
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z:f z 4;��4e-
Signature of Land Applier
1/21/2024
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
David Sartin
Operator: David Sartin
Crop 1 Name: Bermuda -Pasture
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 141.33 Site #:
Predominant Soil Series: ToB
Crop 1 Max. PAN:
117.75
Crop 2 Name:
Acres Utilized:
CS 14 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
75.78
75.78
0
o �
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
�a
F
w
*o•
o
,•d
�,
#
-
w •,
* N
*�
TKN
mg/kg
Z
;
o
M o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/25
130000
3.98
0.285
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
15.220
NA
Fescue
7/26
214500
3.98
0.470
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
25.113
NA
Fescue
7/27
234000
3.98
0.512
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
27.396
NA
Fescue
7/28
117000
3.98
0.256
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
13.698
NA
Fescue
7/31
156000
3.98
0.342
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
18.264
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
851500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
99.6goT
o.000
Lime Applied
Annuallbs/acre
0.047
0.009
1.532
0.150
0.180
0.017
0.035
0.195
0.047
8.197
81.687
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.535
0.163
19.802
3.219
2.933
0.073
0.556
3.02
0.422
86.299
Current Cumulative lbs/ac
0.582
1 0.172
21.334
3.369
3.113
0.090
0.591
3.215
0.469
94.496
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit lst/2nd Crop
117.75
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4�4- *Application Method: S - Surface, IN - Injection, INC - Incorporation
vv''t���'^�-- 1/21/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Danville Total Dry Tons Applied (Annual): 20.50
Permit #: WQ0036561 Cation Exchange Capacity (non 503 only):
Operator: David Sartin Owner: David Sartin Predominant Soil Series: FbB2
Acres Used: 6.38 Acres Permitted: 6.38 Site #: CS 14 Field #: 3
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
1
2
3
4
5j
6j
7j
8j
9j
10
11
12
DT/Ac./
App.
.fir
Event
3.21
Arsenic
0.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Cadmium
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
2.639
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.639
Chromium
0.259
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.259
Lead
0.309
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.309
Mercury
0.029
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.029
Molyb-
0.061
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.061
denum
Nickel
0.337
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.337
Selenium
0.081
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.081
Zinc
14.121
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
14.121
Total
Phos-
140.729
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
140.729
horus
"I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z:f z 4;��4e-
Signature of Land Applier
1/21/2024
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
City of Danville
David Sartin
Operator: David Sartin
Crop 1 Name: Fescue -Hay
WQ Permit #: WQ0036561 Field #:
Annual Dry Tons Applied: 20.50 Site #:
Predominant Soil Series: FbB2
Crop 1 Max. PAN:
188
Crop 2 Name:
Acres Utilized:
CS 14 Acres Permitted:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
6.38
6.38
0
o �
N
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(may'
Wet,
Moist)
Precip.
Past 24
Ms.
inches
a
�a
F
w
*o•
o
,•d
�,
#
w •,
* N
*�
TKN
mg/kg
Z
;
o
as o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/25
123500
3.98
3.213
Northside WWTP
Dry
<.5"
S
0.5
0.3
79400
13912.5
125.75
171.738
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
123500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
171.738
0.000
Lime Applied
Annuallbs/acre
0.081
0.016
2.639
0.259
0.309
0.029
0.061
0.337
0.081
14.121
140.729
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.324
0.141
10.931
1.515
1.565
0.052
0.309
1.654
0.34
57.516
Current Cumulative lbs/ac
0.405
0.157
13.570
1.774
1.874
0.081
0.370
1.991
0.421
71.637
Permitted C. P. L. R.****
36
34
1 1338
1
267
1 15
374
1 89
2498
Permit PAN Limit lst/2nd Crop
188
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
4�4. *Application Method: S - Surface, IN - Injection, INC - Incorporation
vv''t���'^�-- 1/21/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
4/19/2023
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 23-094-0014
Project Description: VPDES Permit# VA0060593
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 14

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-094-0014
Client Project Description: VPDES Permit# VAOO6O593
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
9045D
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-2320 B
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
6010D
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
4500NO3F-2011
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SW-7471B
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-4500-NH3C
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-4500-NH3C-TKN
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-2540G
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
SW-9045C
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
SW-7.3.4
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
SW-7.3.3
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
ASTM D93-80
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
SW-1311 (ZHE)
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
SW-1311
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8270C
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8260B
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8151A
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8081A
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
7470A
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
6010D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 14

�'
WayP
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES
Permit# VA0060593
A/P
Report
Date : 04/19/2023
Northside WWTP
Information :
Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61588
Matrix: Solids
Sample ID : LTS A -Basin 23-1245 A
Sampled: 4/3/2023
8:05
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Potassium
3980
mg/Kg -
dry
250
1
04/07/23 06:51
BKN
6010D
Magnesium
3550
mg/Kg -
dry
125
1
04/07/23 06:51
BKN
6010D
Sodium
17700
mg/Kg -
dry
625
1
04/07/23 06:51
BKN
6010D
Iron
30300
mg/Kg -
dry
250
1
04/07/23 06:51
BKN
6010D
Zinc
2390
mg/Kg -
dry
31.3
1
04/07/23 06:51
BKN
6010D
Ammonia Nitrogen
22400
mg/Kg -
dry
2500
1
04/06/23 05:50
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<125
mg/Kg -
dry
125
1
04/11/23 12:44
ZBD
4500NO3F-2011
Cadmium
<2.50
mg/Kg -
dry
2.50
1
04/07/23 06:51
BKN
6010D
Chromium
43.3
mg/Kg -
dry
6.25
1
04/07/23 06:51
BKN
6010D
Mercury
<4.70
mg/Kg -
dry
4.70
1
04/07/23 11:40
FDS
SW-7471B
pH
7.3
S.U.
1
04/10/2311:30
HBT
9045D
Molybdenum
9.78
mg/Kg -
dry
6.25
1
04/07/23 06:51
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
60800
mg/Kg -
dry
2500
1
04/11/23 09:45
TKM
SM-2320 B
Total Solids
3.97
%
0.010
1
04/10/23 14:09
JLS
SM-2540G
Aluminum
29300
mg/Kg -
dry
125
1
04/07/23 06:51
BKN
6010D
Selenium
<12.5
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Sulfur
12900
mg/Kg -
dry
250
1
04/07/23 06:51
BKN
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 3 of 14

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Project VPDES Permit# VA0060593
A/P Report Date : 04/19/2023
Northside WWTP Information : Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014 REPORT OFANALYSIS
Lab No : 61588
Sample ID : LTS A -Basin 23-1245 A
Matrix: Solids
Sampled: 4/3/2023 8:05
Moisture
96.0
%
0.010
1
04/10/2314:09
JLS
SM-2540G
Total Kjeldahl Nitrogen
71000
mg/Kg -
dry
6250
1
04/07/23 11:00
CLP ;M-4500-NH3C-TKl`
Phosphorus
22500
mg/Kg -
dry
125
1
04/07/23 06:51
BKN
6010D
Calcium
16500
mg/Kg -
dry
1250
1
04/07/23 06:51
BKN
6010D
Manganese
900
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Copper
440
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Organic N
48600
mg/Kg -
dry
6250
1
04/06/23 05:50
CALCULATION
Nickel
55.0
mg/Kg -
dry
6.25
1
04/07/23 06:51
BKN
6010D
Lead
48.5
mg/Kg -
dry
7.50
1
04/07/23 06:51
BKN
6010D
Arsenic
<12.5
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Total Volatile Solids
52.1
%
0.010
1
04/10/23 14:09
JLS
SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES Permit# VA0060593
A/P
Report Date : 04/19/2023
Northside WWTP
Information :
Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61589
Matrix: Solids
Sample ID : LTS A -Basin 23-1245 B
Sampled: 4/3/2023 8:05
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Sulfide (Reactivity)
<25.3
mg/Kg
25.3 1 04/13/23 10:30 CNB SW-7.3.4
Cyanide (Reactivity)
<0.125
mg/Kg
0.125 1 04/12/23 10:30 CNB SW-7.3.3
Ignitability
>96
degrees C
1 04/12/23 04:45 JFM ASTM D93-80
pH
Qualifiers/ DF Dilution Factor
Definitions
1 04/17/2317:03 CNB SW-9045C
MQL Method Quantitation Limit
Page 5 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES Permit#
VA0060593
A/P
Report Date : 04/19/2023
Northside WWTP
Information :
Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61590
Matrix: TCLP
Sample ID : LTS A -Basin 23-1245 C
Sampled: 4/3/2023 8:05
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
TCLP Herbicide Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP Metals Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP Pesticide Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP SVOC Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP VOC ZHE Extraction
Combined
1
04/10/23 13:00
ALM SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
L675452
04/11/23 13:52
Prep Method: 3015A
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Batch
TCLP Arsenic
<0.250
mg/L
0.250
1
04/11/23 19:04
JTR L675662
TCLP Barium
<0.250
mg/L
0.250
1
04/11/23 19:04
JTR L675662
TCLP Cadmium
<0.0500
mg/L
0.0500
1
04/11/23 19:04
JTR L675662
TCLP Chromium
<0.100
mg/L
0.100
1
04/11/23 19:04
JTR L675662
TCLP Lead
<0.100
mg/L
0.100
1
04/11/23 19:04
JTR L675662
TCLP Selenium
<0.500
mg/L
0.500
1
04/11/23 19:04
TJS L675662
TCLP Silver
<0.0500
mg/L
0.0500
1
04/11/23 19:04
JTR L675662
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES Permit#
VA0060593
A/P
Report Date : 04/19/2023
Northside WWTP
Information :
Received
: 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61590
Matrix: TCLP
Sample ID : LTS A -Basin 23-1245 C
Sampled: 4/3/2023 8:05
Analytical Method: 7470A
Prep Batch(es):
L675539
04/12/23 07:55
Prep Method: 7470A
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Mercury
<0.0200
mg/L
0.0200
1 04/12/23 13:42 FDS
L675724
Analytical Method: 8081A
Prep Batch(es):
L676046
04/13/23 17:00
Prep Method: 3510C
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Endrin
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP gamma-BHC
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP Methoxychlor
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP Toxaphene
<0.006000
mg/L
0.006000
10 04/14/23 16:58 VIC
L676321
TCLP Chlordane
<0.004000
mg/L
0.004000
10 04/14/23 16:58 VIC
L676321
TCLP Heptachlor Epoxide
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP Heptachlor
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
Surrogate: Decachlorobiphenyl
64.86
Limits: 36-116% 10 04/14/23 16:58 VIC
L676321
Surrogate: Tetrachloro-m-xylene
60.58
Limits: 25-123% 10 04/14/23 16:58 VIC
L676321
Analytical Method: 8151A
Prep Batch(es):
L676065
04/14/23 18:00
Prep Method: 8151A
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP 2,4-D
<0.0200
mg/L
0.0200
1 04/17/23 23:29 VIC
L676737
TCLP 2,4,5-TP (Silvex)
<0.0020
mg/L
0.0020
1 04/17/23 23:29 VIC
L676737
Surrogate: DCAA
65.80
Limits: 20-120% 1 04/17/23 23:29 VIC
L676737
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 7 of 14

waypANALYTICAL
79434
Infra ma rk
Project
A/P
Northside WWTP
Information
229 Northside Drive
Danville , VA 24540
Report Number : 23-094-0014
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
VPDES Permit# VA0060593
REPORT OFANALYSIS
Report Date : 04/19/2023
Received : 04/04/2023
Brandi Watson
Lab No : 61590
Matrix: TCLP
Sample ID : LTS A -Basin 23-1245 C
Sampled: 4/3/2023 8:05
Analytical Method: 8260B
Prep Batch(es):
L676130 04/13/23 08:23
Prep Method: 5030B
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Benzene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Carbon Tetrachloride
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Chlorobenzene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Chloroform
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP 1,4-Dichlorobenzene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP 1,2-Dichloroethane
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP 1,1-Dichloroethene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Methyl Ethyl Ketone (MEK)
<0.200
mg/L
0.200
1
04/13/23 13:07 ASH
L676139
TCLP Tetrachloroethene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Trichloroethene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Vinyl Chloride
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
Surrogate:4-Bromofluorobenzene
92.2
Limits:71-137%
1 04/13/23 13:07 ASH
L676139
Surrogate: Dibromofluoromethane
90.0
Limits: 70-128%
1 04/13/23 13:07 ASH
L676139
Surrogate: 1,2-Dichloroethane - d4
116
Limits: 63-136%
1 04/13/23 13:07 ASH
L676139
Surrogate: Toluene-d8
93.8
Limits: 70-130%
1 04/13/23 13:07 ASH
L676139
Analytical Method: 8270C
Prep Batch(es):
L675936 04/13/23 11:00
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP 3&4 Methylphenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP 2,4-Dinitrotoluene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 8 of 14

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Project VPDES Permit# VA0060593
A/P Report Date : 04/19/2023
Northside WWTP Information : Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014 REPORT OFANALYSIS
Lab No : 61590
Sample ID : LTS A -Basin 23-1245 C
Matrix: TCLP
Sampled: 4/3/2023 8:05
Analytical Method: 8270C
Prep Batch(es):
L675936 04/13/23 11:00
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Hexachlorobenzene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Hexachlorobutadiene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Hexachloroethane
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Nitrobenzene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Pentachlorophenol
<0.0500
mg/L
0.0500
1
04/13/23 20:12 VBW
L676114
TCLP Pyridine
<0.0500
mg/L
0.0500
1
04/13/23 20:12 VBW
L676114
TCLP 2,4,5-Trichlorophenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP 2,4,6-Trichlorophenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
Surrogate: TCLP 2,4,6-Tribromophenol
65.0
Limits: 42-102%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP 2-Fluorobiphenyl
57.5
Limits: 24-86%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP 2-Fluorophenol
27.3
Limits: 13-37%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP 4-Terphenyl-d14
75.0
Limits: 30-122%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP Nitrobenzene-d5
60.0
Limits: 25-78%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP Phenol-d6
17.1
Limits: 9-27%
1 04/13/23 20:12 VBW
L676114
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 9 of 14

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Inframark CASE NARRATIVE
Project: VPDES Permit# VA0060593
Lab Report Number: 23-094-0014
Date: 4/18/2023
Separatory Funnel Extraction 8081 Method 3510C
Sample 61590 (LTS A -Basin 23-1245 C)
QC Batch No: L676046/L676046
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Separatory Funnel Extraction 8270 Method 3510C
Sample 61590 (LTS A -Basin 23-1245 C)
QC Batch No: L675936/L675936
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Metals Analysis Method 601 OD
Sample 61588 (LTS A -Basin 23-1245 A)
Analyte: Aluminum
QC Batch No: L674758/L674295
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61588 (LTS A -Basin 23-1245 A)
Analyte: Iron
QC Batch No: L674758/L674295
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61588 (LTS A -Basin 23-1245 A)
Analyte: Potassium
QC Batch No: L674758/L674295
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 10 of 14

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 23-094-0014
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 04/04/2023 13:16:47
Page 11 of 14

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sa;Lslllt;;r-1 p :# ).loll
:011111N pa!1z)
U107t OU DOA/Hell IN3/HcI.L H113 -I .I.g3d VNfl DOA :101111s-
B,1()
E65 300dA #liwiad 530dl1 1.1nD A]! ►!lytaaZl W "D IQ OS:2V "H tid AD E]7 vq SV :s�!s1ssl�.roul
CTlWIN i E l II ll uu`` II II ii ff ,1,ewe,lul
(.[ojt�1❑t t.I l7j, llf 1 Ito[1]7W
-- I 'I I Iui1v 1111ncl,il:M
Page 14 of 14

Danville 4/3/23
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 17700 702.69 23 30.55174
Calcium 16500 655.05 20 32.7525
Magnesium 3550 140.935 12 11.74458
Percent Solids 3.97
SAR 6.48
SAR
Na+
a (Ca2+ + M92+)
30.55174
0.5( 32.753 2 + 11.74458 2 )

Waypointo
ANALYTICAL
4/27/2023
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 23-109-0007
Project Description: VPDES Permit # VA0060593
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/19/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-109-0007
Client Project Description: VPDES Permit # VAOO6O593
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
61824
LTS A -Basin
23-1298
Solids
04/18/2023 08:05
04/19/2023
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
SM-2320 B
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

�'
WayP
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES
Permit # VA0060593
A/P
Report
Date : 04/27/2023
Northside WWTP
Information :
Received : 04/19/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-109-0007
REPORT OFANALYSIS
Lab No : 61824
Matrix: Solids
Sample ID : LTS A -Basin 23-1298
Sampled: 4/18/2023 8:05
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.0
%
0.010
1
04/25/2316:30
JLS
SM-2540G
Sulfur
10200
mg/Kg -
dry
250
1
04/22/23 03:10
TJS
6010D
Calcium
13600
mg/Kg -
dry
1250
1
04/22/23 03:10
TJS
6010D
Manganese
733
mg/Kg -
dry
12.5
1
04/22/23 03:10
TJS
6010D
Zinc
1930
mg/Kg -
dry
31.3
1
04/22/23 03:10
TJS
6010D
Nickel
44.8
mg/Kg -
dry
6.25
1
04/22/23 03:10
TJS
6010D
Lead
38.8
mg/Kg -
dry
7.50
1
04/22/23 03:10
TJS
6010D
Arsenic
<12.5
mg/Kg -
dry
12.5
1
04/22/23 03:10
TJS
6010D
Selenium
<12.5
mg/Kg -
dry
12.5
1
04/22/23 03:10
TJS
6010D
pH
7.4
S.U.
1
04/25/2316:30
CNB
9045D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
56500
mg/Kg -
dry
2500
1
04/24/23 09:20
AMS
SM-2320 B
Organic N
67050
mg/Kg -
dry
6250
1
04/24/23 12:00
CALCULATION
Total Solids
4.01
%
0.010
1
04/25/23 16:30
JLS
SM-2540G
Phosphorus
19200
mg/Kg -
dry
125
1
04/22/23 03:10
TJS
6010D
Copper
348
mg/Kg -
dry
12.5
1
04/22/23 03:10
TJS
6010D
Magnesium
3000
mg/Kg -
dry
125
1
04/22/23 03:10
TJS
6010D
Molybdenum
7.50
mg/Kg -
dry
6.25
1
04/22/23 03:10
TJS
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 3 of 8

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Project VPDES Permit # VA0060593
A/P Report Date : 04/27/2023
Northside WWTP Information : Received : 04/19/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-109-0007 REPORT OFANALYSIS
Lab No : 61824 Matrix: Solids
Sample ID : LTS A -Basin 23-1298 Sampled: 4/18/2023 8:05
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium 17100 mg/Kg - dry 625 1 04/22/23 03:10 TJS 6010D
Total Kjeldahl Nitrogen
79000
mg/Kg -
dry
6250
1
04/25/23 09:30
CLP ;M-4500-NH3C-TKI`
Potassium
3650
mg/Kg -
dry
250
1
04/22/23 03:10
TJS
6010D
Iron
24400
mg/Kg -
dry
250
1
04/22/23 03:10
TJS
6010D
Aluminum
23500
mg/Kg -
dry
125
1
04/22/23 03:10
TJS
6010D
Ammonia Nitrogen
12000
mg/Kg -
dry
2500
1
04/24/23 12:00
CLP
SM-4500-NH3C
Nitrate+Nitrite-N
<125
mg/Kg -
dry
125
1
04/20/23 14:35
ZBD
4500NO3F-2011
Cadmium
<2.50
mg/Kg -
dry
2.50
1
04/22/23 03:10
TJS
6010D
Chromium
36.0
mg/Kg -
dry
6.25
1
04/22/23 03:10
TJS
6010D
Mercury
<4.53
mg/Kg -
dry
4.53
1
04/20/23 12:53
FDS
SW-7471B
Total Volatile Solids
52.0
%
0.010
1
04/25/23 16:30
JLS
SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Inframark CASE NARRATIVE
Project: VPDES Permit # VA0060593
Lab Report Number: 23-109-0007
Date: 4/26/2023
Metals Analysis Method 601 OD
Sample 98538 (TOCSOSB0320-24)
Analyte: Aluminum
QC Batch No: 1-678073/1-677142
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98538 (TOCSOSB0320-24)
Analyte: Aluminum
QC Batch No: 1-678312/1-677142
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98538 (TOCSOSB0320-24)
Analyte: Iron
QC Batch No: L677789/L677142
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 98538 (TOCSOSB0320-24)
Analyte: Potassium
QC Batch No: L677789/L677142
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 8

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 23-109-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 04/19/2023 12:40:38
Page 6 of 8

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Page 7 of 8

't•
Required Biosolids Tests for Inframark Danville, VA WWTP (Waypoint VA Account 79434)
Sample: LTS A Basin 23 — I a98 PO: 1SZ575
%TS
%TVs
pH
Alkalinity
TKN
Ammonia -Nitrogen
Nitrate + Nitrite as Nitrogen
Organic Nitrogen (calculation)
--Phosphorus
Potassium
Sulfur
Calcium
Magnesium
Sodium
Iron
Aluminum
--- Manganese
"Copper
— Zinc
"Cadmium
—Chromium
Mickel
— Lead
Arsenic
Mercury
Selenium
Molybdenum
Page 8 of 8

Danville 4/18/23
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 17100 685.71 23 29.81348
Calcium 13600 545.36 20 27.268
Magnesium 3000 120.3 12 10.025
Percent Solids 4.01
SAR 6.90
SAR
Na+
a (Ca2+ + M92+)
29.81348
0.5( 27.268 2 + 10.02500 2 )

Waypointo
ANALYTICAL
5/10/2023
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 23-122-0006
Project Description: VPDES Permit #: VA0060593
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/2/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-122-0006
Client Project Description: VPDES Permit #: VAOO6O593
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
61897
LTS A -basin
23-1332
Solids
05/01/2023 08:00
05/02/2023
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
SM-2320 B
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

�'
WayP
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES
Permit #: VA0060593
A/P
Report
Date : 05/10/2023
Northside WWTP
Information :
Received : 05/02/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-122-0006
REPORT OFANALYSIS
Lab No : 61897
Matrix: Solids
Sample ID : LTS A -basin 23-1332
Sampled: 5/1/2023 8:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.0
%
0.010
1
05/08/2316:55
JLS
SM-2540G
Sulfur
12400
mg/Kg -
dry
250
1
05/03/23 21:35
TJS
6010D
Calcium
15900
mg/Kg -
dry
1250
1
05/03/23 21:35
TJS
6010D
Manganese
983
mg/Kg -
dry
12.5
1
05/03/23 21:35
TJS
6010D
Zinc
2350
mg/Kg -
dry
31.3
1
05/03/23 21:35
TJS
6010D
Nickel
56.0
mg/Kg -
dry
6.25
1
05/03/23 21:35
TJS
6010D
Lead
54.3
mg/Kg -
dry
7.50
1
05/03/23 21:35
TJS
6010D
Arsenic
<12.5
mg/Kg -
dry
12.5
1
05/03/23 21:35
TJS
6010D
Selenium
<12.5
mg/Kg -
dry
12.5
1
05/03/23 21:35
TJS
6010D
pH
7.6
S.U.
1
05/03/2316:00
CNB
9045D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
52300
mg/Kg -
dry
2500
1
05/09/23 09:35
AMS
SM-2320 B
Organic N 105500
mg/Kg -
dry
6250
1
05/08/23 10:30
CALCULATION
Total Solids
4.02
%
0.010
1
05/08/23 16:55
JLS
SM-2540G
Phosphorus
23700
mg/Kg -
dry
125
1
05/03/23 21:35
TJS
6010D
Copper
450
mg/Kg -
dry
12.5
1
05/03/23 21:35
TJS
6010D
Magnesium
3650
mg/Kg -
dry
125
1
05/03/23 21:35
TJS
6010D
Molybdenum
10.9
mg/Kg -
dry
6.25
1
05/03/23 21:35
TJS
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 3 of 8

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Project VPDES Permit #: VA0060593
A/P Report Date : 05/10/2023
Northside WWTP Information : Received : 05/02/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-122-0006 REPORT OFANALYSIS
Lab No : 61897 Matrix: Solids
Sample ID : LTS A -basin 23-1332 Sampled: 5/1/2023 8:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium 16700 mg/Kg - dry 625 1 05/03/23 21:35 TJS 6010D
Total Kjeldahl Nitrogen
115000
mg/Kg -
dry
6250
1
05/08/23 10:30
JPJ
;M-4500-NH3C-TKI`
Potassium
4000
mg/Kg -
dry
250
1
05/03/23 21:35
TJS
6010D
Iron
32300
mg/Kg -
dry
250
1
05/03/23 21:35
TJS
6010D
Aluminum
31800
mg/Kg -
dry
125
1
05/03/23 21:35
TJS
6010D
Ammonia Nitrogen
9550
mg/Kg -
dry
2500
1
05/09/23 11:00
CLP
SM-4500-NH3C
Nitrate+Nitrite-N
<125
mg/Kg -
dry
125
1
05/08/23 15:12
ZBD
4500NO3F-2011
Cadmium
<2.50
mg/Kg -
dry
2.50
1
05/03/23 21:35
TJS
6010D
Chromium
43.0
mg/Kg -
dry
6.25
1
05/03/23 21:35
TJS
6010D
Mercury
<4.48
mg/Kg -
dry
4.48
1
05/08/23 12:48
FDS
SW-7471B
Total Volatile Solids
52.0
%
0.010
1
05/08/23 16:55
JLS
SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Inframark CASE NARRATIVE
Project: VPDES Permit #: VA0060593
Lab Report Number: 23-122-0006
Date: 5/9/2023
Metals Analysis Method 601 OD
Sample 86092 (ST23MAY01-03-001)
Analyte: Aluminum
QC Batch No: 1-679930/1-679600
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 86092 (ST23MAY01-03-001)
Analyte: Iron
QC Batch No: 1-679930/1-679600
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 86092 (ST23MAY01-03-001)
Analyte: Potassium
QC Batch No: 1-679930/1-679600
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 86092 (ST23MAY01-03-001)
Analyte: Sulfur
QC Batch No: 1-679930/1-679600
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 8

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 23-122-0006
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 05/02/2023 11:15:01
Page 6 of 8

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Page 7 of 8

Required Biosolids Tests for Inframark Danville, VA WWTP (Waypoint VA Account 79434)
Sample: LTS A Basin 23 — PP: 152575
%TS
%TVs
PH
— Alkalinity
TKN
__ Ammonia -Nitrogen
" Nitrate + Nitrite as Nitrogen
v
— Organic Nitrogen (calculation)
Q m
rn
0
Phosphorus
C
— Potassium
Sulfur
- Calcium
i
Magnesium
Sodium
i
Iron
N
w
v N
0
Aluminum
'
W
— Manganese
r Copper
Zinc
Cadmium
— Chromium
Nickel
Lead
Arsenic
-- Mercury
— Selenium
--Molybdenum
Page 8 of 8

Danville 5/1 /23
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 16700 671.34 23 29.1887
Calcium 15900 639.18 20 31.959
Magnesium 3650 146.73 12 12.2275
Percent Solids 4.02
SAR 6.21
SAR
Na+
a (Ca2+ + M92+)
29.18870
0.5( 31.959 2 + 12.22750 2 )

Waypointo
ANALYTICAL
5/25/2023
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 23-136-0007
Project Description: VPDES Permit #: VA0060593
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 5/16/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-136-0007
Client Project Description: VPDES Permit #: VAOO6O593
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
62039
LTS A -Basin
23-1374
Solids
05/15/2023
08:10
05/16/2023
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
SM-2320 B
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

�'
WayP
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES
Permit #: VA0060593
A/P
Report
Date : 05/25/2023
Northside WWTP
Information :
Received : 05/16/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-136-0007
REPORT OFANALYSIS
Lab No : 62039
Matrix: Solids
Sample ID : LTS A -Basin 23-1374
Sampled: 5/15/2023 8:10
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.1
%
0.010
1
05/22/2317:15
JLS
SM-2540G
Sulfur
12700
mg/Kg -
dry
256
1
05/19/23 01:29
BKN
6010D
Calcium
14900
mg/Kg -
dry
1280
1
05/19/23 01:29
BKN
6010D
Manganese
838
mg/Kg -
dry
12.8
1
05/19/23 01:29
BKN
6010D
Zinc
2120
mg/Kg -
dry
32.1
1
05/19/23 01:29
BKN
6010D
Nickel
53.8
mg/Kg -
dry
6.41
1
05/19/23 01:29
BKN
6010D
Lead
51.0
mg/Kg -
dry
7.69
1
05/19/23 01:29
BKN
6010D
Arsenic
<12.8
mg/Kg -
dry
12.8
1
05/19/23 01:29
BKN
6010D
Selenium
<12.8
mg/Kg -
dry
12.8
1
05/19/23 01:29
BKN
6010D
pH
7.5
S.U.
1
05/23/2316:00
CNB
9045D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
72100
mg/Kg -
dry
2560
1
05/18/23 09:45
BLM
SM-2320 B
Organic N
40900
mg/Kg -
dry
6410
1
05/24/23 10:00
CALCULATION
Total Solids
3.91
%
0.010
1
05/22/23 17:15
JLS
SM-2540G
Phosphorus
22200
mg/Kg -
dry
128
1
05/19/23 01:29
BKN
6010D
Copper
405
mg/Kg -
dry
12.8
1
05/19/23 01:29
BKN
6010D
Magnesium
3490
mg/Kg -
dry
128
1
05/19/23 01:29
BKN
6010D
Molybdenum
9.54
mg/Kg -
dry
6.41
1
05/19/23 01:29
BKN
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 3 of 8

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Project VPDES Permit #: VA0060593
A/P Report Date : 05/25/2023
Northside WWTP Information : Received : 05/16/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-136-0007 REPORT OFANALYSIS
Lab No : 62039 Matrix: Solids
Sample ID : LTS A -Basin 23-1374 Sampled: 5/15/2023 8:10
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Sodium 16600 mg/Kg - dry 641 1 05/19/23 01:29 BKN 6010D
Total Kjeldahl Nitrogen
52600
mg/Kg -
dry
6410
1
05/24/23 10:00
JPJ
;M-4500-NH3C-TKI`
Potassium
3970
mg/Kg -
dry
256
1
05/19/23 01:29
BKN
6010D
Iron
29700
mg/Kg -
dry
256
1
05/19/23 01:29
BKN
6010D
Aluminum
27700
mg/Kg -
dry
128
1
05/19/23 01:29
BKN
6010D
Ammonia Nitrogen
11700
mg/Kg -
dry
2560
1
05/24/23 14:40
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<128
mg/Kg -
dry
128
1
05/17/23 14:25
ZBD
4500NO3F-2011
Cadmium
<2.56
mg/Kg -
dry
2.56
1
05/19/23 01:29
BKN
6010D
Chromium
39.0
mg/Kg -
dry
6.41
1
05/19/23 01:29
BKN
6010D
Mercury
<4.31
mg/Kg -
dry
4.31
1
05/19/23 13:57
FDS
SW-7471B
Total Volatile Solids
52.4
%
0.010
1
05/22/23 17:15
JLS
SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Inframark CASE NARRATIVE
Project: VPDES Permit #: VA0060593
Lab Report Number: 23-136-0007
Date: 5/24/2023
Metals Analysis Method 601 OD
Sample 94565
QC Batch No: L682967/L682391
One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are
required.
Sample 94565
Analyte: Aluminum
QC Batch No: L683074/L682391
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94565
Analyte: Calcium
QC Batch No: L683074/L682391
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94565
Analyte: Iron
QC Batch No: L683074/L682391
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94565
Analyte: Magnesium
QC Batch No: L683074/L682391
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 94565
Analyte: Manganese
QC Batch No: L683074/L682391
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 8

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 23-136-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 05/16/2023 11:44:00
Page 6 of 8

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Page 7 of 8

Required 6iosolids Tests for tnframark Danville, VA VOA TP (Waypoint VA Account 79434)
Sample: Lis A Basin 23 — 1 571 PO: 152575
%NS
pH
r:
o-
Alkalinity
m 1
zFm
rKN
Ammonia -Nitrogen
Nitrate +Nitrite as Nitrogen
w
Organic Nitrogen (cafculation)
Phosphorus
Potassium
SulfurFQ
w
Calcium
V
V
Magnesium
Sodium
Iron
Aluminum
Manganese
Copper
Zinc
Cadmium
Chromium
Nickel
Lead
Arsenic
Mercury
Selenium
Molybdenum
Page 8 of 8

Danville 5/15/23
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
16600
649.06
23 28.22
Calcium
14900
582.59
20 29.1295
Magnesium
3490
136.459
12 11.37158
Percent Solids
3.91
SAR
6.27
SAR
Na+
a (Ca2+ + M92+)
28.22000
0.5( 29.13 2 + 11.37158 2 )

Waypointo
ANALYTICAL
4/19/2023
Inframark
A/P
Northside WWTP
229 Northside Drive
Danville, VA, 24540
Ref: Analytical Testing
Report Number: 23-094-0014
Project Description: VPDES Permit# VA0060593
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear A/P:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 14

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-094-0014
Client Project Description: VPDES Permit# VAOO6O593
Lab No
Client Sample ID
Matrix
Date Collected
Date Received
Method
Lab ID
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
9045D
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-2320 B
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
6010D
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
4500NO3F-2011
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SW-7471B
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-4500-NH3C
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-4500-NH3C-TKN
WP MTN
61588
LTS A -Basin 23-1245 A
Solids
04/03/2023 08:05
04/04/2023
SM-2540G
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
SW-9045C
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
SW-7.3.4
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
SW-7.3.3
WP MTN
61589
LTS A -Basin 23-1245 B
Solids
04/03/2023 08:05
04/04/2023
ASTM D93-80
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
SW-1311 (ZHE)
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
SW-1311
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8270C
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8260B
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8151A
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
8081A
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
7470A
WP MTN
61590
LTS A -Basin 23-1245 C
TCLP
04/03/2023 08:05
04/04/2023
6010D
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 14

�'
WayP
7621 Whitepine
Road, Richmond,
VA 23237
Main 804-743-9401 Fax
804-271-6446
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES
Permit# VA0060593
A/P
Report
Date : 04/19/2023
Northside WWTP
Information :
Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61588
Matrix: Solids
Sample ID : LTS A -Basin 23-1245 A
Sampled: 4/3/2023
8:05
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Potassium
3980
mg/Kg -
dry
250
1
04/07/23 06:51
BKN
6010D
Magnesium
3550
mg/Kg -
dry
125
1
04/07/23 06:51
BKN
6010D
Sodium
17700
mg/Kg -
dry
625
1
04/07/23 06:51
BKN
6010D
Iron
30300
mg/Kg -
dry
250
1
04/07/23 06:51
BKN
6010D
Zinc
2390
mg/Kg -
dry
31.3
1
04/07/23 06:51
BKN
6010D
Ammonia Nitrogen
22400
mg/Kg -
dry
2500
1
04/06/23 05:50
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<125
mg/Kg -
dry
125
1
04/11/23 12:44
ZBD
4500NO3F-2011
Cadmium
<2.50
mg/Kg -
dry
2.50
1
04/07/23 06:51
BKN
6010D
Chromium
43.3
mg/Kg -
dry
6.25
1
04/07/23 06:51
BKN
6010D
Mercury
<4.70
mg/Kg -
dry
4.70
1
04/07/23 11:40
FDS
SW-7471B
pH
7.3
S.U.
1
04/10/2311:30
HBT
9045D
Molybdenum
9.78
mg/Kg -
dry
6.25
1
04/07/23 06:51
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Alkalinity (as CaCO3)
60800
mg/Kg -
dry
2500
1
04/11/23 09:45
TKM
SM-2320 B
Total Solids
3.97
%
0.010
1
04/10/23 14:09
JLS
SM-2540G
Aluminum
29300
mg/Kg -
dry
125
1
04/07/23 06:51
BKN
6010D
Selenium
<12.5
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Sulfur
12900
mg/Kg -
dry
250
1
04/07/23 06:51
BKN
6010D
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 3 of 14

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Project VPDES Permit# VA0060593
A/P Report Date : 04/19/2023
Northside WWTP Information : Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014 REPORT OFANALYSIS
Lab No : 61588
Sample ID : LTS A -Basin 23-1245 A
Matrix: Solids
Sampled: 4/3/2023 8:05
Moisture
96.0
%
0.010
1
04/10/2314:09
JLS
SM-2540G
Total Kjeldahl Nitrogen
71000
mg/Kg -
dry
6250
1
04/07/23 11:00
CLP ;M-4500-NH3C-TKl`
Phosphorus
22500
mg/Kg -
dry
125
1
04/07/23 06:51
BKN
6010D
Calcium
16500
mg/Kg -
dry
1250
1
04/07/23 06:51
BKN
6010D
Manganese
900
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Copper
440
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Organic N
48600
mg/Kg -
dry
6250
1
04/06/23 05:50
CALCULATION
Nickel
55.0
mg/Kg -
dry
6.25
1
04/07/23 06:51
BKN
6010D
Lead
48.5
mg/Kg -
dry
7.50
1
04/07/23 06:51
BKN
6010D
Arsenic
<12.5
mg/Kg -
dry
12.5
1
04/07/23 06:51
BKN
6010D
Total Volatile Solids
52.1
%
0.010
1
04/10/23 14:09
JLS
SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES Permit# VA0060593
A/P
Report Date : 04/19/2023
Northside WWTP
Information :
Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61589
Matrix: Solids
Sample ID : LTS A -Basin 23-1245 B
Sampled: 4/3/2023 8:05
Test
Results
Units
MQL DF Date / Time By Analytical
Analyzed Method
Sulfide (Reactivity)
<25.3
mg/Kg
25.3 1 04/13/23 10:30 CNB SW-7.3.4
Cyanide (Reactivity)
<0.125
mg/Kg
0.125 1 04/12/23 10:30 CNB SW-7.3.3
Ignitability
>96
degrees C
1 04/12/23 04:45 JFM ASTM D93-80
pH
Qualifiers/ DF Dilution Factor
Definitions
1 04/17/2317:03 CNB SW-9045C
MQL Method Quantitation Limit
Page 5 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES Permit#
VA0060593
A/P
Report Date : 04/19/2023
Northside WWTP
Information :
Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61590
Matrix: TCLP
Sample ID : LTS A -Basin 23-1245 C
Sampled: 4/3/2023 8:05
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Method
TCLP Herbicide Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP Metals Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP Pesticide Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP SVOC Extraction
Combined
1
04/10/23 13:00
ALM SW-1311
TCLP VOC ZHE Extraction
Combined
1
04/10/23 13:00
ALM SW-1311 (ZHE)
Analytical Method: 6010D
Prep Batch(es):
L675452
04/11/23 13:52
Prep Method: 3015A
Test
Results
Units
MQL
DF
Date / Time
By Analytical
Analyzed
Batch
TCLP Arsenic
<0.250
mg/L
0.250
1
04/11/23 19:04
JTR L675662
TCLP Barium
<0.250
mg/L
0.250
1
04/11/23 19:04
JTR L675662
TCLP Cadmium
<0.0500
mg/L
0.0500
1
04/11/23 19:04
JTR L675662
TCLP Chromium
<0.100
mg/L
0.100
1
04/11/23 19:04
JTR L675662
TCLP Lead
<0.100
mg/L
0.100
1
04/11/23 19:04
JTR L675662
TCLP Selenium
<0.500
mg/L
0.500
1
04/11/23 19:04
TJS L675662
TCLP Silver
<0.0500
mg/L
0.0500
1
04/11/23 19:04
JTR L675662
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 6 of 14

�'
WayP
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
79434
Inframark
Project
VPDES Permit#
VA0060593
A/P
Report Date : 04/19/2023
Northside WWTP
Information :
Received
: 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014
REPORT OFANALYSIS
Lab No : 61590
Matrix: TCLP
Sample ID : LTS A -Basin 23-1245 C
Sampled: 4/3/2023 8:05
Analytical Method: 7470A
Prep Batch(es):
L675539
04/12/23 07:55
Prep Method: 7470A
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Mercury
<0.0200
mg/L
0.0200
1 04/12/23 13:42 FDS
L675724
Analytical Method: 8081A
Prep Batch(es):
L676046
04/13/23 17:00
Prep Method: 3510C
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP Endrin
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP gamma-BHC
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP Methoxychlor
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP Toxaphene
<0.006000
mg/L
0.006000
10 04/14/23 16:58 VIC
L676321
TCLP Chlordane
<0.004000
mg/L
0.004000
10 04/14/23 16:58 VIC
L676321
TCLP Heptachlor Epoxide
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
TCLP Heptachlor
<0.000800
mg/L
0.000800
10 04/14/23 16:58 VIC
L676321
Surrogate: Decachlorobiphenyl
64.86
Limits: 36-116% 10 04/14/23 16:58 VIC
L676321
Surrogate: Tetrachloro-m-xylene
60.58
Limits: 25-123% 10 04/14/23 16:58 VIC
L676321
Analytical Method: 8151A
Prep Batch(es):
L676065
04/14/23 18:00
Prep Method: 8151A
Test
Results
Units
MQL
DF Date / Time By
Analytical
Analyzed
Batch
TCLP 2,4-D
<0.0200
mg/L
0.0200
1 04/17/23 23:29 VIC
L676737
TCLP 2,4,5-TP (Silvex)
<0.0020
mg/L
0.0020
1 04/17/23 23:29 VIC
L676737
Surrogate: DCAA
65.80
Limits: 20-120% 1 04/17/23 23:29 VIC
L676737
Qualifiers/ DF Dilution Factor
MQL Method Quantitation Limit
Definitions
Page 7 of 14

waypANALYTICAL
79434
Infra ma rk
Project
A/P
Northside WWTP
Information
229 Northside Drive
Danville , VA 24540
Report Number : 23-094-0014
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
VPDES Permit# VA0060593
REPORT OFANALYSIS
Report Date : 04/19/2023
Received : 04/04/2023
Brandi Watson
Lab No : 61590
Matrix: TCLP
Sample ID : LTS A -Basin 23-1245 C
Sampled: 4/3/2023 8:05
Analytical Method: 8260B
Prep Batch(es):
L676130 04/13/23 08:23
Prep Method: 5030B
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Benzene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Carbon Tetrachloride
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Chlorobenzene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Chloroform
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP 1,4-Dichlorobenzene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP 1,2-Dichloroethane
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP 1,1-Dichloroethene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Methyl Ethyl Ketone (MEK)
<0.200
mg/L
0.200
1
04/13/23 13:07 ASH
L676139
TCLP Tetrachloroethene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Trichloroethene
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
TCLP Vinyl Chloride
<0.0100
mg/L
0.0100
1
04/13/23 13:07 ASH
L676139
Surrogate:4-Bromofluorobenzene
92.2
Limits:71-137%
1 04/13/23 13:07 ASH
L676139
Surrogate: Dibromofluoromethane
90.0
Limits: 70-128%
1 04/13/23 13:07 ASH
L676139
Surrogate: 1,2-Dichloroethane - d4
116
Limits: 63-136%
1 04/13/23 13:07 ASH
L676139
Surrogate: Toluene-d8
93.8
Limits: 70-130%
1 04/13/23 13:07 ASH
L676139
Analytical Method: 8270C
Prep Batch(es):
L675936 04/13/23 11:00
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP 2-Methylphenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP 3&4 Methylphenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP 2,4-Dinitrotoluene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
Qualifiers/ DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 8 of 14

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
79434
Inframark Project VPDES Permit# VA0060593
A/P Report Date : 04/19/2023
Northside WWTP Information : Received : 04/04/2023
229 Northside Drive
Danville , VA 24540
Brandi Watson
Report Number : 23-094-0014 REPORT OFANALYSIS
Lab No : 61590
Sample ID : LTS A -Basin 23-1245 C
Matrix: TCLP
Sampled: 4/3/2023 8:05
Analytical Method: 8270C
Prep Batch(es):
L675936 04/13/23 11:00
Prep Method: 3510C
Test
Results
Units
MQL
DF
Date / Time By
Analytical
Analyzed
Batch
TCLP Hexachlorobenzene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Hexachlorobutadiene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Hexachloroethane
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Nitrobenzene
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP Pentachlorophenol
<0.0500
mg/L
0.0500
1
04/13/23 20:12 VBW
L676114
TCLP Pyridine
<0.0500
mg/L
0.0500
1
04/13/23 20:12 VBW
L676114
TCLP 2,4,5-Trichlorophenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
TCLP 2,4,6-Trichlorophenol
<0.0250
mg/L
0.0250
1
04/13/23 20:12 VBW
L676114
Surrogate: TCLP 2,4,6-Tribromophenol
65.0
Limits: 42-102%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP 2-Fluorobiphenyl
57.5
Limits: 24-86%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP 2-Fluorophenol
27.3
Limits: 13-37%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP 4-Terphenyl-d14
75.0
Limits: 30-122%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP Nitrobenzene-d5
60.0
Limits: 25-78%
1 04/13/23 20:12 VBW
L676114
Surrogate: TCLP Phenol-d6
17.1
Limits: 9-27%
1 04/13/23 20:12 VBW
L676114
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 9 of 14

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Client: Inframark CASE NARRATIVE
Project: VPDES Permit# VA0060593
Lab Report Number: 23-094-0014
Date: 4/18/2023
Separatory Funnel Extraction 8081 Method 3510C
Sample 61590 (LTS A -Basin 23-1245 C)
QC Batch No: L676046/L676046
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Separatory Funnel Extraction 8270 Method 3510C
Sample 61590 (LTS A -Basin 23-1245 C)
QC Batch No: L675936/L675936
The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample.
Reporting limits are factored for the sample size reduction.
Metals Analysis Method 601 OD
Sample 61588 (LTS A -Basin 23-1245 A)
Analyte: Aluminum
QC Batch No: L674758/L674295
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61588 (LTS A -Basin 23-1245 A)
Analyte: Iron
QC Batch No: L674758/L674295
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61588 (LTS A -Basin 23-1245 A)
Analyte: Potassium
QC Batch No: L674758/L674295
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 10 of 14

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 79434
Customer Name: Inframark
Report Number: 23-094-0014
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 04/04/2023 13:16:47
Page 11 of 14

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Page 13 of 14

bT 30 bT 9SUd
Wa}'paint Analytical Labtrraiary IIl�IH fl�il�ll III�Ii�IIiIIl V�l1I�II�III I� o79434 3�
Method 1311 '1'CLP Prep Slier(
11101-ganim As M-1 Cd Cr Pb Ho Ag SVLn Cu Ni Reactivity Cnrl Intramark 13.10-45
VPOES Permit# VAOD60593
01-gartics: WUC BNA PEST HEIZB T'Pi- cI m "1'PI-IIVoc 13en•r-ent
Clicnt prime: GM11,rrluit
Repw•t #: vi --o¢, d 14 Leachates
Sample Dale; 4:-3- F il(mllcs
1)atc Ar•rived ; Matrix: AQU Li uid/oiUSolidlOt11cI.
E)atr )r:x[rarlctl: i:xtrac(itrn Trcltn.:
Balance ID: p1.1 Calihraliun Reference;
! SVOC/Mcfals
I.aU ID #:
�. Gas 1 o
E Colsja
OC
Lab IC) ":
f r
dal
4
Characterization fir 1:: xtracl 1 laid
5allll�le Initial Second Extract
weight f� f p 13H Fluid #
C11a1'iltl�l'iII111011 10I' r_xtrut i'luid
Sample Initial Second Ex[rarc[
V+'ci 11tit Fluid #
f=i
1-I
l xtrac[iorl
weight tills
graims Fluid
I'mravt'1011
wci�dlit rills
Fluid
Final
pl-f
Fluid
F i11a1
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Size
Reduction
YIN
13ntllc
#
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Pressurt
Maintained
YIN
II IF. -
Ili
N
YIN
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1 Lah ID #: Beaker Beaker Sample I Flask I. -Ins I: Filter i=iIter ! iltratc I Solid
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F"Irilo km Bach I I );
I cilW. Min' Ian Rrading:
R'l.P LO-in Work1,1le01 1 ; I 1 082718

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Danville WQ Permit Number: WQ0036561
WWTP Name: Northside WWTP NPDES Number: VA0060593
Monitoring Period: From 4/3/2023 To 4/3/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAlt. (1) Fecal Density El
7AIt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
JAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
dences
Frequency
of Analysis
Sample
'Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximud
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
2380
2596
2780
CFU/ g
0
Quarterly
l
G
SM9222D
1000 mpn per gram
of total solid (dry
wei t
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) v
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Alan Gould - Project Manager
Preparer Name and Title (type or print)
e
Ala 6, 202412:35 EST)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
26/01 /2( ev
1/21/2024
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
April 06, 2023
Kimberly Wickemeyer
Inframark
229 Northside Drive
Danville, VA 24540
RE: Project: INFRAMARK-DANVILLE VA0060593
Pace Project No.: 30574814
Dear Kimberly Wickemeyer:
Enclosed are the analytical results for sample(s) received by the laboratory on April 03, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Beaver
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cynthia Walker
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
CERTIFICATIONS
Project: INFRAMARK-DANVILLE VA0060593
Pace Project No.: 30574814
Pace Analytical Services Beaver
225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466
Virginia VELAP 460148 Kentucky Wastewater Certification KY90039
West Virginia DEP 060 Pennsylvania DEP 68-00839
West Virginia DHHR 00412CM
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE SUMMARY
Project: INFRAMARK-DANVILLE VA0060593
Pace Project No.: 30574814
Lab ID
Sample ID
Matrix
Date Collected
Date Received
30574814001
A BASIN #1
Solid
04/03/23 07:20
04/03/23 12:10
30574814002
A BASIN #2
Solid
04/03/23 07:25
04/03/23 12:10
30574814003
A BASIN #3
Solid
04/03/23 07:30
04/03/23 12:10
30574814004
A BASIN #4
Solid
04/03/23 07:45
04/03/23 12:10
30574814005
A BASIN #5
Solid
04/03/23 07:55
04/03/23 12:10
30574814006
A BASIN #6
Solid
04/03/23 08:00
04/03/23 12:10
30574814007
A BASIN #7
Solid
04/03/23 08:05
04/03/23 12:10
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
INFRAMARK-DANVILLE VA0060593
30574814
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
30574814001
A BASIN #1
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30574814002
A BASIN #2
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30574814003
A BASIN #3
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30574814004
A BASIN #4
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30574814005
A BASIN #5
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30574814006
A BASIN #6
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30574814007
A BASIN #7
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
PASI-BV = Pace Analytical Services - Beaver
PASI-LE = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: INFRAMARK-DANVILLE VA0060593
Pace Project No.: 30574814
Sample: A BASIN #1
Lab ID: 30574814001 Collected: 04/03/23 07:20 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
96.4 % 0.10 1 04/04/23 09:16 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
ND CFU/g 2780 2.778 04/03/23 14:35 04/04/23 12:12
Sample: A BASIN #2
Lab ID: 30574814002 Collected: 04/03/23 07:25 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
95.8 % 0.10 1 04/04/23 09:18 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
ND CFU/g 2380 2.381 04/03/23 14:35 04/04/23 12:12
Sample: A BASIN #3
Lab ID: 30574814003 Collected: 04/03/23 07:30 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
96.3 % 0.10 1 04/04/23 09:21 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
ND CFU/g 2700 2.703 04/03/23 14:35 04/04/23 12:12
Sample: A BASIN #4
Lab ID: 30574814004 Collected: 04/03/23 07:45 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Percent Moisture
Date: 04/06/2023 05:15 PM
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
96.0 % 0.10 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
04/04/23 09:22
N2
Page 5 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: INFRAMARK-DANVILLE VA0060593
Pace Project No.: 30574814
Sample: A BASIN #4 Lab ID: 30574814004 Collected: 04/03/23 07:45 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 2500 2.5 04/03/23 14:35 04/04/23 12:12
Sample: A BASIN #5 Lab ID: 30574814005 Collected: 04/03/23 07:55 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
95.9 % 0.10 1 04/04/23 09:25 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
ND CFU/g 2440 2.44 04/03/23 14:35 04/04/23 12:12
Sample: A BASIN #6
Lab ID: 30574814006 Collected: 04/03/23 08:00 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
96.3 % 0.10 1 04/04/23 09:25 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
ND CFU/g 2700 2.703 04/03/23 14:35 04/04/23 12:12
Sample: A BASIN #7
Lab ID: 30574814007 Collected: 04/03/23 08:05 Received: 04/03/23 12:10 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
96.3 % 0.10 1 04/04/23 09:27 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
ND CFU/g 2700 2.703 04/03/23 14:35 04/04/23 12:12
Date: 04/06/2023 05:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALIFIERS
Project: INFRAMARK-DANVILLE VA0060593
Pace Project No.: 30574814
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/06/2023 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: INFRAMARK-DANVILLE VA0060593
Pace Project No.: 30574814
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
30574814001
A BASIN
#1
SM
2540G-15
578212
30574814002
A BASIN
#2
SM
2540G-15
578212
30574814003
A BASIN
#3
SM
2540G-15
578212
30574814004
A BASIN
#4
SM
2540G-15
578212
30574814005
A BASIN
#5
SM
2540G-15
578212
30574814006
A BASIN
#6
SM
2540G-15
578212
30574814007
A BASIN
#7
SM
2540G-15
578212
30574814001
A BASIN
#1
SM
9222D-2015
578374
SM
9222D-2015
578376
30574814002
A BASIN
#2
SM
9222D-2015
578374
SM
9222D-2015
578376
30574814003
A BASIN
#3
SM
9222D-2015
578374
SM
9222D-2015
578376
30574814004
A BASIN
#4
SM
9222D-2015
578374
SM
9222D-2015
578376
30574814005
A BASIN
#5
SM
9222D-2015
578374
SM
9222D-2015
578376
30574814006
A BASIN
#6
SM
9222D-2015
578374
SM
9222D-2015
578376
30574814007
A BASIN
#7
SM
9222D-2015
578374
SM
9222D-2015
578376
Date: 04/06/2023 05:15 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 10

CHAIN -OF -CUSTODY Analytical Bequest Document
2ceAnatyfical�
Chain-of-Custodylsa LEGAL DOCUMENT - Compieteallreleventffelds
LAB USE ONLY- Affix Workorder/Login Label Here or List Pace Workorder Number or
MTJL Lag -In Number Here
', WD# : 30574814
A
Company:
Inframark-Danville
Billing Information:
Inframark-Danville WWTP
229 i Drive
Danville. , VA 2A 4540
Container Prl II I III III IIII I �� II III
U `
"Preservative Types: (1)nitr 30574814 Late,
(6) methanol, (7) sodium blsulta._, ,_,
(C) ammonium hydroxide, (U) TSP, (U) Unpreserved, JO) Other
Address:
229 Northside Dr., Danville, VA 2454D
Report To: [e-mail]
EmaliT°: aiicia.crumpton C@i inframark.com
Copy To:
[e-mail]
Site Collection Info -/Address:
Danville VA ydWTP 229 Nonhside, Dr., Danville, VA 24540
Analyses
Lab Prorlle/Line:
Customer Project Name/Number:
Inframark-Danville (client #: 92-618203)
State: County/City: Time Zone Collected:
VA /Danville ( ] PT [ I MT [ ] CT 64 FT
U
�,
N
2
❑-
W
V)
J
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U
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N
ILL
i
Lab Sample Receipt checklist:
#
Custody seals Present/intact Y N NA
Custody Signatures Present Y N NA
Collector Signature Present Y N NA t
Bottles Intact Y N NA
Correct Bottles Y N NA
Sufficient volume Y N NA
Samples Received on Ice Y N WA
voA - Headspaae Acceptable Y N NA
Regulated Solis Y N NA
Samples in Holding Time Y IQ NA
Samp
Residual Chlorine Present Y 14 NA
Cl Strips:
Sample pH Acceptable Y N NA
pH Strips:
Sulfide Present Y N NA
Lead Acetate strips:
LAB asE ONLY:
Lab Sample d / Comments;
Phone; 434-799-5137
Email: ldmbariy.wlckemeyarainrramark.com
Site/Facllity ID
Danville, VA WWTP permit VA0060593
Compliance Monitoring?
[ Oes [ ] No
Collected By (print):
Robert Clifton
Purchase Order M 152847
Quote #: 00128560
DW PWS ID #:
DW Location Code:
Collected By i atu e):
Turnaround Date Re uired:
results by b4118/2023
immediately Pace on Ice;
[Ivyes [ ] No
Sample Disposal:
[k� Dispose as appropriate [ ] Return
[ )Arch€ve:
[ )Hold:
Rush:
[ ] Same Day [ I Next Day
[ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] S Day
{Expedite Charges Apply)
Field Filtered (if applicable):
[ ] Yes No
Analysis:
*Matrix Codes (Insert in Matrix box below): Drinking Water (DW), Ground Water(GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe {WPj, Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample ID
Matrix
Comp/
Grab
Collected (or
Composite Start)
Composite End
Res
CI
#of
Ctns
Date
Time
Date
Time
Basin #1
SL*
Grab
04/03/23
0720
- - - -
- - - -
No
1
Basin #2
SL*
Grab
04/03/23
0725
---_
----
No
1
Basin #3
SL*
Grab
04/03/23
0730
- - - -
- - -
No
1
A Basin #4
SL*
Grab
04/03/23
0745
- - - -
- - -
No
1
asin
SL*
Grab
04/03/23
0705
- - - -
- - - -
NO
1
asin #6
SL*
Grab
04/03/23
0
- - - -
- - - -
No
1
Basin #7
SL*
Grab
04/03/23
0805
----
----
No
1
Customer Remarks /Special Conditions /Possible Hazards:
Type of Ice Used: a Blue Dry None
SHORT HOLDS PRESENT (<72 hours) N/A
Lab Sample Temperature Info:
Temp lReceived: Y NA
Therm0#D#: :
Packing Material Used:
Lab Tracking#:
siosoflds for Fecal Coliform
Cooler 1 Temp Upon Recelpmj oC
Cooler 1 Therm Corr. Factor.+ oC
Cooler 1 Corrected TernoC
Comments:
Radchem sample{s) screened (<500 rpm}: Y N NA
Samples received via:
FEDEX UPS lien Courier Pace Courier
Rellg uls�he�d by/Company; (Signature)
Date/Time:Date/Time,
z q }
Received by/Company: {Signature]
/ u
I Z
-3`2�
MTJL LAB USE ONLY
Table
Acctnt=
Prelogine
pM;
PM
Relinquished by/Company: (signature)
JGDI
Date/Tim ,�.,?;3
Re e' ` /Company; (Signature)
(JJ LI 3 • Z �
D t{o//Time:
16 ,
Trip Blank Received; Y N NA
HCL McOH TSP Other
/Co p%an?y: (Signature)
7�wr"f J - 2�
Date/Time:
Rece/i{}ve`d�-by/Company: (Signature)
I I y
Date/Time:
Non Confarmance(s):
YES / NO
Page: Pa�P 99 of 1
of:

LIMS73 Lab Sample Condition Upon Receipt (West Virg WO# ; 30574814
'�'caAt t cal PM: CEW Due Date: 04/13/23
Client Name:i,Lrr.�-,�k CLIENT: INFRAMARK
Courier: ❑ Fed Ex ❑ UPS ❑ USPS 0client ❑ Commercial ❑ Pace L. umer:
Tracking #:
Custody Seal on CoolerIBo),JContainers Present: ❑ yes Xno Seals intact: ❑ yes ❑ no
Thermometer Used L'�'Tl" z4J Type of Ice: We Blue None
Cooler Temperature Observed Temp j : 2 C Correction Factor:. C Final Temp: C
Comments: pH paper Lot# Date and Initials of person examining
contents:
Yes
No
NIA
Chain of Custody Present:
1.
Chain of Custody Filled Out:
2.
Chain of Custody Relinquished:
f
/
1
Sampler Name & Signature on COC:
%
4.
Sample Labels match COC:
-Includes dateibme/ID Matrix:
5.
Samples Arrived within Mold Time:
6.
Short Hold Time Analysis (<72hr remaining):
7.
Rush Turn Around Time Requested:
/
/
8.
Sufficient Volume:
9.
Correct Containers Used:
-Pace Containers Used:
10.
Containers Intact:
Orthophosphate field filtered:
12.
Hex Cr Aqueous sample field filtered:
-pH adjusted within 24 hours? (If yes, indicate acid lot #)
/
13.
Filtered volume received for Dissolved tests:
14.
All containers have been checked for preservation:
exceptions: VOA, coliform, O&G, LLMercury, Non -aqueous matrix
Al] containers meet method preservation requirements:
15.
Initial when f ��/?
completed 1 t/�'
Date/time samples
provided to tab rU
Tests not preserved:
Headspace in VOA Vials:
16,
Trip Blank Present:
Trip Blank Custody Seals Present:
%
17.
Initial w en i
completed: 1G�
Dater~ —z3
Client Notification! Resolution:
Person Contacted:
Comments/ Resolution:
Date/Time:
Contacted By:
❑ A check in this box indicates that additional information has been stored in ereports.
"PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section
of the Workorder Edit Screen.
A,
0
SCU R_W V - rev.082219

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Report Date: 7/6/2023
Date Sample Rcvd: 5/23/2023
Vector Attraction Reduction L Aerobically Digested Sludge 30 Day Test)
Meritech Work Order # 05232336 Sample: Danville #1 Composite 5/23/23
Total Solids Watile Solids % Volatile Solids
Week 1 1.25 0.64 0.512
Week 2,
1.17
0.61
0.520
Week 3.
1.06
0.56
0.528
Week 4
1.00
0.54
0.538
Week 5
0.98
0.52
0.527
Van Kleek Reduction (%): -6.24
I hereby certify that I have reviewed and approve these data.�dq���(X pC�
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

-n w .CDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2015
lyst: B - A x 100 = % TOTAL SOLIDS
C
Irded By: _ F---Clean IN 550°C Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
�I C
1st Sample IN 104°C — 1st Sample OUT 104°C 1st Sample IN 550°C Ist Sample OUT 5500C
2nd Sample IN 104°C 2nd Sample OUT 104°C I 2nd Sample IN 550°C 2nd Sample OUT 550°C
C A B
Dry Wt Diff
SAMPLE
USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
final -initial
% TOT SOLIDS
I
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
SAMPLE
g USED
DISH #
TARE WT. W
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
(initial ignition 550°C for I hour)
(repeat iginition 550°C for I hour)
D
Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
�1sstteI-gnition
O / 5
r:
SAMPL
g USED
DISH #
TARE WT.
1st Dry Wt
2nd DrX Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for I hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WtDiff
(final -initial)
% VOL SOLIDS
Dry Wt Diff
SAMFkE
U Ejp
DISH #
TARE WT. W
1st Dry Wt
2nd D Wt
final -initial
% TOT SOLIDS
-
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
I D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
t

SM 2540 B-2015
Analyst:
Date: '� C�
Recorded By: `" J FClean IN 5500C Clean OUT 550°C
1st Sample IN 104°C 1st Sample OUT 104°C
2nd Sample IN 1040C ZaLsamzac OUT 104°C
C A
B=A_ x 100 = % TOTAL SOLIDS
C
B - D x 100 = % VOLATILE SOLIDS
C
1 st Sample IN 550°C 1 st Sample OUT 5500C
2nd Sample IN 5500C 2nd Sample OUT 550°C
R
SAMPLE
g USED
DISH #
TARE WT. W
1st Dry Wt
2nd Dry Wt W
Dry Wt Diff
(final -initial)
% TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
0
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff I
(final -initial) I % VOL SOLIDS
SAMPLE
g USED
DISH #
TARE WT. )
1st Dry Wt W
2nd Dry Wt (g
Dry Wt Diff
final -initial)
% TOT SOLIDS
s ,
,a�a
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
SAI iI'LE
g USED
DISH #
TARE WT. (
1st Dry Wt 10
2nd Dry Wt ( )
Dry Wt Diff
(final -initial)
%TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
ro
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(renal -initial)
% VOL SOLIDS
SAMP E
g USED
DISH #
TARE WT. g
1st Dry Wt
2nd Dry Wt g)
Dry Wt Diff
final -initial
% TOT SOLIDS
NJ
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 1 hour)
0
1st Ignition Wt (g)
2nd Ignition Wt )
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
-� a
i

Date- % '(fy J
Recorded By: Clean IN 550°C Clean UT 550°C
1st Sample IN 104°C Ist Sample OUT 104°C
2nd Sample IN 104°C 2nd Sample OUT 104°C
c ki
B - A_ x 100 = % TOTAL SOLIDS
C
B - D x 100 = % VOLATILE SOLIDS
C
lst Sample IN 5500C 1st Sample OUT 5500C
2nd Sample IN 5500C 2nd Sample OUT 550°C
n
SAMPLE
g USED
DISH #
TARE WT. W
1st Dry Wt
2nd Dry Wt
Dry WtDiff
(final -initial)
% TOTSOLIDS
oS2 3 2 3_ 3 e 1
3951�
l3
- 033
��_ 2c
5 -20
D
Ignite Wt Diff
(initial ignition 550"C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) (final -initial) % VOL SOLIDS
(repeat iginition 550°C for 1 hour) S 6 - // 9 56- l / U q
SAMPLE
USED
DISH # TARE WT. Q 1st Dry Wt (2) 2nd Dry Wt (9)
Dry Wt Diff
(final -initial)
% TOT SOLIDS
L -l1I
o
59.5qo 9.7335
L5q.73 35
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff j
(final -initial) % VOL SOLIDS
754
'59
SAMPLE
g USED
DISH #
TARE WT. (2)
15t Dry Wt (g)
2nd Dry Wt (a)
Dry Wt Diff
(final -initial)
% TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
Ignite Wt Diff
1st Ignition Wt (g) 2nd Ignition Wt (g) (final -initial) % VOL SOLIDS
143 3 U 1U7-6 3 3 u
SAiVPLE L_ USED
DISH #
TARE WT. ) { 1st Dr Wt W 2nd Dry Wt W
Dry Wt Diff
final -initial)
% TOT SOLIDS
Iq-13 c
l d/5
1,5100 53,011 53Yu I I
�-
D
Ignite Wt Diff
(initial ignition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) (final -initial) % VOL SOLIDS
(repeat iginition 550°Cfor 1 hour) 1,i' 5 3

Analyst: _
Date:
Recorded By: T'
SM 2540 B-2015 /
/ B - A x 100 = %TOTAL SOLIDS
Clean IN 550°C Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
C
Ist Sample IN 104°C 1st Sample OUT 104°C Ist Sample IN 550°C Ist Sample OUT 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C 2nd Sample IN 550°C 2nd Sample OUT 550°C
C A B
Dry W t Diff
SAMPLE
USED
DISH r#
TARE WT.
1st D Wt
2nd Dr Wt
final -initial)
% TOT SOLIDS
(initial ignition 550°C for I hour)
(repeat iginition 550°C for I hour)
D
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
O
SAMPLE)
Q USED
DISH #
TARE WT. (
1st Dry W t
2nd Dry Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
3
35
l
t3
d
(initial ignition 550°C for I hour)
(repeat iginition 550°C for I hour)
SAMPLE
{
I USED
DISH it
TART: WT.
)
(initial ignition 550°C for I hour)
(repeat for I hour)
SAMPLE
e USED
�550°C
�iginition
DII SH k
TARE, WVT
D
Ist Ignition Wt (g)
Ignite Wt Diff
2nd Ignition Wt (g) (final -initial)
% VOL SOLIDS
_-
Dry Wt Diff
Dr Wt ( final -initial) % TOT SOLIDS
t�
D
Ist Ignition Wt ()
2nd Ignition Wt ()
gnite Wt Diff
(final -initial)
% VOL SOLIDS
-3
u�•3�
Ist Dry Wt ° 2nd Dr
D
Dry Wt Diff
final -initial % TOT SOLIDS
�o
Ignite Wt Diff
(initial ignition 550°C for I hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) (final -initial) % VOL SOLIDS
(repeat iginition 550°C for I hour) 36.712(

d

L9-2016 Chain of Custody Record (COC)
NPDES#:
Client: EMA Resources Inc. Phone:_ 336-751-1441
Address: 755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email: [e-mail]
Project:
P.O.#:
Attention:_ Brent Collins Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that applxgz eferred) , Fax, Mail S L10 days) 3 - 5 Days 2Ors
l J l
JUSe
ME R ITE C H INC.
1
\ ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
- Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample (Sign/Print): :7
�� Orsnr �l/,�,,5
Lab 011� y
Start
End
Go b?
Cont.
Test(s) Required
On Ice?
Yes / No
H OK?
Cl OK?
Date
Time
Date
Time
S-1L3
5. D $
C
j
30 Day Bench Digestion
Temperature Upon
Receipt: C —
t
Method of
Shipment:
"` Dechlorination (c0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples
must be done in the field prior to preservation. ***
Comments:
Please send calculation sheets with results
Compositor #
Jug #
UPS
❑ Fed Ex
Are these results for regulatory purposes? Yes IR'- No ❑
Report results in: mg/L ❑ mg/kg G''� ug/L ❑
❑ Hand Delivery
Relinquished by: t.�/ Date: Time: �D
% �
Received by: Date: Time:
❑ Other
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Received a Date;(_., TMf-]".

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Danville WQ Permit Number: WQ0036561
WWTP Name:
Northside WWTP
NPDES Number: VA0060593
Monitoring Period: From 4/18/2023 To 4/18/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) ❑
A1t.D (No Prior Test)
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAlt. (1) Fecal Density El
7AIt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
JAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
'Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximud
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
239
268
323
CFU/ g
0
Quarterly
l
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) v
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Alan Gould - Project Manager
Preparer Name and Title (type or print)
e
Ala 6, 202412:35 EST)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
26/01 /2( d-Y
1/21/2024
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
April 26, 2023
Kimberly Wickemeyer
Inframark
229 Northside Drive
Danville, VA 24540
RE: Project: VA0060593
Pace Project No.: 30579756
Dear Kimberly Wickemeyer:
Enclosed are the analytical results for sample(s) received by the laboratory on April 18, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Beaver
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cynthia Walker
[e-mail]
[phone]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
CERTIFICATIONS
Project: VA0060593
Pace Project No.: 30579756
Pace Analytical Services Beaver
225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466
Virginia VELAP 460148 Kentucky Wastewater Certification KY90039
West Virginia DEP 060 Pennsylvania DEP 68-00839
West Virginia DHHR 00412CM
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE SUMMARY
Project: VA0060593
Pace Project No.: 30579756
Lab ID
Sample ID
Matrix
Date Collected
Date Received
30579756001
A BASIN #1
Solid
04/18/23 08:00
04/18/23 15:30
30579756002
A BASIN #2
Solid
04/18/23 07:30
04/18/23 15:30
30579756003
A BASIN #3
Solid
04/18/23 07:55
04/18/23 15:30
30579756004
A BASIN #4
Solid
04/18/23 07:35
04/18/23 12:00
30579756005
A BASIN #5
Solid
04/18/23 07:50
04/18/23 12:00
30579756006
A BASIN #6
Solid
04/18/23 07:40
04/18/23 12:00
30579756007
A BASIN #7
Solid
04/18/23 08:05
04/18/23 12:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
VA0060593
30579756
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
30579756001
A BASIN #1
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30579756002
A BASIN #2
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30579756003
A BASIN #3
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30579756004
A BASIN #4
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30579756005
A BASIN #5
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30579756006
A BASIN #6
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30579756007
A BASIN #7
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
PASI-BV = Pace Analytical Services - Beaver
PASI-LE = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30579756
Sample: A BASIN #1 Lab ID: 30579756001 Collected: 04/18/23 08:00 Received: 04/18/23 15:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.1 % 0.10 1 04/21/23 10:33 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 257 0.257 04/19/23 07:30 04/20/23 08:30
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30579756
Sample: A BASIN #2 Lab ID: 30579756002 Collected: 04/18/23 07:30 Received: 04/18/23 15:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 95.8 % 0.10 1 04/21/23 10:35 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 239 0.239 04/19/23 07:30 04/20/23 08:30
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30579756
Sample: A BASIN #3 Lab ID: 30579756003 Collected: 04/18/23 07:55 Received: 04/18/23 15:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.3 % 0.10 1 04/21/23 10:45 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 271 0.271 04/19/23 07:30 04/20/23 08:30
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30579756
Sample: A BASIN #4 Lab ID: 30579756004 Collected: 04/18/23 07:35 Received: 04/18/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.9 % 0.10 1 04/21/23 10:09 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 323 0.323 04/19/23 07:30 04/20/23 08:30
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30579756
Sample: A BASIN #5 Lab ID: 30579756005 Collected: 04/18/23 07:50 Received: 04/18/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 95.8 % 0.10 1 04/21/23 10:12 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 239 0.239 04/19/23 07:30 04/20/23 08:30
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30579756
Sample: A BASIN #6 Lab ID: 30579756006 Collected: 04/18/23 07:40 Received: 04/18/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.4 % 0.10 1 04/21/23 10:23 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 278 0.278 04/19/23 07:30 04/20/23 08:30
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30579756
Sample: A BASIN #7 Lab ID: 30579756007 Collected: 04/18/23 08:05 Received: 04/18/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.4 % 0.10 1 04/21/23 10:24 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform ND CFU/g 278 0.278 04/19/23 07:30 04/20/23 08:30
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALIFIERS
Project: VA0060593
Pace Project No.: 30579756
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 04/26/2023 12:03 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: VA0060593
Pace Project No.: 30579756
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
30579756001
A BASIN
#1
SM
2540G-15
582594
30579756002
A BASIN
#2
SM
2540G-15
582594
30579756003
A BASIN
#3
SM
2540G-15
582594
30579756004
A BASIN
#4
SM
2540G-15
582594
30579756005
A BASIN
#5
SM
2540G-15
582594
30579756006
A BASIN
#6
SM
2540G-15
582594
30579756007
A BASIN
#7
SM
2540G-15
582594
30579756001
A BASIN
#1
SM
9222D-2015
582309
SM
9222D-2015
582310
30579756002
A BASIN
#2
SM
9222D-2015
582309
SM
9222D-2015
582310
30579756003
A BASIN
#3
SM
9222D-2015
582309
SM
9222D-2015
582310
30579756004
A BASIN
#4
SM
9222D-2015
582309
SM
9222D-2015
582310
30579756005
A BASIN
#5
SM
9222D-2015
582309
SM
9222D-2015
582310
30579756006
A BASIN
#6
SM
9222D-2015
582309
SM
9222D-2015
582310
30579756007
A BASIN
#7
SM
9222D-2015
582309
SM
9222D-2015
582310
Date: 04/26/2023 12:03 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 15

CHAIN -OF -CUSTODY Analytical Request Document
�aciqAnalXical'
Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields
LAD USE0' �/� 3057975fi nberor
V
II I III III III I IIII II III
Container 30579756
U1 1
Company:
I nframark- Danville
Billing Information:
Inframark-Danville WWTP
229 Northside Drive
Danville, VA 24540
Address: 229 Northside Dr., Danville, VA 24540
Report To: [e-mail]
Email To: [e-mail]
"Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thlosulfate, (9) hexane, (A) ascorbic acid, (B) ammonium sulfate,
(C) ammonium hydroxide, (D)T5P, (U] Unpreserved, (0) Other
Copy To : Kimberly.WlCi<[e-mail]
S Collection Info/Address:
Danville VA WWTP 229 Nonhside, Dr., Danville, VA 24540
Analyses
lLab Profile/Line:
Customer Project Name/Number;
Inframark-Danville (client #: 92-618203)
State: County/City; Time Zone Collected:
VA /Danville [ ] PT [ ] MT [ I CT :VET
U
V1
�-
[p
E
t�f3
v
E
"=
(,
U
N
U_
Lab Sample Receipt. checklist:
Custody Seals Present/Intact Y N NA
Custody signatures Present Y N NA
Collector Signature Present Y N NA
Bottles Intact Y N NA
Correct Bottles Y N NA
Sufficient Volume Y N NA
Samples Received on Ice Y N NA
Acceptable Y N NA
VOA - Regulated
USDA Regulated Soils X N NA
Samples in Holding Time Y N NA
Residual chlorine Present Y N NA
SCI ample table Y N NR
p pH Acceptable
pH Stripa;
Sulfide Present Y N NA
Lead Acetate Strips:
LAB USE ONLY:
Lab Sample. 4 ! Comments:
Phone:[phone]
Email: kimbeny.,[e-mail]
Site/Facility ID #:
Danville, VA WWTP permit VA0060593
_
Compliance Monitoring?
[ WYes [ ] No
Collected By (print):
Robert Clifton
Purchase Order #; 152847
quote #: 00128560
DW PWS ID #:
OW Location Code:
Colle ed B si na ure :
f g �—v
Turnaround Date Re wired:
results by b510212023
Immediately Pace on Ice;
{IV yes ( ] No
Sample Disposal:
jt� Dispose as appropriate [ ] Return
I I Archive:
] ]Hold:
Rush:
I ] Same Day [ ] Next Day
[ ] 2 Day [ ] 3 Day [ ] 4 Day [ ] 5 Day
(Expedite Charges Apply)
Field Filtered (if applicable):
[ ) Yes j/J No
Analysis:
• Matrix Codes (insert in Matrix box below); Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor {V), Other (OT)
Customer Sample ID
Matrix *
Comp /
Grab
Collected (or
Composite Start)
Composite End
Res
Cl
# of
Ctns
Date
I Time
Date
Time
Basin #1
SL*
JGrab
04/18/23
680(D
__ --
----
No
1
Basin #2
SL*
Grab
04/18/23
0?50
----
----
No
1
Basin #3
SL*
Grab
4118123
pZsS
----
----
No
1
A Basin #4
SL*
Grab
04/18/23
073
----
----
No
1
Basin #5
SL*
Grab
04/18/23
[)7750
----
----
No
1
Basin #6
SL*
Grab
04118/23
1 ()7 YC)
_ _ _ _
_ - _ _
No
1
Basin #7
SL*
Grab
04/18/23
6) VD
- - - -
- - - -
No
1
Customer Remarks / Special Conditions / Possible Hazards:
'Biosolids for Fecal Coliform
Type of Ice Used: Wet Blue Dry None
SHORT HOLDS PRESENT (<72 hours):
Y N N/A
Lab Sample Temperature Info:
Temp Blank R C IYe JNA
Therm 109:
Cooler 1 Temp Upon Recelpt:QLU oC
Cooler 1 Therm Corr. Factor:D_�__oC
Cooler 1 Corrected Temp: oc
Comments:
Packing Material Us •
Lab Tracking #:
Radchem sample(s) screened (<500 cpm): Y N NA
Samples received via:
FEDFX UPS Client Courier Pace Courier
Relinquished by/Company: (Signature)
n / f��
!aI r�r�
Date/Time:
1
%"r�_�i
Received by/Compan : re}
Date/Timel 1 ,[ ,
I t
MTJL LAO USE ONLY
Tabletl:
Accinum:
cctn
Relinquished by/Com an : (Signature)
Date/Tim
lY !U1
Recelved by�Company: Signature)
" Ly 4 �,�
�r1J
Date Ime:
�/�/1
Template:
Prelogin:
PM:
PB:
Trip Blank Received: Y N NA
HCL McOH TSP Other
—"" --Page 14 off
Non Conformance(s); I Page:
YES / NO of:
Relln d by/Com any: (Signature)
Q� 7
Z f y
Date/Time:
Received by/Company: (Signature)
Date/Tlme:

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Page 15 of 15

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
w
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Report Date: 7/6/2023
Date Sample Rcvd: 5/23/2023
Vector Attraction Reduction Aerobically Digested Sludge 30 Day Test
Meritech Work Order # 05232337 Sample: Danville #2 Composite 5/23/23
Total Solids Volatile Solids % Volatile Solids
Week 1 1.88 0.97 0.519
Week 2
1.52
0.78
0.513
Week 3.
1.39
0.72
0.522
Week 4
1.33
0.70
0.529
Week 5
1.43
0.75
0.521
Van Kleek Reduction (%): -0.82
I hereby certify that I have reviewed and approve these data.�nd�Nq��Lp��t
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Analyst:_ INA1
Date:
Recorded By: 3
1st Sample IN 104'C
2nd Sample IN 104°C
C
'AT' SPZZDS%`PF.RcF.NT V(7T.ATTC.F SOLIDS
SM 2540 B-2015
B!A x 100 = % TOTAL SOLIDS
C
Clean IN 5500C Clean OUT 5500C B - D x 100 = % VOLATILE SOLIDS
C
_ 1st Sample OUT 1040C 1st Sample IN 5500C 1st SampleOUT 5500C_
2nd Sample OUT 1040C 2nd Sample IN 550'C 2nd Sample OUT 5500C
A B
SAMPLE
USED
DISH #
TARE-WT. W
1st Dry Wt
2ndD Wt
Dry Wt Diff
(final -initial)
%TOTSOLIDS
I
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
SAMPLE
USED
DISH t#
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
ry'
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
(initial ignition 550'C for 1 hour)
(repeat iginition 550°C for 1 hour)
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
1st Ignition Wt (g)
2nd Ignition Wt (g)
IgniteWtDiff
(final -initial)
I % VOL SOL IDS
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
i
�
1
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS

Analyst:-
Date:
Recorded By:
/ B - A x 100 = % TOTAL SOLIDS
v/ C
Clean IN 5500C Clean OUT 5500C B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 104°C 1st Sample OUT 104°C 1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C 2nd Sample IN 550°C 2nd Sample OUT 5500C
C A R
SAMPLE
USED
DISH#
TARENVT.
1st Dry Wt )
2nd Dry Wt )
Dry Wt Diff
final -initial
%TOTSOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
Ignite Wt Diff
1st Ignition Wt (g)
2nd Ignition Wt (g)
(final -initial)
% VOL SOLIDS
Dry Wt Diff
Dry Wt Diff
SANLP
E
o USED
DISH #
TARE )VT.
1st Drx Wt
2nndd D Wt
final -initial)
% TOT SOLIDS
�i
t4t t
I
v
-
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
USED I DISH # 1 TARE Wr.
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
I]
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
Dry Wt Diff
Wt W (final -initial %TOT SOLIDS
D
1st Ignition Wt (g)
I 2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
SANLPLE
I g USED
DISH #
TARE WT. (p)
1st Dry Wt (e
2nd Dry Wt O
Dry Wt Diff
final -initial)
% TOT SOLIDS
i5
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
111
1st Ignition Wt (g)
2nd Ignition Wt )
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
N6�5
,1*.
0.
QL

SM 2540 B-2015
Analyst: I
Date:
Recorded By: Clean IN 550°C Clean OUT 550°C
F1st Sample IN 104°C 1st Sample 104°C 1st Sample IN 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C 2nd Sample IN 550°C
C A
B - A_ x 100 = % TOTAL SOLIDS
C
B - D x 100 = % VOLATILE SOLIDS
C
1st Sample OUT 550°C
2nd Sample OUT 550°C
B
Dry Wt Diff
SAMPLE
USED
DISH #
TARE WT. {)
1st Dry Wt [�}
2nd Dry 4Vt
(final -initial)
%TOT SOLIDS
052323- � Q 2
I -99�
C3
l.0126
5/,3_
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Iwvnite Wt Diff
(final -initial)
% VOL SOLIDS
51430
503c 2
c
671,
Dry Wt Diff
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt g
(final -initial)_) % TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
u
d4 919
L?&
SAMPLE
I g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt W
Dry Wt Diff
(final -initial)
%TOT SOLIDS
c
. I-
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 1 hour)
D
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(F�alfinal�niriall
% VOL SOLIDS
c►
;�_7
SAMP
USED
DISH #
TARE WT. O
1st Dry Wt
2nd Dry Wt )
Dry Wt Diff
'final -initial)
%TOT SOLIDS
F
Nq'•
56
0 S 54
C,
,3
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
-11?-5 I
uF_53-)
C
iGIR-3

SM 2540 B-2015
Analyst: _ � B - A_ x 100 = %TOTAL SOLIDS
Date: �~I C
Recorded By: l(p Clean IN 550°C Clean OUT 550°C BBD x 100 = % VOLATILE SOLIDS
C
1st Sample IN 104°C _ 1st Sample OUT 104°C 1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C 2nd Sample IN 550°C 2nd Sample OUT 550°C
C A B
SAMPLE
USED
DISH #
TARE WT. ( 1st Dry Wt )
2nd Dry Wt
Dry Wt,Diff
final -initial
% TOT SOLIDS
p
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
21-6 7
2i-676--1
b
SAMPLE
>r USED
DISH #
L-kRf WT. (g)
Ist Dr_v Wt e)
god Dr Wt (g)
Dry Wt Diff
(final -initial)
%TOT SOLIDS
her
o
11� I 9 -K
_ e-1
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 1 hour)
D
ISE Ignition Wt (g)
Ignition Wt
tt1(g)
Ignite Wt Diff
(final -initial)
f % VOL SOLIDS
r72nd
SAMPL
I g USED
DISH #
TARE WT. (g)
1st Dry VVt (g)
2nd Dry Wt (2)
Dry Wt Diff
(final -initial)
% TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
I 2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
12 I- 2
I V i 2
Dry Wt Diff
I
SA1YIP E
g USED
DISH #
TARE WT. (Q)
1st Dry Wt (g)
2nd Dry Wt (g)
{final -initial)
% TOT SOLIDS
q
3
U W U
1E
t
e
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
I % VOL SOLIDS

vERCENT TOTAL SOLIDS / PERCENT VOLAT SOLIDS
SM 2540 B-2015
Analyst:.'Z B - A- x 10 0 = % TOT AL SOLIDS
Date: C
Recorded By: an IN 550°C Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 1040C Ist Sample OUT 1040C 1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C 2nd Sample IN 5500C 2nd Sample OUT 5500C
C A R
SAMPLE
USED
DISH #
TARE WT.
1st Dr Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
%TOT SOLIDS
o5'Z_�23_37 anvi P,9Z
H.00dc
1.5
13q•2
�`li ' 1 11
(initial ignitioo 550°C for I hour)
(repeat iginition 550°C for i hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WtDiff
(fr:al -initial]
i
% VOL SOLIDS
39.1i079
3�7.uc 9
0
::..r b
Dry WtDiff
SAMPLE
g USED
DISH #
TARE WT. E)
1st Dr W t (e
2nd Dr Wt f)
(final -initial)
% TOT SOLIDS
I �?q
o-
L2
1�y1�� ^
1,U q
i4vsla
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WtDiff
(final -initial)
% VOL SOLIDS
ill -� -177
a/,2�77-
C
s:645
SANIPL
g USED
DISH #
TARE WT. (eZ_
1st Dry Wt (g)
2nd Dry Wt(e)
Dry Wt Diff
(final -initial
% TOT SOLIDS
I 3 VZ
sn
_
3� '7155
;9 �' 14`��
-'��
(initial ignition 550"C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial) % VOL SOLIDS
-3 1, �'2 7c
3 9-V �r
P i : t� q
SANtYLE g USED
DISH #
TARE WT. (g)
1st Dry Wt (2)
2nd Dry Wt (g)
Dry W t Diff
(final -initial)
L.". TOT SOLIDS
I�- I55
)
3 457 N
In i
b
D
Ignite WtDiff
(initial ignition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) I (final -initial) % VOL SOLIDS
(repeat iginition 550'C for 1 hour) j C 3 6 •Z T C o

59101fi
Chain of Custody Record (COC)
NPDES#:
lient: EMA Resources Inc. Phone:-336-751-1441
Address:_ 755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email:_ hront rouingeemaresourcesinc.com
Project:_
P.O.#:
Turn Around Time'
Attention:_ Brent Collins *RUSH work needs prior approval.
How would you like your report sent?
Std110da s) 3-5 Da s ?a-A2Hrs
Circle all that apply: Email eferred) , Fax, Mail I— ---� ❑—�
Person Taking Sample (Sign/Print): 2 , Lab Use Only
MERITECH 1 INC.•
ENVIRONMENTAL LABORATORIES
642TamcoRd. Phone: [phone]
Reidsville INC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates & Times
P g
Start
End
Comp?
Grab?
aof
Cont.
Test(s)
on Ice?
on Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
III
l� Z
61123
91 IS
c
j
30 Day Bench Digestion '3
C
Temperature Upon
Receipt: 1),4 1,L
Method of
Shipment:
'Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. "`
Comments:
Please send calculation sheets with results
tor #
posit
Coposi
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes
No ❑
Report results in: mg/L ❑ mg/kg � ug/L ❑
Received by: Date: Time:
Received by: Date: Time:
❑ Hand Delivery
Relinquished by: Date:
Time:
�l �G
❑ Other
Relinquished by: Date:
Time:
Relinquished by: Date:
Time:
Rece" y Lab: t Time: rG
OR

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Danville WQ Permit Number: WQ0036561
WWTP Name: Northside WWTP NPDES Number: VA0060593
Monitoring Period: From 5/1/2023 To 5/1/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
I Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
He Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAlt. (1) Fecal Density El
FAlt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
JAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number of
Excee-
dences
Frequency
of Analysis
Sample
'Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximud
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
<10
<10
<10
col/ g
0
Quarterly
l
G
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Alan Gould -Project Manager
Preparer Name and Title (type or print)
e
Ala 6, 202412:35 EST)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
26/01 /2 ( ;d-i 1/30/2023
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
May 12, 2023
Kimberly Wickemeyer
Inframark
229 Northside Drive
Danville, VA 24540
RE: Project: DANVILLE VA0060593
Pace Project No.: 30583218
Dear Kimberly Wickemeyer:
Enclosed are the analytical results for sample(s) received by the laboratory on May 01, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Beaver
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cynthia Walker
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
CERTIFICATIONS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Pace Analytical Services Beaver
225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466
Virginia VELAP 460148 Kentucky Wastewater Certification KY90039
West Virginia DEP 060 Pennsylvania DEP 68-00839
West Virginia DHHR 00412CM
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

aceAnalytical
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Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE SUMMARY
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Lab ID
Sample ID
Matrix
Date Collected
Date Received
30583218001
A BASIN #1
Solid
05/01/23 07:30
05/01/23 12:00
30583218002
A BASIN #2
Solid
05/01/23 07:35
05/01/23 12:00
30583218003
A BASIN #3
Solid
05/01/23 07:40
05/01/23 12:00
30583218004
A BASIN #4
Solid
05/01/23 07:45
05/01/23 12:00
30583218005
A BASIN #5
Solid
05/01/23 07:50
05/01/23 12:00
30583218006
A BASIN #6
Solid
05/01/23 07:55
05/01/23 12:00
30583218007
A BASIN #7
Solid
05/01/23 08:00
05/01/23 12:00
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 15

aceAnalytical
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Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
DANVILLE VA0060593
30583218
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
30583218001
A BASIN #1
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30583218002
A BASIN #2
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30583218003
A BASIN #3
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30583218004
A BASIN #4
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30583218005
A BASIN #5
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30583218006
A BASIN #6
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30583218007
A BASIN #7
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
PASI-BV = Pace Analytical Services - Beaver
PASI-LE = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Sample: A BASIN #1 Lab ID: 30583218001 Collected: 05/01/23 07:30 Received: 05/01/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 95.9 % 0.10 1 05/05/23 11:53 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Sample: A BASIN #2 Lab ID: 30583218002 Collected: 05/01/23 07:35 Received: 05/01/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.8 % 0.10 1 05/05/23 11:56 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Sample: A BASIN #3 Lab ID: 30583218003 Collected: 05/01/23 07:40 Received: 05/01/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.9 % 0.10 1 05/05/23 12:47 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Sample: A BASIN #4 Lab ID: 30583218004 Collected: 05/01/23 07:45 Received: 05/01/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 98.7 % 0.10 1 05/05/23 12:47 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Sample: A BASIN #5 Lab ID: 30583218005 Collected: 05/01/23 07:50 Received: 05/01/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 97.1 % 0.10 1 05/05/23 12:48 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Sample: A BASIN #6 Lab ID: 30583218006 Collected: 05/01/23 07:55 Received: 05/01/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 96.5 % 0.10 1 05/05/23 12:49 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Sample: A BASIN #7 Lab ID: 30583218007 Collected: 05/01/23 08:00 Received: 05/01/23 12:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture 97.0 % 0.10 1 05/05/23 12:50 N2
LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALIFIERS
Project: DANVILLE VA0060593
Pace Project No.: 30583218
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/12/2023 03:20 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: DANVILLE VA0060593
Pace Project No.: 30583218
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
30583218001
A BASIN
#1
SM
2540G-15
586021
30583218002
A BASIN
#2
SM
2540G-15
586021
30583218003
A BASIN
#3
SM
2540G-15
586021
30583218004
A BASIN
#4
SM
2540G-15
586021
30583218005
A BASIN
#5
SM
2540G-15
586021
30583218006
A BASIN
#6
SM
2540G-15
586021
30583218007
A BASIN
#7
SM
2540G-15
586021
30583218001
A BASIN
#1
SM
9222D-2015
585394
SM
9222D-2015
585499
30583218002
A BASIN
#2
SM
9222D-2015
585394
SM
9222D-2015
585499
30583218003
A BASIN
#3
SM
9222D-2015
585394
SM
9222D-2015
585499
30583218004
A BASIN
#4
SM
9222D-2015
585394
SM
9222D-2015
585499
30583218005
A BASIN
#5
SM
9222D-2015
585394
SM
9222D-2015
585499
30583218006
A BASIN
#6
SM
9222D-2015
585394
SM
9222D-2015
585499
30583218007
A BASIN
#7
SM
9222D-2015
585394
SM
9222D-2015
585499
Date: 05/12/2023 03:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 15

it IAiL AAr/tiww�
CHAIN -OF -CUSTODY Analytical Request Document
aceAnalytical
Chain -of -Custody is a LEGAL DOCUMENT -Complete all relevent fields
LAB Us[ w�/* • �Vumberor
30583218
Container Preservative Type " wu r-. J«,
U
company` [nframark�Danville
Billing Information:
Inframark-Danville WWTP
229 Northside Drive
Danville, VA 24540
Address: 229 Northside Dr., Danville, VA 24540
ReportT°` [e-mail]
Email To: allcla,[e-mail]
"Preservative
(6) methanol,
(C) ammonium
Types: (1)
(7) sodium
hydroxide,
nitric acid, (2)
bisulfate, (a) sodium
(D) TSP, (U) Unpreserved,
sulfuric
acid, (3) hydrochloric acid, (4) sodium hydroxide, JS) zinc acetate,
thiosulfate, (9) hexane, [A) ascorbic acid, (B) ammonium sulfate,
(0) other
Copy TO: [e-mail]
Site Collection Info/Address:
Danville VA WWTP 229 Northside, Dr., Danville, VA 24540
Analyses
Lab Profile/Line:
Customer Project Name/Number:
Inframark-Danville (client #: 92-618203)
State: County/City: Time Zone Collected,
VA /Danville [ ]PT( ]MT( ] CT VET
U
;,_,
In
@
0-
(1)
fn
J
c
C
lL0
u
E
IP
O
0
0
ILL
Lab Sample Receipt Checklist;
Custody Seals Present/Intact Y N NA
Custody Signatures Present Y N NA
Collector Signature Present Y N NA
Bottles Intact Y N NA
Correct Bottles Y,N NA
sufficient Volume Y N NA
Samples Received on Ice Y N NA
VOA - Headspace Acceptable Y N NA
USDA Regulated Soils Y N NA
Samples in Holding Time Y tJ NA
Residual chlorine Present Y N NA
0 Strips;
Sample pH Acceptable Y N NA
pH strips;
Sulfide Present Y N NA
Lead Acetate strips:
LAB USE ONLY:
Lab sample J / Comments:
Phone:[phone]
Email: [e-mail]
Site/Facility ID M
Danville, VA WWTP permit VA0060593
Compliance Monitoring?
[ Oes [ ] No
Collected By (print):
Robert Clifton
Purchase Order #: 152847
Quote #: 00128560
DW PWS ID #:
DW Location Code:
Coll ted By (si natur ]:
C i
Turnaround Date Required:
results by 05/16/2023
mme iate y Pace on Ice:
Immediately
s/
16yes ( lNo
Sample Disposal:
[✓I Dispose as appropriate [ ] Return
[ ] Archive:
[ ] Hold:
Rush:
[ j Same Day [ ] Next Day
[ ] 2 Day ( ] 3 Day [ ] 4 Day [ ] 5 Day
(Expedite Cha m A I
pPY)
Field Filtered (if applicable):
[ ] Yes J4 No
Analysis:
* Matrix Codes (Insert in Matrix box below]: Drinking Water (DW), Ground Water (GW), Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bloassay (B), Vapor (V), Other (OT)
Customer Sample ID
Matrix *
Comp /
Grab
Collected (or
Composite Start)
Composite End
Res
Cl
# of
Ctns
Date I
Time
Date
Time
Basin #1
SL*
Grab
05/01/23
0730
- - - -
- - - -
No
1
Basin 42
SL*
Grab
05/01123
0735
- - - -
- - - -
No
1
Basin #3
SL*
Grab
05/01123
7
----
----
No
1
A Basin #4
SL*
Grab
05/01123
0745
----
----
No
1
Basin #5
SL*
Grab
05/01/23
0750
- - - -
- - - -
No
9
Basin #6
SL*
Grab
05/01/23
0755
- - - -
- - - -
INO
1
Basin #7
SL*
Grab
05101/23
----
----
No
1
Customer Remarks/ Special Conditions/ Possible Hazards:
for Fecal Coliform
Typo of Ice Used: Wet Blue Dry None
SHORT HOLDS PRESENT [02 hours]: Y
N N/A
Lab Sample Temperature Info:
TempB'anky,:,e',, .Y) NA
Therm IDIP�`Biosolids
Cooler 1 Ten Receipt: - oC
Cooler 1 Therm Corr. Factor:0 , [ oC
Cooler 1 Corrected Temp: `-q—ac
Comments:
Packing Material
Lab Tracking #:
Radchem sample(s) screened (<S00 cam); Y N NA
Samples received via:
FEDEX UPS Client Courier Pace Courier
Rel[ quishjed by/Company: (Signature)
WIZ.
�tani2
Date/Time:
51123 >`�d�
Received by/Company: (Signatur
Date/Time f .
j(O�QQ
MTJL LAB USE ONLY
Table #;
Acctnum:
Relinquished by Company: (Signature)
f� If/L✓]
Date/Time5 �1-
of a
Re iv /Company: (Signature)
f- Zr 2
J -
D to ime:
�
Template:
Prel°gin:
PM:
PB:
Trip Blank Received: Y N NA
p
HCL McOH TSP Other
Relinquished by/Company: (Signature]
�J� 5 ' L z
Date/Time:
Received by/Company: (Signature]
Date/Time:
Non Cnnformance(s):
YES I NO
Page: Page 14 of 1
of: +

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Page 15 of 15

a
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
M eritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Report Date: 7/6/2023
Date Sample Rcvd: 6/1/2023
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test
Meritech Work Order # 06012309 Sample: Danville #3 Composite 6/1/23
Total Solids Volatile Solids % Volatile Solids
Week 1 1.16 0.61 0.522
Week 2
0.92
0.50
0.542
Week 3
0.88
0.47
0.534
Week 4
0.86
0.48
0.558
Week 5
0.80
0.45
0.567
Van Kleek Reduction (%): -19.99
I hereby certify that I have reviewed and approve these data. 'Aj]00.n&CL ka�'K'
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

PERCENT TOTAL SOLIDS J PERCENT VOLATILE SOLIDS
SM 2540 B-2015 ,
Analyst: _ B - A x 100 = % TOTAL SOLIDS
Date: ��_ C -
Recorded By: (_ Clean IN 550°C- Clean UT 550°C B - D x 100 = % VOLATILE SOLIDS
�4(fil(/ T C
1st Sample IN 104°C 1st Sample OUT 104°C 1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C� 2nd Sample IN 550°C 2nd Sample OUT 550°C
C A R
SAMPLE
g USED
DISH 9
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
(.jam kle, [H--� .
96,nla
I 0I
i
, QL '
n>
'14;'
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
Ignite Wt Diff
2nd Ignition Wt (g) (final -initial)
i
% VOL SOLIDS
uu o 3
a •7u o 3 c
-:
-_
SAMPLE
g USED
DISH !#
TARE WT. (e)
1st Dry Wt
2nd Dry Wt )
Dry Wt Diff
(final -initial)
%TOT SOLIDS
21
F �UM
1 ' i
C�
10- 1101 _
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g) I
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial) % VOL SOLIDS
tJl-38u3
ut.3�u3
0 -
SAMPLE
USED
DISH !#
TARE WT. )
1st Dr Wt
y (e) 2nd Dry Wt {e]
Dry Wt Diff
final -initial
%TOT SOLIDS
Q5sl
3 ,�l 3
3� Z—S
C>
-rC
SANIPLE
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for I hour)
USED DISH f# I TARE WT
3c �
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for I hour)
D
1st Ignition Wt (g)
I 2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial) % VOL SOLIDS
13
S --
Dry Wt Diff
1st Dry Wt () 2nd Dry Wt (e) (final -initial) % TOT SOLIDS
D
1st Ignition Wt (g)
2ndIgnition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
e
C�

I V VLAI ILr- JVLl17+J
SNI 2540 B-2015
Analyst:_ B - A_ x 100 = % TOTAL SOLIDS
Date: C
Recorded By: Clean IN 550°C Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 104°C 1st Sample OUT 104°C 1st Sample IN 550°C Ist Sample OUT 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C 2nd Sample IN 550°C 2nd Sample OUT 550°C
C A B
Dry Wt Diff
SAMPLE
USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
final -initial)
%T'OT SOLIDS
+ J
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WtDiff
(final -initial)
% VOL SOLIDS
3 -2172
37-2-3K
0
a )
SAMP E
g USED
DISH #
TARE WT. )
Ist Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
,
3 5,q 5TS
e
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
35.DW)
3S.3301
10
10:�11-1
SANIPL
g USED
DISH #
TARE WT.
1st Dry Wt )
2nd Dry Wt
Dry Wt Diff
(final -initial) % TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550oC for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
I (final -initial)
% VOL SOLIDS
3 6 -
1
3 -73
1 c
10, 5c
SAMPL
g USED
DISH #
TARE WT.
Ist Dry Wt )
2nd Dry Wt (
Dry Wt Diff
final -initial
% TOT SOLIDS
3��44,(n
D
Ignite WtDiff
(initial ignition 550°C for 1 hour) 1st Ignition Wt (g) 2nd Ignition Wt (g) (final -initial) % VOL SOLIDS
(repeat iginition 550°C for I hour) U u - 039C, P0.0 39 0 C' 0

131y1 IL D- VID
Analyst:— BBA x 100 = % TOTAL SOLIDS
Date: - �? "7 C
Recorded By:. Clean IN 550°C Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
C
lst Sample IN 104°C lst Sample OUT 1040C lst Sample IN 5500C Ist Sample OUT 5500C
2nd Sample IN 1040C 2nd Sample OUT 1040C 2nd Sample IN 5500C 2nd Sample OUT 5500C
r A u
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
OW,�2j
I t
t
l o`5
6
a -
I
(initial ignition 550°C for 1 hour)
(repeat iginition 5500C for 1 hour)
M
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
ui. gr
ul Z701
o
SANI E
gUSED
DISH#
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry WtDiff
(final -initial)
%TOT SOLIDS
->
(initial ignition 550'C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WtDiff
(final -initial)
% VOL SOLIDS
3V
3 <.
c
SANIP E
g USED
DISH #
TARE WT.
1st Dr Wt
2nd D Wt g
Dry Wt Diff
final -initial
% TOT SOLIDS
a—.
e
O
= =
1
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
U416 a 7
q6l(cl
c
T=
SAMPL
g USED
DISH#
TARE WT. g
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial
%TOTSOLIDS
61
,
a
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL OLIDS

SM 2540 B-2015
Analyst: B - A_ x 100 = % TOTAL SOLIDS
Date: C
Recorded By: i Clean IN 550°C Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 104°C 1st Sample OUT 104 1st Sample IN 550°C 1st Sample OUT 550°C
2,sd a..�n� IN 104°C 2nd Sample OUT 1 4°C 2nd Sample IN 550°C 2nd Sample OUT 550°C
C A B
SAMPLE
USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 1 hour)
`1
Ignition Wt (g)
2nd Ignitition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
gist
SAMPLE
USED
DISH #
TARE
TARE WT.
1st Dr Wt
2nd Dr Wt
Dry Wt Diff
I-,
% TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
n '
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
SAMPLE
g USED DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
(final -initial
%TOT SOLIDS
S
v�
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for I hour)
D
1st Ignfition Wt (22g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
l 1
5 J
lz-�5 I :
O
- -
SAMPLE
g USED
DISH #
TARE WT. W
1st Dry Wt Q)
2nd Dry Wt
Dry WtDiff
final -initial
% TOT SOLIDS
19-51T�z
Jcl\
— - IU S
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOLSOLIDS

Analyst: /T✓17
Date:
Recorded By:
�Q
1st Sample IN 104°C,
2nd Sample IN 104°C
C
SM 2540 B-2015
Clean IN 550°C Clean OUT 550°C
1st Sample O T 04°C_
2nd Sample O 1040C
A
B - A x 100 = % TOTAL SOLIDS
C
B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 550°C 2nd Sample OUT 550°C
B
SAMPLE
USED
DISH #
TARE WT. 1st Dr Wt
2nd Dry Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
23,ol paytv1 (9 ')
0a-2 g
oX
1,5�41 u a
�.
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for I hour)
D ,
1st Ignition Wt (g)
2nd Igniti n Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS69
I If
SAMPL
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt (
Dry Wt Diff
final -initial)
% TOT SOLIDS
20-
c E%
5�,
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
50- 141?I.!�
50- MI5
c
S LE
g USED
DISH #
TARE WT. 1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial
% TOT SOLIDS
C 3
c o 5 1
51. kr
:D
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for I hour)
c
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
'51-02 0
5 0 20
c
'
S 1NIPLE
g USED
DISH k
TARE WT. (
1st Dry Wt a
2nd Dry Wt a
Dry Wt Diff
final-initiall
% TOT SOLIDS
(initial ignition 550°C for I hour)
(repeat iginition 550°C for 1 hour)
II]
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
2
5s'. �3�2
c
G.

5-9.2016 Chain of Custody Record (COC)
NPDES#:
Client: EMA Resources Inc. Phone:-336-751-1441
Address: 755 Yadkinville Rd Fax: [phone]
Mocksville NC 27028 Email: brent.collins0emaresourcesmc.co
Project:
P.O.#:
Attention:_ Brent Collins Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
Circle all that apply: mail eferred), Fax, Mail Si—�lodays� [-5 Days �❑S
ME RITECH INC.
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
` Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates & Times
Person Taking Sample(Sign/Print): /
Gl/%, s
b l LaUse On Y
Start
End
Grab?
Cont.
Test
(s) Required
On Ice?
Yes / No
H OK?
Cl OK?
Date
Time
Date
Time
}`3
c
1
30 Day Bench Digestion
Temperature Upon
Receipt: <
Method of
Shipment:
*** Dechlorination (<0.5 m) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation.
Comments:
Please send calculation sheets with results
Compositor #
Jug#
❑ UPS
❑ Fed Ex
Are these results for regulatory purposes? Yes le No ❑
Report results in: mg/L ❑ mg/kg o- ug/L ❑
Hand Delivery
Relinquished by: Date: Time:
7 li��
Received by: Date: Time:
❑ Other
Relinquished by: Date: Time:
Received by: Date: Time:
Relinquished by: Date: Time:
Reced by Lab: �" 1'1D T'rU;- (�

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Danville WQ Permit Number: WQ0036561
WWTP Name:
Northside WWTP
NPDES Number: VA0060593
Monitoring Period: From 5/15/2023 To 5/15/2023
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
1 Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
1 Process to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
JAlt. (1) Fecal Density El
7AIt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
JAerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
g y
Number o
Excee-
Frequency
of Analysis
Sample
'Type
Analytical
Tech-nique
Minimum
Geo. Mean
Maximud
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
222
242
263
CFU/ g
0
l
Quarterly
G
SM9222D
1000 mpn per gram
of total solid (dry
wei t
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
I weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. OZ uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAlt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
© "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Alan Gould - Project Manager
Preparer Name and Title (type or print)
e
Ala 6, 202412:35 EST)
Signature of Preparer*
Brent Collins; Director of Technical Services
Land Applier Name and Title (if applicable)(type or print)
26/01 /2 ( ;dY
1/24/2024
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
May 23, 2023
Kimberly Wickemeyer
Inframark
229 Northside Drive
Danville, VA 24540
RE: Project: VA0060593
Pace Project No.: 30587678
Dear Kimberly Wickemeyer:
Enclosed are the analytical results for sample(s) received by the laboratory on May 15, 2023. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Beaver
• Pace Analytical Services - Lexington
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Cynthia Walker
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 15

aceAnalytical
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Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
CERTIFICATIONS
Project: VA0060593
Pace Project No.: 30587678
Pace Analytical Services Beaver
225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466
Virginia VELAP 460148 Kentucky Wastewater Certification KY90039
West Virginia DEP 060 Pennsylvania DEP 68-00839
West Virginia DHHR 00412CM
Pace Analytical Services Lexington
782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 15

aceAnalytical
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Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE SUMMARY
Project: VA0060593
Pace Project No.: 30587678
Lab ID
Sample ID
Matrix
Date Collected
Date Received
30587678001
A BASIN #1
Solid
05/15/23 07:35
05/15/23 12:44
30587678002
A BASIN #2
Solid
05/15/23 07:40
05/15/23 12:44
30587678003
A BASIN #3
Solid
05/15/23 07:45
05/15/23 12:44
30587678004
A BASIN #4
Solid
05/15/23 07:55
05/15/23 12:44
30587678005
A BASIN #5
Solid
05/15/23 08:00
05/15/23 12:44
30587678006
A BASIN #6
Solid
05/15/23 08:05
05/15/23 12:44
30587678007
A BASIN #7
Solid
05/15/23 08:10
05/15/23 12:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
VA0060593
30587678
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
30587678001
A BASIN #1
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30587678002
A BASIN #2
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30587678003
A BASIN #3
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30587678004
A BASIN #4
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30587678005
A BASIN #5
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30587678006
A BASIN #6
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
30587678007
A BASIN #7
SM 2540G-15
AK
1
PASI-BV
SM 9222D-2015
TLB1
1
PASI-LE
PASI-BV = Pace Analytical Services - Beaver
PASI-LE = Pace Analytical Services - Lexington
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 4 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30587678
Sample: A BASIN #1
Lab ID: 30587678001 Collected: 05/15/23 07:35 Received: 05/15/23 12:44 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
96.1 % 0.10 1 05/17/23 09:24 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
<256.41 CFU/g 0.26 0.257 05/16/23 07:30 05/17/23 08:15
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30587678
Sample: A BASIN #2
Lab ID: 30587678002 Collected: 05/15/23 07:40 Received: 05/15/23 12:44 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
96.2 % 0.10 1 05/17/23 09:27 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
<263.16 CFU/g 0.26 0.264 05/16/23 07:30 05/17/23 08:15
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 6 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30587678
Sample: A BASIN #3
Lab ID: 30587678003 Collected: 05/15/23 07:45 Received: 05/15/23 12:44 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
96.2 % 0.10 1 05/17/23 09:30 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
<263.16 CFU/g 0.26 0.264 05/16/23 07:30 05/17/23 08:15
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30587678
Sample: A BASIN #4
Lab ID: 30587678004 Collected: 05/15/23 07:55 Received: 05/15/23 12:44 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
95.5 % 0.10 1 05/17/23 09:33 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
<222.22 CFU/g 0.22 0.223 05/16/23 07:30 05/17/23 08:15
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30587678
Sample: A BASIN #5
Lab ID: 30587678005 Collected: 05/15/23 08:00 Received: 05/15/23 12:44 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
95.9 % 0.10 1 05/17/23 09:34 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
<243.9 CFU/g 0.24 0.244 05/16/23 07:30 05/17/23 08:15
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 9 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30587678
Sample: A BASIN #6
Lab ID: 30587678006 Collected: 05/15/23 08:05 Received: 05/15/23 12:44 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
95.6 % 0.10 1 05/17/23 09:35 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
<227.27 CFU/g 0.23 0.228 05/16/23 07:30 05/17/23 08:15
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
ANALYTICAL RESULTS
Project: VA0060593
Pace Project No.: 30587678
Sample: A BASIN #7
Lab ID: 30587678007 Collected: 05/15/23 08:10 Received: 05/15/23 12:44 Matrix: Solid
Results reported on a "dry weight"
basis and are adjusted for percent moisture, sample size and any dilutions.
Parameters
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
BVR Percent Moisture
Analytical Method: SM 254OG-15
Pace Analytical Services - Beaver
Percent Moisture
95.5 % 0.10 1 05/17/23 09:38 N2
LBIO Fecal Coliform By MF
Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015
Pace Analytical Services - Lexington
Fecal Coliform
<222.22 CFU/g 0.22 0.223 05/16/23 07:30 05/17/23 08:15
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 11 of 15

aceAnalytical
www.paeelabs.enm
Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALIFIERS
Project: VA0060593
Pace Project No.: 30587678
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 05/23/2023 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15

aceAnalytical
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Pace Analytical Services, LLC
1638 Roseytown Road - Suites 2,3,4
Greensburg, PA 15601
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: VA0060593
Pace Project No.: 30587678
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
30587678001
A BASIN
#1
SM
2540G-15
588627
30587678002
A BASIN
#2
SM
2540G-15
588627
30587678003
A BASIN
#3
SM
2540G-15
588627
30587678004
A BASIN
#4
SM
2540G-15
588627
30587678005
A BASIN
#5
SM
2540G-15
588627
30587678006
A BASIN
#6
SM
2540G-15
588627
30587678007
A BASIN
#7
SM
2540G-15
588627
30587678001
A BASIN
#1
SM
9222D-2015
588379
SM
9222D-2015
588381
30587678002
A BASIN
#2
SM
9222D-2015
588379
SM
9222D-2015
588381
30587678003
A BASIN
#3
SM
9222D-2015
588379
SM
9222D-2015
588381
30587678004
A BASIN
#4
SM
9222D-2015
588379
SM
9222D-2015
588381
30587678005
A BASIN
#5
SM
9222D-2015
588379
SM
9222D-2015
588381
30587678006
A BASIN
#6
SM
9222D-2015
588379
SM
9222D-2015
588381
30587678007
A BASIN
#7
SM
9222D-2015
588379
SM
9222D-2015
588381
Date: 05/23/2023 04:46 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 15

CHAIN -OF -CUSTODY Analytical Request Document
aceAnalytical'
Chain -of -Custody is a LEGAL DOCUMENT -Complete all releventflelds
LAB USE ONLY- Affix Workorder/Login Label Here or List Pace Workorder Number or
MTJLlop' WO# : 3m587678
ALL SHADED AREJ
container Preservative T e
U **_ 30587678
- PreservativeTypes: (1) nitric acid, (2) sulfuric acid, (3) hy, __...• „r ,un,ue, i» zinc acetate,
(6) methanol, (7) sodium bisulfate, (8) sodium thiosulfate, (9) hexane, (A) ascorbic acid, (B) ammon€um sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) other
Company' lnframark-Danville
Billing Information:
lnframark-Danville WWTP
229 Northside Drive
Danville, VA 24540
Address: 229 Northside Dr., Danville, VA 24540
Report To: [e-mail]
Email To: alicia.erumpton@inframark,com
copy ro: Kimberl .Wickeme er I nframark.COm
y Y �%
Site Collection Info/Address:
Danville VA WVIITP 229 Norlhside, Dr., Danville, VA 24540
Analyses
Lab Profile/Line;
Customer Project Name/Number:
lnframark-Danville (client #: 92-618203)
State: County/City: Time Zone Collected:
VA /Danville [ ] PT [ ]MT[ ] CT VET
VJ
N
CL
N
,J
E
to
,-
0
O
(}
N
LL
Lab sample Receipt Checklist:
Custody Seals Present/Intact Y N NA
Custody Signatures Present Y N NA
Collector Signature Present Y N NA
Bottles Intact Y N NA
correct Bottles Y N NA
sufficient Volume Y N NA
Samples Received on Ice Y N NA
VOA - fieadspace Acceptable Y N NA
USDA Regulated soils X N NA
Samples in Holding Time Y N NA
Residual Chlorine Present Y N NA
Cl Strips,.
Sample pH Acceptable Y N NA
pH Strips;
Sulfide Present Y N NA
lead Acetate Strips:
LAD USE ONLY:
Lab sample I I Comments:
Phone:[phone]
Email: kimberfy.wfckemeyer@infmmark,com
Site/Facility ID#;
Danville, VA WWTP permit VA0060593
—
Compliance Monitoring?
[ Oes [ ] No
Collected By (print):
Robert Clifton
Purchase Order #: 152847
Quote #: Q0128580
DW PWS ID M
DW Location Code:
C/ollected By (signatNre):
(
Turnaround Date Required:
results by 05/30/2023
Immediate Packed an Ice:
Y
[Vyes [ IN.
Sample Disp sal:
Dispose as appropriate I j Return
( l Archive:
( IHold:
Rush:
[ ] Same Day I ] Next Day
[ J 2 Day [ ] 3 Day ( ] 4 Day [ ] 5 Day
{Expedite Charges Apply)
Field Filtered (if applicable):
[ ] Yes No
Analysis:
* Matrix Codes (insert in Matrix box below): Drinking Water (DW), Ground Water (GW], Wastewater (WW),
Product (P), Soil/Solid (SL), Oil (OL), Wipe (WP), Air (AR), Tissue (TS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample ID
Matrix *
Comp/
Grab
Collected (or
Composite Starts
Composite End
Res
CI
#of
Ctns
Date
I Time
Date
I Time
Basin #1
SL*
Grab
05/15/23
,a735
No
1
asin #
SL*
Grab
05/15/23
b140
- - - -
- - - -
NO
1
Basin #3
SL*
Grab
05/15/23
O-rg13j
_ _ _ _
- --
NO
1
A Basin #4
SL*
Grab
05/15/23
0755
_ _ . _
- - -
No
1
Basin #5
SL*
Grab
05/15/23
4)boa
- - --
- - --
No
1
asin 4b
SL*
Grab
05/15/23
r)
- _ _ _
_ _ _ _
No
1
A—Sa—sin #7
SL*
Grab
05115/23
00ot
_ - - _
_ _ _ _
No
1
Customer Remarks / Special Conditions / Possible Hazards:
*Biosollds for Fecal Coliform
Type of Ice Used: a Blue Dry None
SHORT HOLDS PRESENT (<72 hours);
Y N N/A
Lab Sample Temperature Info;
Temp Blank Received: Y N NA
Therm 1D#: z-q
Cooler 1 Temp Upon Receipt:? -I oC
Cnoler 1 Therm Carr. Factor: -t-- r I oC
Cooler 1 Corrected Temp: ��oC
Comments:
Packing Material Used:
Lab Tracking#:
Radchem sample(s) screened (<500 cpm): Y N NA
Samples received via:
FEDFX UPS to Courier Pace Courier
Relinquished by/Comps : (Signature)
!n/r�i4ova�L'(
Date/Time:
C`Z. �
5 is
Received byX pang: (Signature)
Pate/Time: iZ q I
'T
X-/-C 2
MTJL LAB USE ONLY
Table d:5e�
Acctnum:
Template:
Prelagln:
P
PD:B;
Relinquished by/Company: (Signature]
Date/Timl -1 ` -073
�j
Re ived by/Company: (Signature)
,
�Cjnje
+ C
Trip Blank Received: Y NA
N
HCL McOH TSP Other
Relinquished b /Company: (Signature)
T
i 2, ^
y: Received by/Comp Sign to )
Date
�f
Non Conformance(s):
YES / NO
age o
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Page 15 of 15

h
Contact: Brent Collins
Client: EMA Resources, Inc
7SS Yadkinville Road
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Report Date: 7/6/2023
Mocksville, NC 27028
Date Sample Rcvd: 6/1/2023
Vector Attraction Reduction
/ Aerobically Digested
Sludge (30 Day Test)
Meritech
Work Order # 06012310
Sample: Danville #4 Composite 6/1/23
Total Solids
Volatile Solids
% Volatile Solids
Week 1
1.09
0.58
0.S27
Week 2
0.91
0.S0
0.SS1
Week 3
0.84
0.46
0.549
Week 4
0.93
0.49
0.S2S
Week 5
0.83
0.4S
0.S42
Van Kleek Reduction (%): -6.16
I hereby certify that I have reviewed and approve these data. �—
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

...... uvu ay:_ — — I(/�
]st Sample IN 104°C
2nd Sample IN 104°C
C
C
Clean IN 550°C lean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
C
1st Sample OUT 104°P lst Sample IN 550°C 1st Sample OUT 550°C
2nd Sample OUT 16214C 2nd Sample IN 550°C 2nd Sample OUT 550°C
A B
SAMPLE
g USED DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt (
Dry Wt Diff
final -initial
% TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 5500C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
y - 922
0 92Z
=
SAMPL
g USED
DISH #
TARE WT.
1st Dr Wt
2nd Dr Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
Ala
t i
-, ;
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
I (final -initial)
% VOL SOLIDS
14I-63u
1-0341
n
a,59
SAMPLI:
g
DISH
TARE WT.
1st Dr Wt
2nd Dry Wt
Dry Wt Diff
LILinal-initial)
%TOT SOLIDS
+USED
�#
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WIDiff
(final -initial)
% VOL SOLIDS
U Ti lU
Dry Wt Diff
SA1YLPL E
g USED
DISH #
TARE WT.
1st Dry Wt g
2nd D Wt
_(final -initial)
% TOT SOLIDS
1
�V
L—J
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Dif1-
(final -initial)
% VOL SOLIDS
3012L4
M.22 0
I a

0"Lr-vL7 / r r.ICI L.I�1 .� V VLAILLL' .7VL11J�
SM 2540 B-2015
Analyst:_ � B - A_ x 100 = %TOTAL SOLIDS
Date: C
Recorded By: '} Clean IN 550°C Clean OUT 550°C B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 104°C 1st Sample OUT 104°C 1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 104°C 2nd Sample OUT 104°C I 2nd Sample IN 550°C 2nd Sample OUT 550°C
C A R
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
[final -initial] I
% TOT SOLLDS
� I
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
1st Ignition Wt (g)
Ignite Wt Diff
2nd Ignition Wt (g) (final -initial)
% VOL SOLIDS
3 lP
�� ��( o
.o- 5---
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt g
Dry Wt Diff
(final -initial)
% TOT SOLIDS
,-3cl 6Co
3 r)rn
1 o
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
I DISH # I TARE WT
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
SAMPLE g USED DISH # TARE WT-
, s� 1
V
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
0
1st Ignition Wt (g)
Ignite Wt Diff
2nd Ignition Wt (g) (final -initial)
% VOL SOLIDS
39_ 6 4, 0 5
39- 6605 n
OT"t)
Dry Wt Diff
1st Dry Wt 2nd Dry Wt a(final-initial) % TOT
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
LJ�rinal-ini
Diff
t Dr Wt ) 2nd Dry Wt tiall%TOT SOLIDS
t
D
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
3- U
_ 5
0
0--U q r
c—

Analyst:
Date:
Recorded By:
31V1 AD, iS-GU1�
lClean IN 550°C Clean OUT 550°C
1st Sample IN 104°C 1st Sample OUT 104°C
2nd Sample IN 104°C 2nd Sample OUT 104°C
C A
B - A x 100 = % TOTAL SOLIDS
C
B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 5500C 2nd Sample OUT 5500C
«_ R _
SAMPLE
USED
DISH #
TARE WT.
1st Dry Wt ()
2nd Dry Wt
Dry Wt Diff
(final -initial)
% TOT SOLIDS
`
, 1
�V r •
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
I
fil
Ist Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WtDiff
(final -initial)
% VOL SOLIDS
30
SAMPLE
g USED
DISH #
TARE WT. W
1st Dry Wt
2nd Drj Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
n
D
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
SAMPLE
g USED
DISH#
TAREWT.
1st Dry Wt
2nd Wt
Dry Wt Diff
final -initial
%TOTSOLIDS
n
(Dry
iVV J
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
117
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
Dry Wt Diff
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt )
2nd Dry Wt
final -initial
% TOT SOLIDS
-17
n
u
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Di
(final -initial)
% VOL S IDS
39-3 8?
3� -3 7 F
na

PERCENT TOTAL SOLIDS / PERCENT VOLATILE SOLIDS
SM 2540 B-2015
Analyst: _ _ _ BBA x 100 = % TOTAL SOLIDS
Date: �1 C
Recorded By: Clean IN 5500C Clean OUT 55 C_ B - D x 100 = % VOLATME SOLIDS
— C
1 st Sample IN 1040C 1 st Sample OUT 104°C V 1st Sample IN 5500C 1st Sample OUT 5500C
2nd Sample IN 1040C 2nd Sample OUT 104°C 2nd Sample IN 5500C 2nd Sample OUT 5500C
c A R
SAMPLE
9 USED
DISH
NJ
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
%TOTSOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 5500C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignitions Wt (g)
Ignite Wt Diff
(final -initial)
% VOLSOLIDS
I 1
�t `J 1CY��
-: ; -. -
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt
2nd DryWt (
Dry Wt Diff
final -initial)
% TOT SOLIDS
9
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
it
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
(final -initial)
I % TOT SOLIDS
(initial ignition 550°C for 1 hour)
(repeat iginition 5500C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite WtDiff
I (final -initial)
% VOL SOLIDS
1 of
�r1­ —�
0
SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt )
2nd Dry Wt
Dry Wt Diff
(final -initial)
% TOT SOLIDS
(initial ignition 5500C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt ()
Ignite Wt Diff
(final -initial)
% VOL SOLIDS

SM 2540 B-2015
Analyst: —T
Date:
Recorded By: Clean IN 550° Clean OUT 550°C
r I - F .
F
t Sample IN 104°C 1st Sam e OUT 104°C
d Sample IN 104°C 2nd Sar4ple OUT 104°C
C A
B - A_ x 100 = % TOTAL SOLIDS
C
B - D x 100 = % VOLATILE SOLIDS
C
1st Sample IN 550°C 1st Sample OUT 550°C
2nd Sample IN 550°C 2nd Sample OUT 550°C
R
SAMP
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt (
Dry Wt Diff
final -initial
% TOT SOLIDS
c o Rq- t
l -5'/ / 2
20
3 S 12
S �
0l ,..
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
35. ZI 5'
35.2 SI
o
-.7- Wtt-
SAMPLE
2 USED
DISH #
TARE WT. W
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
%TOTSOLIDS
39Y
I22
3-q3
=
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
3-q q
V 3 91 2
_ SAMPLE
g USED
DISH #
TARE WT.
1st Dry Wt
2nd Dry Wt
Dry Wt Diff
final -initial)
% TOT SOLIDS
I5
c
3 o
t�c5
O
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignitionn Wt (g)
2nd Ignition Wt (g)_
Ignite Wt Diff
(final -initial)
% VOL SOLIDS
2 2
SAMPL I
gUSED
DISH #
TARE WT.
1st Dry Wt )
2nd Dry Wt )
Dry W t Di ff
(final -initial)
%TOT SOLIDS
?. 0C
5 _3 2
5Qrs
�5
►
(initial ignition 550°C for 1 hour)
(repeat iginition 550°C for 1 hour)
D
1st Ignition Wt (g)
2nd Ignition Wt (g)
Ignite Wt Diff
(final -initial)
% VOL SOLIDS

5.9-2016
Chain of Custody Record (COC)
NPDES#:
Client: EMA Resources Inc. Phone:_ 336-7S1-1441
Address: 7SS Yadkinville Rd Fax: 336-7S1-1442
Mocksville NC 27028 Email: Brent.colfinsCdemaresourcesinc.com
Project:
P.O.#:
Attention:_ Brent Collins Turn Around Time*
How would you like your report sent? *RUSH work needs prior approval.
St�jlOdays)-S Days ?Os
Circle all that apply: (preferred) , Fax, Mail ]]
ME R ITE C H INC.
1
ENVIRONMENTAL LABORATORIES
642 Tamco Rd. Phone: [phone]
Reidsville NC 27320 Fax: [phone]
Email: [e-mail]
www.meritechlabs.com
Sample Location and/or ID #
Sampling Dates &Times
Person Taking Sample (Sign/Print):
f���//�,f
Lab Use Only
Start
End
Comp?
Grab?
#of
Cont.
Test(s)
Required
On Ice?
Yes / No
pH OK?
Cl OK?
Date
Time
Date
Time
\
L,ornj i l l e
00
C
L
30 Day Bench Digestion U
1
1
�
Temperature Upon
Receipt: t
Method of
"' Dechlorination (<0.5 ppm) of Ammonia, Cyanide,
Phenol and TKN samples must be done in the field prior to preservation.
Shipment:
Comments:
Please send calculation sheets with results
Compositor #
❑ UPS
Jug #
❑ Fed Ex
Are these results for regulatory purposes? Yes
L�-- No ❑
Report results in: mg/L ❑ mg/kg Q— ug/L ❑
El Hand Delivery
Relinquished by: Dater/,
a--
Time:
Received by: Date: Time:
❑ Other
Relinquished by: Date:
Time:
Received by: Date: Time:
Relinquished by: Date:
Time:
Rec by =f j J B$e'� �` 1�IR�.
/

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY24-SL006076
k5i I"14'4+; 4 L
Client: James Y Blackwell
Advisor: Brent Collins
Predictive
7402 NC Hwy 158 W
EMA Resources Inc
°± f'
Yanceyville, NC 27379
755 Yadkinville Rd
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County : Caswell
_1
Links to Helpful Information
Sampled: Received: 10/03/2023 Completed: 10/11/2023 Farm: CS06
Client ID: 242509
Advisor ID: 405413
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
60 0 0 pH$ 0
0 0
Note: 12 Note: $
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.36 1.07 13.4 100 0.0 7.2 146 37 88 11
58 807 484 536 536
288 0.2 1
North Carolina
Tai wLv Truk f and Ct wmisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

Page 1 of 1
Report No: 23-268-0531
Account No: 46245
Advisor: EMA Resources Inc
755 Yadkinville Road
Mocksville NC 27028
Waypo'10 t
ANALYTICAL
Client: James Blackwell
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 ° Fax [phone]
www.waypointanalytical.com
Farm: CS06
Date Received: 09/25/2023
Date of Report: 09/26/2023
Lab No Field ID Sample ID
Soil Class HM% W/V pH
Ac
P-1 K-1
S-1
Mn-1
Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 CEC BS% Ca% Mg% ESP Na
24582 3 03
MIN 2.1 5.5
1.9
111 47
56
294
201 0 403 403 585 7.5 75 48 21 2.6 0.2
Crop Recommendations:
Rec Uom Lime (Vacre)
N
P205 K2
S
Mn
Zn Cu B Mg Last Crop
1- Fescue Hay
lb/acre 0.9
150
0 40
20
0
0 0 0 0
Comment
Test result units = CEC and Na in meq/100cm3; NO3 N in mg/dm3; W/V in g/cm3
North Carolina Division of Water Quality Certification #257, Analysis and fertility recommendations shown on this report are performed in accordance within NCDA guidelines, Analysis prepared by: Waypoint Analytical Virginia, Inc.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY24-SL003444
kSi l"14'4+;4
Client: James Y Blackwell
Advisor:
Predictive
7402 NC Hwy 158 W
Yanceyville, NC 27379
�- Soil Report Mehlich-3 Extraction
Sampled County : Caswell
_1
Links to Helpful Information
Sampled: Received: 09/07/2023 Completed: 09/14/2023 Farm: CS06
Client ID: 242509
Advisor ID:
Sample ID: 00005
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.6 120-200 0
0 0 0 0 0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 0
0 0 0 0 0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.60 1.06 6.8 80 1.4 5.6 86 79 52 22
74 952 588 588 381 381
327 0.2
3
North Carolina
Tcbwiv Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY24-SL003641
k5i I"14'4+;4,
Client:
Margarett Rowland
Advisor:
Brent Collins
Predictive
3233 Allison Rd.
EMA Resources Inc
°± f'
Pelham, NC 27311
755 Yadkinville Rd
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County : Caswell
_1
Links to Helpful Information
Sampled: Received: 09/11/2023 Completed: 09/19/2023 Farm: CS12
Client ID:
546864
Advisor
ID: 405413
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.4 120-200 60
30
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 60
30
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.51 0.96 5.1 56 2.2 5.0 32 57 32 18
75 119
88 88
176
176
43
0.3 6
Sample ID: 00005
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.4 120-200 0
100
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 0
100
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.32 1.04 7.5 80 1.5 5.8 189 22 58 21
34 159
112 112
670
670
368
0.1 1
North Carolina
Tai wLv Truk f and Ct wmisskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY24-SL003447
k5i I"14'4+;4,
Client:
David / Sledge Sartin
Advisor:
Brent Collins
Predictive
3404 Park Springs Rd
EMA Resources Inc
°± f'
Providence, NC 27315
755 Yadkinville Rd
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County : Caswell
_1
Links to Helpful Information
Sampled: Received: 09/07/2023 Completed: 09/14/2023 Farm: CS14
Client ID:
347847
Advisor
ID: 405413
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.6 120-200 0
0
0 0 0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 0
0
0 0 0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.32 1.04 9.2 80 1.8 5.7 289 98 54 21
109 370
239 239 1545
1545
537
0.5 5
Sample ID: 00003
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.7 120-200 0
70
0 0 0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 0
70
0 0 0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2 Zn-I
Zn-AI
Cu-I
Na ESP SS-1 NO3-N
0.36 0.97 8.2 80 1.7 5.6 163 34 55 23
71 223
151 151 965
965
388
0.3 4
North Carolina
Tai wLv Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

Signature Pages
Final Audit Report
Created: 2024-01-26
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAANt7dilUpmBYaJMuspOTtrb4leHCgrdZ5
"Signature Pages" History
Document created by Brent Collins([e-mail])
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2024-01-26
.4 Document e-signed by Alan Gould ([e-mail])
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Agreement completed.
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Signature Pages
Final Audit Report
Created: 2024-01-26
By: Brent Collins([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAA8g8mcAQJOUndNnNl7gxagr1_GoQXXoOi
"Signature Pages" History
Document created by Brent Collins([e-mail])
2024-01-26 - 7:32:06 PM GMT- IP address: 206.85.202.26
'. Document emailed to Alan Johnson [e-mail]) for signature
2024-01-26 - 7:32:11 PM GMT
Email viewed by Alan Johnson [e-mail])
2024-01-29 - 8:23:50 PM GMT- IP address: 216.146.48.10
2024-01-29
d© Document e-signed by Alan Johnson [e-mail])
Signature Date: 2024-01-29 - 8:24:42 PM GMT - Time Source: server- IP address: 216.146.48.10
Agreement completed.
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