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HomeMy WebLinkAboutWQ0028547_Renewal Application_20240510Initial Review Reviewer nathaniel.thorn burg Is this submittal an application? (Excluding additional information.) * Yes No Permit Number (IR) * WQ0028547 Applicant/Permittee Town of Yanceyville Applicant/Permittee Address PO Box 727, Yanceyville, NC 27379 Is the owner in BIMS? Yes ) No Is the facility in BIMS? Yes No Owner Type Facility Name County Fee Category Minor Is this a complete application?* Yes No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Municipal Town of Yanceyville Class B Residuals Program Caswell Does this need review by the hydrogeologist? * Yes No Regional Office CO Reviewer Admin Reviewer Fee Amount Complete App Date 05110/2024 $0 Below list any additional email address that need notification about a new project. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Brent Collins Email Address* brent.collins@emaresourcesinc.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 3363993646 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0028547 Has Current Existing permit number Applicant/Permittee* Town of Yanceyville Applicant/Permittee Address* PO Box 727, Yanceyville, NC 27379 Facility Name* Town of Yanceyville Class B Residuals Program Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Permit Renewal - Town of Yanceyville WQ0028547.pdf 14.53MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 5/10/2024 May 8, 2024 Division of Water Resources Water Quality Permitting Section Non -Discharge Permitting Unit 1617 Mail Services Center Raleigh, NC 27699-1617 RE: Permit Renewal — WQ0028547 To Whom it May Concern: EMA Resources is submitting the included permit renewal for The Town of Yanceyville's land application permit - WQ0028547. The fields that are marked as modified (M) in the LASC form have been re -mapped using ARCGis to reflect the acres more accurately. The old maps were not very clear and not as precise. We have had trouble locating Jennifer Hodges NC-CS-09-11 for a new landowner agreement but we believe she still wishes to participate in the program. We will submit the LOA as soon as we receive it and will not spread on that field until a new LOA has been executed and submitted. If you have any questions concerning this renewal, please contact Brent Collins — Director of Technical Services Respectfully, Z�z 4;2�_ Brent Collins Director of Technical Services brent.collinsgemaresourcesinc.com (336) 399-3646 Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 g Inc. Permit Renewal Application For The Town of Yanceyville WQ0028547 Land Application of Residuals Prepared By: EMA Resources Inc. 755 Yadkinville Road Mocksville, NC 27028 336-751-1441 May 8, 2024 Phone 336975191441 — Fax 336975191442 755 Yadkinville Road — Mocksville, NC 27028 Table of Contents 1) RLAP Form a) Current Permit 2) RSC Form a) Vicinity Map b) Process Flow Diagram c) Quantitative Justification d) Laboratory Analytical Reports 3) Operation & Maintenance Plan 4) Residuals Information Sheet 5) LASC Form a) Per Site Information i) Landowner Agreement b) Vicinity Map c) Aerial/Application Map d) Current Cumulative Loadings State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — RESIDUALS LAND APPLICATION PROGRAM FORM: RLAP 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: Town of Yanceyville Applicant type: ❑ Individual ❑ Corporation ❑ General Partnership Privately -Owned Public Utility ❑ Federal 0 State ® Municipal County Signature authority's name per 15A NCAC 02T .0106: Kamara Barnett Title: Town Manager Applicant's mailing address: 158 East Church St, PO Box 727 City: Yanceyville State: NC Zip: 27379 Telephone number: (336) 694-5431 Email Address: townmana eg_r(a�yanceyvillenc.g_ov 2. Consultant's name: Brent Collins License Number (for RE.):" Affiliation: ❑ On Staff ® Retained (Firm: EMA Resources Inc.) Consultant's mailing address: 755 Yadkinville Rd City: Mocksville State: NC Zip: 27028 Telephone number: (336) 399-3646 Email Address: breast.collinskemaresourcesinc.com 3. Agronomist's name: License Number: W Affiliation: ❑ N/A [j On Staff 0 Retained (Firm: �) Agronomist's mailing address: _ City: `A State: _ Zip: W-no Telephone number: (A) Email Address: _ 4. Soil Scientist's name: AN License Number: 72 Affiliation: ❑ N/A [I On Staff 0 Retained (Firm: ) Soil Scientist's mailing address: _ City: State: Zip: K__-J Telephone number: (_) = Email Address: _ 5. Fee submitted: $0.00 (See Instruction B) IL PERMIT INFORMATION: 1. Application is for (check all that apply): 0 new, a modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00028547 Date of most -recently issued permit: 05/16/2019 Date of most -recently certified Attachment A (if different than the permit): 05/16/2019 Date of most -recently certified Attachment B (if different than the permit): 05/16/2019 FORM: RLAP 06-16 Page 1 of 5 III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION: 1. Residuals Processing Facility's physical address: 666 Pine Dr City: Yanceyville State: NC Zip: 27379 Coordinates: Latitude: 36' 23' 39" Longitude: 79. 20' 27" Datum: NAD83 Method of measurement: GPS Level of accuracy: Nearest Second 2. County where residuals land application program is headquartered: Caswell 3. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application program, their certification numbers, and their affiliations in the following table: Designation Name Affiliation Certification Number ORC Roy Whitaker EMA Resources Inc. LA13283 Back -Up ORC Brent Collins EMA Resources Inc. LA27651 Additional Back -Up ORCs (if applicable) If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's completion of the required training school and certification test: 4. Complete the following tables regarding management of the residuals land application program: a. Plant Available Nitrogen Summary: Determine the maximum plant available nitrogen (PAN) generated by all residuals source -generating facilities as currently certified and proposed for certification with this application and list the results in the following table: Maximum amount of residuals to be certified: 319 dry tons per year. PAN Pounds of PAN per Dry Ton (Weighted Average) Pounds of PAN per Year Surface Incorporation or Injection Surface Incorporation or Injection First -Year 66.23 70.54 21,127 22,502 Five -Year Maximum Adjusted 85.14 89.44 27,160 28,531 b. Land Application Site Use Summary: Summarize information regarding the land application sites as currently certified and proposed for certification with this application: Category Use Acres Comments Crops Forest or Plantation 0 Row Crops 0 Hay/Pasture 160.89 Total: 160.89 Methods Surface 160.89 Incorporation or Injection 0 Total: 160.89 FORM: RLAP 06-16 Page 2 of 5 c. Residuals Land Application Summary: Determine the minimum acreage required to land apply the residuals as currently certified and proposed for certification assuming the scenarios listed in the following table: Assumed Application Rate (lbs PAN/ac yr) Acres Required Using First -Year PAN Concentrations Acres Required Using Five -Year Maximum Adjusted PAN Concentrations Surface Incorporation or Injection Surface Incorporation or Injection 50 423 450 543 571 100 211 225 272 285 150 141 150 181 190 200 106 113 136 143 6. If applicable, provide a plan and a schedule to resolve any known issues that would prevent land application of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage, not enough land, vector reduction practices not in place, etc.):' 7. Specify type of residuals program (See Instruction F): E Non -dedicated ❑ Dedicated If Dedicated, specify the following (check all that apply): Residuals program contains any land application site(s) that receives residuals at rates or frequencies greater than agronomic rates, explain; I_ ❑ Residuals program contains any land application site(s) that is used primarily for residuals disposal, and agricultural crop production is of secondary importance, explain; "-'9r ❑ Residuals program contains any land application site(s) that receives residuals through fixed irrigation facilities or irrigation facilities fed through a fixed supply system, explain; -A IV. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the following Residuals Source Certification and all associated documentation. IR Residuals Source Certification V. LAND APPLICATION SITE INFORMATION: (Required for all new, renewed, or modified land application site) Complete and submit the following Land Applications Site Certification and all associated documentation. IR Land Application Siite Certification. doc FORM: RLAP 06-16 Page 3 of 5 Note: Item VI. Applicable to Dedicated Program with fixed irrigation system only. VI. DESIGN INFORMATION FOR FIXED IRRIGATION SYSTEM 1. The irrigation system is: ❑ Spray ❑ Drip 2. Disposal system is: ❑ existing ❑ proposed. 3. Minimum depth to mean seasonal high water table (SHWT) within irrigation sites(s) per Soil Scientist's Evaluation: feet below ground surface. Rules 15A NCAC 02T .0505(n) requires at least one -foot vertical separation between SHWT and ground surface. 4. Are there any artificial drainage or water movement structures within 200 feet of any irrigation area? ❑ Yes or ❑ No If Yes, please explain if the soil scientist report addresses artificial structures and please indicate if structures are to be maintained or modified: 5. Loading rates recommended by the Soil Scientist Evaluation: Soil Series Fields within Soil Area Recommended Loading Rate in/hr Recommended Loading Rate in/vr 6. Design loading rates are equal or less than the loading rates recommended by Soil Scientist? ❑ Yes or ❑ No If No, explain why 15A NCAC 02T .0505(n) is not met: 7. Non -dedicated System Design (fill in the appropriate information for either a spray or drip irrigation system): Field /Zone Design Area (ftZ Number of Nozzles Maximum Application Rate allons/hr Design Annual Loading Rate allons/ r Total Spray Irrigation Design Element Plan Sheet Number Specification Pa a Number Wetted diameter of nozzles ft Wetted area of nozzles ft2 Nozzle capacity gpm Nozzle manufacturer / model / Elevation of highest nozzle ft FORM: RLAP 06-16 Page 4 of 5 Applicant's Certification (signing authority must be in compliance with 15A NCAC 02T .0106): The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes ❑ No, Explain; I, Kamara Barnett — Town Manager (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for Town of Yancgyville (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.613, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up to $25,000 per violation. kawal-a Eamett 05/10/2024 Signature: K,-B-,tt(M,V 1J, 202419:22 EDT) Date: FORM: RLAP 06-16 Page 5 of 5 ROY COOPER Governor ELIZABETH S. BISER Secretary RICHARD E. ROGERS, JR. Director KAMARA BARNETT — TOWN MANAGER TOWN OF YANCEYVILLE POST OFFICE BOX 727 YANCEYVILLE, NORTH CAROLINA 27379 Dear Ms. Barnett: NORTH CAROLINA Environmental Quality August 25, 2022 Subject: Permit No. WQ0028547 Correction Town of Yanceyville Class B Residuals Program Land Application of Class B Residuals Caswell County In accordance with a written request from you and Brent Collins received July 21, 2022, we are forwarding herewith corrected Attachment A of Permit No. WQ0028547 issued May 16, 2019. The correction to the subject permit is as follows: 1. Addition of Footnote 6 in Attachment A pertaining to the vector attraction reduction requirements for non -biological residuals. Please replace Attachment A of Permit No. WQ0028547 issued May 16, 2019 with the enclosed corrected Attachment A. If you need additional information concerning this permit correction, please contact Erick Saunders at (919) 707-3659 or erickson.saunders&ncdenr. og_v. Sincerely, Richard E. Rogers, Jr., Director Division of Water Resources Enclosure cc: Caswell County Health Department (Electronic Copy) Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy) Brent Collins — EMA Resources, Inc. (Electronic Copy) Digital Permit Archive WQ0028547 (Electronic Copy) Laserfiche File (Electronic Copy) � North Carolina Department of Environmental Quality I Division of Water Resources 512 North Salisbury Street 11617 Mail Service Center I Raleigh, North Carolina 27699-1617 NORTH GAROLINA + 919.707.9000 ROY COOPER Governor MICHAEL S. REGAN Secretary LW DA CULPEPPER Director BRIAN COLLIE — TOWN MANAGER TOWN OF YANCEYVILLE POST OFFICE BOX 727 YANCEYVILLE, NORTH CAROLINA 27379 Dear Mr. Collie: NORTH CAROLINA Environmental Quality May 16, 2019 Subject: Permit No. WQ0028547 Town of Yanceyville RLAP Land Application of Class B Residuals Caswell County In accordance with your permit major modification and renewal request received February 27, 2019, and subsequent additional information received April 24, 2019, we are forwarding herewith Permit No. WQ0028547 dated May 16, 2019, to the Town of Yanceyville for the continued operation of the subject residuals management program. Modifications to the subject permit are as follows: Removal of one field in Caswell County totaling 6.36 acres, that field being NC-CS-80- 03. • Addition of five fields in Caswell County totaling 69.65 acres, those fields being NC-CS- 09-11 and NC-CS-82-01 to -04. This permit shall be effective from the date of issuance through October 31, 2024, shall void Permit No. WQ0028547 issued April 21, 2014, and shall be subject to the conditions and limitations as specified therein. The Permittee shall submit a renewal application no later than May 4, 2024. Please pay particular attention to the monitoring requirements listed in Attachment A for they may differ from the previous permit issuance. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. Please note that on September 1, 2018, North Carolina Administrative Code Title 15A Subchapter 02T — Waste not Discharged to Surface Waters was readopted. Accordingly, this permit incorporates the requirements of these rules, therefore, please take the time to review this permit thoroughly. The Division has removed the following permit conditions since the last permit issuance dated April 21, 2014: ➢ Old Conditions I.2., I.3. and I.4. — These conditions have been fulfilled. ➢ Old Condition II.8. — Replaced by Condition 11.8. ➢ Old Condition III.10. — Redundant since the vegetative cover requirement stipulated in Old Condition III.11.i. and Condition III.10.h. D.._ North Carolina Department of Environmental Quality I Division of Water Resources NORrr+ av+ouran � �' 512 North Salisbury Street 1 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 u 919.707.9000 Mr. Brian Collie May 16, 2019 Page 2 of 2 ➢ Old Condition III.1 Lh. — Redundant since the soil pH requirement stipulated in Old Condition III.11.1. and Condition 1II.10.k. ➢ Old Condition IV.8. — Replaced by Condition IV.8. ➢ Old Condition VI.2. — This condition has been removed because the permit is not voidable. ➢ Old Condition VI.9. — Replaced by Condition VI.8. The following permit conditions are new since the last permit issuance dated April 21, 2014: ➢ Condition II.8. — The setback requirements for land application sites are listed in this condition. ➢ Condition I1I.10.1. — This condition lists the types of watersheds where new land application fields are not to be permitted. ➢ Condition 1II.1 l.c. — Public access restrictions to dedicated sites have been added. Note that there are no dedicated sites in this permit. ➢ Condition IV.8. — The annual report shall consist of one paper copy and one electronic (.pdf) copy. ➢ Condition VI.8. — The permit cannot be renewed without annual fees being paid. ➢ Attachment B — The changes to the land application sites were listed earlier in this letter. If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Otherwise, this permit shall be final and binding. If you need additional information concerning this permit, please contact Troy Doby at (919) 707- 3655 or troy ob &ncdenr. ov. Sincerely, mda Culpepper, Director Division of Water Resources cc: Yancey County Health Department (Electronic Copy) Winston-Salem Regional Office, Water Quality Regional Operations Section (Electronic Copy) Brent Collins — EMA Resources, Inc. (Electronic Copy) Beth Buffington — Protection and Enforcement Branch (Electronic Copy) Laserfiche File (Electronic Copy) Digital Permit Archive (Electronic Copy) Central Files NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENTAL QUALITY RALEIGH LAND APPLICATION OF CLASS B RESIDUALS PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO Town of Yanceyville Caswell County FOR THE continued operation of a residuals management program for the Town of Yanceyville and consisting of the land application of Class B residuals generated by the approved facilities listed in Attachment A to the approved fields listed in Attachment B, with no discharge of wastes to surface waters, pursuant to the application received February 27, 2019, subsequent additional information received April 24, 2019, and in conformity with other supporting data subsequently filed and approved by the Department of Environmental Quality and considered a part of this permit. The disposal of residuals is regulated under Title 40 Code of Federal Regulations Part 503. This permit does not exempt the Permittee from complying with Federal Regulation 40 CFR Part 503. This permit shall be effective from the date of issuance through October 31, 2024, shall void Permit No. WQ0028547 issued April 21, 2014, and shall be subject to the following conditions and limitations: I. SCHEDULES 1. The Permittee shall request renewal of this permit on Division -approved forms no later than May 4, 2024. [15A NCAC 02T .0105(b), 02T .0109] II. PERFORMANCE STANDARDS The Permittee shall maintain and operate the subject residuals management program so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the residuals management program fails to perform satisfactorily, including the creation of nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease land applying residuals, take immediate corrective actions, and contact the Winston-Salem Regional Office supervisor. [15A NCAC 02T .0108(b)(1)(A)l 2. This permit shall not relieve the Permittee of their responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [15A NCAC 02T .0108(b)(1)(A)] 3. Only residuals generated by the facilities listed in Attachment A are approved for land application in accordance with this permit. [ 15A NCAC 02T .1101 ] WQ0028547 Version 3.0 Shell Version 181130 Page 1 of 12 4. Only the fields listed in Attachment B are approved for residuals land application. [G.S. 143- 215. 1 (a)(9)] 5. Pollutant concentrations in residuals land applied to the sites listed in Attachment B shall not exceed the following Ceiling Concentrations or Cumulative Pollutant Loading Rates (CPLRs), on a dry weight basis: Parameter Arsenic Cadmium Ceiling Concentration Cumulative Pollutant Loading Rates (mg/kg) (kg/ha) (lbs/ac) 75 41 36 85 4,300 39 1,500 34 1,338 Copper Lead 840 300 267 Mercury 57 17 15 Molybdenum 75 N/A N/A Nickel 420 420 374 Selenium 100 100 89 Zinc 7,500 2,800 2,498 The Permittee shall determine compliance with the CPLRs using one of the following methods: a. By calculating the existing cumulative level of pollutants using actual analytical data from all historical land application events of residuals, or b. For land where residuals application has not occurred or for which the required data is incomplete, by determining background concentrations through representative soil sampling. [15ANCAC 02T .1105(a), 02T .1105(b)] 6. Class B biological residuals shall meet the pathogen reduction requirements in 15A NCAC 02T .1106 (b). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1106(b), 02T .1106(d)] 7. Class B biological residuals shall meet one of the vector attraction reduction alternatives in 15A NCAC 02T .1107(a). Exemptions to this requirement shall be specified in Attachment A. [15A NCAC 02T .1107(a), 02T .1107(c)] WQ0028547 Version 3.0 Shell Version 181130 Page 2 of 12 8. The facilities and sites herein were permitted per the following setbacks: a. Setbacks for Class B land application sites are as follows (all distances in feet): i. Each habitable residence or place of assembly under separate ownership: ii. Each habitable residence or places of assembly owned by the Permittee, the owner of the land, or the lessee or operator of the land: iii. Each property line: iv. Public right of way: v. Each private or public water supply source: vi. Surface waters such as intermittent and perennial streams, perennial waterbodies, and wetlands: vii. Surface water diversions such as ephemeral streams, waterways, and ditches: viii. Groundwater lowering ditches where the bottom of the ditch intersects the SHWT: ix. Subsurface groundwater lowering systems: x. Each well with exception of monitoring wells: xi. Bedrock outcrops: xii. Top of slope of embankments or cuts of two feet or more in vertical height: xiii.Each building foundation or basement: xiv. Each water line: xv. Nitrification field: Surface Irrigation Injection / Application Surface Incorporation by Vehicle Application 400 400 200 0 200 0 50 1 150 1 50' 50 50 50 100 100 100 32.8 32.8 32.8 25 25 25 25 100 25 0 100 0 100 100 100 25 25 25 15 15 15 0 15 0 0 10 0 0 20 0 ' Setbacks to property lines are not applicable when the Permittee, or the entity from which the Permittee is leasing, owns both parcels separated by the property line. [15A NCAC 02T .1108(c)] 9. Class B land application areas shall be clearly marked on each site prior to and during any residuals application event. [15A NCAC 02T .0110(g)] WQ0028547 Version 3.0 Shell Version 181130 Page 3 of 12 10. Residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (http://nutrients.soil,ncsu.edu/yields/index.php). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.6. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 (http://www.ncaar.gov/SWC/tech/documents/9th Guidance Doc 100109.12dt). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (MRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards(ftp://ftp-fc.sc.eov.usda.p-ov/NHO/practice-standards/standards/590.pdf). d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. [ 15A NCAC 02T .1109(a)(1)(K)] 11. When residuals are land applied to grazed pasture, hay crop realistic nitrogen rate shall be reduced by 25%. [15ANCAC 02T .0108(b)(1)(A)] 12. If residuals land application sites are to be over -seeded or double -cropped (e.g., bermuda grass in the summer and rye grass in the winter with both crops to receive residuals), then the second crop can receive an application of PAN at a rate not to exceed 50 pounds per acre per year (lbs/ac/yr). This practice may be allowed as long as the second crop is to be harvested or grazed. If the second crop is to be planted for erosion control only and is to be tilled into the soil, then no additional PAN shall be applied. [15A NCAC 02T .0108(b)(1)(A)] 13. Prior to land application of residuals containing a sodium adsorption ratio (SAR) of 10 or higher, the Permittee shall obtain and implement recommendations from at least one of the following: the local Cooperative Extension Office; the Department of Agriculture and Consumer Services; the Natural Resource Conservation Service; a North Carolina Licensed Soil Scientist; or an agronomist. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth. The Permittee shall maintain written records of these recommendations and details of their implementation. [ 15A NCAC 02T .0108(b)(1)(A)] 14. Residuals land application fields permitted on or after December 30, 1983 have a compliance boundary that is either 250 feet from the residual land application area, or 50 feet within the property boundary, whichever is closest to the residual land application area. Any exceedance of groundwater standards at or beyond the compliance boundary shall require corrective action. Division -approved relocation of the compliance boundary shall be noted in Attachment B. Multiple contiguous properties under common ownership and permitted for use as a disposal system shall be treated as a single property with regard to determination of a compliance boundary. [15A NCAC 02L .0106(d)(2), 02L .0107(b), 02T .0105(h), G.S. 143-215.1(i), G.S. 143-215.1(k)] WQ0028547 Version 3.0 Shell Version 181130 Page 4 of 12 15. The review boundary is midway between the compliance boundary and the residual land application area. Any exceedance of groundwater standards at or beyond the review boundary shall require preventative action. [ 15A NCAC 02L.0106(d)(1), 02L .0108] III. OPERATION AND MAINTENANCE REO UIREMENTS 1. The Permittee shall operate and maintain the residuals management program as a non -discharge system. [15A NCAC 02T .1100] The Permittee shall notify the Winston-Salem Regional Office, telephone number (336) 776-9800, and the appropriate local government official (i.e., county manager, city manager, or health director) at least two business days in advance of a site's initial residuals land application event. [15A NCAC 02T .0108(b)(1)(A)] 3. The Permittee shall notify the Winston-Salem Regional Office, telephone number (336) 776-9800, at least one business day in advance of conducting any land application activity. Notification shall include the anticipated application date, time, and field name as listed in Attachment B. Exceptions to this requirement shall be approved by the Winston-Salem Regional Office. [15A NCAC 02T .0108(b)(1)(A)] 4. The Permittee shall maintain a Division -approved Operation and Maintenance Plan that shall include: a. Description of the program, and associated facilities and equipment, in sufficient detail to show what operations are necessary for the program to function and by whom the functions are to be conducted; b. Description of anticipated maintenance of facilities and equipment associated with the program; c. Include provisions for safety measures, including restriction of access to sites and equipment; d. Spill control provisions: i. Response to upsets and bypasses including control, containment, and remediation; and ii. Contact information for plant personnel, emergency responders, and regulatory agencies; e. Detailed inspection procedures: i. Names or titles of personnel responsible for conducting inspections; ii. Frequency and location of inspections, and procedures to assure that the selected locations and inspection frequency are representative of the residuals management program; and iii. Description of record keeping and actions to be taken by the inspector in the event that noncompliance is observed; f. Detailed sampling and monitoring procedures: i. Names or titles of personnel responsible for conducting sampling and monitoring; ii. Description of monitoring procedures including parameters to be monitored; and iii. Sampling frequency and procedures to assure that representative samples are collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements. [ 15A NCAC 02T. I I I 0(a)] WQ0028547 Version 3.0 Shell Version 181130 Page 5 of 12 5. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the residuals management program, the Permittee shall designate and employ a certified operator in responsible charge (ORC), and one or more certified operators as back-up ORCs. The ORC or their back-up shall visit the facilities in accordance with 15A NCAC 08G 0204 and shall comply with all other requirement in 15A NCAC 08G 0204. [15A NCAC 02T .0117, 08G .0204] 6. The Permittee shall ensure that a copy of this permit and the Division -approved Operation and Maintenance Plan is available when land applying residuals. [15A NCAC 02T .1110(b)] 7. The Permittee shall ensure that spill control provisions are available when residuals are transported or land applied. [15A NCAC 02T .1110(a)(4)] 8. Class B residuals shall not be stored or staged at any land application site without prior written approval from the Division. Class B residuals approved for storage shall be stored or staged in a manner to prevent runoff of leachate and other wastewaters generated. [ 15A NCAC 02T .1110(c), 02T .1110(e)] 9. Adequate measures shall be taken to prevent wind erosion and runoff from the land application sites listed in Attachment B. [15A NCAC 02T .0108(b)(1)(A)] 10. Class B residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen, or snow-covered, or is otherwise in a condition such that runoff of the residuals would occur; e. Within the 100-year flood elevation, unless the residuals are injected or incorporated within a 24- hour period following a residuals land application event; f. During precipitation events, or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope of the land is greater than 10% when liquid residuals are surface applied, or if the slope of the land is greater than 18% when liquid residuals are injected or incorporated; h. If the land does not have an established vegetative cover crop unless the land is a Division -approved no -till site, or the residuals are incorporated within a 24-hour period following the injection or application of residuals; i. If the vertical separation of the seasonal high water table and the depth of residuals application is less than one foot; j. If the vertical separation of the depth to bedrock and the depth of residuals application is less than one foot; k. If the application exceeds agronomic rates; 1. If the land application sites are located within a W S-I watershed pursuant to 15A NCAC 02B .0212 or within the Critical Area of a WS-II pursuant to Sub -Item (4)(g) of Rule 15A NCAC 02B .0212, or within the Critical Area of a WS-III or WS-IV watershed pursuant to Sub -Item (4)(h) of Rules 15A NCAC 02B .0215, and .0216. [15A NCAC 02T. I 109(a)(1)) WQ0028547 Version 3.0 Shell Version 181130 Page 6 of 12 11. Class B land application sites shall have the following public access restrictions: a. Public access to public contact sites shall be restricted for one calendar year after a residuals land application event; b. Public access to non-public contact sites shall be restricted for 30 days after a residuals land application event; Public access to land associated with a dedicated land application site shall be restricted continuously while the land is permitted for active use, and for one calendar year after the final land application of residuals. [15A NCAC 02T .1109(a)(2)] 12. Class B land application sites shall have the following harvesting and grazing restrictions: a. Animals shall not be allowed to graze on land for 30 calendar days after any land application of residuals; b. Food crops, feed crops, and fiber crops shall not be harvested for 30 calendar days after any land application of residuals; c. Food crops with harvested parts that touch the mixture of residuals and soil and are totally above the land surface shall not be harvested for 14 months after any land application of residuals; d. Food crops with harvested parts below the land surface shall not be harvested for 20 months after any land application of residuals if the residuals remain on the land surface for four months or longer prior to incorporation into the soil; e. Food crops with harvested parts below the land surface shall not be harvested for 38 months after any land application of residuals if the residuals remain on the land surface for less than four months prior to incorporation into the soil; and f. Turf grown on land where residuals are applied shall not be harvested for one calendar year after any land application of residuals. [15A NCAC 02T .1109(a)(3)] 13. The Permittee shall acquire from each landowner or lessee/operator a statement detailing the volume of other nutrient sources (i.e., manufactured fertilizers, manures, or other animal waste products) that have been applied to the site, and a copy of the most recent Nutrient Management Plan (NMP) for those operations where a NMP is required by the US Department of Agriculture — National Resources Conservation Service (NRCS) or other State Agencies. The Permittee shall calculate allowable nutrient loading rates based on the provided information and use appropriate reductions. For the purpose of this permit condition, a Crop Management Plan (CMP), Waste Utilization Plan (WUP) or Certified Nutrient Management Plan (CNMP) shall also be considered a Nutrient Management Plan. [15A NCAC 02T .0108(b)(1)(A), 02T .1104(c)(3)] 14. Class B residuals shall not be land applied to the fields listed in Attachment B unless the Land Owner Agreement between the Permittee and the respective field owners or lessees/operators of the land application site is valid. The Land Owner Agreements shall expire concurrent with the permit expiration date of October 31, 2024. [ 15A NCAC 02T .1104(c)(4)] WQ0028547 Version 3.0 Shell Version 181130 Page 7 of 12 IV. MONITORING AND REPORTING REQUIREMENTS 1. The Permittee shall conduct and report any Division required monitoring necessary to evaluate this program's impact on groundwater and surface water. [15A NCAC 02T .0108(c)] 2. The residuals from each source generating facility shall be analyzed to demonstrate they are non- hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that test or are classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be land applied. The analyses (i.e., corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)) shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for five years. Any exemptions from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters, and the Federal regulatory level (mg/L) is in parentheses: Arsenic 1,4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene 1,1-Dichloroethylene (0.7) Pyridine (5.0) Selenium (1.0) Cadmium 2,4-Dinitrotoluene (0.13) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Heptachlor (and its epoxide) (0.008) Tetrachloroethylene (0.7) Chlorobenzene (100.0) Hexachlorobenzene (0.13) Toxaphene (0.5) Chloroform (6.0) Hexachlorobutadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200,0) Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) Vinyl chloride (0.2) Cresol (200.0) Methoxychlor (10.0) 2,4-D (10.0) Methyl ethyl ketone (200.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. [15A NCAC 13A .0102(b), 02T .1101, 02T .1105] WQ0028547 Version 3.0 Shell Version 181130 Page 8 of 12 3. The residuals from each source generating facility shall be analyzed at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. Each analysis shall include the following parameters: Aluminum Mercury Potassium Ammonia -Nitrogen Molybdenum Selenium Arsenic Nickel Sodium Sodium Adsorption Ratio (SAR) Cadmium Nitrate -Nitrite Nitrogen Calcium Percent Total Solids TKN Copper pH Zinc Lead Phosphorus Magnesium Plant Available Nitrogen (by calculation) [15A NCAC 02T .1101] 4. Residuals shall be monitored for compliance with pathogen and vector attraction reduction requirements at the frequency specified in Attachment A. The monitoring results shall specify the stabilization process utilized, and demonstrate compliance with the Class B pathogen reduction requirements in 15A NCAC 02T .1106(b), and one vector attraction reduction requirement in 15A NCAC 02T .1107(a) shall be met. Any exemptions from the requirements in this condition shall be specified in Attachment A. [15A NCAC 02T .1106(b), 02T .1107(a), 02T .1111(c)] An annual representative soils analysis (i.e., Standard Soil Fertility Analysis) shall be conducted on each land application site listed in Attachment B that received residuals during the calendar year. This analysis shall be in accordance with the soil sampling guidance located in the Sampling Instructions section of the NC Department of Agriculture & Consumer Services' website (h=://www.ncagr.gov/agronomi/pubs.htin) The Pennittee shall maintain these results for a period of no less than five years, and these results shall be made available to the Division upon request. Each Standard Soil Fertility Analysis shall include the following parameters: Acidity Base Saturation (by calculation) Calcium ble Sodium Percentage Phosphorus Magnesium Potassium Manganese Sodium Cation Exchange Capacity Percent Humic Matter Zinc Copper pH [15A NCAC 02T .0108(c), 15A NCAC 02T. I 111(d)] 6. Representative samples of residuals that are prepared for land application shall be collected and analyzed. [15A NCAC 02T .1111(a)] WQ0028547 Version 3.0 Shell Version 181130 Page 9 of 12 7. The Permittee shall maintain records for all residual land application events. These records shall include the following: a. Residuals source (as listed in Attachment A); b. Date of application; c. Location of land application (field name as listed in Attachment B); d. Approximate acreage applied; e. Method of application; f. Weather conditions; g. Dominant soil series; h. Soil conditions; i. Proposed crop; j. Nitrogen Application Rate based on RYEs; k. Volume of residuals applied per acre in gallons, cubic yards, dry tons, or wet tons; 1. Volume of animal waste or other nutrient source applied per acre in gallons, cubic yards, dry tons, or wet tons; in. Volume of soil amendments applied per acre in gallons, cubic yards, dry tons, or wet tons; and n. Annual and cumulative totals applied to each field for the following: i. Class A and Class B residuals (dry tons per acre); ii. Animal waste and other sources of nutrients (dry tons per acre); iii. Heavy metals as specified in Condition 1I.5. (pounds per acre); iv. Plant available nitrogen (pounds per acre); and v. Phosphorus (pounds per acre). [15A NCAC 02T .0108(c)] 8. One hard copy and one electronic copy of an annual report shall be submitted on or before March I". The annual report shall meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms. Instructions for reporting and annual report forms are available at http://deg.nc. gov/about/divisions/water-resources/water-resources-permits/wastewater-branch/non- discharge-permitting-unit/reporting-forms, or can be obtained by contacting the Non -Discharge Branch directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [15A NCAC 02T .1111(d)] 9. Noncompliance Notification The Permittee shall report to the Winston-Salem Regional Office, telephone number (336) 776-9800, within 24 hours of first knowledge of the: a. Any process unit failure (e.g., mechanical, electrical, etc.) rendering the facility incapable of adequate residual treatment. b. Any failure resulting in a discharge to surface waters. Any time self -monitoring indicates the program has gone out of compliance with its permit limitations. d. Land application of residuals abnormal in quantity or characteristic. e. Any discharge from a vehicle or piping system transporting residuals. Emergencies requiring reporting outside normal business hours shall call the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300. All noncompliance notifications shall file a written report to the Winston-Salem Regional Office within five days of first knowledge of the occurrence, and this report shall outline the actions proposed or taken to ensure the problem does not recur. [15ANCAC 02T .0108(b)(1)(A)] WQ0028547 Version 3.0 Shell Version 181130 Page 10 of 12 V. INSPECTIONS 1. The Permittee shall perform inspections and maintenance to ensure proper operation of the storage, distribution, and application facilities. [15A NCAC 02T .1110(f)] 2. The Permittee shall inspect the residuals storage, transport, and application facilities to prevent malfunctions, facility deterioration, and operator errors that may result in discharges of wastes to the environment, threats to human health, or public nuisances. The Permittee shall maintain an inspection log that includes the date and time of inspection, observations made, and maintenance, repairs, or corrective actions taken. The Permittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0 1 08(b) (1)(A), 02T .1110(f)] 3. Division authorized representatives may, upon presentation of credentials, enter and inspect any property, premises, or place related to the land application sites or facilities permitted herein at any reasonable time for determining compliance with this permit. Division authorized representatives may inspect or copy records maintained under the terms and conditions of this permit, and may collect groundwater, surface water, or leachate samples. [G.S. 143-215.3(a)(2)] VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to a Division enforcement action. [G.S. 143-215.6A, 143-215.613, 143-215.6C] 2. This permit is effective only with respect to the nature and volume of wastes described in the permit application, and Division -approved plans and specifications. [G.S. 143-215.1(d)] 3. Unless specifically requested and approved in this permit, there are no variances to administrative codes or general statutes governing the construction or operation of the facilities permitted herein. [I 5A NCAC 02T .0105(n)] 4. The issuance of this permit does not exempt the Permittee from complying with all statutes, rules, regulations, or ordinances that other jurisdictional government agencies (e.g., local, state, and federal) may require. [15A NCAC 02T .0105(c)(6)] 5. If the permitted residuals program change ownership, or the Permittee changes their name, the Permittee shall submit a permit modification request on Division -approved forms. The Permittee shall comply with all terms and conditions of this permit until the permit is transferred to the successor - owner. [G.S. 143-215.1(d3)] 6. This permit is subject to revocation or modification upon 60-day notice from the Division Director, in whole or part for: a. violation of any terms or conditions of this permit or Administrative Code Title 15A Subchapter 02T; b. obtaining a permit by misrepresentation or failure to disclose all relevant facts; c. the Permittee's refusal to allow authorized Department employees upon presentation of credentials: i. to enter the Permittee's premises where a system is located or where any records are required to be kept; ii. to have access to any permit required documents and records; iii. to inspect any monitoring equipment or method as required in this permit; or iv. to sample any pollutants; d. the Permittee's failure to pay the annual fee for administering and compliance monitoring; or WQ0028547 Version 3.0 Shell Version 181130 Page 11 of 12 e. a Division determination that the conditions of this permit are in conflict with North Carolina Administrative Code or General Statutes. [15A NCAC 02T .0110] 7. Unless the Division Director grants a variance, expansion of the facilities permitted herein shall not occur if any of the following apply: a. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has been convicted of environmental crimes under G.S. 143-215.613, or under Federal law that would otherwise be prosecuted under G.S. 143-215.6B, and all appeals of this conviction have been abandoned or exhausted. b. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has previously abandoned a wastewater treatment facility without properly closing the facility. c. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid a civil penalty, and all appeals of this penalty have been abandoned or exhausted. d. The Permittee or any parent, subsidiary, or other affiliate of the Permittee is currently not compliant with any compliance schedule in a permit, settlement agreement, or order. e. The Permittee or any parent, subsidiary, or other affiliate of the Permittee has not paid an annual fee. [15A NCAC 02T .0120(b), 02T .0120(d)] 8. This permit shall not be renewed if the Permittee or any affiliation has not paid the required annual fee. [15A NCAC 02T .0120(c)] Permit issued this the 16'' day of May 2019 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION Z.a�� �Q�k ?Linda Culpepper, Director Division of Water Resources By Authority of the Environmental Manage ent Commission Permit Number WQ0028547 WQ0028547 Version 3.0 Shell Version 181130 Page 12 of 12 ATTACHMENT A — APPROVED RESIDUAL SOURCES Town of Yanceyville Certification Date: May 16, 2019 Permit Number: WQ0028547 Version: 3.0 Monitoring Monitoring Monitoring Biological Maximum Frequency for Frequency for Frequency for Approved Owner Facility Name County Permit Number Residuals Dry Tons Non -hazardous Metals and Pathogen & Mineralization per Year r Characteristics Nutrients Vector Attraction Rate Reductions a, 5 Town of Yanceyville Yanceyville WTP Caswell NCO217010 — WP1 No 75 Annually Annually Annually 6 0.4 Town of Yanceyville Yanceyville WWTP Caswell NCO040011 Yes 244 Annually Annually Annually 0.3 Total 319 1. Maximum Dry Tons per Year is the amount of residuals approved for land application from each permitted facility. 2. Analyses to demonstrate that residuals are non -hazardous (i.e., TCLP, ignitability, reactivity, and corrosivity) as stipulated under permit Condition IV.2. 3. Testing of metals and nutrients as stipulated under permit Condition IV.3. 4. Analyses of pathogen and vector attraction reductions as stipulated under permit Condition IVA. 5. Monitoring frequencies are based on the actual dry tons applied per year using the table below, unless specified above. Dry Tons Applied Monitoring Frequency Dry Tons Applied (metric tons) (short tons per year) (40 CFR 503 and 15A NCAC 02T .1111 c < 290 < 319 Once per year (Annually) > 290 to < 1,500 > 319 to < 1,650 Once per quarter (4 x Year) > 1,500 to < 15,000 > 1,650 to < 16,500 Once per 60 days (6 x Year) > 15,000 > 16,500 Once per month (12 x Year) 6. Water Treatment Plant (WTP) residuals are exempt from meeting the vector attraction requirements in Condition IVA, provided they are not mixed with residuals that have been generated during the treatment of domestic wastewater, the treatment of animal processing wastewater, or the biological treatment of industrial wastewater. The WTP residuals must be treated and processed in a manner as to not meet the definition of Biological Residuals" as defined in 15A NCAC 02T .1102(6). If no land application events occur during a required sampling period (e.g., no land application occur during an entire year when annual monitoring is required), then no sampling data is required during the period of inactivity. The annual report shall include an explanation for missing sampling data. Those required to submit the annual report to United States Environmental Protection Agency (US EPA) may be required to make up the missed sampling. Contact the US EPA for additional information. WQ0028547 Version 3.0 Attachment A Page 1 of 1 ATTACHMENT B — APPROVED LAND APPLICATION SITES Town of Yanceyville — Town of Yanceyville RLAP Certification Date: May 16, 2019 Permit Number: WQ0028547 Version: 3.0 Field Owner Lessee County Latitude Longitude Net Acreage Dominant Soil Series Figures NC-CS-09-11 Hodges, Jennifer W. Caswell 36.4291250 -79.4408110 38.00 224B — Fairview 1 NC-CS-80-01 Hodges, Wayne Edward; Hodges, Virginia N. Caswell 36.4850470 -79.3836030 3.17 224B - Fairview 2 NC-CS-80-02 Hodges, Wayne Edward; Hodges, VirginiaN. Caswell 36.4832670 -79.3875060 11.06 263C -Poindexter 2 NC-CS-80-04 Hovatter, Ruby S. Sartin, David Caswell 36.4798030 -79.3903530 22.28 9.69 224B - Fairview 250B - Iredell 3 NC-CS-81-01 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3366720 -79.2479250 4 NC-CS-81-02 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3347190 -79.2466060 5.14 250B - Iredell 4 NC-CS-81-03 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3330530 -79.2462080 3.50 250B - Iredell 4 NC-CS-81-04 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3360530 -79.243022' 11.97 250B - Iredell 4,5 NC-CS-81-05 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3338860 -79.2418360 15.43 Orange 4,5 NC-CS-81-06 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3372280 -79.2404420 5.77 Helena 5 NC-CS-81-07 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3388530 -79.2425170 15.73 250B - Iredell 5 NC-CS-81-08 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3390940 -79.2384440 8.38 Helena 5 NC-CS-81-09 Williamson, Vernon H.; Williamson, Sylvia Caswell 36.3375060 -79.2383080 7.15 Helena 5 NC-CS-82-01 Crispin, Jon; Crispin, Bonnie; Smith, Dennis Paul Caswell 36.5010940 -79.271119' 4.75 224B — Fairview 6 NC-CS-82-02 Crispin, Jon; Crispin, Bonnie; Smith, Dennis Paul Caswell 36.5027740 -79.2723210 7.00 224B — Fairview 6 NC-CS-82-03 Crispin, Jon; Crispin, Bonnie; Smith, Dennis Paul Caswell 36.501675' -79.274375' 8.50 224B — Fairview 6 NC-CS-82-04 Crispin, Jon; Crispin, Bonnie; Smith, Dennis Paul Caswell 36.504599' -79.2767750 10.90 224B - Fairview 6 Total 188.42 WQ0028547 Version 3.0 Attachment B Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Town of Yanceyville Status Code a Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current n Proposed R Town of Yanceyville Yanceyville WWTP Caswell NCO040011 244 244 R Town of Yanceyville Yanceyville WTP Caswell 02-17-010 75 75 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) 'The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Yanceyville WWTP 2. Facility permit holder is: ❑ Federal, I❑ State, E Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, rl Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Matthew Malone — ORC Complete mailing address: I City: State: AM Zip: - Telephone number: (434) 203-7056 E-mail address: matthew/maloneginframark.com 4. Facility physical address: 666 Pine Drive City: Yanceyville State: NC Zip: 27379- Coordinates: Latitude: 36' 23' 39" Longitude: 79. 20' 27" Datum: NAD83 Level of accuracy: nearest second Method of measurement: GPS 5. Purpose of the facility: ® treatment of municipal wastewater, p treatment of 100% domestic wastewater, ❑ treatment of potable water, p treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and _= % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow:.45 MGD and facility average daily flow:.25 MGD 8. Average amount of residuals being generated at this facility 244 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: 2 sequential batch reactors — 270,000 gallons each Type and volume of residuals storage (i.e., outside of residuals treatment units): 5 acre lagoon — approximately 10,000,000 gallons II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ® 40 CFR Part 503 or ❑ 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ® Biological 0 Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): 3- b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 09/26/2023 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 <pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >170 OF (> 140°F) Passed reactivity test: J' yes r]no. HCN: <.25 mg/kg (<250) & H2S: 75 mg/kg (<500) TCLP Parameter Limit (mg//) Result (mgfi) TCLP Parameter Limit (mgfi) Result (mgfi) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 214,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 214,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 09/27/2023 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 <13.2 Cadmium 85 39 <<2.63 Copper 4,300 1,500 404 Lead 840 300 66.8 Mercury 57 17 1.61 Molybdenum 75 n/a <7.89 Nickel 420 420 33.8 Selenium 100 100 <18.4 Zinc 7,500 2,800 937 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 1.91 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: WMpoint Analytical and Date of analysis: 09/27/2023 Parameter Result (mglkg) Aluminum 23,300 Ammonia -Nitrogen 4,090 Calcium 21,400 Magnesium 3,980 Nitrate -Nitrite Nitrogen 19,800 pH (Standard Unit) 7.3 Phosphorus 20,400 Potassium 3,510 Sodium 2,720 Total Kjeldahl Nitrogen 64,700 c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): .62 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 30 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1s) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 40,030 50,935 Injection/Incorporation 42,075 52,980 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B. ® Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T. 1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, V air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ® Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ® Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T. 1107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of I%.r Data use subject to license. #TN ® DeLorme. Map® 8. fm (9,V" www.delorme.com Quantitative Justification for Residuals Production Rate Facility: Town of Yanceyville WWTP Town of Yanceyville WTP Requested Permitted Rate: 244 dry tons/year— WWTP 75 dry tons/year - WTP Justification WWTP: The Town of Yanceyville WWTP currently produces roughly 250 dry tons of biosolids, based on the calculations below. Justification WTP: The Town of Yanceyville WTP currently produces roughly 75 dry tons of biosolids, based on the calculations below. Calculations WWTP: Based on the most recent hauling year of 2023, there were 442,500 gallons applied. Using 1,000,000 in our calculation and the most recent sampling data showing 1.91% residual solids. (1,000,000 gal/yr) x (1.91% solids) x (8.34 Ibs/gal) = 80 dt/yr (2,000 Ibs/ton) Calculations WTP: Based on the most recent hauling year of 2022, there were 344,500 gallons applied. Using 1,000,000 in our calculation and the most recent sampling data showing 2% residual solids. (1,000,000 gal/yr) x (2% solids) x (8.34 Ibs/gal) = 83.4 dt/yr (2,000 Ibs/ton) Waypointo ANALYTICAL 10/9/2023 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 23-271-0003 Client Project Description: Yanceyville 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 9/28/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/29/2024 Arkansas State Program 88-0650 02/07/2024 California State Program 2904 06/30/2024 Florida State Program - NELAP E871157 06/30/2024 Georgia State Program C044 11/14/2025 Georgia State Program 04015 06/30/2024 Illinois State Program - NELAP 200078 10/31/2024 Kentucky State Program 80215 06/30/2024 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2024 Mississippi State Program MS 11/14/2025 North Carolina State Program 47701 07/31/2024 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2024 South Carolina State Program 84002 06/30/2024 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2024 Virginia State Program 00106 06/30/2024 Virginia State Program - NELAP 460181 09/14/2024 Page 1 of 1 00001/23-271-0003 Page 2 of 8 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 23-271-0003 Client Project Description: Yanceyville Lab No Client Sample ID Matrix Date Collected Date Received 88155 Yancyville WWTP Solids 09/27/2023 10:00 09/28/2023 Page 3 of 8 Waypointo ANALYTICAL Client: EMA Resources Inc Project: Yanceyville Lab Report Number: 23-271-0003 Date: 10/9/2023 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 fax 901.213.2440 www.waypointanalytical.com CASE NARRATIVE Metals Analysis Method 601 OD Sample 83723 (Grab) Analyte: Aluminum QC Batch No: 1-708175/1-707770 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 83723 (Grab) Analyte: Calcium QC Batch No: 1-708175/1-707770 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 83723 (Grab) Analyte: Iron QC Batch No: 1-708175/1-707770 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 83723 (Grab) Analyte: Potassium QC Batch No: 1-708544/1-707770 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 83723 (Grab) Analyte: Magnesium QC Batch No: 1-708175/1-707770 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 83723 (Grab) Analyte: Manganese QC Batch No: 1-708175/1-707770 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 Waypointo ANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Project Yanceyville Information : 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Report Date : 10/09/2023 nReceived : 09/28/2023 C-�*�-� = Connie Cook Report Number : 23-271-0003 REPORT OFANALYSIS Project Manager Lab No : 88155 Matrix: Solids Sample ID : Yancyville WWTP Sampled: 9/27/2023 10:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 98.1 % 1 09/29/23 16:05 CAH SW-DRYWT Ammonia Nitrogen 40903 mg/Kg - dry 842 5260 1 10/05/23 12:04 JPJ 4500NH3C-2011 Nitrate+Nitrite-N 19800 mg/Kg - dry 52.6 263 1 10/05/23 11:38 CLP 4500NO3F-2016 Organic N 606303 mg/Kg - dry 842.1 5263 1 10/05/23 07:05 CALCULATION pH 7.3 S.U. 1 10/02/2316:45 CNB 9045D Total Solids 1.91 % 0.010 0.010 1 09/29/23 16:05 CAH 2540G-2011 Total Volatile Solids 55.1 % 0.010 0.010 1 09/29/23 16:05 CAH 2540G-2011 Total Kjeldahl Nitrogen 64700 mg/Kg - dry 526 13200 1 10/05/23 07:05 JPJ ;M-4500-NH3C-TKI` Phosphorus 20400 mg/Kg - dry 147 263 1 10/02/23 20:42 BKN 6010D Aluminum 23300 mg/Kg - dry 245 263 1 10/02/23 20:42 BKN 6010D Arsenic <13.2 mg/Kg - dry 13.2 26.3 1 10/02/23 20:42 BKN 6010D Cadmium <2.63 mg/Kg - dry 2.63 5.26 1 10/02/23 20:42 BKN 6010D Calcium 21400 mg/Kg - dry 2040 2630 1 10/02/23 20:42 BKN 6010D Chromium 45.1 mg/Kg - dry 13.2 13.2 1 10/02/23 20:42 BKN 6010D Copper 404 mg/Kg - dry 15.8 26.3 1 10/02/23 20:42 BKN 6010D Iron 24800 mg/Kg - dry 450 526 1 10/02/23 20:42 BKN 6010D Lead 66.8 mg/Kg - dry 10.5 15.8 1 10/02/23 20:42 BKN 6010D Magnesium 3980 mg/Kg - dry 137 263 1 10/02/23 20:42 BKN 6010D Manganese 526 mg/Kg - dry 18.4 26.3 1 10/02/23 20:42 BKN 6010D Mercury 1.613 mg/Kg - dry 1.17 9.74 1 10/03/23 12:12 MRE 7471A Molybdenum <7.89 mg/Kg - dry 7.89 13.2 1 10/02/23 20:42 BKN 6010D Nickel 33.8 mg/Kg - dry 7.89 13.2 1 10/02/23 20:42 BKN 6010D Potassium 3510 mg/Kg - dry 326 526 1 10/02/23 20:42 BKN 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Page 5 of 8 • Waypoint 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Project Yanceyville Mr. Brent Collins Report Date : 10/09/2023 755 Yadkinville Rd Information : Received : 09/28/2023 Mocksville , NC 27028 Connie Cook Report Number : 23-271-0003 REPORT OFANALYSIS Project Manager Lab No : 88155 Matrix: Solids Sample ID : Yancyville WWTP Sampled: 9/27/2023 10:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium <18.4 mg/Kg - dry 18.4 26.3 1 10/02/23 20:42 BKN 6010D Sodium 2720 mg/Kg - dry 684 1320 1 10/02/23 20:42 BKN 6010D Zinc 937 mg/Kg - dry 44.7 65.8 1 10/02/23 20:42 BKN 6010D Sulfur 14400 mg/Kg - dry 274 526 1 10/02/23 20:42 BKN 6010D Sodium Absorption Ratio 0.61 Ratio 0.01 0.01 1 10/02/23 20:42 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 6 of 8 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 23-271-0003 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IT100 Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IMakayla Weaver Date & Time: 09/28/2023 09:01:50 Page 7 of 8 0 a N LLCj) '� E E E cJ 4 P N 0 m m 0 ON U? � N U C � E � Ll Z MEv V a= d V u M O a a Q 0- ^� 0u7zzTmmu Q 3 m [n m CL o iL W L4 n' a :: of Q m u o 0 x_ N c w s C� 7 a Z z w n y� V y � y W T T 7• � Q `ter Ir _J E E U p ° SAI F F r L Q u O h t `�-- a 0. c a r W iY 0 ,w �❑ a H m ❑ m ❑ m ❑ SPHOS 1210l is C v Q. CL Q V7 3 6 im m "IN 3lUebJO/aMlllN � a ] eiuourUry1N}�1 w oa W o 0 z y � I W W LU Y O V oGo N w C CC ' GC D Fi a mWoLog1 11 5le�aW ` z 2 0 p IL a0 � V t7 CJ N C7 N alisodwo(7J jo C m C Vi ❑ N y �` 4 V t Q a gea(g) a .0 a (Aa)j of japa l) xia3eW t , 7 a a C a C c C sjauieluoo;o lagwnN a a V cC � N C mC[If a ti! a o iu m CV) v- N a U 4 w a a CL a c yCL E w } n co Q a o =F p NOEL n `w a �Z a v �¢ W z °o 0 C EN SC fl7 u y j r v�� O a o N p V W 1` 7i 0. 0. Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 J_..a Contact: Brent Collins Client: GMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech Work Order # 09262312 Parameters gei > % Total Solids 1.96 % Fecal Coliform (Class B Sludge) 10,204 CFU/g Meritech Work Order # 09262313 Parameters Result % Total Solids 2.13 % Fecal Coliform (Class B Sludge) 9,859 CFU/g Meritech Work Order # 0926231 Parameteu % Total Solids Fecal Coliform (Class B Sludge) Sample: Yanceyville 1 Analysis Date 9/27/23 dry wt 9/26/23 Sample: Yanceyville 2 Analysis Date 9/27/23 dry wt 9/26/23 4 Sample: Yanceyville 3 Result Analysis Date 1.61 % 9/27/23 2,258 CFU/g dry wt 9/26/23 Meritech Work Order # 09262315 Sample: Yanceyville 4 Parameters Result Analysis Date % Total Solids 1.97 % 9/27/23 Fecal Coliform (Class B Sludge) 14,213 CFU/g dry wt 9/26/23 Revised Report Date: Report Date: Date Sample Rcvd: Reporting Limit 0-100 % 130 CFU/g dry wt Reporting Limit 0-100 % 130 CFU/g dry wt Reporting Limit 0-100 % 130 CFU/g dry wt Repo fi g-Limit 0-100 % 130 CFU/g dry wt Page 1 1012 612023 10/3/2023 9/26/2023 9/26/23 Method SM 2540B SM 9222D 9/26/23 Method SM 2540B SM 9222D 9/26/23 Meth SM 2540B SM 9222D 9/26/23 Me tt god SM 2540B SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No. 165 • Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Meritech Work Order # 09262316 Parameters Result % Total Solids 2.07 % Fecal Coliform (Class B Sludge) 4,392 CFU/g Meritech Work Order # 0926231 Parameters % Total Solids Fecal Coliform (Class B Sludge) 2.40 % 1,515 CFU/g Meritech Work Order # 09262318 Parameterj Result % Total Solids 2.31 % Fecal Coliform (Class B Sludge) 3,148 CFU/g Sample: Yanceyville 5 Analysis Date 9/27/23 dry wt 9/26/23 Sample: Yanceyville 6 Analysis Date 9/27/23 dry wt 9/26/23 Sample: Yanceyville 7 Analysis Date 9/27/23 dry wt 9/26/23 1 hereby certify that 1 have reviewed and approve these data. Revised Report Date: Report Date: Date Sample Rcvd: Reporting Limit 0-100 % 130 CFU/g dry wt Reporting Limit 0-100 % 130 CFU/g dry wt Reporting Limit 0-100 % 130 CFU/g dry wt Page 2 1012612023 10/3/2023 9/26/2023 9/26/23 Method SM 2540B SM 9222D 9/26/23 Method SM 2540B SM 9222D 9/26/23 Nlgth9d SM 2540B SM 9222D Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 6A-1016 Chain of Custody Record (COC) NPDES#: Client: EMA Resources Inc. Phone: 336-751-1441 Address:_ 755 Yadkinville Rd Fax: 336-751-1442 Mocksville NC 27028 Email:�brent.collins@emarescurcesinc.com Project: P.O.#: Attention:_Brent Collins Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. Circle all that apply: mai preferred), Fax, Mail Sftl�l°—days) 3Cy� zOS J MERITECH INC. 1 ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechlabs.com Sample Location and/or ID # Sampling Dates &Times Person Taking Sample (Sign/Print): Lab Use Only Start End comp? Grab? a of Cont. Test(s) Required On Ice? M / No pH OK? Cl OK? Date Time Date Time YOACeyvilit- j 9%21i12-3 /p;IS G 1 Fecal Coliform 2 17 3 Vy -7 V V 1 Temperature Upo�f Receipt: rL Method of Shipment: `** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Comments: Compositor # JJug # ❑ UPS ❑ Fed Ex Are these results for regulatory purposes? Yes 0 No ❑ Report results in: mg/L ❑ mg/kg o- ug/L ❑ Hand Delivery Relinquished by: / Date: Time: � � y�y� 2.3 Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: ed b j I) ,BAteti j lTin L Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 ;a ; Contact: Brent Collins Report Date: 10/2/2023 Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Date Sample Rcvd: 9/26/2023 Meritech Work Order # 09262319 Sample: Yanceyville - VS In Grab 9/26/23 Parameters Result Analysis Date Reporting Limit Method • Total Solids 0.29 % 9/27/23 0-100 % SM 2540B • Volatile Solids 0.21 % 9/27/23 0-100 % SM 2540E Meritech Work Order # 09262320 Sample: Yanceyville - VS Out Grab 9/26/23 Parameters Result Analysis Date Reporting Limit Method • Total Solids 2.91 % 9/27/23 0-100 % SM 2540B • Volatile Solids 0.86 % 9/27/23 0-100 % SM 2540E 1 hereby certify that 1 have reviewed and approve these data. Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 5-9-2016 Chain of Custody Record (COC) NPDES#: Client: EMA Resources Inc. Phone:336-751-1441 Address: 755 Yadkinville Rd Fax: 336-751-1442 Mocksville NC 27028 Email: brent.collins@emaresourcesinc.com Project: P.O.#: Attention: Brent Collins Turn Around Time* How would you like your report sent? *RUSH work needs prior approval. stCd1lOdays) 3-5 Days z= s Circle all that apply: S (preferred), Fax, Mail L ] L JUSe ME RITECH INC. ENVIRONMENTAL LABORATORIES 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com WWW.fYlerltecillabS.COfYI Sample Location and/or ID # Sampling Dates &Times l Person Taking Sample (Sign/Print): ' Lab Only Y Start End Comp? Grab? Cont.nt Test(s) Required On Ice? Yes / No pH OK? Cl OK? Date Time Date Time you c e-%j; 1 N 91,Wok3 io : 0-0 C. I Volatile Solids V \Is O j T 9/26,/8 /b: r S Temperature Upon Receipt: zy Method of Shipment: *** Dechlorination <0.5 p m of Ammonia, Cvanide, Phenol and TKN samples must be done in the field prior to preservation. *** Comments: Compositor # ❑ UPS _ Jug # ❑ Fed Ex Are these results for regulatory purposes? Yes 9-� No ❑ Report results in: mg/L ❑ mg/kg EJ' ug/L ❑ Hand Delivery Relinquished by: jai/ Date: Time: `��.�- 9�Za/Zj /o; �Q Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: eceived'Isy Le � � [ TL Z l I 13 ace Analytical ' ANALYTICAL REPORT October 09, 2023 EMA Resources Sample Delivery Group: L166O181 Samples Received: 09/27/2023 Project Number: Description: Sludge Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By zez�7��' Reagan Johnson Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 1 of 22 TABLE OF CONTENTS Cp: Cover Page u Tc: Table of Contents 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 Fss] YANCEYVILLE L1660181-01 5 Fn Qc: Quality Control Summary 7 Wet Chemistry by Method 9012 B 7 Fr Wet Chemistry by Method 9034-9030B 8 Wet Chemistry by Method 9045D 9 Rc Wet Chemistry by Method D93/1010A 10 F Mercury by Method 7470A 11 Metals (ICP) by Method 6010D 12 [Al Volatile Organic Compounds (GC/MS) by Method 8260D 14 Chlorinated Acid Herbicides (GC) by Method 8151A 16 RC Pesticides (GC) by Method 8081B 17 Semi Volatile Organic Compounds (GC/MS) by Method 8270E 18 GI: Glossary of Terms 20 al: Accreditations & Locations 21 Sc: Sample Chain of Custody 22 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 2 of 22 YANCEYVILLE L1660181-01 Waste Method Preparation by Method 1311 Preparation by Method 1311 Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260D Chlorinated Acid Herbicides (GC) by Method 8151A Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270E SAMPLE SUMMARY Collected by Brent Collins Collected date/time Received date/time 09/26/2310:00 09/27/23 09:00 C P Batch Dilution Preparation Analysis date/time date/time WG2141719 1 09/29/2316:39 09/29/2316:39 WG2141899 1 09/29/2314:08 09/29/2314:08 WG2142337 1 09/30/2317:54 10/01/23 20:55 WG2143775 1 09/30/23 09:21 10/02/23 20:00 W G 2141964 1 09/2 9/2313:41 10/02/2314:19 WG2143483 1 10/03/23 02:56 10/03/23 02:56 W G 2143179 1 10/02/231133 10/02/2316:03 W G 21432 55 1 10/02/2312:33 10/02/2317:2 8 W G 2142404 1 10/01/2315:27 10/01/2315:27 W G 2142 975 1 10/02/2314:22 10/03/2312:40 WG2144467 1 10/04/23 2100 10/05/23 03:57 WG2144463 1 10/05/23 05:49 10/05/23 20:28 Analyst PNK BTP LDT CAT ARID WOS NDL DJS DYW HMH JMB AED Location FC Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fn Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fr Mt. Juliet, TN Mt. Juliet, TN Rc Mt. Juliet, TN Mt. Juliet, TN GI F RC ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 3 of 22 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the FP appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 0 Fr -� Rc GI Reagan Johnson [Al Project Manager RC Project Narrative All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 4 of 22 SAMPLE RESULTS - 01 L1660181 YANCEYVILLE Collected date/time: 09/26/23 10:00 Preparation by Method 1311 Result Analyte TCLP Extraction TCLP ZHE Extraction - Initial pH 6.73 Final pH 6.05 Wet Chemistry by Method 9012 B Qualifier Prep Batch date / time 9/29/2023 4:39:41 PM WG2141719 9/29/2023 2:08:35 PM WG2141899 9/29/2023 4:39:41 PM WG2141719 9/29/2023 4:39:41 PM WG2141719 Result Qualifier RDL Analyte mg/kg mg/kg Reactive Cyanide ND 0.250 Wet Chemistry by Method 9034-9030B Dilution Analysis Batch date / time 1 10/01/2023 20:55 WG2142337 Result Qualifier RDL Dilution Analysis Batch Analyte mg/kg mg/kg date / time Reactive Sulfide ND 75.0 1 10/02/2023 20:00 WG2143775 Wet Chemistry by Method 9045D Result Qualifier Dilution Analysis Batch Analyte su date / time Corrosivity by pH 6.93 T8 1 10/02/202314:19 WG2141964 Sample Narrative: L1660181-01 WG2141964: 6.93 at 22.9C Wet Chemistry by Method D93/1010A Result Analyte Deg. F Ignitability DNI at170 Mercury by Method 7470A Result Analyte mg/I Mercury ND Metals (ICP) by Method 6010D Qualifier Dilution Analysis Batch date / time 1 10/03/2023 02:56 WG2143483 Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I date / time 0.0100 0.20 1 10/02/202316:03 WG2143179 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Arsenic ND 0.100 5 1 10/02/202317:28 WG2143255 Barium ND 0.100 100 1 10/02/202317:28 WG2143255 Cadmium ND 0.100 1 1 10/02/202317:28 WG2143255 Chromium ND 0.100 5 1 10/02/202317:28 WG2143255 Lead ND 0.100 5 1 10/02/202317:28 WG2143255 Selenium ND 0.100 1 1 10/02/202317:28 WG2143255 Silver ND 0.100 5 1 10/02/202317:28 WG2143255 Volatile Organic Compounds (GC/MS) by Method 8260D Analyte Benzene Carbon tetrachloride Chlorobenzene Chloroform 1,2-Dichloroethane Result Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I mg/I date/time ND 0.0500 0.50 1 10/01/202315:27 WG2142404 ND 0.0500 0.50 1 10/01/202315:27 WG2142404 ND 0.0500 100 1 10/01/202315:27 WG2142404 ND 0.250 6 1 10/01/202315:27 WG2142404 ND 0.0500 0.50 1 10/01/202315:27 WG2142404 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 5 of 22 YANCEYVILLE SAMPLE RESULTS Collected date/time: 09/26/23 10:00 L1660181 Volatile Organic Compounds (GC/MS) by Method 8260D - 01 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,1-Dichloroethene ND 0.0500 0.70 1 10/01/202315:27 WG2142404 2-Butanone (MEK) ND 0.500 200 1 10/01/202315:27 WG2142404 Tetrachloroethene ND 0.0500 0.70 1 10/01/202315:27 WG2142404 Trichloroethene ND 0.0500 0.50 1 10/01/202315:27 WG2142404 Vinyl chloride ND 0.0500 0.20 1 10/01/202315:27 WG2142404 (S) Toluene-dH 110 80.0-120 101011202315.27 WG2142404 (S) 4-Bromofluorobenzene 878 77.0-126 101011202315.27 WG2142404 (S) 1,2-Dichloroethene-d4 116 70.0-130 101011202315.27 WG2142404 Chlorinated Acid Herbicides (GC) by Method 8151A Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 2,4,5-TP (Silvex) ND 0.00200 1 10/03/202312:40 WG2142975 2,4-D ND 0.00200 1 10/03/202312:40 WG2142975 (S) Z4-Dichlorophenyl Acetic Acid 90.0 14.0-158 101031202312.40 WG2142975 Pesticides (GC) by Method 8081B Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Chlordane ND 0.00500 0.03 1 10/05/2023 03:57 WG2144467 Endrin ND 0.00500 0.02 1 10/05/2023 03:57 WG2144467 Heptachlor ND 0.00500 0.0080 1 10/05/2023 03:57 WG2144467 Heptachlor epoxide ND 0.00500 0.0080 1 10/05/2023 03:57 WG2144467 Lindane ND 0.00500 0.40 1 10/05/2023 03:57 WG2144467 Methoxychlor ND 0.00500 10 1 10/05/2023 03:57 WG2144467 Toxaphene ND 0.0100 0.50 1 10/05/2023 03:57 WG2144467 (S) Decochlorobiphenyl 53.2 10.0-128 1010512023 03.57 WG2144467 (S) Tetrochloro-m-xylene 84.2 10.0-127 1010512023 03.57 WG2144467 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Analyte 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachlorobenzene Hexachloro-1,3-butadiene Hexachloroethane Nitrobenzene Pyridine 3&4-Methyl Phenol 2-Methylphenol Pentachlorophenol 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol (S) 2-Fluorophenol (S) Phenol-d5 (S) Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Z4,6-Tribromophenol (S) p-Terphenyl-d14 ACCOUNT: EMA Resources Result Qualifier RDL Limit Dilution Analysis Batch mg/I mg/I mg/I date/time ND 0.100 7.50 1 10/05/2023 20:28 WG2144463 ND 0.100 0.13 1 10/05/2023 20:28 WG2144463 ND 0.100 0.13 1 10/05/2023 20:28 WG2144463 ND 0.100 0.50 1 10/05/2023 20:28 WG2144463 ND 0.100 3 1 10/05/2023 20:28 WG2144463 ND 0.100 2 1 10/05/2023 20:28 WG2144463 ND 0.100 5 1 10/05/2023 20:28 WG2144463 ND 0.100 400 1 10/05/2023 20:28 WG2144463 ND 0.100 200 1 10/05/2023 20:28 WG2144463 ND 0.100 100 1 10/05/2023 20:28 WG2144463 ND 0.100 400 1 10/05/2023 20:28 WG2144463 ND 0.100 2 1 10/05/2023 20:28 WG2144463 28.4 10.0-120 101051202320.28 WG2144463 19.6 10.0-120 101051202320.28 WG2144463 79.8 10.0-127 101051202320.28 WG2144463 65.3 10.0-130 101051202320.28 WG2144463 78.0 10.0-155 101051202320.28 WG2144463 79.8 10.0-128 101051202320.28 WG2144463 PROJECT: SDG: DATE/TIME: PAGE: L1660131 10/09/23 11:09 6 of 22 WG2142337 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9012 B L1660181-01 Method Blank (MB) (MB) R3930233-1 10/01/23 20:45 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Reactive Cyanide U 0.0390 0.250 L1660272-01 Original Sample (OS) • Duplicate (DUP) (OS) L1660272-01 10/01/23 21:08 • (DUP) R3930233-3 10/01/23 2109 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg Reactive Cyanide 0.851 1.23 1 36.7 P1 20 Sample Narrative: DUP: RPD failure due to matrix interference. L1660630-01 Original Sample (OS) • Duplicate (DUP) (OS) L1660630-01 10/01/23 21:11 • (DUP) R3930233-4 10/01/23 2112 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg Reactive Cyanide ND ND 1 0.000 20 Laboratory Control Sample (LCS) (LCS) R3980233-2 10/01/23 20:46 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/kg mg/kg Reactive Cyanide 2.50 2.48 99.3 85.0-115 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 7 of 22 WG2143775 Wet Chemistry by Method 9034-9030B Method Blank (MB) (MB) R3980852-1 10/02/23 2000 MB Result Analyte mg/kg Reactive Sulfide U MB Qualifier MB MDL MB RDL mg/kg mg/kg 30.0 75.0 Laboratory Control Sample (LCS) (LCS) R3980852-2 10/02/23 20:00 Spike Amount LCS Result Analyte mg/kg mg/kg Reactive Sulfide 100 76.4 QUALITY CONTROL SUMMARY L1660181-01 LCS Rec. Rec. Limits LCS Qualifier 76.4 53.8-124 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 3 of 22 WG2141964 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9045D L1660181-01 Laboratory Control Sample (LCS) C (LCS) R3930563-1 10/02/231419 p Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier ITC] Analyte su su % % Corrosivity by pH 10.0 9.99 99.9 99.0-101 F Sample Narrative: SS LCS: 9.99 at 21.6C [Cn] 5 Sr �GI FAI FSC1 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 9 of 22 WG2143483 QUALITY CONTROL SUMMARY Wet Chemistry by Method D93/1010A L1660181-01 L1660066-01 Original Sample (OS) • Duplicate (DUP) (OS) L1660066-01 10/03/23 02:56 • (DUP) R3930756-3 10/03/23 02:56 Original Result DUP Result Dilution DUP RPD Analyte Deg. F Deg. F Ignitability DNI at170 DNI at170 1 0.000 L1660377-02 Original Sample (OS) • Duplicate (DUP) DUP Qualifier DUP RPD Limits i 10 (OS) L1660377-02 10/03/23 02:56 • (DUP) R3930756-4 10/03/23 02:56 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte Deg. F Deg. F Ignitability DNI at170 DNI at170 1 0.000 10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3930756-1 10/03/23 02:56 • (LCSD) R3930756-2 10/03/23 02:56 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte Deg. F Deg. F Deg. F Ignitability 126 125 127 98.8 100 95.6-104 1.59 10 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 10 of 22 WG2143179 QUALITY CONTROL SUMMARY Mercury by Method 7470A L1660181-01 Method Blank (MB) (MB) R3930639-1 10/02/231519 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Mercury U 0.00330 0.0100 Laboratory Control Sample (LCS) (LCS) R3980639-2 10/02/2315:26 Spike Amount LCS Result LCS Rec. Analyte mg/I mg/I Mercury 0.0300 0.0286 95.4 Rec. Limits LCS Qualifier 80.0-120 L1660170-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1660170-03 10/02/23 15:29 • (MS) R3930639-3 10/02/2315:31 • (MSD) R3930639-4 10/02/23 15:34 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Mercury 0.0300 ND 0.0297 0.0301 99.0 100 1 75.0-125 1.34 20 L1660194-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1660194-02 10/02/2316:06 • (MS) R3930639-5 10/02/2315:39 • (MSD) R3930639-6 10/02/2315:41 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Mercury 0.0300 ND 0.0258 0.0296 86.1 98.7 1 75.0-125 13.6 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 11 of 22 WG2143255 Metals (ICP) by Method 6010D Method Blank (MB) (MB) R3930304-1 10/02/2316:42 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Arsenic U 0.0333 0.100 Barium U 0.0333 0.100 Cadmium U 0.0333 0.100 Chromium U 0.0333 0.100 Lead U 0.0333 0.100 Selenium U 0.0333 0.100 Silver U 0.0333 0.100 Laboratory Control Sample (LCS) (LCS) R3980804-2 10/02/23 16:45 QUALITY CONTROL SUMMARY L1660181-01 Spike Amount LCS Result LCS Rec. Rec. Limits Analyte mg/I mg/I Arsenic 10.0 10.7 107 80.0-120 Barium 10.0 9.94 99.4 80.0-120 Cadmium 10.0 9.91 99.1 80.0-120 Chromium 10.0 9.57 95.7 80.0-120 Lead 10.0 9.75 97.5 80.0-120 Selenium 10.0 10.3 103 80.0-120 Silver 2.00 1.73 86.7 80.0-120 LCS Qualifier L1660194-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1660194-02 10/02/2316:43 • (MS) R3930304-4 10/02/2316:53 • (MSD) R3930304-5 10/02/2316:56 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Arsenic 10.0 ND 10.5 10.4 105 104 Barium 10.0 0.106 10.4 10.2 103 101 Cadmium 10.0 ND 9.89 9.78 98.9 97.8 Chromium 10.0 ND 9.83 9.63 98.3 96.3 Lead 10.0 ND 9.82 9.65 98.2 96.5 Selenium 10.0 ND 9.86 9.65 98.6 96.5 Silver 2.00 ND 1.72 1.71 86.1 85.4 Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 75.0-125 1.12 20 1 75.0-125 1.41 20 1 75.0-125 1.12 20 1 75.0-125 2.10 20 1 75.0-125 1.73 20 1 75.0-125 2.12 20 1 75.0-125 0.816 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 12 of 22 WG2143255 QUALITY CONTROL SUMMARY Metals (ICP) by Method 6010D L1660181-01 L1660460-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1660460-02 10/02/2316:59 • (MS) R3930304-6 10/02/23 17:02 • (MSD) R3930304-7 10/02/23 17:04 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Arsenic 10.0 ND 10.8 10.8 108 108 Barium 10.0 0.880 11.0 10.9 101 100 Cadmium 10.0 ND 10.1 10.0 101 100 Chromium 10.0 ND 9.78 9.71 97.8 97.1 Lead 10.0 ND 9.89 9.91 98.9 99.1 Selenium 10.0 ND 10.4 10.4 103 103 Silver 2.00 ND 1.77 1.75 88.6 87.7 ACCOUNT: EMA Resources PROJECT: Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 75.0-125 0.775 20 1 75.0-125 0.964 20 1 75.0-125 0.620 20 1 75.0-125 0.726 20 1 75.0-125 0.251 20 1 75.0-125 0.658 20 1 75.0-125 1.01 20 SDG: DATE/TIME: PAGE: L1660131 10/09/23 11:09 13 of 22 WG2142404 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260D L1660181-01 Method Blank (MB) (MB) R3931330-3 10/01/231109 MB Result Analyte mg/I Benzene U Carbon tetrachloride U Chlorobenzene U Chloroform U 1,2-Dichloroethane U 1,1-Dichloroethene U 2-Butanone (MEK) U Tetrachloroethene U Trichloroethene U Vinyl chloride U (S) Toluene-dH 109 (S) 4-Bromofluorobenzene 89.3 (S) 1,2-Dichloroethane-d4 112 MB Qualifier MB MDL mg/I MB RDL mg/I 0.0167 0.0500 0.0167 0.0500 0.0167 0.0500 0.0833 0.250 0.0167 0.0500 0.0167 0.0500 0.167 0.500 0.0167 0.0500 0.0167 0.0500 0.0167 0.0500 80.0-120 77.0-126 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3981330-1 10/01/23 09:43 • (LCSD) R3981330-2 10/01/2310:05 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits Analyte mg/I mg/I mg/I Benzene 0.250 0.262 0.260 105 104 70.0-123 Carbon tetrachloride 0.250 0.269 0.276 108 110 68.0-126 Chlorobenzene 0.250 0.259 0.251 104 100 80.0-121 Chloroform 0.250 0.278 0.278 ill ill 73.0-120 1,2-Dichloroethane 0.250 0.242 0.241 96.8 96.4 70.0-128 1,1-Dichloroethene 0.250 0.255 0.248 102 99.2 71.0-124 2-Butanone (MEK) 1.25 1.14 1.07 91.2 85.6 44.0-160 Tetrachloroethene 0.250 0.257 0.270 103 108 72.0-132 Trichloroethene 0.250 0.241 0.245 96.4 98.0 78.0-124 Vinyl chloride 0.250 0.212 0.244 84.8 97.6 67.0-131 (S) Toluene-dH 106 105 80.0-120 (S) 4-Bromofluorobenzene 90.1 90.9 77.0-126 (S) 1,2-Dichloroethane-d4 105 108 70.0-130 LCS Qualifier LCSD Qualifier RPD 0.766 2.57 3.14 0.000 0.414 2.78 6.33 4.93 1.65 14.0 RPD Limits 20 20 20 20 20 20 20 20 20 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 14 of 22 WG2142404 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260D L1660181-01 L1659704-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1659704-02 10/01/23 12:14 • (MS) R3931330-4 10/01/23 13:40 • (MSD) R3931330-5 10/01/23 19:01 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Benzene 0.250 ND 0.192 0.196 76.8 78.4 Carbon tetrachloride 0.250 ND 0.232 0.207 92.8 82.8 Chlorobenzene 0.250 ND 0.189 0.194 75.6 77.6 Chloroform 0.250 ND ND ND 91.2 94.0 1,2-Dichloroethane 0.250 ND 0.201 0.207 80.4 82.8 1,1-Dichloroethene 0.250 ND 0.207 0.195 82.8 78.0 2-Butanone (MEK) 1.25 ND 0.824 0.957 65.9 76.6 Tetrachloroethene 0.250 ND 0.182 0.196 72.8 78.4 Trichloroethene 0.250 ND 0.177 0.183 70.8 73.2 Vinyl chloride 0.250 ND 0.165 0.153 66.0 61.2 (S) Toluene-dH 104 106 (S) 4-Bromofluorobenzene 86.3 85.4 (S) 1,2-Dichloroethane-d4 116 114 ACCOUNT: EMA Resources PROJECT: Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 17.0-158 2.06 27 1 23.0-159 11.4 28 1 33.0-152 2.61 27 1 29.0-154 3.02 28 1 29.0-151 2.94 27 1 11.0-160 5.97 29 1 10.0-160 14.9 32 1 10.0-160 7.41 27 1 10.0-160 3.33 25 1 10.0-160 7.55 27 80.0-120 77.0-126 70.0-130 SDG: DATE/TIME: PAGE: L1660131 10/09/23 11:09 15 of 22 WG2142975 Chlorinated Acid Herbicides (GC) by Method 8151A Method Blank (MB) (MB) R3931026-1 10/03/23 04:47 MB Result Analyte mg/I 2,4,5-TP (Silvex) U 2,4-D U (S) Z4-Dichlorophenyl Acetic 84.0 Acid QUALITY CONTROL SUMMARY L1660181-01 MB Qualifier MB MDL MB RDL mg/I mg/I 0.000667 0.00200 0.000667 0.00200 14.0-158 Laboratory Control Sample (LCS) (LCS) R3981026-2 10/03/23 04:58 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I 2,4,5-TP (Silvex) 0.0500 0.0400 80.0 50.0-125 2,4-D 0.0500 0.0533 107 50.0-120 E (S) Z4-Dichlorophenyl Acetic 84.2 14. 0-158 Acid L1659612-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1659612-01 10/03/23 05:31 • (MS) R3931026-3 10/03/23 05:43 • (MSD) R3931026-4 10/03/23 05:54 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I 2,4,5-TP (Silvex) 0.0500 ND 0.0559 0.0374 112 74.8 2,4-D 0.0500 ND 0.0758 0.0574 152 115 (S) Z4-Dichlorophenyl Acetic 842 242 Acid Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits 1 50.0-125 E J3 39.7 20 1 50.0-120 E J5 E J3 27.6 20 14.0-158 11 11 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 16 of 22 WG2144467 QUALITY CONTROL SUMMARY Pesticides (GC) by Method 8081B L1660181-01 Method Blank (MB) (MB) R3932203-1 10/05/23 00:55 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Chlordane U 0.00167 0.00500 Endrin U 0.00167 0.00500 Heptachlor U 0.00167 0.00500 Heptachlor epoxide U 0.00167 0.00500 Lindane U 0.00167 0.00500 Methoxychlor U 0.00167 0.00500 Toxaphene U 0.00333 0.0100 (S) Decochlorobiphenyl 74.6 10.0-128 (S) Tetrochloro-m-xylene 99.3 10.0-127 Laboratory Control Sample (LCS) (LCS) R3932203-5 10/05/23 0107 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I Endrin 0.0100 0.00978 97.8 57.0-134 Heptachlor 0.0100 0.00913 91.3 27.0-132 Heptachlor epoxide 0.0100 0.00972 97.2 57.0-130 Lindane 0.0100 0.00969 96.9 55.0-129 Methoxychlor 0.0100 0.00906 90.6 54.0-155 (S) Decochlorobiphenyl 64.8 10.0-128 (S) Tetrochloro-m-xylene 92.4 10.0-127 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 17 of 22 WG2144463 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1660181-01 Method Blank (MB) (MB) R3932963-2 10/05/231319 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I 1,4-Dichlorobenzene U 0.0333 0.100 2,4-Dinitrotoluene U 0.0333 0.100 Hexachlorobenzene U 0.0333 0.100 Hexachloro-1,3-butadiene U 0.0333 0.100 Hexachloroethane U 0.0333 0.100 Nitrobenzene U 0.0333 0.100 Pyridine U 0.0333 0.100 3&4-Methyl Phenol U 0.0333 0.100 2-Methylphenol U 0.0333 0.100 Pentachlorophenol U 0.0333 0.100 2,4,5-Trichlorophenol U 0.0333 0.100 2,4,6-Trichlorophenol U 0.0333 0.100 (S) 2-Fluorophenol 30.6 10.0-120 (S) Phenol-d5 19.4 10.0-120 (S) Nitrobenzene-d5 91.6 10.0-127 (S) 2-Fluorobiphenyl 64.4 10.0-130 (S) 2,4,6-Tribromophenol 78.5 10.0-155 (S) p-Terphenyl-d14 77.3 10.0-128 Laboratory Control Sample (LCS) (LCS) R3982968-1 10/05/2317:58 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I 1,4-Dichlorobenzene 0.500 0.260 52.0 18.0-120 2,4-Dinitrotoluene 0.500 0.419 83.8 49.0-124 Hexachlorobenzene 0.500 0.380 76.0 44.0-120 Hexachloro-1,3-butadiene 0.500 0.335 67.0 19.0-120 Hexachloroethane 0.500 0.293 58.6 15.0-120 Nitrobenzene 0.500 0.372 74.4 27.0-120 Pyridine 0.500 0.0866 17.3 10.0-120 3&4-Methyl Phenol 0.500 0.196 39.2 31.0-120 2-Methylphenol 0.500 0.176 35.2 28.0-120 Pentachlorophenol 0.500 0.382 76.4 23.0-120 2,4,5-Trichlorophenol 0.500 0.376 75.2 44.0-120 2,4,6-Trichlorophenol 0.500 0.392 78.4 42.0-120 (S) 2-Fluorophenol 27.1 10.0-120 (S) Phenol-d5 18.4 10.0-120 (S) Nitrobenzene-d5 69.7 10.0-127 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660181 10/09/23 11:09 18 of 22 WG2144463 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1660181-01 Laboratory Control Sample (LCS) (LCS) R3982968-1 10/05/2317:58 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I (S) 2-Fluorobiphenyl 65.3 10.0-130 (S) 2,4,6-Tribromophenol 75.0 10.0-155 (S) p-Terphenyl-d14 69.7 10.0-128 L1660047-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1660047-01 10/05/2313:41 • (MS) R3982968-3 10/05/2319:02 • (MSD) R3982968-4 10/05/2319:24 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits Analyte mg/I mg/I mg/I mg/I 1,4-Dichlorobenzene 0.500 ND 0.275 0.269 55.0 53.8 1 17.0-120 2,4-Dinitrotoluene 0.500 ND 0.447 0.444 89.4 88.8 1 39.0-125 Hexachlorobenzene 0.500 ND 0.413 0.411 82.6 82.2 1 35.0-122 HexachIaro-1,3-butadiene 0.500 ND 0.372 0.389 74.4 77.8 1 12.0-120 Hexachloroethane 0.500 ND 0.291 0.309 58.2 61.8 1 10.0-120 Nitrobenzene 0.500 ND 0.443 0.468 88.6 93.6 1 12.0-120 Pyridine 0.500 ND 0.123 ND 24.6 17.5 1 10.0-120 3&4-Methyl Phenol 0.500 ND 0.186 0.238 37.2 47.6 1 10.0-120 2-Methylphenol 0.500 ND 0.174 0.221 34.8 44.2 1 10.0-120 Pentachlorophenol 0.500 ND 0.474 0.493 94.8 98.6 1 10.0-128 2,4,5-Trichlorophenol 0.500 ND 0.371 0.429 74.2 85.8 1 33.0-120 2,4,6-Trichlorophenol 0.500 ND 0.365 0.426 73.0 85.2 1 26.0-120 (S) 2-Fluorophenol 23.3 30.6 10.0-120 (S) Phenol-d5 20.1 20.3 10.0-120 (S) Nitrobenzene-d5 81.4 89.9 10.0-127 (S) 2-Fluorobiphenyl 75.2 77.4 10.0-130 (S) 2,4,6-Tribromophenol 76.5 92.5 10.0-155 (S) p-Terphenyl-d14 76.4 75.0 10.0-128 MS Qualifier MSD Qualifier RPD RPD Limits 2.21 40 0.673 25 0.485 24 4.47 34 6.00 40 5.49 30 34.0 37 24.5 36 23.8 30 3.93 37 14.5 31 15.4 31 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 19 of 22 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions u Fc Fss] MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). Fn RDL Reported Detection Limit. Rec. Recovery. Fr RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and F (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the F Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Rc These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe samples from the time of collection until delivery to the laboratory for analysis. This section ofyour report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description E The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial calibration (ICAL). J1 Surrogate recovery limits have been exceeded, values are outside upper control limits. J3 The associated batch QC was outside the established quality control range for precision. J5 The sample matrix interfered with the ability to make any accurate determination, spike value is high. P1 RPD value not applicable for sample concentrations less than 5 times the reporting limit. T8 Sample(s) received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1660131 10/09/23 11:09 20 of 22 ACCREDITATIONS & LOCATIONS Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska N E-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 California 2932 New Mexico TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 _ Georgia NELAP North Carolina 3 41 Georgia' 923 North Dakota R-140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky' 6 KY90010 South Carolina 84004002 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee'" 2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas5 LABO152 Maryland 324 Utah TN000032021-11 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2 LA A2LA— ISO17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2 LA — ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. Rc ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1660131 10/09/23 11:09 PAGE: 21 of 22 Company Name/Address: Billing Information: _T Ana y�ik Container Pr =tjj--- i- ervat v Chain of Custody Page _ of_ EMA Resources Mr. Brent Collins LPChk755 Yadkinville Road aceAnalytical 755 Yadkinville Road Mocksville, NC 27028 Mocksville, NC 27028 I 12065 Lebanon Rd Mount Juliet. TN 37122 Report to: Email To: Mr. Brent Collins brent.collins emaresourcesinc.com;ro .whitak @ submitting a sample yra this chain of custody constitutes acknoydedgment and acceptance of the t ^_ - �' Pace Terms and Conditions found at: https:H�nfo.pacelabs.com/hubfs/pas-standard- Project Description: City/State q�tyV7TTt Please Circle: Sludge Collected: PT MT CT terms.pdr ISDG # Client Project # Lab Project # Phone: 336-751-1441 Jo69 — Collected by (print): Site/Facility ID # P.O. #06 %� o Acctnum: EMARES p" Template:T11413 Collected b (signature): ? Quote # Rush. (Lab MUST Be Notified) Day Five Day Z U J Prelogin: P895391 _Same _ _ Next Day _ 5 Day (Rad Only) Date Results Needed 2= PM: 607 immediately - / —Two Day _ 10 Day (Rad Only) No. JJ.stIn �.rr PB , Packed on Ice N_ Y `� _Three Day of 4-- Shipped V#ia: Fed)EX Ground Sample ID Comp/Grab Matrix • Depth Date Time ntrs - 1 cc U Remarks Sample # (lab only) C Ss 39 10;o0 z x x Yanc v v; e— i I I I I 1 1 I 1 I t 1 1 I l ' Matrix: Remarks: Sample R ntacth S-Soil AIR -Air F-Filter I pH _ Temp COC Seal Present/i: P Y N COC Signed/Accurate: �rf�N GW- Groundwater B- Bioassay Flow Other Bottles arrive intact: � N III W - Waste Water Correct bottles used: ,X N DW- DrinkingW ter Sufficient volume sent: Samples returned via: OT - Other 5 �Jt _UPS FedEx Courier Tracking # 3-€_BPe]a.,;-a_§J1 VOA Zero Headspace: Y N Relin uis d b (Signature) Date: Time: Received b (Signature) TripBlank Received: Yes Preservation Correct/Checked: Y ^N Q y' ( g ) Y- ( g ) PAD Screen <0.5 Whr: �_N C) �� ?� HCL/MeoH 7 �•J I �) TB R Relinquished by: (Signature) Date: Time: Received by: (Signature) Temp: °C Bottles R ceived: If preservation required by Login: Date/Time S,y 5, Relinquished by: (Signature) Date: Time: Received for I Signature Da Time: Hold: Conditi o NCFj /� /�d '7 PG/!/ State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ❑ Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ❑ Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ❑ For each source facility, attach the following: ❑ Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ❑ Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ❑ Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ❑ For each source facility, attach the following: ❑ Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ❑ Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 RESIDUALS SOURCE FACILITY SUMMARY Applicant's name: Town of Yanceyville Status Code a Facility Permit Holder Facility Name County Permit Number Maximum Dry Tons Per Year Current n Proposed R Town of Yanceyville Yanceyville WWTP Caswell NCO040011 244 244 R Town of Yanceyville Yanceyville WTP Caswell 02-17-010 75 75 a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) ♦ M (Modified) ♦ D (Deleted) 'The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility). SUMMARY FOR FORM: RSC 06-16 Page 1 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: Yanceyville WTP 2. Facility permit holder is: ❑ Federal, I❑ State, E Local Government, or ❑ Private. Facility permit issued by: ® Div. of Water Resources, rl Div. of Environmental Health, or ❑ Other (explain: ). 3. Facility contact person and title: Complete mailing address: = City: State: AM Zip: - Telephone number: (_) _ E-mail address: 4. Facility physical address: 1316 Badgett Sisters Parkway City: Yanceyville State: NC Zip: 27379- Coordinates: Latitude: 36' 23' 27" Longitude: 79. 20' 52" Datum: NAD83 Level of accuracy: nearest second Method of measurement: GPS 5. Purpose of the facility: ❑ treatment of municipal wastewater, p treatment of 100% domestic wastewater, ® treatment of potable water, p treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and -M % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: Yes No 7. Facility permitted/design flow: JI& MGD and facility average daily flow: F� MGD 8. Average amount of residuals being generated at this facility 0 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: —0 Type and volume of residuals storage (i.e., outside of residuals treatment units): IL RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: 11 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ❑ Biological ® Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): 3- b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Pace Analytical and Date of analysis: 07/25/2022 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 <pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >170 OF (> 140°F) Passed reactivity test: J' yes r]no. HCN: <.25 mg/kg (<250) & H2S: 75 mg/kg (<500) TCLP Parameter Limit (mg//) Result (mgfi) TCLP Parameter Limit (mgfi) Result (mgfi) Arsenic 5.0 ND Hexachlorobenzene 0.13 ND Barium 100.0 ND Hexachloro-1,3-Butadiene 0.5 ND Benzene 0.5 ND Hexachloroethane 3.0 ND Cadmium 1.0 ND Lead 5.0 ND Carbon Tetrachloride 0.5 ND Lindane 0.4 ND Chlordane 0.03 ND Mercury 0.2 ND Chlorobenzene 100.0 ND Methoxychlor 10.0 ND Chloroform 6.0 ND Methyl Ethyl Ketone 200.0 ND Chromium 5.0 ND Nitrobenzene 2.0 ND m-Cresol 200.0 ND Pentachlorophenol 100.0 ND o-Cresol 200.0 ND Pyridine 5.0 ND p-Cresol 200.0 ND Selenium 1.0 ND Cresol 200.0 ND Silver 5.0 ND 2,4-D 10.0 ND Tetrachloroethylene 0.7 ND 1,4-Dichlorobenzene 7.5 ND Toxaphene 0.5 ND 1,2-Dichloroethane 0.5 ND Trichloroethylene 0.5 ND 1,1-Dichloroethylene 0.7 ND 214,5-Trichlorophenol 400.0 ND 2,4-Dinitrotoluene 0.13 ND 214,6-Trichlorophenol 2.0 ND Endrin 0.02 ND 2,4,5-TP (Silvex) 1.0 ND Heptachlor and its Hydroxide 0.008 ND Vinyl Chloride 0.2 ND FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distribution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: 07/25/2022 Parameter Ceiling Concentration Limits (ClassA & ClassB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 26.9 Cadmium 85 39 <1 Copper 4,300 1,500 48.1 Lead 840 300 11.4 Mercury 57 17 <0.342 Molybdenum 75 n/a <6.75 Nickel 420 420 17.2 Selenium 100 100 <16 Zinc 7,500 2,800 62 b. For Surface Disposal Unit (landfill): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/kg) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 2 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: WMpoint Analytical and Date of analysis: 07/25/2022 Parameter Result (mglkg) Aluminum 188,000 Ammonia -Nitrogen 5,000 Calcium <1940 Magnesium 1,340 Nitrate -Nitrite Nitrogen <250 pH (Standard Unit) 6.3 Phosphorus 2,190 Potassium 865 Sodium <650 Total Kjeldahl Nitrogen 24,700 c. Using the results listed in Item IL 5b. above, calculate the sodium adsorption ration (SAR): 0.39 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 40 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (1s) Year PAN Five -Year Maximum Adjusted PAN (mglkg) (mg/kg) Surface 10,630 13,130 Injection/Incorporation 15,355 17,855 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 4 of 7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B. ® Alternative 1 [15A NCAC 02T.I 106(c)(1)] - Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T. 1106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, V air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T. 1107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T. 1107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T. 1107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 5 of r9 r 2 • In section 1- raw water is treated using Alum and Polymer to form floc. • In Section 2- treated source water is settling the Alum floc in this chamber. • In section 3- treated source water is filtered. Residual turbidity is filtered here. • From section 2 Alum residual sludge is forced to section 4. When basins are cleaned. • From section 3 turbidity is washed out of the filters every 96 hours. To section 4. • Section 4 collects the majority of the sludge and water goes to section 5 were the rest of the slur 5 water is decanted to a reservoir. • In section 3- 25 %caustic soda is added to the water along with chlorine. • In section 5- the decanted water is treated with a dechloring agent. Waypointo ANALYTICAL 8/3/2022 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 22-207-0025 Client Project Description: Yanceyville 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 7/26/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00001/22-207-0025 Page 2 of 8 Waypoint ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Sample Summary Table Report Number: 22-207-0025 Client Project Description: Yanceyville Lab No Client Sample ID Matrix Date Collected Date Received 91150 Yanceyville V TP Solids 07/25/2022 09:20 07/26/2022 Page 3 of 8 Waypointo ANALYTICAL 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Project Yanceyville Information : 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Report Date : 08/03/2022 nReceived : 07/26/2022 C-�*�-� = Connie Cook Report Number : 22-207-0025 REPORT OFANALYSIS Project Manager Lab No : 91150 Matrix: Solids Sample ID : Yanceyville WTP Sampled: 7/25/2022 9:20 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 98.0 % 1 07/29/22 15:56 FMM SW-DRYWT Ammonia Nitrogen 5000 mg/Kg - dry 800 5000 1 08/02/22 14:30 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <250 mg/Kg - dry 250 250 1 08/01/22 13:53 ZBD 4500NO3F-2016 Organic N 19650 mg/Kg - dry 800.0 5000 1 08/02/22 10:30 DH CALCULATION pH 6.3 S.U. 1 08/01/2216:03 DRS 9045D Total Solids 2.00 % 0.010 0.010 1 07/29/22 15:56 FMM 2540G-2011 Total Volatile Solids 32.7 % 0.010 0.010 1 07/29/22 15:56 FMM 2540G-2011 Total Kjeldahl Nitrogen 24700 mg/Kg - dry 500 12500 1 08/02/22 10:30 JPJ ;M-4500-NH3C-TKI` Phosphorus 2190 mg/Kg - dry 138 250 1 07/27/22 21:46 EAL 6010D Aluminum 188000 mg/Kg - dry 231 250 1 07/27/22 21:46 EAL 6010D Arsenic 26.9 mg/Kg - dry 12.0 25.0 1 07/27/22 21:46 EAL 6010D Cadmium <1.00 mg/Kg - dry 1.00 5.00 1 07/27/22 21:46 EAL 6010D Calcium <1940 mg/Kg - dry 1940 2500 1 07/27/22 21:46 EAL 6010D Chromium 32.3 mg/Kg - dry 11.8 12.5 1 07/27/22 21:46 EAL 6010D Copper 48.1 mg/Kg - dry 15.5 25.0 1 07/27/22 21:46 EAL 6010D Iron 30900 mg/Kg - dry 426 500 1 07/27/22 21:46 EAL 6010D Lead 11.43 mg/Kg - dry 9.00 15.0 1 07/27/22 21:46 EAL 6010D Magnesium 1340 mg/Kg - dry 129 250 1 07/27/22 21:46 EAL 6010D Manganese 925 mg/Kg - dry 16.3 25.0 1 07/27/22 21:46 EAL 6010D Mercury <0.342 mg/Kg - dry 0.342 7.85 1 07/27/22 12:31 TJS 7471A Molybdenum <6.75 mg/Kg - dry 6.75 12.5 1 07/27/22 21:46 EAL 6010D Nickel 17.2 mg/Kg - dry 6.00 12.5 1 07/27/22 21:46 EAL 6010D Potassium 865 mg/Kg - dry 309 500 1 07/27/22 21:46 EAL 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Page 4 of 8 • Waypoint 27090 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalyiical.com 46245 EMA Resources Inc Project Yanceyville Mr. Brent Collins Report Date : 08/03/2022 755 Yadkinville Rd Information : Received : 07/26/2022 Mocksville , NC 27028 Connie Cook Report Number : 22-207-0025 REPORT OFANALYSIS Project Manager Lab No : 91150 Matrix: Solids Sample ID : Yanceyville WTP Sampled: 7/25/2022 9:20 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium <16.0 mg/Kg - dry 16.0 25.0 1 07/27/22 21:46 EAL 6010D Sodium <650 mg/Kg - dry 650 1250 1 07/27/22 21:46 EAL 6010D Zinc 62.03 mg/Kg - dry 40.5 62.5 1 07/27/22 21:46 EAL 6010D Sulfur 5050 mg/Kg - dry 259 500 1 07/27/22 21:46 EAL 6010D Sodium Absorption Ratio <0.01 Ratio 0.01 0.01 1 07/27/22 21:46 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 5 of 8 s WayPAoi nt ..(2) �79p Whitten Road,3.240 Memphis, TN 38133 21.2440 Main 901.213.240fl °Fax 901.213.2440 N A LYT I C A L www.waypointanalytical.com Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 22-207-0025 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IT135 Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: lEmily M. Peterson Date & Time: 07/26/2022 09:25:34 Page 6 of 8 � c d N p LL Y m a N r 3 q T � p = H w . o ac+ e n r` o M z 9 N LIr n � L 7-m w E p C'7J ❑ 0 A Vi Y V O= M a❑ V Ln y d C p o ry o m i u mm U�zzzxxxg r Q ❑ i Y 3 •� V7 �•1 MM LL — v ` 0 o0. V1 Q m U O w y. m W W W D .� > a Z a z J N LL (D N v El" /�{/ m v /�� E `1.i GY N y 0] C? �; t/ / 1'� fi E n ® J snl� - N GENE E °au Q c v d sp!!Os Ielol a , 1 a N Diue6apl01eAIN �V o E u o ° z W efuowwylNNl v_ i+ G E G! Q❑ w V) R G ^ D R' D C 7 v C m r=o a r 00 Los) sle C ~ ❑ 7 a m Cs l a` U 2 C7 2 C7 c L] s n d y C a '^ v v m Q a ai!sodwa(�j �o ge�(gj L� z m M w .a a v (RaH Dina;aaj x!�ieyi a C a } a 7 w 3 rn 7 E c c c saau!eiuo:);o iagwnm Qj a QZt U 4d = a C y fa II] mA O L a `-' ' G LL q C] 6 c ~ C y m y ° °'D C E G u h o a r V m a a CO ❑ a E , a z _a y o .s co � r� ¢ ■.�. 7-- o ° i } =DOlza 4�aj kEEN1U R N61 ❑ 2 N LO d v v m 4) �LO o a d o ❑ V LLI 1- d 1 Page 7 of 8 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Page 1 Report Date: 8/3/2022 Date Sample Rcvd: 7/25/2022 Meritech Work Order # 07252204 Sample: Yanceyville WTP 1 Grab 7/25/22 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.92 % 7/27/22 0-100 % SM 2540B Fecal Coliform (Sludge) <473 CFU/g dry wt 7/25/22 473 CFU/g dry wt SM 9222D Meritech Work Order # 07252205 Sample: Yanceyville WTP 2 Grab 7/25/22 Parameters Result Analysis Date Reporting Limit Method %Total Solids 1.83 % 7/27/22 0-100 % SM 2540B Fecal Coliform (Sludge) <497 CFU/g dry wt 7/25/22 497 CFU/g dry wt SM 9222D Meritech Work Order # 07252206 Sample: Yanceyville WTP 3 Grab 7/25/22 Parameters Result Analysis Date Reporting Limit Method %Total Solids 2.05 % 7/27/22 0-100 % SM 2540B Fecal Coliform (Sludge) <443 CFU/g dry wt 7/25/22 443 CFU/g dry wt SM 9222D Meritech Work Order # 07252207 Sample: Yanceyville WTP 4 Grab 7/25/22 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.89 % 7/27/22 0-100 % SM 2540B Fecal Coliform (Sludge) <481 CFU/g dry wt 7/25/22 481 CFU/g dry wt SM 9222D 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 Meritech, Inc. Environmental Laboratory Laboratory Certification No.165 R Contact: Brent Collins Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Page 2 Report Date: 8/3/2022 Date Sample Rcvd: 7/25/2022 Meritech Work Order # Parameters % Total Solids Fecal Coliform (Sludge) 07252208 Sample: Yanceyville WTP 5 Grab Result Analysis Date Reporting Limit 1.91 % 7/27/22 0-100 % <476 CFU/g dry wt 7/25/22 476 CFU/g dry wt 7/25/22 Method SM 2540B SM 9222D Meritech Work Order # 07252209 Sample: Yanceyville WTP 6 Grab 7/25/22 Parameters Result Analysis Date Reporting Limit Method % Total Solids 1.86 % 7/27/22 0-100 % SM 2540B Fecal Coliform (Sludge) <489 CFU/g dry wt 7/25/22 489 CFU/g dry wt SM 9222D Meritech Work Order # 07252210 Sample: Yanceyville WTP 7 Grab 7/25/22 Parameters Result Analysis Date. Reporting Limit Method % Total Solids 1.94 % 7/27/22 0-100 % SM 2540B Fecal Coliform (Sludge) <469 CFU/g dry wt 7/25/22 469 CFU/g dry wt SM 9222D I hereby certify that have reviewed and approve these data, Laboratory Representative 642 Tamco Road, Reidsville, North Carolina 27320 tel.(336)342-4748 fax.(336)342-1522 5-9-2016 Chain of Custody Record (COC) NPDES#: Client: EMA Resources Inc. Phone:_ Address: 755 Yadkinville Rd Fax: Mocksville NC 27028 Email: Project: P.O.#: Attention: Brent Collins How would you like your report sent? Circle all that apply: l preferred) , Fax, Mail 336-751-1441 336-751-1442 brent.collins@emaresourcesinc.com Turn Around Time* *RUSH work needs prior approval. Std(1Dda S) 3-5 Da s 24-49Hrs I— ME R ITE CH INC. ENVIRONMENTAL LABORATORIES r 642 Tamco Rd. Phone: 336-342-4748 Reidsville NC 27320 Fax: 336-342-1522 Email: info@meritechlabs.com www.meritechlabs.com Sample Location and/or ID # Sampling Dates &Times Person Taking Sample (Sign/Print): Lab Use Only v - Start End Comp? Grab? #of Cont. Test(s) Required On Ice? Yes / No pH OK? Cl OK? Date Time Date Time yQAre�%rj li1. HfTP I 7/,2-S 9: 2W Feca l Cot, -&-,vi t� Z 0S, 3 �(, y W % ` v v Temperature Upon Receipt:. L� 1 `Method of Shipment: *** Dechlorination (<0.5 ppm) of Ammonia, Cyanide, Phenol and TKN samples must be done in the field prior to preservation. *** Comments: Compositor # ❑ UPS Fug # ❑ Fed Ex Are these results for regulatory purposes? Yes �� No ❑ Report results in: mg/L El-, mg/kg Pug/L ❑ Hand Delivery _ _ Relinquished by: Date: 7�35 i� Time: 10 �24 Received by: Date: Time: ❑ Other Relinquished by: Date: Time: Received by: Date: Time: Relinquished by: Date: Time: Rec (J t i� (� ace Analytical ANALYTICAL REPORT August 05, 2022 EMA Resources Sample Delivery Group Samples Received: Project Number: Description: Report To: L1518453 07/26/2022 Sludge Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By zw ��w -a T. Alan Harvill Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided, and as the samples are received. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 1 of 22 TABLE OF CONTENTS Cp: Cover Page Tc: Table of Contents Ss: Sample Summary Cn: Case Narrative Sr: Sample Results YANCEYVILLE L1518453-01 Qc: Quality Control Summary Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260D Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270E GI: Glossary of Terms al: Accreditations & Locations Sc: Sample Chain of Custody 2 3 4 5 5 7 7 9 10 11 12 13 14 16 17 18 20 21 22 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 2 of 22 YANCEYVILLE L1518453-01 Waste Method Preparation by Method 1311 Preparation by Method 1311 Wet Chemistry by Method 9012 B Wet Chemistry by Method 9034-9030B Wet Chemistry by Method 9045D Wet Chemistry by Method D93/1010A Mercury by Method 7470A Metals (ICP) by Method 6010D Volatile Organic Compounds (GC/MS) by Method 8260D Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 Pesticides (GC) by Method 8081B Semi Volatile Organic Compounds (GC/MS) by Method 8270E SAMPLE SUMMARY Collected by Brent Collins Batch WG1901366 WG1901367 WG1899053 WG1903690 WG1901497 WG1901992 WG1902177 WG1902441 WG1902474 WG1903776 WG1902977 WG1902662 Dilution Preparation date/time 1 07/27/22 1321 1 07/27/22 10:30 1 07/28/22 0357 1 08/02/2212:00 1 07/27/22 09:43 1 07/28/22 0110 1 07/28/2210:00 1 07/28/2216:34 1 07/29/22 0131 1 08/01/221136 1 07/30/2210:17 1 07/29/22 08:42 Collected date/time Received date/time 07/25/22 09:20 07/26/22 09:15 C P Analysis date/time 07/27/2213:21 07/27/2210:30 07/29/22 1130 08/02/22 15:00 07/27/2214:00 07/28/22 0110 07/30/22 0832 07/28/22 22:44 07/29/22 0131 08/02/22 12:46 07/30/22 2101 07/29/22 16:26 Analyst JWS BTP LDT RMR SIDE WOS SRT CCE ADM GKM JMB JNJ Location FC Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fn Mt. Juliet, TN Mt. Juliet, TN Mt. Juliet, TN Fr Mt. Juliet, TN Mt. Juliet, TN Rc Mt. Juliet, TN Mt. Juliet, TN GI F RC ACCOUNT: PROJECT: SDG: EMA Resources L1513453 DATE/TIME: PAGE: 03/05/22 13:26 3 of 22 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the FP appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FC have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, a non-conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FS knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. 0 Fr Rc aV3� /,07 Wa GI T. Alan Harvill [Al Project Manager RC Project Narrative All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 4 of 22 SAMPLE RESULTS - 01 L1518453 YANCEYVILLE Collected date/time: 07/25/22 09:20 Preparation by Method 1311 Result Qualifier Prep Batch Analyte date / time TCLP Extraction 7/27/202210:30:10 AM WG1901367 TCLP ZHE Extraction - 7/27/202212149 PM WG1901366 Fluid 1 7/27/202210:30:10 AM WG1901367 Initial pH 5.73 7/27/202210:30:10 AM WG1901367 Final pH 4.95 7/27/202210:30:10 AM WG1901367 Wet Chemistry by Method 9012 B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Cyanide ND 0.250 Wet Chemistry by Method 9034-9030B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Sulfide ND 75.0 Wet Chemistry by Method 9045D Dilution Analysis Batch date / time 1 07/29/20221130 WG1899053 Dilution Analysis Batch date / time 1 08/02/202215:00 WG1903690 Result Qualifier Dilution Analysis Batch Analyte su date / time Corrosivity by pH 6.66 T8 1 07/27/202214:00 WG1901497 Sample Narrative: L1518453-01 WG1901497: 6.66 at24.3C Wet Chemistry by Method D93/1010A Result Analyte Deg. F Ignitability DNI at170 Mercury by Method 7470A Qualifier Dilution Analysis Batch date / time 1 07/28/2022 0110 WG1901992 Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Mercury ND 0.0100 0.20 Metals (ICP) by Method 6010D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Arsenic ND 0.100 5 Barium ND 0.100 100 Cadmium ND 0.100 1 Chromium ND 0.100 5 Lead ND 0.100 5 Selenium ND 0.100 1 Silver ND 0.100 5 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Analyte mg/I mg/I mg/I Benzene ND 0.0500 0.50 Carbon tetrachloride ND 0.0500 0.50 Chlorobenzene ND 0.0500 100 Chloroform ND 0.250 6 ACCOUNT: PROJECT: EMA Resources Dilution Analysis Batch date / time 1 07/30/2022 08:32 WG1902177 Dilution Analysis Batch date / time 1 07/28/2022 22:44 WG1902441 1 07/28/2022 22:44 WG1902441 1 07/28/2022 22:44 WG1902441 1 07/28/2022 22:44 WG1902441 1 07/28/2022 22:44 WG1902441 1 07/28/2022 22:44 WG1902441 1 07/28/2022 22:44 WG1902441 Dilution Analysis Batch date / time 1 07/29/2022 0131 WG1902474 1 07/29/2022 0131 WG1902474 1 07/29/2022 0131 WG1902474 1 07/29/2022 0131 WG1902474 SDG: DATE/TIME: PAGE: L1513453 03/05/22 13:26 5 of 22 YANCEYVILLE SAMPLE RESULTS Collected date/time: 07/25/22 09:20 L1518453 Volatile Organic Compounds (GC/MS) by Method 8260D - 01 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,2-Dichloroethane ND 0.0500 0.50 1 07/29/2022 0131 WG1902474 1,1-Dichloroethene ND 0.0500 0.70 1 07/29/2022 0131 WG1902474 2-Butanone (MEK) ND 0.500 200 1 07/29/2022 0131 WG1902474 Tetrachloroethene ND 0.0500 0.70 1 07/29/2022 0131 WG1902474 Trichloroethene ND 0.0500 0.50 1 07/29/2022 0131 WG1902474 Vinyl chloride ND 0.0500 0.20 1 07/29/2022 0131 WG1902474 (S) Toluene-dH 102 80.0-120 0712912022 01.31 WG1902474 (S) 4-Bromofluorobenzene 98.3 77.0-126 0712912022 01.31 WG1902474 (S) 1,2-Dichloroethane-d4 107 70.0-130 071291202201.31 WG1902474 Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 Result Qualifier RDL Analyte mg/I mg/I 2,4-D ND 0.0200 2,4,5-TP (Silvex) ND 0.0200 (S) Z4-DB-D3 119 70.0-130 Pesticides (GC) by Method 8081B Limit Dilution Analysis Batch mg/I date / time 10 1 08/02/202212:46 WG1903776 1 1 08/02/202212:46 WG1903776 0810212022 12.46 WG1903776 Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Chlordane ND 0.00500 0.03 1 07/30/2022 21:01 WG1902977 Endrin ND 0.00500 0.02 1 07/30/2022 21:01 WG1902977 Heptachlor ND 0.00500 0.0080 1 07/30/2022 21:01 WG1902977 Heptachlor epoxide ND 0.00500 0.0080 1 07/30/2022 21:01 WG1902977 Lindane ND 0.00500 0.40 1 07/30/2022 21:01 WG1902977 Methoxychlor ND 0.00500 10 1 07/30/2022 21:01 WG1902977 Toxaphene ND 0.0100 0.50 1 07/30/2022 21:01 WG1902977 (S)Decochlorobiphenyl 70.3 10.0-128 071301202221.01 WG1902977 (S) Tetrochloro-m-xylene 64.6 10.0-127 071301202221.01 WG1902977 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Analyte mg/I 1,4-Dichlorobenzene ND 2,4-Dinitrotoluene ND Hexachlorobenzene ND HexachIoro-1,3-butadiene ND Hexachloroethane ND Nitrobenzene ND Pyridine ND 3&4-Methyl Phenol ND 2-Methylphenol ND Pentachlorophenol ND 2,4,5-Trichlorophenol ND 2,4,6-Trichlorophenol ND (S) 2-Fluorophenol 19.4 (S) Phenol-d5 11.0 (S) Nitrobenzene-d5 56.3 (S) 2-Fluorobiphenyl 59.6 (S) Z4,6-Tribromophenol 73.0 (S) p-Terphenyl-d14 65.7 Qualifier RDL mg/I 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 0.100 10.0-120 10.0-120 10.0-127 10.0-130 10.0-155 10.0-128 Limit mg/I 7.50 0.13 0.13 0.50 3 2 5 400 200 100 400 2 Dilution Analysis Batch date / time 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 07/29/2022 16:26 0712912022 16.26 0712912022 16.26 0712912022 16.26 0712912022 16.26 0712912022 16.26 0712912022 16.26 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 WG1902662 ACCOUNT: PROJECT: SDG: EMA Resources L1513453 DATE/TIME: PAGE: 03/05/22 13:26 6 of 22 WG1899053 Wet Chemistry by Method 9012 B Method Blank (MB) (MB) R3320615-1 07/29/22 1104 MB Result Analyte mg/kg Reactive Cyanide U MB Qualifier MB MDL MB RDL mg/kg mg/kg 0.0390 0.250 L1517670-01 Original Sample (OS) • Duplicate (DUP) QUALITY CONTROL SUMMARY L1518453-01 (OS) L1517670-01 07/29/22 11:13 • (DUP) R3320615-3 07/29/22 1114 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg Reactive Cyanide 1.13 1.12 1 0.808 20 L1517919-01 Original Sample (OS) • Duplicate (DUP) (OS) L1517919-01 07/29/22 1119 • (DUP) R3320615-6 07/29/22 1120 Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD Limits Analyte mg/kg mg/kg Reactive Cyanide ND ND 1 1.32 20 Laboratory Control Sample (LCS) (LCS) R3820615-2 07/29/22 1105 Spike Amount LCS Result LCS Rec. Analyte mg/kg mg/kg Reactive Cyanide 2.50 2.46 98.3 Rec. Limits LCS Qualifier 85.0-115 L1517670-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1517670-01 07/29/22 11:13 • (MS) R3320615-4 07/29/22 1117 • (MSD) R3320615-5 07/29/22 1118 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg Reactive Cyanide 1.67 1.13 2.63 2.70 90.0 94.1 1 75.0-125 2.53 20 L1517919-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1517919-01 07/29/22 1119 • (MS) R3320615-7 07/29/22 1121 • (MSD) R3320615-8 07/29/22 1122 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg mg/kg mg/kg mg/kg Reactive Cyanide 1.67 ND 0.788 0.602 40.2 29.1 1 75.0-125 J6 J3 J6 26.8 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 7 of 22 WG1899053 Wet Chemistry by Method 9012 B QUALITY CONTROL SUMMARY L1518453-01 L1517919-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1517919-01 07/29/22 1119 • (MS) R3320615-7 07/29/22 1121 • (MSD) R3320615-8 07/29/22 1122 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/kg _ mg/kg mg/kg mg/kg Sample Narrative: MS: Matrix spike failure due to matrix interference. MSD: Matrix spike failure due to matrix interference. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 3 of 22 -------------- WG1903690 Wet Chemistry by Method 9034-9030B Method Blank (MB) (MB) R3321777-1 03/02/22 15:00 MB Result MB Qualifier MB MDL MB RDL Analyte mg/kg mg/kg mg/kg Reactive Sulfide U 30.0 75.0 QUALITY CONTROL SUMMARY L1518453-01 Laboratory Control Sample (LCS) (LCS) R3321777-2 03/02/22 15:00 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/kg mg/kg Reactive Sulfide 100 73.8 73.8 53.8-124 L1519458-20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1519453-20 03/02/22 15:00 • (MS) R3321777-3 03/02/22 15:00 • (MSD) R3321777-4 03/02/22 15:00 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD Analyte mg/kg mg/kg mg/kg mg/kg Reactive Sulfide 100 ND ND ND 0.000 0.000 1 10.0-136 J6 J6 0.000 RPD Limits 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 9 of 22 WG1901497 QUALITY CONTROL SUMMARY Wet Chemistry by Method 9045D L1518453-01 Laboratory Control Sample (LCS) C (LCS) R3819745-1 07/27/22 1400 p Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier ITC] Analyte su su % % Corrosivity by pH 10.0 10.0 100 99.0-101 F Sample Narrative: SS LCS:10 at 23.5C [Cn] 5 Sr �GI FAI FSC1 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 10 of 22 WG1901992 QUALITY CONTROL SUMMARY Wet Chemistry by Method D93/1010A L1518453-01 L1517289-01 Original Sample (OS) • Duplicate (DUP) (OS) L1517239-01 07/23/22 01:10 • (DUP) R3319942-3 07/23/22 0110 Original Result DUP Result Dilution DUP RPD Analyte Deg. F Deg. F Ignitability DNI at170 DNI at170 1 0.000 DUP Qualifier DUP RPD Limits i 10 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3819942-1 07/28/22 01:10 • (LCSD) R3819942-2 07/28/22 0110 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits Analyte Deg. F Deg. F Deg. F Ignitability 126 126 130 99.9 103 95.6-104 3.13 10 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 11 of 22 WG1902177 QUALITY CONTROL SUMMARY Mercury by Method 7470A L1518453-01 Method Blank (MB) (MB) R3320337-1 07/30/22 07:55 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Mercury U 0.00330 0.0100 Laboratory Control Sample (LCS) (LCS) R3820887-2 07/30/22 07:57 Spike Amount LCS Result LCS Rec. Analyte mg/I mg/I Mercury 0.0300 0.0309 103 Rec. Limits LCS Qualifier 80.0-120 L1518427-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1513427-01 07/30/22 07:59 • (MS) R3320337-3 07/30/22 08:01 • (MSD) R3320337-4 07/30/22 08:03 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Mercury 0.0300 ND 0.0311 0.0302 104 101 1 75.0-125 2.63 20 L1518596-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1513596-01 07/30/22 08:05 • (MS) R3320337-5 07/30/22 08:07 • (MSD) R3320337-6 07/30/22 08:09 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Mercury 0.0300 ND 0.0320 0.0305 107 102 1 75.0-125 4.84 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 12 of 22 WG1902441 Metals (ICP) by Method 6010D Method Blank (MB) (MB) R3320466-1 07/23/22 2155 MB Result MB Qualifier MB MDL Analyte mg/I mg/I Arsenic U 0.0333 Barium U 0.0333 Cadmium U 0.0333 Chromium U 0.0333 Lead U 0.0333 Selenium 0.0366 J 0.0333 Silver U 0.0333 Laboratory Control Sample (LCS) (LCS) R3820466-2 07/28/22 2157 Spike Amount LCS Result Analyte mg/I mg/I Arsenic 10.0 9.59 Barium 10.0 9.83 Cadmium 10.0 9.71 Chromium 10.0 9.50 Lead 10.0 9.59 Selenium 10.0 10.1 Silver 2.00 1.86 LCS Rec. 95.9 98.3 97.1 95.0 95.9 101 93.1 QUALITY CONTROL SUMMARY L1518453-01 MB RDL mg/I 0.100 0.100 0.100 0.100 0.100 0.100 0.100 Rec. Limits 80.0-120 80.0-120 80.0-120 80.0-120 80.0-120 80.0-120 80.0-120 LCS Qualifier L1518212-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1513212-02 07/23/22 22:00 • (MS) R3320466-4 07/23/22 22:05 • (MSD) R3320466-5 07/23/22 22:08 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Arsenic 10.0 ND 9.70 9.63 97.0 96.3 Barium 10.0 ND 9.83 9.80 98.3 98.0 Cadmium 10.0 ND 9.79 9.74 97.9 97.4 Chromium 10.0 ND 9.33 9.40 93.3 94.0 Lead 10.0 ND 9.50 9.50 95.0 95.0 Selenium 10.0 ND 10.1 9.96 101 99.6 Silver 2.00 ND 1.87 1.87 93.3 93.6 Dilution Rec. Limits 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 1 75.0-125 MS Qualifier MSD Qualifier RPD 0.697 0.306 0.496 0.781 0.00731 0.970 0.238 RPD Limits 20 20 20 20 20 20 20 ACCOUNT: EMA Resources PROJECT: SDG: L1513453 DATE/TIME: 03/05/22 13:26 PAGE: 13 of 22 WG1902474 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260D L1518453-01 Method Blank (MB) (MB) R3323069-3 07/29/22 00:24 MB Result Analyte mg/I Benzene U Carbon tetrachloride U Chlorobenzene U Chloroform U 1,2-Dichloroethane U 1,1-Dichloroethene U 2-Butanone (MEK) U Tetrachloroethene U Trichloroethene U Vinyl chloride U (S) Toluene-dH 104 (S) 4-Bromofluorobenzene 97.7 (S) 1,2-Dichloroethane-d4 105 MB Qualifier MB MDL mg/I MB RDL mg/I 0.0167 0.0500 0.0167 0.0500 0.0167 0.0500 0.0833 0.250 0.0167 0.0500 0.0167 0.0500 0.167 0.500 0.0167 0.0500 0.0167 0.0500 0.0167 0.0500 80.0-120 77.0-126 70.0-130 Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD) (LCS) R3823069-1 07/28/22 22:30 • (LCSD) R3823069-2 07/28/22 22:52 Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits Analyte mg/I mg/I mg/I Benzene 0.250 0.252 0.270 101 108 70.0-123 Carbon tetrachloride 0.250 0.271 0.251 108 100 68.0-126 Chlorobenzene 0.250 0.259 0.267 104 107 80.0-121 Chloroform 0.250 0.253 0.271 101 108 73.0-120 1,2-Dichloroethane 0.250 0.291 0.291 116 116 70.0-128 1,1-Dichloroethene 0.250 0.257 0.229 103 91.6 71.0-124 2-Butanone (MEK) 1.25 1.88 1.85 150 148 44.0-160 Tetrachloroethene 0.250 0.236 0.247 94.4 98.8 72.0-132 Trichloroethene 0.250 0.257 0.276 103 110 78.0-124 Vinyl chloride 0.250 0.260 0.248 104 99.2 67.0-131 (S) Toluene-dH 104 103 80.0-120 (S) 4-Bromofluorobenzene 101 98.6 77.0-126 (S) 1,2-Dichloroethane-d4 104 103 70.0-130 LCS Qualifier LCSD Qualifier RPD 6.90 7.66 3.04 6.87 0.000 11.5 1.61 4.55 7.13 4.72 RPD Limits 20 20 20 20 20 20 20 20 20 20 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 14 of 22 WG1902474 QUALITY CONTROL SUMMARY Volatile Organic Compounds (GC/MS) by Method 8260D L1518453-01 L1518722-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1513722-02 07/29/22 01:53 • (MS) R3323069-4 07/29/22 03:52 • (MSD) R3323069-5 07/29/22 09:14 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I Benzene 0.250 ND 0.170 0.240 68.0 96.0 1 17.0-158 J3 34.1 27 Carbon tetrachloride 0.250 ND 0.156 0.267 62.4 107 1 23.0-159 J3 52.5 28 Chlorobenzene 0.250 ND 0.192 0.241 76.8 96.4 1 33.0-152 22.6 27 Chloroform 0.250 ND ND ND 76.8 98.4 1 29.0-154 24.7 28 1,2-Dichloroethane 0.250 ND 0.261 0.291 104 116 1 29.0-151 10.9 27 1,1-Dichloroethene 0.250 ND 0.135 0.226 54.0 90.4 1 11.0-160 J3 50.4 29 2-Butanone (MEK) 1.25 ND 1.91 1.85 153 148 1 10.0-160 3.19 32 Tetrachloroethene 0.250 ND 0.133 0.215 53.2 86.0 1 10.0-160 J3 47.1 27 Trichloroethene 0.250 ND 0.171 0.243 68.4 97.2 1 10.0-160 J3 34.8 25 Vinyl chloride 0.250 ND 0.130 0.227 52.0 90.8 1 10.0-160 J3 54.3 27 (S) Toluene-dH 104 104 80.0-120 (S) 4-Bromofluorobenzene 96.8 99.7 77.0-126 (S) 1,2-Dichloroethane-d4 104 109 70.0-130 L1518431-04 Original Sample (OS) • Matrix Spike (MS) (OS) L1513431-04 07/29/22 01:09 • (MS) R3323069-6 07/29/22 09:36 Spike Amount Original Result MS Result MS Rec. Dilution Rec. Limits MS Qualifier Analyte mg/I mg/I mg/I Benzene 0.250 ND 0.254 102 1 17.0-158 Carbon tetrachloride 0.250 ND 0.277 ill 1 23.0-159 Chlorobenzene 0.250 ND 0.264 106 1 33.0-152 Chloroform 0.250 ND 0.265 106 1 29.0-154 1,2-Dichloroethane 0.250 ND 0.283 113 1 29.0-151 1,1-Dichloroethene 0.250 ND 0.233 93.2 1 11.0-160 2-Butanone (MEK) 1.25 ND 1.84 147 1 10.0-160 Tetrachloroethene 0.250 ND 0.246 98.4 1 10.0-160 Trichloroethene 0.250 ND 0.254 102 1 10.0-160 Vinyl chloride 0.250 ND 0.245 98.0 1 10.0-160 (S) Toluene-dH 106 80.0-120 (S) 4-Bromofluorobenzene 98.1 77.0-126 (S) 1,2-Dichloroethane-d4 108 70.0-130 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 15 of 22 WG1903776 QUALITY CONTROL SUMMARY Semi -Volatile Organic Compounds (LCMS) by Method SW-846 8321 L1518453-01 Method Blank (MB) (MB) R3822047-2 03/02/22 1059 MB Result Analyte mg/I 2,4-D U 2,4,5-TP (Silvex) U (S) Z4-DB-D3 125 MB Qualifier MB MDL MB RDL mg/I mg/I 0.00667 0.0200 0.00667 0.0200 70.0-130 Laboratory Control Sample (LCS) (LCS) R3822047-1 08/02/22 10:41 Spike Amount LCS Result Analyte mg/I mg/I 2,4-D 0.200 0.218 2,4,5-TP (Silvex) 0.200 0.212 (S) Z4-DB-D3 LCS Rec. Rec. Limits LCS Qualifier 109 70.0-130 106 70.0-130 113 70.0-130 L1519458-20 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1519453-20 03/02/22 11:52 • (MS) R3322047-3 03/02/22 11:17 • (MSD) R3322047-4 03/02/22 1135 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I 2,4-D 0.200 ND 0.223 0.215 112 108 2,4,5-TP (Silvex) 0.200 ND 0.225 0.216 113 108 (S) Z4-DB-D3 106 117 Dilution Rec. Limits 1 70.0-130 1 70.0-130 70.0-130 MS Qualifier MSD Qualifier RPD RPD Limits 3.65 30 4.08 30 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 16 of 22 WG1902977 Pesticides (GC) by Method 8081B Method Blank (MB) QUALITY CONTROL SUMMARY L1518453-01 (MB) R3321005-1 07/30/22 19:58 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I Chlordane U 0.00167 0.00500 Endrin U 0.00167 0.00500 Heptachlor U 0.00167 0.00500 Heptachlor epoxide U 0.00167 0.00500 Gamma BHC U 0.00167 0.00500 Methoxychlor U 0.00167 0.00500 Toxaphene U 0.00333 0.0100 (S) Decachlorobiphenyl 76.6 10.0-128 (S) Tetrochloro-m-xylene 65.0 10.0-127 Laboratory Control Sample (LCS) (LCS) R3821005-2 07/30/22 20:07 Spike Amount LCS Result Analyte mg/I mg/I Endrin 0.0100 0.00947 Heptachlor 0.0100 0.0104 Heptachlor epoxide 0.0100 0.00948 Gamma BHC 0.0100 0.00884 Methoxychlor 0.0100 0.0109 (S) Decachlorobiphenyl (S) Tetrochloro-m-xylene LCS Rec. Rec. Limits LCS Qualifier 94.7 104 94.8 88.4 109 77.6 70.5 57.0-134 27.0-132 57.0-130 55.0-129 54.0-155 10.0-128 10.0-127 L1518453-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1513453-01 07/30/22 21:01 • (MS) R3321005-3 07/30/22 21:10 • (MSD) R3321005-4 07/30/22 2118 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Analyte mg/I mg/I mg/I mg/I Endrin 0.0100 ND 0.00838 0.00870 83.8 87.0 Heptachlor 0.0100 ND 0.00937 0.00982 93.7 98.2 Heptachlor epoxide 0.0100 ND 0.00831 0.00866 83.1 86.6 Gamma BHC 0.0100 ND 0.00777 0.00809 77.7 80.9 Methoxychlor 0.0100 ND 0.00983 0.0105 98.3 105 (S) Decachlorobiphenyl 68.8 73.6 (S) Tetrochloro-m-xylene 59.9 63.6 Dilution Rec. Limits 1 10.0-160 1 16.0-136 1 10.0-160 1 14.0-141 1 10.0-160 10.0-128 10.0-127 MS Qualifier MSD Qualifier RPD RPD Limits 3.75 39 4.69 40 4.12 36 4.04 40 6.59 34 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 17 of 22 WG1902662 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1518453-01 Method Blank (MB) (MB) R3820816-2 07/29/22 1436 MB Result MB Qualifier MB MDL MB RDL Analyte mg/I mg/I mg/I 1,4-Dichlorobenzene U 0.0333 0.100 2,4-Dinitrotoluene U 0.0333 0.100 Hexachlorobenzene U 0.0333 0.100 Hexachloro-1,3-butadiene U 0.0333 0.100 Hexachloroethane U 0.0333 0.100 Nitrobenzene U 0.0333 0.100 Pyridine U 0.0333 0.100 3&4-Methyl Phenol U 0.0333 0.100 2-Methylphenol U 0.0333 0.100 Pentachlorophenol U 0.0333 0.100 2,4,5-Trichlorophenol U 0.0333 0.100 2,4,6-Trichlorophenol U 0.0333 0.100 (S) 2-Fluorophenol 27.E 10.0-120 (S) Phenol-d5 15.8 10.0-120 (S) Nitrobenzene-d5 66.4 10.0-127 (S) 2-Fluorobiphenyl 71.3 10.0-130 (S) 2,4,6-Tribromophenol 79.5 10.0-155 (S) p-Terphenyl-d14 66.3 10.0-128 Laboratory Control Sample (LCS) (LCS) R3820816-1 07/29/22 1413 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I 1,4-Dichlorobenzene 0.500 0.323 64.6 18.0-120 2,4-Dinitrotoluene 0.500 0.438 87.6 49.0-124 Hexachlorobenzene 0.500 0.320 64.0 44.0-120 Hexachloro-1,3-butadiene 0.500 0.457 91.4 19.0-120 Hexachloroethane 0.500 0.325 65.0 15.0-120 Nitrobenzene 0.500 0.360 72.0 27.0-120 Pyridine 0.500 0.0746 14.9 10.0-120 3&4-Methyl Phenol 0.500 0.257 51.4 31.0-120 2-Methylphenol 0.500 0.240 48.0 28.0-120 Pentachlorophenol 0.500 0.431 86.2 23.0-120 2,4,5-Trichlorophenol 0.500 0.476 95.2 44.0-120 2,4,6-Trichlorophenol 0.500 0.459 91.8 42.0-120 (S) 2-Fluorophenol 31.1 10.0-120 (S) Phenol-d5 17.7 10.0-120 (S) Nitrobenzene-d5 62.6 10.0-127 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1518453 08/05/22 13:26 18 of 22 WG1902662 QUALITY CONTROL SUMMARY Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1518453-01 Laboratory Control Sample (LCS) (LCS) R3320316-1 07/29/22 1413 Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier Analyte mg/I mg/I (S) 2-Fluorobiphenyl 76.6 10.0-130 (S) 2,4,6-Tribromophenol 92.5 10.0-155 (S) p-Terphenyl-d14 41.6 10.0-128 L1518453-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD) (OS) L1513453-01 07/29/22 16:26 • (MS) R3320316-3 07/29/22 16:43 • (MSD) R3320316-4 07/29/22 1710 Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD RPD Limits Analyte mg/I mg/I mg/I mg/I 1,4-Dichlorobenzene 0.500 ND 0.275 0.250 55.0 50.0 1 17.0-120 9.52 40 2,4-Dinitrotoluene 0.500 ND 0.390 0.371 78.0 74.2 1 39.0-125 4.99 25 Hexachlorobenzene 0.500 ND 0.418 0.413 83.6 82.6 1 35.0-122 1.20 24 HexachIaro-1,3-butadiene 0.500 ND 0.419 0.398 83.8 79.6 1 12.0-120 5.14 34 Hexachloroethane 0.500 ND 0.275 0.256 55.0 51.2 1 10.0-120 7.16 40 Nitrobenzene 0.500 ND 0.318 0.300 63.6 60.0 1 12.0-120 5.83 30 Pyridine 0.500 ND ND ND 12.1 12.2 1 10.0-120 1.15 37 3&4-Methyl Phenol 0.500 ND 0.187 0.172 37.4 34.4 1 10.0-120 8.36 36 2-Methylphenol 0.500 ND 0.184 0.171 36.8 34.2 1 10.0-120 7.32 30 Pentachlorophenol 0.500 ND 0.338 0.330 67.6 66.0 1 10.0-128 2.40 37 2,4,5-Trichlorophenol 0.500 ND 0.382 0.361 76.4 72.2 1 33.0-120 5.65 31 2,4,6-Trichlorophenol 0.500 ND 0.370 0.352 74.0 70.4 1 26.0-120 4.99 31 (S) 2-Fluorophenol 23.6 19.9 10.0-120 (S) Phenol-d5 13.4 12.7 10.0-120 (S) Nitrobenzene-d5 57.4 54.6 10.0-127 (S) 2-Fluorobiphenyl 71.4 66.1 10.0-130 (S) 2,4,6-Tribromophenol 78.0 76.0 10.0-155 (S) p-Terphenyl-d14 61.1 63.1 10.0-128 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 19 of 22 GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and ifyou have additional questions please contactyour project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions u Fc Fss] MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). Fn RDL Reported Detection Limit. Rec. Recovery. Fr RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and F (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the F Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. Rc These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe samples from the time of collection until delivery to the laboratory for analysis. This section ofyour report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description J The identification ofthe analyte is acceptable, the reported value is an estimate. J3 The associated batch QC was outside the established quality control range for precision. J6 The sample matrix interfered with the ability to make any accurate determination, spike value is low. T8 Sample(s) received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1513453 03/05/22 13:26 20 of 22 ACCREDITATIONS & LOCATIONS Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122 Alabama 40660 Nebraska N E-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 California 2932 New Mexico TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 _ Georgia NELAP North Carolina 3 41 Georgia' 923 North Dakota R-140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky' 6 KY90010 South Carolina 84004002 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee'" 2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas5 LABO152 Maryland 324 Utah TN000032021-11 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2 LA A2LA— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2 LA — ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. Rc ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1513453 03/05/22 13:26 PAGE: 21 of 22 Company Name/Address: EMA Resources 755 Yadkinville Road Mocksville, NC 27028 Report to: Mr. Brent Collins Project Description: Sludge Phone: 336-751-1441 Collected by (print): �-•n�4- (A I I � � s Collected by (signature): Immediately Packed on Ice N Y Sample ID o�ctaf v% i1 Billing Information- l t A alvsis i Ccinta,iQer1,PrI;servat,t2�Cham of Custody Page _of _ Mr. Brent Collins Pres 755 Yadkinville Road Chk Mocksvilie, NC 27028 �JceAnalytical rbrent. a it To: IN65 Lebanon Rd Mount luRet. TN 37122 Submttiry v a W4 Na this drain of antode coilins@emaresourcesinc.com;roy,whitak cw„eman,uno.i,aimentand ac .0w, of the Pace Terms aid CO"M. found at City/State J_ Please Circle- httPsi/inro wsaiaba mm/hOfs/Pas-standard- Collected: ' I i �iU" PT MT CT ET t, ms Pm O/1tl.rf Client Project q Lab Project q �SDG q J 17 5 Site/Facility ID q P.O. q a Acctnum: EMARES ian cex'd i ll e. V z Rush? (Lab MUST Be Notified) Quote k a _� emplate;T11413 ° Prelo in: P895417 _Same Day _Five Day Z J g —Next Day _ 5 Day (Rad Only) Date Results Needed "' PM: 807 - Justin Carr _Two Day _ 10 Day (Rad Only) No. U = _Three Day of tJ-1 PB. Shipped via: FedEX Ground Comp/Grab Matrix ` Depth Date Time ntrs > U Remarks Sample a(lab onh/) -- -- U F- 0 ss 3` >/�s/72 9, 2a 2 x x I `Matrix: Niennarks: Sample Receipt Checklist SS -Soil AIR -Air F - Filter pH Temp COC Seal Present/Intact: _NP _.4 _N GW - Groundwater B - Bioassay COC Signed/Accurate: Y _N WW-Waste Water Flow Other Bottles arrive intact: Y _N Correct bottles used: Y N DW - Drinking Water OT- Other_. Samples returned via: jj 1Trackinga 5g9q - i5, (03� Sufficient volume sent: Y N 'N _UPS _FedEx _Courier 11 l [Trip VOA Zero Hea pacJL.�eli�� Y Preservation Correct/Checked: Y / Relinquished by: (Signature) Date: Time: Received by (Signature) Blank Received: Yes o e1 7/Z,C/Zz 3 o HCL/MeoH PAD Screen <0.5 mR/hr: :L —N :'5.vi�7�i� •.3 TBR 0 Relinquis ed by :(Signature) Date: Time: Received by: (Signature) Temp: °C Bottles Received* If preservation required by Login: Date/Time Q- ^ .r, Z Relinquished by: (Signature) Date Time: Received for lab by: (Signature) Date: Time: Hold: i Condit06 A_ - 14, i , NCF / L- Standard Operating Procedure and Operation and Maintenance Plan for the Town of Yanceyville - Land Application Program 1. Purpose a. Ensure the requirements of the Town of Yanceyville, NC Non -Discharge Permit#WQ0028547 are met. 2. Personnel a. The following is a list of personnel in order they are to be contacted when information needs to be shared. Ira► I_\:ZalyIW-MM 1. Brandon Shaffer — Project Manager 336-978-3245 2. Roy Whitaker — Director of Bus.Dvlpmt./Ops. 336-909-1718 3. Brent Collins — Director of Technical Services 336-399-3646 ii. Town of Yanceyville, NC 1. Kamara Barnett - Town Manager 336-694-5431 3. Operational Functions a. The operational function of this project it going to involves transporting the thickened liquid residuals via tanker trailers to a staging area in the receiver sites. The liquid residuals will be off-loaded into tractor/pull tank spreader and land applied in a uniform application. It is going to be spread at agronomic rates that are determined using the Realistic Yield Expectations (RYE) as outlined in the permit, the amount of other nutrient sources the landowner and operator has applied, and the residuals nutrient and metal sample that is current for that monitoring period. The material is going to be land applied on fields that have a crop growing on them that are going to either be grazed or cut for animal feed or row crops for feed or fiber. Application rates will be reduced by 25% on fields that are primarily used for grazing in accordance with USDA-NRCS 590. Grazed fields will be determined by the farmers and EMA project managers. 4. Maintenance Schedule a. EMA Resources Inc. will follow the maintenance schedule as recommended by the EMA Resources EHS&T Director for the equipment necessary to complete the job. 5. Safety Measures a. The Town of Yanceyville and EMA Resources Inc. believe in operating in a safety conscious manner and all employees participate in safety training that is designed to help employees recognize safety issues and take steps to prevent accidents from occurring. In addition, EMA Resources employees have the authority to stop operations if they think any aspect of the operation is going to cause environmental or personal harm. 6. Spill Response Plan a. In the unlikely event of a spill, the following action shall be taken immediately. i. Management of Spill Clean-up Activities: The EMA Resources Project Manager shall take immediate charge and initiate clean-up activities. EMA Resources labor and equipment is to be utilized. In the event additional labor and equipment is required, assistance may be requested from the Town of Yanceyville, The NC Department of Transportation, and other private contractors as necessary. ii. Halt the Source of the Spill: Such as a ruptured container or damaged transport unit. iii. Contain the Spill: Form a barrier. Sufficient quantities of straw shall be used for such purposes. Earthen barriers may be constructed to augment the straw bale containment area of the spill. The Operations Manager or the person in charge on the spill site will be advise the clean-up personnel where to get the straw, lime, and other items necessary to complete the clean-up operation. le. local farmers, farm supply centers, nurseries. iv. Initial Clean -Up: Employ front-end loaders, vacuum equipment, sludge application vehicles, and/or local septic tank service to remove as much of the spilled material as possible. Straw and/or sand should be scattered in the spill area to soak up the remaining material. The straw and sand soaked material will be collected and removed to a disposal area approved by representatives of the state regulatory agency. v. Final Clean-Ua: Employ rotary brush sweeper if needed and apply lime to the spill area upon the approval of the clean-up efforts by the state regulatory representative. If the event occurs on private property, the clean-up will be completed to the satisfactory of the property owner and state regulatory representatives. The ultimate goal will be restore the spill area to its original condition if possible. vi. Notification: As soon as possible after the spill occurs, the EMA Resources Project Manager or designee will notify the Town of Yanceyville and the EMA Resources main office. EMA Resources office staff is then responsible for notifying other key EMA Resources personnel. vii. Reporting_ EMA Resources staff will notify the Winston-Salem regional office of the NCDENR by telephone (336) 776-9800 as soon as possible, but not more than 24 hours after, or on the next working day following the occurrence. The EMA Project Manager shall provide a written report with 48 hours of the spill to the EMA Resources Director of Technical Services and the Town of Yanceyville staff. The report shall list all relative information and actions taken. With the assistance of EMA Resources personnel, and the Town of Yanceyville personnel, a written report will be filed with the Raleigh regional office within 5 days of the occurrence. For after-hours reporting, the Division's emergency number shall be called to report all incidences (800) 662-7956. 7. Inspection Plan a. Inspection for the land application of residuals will conducted on a minimum of a weekly basis at the land application site during land application activities. The inspection frequency is based on the time frame that it is going to take to complete the project and the amount of dry tons to be land applied from this facility. The inspections will consist of inspecting a current field that is being applied as well as inspecting random fields that have been completed. Inspections will be conducted by Brandon Shaffer — Project Manager. These inspections will consist of the following: i. Verifying the application rates for each field that plan on receiving material. ii. Checking the calculated loads to ensure the correct amount of residuals are being land applied. iii. Ensure that all manned equipment has a copy of the permit and the operation and maintenance plan. iv. Ensure that the field has been flagged properly and that all buffers are being adhered to. v. Ensure proper signage has been posted vi. Verify that the proper number of samples of the residuals have been taken and that it meets the criteria for land application. vii. The records will be kept in the EMA Resources project files in the main office. Copies of all analyses and records will be forwarded to the Town of Yanceyville and kept on file. viii. EMA Resources and the Town of Yanceyville staff will immediately inform the other party if any of the following conditions are noted. 1. Any occurrence with the distribution program resulting in the land application of significant amounts of material that is abnormal in quantity or characteristics. 2. Any failure of the distribution system that results in the release to surface waters. 3. Any time that self -monitoring indicates that the facility has gone out of compliance with the permit. 4. Any process failure that results in the system not adequately treating the residuals. 5. Any spill or discharge from a vehicle or piping system during residuals transportation. 6. Any release that requires immediate reporting outside normal business hours shall be called in by EMA Resources staff to DENR at (800) 662-7956. This number is to be called in the event of a release to surface waters or imminent failure of a storage system when the event occurs outside of normal business hours. 8. Sampling and Monitoring Plan a. Sampling for this project consists of sampling the residuals prior to land application occurring in order to ensure that the residuals are suitable for land application. b. The samples will be collected from the two storage lagoons that holds the thickened residuals c. Brandon Shaffer, Brent Collins, or other designee will be responsible for sample collection for nutrient and metal, TCLP, and fecal coliform. d. Nutrient, metal and TCLP sample aliquots will be collected randomly and consist of at least 7 individual aliquots mixed together in order to get the composite sample for these parameters. e. The residuals will be sampled annually for TCLP including the RClls. f. Metal and nutrient parameters will be collected and analyzed based on the requested dry ton numbers in the permit application. g. Residuals will be sampled for fecal coliform to demonstrate pathogen requirements have been met. Seven separate samples will be collected and analyzed. 9. Environmental Impacts a. The environmental impacts for residuals may be affected by this procedure. b. This procedure helps assure that land application is conducted in a safe and efficient manner while ensuring compliance with the laws and regulations and to minimize exposure, negative environmental impacts and public relation concerns. Residuals Information Sheet Generator: Town of Yanceyville Facility: Yanceyville WWTP/WTP Add ress: PO Box 727 Yanceyville, NC 27379 Phone: (434) 203-7056 Contact: Matthew Malone Land Application Contractor: EMA Resources Inc. 755 Yadkinville Rd Mocksville, NC 27028 Phone: 336-751-1441 Contact: Roy Whitaker Please Note: The application of these residuals is only allowed in accordance with subject permit. (W Q0028547 ) All applicable setbacks in accordance with 15A NCAC 02T .1108(b) will be adhered and is the responsibility of the land application contractor. Application rates shall be applied at agronomic rates for intended uses. No residuals shall be applied to any site that is flooded, frozen, or snow covered. Adequate procedures will be implemented to prevent surface runoff of residuals in any surface waters. The attached residuals analysis report is a summary of major and micro -nutrients available in the residuals. If you have any questions concerning this information, you may contact EMA Resources Inc, at the number listed above. Applicant's name: Town of Yancey Land application sites currently certified: 188.42 net acres and Total to be certified: 160.89 net acres. L LAND APPLICATION SITE INFORMATION (See Instruction B): Status Codes Site/Field ID Landowners �� Lessees or Operator(s) �� Net Acres County tY Crop(s) s P�) Predominant Soil Series Name b Mapping Unit or Rep. Slope' R/M NC-CS09-11 Jennifer Hodges 28.85 Caswell Fescue Fairview FbB2 D NC-CS80-01 Wayne & Virginia Hodges 3.17 Caswell Fescue Fairview D NC-CS80-02 Wayne & Virginia Hodges 11.06 Caswell Fescue Poindexter R/M NC-CS80-04 Ruby Hovatter 22.28 Caswell Fescue Fairview FbB2 R NC-CS81-01 Vernon & Sylvia Williamson 9.69 Caswell Fescue Iredell IrB R NC-CS81-02 Vernon & Sylvia Williamson 5.14 Caswell Fescue Iredell IrB R NC-CS81-03 Vernon & Sylvia Williamson 3.5 Caswell Fescue Helena HeB R NC-CS81-04 Vernon & Sylvia Williamson 11.97 Caswell Fescue Iredell IrB R NC-CS81-05 Vernon & Sylvia Williamson 15.43 Caswell Fescue Orange OrB R NC-CS81-06 Vernon & Sylvia Williamson 5.77 Caswell Fescue Helena HeB R NC-CS81-07 Vernon & Sylvia Williamson 15.73 Caswell Fescue Iredell IrB R NC-CS81-08 Vernon & Sylvia Williamson 8.38 Caswell Fescue Helena HeB R NC-CS81-09 Vernon & Sylvia Williamson 7.15 Caswell Fescue Helena HeB R/M NC-CS82-01 Jon Crispin 4.49 Caswell Fescue Fairview FbB2 R/M NC-CS82-02 Jon Crispin 6.21 Caswell Fescue Fairview FbB2 R/M NC-CS82-03 Jon Crispin 6.47 Caswell Fescue Fairview FbB2 R/M NC-CS82-04 Jon Crispin 9.83 Caswell Fescue Fairview FbB2 DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Town of Yanceyville hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-CS-09-11 No Hay/Pasture Feed The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 L STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terns and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. IL RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(hl allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ® A re -defined compliance boundary is needed for field(s) ID: NC-CS-09-11 (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 3 r Coo T •Rt� i w _fit; Well ■ Off Site Dwelling I� ► a' �- Drain Field Boundary jr,rr tir�r� Property Boundary Buffer Field Total Acres Applicable Acres ;+. ,,► "'`' ti,,� — — — Ditch 11 52.33 28.85 crr x SCALE: 1":440' �\ FIGURE NO. 7-� Town of Yanceyville DATE 5/6/2024 °'vMA Land Application Program DRAWN BY: BC Resources, Inc. 2 PROJECT NO: CS09 WQ0028547 Jennifer Hodges Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Jennifer Hodges Operator: Glen Hodges Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 92.26 Site #: Predominant Soil Series: FbB2 Crop 1 Max. PAN: 141 Crop 2 Name: Acres Utilized: CS09 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 38 38 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o oa o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5/4 110500 3.76 0.456 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 3.471 NA Fescue 5/5 78000 3.76 0.322 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 2.450 NA Fescue 5/7 156000 3.76 0.644 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 4.901 NA Fescue 5/8 71500 3.76 0.295 Yancey WTP D <.5" S 0.5 0.3 9460 3960 177 2.246 NA Fescue 0.000 0.000 0.000 4/10 169000 3.84 0.712 Unifi,Inc. Dry <.5" S 0.5 0.3 18700 8470 132 10.591 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 585000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 23.660 0.000 Lime Applied Annuallbs/acre 0.067 0.008 0.888 0.101 0.121 0.002 0.021 0.043 0.078 1.321 6.804 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.067 0.008 0.888 0.101 0.121 0.002 0.021 0.043 0.078 1.321 Permitted C. P. L. R.**** 36 34 1 1338 1 267 1 15 374 1 89 2498 Permit PAN Limit Ist/2nd Crop i r 141 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 1/21/2021 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Town of Yanceyville hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-CS-80-04 No Hay/Pasture Feed The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 L STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terns and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. IL RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(hl allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: 1 certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners Ql that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: R w6:, 16v. } vo r Address: `ZI9 I New. i•'atsPj City: Phone: 334 - 3 $S - 2-y9 5 State Nc E-mail address: zip: _ 7 Signature: � , ` Date: 5I2 q NORTH CAROLINA, _ ♦+ t I COUNTY I, the undersigned Notary Public do hereby certify that R.+ 6y S . ) 42,A, 4-"u personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the day of M. Brent Collin$ Signature and seal: My commission expires: 313012-4, Davie Courtly, NG Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone - Signature: Permittee's Certification: State: E-mail address: Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: _ Kam;; Barnet' kawai-a Evm� 'tt Signature: �ama�Ra.�o�„M� V-4.:�Fnn, Date: 05/10/2024 FORM: LOA 06-16 Page 3 of 3 E 62 tax . Ism CF- N C 340 Pm Id ce -Fie1ds�j,::4 LW M2 < Uar Red A` at 323 s MS �17 AIN 86 up lama an 131 1310 08969 fail 1705 Le top Casa! 4 f 86' Tomt- 1121 62 06 Ing ITJO NC-CS-81 V�- if - , ' r ` +`n ,ust'~ �� y ' -Fields'l'--9-' Ira 17 Im 2749 1727 .31 ru IN/ 111Y11 -7' LUM If 711 If LW ME LM rm b" Ib 62 Legend W 1 0 2 Field Boundary Miles IV Scale: 1 inch equals 2 miles NC-CS-80(1 - 4) LOCATION MAP Figure Drawn by: CSC Town of YanccyviRe ©ass B Residual Permit Reviewed by: SOEL Yanccy-v-illc, North CarolinaPLUS Date: Oct '13 Soil Plus Project # 201205A10 kitr en N a �tes ' , ,r » NC �S 63 ?W�- Davtid:Brown "fir:. ff ► u s �1 7.07 r s Ac. I - " 4-aaz arlton .,_ ` 1.06 et C. l Foster, 0' T. � A. � Mar9PIrett Marshall "'►' _ r 1 , W + Y * iitginea Hod eOhio 'tRuby Hovatieryr '4 NC -CS.. 4 *7 A25.89 Gross Ac. 25:89"Gr s•AC4 o Park Springs 22:28 Net Ac. ! tor. Pentacostal r d 1 ,;Iy Church Ruby Hoi Mary hod s 'N.C-CS-80-4 22.28 Net E. �jW I,,. I i-,vat i IA*md Ma Hiidges , House Xla.x Hodgesy A Structure • Well ` ----W- Ditch —No- Stream ` ® Buffer Q Field Boundary Q Field Boundary © Net Area Pond r 0 Property Boundary ' I 400 200 0 400 1 Felt Scale: 1 inch equals 400 feet NC-CS-80 BUFFER MAP (Field 4) Figure ,Drawn bv: CSC Town of Yanceyl•ille Class B Residual Permit Rcvicwcd bv: SOIL Yanccvvillc, North Carolina 3 PLUS Date: Oct.'13 Soil Plus Proiect # 201205.A10 I Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Ruby Hovatter Operator: Wayne Hodges Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 19.36 Site #: Predominant Soil Series: FrD2 Crop 1 Max. PAN: 115 Crop 2 Name: 4 CS 80 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 22.28 22.28 0 o � N Q Volume applied enter one Solids/ ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/17 84500 2.1 0.332 Yanceyville WTP D <.5" S 0.5 0.4 7580 50 2.13 2.019 NA Fescue 10/18 136500 2.1 0.537 Yanceyville WTP D <.5" S 0.5 0.4 7580 50 2.13 3.261 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 221000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 5.280 0.000 Lime Applied Annuallbs/acre 0.010 0.003 0.026 0.050 0.010 0.001 0.020 0.100 0.009 0.063 1.665 Date lbs/ac 2000 Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 Current Cumulative lbs/ac 0.010 0.003 0.026 0.050 0.010 0.001 0.020 0.100 0.009 0.063 Permitted C. P. L. R. * * * * 1 36 34 1 133 S 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop I F-115 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/9/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Town of Yanceyville hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-CS-81-(1-9) No Hay/Pasture Feed The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 L STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terns and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. IL RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(hl allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ❑ A re -defined compliance boundary is needed for field(s) ID: (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ® A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded Iandowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: `ft(^0n WIl1;0MSOn Address: 84,40 O NC F+t.. u AV& City: _Vae [� ,y l l i Phone: —336_- S/ `1- State: /x Zip: 27;79 _ E-mail address: iature: e: NORTH CAROLINA, _6jf&•!i COUNTY I, the undersigned Notary Public do hereby certify that _ ef4o4 personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the ZSt� day of— c: 20 211 Signature and seal M. Brent Collins My commission expires: 4relZ(+ My Commission Expires March 30, 2026 Lessee's/Operator's Certification: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail address: Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: _Kamara Bame« — — kawla-a EanWr 05/10/2024 Signature: Kama., aa, att iMa„ in iron FnT) Date: FORM: LOA 06-16 Page 3 of 3 57 62 tits , `\! N� Isis- 4 NC-CS=80;�_ `!]iu ,+ Lst ! MAW / ]]6Sr 1iL isu t < Fie\lds4. ,;A ProaWer�a�J - \J(.'.. J`i��- un % ,lHM �� s«N + y MU •lied . Prim ti 2mg ]m f lid ' ` >� COOII�l1 ! f tO} V l iqr AEii s� r /L7ij r .O ]ice 1` /1 J 1 • \`;1 1' 11.30111 ,q �i•--�./ �� 1 to '1 « \ ~ + �� r�• C I ,_ j� i` / / �. �. ^. �1 J f ` 1i 62 Lam IN 06 TIvaT f°'� 1311 s 1i ys� 62 r � ti. � �� � � o ►ter '•, .��...� � � ---... �,•�,. _ � / ll2l �62� rY'� Ala �- rrta p of a � Ii_ ♦ /l to hilt N�C.S-CS t r tam ' _� �,p Ficid an, lab \~N Mtlaailk ,t -! J i�S� l �� \ 1 y inaa_ u9s 110 �, •. -� / 1J '� �� tom+ Lumm g ]l44��- L { _��. ^� t.+ �e�.,}tzl / Legend stop-2 1 0 .. 2 1 Field Boundary Miles sy errrlmp Scale: 1 inch equals 2 miles NC-CS-81(1- 9) LOCATION MAP Figure Drawn b : CSC Town of Yanceyville Glass B Residual Permit Rcviewed by: �U Yance ille, North Carolina 1 Date: Oct.'13 Soil Plus Project # 201205.A10 "Harold Cobb -cs eta u k 8.71 Gross C. NC -CS 81-9 Marks& Crary Cobb'*';Ph71 yllisti , ti 12.63 Gross Ac.,' Carneal 1 NC-CS-81-6 `Willm - ia'', � '`�' Parsons NC-CS-81-1 9.44 Gross Ac. 5.77 Net Ac. _ t'r1T+i11 ,i NC-CS-814 9.69Net 1. 'S)1 ai Willi anisoti 6.91Net Ac. NBC-CS-81-9 v � � Q ti y' 2.54�Grose.Ac. � jam 2.97 Gross Ac. V N Williamson a NC-CS-81 4 }}++ 1 ~ y 2.53 Net Ac. 13.76 Grose Ac. a 3 z uJ �.6.34 Gross Ac. u 4J E i � f�+ NC-CS-81-2 Shirle V ° C. Cecil, 10.47 Net Ac. NC-CS-81-5 Tara Patterson e� 4 ao +E �►�i 6.61 Gross Ac. - 3.50 Gross A,. 1 • 1 ' NC:CS-81-3 NC CS81-5 LTr 'd 3.50 Net Ac 4.96 Net Ac. • _ Vernon & � `� Willis Age"d lva Williamson �i� A AL- j . Thensa; ■ House v A Structure �� ,Vernon & :� Sylva Wilffia'rris�o ' • Well a 1q _...� Ditch Or 4U ,� 1 • ,� —110- Stream r Shirley Vernon ® Buffer' © Net Area a. V Q Field Boundary ProBoundary rY - _ Pond 4()0 200 0 400 r• u v v Ij i! V Annette Annette i� McDuff a w t �. MCDuffiey r� n i w t;e ` + 44 Mc lteffi Ijw P ! 995 Gross Ac. Vernon & S'O>,'a Williamson 20.92 Gross Ac. 1' NGCS-81-8 Y ti ISM Net Ac. NC-81-7 y �pa ge fit' � O 8 t"" AL.Haze! Low 4 Ma cc . .. o o 0 8.71 Gross Ac.■ Y, ti 7.48 Gross Ac. NC -CS 81-1 i� 4 - NC-CS-81-6 I. A- & a J._, ry �. NGCS-81-9 rIs W Wendy Scott {] c „ P. 9.44 Gross Ac: 5.77 1Vei'Ac. 5.76 Net Ac. L�ti (, C Z ?, LA NC-CS-81-4 r(/} y F 1 k a William$on �y 6,91 Net Ac. NC-GS-B]-9 a u y 2.54.GrosslAc. 1:39 Net-Ac. I rMa ha Scotty' a Z97Gross Ac. $� 4 NC-CS41-4 2.53 Net Ac. 13.76 Gross Ac. k .` • ' . 1 l egrnti 1 Grose C. � I . House '6 r l' Shirley Vernon Structure 10.47 Net Ae. well NC-CS-81-5 v , - — Ditch —► Stream Buffer Net Area 3.% Gtoss A,6.61 Gross Ac. _ G 4� r t� Field Boundary NC-Ib -81-3 NC-Cs-81-5 0 Property Boundary '' + • Q �' vVi M 3.50 Net Ac. 4.96 Net Ac. Pond � Thensa Willis h >~ a 400 20(l 0 400 C Vernon &_ There is no cumulative data for fields NC-CS-81-01,02,03,08 Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Vernon Williamson Operator: Vernon Williamson Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 6.83 Site #: Predominant Soil Series: IrB Crop 1 Max. PAN: 87 Crop 2 Name: 4 CS81 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 11.97 11.97 0 o � N Q Volume applied enter one Solids/ ) Liquid Cu_ Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # - w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/19 78000 2.1 0.571 Yanceyville WTP D <.5" S 0.5 0.4 7580 50 2.13 3.468 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 78000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 3.468 0.000 Lime Applied Annuallbs/acre 0.007 0.002 0.017 0.033 0.007 0.000 0.013 0.066 0.006 0.041 1.094 Date lbs/ac Prior Years Cumulative lbs/ac 0.076 0.033 2.872 1.011 0.423 0.014 0.092 0.399 0.07 5.137 Current Cumulative lbs/ac 0.083 1 0.035 2.889 1.044 0.430 0.014 0.105 0.465 0.076 5.178 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 1 15 1 1 374 89 2498 Permit PAN Limit Ist/2nd Crop 1 87 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/9/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Vernon Williamson Operator: Vernon Williamson Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 35.09 Site #: Predominant Soil Series: OaA Crop 1 Max. PAN: 81 Crop 2 Name: Acres Utilized: CS81 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 15.43 15.43 0 o � N Q Volume applied enter one Solids/ ) Liquid Cu_ Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # - w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/18 58500 6.75 1.067 Yanceyville WWTT D <.5" S 0.5 0.3 28700 3990 62.4 20.213 NA Fescue 4/20 52000 6.75 0.949 Yanceyville WWTT D <.5" S 0.5 0.3 28700 3990 62.4 17.967 NA Fescue 10/19 45500 2.1 0.258 Yanceyville WTP D <.5" S 0.5 0.4 7580 50 2.13 1.570 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 156000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 39,7491 0.000 Lime Applied Annuallbs/acre 0.015 0.009 1.201 0.311 0.206 0.003 0.026 0.194 0.023 2.527 42.024 Date lbs/ac Prior Years Cumulative lbs/ac 0.09 0.037 3.349 1.39 0.528 0.016 0.105 0.5 0.08 5.863 Current Cumulative lbs/ac 0.105 1 0.046 4.550 1.701 0.734 0.019 0.131 0.694 0.103 8.390 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 81 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/9/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Vernon Williamson Operator: Vernon Williamson Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 20.13 Site #: Predominant Soil Series: HeB Crop 1 Max. PAN: 122 Crop 2 Name: 6 CS81 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 5.77 5.77 0 o � N Q Volume applied enter one Solids/ ) Liquid Cu_ Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # - w •, * N *� TKN mg/kg Z ; o as o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/21 71500 6.75 3.488 Yanceyville WWTT D <.5" S 0.5 0.3 28700 3990 62.4 66.065 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 71500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 66.065 o.000 Lime Applied Annuallbs/acre 0.021 0.014 2.065 0.513 0.352 0.005 0.035 0.285 0.035 4.339 71.853 Date lbs/ac Prior Years Cumulative lbs/ac 0.087 0.038 4.105 1.357 0.567 0.018 0.111 0.531 0.079 7.219 Current Cumulative lbs/ac 0.108 1 0.052 6.170 1.870 0.919 0.023 0.146 0.816 0.114 11.558 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 1 15 1 1 374 89 2498 Permit PAN Limit lst/2nd Crop 1 122 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/9/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Vernon Williamson Operator: Vernon Williamson Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 12.80 Site #: Predominant Soil Series: IrB Crop 1 Max. PAN: 87 Crop 2 Name: Acres Utilized: CS81 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 15.73 15.73 0 o � N Q Volume applied enter one Solids/ ) Liquid Cu_ Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/20 13000 6.75 0.233 Yanceyville WWTT D <.5" S 0.5 0.3 28700 3990 62.4 4.406 NA Fescue 4/21 32500 6.75 0.582 Yanceyville WWTT D <.5" S 0.5 0.3 28700 3990 62.4 11.015 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 45500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 15.421 o.000 Lime Applied Annuallbs/acre 0.005 0.003 0.482 0.120 0.082 0.001 0.008 0.066 0.008 1.013 16.768 Date lbs/ac Prior Years Cumulative lbs/ac 0.016 0.008 1.484 0.226 0.144 0.002 0.023 0.136 0.019 2.988 Current Cumulative lbs/ac 0.021 0.011 1.966 0.346 0.226 0.003 0.031 0.202 0.027 4.001 Permitted C. P. L. R.**** 36 34 1 1338 1 267 1 15 374 1 89 2498 Permit PAN Limit Ist/2nd Crop 1 87 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/9/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Vernon Williamson Operator: Vernon Williamson Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 20.13 Site #: Predominant Soil Series: HeB Crop 1 Max. PAN: 122 Crop 2 Name: 9 CS81 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 7.15 7.15 0 o � N Q Volume applied enter one Solids/ ) Liquid Cu_ Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # - w •, * N *� TKN mg/kg Z ; o M o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4/21 71500 6.75 2.815 Yanceyville WWTT D <.5" S 0.5 0.3 28700 3990 62.4 53.314 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 71500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 53.314 o.000 Lime Applied Annuallbs/acre 0.017 0.011 1.666 0.414 0.284 0.004 0.028 0.230 0.028 3.502 57.989 Date lbs/ac Prior Years Cumulative lbs/ac 0.033 0.022 4.663 0.917 0.519 0.015 0.07 0.442 0.022 8.19 Current Cumulative lbs/ac 0.050 1 0.033 6.329 1.331 0.803 0.019 0.098 0.672 0.050 11.692 Permitted C. P. L. R.**** 36 34 1 1338 1 1 267 1 15 1 1 374 89 2498 Permit PAN Limit lst/2nd Crop 122 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/9/2018 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) DWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources 15A NCAC 02T .1100 — LAND OWNER AGREEMENT FORM: LOA 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting General — This document is an agreement between the Applicant and land owner(s) of residuals receiving sites for land application of Class B residuals (may include water treatment plant or other type residuals) in accordance with 15A NCAC 02T .1100. Do not submit this agreement for review without a corresponding application form (FORM: RLAP 06-16). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Land Owner Agreement (FORM: LOA 06-16): ❑ Submit the completed and appropriately executed Land Application Site Certification (FORM: LASC 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ❑ Prepare a separate agreement for each set of land application sites that are owned or operated by an entity other than the Applicant. ❑ A copy of the completed and appropriately executed agreement must be provided to the landowner and the lessee/operator. AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS TO PRIVATELY OWNED LAND The undersigned landowner or his representative hereby permits: Applicant's name: Town of Yanceyville hereinafter referred to as the Permittee, to land apply residuals from the following facility(ies) onto the following land application site(s) (i.e., see attached setback maps) in accordance with the stipulations and restrictions as given in this Agreement: Site/Field ID Lease (yes/no) Land Use or Cropping Patterns Intended Use of Crops Residuals Source (optional) Special note (no-till/over-seed/ pasture) NC-CS-82-(1-4) No Hay/Pasture Feed The landowner or his representative receives, in consideration, full use of the nutrient value of the applied residuals while the Permittee receives, in consideration, the use of the land application site(s) described above for the disposal of the residuals. This Agreement shall remain in effect for the length of the Division's permit for the residuals land application program and shall be renewed each time this permit is renewed. The undersigned landowner or his representative and the Permittee agree to abide with the following restrictions and stipulations until such time as written notification, given 30 calendar days in advance, modifies or cancels this Agreement. FORM: LOA 06-16 Page 1 of 3 L STIPULATIONS: 1. The landowner or his representative shall not enter into any additional residuals application contracts or agreements with another permitted entity for the site(s) specified by this Agreement. 2. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) to a third party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions of this Agreement. 3. The landowner or his representative shall adhere to the provisions of this Agreement until all of the site restrictions (under Section II) are met. 4. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWR, Non -Discharge Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617. 5. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application site(s) to a new landowner. In addition, the current landowner shall give a notice to the new landowner that gives full details of the residuals applied at the land application site(s). 6. The Permittee has provided the landowner or his representative with information and data concerning the residuals land application program, including an analysis of constituents of the residuals, residuals application methods, schedules for typical cropping patterns, a description of the equipment used by the Permittee. 7. The Permittee will provide the landowner or his representative with a copy of the residuals permit prior to commencement of any residuals land application event and a copy of the results of each soil analysis. 8. If the soil pH of the land application site(s) is not maintained at 6.0 or greater, sufficient amounts of lime shall be applied to achieve a final soil pH of at least 6.0, unless an agronomist provides information indicating that the pH of the soil, residuals and lime mixture is suitable for the specified crop. 9. The landowner or his representative and the Permittee will agree on residuals application rates and schedules based on crop patterns, results of soil samples, and the permitted application limits. 10. The landowner or his representative will provide the Permittee with information regarding the amount and analysis of other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application site(s). 11. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this Agreement and schedule residuals land application events at appropriate periods. 12. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee, the landowner, or his representative prior to and during a residuals land application event. 13. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their representatives to; enter and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose of determining compliance with the permit; establish monitoring facilities on or near the land application site(s) as required by the permit; copy any records that must be kept under the terns and conditions of the permit; take necessary leachate, surface water, groundwater, or soil samples during the term of, and 12 months after termination of, this Agreement. IL RESTRICTIONS: 1. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access to the land application site(s) during active use and for the 12-month period following a residuals land application event. Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s). 2. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during these periods after such residuals land application events. 3. Food crops, feed crops, and fiber crops shall not be harvested for a 30-day period following a residuals land application event. 4. Food crops with harvested parts that touch the residuals/soil mixture and are totally above the land surface shall not be harvested for a 14-month period following a residuals land application event. 5. Food crops with harvested parts below the surface of the land shall not be harvested for a 20-month period following a residuals land application event when the residuals remain on the land surface for four months or longer prior to incorporation into the soil. 6. Food crops with harvested parts below the surface of the land shall not be harvested for a 38-month period following a residuals land application event when the residuals remain on the land surface for less than four months prior to incorporation into the soil. 7. Turf grown on land where residuals are applied shall not be harvested for a 12-month period following a residuals land application event. III. ALTERNATIVES FOR WATER SUPPLY WELLS INSIDE THE COMPLIANCE BOUNDARY: (please check one) 15A NCAC 02L .0107(d) prohibits water supply wells within the compliance boundary. However, 15A NCAC 02T .0105(hl allows the compliance boundary to be placed closer to the waste disposal area, such that the water supply well is situated outside of the compliance boundary provided the groundwater standards can be met at the newly -established compliance boundary. Please mark one of the following; ® A re -defined compliance boundary is needed for field(s) ID: NC-CS-82-01.02.03 (Please include the rationale for the requested re -location of the compliance boundary and attach a map showing the newly proposed compliance boundary to the application package) ❑ A re -defined compliance boundary is not needed for this site. IV. ACKNOWLEDGEMENT OF FIELD TRANSFER: (if needed) ❑ The land application field(s) ID: is currently permitted under another residuals land application program; Permit Number WQ: The land owner hereby acknowledge that by signing this agreement, he/she is requesting that the field(s) be removed from the previously permitted residuals land application program and transferred into the new program; (Name of the new program) FORM: LOA 06-16 Page 2 of 3 Landowner's Certification: I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land application site(s) are not included in any waste disposal contract or agreement with another municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the stipulations, restrictions, alternatives for water supply wells inside the compliance boundary, acknowledgement of field transfer, and do hereby grant permission to the Permittee to land apply residuals to the land application site(s) as specified herein. Landowner name: _DIVA) r1 Address: � � 1 6 • Q L 4 j G f 244- City: 151-t. Q AJ L 64 State: 14 L Zip: a 07 Phone: �70 - d, Yf- E-mail address: t I AJ ��C�� C. C 6 � F Signature: _ Date: yh�lzy NORTH CA A, �SwZ� I _ COUNTY I, the undersigned Notary Public do hereby certify that ­%^ Cw�1ti+ personally appeared before me this day and acknowledged the due execution of the forgoing instrument. WITNESS my hand and official seal this the ITS, day of _ _T 20 ZY 1 K Brent Win Signature and seal: r! ►. �it�i"� _ -pyVil 'ALM My commission expires: Lessee's/Operator's Certification: 3/3olik-P MY 0MV NO I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Lessee/operator name: Address: City: Phone: Signature: Permittee's Certification: State: E-mail address: Date: Zip: I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as specified herein. Signing official name: Kamara Barnett Signature: _me/CaBWma EL'u Date: 05/10/2024 FORM: LOA 06-16 Page 3 of 3 7 op v'Ar'l I. 2 ", . KT + 2 Ar lee " tAit 7�' 01 Wo W, MIMI 7 17 4�- 77 x - x Fenceline 141 - Buffer uffer I IF An' 9 Well A. On Site Dwelling 0 Off Site Dwelling Field Total Acres Applicable Acres Church 1 5.02 4.49 Field Boundary 2 7.21 6.21 Pond 3 1 6.49 1 6.47 Property Boundary 4 14.69 9.83 SCALE 1":440' Town of Yanceyville DATE 5/6/2024 FIGURE NO. Land Application Program DRAWN BY: LY-./.MA 2 PROJECT NO: BC —Resources, Inc. CS82 WQ0028547 Jon & Bonnie Crispin Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Bonnie Crispin Operator: Jon Crispin Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 2.87 Site #: Predominant Soil Series: FbB2 Crop 1 Max. PAN: 141 Crop 2 Name: Acres Utilized: CS82 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 4.75 4.75 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu_ Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o oa o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/18 4500 1.91 0.075 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 6.041 NA Fescue 10/19 31500 1.91 0.528 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 42.284 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4-0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 36000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 48,3257 0.000 Lime Applied Annuallbs/acre 0.016 25.851 0.488 0.054 0.081 0.002 0.010 0.041 0.022 1.132 24.643 Date lbs/ac Prior Years Cumulative lbs/ac 0.069 0.017 3.904 0.426 0.766 0.004 0.057 0.311 0.088 8.43 Current Cumulative lbs/ac 0.085 25.868 4.392 0.480 0.847 0.006 0.067 0.352 0.110 9.562 Permitted C. P. L. R.**** 1 36 34 1 1338 1 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 141 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/1/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Bonnie Crispin Operator: Jon Crispin Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 6.45 Site #: Predominant Soil Series: FbB2 Crop 1 Max. PAN: 141 Crop 2 Name: 2 Acres Utilized: CS82 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Q Volume applied enter one Solids/ Liquid Cu_ Yds Gallons o /o Solids Volume A lied er pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a c� w *o• o ,•d � # w , * N *� TKN mg/kg Z ; o oa o �• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/17 18000 1.91 0.205 Yancy WWTP D <.5" S 0.5 1 0.3 64700 4090 19800 16.396 NA Fescue 10/18 63000 1.91 0.717 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 57.386 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4-0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 81000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 737782 0.000 Lime App lied Annuallbs/acre 0.024 39.462 0.745 0.083 0.123 0.003 0.015 0.062 0.034 1.728 37.618 Date lbs/ac Prior Years Cumulative lbs/ac 0.08 0.021 4.546 0.498 0.917 0.005 0.067 0.364 0.101 10.036 Current Cumulative lbs/ac 0.104 39.483 5.291 0.581 1.040 0.008 0.082 0.426 0.135 11.764 Permitted C. P. L. R.****1 36 1 34 1 1338 1 1 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 141 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/1/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Bonnie Crispin Operator: Jon Crispin Crop 1 Name: Fescue -Pasture WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 7.89 Site #: Predominant Soil Series: FbB2 Crop 1 Max. PAN: 141 Crop 2 Name: Acres Utilized: CS82 Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 8.5 8.5 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu_ Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o oa o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10/13 49500 1.91 0.464 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 37.132 NA Fescue 10/17 49500 1.91 0.464 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 37.132 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 4-0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 99000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 74,2647 0.000 Lime Applied Annuallbs/acre 0.024 39.718 0.750 0.084 0.124 0.003 0.015 0.063 0.034 1.739 37.862 Date lbs/ac Prior Years Cumulative lbs/ac 0.131 0.009 1.274 0.253 0.274 0.002 0.044 0.158 0.09 2.719 Current Cumulative lbs/ac 0.155 39.727 2.024 0.337 0.398 0.005 0.059 0.221 0.124 4.458 Permitted C. P. L. R.**** 1 36 34 1 1338 1 267 1 15 1 1 374 1 89 1 2498 Permit PAN Limit lst/2nd Crop 141 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/1/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Land Owner: ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Yanceyville Bonnie Crispin Operator: Jon Crispin Crop 1 Name: Fescue -Hay WQ Permit #: WQ0028547 Field #: Annual Dry Tons Applied: 18.04 Site #: Predominant Soil Series: FbB2 Crop 1 Max. PAN: 188 Crop 2 Name: 4 CS82 Acres Utilized: Acres Permitted: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 10.9 10.9 0 o � N Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per pp p Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (may' Wet, Moist) Precip. Past 24 Ms. inches a �a F w *o• o ,•d �, # w •, * N *� TKN mg/kg Z ; o oa o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 9/28 19500 1.91 0.142 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 11.407 NA Fescue 10/10 90000 1.91 0.658 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 52.648 NA Fescue 10/11 67500 1.91 0.493 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 39.486 NA Fescue 10/12 49500 1.91 0.362 Yancy WWTP D <.5" S 0.5 0.3 64700 4090 19800 28.956 NA Fescue 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0 0 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 0.000 0.000 TOTALS: 01 226500 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 132.497 0.000 Lime Applied Annuallbs/acre 0.044 70.834 1.337 0.149 0.221 0.005 0.026 0.112 0.061 3.101 67.524 Date lbs/ac Prior Years Cumulative lbs/ac 0.182 0.029 5.477 0.614 1.01 0.007 0.097 0.439 0.19 10.952 Current Cumulative lbs/ac 0.226 70.863 6.814 0.763 1.231 0.012 0.123 0.551 0.251 14.053 Permitted C. P. L. R.**** 36 34 1 1338 1 267 1 15 374 1 89 2498 Permit PAN Limit lst/2nd Crop i F 188 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation 2/1/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Non -dedicated Residuals Programs Final Audit Report 2024-05-10 Created: 2024-05-08 By: Brent Collins(brent.collins@emaresourcesinc.com) Status: Signed Transaction ID: CBJCHBCAABAApJymWxONxgBDE6fQ2jglYdvmnuiaXGf7 "Non -dedicated Residuals Programs" History Document created by Brent Collins(brent.collins@emaresourcesinc.com) 2024-05-08 - 2:03:10 PM GMT C'. Document emailed to Kamara Barnett (townmanager@yanceyvillenc.gov) for signature 2024-05-08 - 2:03:31 PM GMT Email viewed by Kamara Barnett (townmanager@yanceyviIlenc.gov) 2024-05-10 - 1:20:39 PM GMT 6© Document e-signed by Kamara Barnett (townmanager@yanceyvillenc.gov) Signature Date: 2024-05-10 - 1:22:23 PM GMT - Time Source: server Agreement completed. 2024-05-10 - 1:22:23 PM GMT 0 Adobe Acrobat Sign