NCS000173 DMR SW **Not on DMR Form

I
ANALYTICAL & CONSULTING
CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Catlin Engineers & Scientists Date of Report: Apr 03, 2014
Post Office Box 10279 Customer PO #: 140317-1
Wilmington NC 28404-0279 Report #: 2014-03094
Attention: Dimitri Talbert Report to: Dimitri Talbert
Project ID: NCSPA
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-07524 Site: 103 3/16/2014 7:30 PM Water Dimitri Talbert
Test Method Results Date Analyzed
Lead EPA 200.8 < 0.010 mg/L 3/20/2014
Residue Suspended (TSS) SM2540D 10.5 mg/L 03/18/2014
BOD SM 6210 B 10 mg/L 03/17/2014
COD SM 5220D 49 mg/L 03/1812014
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-07525 Site: 206 3/16/2014 7:00 PM Water Dimitri Talbert
Test Method Results Date Analyzed
Oil & Grease (O&G)
EPA 1664
<5 mg/L
03/31/2014
Lead
EPA 200.8
<0.010 mg/L
03/21/2014
Residue Suspended (TSS)
SM 25400
100 mg/L
03/18/2014
BOD
SM 5210 B
23 mg/L
03/17/2014
COD
SM 52261)
47 mg/L
03/18/2014
Lab ID Sample ID:
Collect Daterrime Matrix Sampled by
14-07526 Site: 606
3/16/2014 6:30 PM Water Dimitri Talbert
Test Method Results Date Analyzed
Oil & Grease (O&G)
EPA 1664
<5 mg/L
03/28/2014
Lead
EPA 200.7
<0.010 mg/L
03/24/2014
Residue Suspended (TSS)
SM 2640 D
<2.8 mg/L
03/18/2014
BOD
SM 5210 B
6 mg/L
03/17/2014
COD
SM 5220D
<20mg/L
03/18/2014
Report S:: 2014-03084 Page 1 of 3

' Environmental Chemists, Inc.
envirochem6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
v ® 710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DIS CERTIFICATE #37729
Catlin Engineers & Scientists
Post Office Box 10279
Wilmington NC 28404-0279
Attention: Dimitri Talbert
Date of Report:
Apr 03, 2014
Customer PO #:
140317-1
Report #:
2014-03094
Report to:
Dimitri Talbert
Project ID: NCSPA
3/16/2014 6:10 PM
Lab ID
Sample 1D:
Results Date Analyzed
Collect Date/Time
Matrix Sampled by
Oil & Grease (O&G)
14-07527
Site: 1001
03/28/2014
3/16/2014 6:10 PM
Water Dimitri Talbert
< 0.010 mg/L
Test
Residue Suspended (TSS)
Method
46.2 mg/L
Results Date Analyzed
Lead
SM 5210 B
EPA 200.8
03/17/2014
< 0.010 mg/L
3/21/2014
Residue Suspended
(TSS)
SM 2540 D
Collect Daterrime
9.2 mg/L
03/18/2014
BOD
3/16/2014 5:20 PM
SM 5210 B
<2 mg/L
03/17/2014
COD
SM 5220D
22 mg/L
03/18/2014
Lab ID
Sample ID:
Collect DatelTime
Matrix Sampled by
14-07528
Site: 1304
3/16/2014 5:45 PM
Water Dimitri Talbert
Test
Method
Results Date Analyzed
03/18/2014
>76 mg/L
Oil & Grease (O&G)
EPA 1664
<5 mg/L
03/28/2014
Lead
EPA 200.8
< 0.010 mg/L
3/21/2014
Residue Suspended (TSS)
SM 2540 D
46.2 mg/L
03/18/2014
BOD
SM 5210 B
<2 mg/L
03/17/2014
COD
SM 6220D
<20 mg/L
03/18/2014
Lab ID Sample ID:
Collect Daterrime
Matrix Sampled by
14-07529 Site: 1704
3/16/2014 5:20 PM
Water Dimitri Talbert
Test Method Results Date Analyzed
Lead EPA 200.8
Residue Suspended (TSS) SM 2540 D
BOD SM 5210 B
All QC requirements for DO depletion not met.
< 0.010 mg/L
3/21/2014
26.3 mg/L
03/18/2014
>76 mg/L
03/17/2014
COD SM 5220D 245 mg/L 03/18/2014
Reportt: 2014-03094 Page 2 of 3

LL envirochem
ANALYTICAL & CONSULTING
CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way • Wilmington, NC 28405
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Catlin Engineers & Scientists
Date of Report: Apr 03, 2014
Post Office Box 10279
Customer PO #: 140317-1
Wilmington NC 28404-0279
Report #: 2014-03094
Attention: Dimitri Talbert
Report to: Dimitri Talbert
Project ID: NCSPA
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-07530 Site: 2011
3/16/2014 5:00 PM Water Dimitri Talbert
Test
Method
Results Date Analyzed
Lead
EPA 200.8
0.013 mg/L
3/21/2014
Residue Suspended (TSS)
SM 2540 D
47.1 mg/L
03/18/2014
BOD
SM 5210 B
3 mg/L
03/17/2014
All QC requirements for DO depletion
not met. Result estimated.
COD
SM 5220D
<20 mg/L
03/18/2014
Lab ID Sample ID:
Collect Daterrime Matrix Sampled by
14-07531 Site: 2006
3/16/2014 4:30 PM Water Dimitri Talbert
Test
Method
Results Date Analyzed
Oil & Grease (O&G)
EPA 1664
<5 mg/L
03/24/2014
Lead
EPA 200.8
0.014 mg/L
3/21/2014
Residue Suspended (TSS)
SM 2540 D
91.4 mg/L
03/18/2014
BOD
SM 5210 B
9 mg/L
03/17/2014
COD
SM 5220D
29 mg/L
03/18/2014
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
14-07532 Site: 2501
3/16/2014 4:00 PM Water Dimitri Talbert
Test
Method
Results Date Analyzed
Lead
EPA 200.8
< 0.010 mg/L
3/21/2014
Residue Suspended (TSS)
SM 2540 D
24.0 mg/L
03/1812014
BOD
SM 5210 B
<2 mg/L
03/17/2014
All QC requirements for DO depletion
not met. Result estimated.
COD
SM 5220D
24 mg/L
03/18/2014
Comment:
Reviewed
Report #:: 2014-03094 Page 3 of 3

Environmental Chemists, Inc.
Tr 6602 Windmill Way • Wilmington, NC 28405
LL envirochem(910) 392-0223 (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
[phone]
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Catlin Engineers & Scientists Date of Report: Mar 26, 2014
Post Office Box 10279 Customer PO #: 140317-3
Wilmington NC 28404-0279 Report #: 2014-03105
Attention: Dimitri Talbert Report to: Dimitri Talbert
Project ID: NCSPA Wilmington
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
14-07559 Site: Vopak N 3/17/2014 10:00 AM Water Dimitri Talbert
Test Method Results Date Analyzed
Lead EPA 200.8 < 0.010 mg/L 3/21/2014
Residue Suspended (TSS) SM 2540 D 7.3 mg/L 03/18/2014
BOD SM 5210 B 2 mg/L 03/19/2014
COD SM 5220D <20 mg/L 03/18/2014
Lab ID Sample ID: Collect DatelTime Matrix Sampled by
14-07560 Site: Vopak S 3/17/2014 10:15 AM Water Dimitri Talbert
Test
Method
Results
Date Analyzed
Lead
EPA 200.8
0.012 mg/L
3/21/2014
Residue Suspended (TSS)
SM 2540 D
4.4 mg/L
03/18/2014
BOD
SM 5210 B
<2 mg/L
03/19/2014
COD
SM 5220D
<20 mg/L
03/18/2014
Comment:
f
Reviewed by: IYi,QA>vo
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Report#.: 2014-03105 Page 1 of 1