WQ0004268_GW Monitoring_20121218

ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:.
L ID NUMBER (from Permit): MW-1 Date sample collected: 11/5112
Depth: ft. Well Diameter: in.
h to Water Level: 18.9 ft. below measuring point Screened Interval: _ft. to —ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
)lea for metals were collected unfiltered: DYES ❑ NO and field acidified• i1 Ycs f-1 un
?RMIT Number: Expiration Date: July 31, 2015
m-Discharge WQ0004268 UIC
DOES Other
(PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery© Spray Field _ ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source. Heat Pump ❑ Other:
FIELD ANALYSES:
pH 4.30 units
Spec. Cond.
Odor
Appearance
Temp. 18 oC DRY at
µMhos I time of
r sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
128 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3).as N
3.85 mgA
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN meNed forhighly turbid samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
416 mgll
At --Aluminum
mgA
pH (when analyzed)
units
Be - Barium
mgA
TOC
5.42 mg/I
Ca - Calcium
mg/l
Chloride
194 mg/I
Cd- Cadmium
mg/I
'
Arsenic
mgll
�� p Chromium: Total
Grease and Oils
mgll
/V^E(��Fi�000
a '%f'�^Aa't�ron
mg/I
.ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
q p/
JAN
mg/1
(Specify test and method C ATTACH LAB REPORT.)
Sulfate
100 mg/I
® 4 2$43Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
725 µMltab_- ijon p K -Potassium
'mgA
VOC ,method #
Total Ammonia
mgA
1) ry6Ba 9ddnetsium
mgll
#
(Fmmonla Nitrogen: NH3es N: A only Nitrogen. Total)
Mn - Manganese
mgA
,method
, method #
TKN as N
mg/1
Ni - Nickel
mg/I
method #
­ 1 ^11 �1­ 11 vya 11, �.ey t^L YY11 �4W nePorr J: anment l otal vacs: P mg/L thluent Total VOCs: _ mq/L VOC Removal%
Robert Caldwell, Assistant Plant Manager
Permittee (or Authorized Apent) Name and Title- Please print or type
GW-59 Rev. 112007

n�narn e� asuviareq�lgggYilJ9:i.ILLY
DWATER QUALITY MONITORING:
ANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:.
L ID NUMBER (from Permit): MW-2 Dale sample collected: 11/5/12
Depth: ft. Well Diameter: in.
h to Water Level: 5.10 ft. below measuring point Screened Interval: ft. to ft.
curing Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
:RMIT Number:
Expiration Date: July 31. 2015
on -Discharge W00004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 5.01 units Temp. 16 eC
Spec. Cond. µMhos
Odor
Appearance
WELL
t sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD
124 mg/l
Nitrite (NO2) as N
mgA
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
0.547 mg/I
Zn - Zinc - mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mgll
(Note: Use MPN method for highly turWd samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
188 mg/l
AI - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOC
4.15 mg/I
Ca - Calcium
mg/I
Chloride
132 mg/1
Cd- Cadmium'
mgA
'
Arsenic
mg/l
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mgA
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
16 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
354 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mgA
Mg - Magnesium
mgA
, method #
(Ammonla Nitrogen: NH3 as Nl Ammonia Nitrogen, Total)
Mn- Manganese
mgA
,method#
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
"r Kemediation systems only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Assistant Plant Manager �it'L-W&AI I
Permittee (or Authorized Anent) Name and Title - Please Print or type Signature of Pennittee (or Authorized Agent)
GW-59 Rev. 112007
at
of
J
t:

, .A ows,1111 tgW-1C iW,
1.
-R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y "'"" NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:,
L ID NUMBER (from Permit): MW-3 Date sample collected: 11/5/12
Depth: ft. Well Diameter. in.
h to Water Level: 1.10 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
)lea for metals were collected unfiltered: DYES ❑ NO and field acidified- fl YFs fl mr)
eRM1T Number: Expiration Date: July 31, 2015
)n-Discharge WQ0004268 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑Other:
FIELD ANALYSES:
pH 5.71 units Temp. 18 oC
Spec. Cond. µMhos
Odor
Appearance
: sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
186 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mgA
Coiiform: MF Feral
1100mi
Nitrate (NO3) as N
0.542 mgA
Zn - Zinc mg/I ,
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN melted for Nghly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
352 mgn
Al - Aluminum
mg/l
pH (when analyzed)
units
Be - Barium
mg/l
TOC
2.02 mg/I
Ca - Calcium
mgA
Chloride
159 mgll
Cd - Cadmium
mg/I
Arsenic
mgll
Chromium: Total
mg/I
Grease and Oils
mgA
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method M ATTACH LAB REPORT.)
Sulfate
64 mg/I
Hg - Mercury _
mgll
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
319 µMhos
_
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/1
Mg - Magnesium
mg/1
#
(Ammonle Nitrogen; NHsas N;Ammonia Niuogan. Total)
Mn- Manganese
mg/l
,method
,method#
TKN as N
mgll
Ni - Nickel
mgA
, method #
VVI a„r�yaseura Willy ingaun Sao neporrsi: mrment total VUUs: mg/L Effluent Total VOCs: mq/L VOC Removal%
Robert Caldwell, Assistant Plant Manager We
���/(� /yr/ gI/z-
Permlttee (or Authorized Apent) Name and Title- Please print or type sipnalure o Permlltee (or Authorized Apent) (Date)
GW-59 Rev. 112007
at
of

ON
r . EPARTMENTOFENVFROMdENTa`NATURALREBOURCCS x
GROUNDWATER QUALITY MONITORING: AASION OFWATER QUALITYJNFORMATION PROCESSINGUNIT
COMPLIANCE REPORT FORM ati iaahi=aFw nra rcu co aril tiro'
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
Y "''`"" NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 13 I
If P 'll
PLING INFORMATION
L ID NUMBER (from Permit): MW-4 Date sample collected: 11/5/12
Depth: ft. Well Diameter: in.
1 to Water Level: 7.20 ft. below measuring point Screened Interval: ft. to ft.
iuring Point Is ft. above land surface Relative M.P. Elevation: ft.
The of water pumped/bailed before sampling: 10+ gallons
:RMIT Number:.
Expiration Date: July 31, 2015
m-Discharge WQ0004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remedlation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 4.01 units
Spec. Cord.
Odor
Appearance
Temp. 19 eC DRY at
time of
--
Date sample analyzed:
Laboratory Name: Microbial; Laboratories
Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD
160 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
5.66 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mgA
(Note: Use Wit method for highly hrtid samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
40.0 mgA
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba- Barium
mg/I
' TOC
1.39 mg/I
Ca - Calcium
moll
Chloride
64.4 mg/I
Cd - Cadmium
mg/I
Arsenic
mgA
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
12 mg/I -
Hg- Mercury
mgA
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
176 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg —Magnesium
mg/I
#
(Ammanha Nitrogen; NHsas 14; Ammonia NlVogon, Total)
Mn - Man
Manganese
9
mgA
,method
method #
TKN as N
mg/I
Ni - Nickel
mg/1
, method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L_. Effluent Total VOCs: moll VOC Removal
Robert Caldwell, Assistant Plant Manager „�„p �allt„r
Permetee (or Authorized Agent) Name and Tille- Please print or type Signature of Per0lttae (or Authorized Agent) (Date)
GW-59 Rev. 112007

DWATER QUALITY MONITORING:
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
IY NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site.Name: No. of wells to be sampled: 13
PERMIT Number: Expiration Date: ..July 31, 2015
Non -Discharge WQ0004268 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remedlation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other: _
L ID NUMBER (from Permit): R-1 Date sample collected: 11/5/12
Depth: ft. Well Diameter: in.
n to Water Level: 2.20 ft. below measuring point Screened Interval: ft. to ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
the of water pumpediballed before sampling: 10+ gallons
FIELD ANALYSES:
pH 4.22 units
Spec. Cond.
Odor
Appearance
Temp. 19 eC DRY at
time of
t sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
368 mg/I
Nitrite (NO2) as N
mgn
Pb - Lead mg/I '
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
0.603 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mgll
(Note: Use MPN method for highly tursid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
256 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
8.05 mgn
Ca - Calcium
mg/I
Chloride
195 mgn
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu- Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
16mg/l
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
451 µMhos
K - Potassium
mg/I
VOC , method #
TotalAmmonia
mg/I
Mg - Magnesium
mg/I,
method#
(Anim als Nitrogen: NH3 as N: Ammonia Nitrogen, rolel)
Mn - Manganese
mg/I
method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
t-or Kemeblatlon systems Only (Attach Lab Reports): Influent Total VOCs; mg/L Effluent Total. VOCs: mg/L VOC Removal%
Robert Caldwell, Assistant Plant Manager[ry ��ldre� y q/ ff
Permitlee (or Authorized Agent) Name and Title - Please print or type SlAnatura of Pprmlttee (or AUNorized Agent) ate)
GW-59 Rev. 1/2007

FlV3fulr�i�J:/PA
ROUNDWATER QUALITY MONITORING:
DMPLIANCE REPORT FORM
Name: Aliens, Inc. -
Name (if different): _
Address: 5900 TurkeV
28393-9703 County
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No, of wells to be sampled: 13
:RMIT Number:
Expiration Date: July 31, 2015
m-Discharge WQ0004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
L ID NUMBER (from Permit): R-2a Date sample collected: 11/5/12 FIELD ANALYSES:
Depth: ft. Well Diameter: — in. pH 4.03 units Temp. 20 eC
h to Water Level: 3.70 ft. below measuring point Screened Interval: _ft. to _ft. Spec. Cord. µMhos
;wring Point is ft. above land surface Relative M.P. Elevation: ft. Odor
lie of water pumpedibailed before sampling: 10+ gallons Appearance
a sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
<10 mg/I
Nitrite (NO2) as N
mgA
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
1.13 mg/I
Zn - Zinc mg/I
Coliform: MF Total
1100ml
Phosphorus: Total as P
mgll
(Nola: Use MPN method for highly lursid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
68 mgll
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
1.45 mgli
Ca - Calcium
mg/I
Chloride
71.7 mg/I
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/1
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and. method #. ATTACH LAB REPORT.)
Sulfate
22 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
110 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
#
(AmmoNe Nitrogen; NHsas N; Ammonia Nitrogen, Totel)
Mn - Manganese
mg/l
,method
, method #
TKN as N
mgA
Ni -,Nickel
mg/l
, method #
ror murneutauon aysiems unity tAttacn Lao Reports): Influent Total VOCs:. mg/L . _ Effluent Total VOCs: mq/L VOC Removal%
Robert Caldwell, Assistant Plant Manager
Pen iree (or Authorized Agenq Name and Title - Please print or type
GW-59 Rev. 1/2007
at
of

UN UNLY
TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 6900 Turkey Highway
y """" NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
L ID NUMBER (from Permit): R-3 Date sample collected: 1115/12
Depth: ft. Well Diameter: in.
h to Water Level: 4.70 ft. below measuring point Screened Interval: ft. to _
curing Point is ft. above land surface Relative M.P. Elevation: ft.
Tie of water pumped/bailed before sampling: 10+ gallons
IRMIT Number: Expiration Date: July 31. 2015
n-Discharge WQ0004268 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedialion: Infiltration Gallery
© Spray Field ❑ Remedialion:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES: WAS
pH 3.76 units Temp. 16 eC DRY at
ft. Spec. Cond. µMhos time of
Odor sampling,
check
Appearance here: ❑
) sample analyzed:
Laboratory Name: Mlcrobac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD
137 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
1.05 mg/I
Zn - Zinc mg/l
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN meMod br tighly turbid
samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
236 mg/1
At - Aluminum
mg/l
pH (when analyzed)
units
Ba - Barium
mg/I
TOG
0.996 mg/I
Ca - Calcium
mg/I
Chloride
171 mg/I
Cd - Cadmium
mg/I
Arsenic
ni
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method C ATTACH LAB REPORT.)
Sulfate
31 ni
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
460 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; Wads N; Ammanla Nitrogen, Tolol)
Mn -Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
i-or Kemedtation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Assistant Plant Manager '(, UU'dwJ /z// g
Permittee (or Authorized Agent) Name and Title- Please print or type Signature of Permiltee (or Authorized Agent) (Date)
GW-59 Rev. 1/2007

rmrera uNLr
DWATER QUALITY MONITORING:
ANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
:Y NC 28393-9703 County Sampson
act Person: Robert Caldwell
Location/Site Name:
L ID NUMBER (from Permit): R-4
Depth: ft.
h to Water Level: 5.10 ft. below measuring point
wring Point is ft. above land surface
Tie of water pumped/bailed before sampling: 10+
Telephone#: [phone]
No. of wells to be sampled: 13
PERMIT Number:
Expiration Date: July 31. 2015
Non -Discharge WQ0004268
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
Date sample collected: 11/5/12
Well Diameter: in.
Screened Interval: _fit. to ft.
Relative M.P. Elevation: ft.
FIELD ANALYSES:
pH 3.87 units
Spec. Cond.
Odor
Appearance
t sample analyzed: Laboratory Name: Microbac Laboratories
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 102 mg/I Nitrite (NO2) as N mg/I Pb - Lead
Coliform: MF Fecal /i 0oml Nitrate (NO3) as N 2.55 mg/I Zn - Zinc
Coliform: MF Total 1100ml Phosphorus: Total as P mg/l
(Note: Use MPN method for hl hl lureid sam les)
Temp. 20 eC DRY at
µMhos time of
Certification No. NC#11 NC#37714
mg/I
mg/I
y Is
Orthophosphate
mgA Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
218 mgA
Al - Aluminum
mgA
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
1.30 mg/I
Ca - Calcium
mg/I
Chloride
154 mg/I
Cd - Cadmium
mgA
Arsenic
mg/I
Chromium: Total
mgA
Grease and Oils
mgA
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
16 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
433 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(AMMMO Reagan: NHras N: Ammonia
Nitrogen, Total)
Mn -Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mgA
, method #
I -or Kemetnation Systems only (Attach Lab Reports): Influent Total VOCs: mg/L . Effluent Total VOCs: mg/L VOC Removal
Robert Caldwell, Assistant Plant Manager (&':Irwin 1Z11Q /1 Z
Permiltee (or Authorized Agent) Name and Tnle- Please print or type Signature of Pennidee (or Authorized Agent) (Dale)
GW-59 Rev. 112007
01

QUALITY MONITORING:
PORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
Y NC 28393-9703 county Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
Number: Expiration Date:
;harge WQ0004268 UIC_
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedialion: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
LL ID NUMBER (from Permit): R-5a
Date sample collected: 11/5112
FIELD ANALYSES:
WAS 11
I Depth: ft.
Well Diameter: _In.
pH 4.02 units Temp. 20 eC
DRY at
th to Water Level: 3.30 ft. below measuring point
Screened Interval:
to
Spec. Cond. µMhos
time of
lsuring Point is ft. above land surface
_ft.
Relative M.P. Elevation:
_ft.
ft.
Odor
sampling,
tme of water pumped/bailed before sampling:
10+ gallons I
Appearance
check
here:
1 Ies for metals were collected unfiltered: ❑YES
(ORATORY INFORMATION
❑ NO and field acidified: ❑ YES
❑ NO
❑
sample analyzed:
Laboratory Name: Microbac
Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 193 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
4,78mgll
Zn - Zinc mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 124 mg/I
AI - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mg/I
TOC 2.18 mg/l
Ca - Calcium
mg/I
Chloride 62.2 mg/I
Cd - Cadmium
mgA
Arsenic mgA
Chromium: Total
mg/I
Grease and Oils mgA
Cu - Copper
mg/I
ORGANICS:.(by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.).
Sulfate 30 mg/I
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance 204 µMhos
K- Potassium
mg/l
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
#
(Ammonia Nitrogen; NH,.. N; Ammonia Nimagen, Total)
Mn - Manganese
mgA
,method
, method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
• �• ••� ••�•• ••• _• �r�•=•••� ----I tav neµuns); mnuent loyal VUUS: 11191L Effluent Total VOCs: ma/L VOC Removal %
Robert Caldwell, Assistant Plant Manager ,, ,14-d d 17119h,
Permittee (or Authorized Anent) Name and Title- Please print or type Signature of Pefmlttee (or Authorized Agent) (Date)
GW-59 Rev. 112007

TER QUALITY MONITORING:
E REPORT FORM
ity Name: Aliens, Inc. - Turkey
lit Name (if different):
ity Address: 5900 Turkey Highway
key NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 13
L ID NUMBER (from Permit): R-7
Depth: ft.
h to Water Level: 3.00 ft. below measuring point
luring Point is ft. above land surface
The of water pumped/bailed before sampling:
10+
Date sample collected: 11/5112
Well Diameter: in.
Screened Interval: _ft. to _ft.
Relative M.P. Elevation: ft.
?RMIT Number: Expiration Date: July 31, 2015
m-Discharge WQ0004268 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH 4.61 units
Spec. Cond.
Odor
Appearance
Temp. 19 oC DRY at
µMhos time of
it sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
146 mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
0.533 Ill
Zn - Zinc mg/I
Coliform: MF Total
/100m1
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly tumid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
112 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba- Barium
mg/I.
TOC
9.94 mg/I
Ca - Calcium
mg/I
Chloride
119mg/I
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/l.
Grease and Oils
mg/I
Cu - Copper
mg/I .
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron -
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
17 mgll
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
211 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/l
Mg - Magnesium
mg/I
#
(Ammone Nitrogen; NHsas N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
,method
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
..ya.c,,,a Willy t..ew6r1 a_no tcupurcal: imluem total VL)cs: mg/L. Effluent Total.VOCs: _ me/L VOC Removal%
Robert Caldwell, Assistant Plant Manager of Permth� I 1 u'd
Permlhee (or Authorized Agent) N.M. and Title- Please print or type Signature ee (or Authorized Agent) (Date)
GW-59 Rev. 1/2007

QUON11l
DWATER QUALITY MONITORING:
ANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
tY NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No, of wells to be sampled: 13
PERMIT Number:
Expiration Date: July 31, 2015
Non -Discharge WQ0004268
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
L ID NUMBER (from Permit): R-8 Dale sample collected: 11/5/12
Depth: ft. Well Diameter: in.
i to Water Level: 4.10 ft. below measuring point Screened Interval: ft. to ft.
.uring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+gallons
)les for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO
FIELD ANALYSES:
pH. 4.01 units
Spec. Cond.
Odor
Appearance
Temp. 20 aC DRY at
µMhos time ..
a sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
113 mgn
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
i 9.59 mg/I
Zn -Zinc mg/I
Coliform: MF Total
1100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN met for highly tureld samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
144 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/1
TOC
1.27 mgn
Ca - Calcium
mg/I
Chloride
55.3 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mgn
Cu - Copper ,
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/1
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
45 mgn
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
246 µMhos
K - Potassium
mgn
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Ammonla Nitrogen: NHsas N; Amon
Ammonia Nitrogen. Total)
Mn -Manganese
mg/I
,method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
GW-59 Rev. 1/2007
in

TER QUALITY MONITORING:
E REPORT FORM
' `Z"w" ' '^�""71
PERMIT Number:
Expiration Date: July 31, 2015
Facility Name: Allens, Inc. - Turkey
Non -Discharge WQ0004268
NPDES
UIC
Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION
❑ Lagoon
BEING MONITORED
❑ Remediation: Infiltration Gallery
Turkey "'"'"" NC 28393-9703 County Sampson
_.iz
© Spray Field
❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor
❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled: 13
❑ Water Source Heat Pump
❑ Other.
Imm Per,nl
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit); R-9
Date sample collected: 11/5/12
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in.
pH 4.06 units Temp. 22 aC
DRY at
Depth to Water Level: 4.11 ft. below measuring point Screened Interval: ft. to
ft. Spec. Cord.
µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
Samples for metals were collected unfiltered: DYES
❑ NO and fielN aririifirri• fl VFC 71 mn
a sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
324 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
5.51 mg/I
Zn -Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for Nghly turloid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
236 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
,Be - Barium
mg/I
TOC
0.868mg/I
Ca - Calcium
mg/I
Chloride
57.4 mg/I
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HP.LC)
Phenol
mg/I
. Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
52 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
232 µMhos
K - Potassium
mg/I
VOc , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
#
(Ammonla Nitrogen; N%as N; Ammonia NiVagen, Total)
Mn- Manganese
mgll
,method
,method#
TKN as N
mg/I
Ni - Nickel
mg/I
method #
GW-59 Rev. 112007

Aliens, Inc
Mr. R--id Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
MW#1
1211053-01
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analytc Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
194
mg/L
I1/6/12
14:20
JR
EPA300.0 A]2,S1,E
COD, Total
128
mg/L
I1/6/12
9:00
DSK
SM 20th Ed. 5220 D
Conductivity
725
umhos/cm
I1/6/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
18.9
feet
11/5/12
8:35
DSD
Field Measurement
Nitrate as N
3.85
mg/L
11/6112
14:20
JR
EPA 300.0
PH, Field Test
4.30
pH Units
11/5112
8:35
DSD
Field
Total Dissolved Solids
416
mg/L
11/6/12
9:45
JAO
SM 20th Ed. 2540 C
Sulfate as SO4
100
. mg/L
1116112
14:20
JR
EPA 300.0 A 12
Temperature
18
°C
I115/12
8:35
DSD
Field
Analyzed by: Miaobac taboatmr , Inc -Ohio Valley
Total Organic Carbon
5.42
mg/L
11/9/12 21:21
DTH
E415.1
Slate Ccnificulions:
Respcclful ly Submitted
NCDNR III
NCDOH 1137714Laz=Lem-
USDA 93787
(/
Jeanne Overstreet. Project Manager
Page 1 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
MW #2
1211053-02
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
AnaMed by: Microbac - FayetteAie Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4..
Temperature
132
mg/L
11/6/12 15:43
JR
EPA300.0
124
mg/L
11/6/12 9:00
DSK
SM 20th Ed. 5220 D
354
umhos/cm
11/6/12 9:30
DSK
SM 20th Ed. 2510 B
5.10
feet
I1/5/12 8:20
DSD
Field Measurement
0.547
mg/L
11/6/12 15:43
JR
EPA300.0
5.01
pH Units
11/5/12 8:20
DSD
Field
188
mg/L
11/6/12 9:45
JAO
SM 20th Ed. 2540 C
16
mg/L.
11/6/12 15:43
JR
EPA 300.0
16
°C
11/5/12 8:20
DSD
Field
Analyzed by: Microbac laboratories, Inc - Ohio Valley
Total Organic Carbon 4.15
Slate Cenificallons:
NCDNR III
NCDOH t137714
USDA #3787
mg/L 11/9/12 21:37 DTH E415.1
Respectfully Submittte�d.
-e22�cr_ C/uriLaZril+ -�
Jeanne Overstreet. Project Manager
19
Page 2 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.19240 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples -3fYearly
MW #3
1211053-03
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4..
Temperature
159
mg/L
11/6/12 16:15
JR
EPA300.0
186
mg/L
11/6/12 9:00
DSK
SM 20th Ed. 5220 D
319
umhos/cm
11/6/12 9:30
DSK
SM 20th Ed. 2510 B
1.10
feet
1115/12 9:00
DSD
Field Measurement
0.542
mg/L
I1/6/12 16:15
JR
EPA300.0
5.71
pH Units
11/5/12 9:00
DSD
Field
352
mgfL
11/6112 9:45
JAO
SM 20th Ed. 2540 C
64
mg/L
11/6/12 16:15
IR
EPA 300.0-
18
°C
I1/5/12 9:00
DSD
Field
Analyzed by: Mivobac laboratories, Inc - Ohio Valley
Total Organic Carbon 2.02
Slate Ccrtilicalions:
NCDNR fl I I
NCDOH 937714
USDA 93787
mg/L I1/9/12 21:51 DiH E415.1
Respectfully Submitted
Joann Overstreet, Project Manager
M
Page 3 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
MW #4
1211053-04
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4 .
Temperature
64.4
mg/L
I1/6/12 16:17
JR
EPA 300.0
160
mg/L
11/6112 9:00
DSK
SM 20th Ed. 5220 D
176
umhos/cm
11/6/12 9:30
DSK
SM 20th Ed. 2510 B
7.20
feet
11/5/12 9:20
DSD
Field Measurement
5.66
mg/L
11/6/12 16:17
JR
EPA300.0
4.01
pH Units
11/5/12 9:20
DSD
Field
40.0
mg/L
11/6/12 9:45
- JAO
SM 20th Ed. 2540 C
12
mg/L
I1/6/12 16:17
JR
EPA300.0
19
°C
I1/5/12 9:20
DSD
Field
Analyred by: Mivobac Laboratories, Inc. - Ohio Valley
Total Organic Carbon 1.39
Slate Certifications:
NCDNR //11
NCDOH #37714
USDA #3787
mg/L 11/9/12 22:04 DiH E415.1
Respectfully Submitted
�.f4/GF� C/G�bL6�iU�
Jeanne Overstreet, Project Manager
0
Page 4 of 13

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Miuobac- Fayetterrlle Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4..
Temperature
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
R-1
1211053-10
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
195
mg/L
11/7/12
8:45
JLR
EPA300.0
368
mg/L
11/6112
9:00
DSK
SM 20th Ed. 5220 D
451
umhos/cm
I116/12
9:30
DSK
SM 20th Ed. 2510 B
2.20
feet
11/5/12
11:25
DSD
Field Measurement
0.603
mg/L
11/7/12
8:45
JLR
EPA300.0
4.22
pH Units
11/5/12
11:25
DSD
Field
256
mg/L
11/6/12
9:45
JAO
SM 20th Ed. 2540 C
16
mg/L
1117/12
8:45
JLR
EPA 300.0
19
°C
I1/5112
11:25
DSD
Field
Analyzed by: Miuobac laboratories, Inc. - Ohio Valley
Total Organic Carbon 8.05
State Certifications:
NCDNR III
NCDOH i137714
USDA #3787
mg/L 11/10/12 0:25 DiH E415.1
Respectfully Submitted
Jeanne Overstreet. Project Manager
Page 10 of 13

Allot, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
W
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/%Vells samples - 3/Yearly
R-2a
1211053-II
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac- Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO
Temperature
71.7
mg/L
I1/7/12
9:02
JLR
EPA30D.0
<I0.0
mg/L
11/12/i2
13:55
DSK
SM 20th Ed. 5220 D
110
umhos/cm
11/6/12
9:30
DSK
SM 20th Ed. 2510 B
3.70
feet
11/5/12
I1:10
DSD
Field Measurement
1.13
mg/L
ll/7/12
9:02
JLR
EPA300.0
4.03
pH Units
11/5112
11:10
DSD
Field
68.0
mg/L
11/6/12
9:45
JAO
SM 20th Ed. 2540 C
22 _
mg/L
I1/7/12
9:02
JLR
EPA300.0
20
°C
11/5/12
11:10
DSD
Field
Analyzed try_ Microbac Laboratories, Inc - Ohio valley
Total Organic Carbon 1.45
State Ceni6cations:
NCDNR AN
NCDOH 037714
USDA 93787
mg/L 11/10/12 0:39 DiH E415.1
Respectfully Submitted
-Ea.I<x� C/tv Lb�iea�
Jeanne Owmireet, Project Manager
Page 11 of 13

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples -3/Yearty
R-3
1211053-12
Date Reported: November 20, 2012,
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Miuobac- Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4,.,.
Temperature
171
mg/L
11/7/12
9:18
JLR
EPA 300.0
137
mg/L
1116/12
9:00
DSK
SM 20th Ed. 5220 D
460
umhos/cm
11/6/12
9:30
DSK
SM 20th Ed. 2510 B
4.70
feet
I1/5/12
10:30
DSD
Field Measurement
1.05
mg/L
I117/12
9:18
JLR
EPA 300.0
3.76
pH Units
11/5/12
10:30
DSD
Field
236
mg/L
11/6/12
9:45
JAO
SM 20th Ed. 2540 C
31
mg/L
I1/7/12
9:18
JLR
EPA 300.0
18
°C
I1/5/12
10:30
DSD
Field
Analyzed by: Miuobac Laboratories, Inc - Ohio Valley
Total Organic Carbon 0.996
Stale Certifiealions:
NCDNR 1111
NCDOH 1137714
USDA 43797
mg/L 11/10/12 0:52 DIH E415.1 J
^Respectfully Submitted
�Y-C4/[nL �LCLL6Zr�_r ��
Jeanne Overstreet, Project Manager
Page 12 of 13

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Microbac- Fayetteville Division
Chloride
154
COD, Total
102
Conductivity
433
Depth to Water Surface
5.10
Nitrate as N
2.55
pH, Field Test
3.87
Total Dissolved Solids
218
Sulfate as SO4
16
Temperature
20
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
Total Organic Carbon
1.30
Notes and Definitions
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
R-4
1211053-13
Date Reported: November 20, 2012
Dale Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
mg/L
11/7/12 9:35
JLR
EPA300.0
mg/L
11/6/12 9:00
DSK
SM 20th Ed. 5220 D Al2
umhos/cm
1116112 9:30
DSK
SM 20th Ed. 2510 B
feet
11/5/12 10:20
DSD
Field Measurement
mg/L
11/7112 9:35
JLR
EPA 300.0
pH Units
11/5/12 10:20
DSD
Field
mg/L
11/6/12 9:45
JAO
SM 20th Ed. 2540 C S l
mg/L
11/7/12 9:35
JLR
EPA 300.0
°C
I1/5/12 10:20
DSD
Field
mg/L 11/10/12 1:05
U Not detected at or above adjusted sample detection limit
SI Relative Percent Difference (RPD) outside accepted recovery limits
J The analyte was positively identified, but the quantitation was below the RL
B Detected in the associated Method Blank
Al2 MSIMSD fail recovery, but the LCS passes criteria.
State Cenircations:
NCDNR It II
NCDOH #37714
USDA N3787
DIH E415.1
^Respectfully Submitted
`�f Zlz2 C/u-riL62.�icr '
Jeanne Overstreet, Project Manager
Page 13 of 13

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
R -Sa
1211053-05
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: M;Mbac - FayettevtTle Division
Chloride
62.2
mg/L
II/6/12 16:33
JR
EPA300.0
COD, Total
193
mg/L
11/6/12 9:00
DSK
SM 20th Ed. 5220 D
Conductivity
204
umtjos/cm
I1/6/I2 9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
3.30
feet
11/5112 10:05
DSD
Field Measurement
Nitrate as N
4.78
mg/L
1.1/6112 16:33
JR
EPA 300.0
pH, Field Test
4.02
pH Units
11/5/12 10:05
DSD
Field
Total Dissolved Solids
124
mg/L
1116/12 9:45
JAO
SM 20th Ed. 2540 C
Sulfate as SO4
30
mg/L
11/6/12 16:33
JR
EPA 300.0
Temperature
20
°C
I1/5/12 10:05
DSD
Field
Analyzed by: Mic obac Laboratories, Inc - Ohio valley
Total Organic Carbon
2.18
mg/L
11/9/12 22:18
DIH
E415.1
State Certifications:
NCDNR till.
NCDOH 1137714
USDA 93787
^Respectfully Submitted
Jeanne Overstreet, Project Manager
13
Page 5 of 13

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
R-6
1211053-06
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
90.6
COD, Total
144
Conductivity
222
Depth to Water Surface
4.80
Nitrate as N
0.600
PH, Field Test
5.11
Total Dissolved Solids
172
Sulfate as SO4
28
Temperature
20
Analyzed by: Mimbac laboratories, Inc - Ohio Valley
Total Organic Carbon
12.4
State Certifications:
NCDNR It II
NCDDH 1137714
USDA 43787
mg/L
I1/6/12 16:50
JR
EPA300.0 B
mg/L
11/6/12 9:00
DSK
SM 20th Ed. 5220 D
utnhos/cm
11/6/12 9:30
DSK
SM 20th Ed. 2510 B
feet
11/5/12 9:55
DSD
Field Measurement
mg/L
11/6112 16:50
JR
EPA300.0
PH Units
11/5/12 9:55
DSD
Field
mg/L
11/6/12 9:45
JAO
SM 20th Ed. 2540 C S 1
mg/L
11/6/12 16:50
JR
EPA300.0
°C
11/5/12 9:55
DSD
Field
mg/L
I1/9/12 23:07
DTH
E415.1
^Respectfully Submitted
Jeanne Overstreet. Project Manager
Page 6 of 13

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
R-7
1211053-07
Date Reported: November 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbae- FayeReville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
119
mg/L
I116/12
17:07
JR
EPA300.0
146
mg/L
11/6/12
9:00
DSK
SM 20th Ed. 5220 D
211
umhos/cm
11/6/12
9:30
DSK
SM 20th Ed. 2510 B
3.00
feet
11/5/12
9:40.
DSD
Field Measurement
0.533
mg/L
11/6112
17:07
JR
EPA300.0
4.61
pH Units
11/5/12
9:40
DSD
Field
112
mg/L
11/6/12
9:45
JAO
SM 20th Ed. 2540 C
17
mg/L
I1/6/12
17:07
JR.
EPA300.0
19
°C
11/5112
9:40
DSD
Field
Analyzed by: Mlaobac labcMtaries, Inc - Ohio Valley
Total Organic Carbon 9.94
Slatc certification:
NCDNR All
NCDOH 1137714
USDA 03787
mg/L 11/9/12 23:22 . DIH E415.1
Respectfully Submitted
-easz�cr_ �iwtaties�
Jeanne Overstreet, Project Manager
9
Page 7 of 13

Allen-, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
N
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Welis samples-3/Yearly
R-8
1211053-08
Date Reported: November, 20, 2012
Date Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Pxk'Wed Dy: Mlaotuc - Fayetteville DivWon
Chloride
55.3
mg/L
I1/6/12
17:23
JR
EPA300.0
COD, Total
113
- mg/L
11/6/12
9:00
DSK
SM 20th Ed. 5220 D
Conductivity
246
umhos/cm
I1/6/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
4.10
feet
11/5/12
9:30
DSD
Field Measurement
Nitrate as N
9.59
mg/L
11/6/12
17:23
JR
EPA 300.0
pH, Field Test
4.01
pH Units
11/5112.
9:30
DSD
Field
Total Dissolved Solids
144
mg/L
11/6/12
9:45
JAO
SM 20th Ed. 2540 C
Sulfate as SO4
45
mg/L
11/6/12
17:23
JR
EPA 300.0
Temperature
20
°C
I1/5/12
9:30
DSD
Field
Analyzed by: Miaobac Laboratories, Inc - Ohio Valley
Total O-ganic Carbon
1.27
mg/L
11/9/12 23:58
DIH
E415.1
Slate Certifications:
NCDNR 1/II
NCDOH 1/37714.
USDA #3797
Respectfully Submitted
Jeanne Overstreet, Project Manager
N
Page 8 of 13

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples-3/Yearly
R-9
1211053-09
Date Reported: November 20, 2012
Dale Received: November 05, 2012
Date Sampled: November 05, 2012
Sampled BY: Davidson
Analyte Resul! Units Analyzed Analyzed By - Method Qualifier
Analyzed by Miuobac- Fayetteville Division
Chloride
57.4
mg/L
11/6/12
17:40
JR
EPA300.0 Al2,B
COD, Total
324
mg/L
11/6/12
9:00
DSK
SM 20th Ed. 5220 D
Conductivity
232
umhos/cm
11/6/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
4.11
feet
11/5/12
11:40
DSD
Field Measurement
Nitrate as N
5.51
mg/L
11/6/12
17:40
JR
EPA 300.0
pH, Field Test
4.06
pH Units
11/5/12
11:40
DSD
Field '
Total Dissolved Solids
236
mg/L
I1/6/I2
9:45
JAO
SM 20th Ed. 2540 C
Sulfate as SO4.
52
mg/L
11/6/12
17:40
1R
EPA 300.0 Al2
Temperature
22
°C
11/5/12
11:40
DSD
Field
Analyzed by Micnobac laboratories, Inc - Ohio Valley
Total Organic Carbon
0.868
mg/L
11/10/12.
0:10
DiH
E415.1 J
State Certifications: Respectfully Submitted
NCDNR 811
NCDDH 1137714 �,e¢�c,cr �ice.La2`f_rr
USDA #3787
Jeanne Overstreet, Project Manager
Page 9 of 13

GW-59A CON'1PLIANCE REPORT FORM Permit # W Q Ooo yob?
(.Submit one each ntonitorh ., period whb GII•-59jarms.)
1 ,
Enter date monitoring results were due. (L�-31-1 1 Will this monitoring report (GIN-59 and GW-59A)
YES
00)
be submitted after the established due date?
Z
Was any required information missing on the GW-59 report forms?
YES
N
IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? if the answer is -Yes". contact the Regional Ogice for guidance.
4
Are any monitored constituents equal to or above the established standards?
E
NO
If the answer to question 4 is "NO", skip to section B.
If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s)
exceeding standards in the space provided below.
R e - Toc- 1a.4 j,g/r`
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YE.
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO'; skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentrations) reported, and sample collection date for each occurrence (for the last two years).
345-1.2
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
O
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answeris "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subiect the Permittee to a Notice of Violation
fines, and/or penalties..
g
The person completing this portion (G W--59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge, that the above information was evaluated and the Information ;submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
0<.� 664vul
dl> L f a I y
Signature of Permittee (or Authorized Agent) bate
GNY-59A 12BI2003

J 1N6 Up ,1 E M OR It SIN eE
Qttltliry Vegetables
5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone]
December 18, 2012
Dept. of Environmental & Natural Resources
Division of Water Quality — Information Processing Unit---
1617 Mail Service Center (�11
Raleigh, NC 27699-1617 I Ca4n
[phone]
RE: Groundwater Quality Monitoring Report
Aliens,Inc.—Turkey, NCFacility occLkIV
Permit # W00004268
Yv�l
Enclosed are the original and one copy of the Groun< G W-59
and GW-59A, and the lab report for Aliens, Inc — Tunvy;-Txc--racmy or sa—>— mp es�ted in
November, 2012.
Monitoring well # R-6 exceeded the 10mg/L limit for TOC as stated in the permit.
This well will be resampled and results submitted as soon as possible.
If you have any questions or require any additional information, please contact me by
phone at [phone].
Sincerely,
Robert Caldwell
Assistant Plant Manager
Aliens, Inc. Turkey facility
CC: Laura Mushinski, Aliens, Inc
Reid Wells, Aliens, Inc — Turkey facility
JAN 0 4 2013
Information P
DWlyr0"Qstng Unk

U, NJ r.M O RI6g SING£
• Quality Vegetables
5900 TURKEY HIGHWAY, TURFY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone]
September 11, 2012
Dept. of Environmental & Natural Resources
Division of Water Quality — Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
RE: Groundwater QualityMonitoring Report
Aliens, Inc. —Turkey, NC Facility
Permit # W00004268
This letter is in response to the Groundwater Monitoring Report dated August 16, 2012 for the Aliens, Inc -
Turkey, NC facility.
The report showed the TOC level in M W # -1 exceeded the 10 mg/L limit, and M W # -3 exceeded the TDS
limit of 500 mg/L as specified in the permit.
The two wells were resampled and the results were within the permit requirements. The results are listed on
the following pages.
If you have any questions or require any additional information, please contact me by phone at (910) 596-
0028 ext # 104.
Sincerely, f
, D
Tim Browers y yvv\ /17� f(OI VAW a a o
Plant Manager !'
Aliens, Inc. Turkey facilityi 7IVff PreI ,Jnit
CC: Laura Mushinski, Aliens, Inc
Reid Wells, Aliens, Inc —Turkey facility JR—F®O
f 0 1 2012
1 )'

rUrtm UN
:R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y """ NC 28393-9703 County Sampson
act Person: Tim Browers
Location/Site Name:_ _
Telephone#: [phone]
No. of wells to be sampled:.
L ID NUMBER (from Permit): MW-1 Date sample collected: 8/23/12
Depth: ft. Well Diameter: — in.
i to Water Level: ft, below measuring point Screened Interval: _ft. to _ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: gallons
:RMIT Number: Expiration Date: July 31, 2015
in -Discharge WQ0004268 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Feld ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH _units Temp.
Spec. Cond. µMhos
Odor
Appearance
oC DRY at
time of
sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
4METERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mgfl Nitrite (NO,) as N mg/I Pb - Lead mg/I
Coliform: MF Fecal /loom] Nitrate (NO3) as N mgll Zn - Zinc mgA
Coliform: MF Total
/loom]
Phosphorus: Total as P
mgll
(Note: Use MPN method for highly turgid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
mg/I
AI - Aluminum
mg/1
(when analyzed)
units
Ba- Barium
mgA
.0 TOC
5.62 mg/I
Ca - Calcium
mgA
n Chloride
D
mg/I
Cd- Cadmium
mgA
p Arsenic
mgll
Chromium: Total
mgll
Grease and Oils
mgll
Cu - Copper
mg/I
ORGANICS: (by.GC, GCIM3': HPLC)
`® Phenol
mgA
Fe - Iron
mg/I
(Specify test and method #1 ATTACH LAB REPORT.)
Sulfate
mgll
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
- Rpecific Conductance
µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mgA
Mg - Magnesium
mg/I
, method #
(Ammonla Nitrogen; NHsas N; Ammonla Nitrogen, Total)
Mn- Manganese
mg/I
,method#
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal°/d
Tim Browers, Plant Manager
Perminee (or Authorized Ageno Name and Title- Please print or type
GW-59 Rev. 112007
701

SUBMIT FORM
?R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 6900 Turkey Highway
:y "`" NC 28393-9703 County Sampson
act Person: Tim Browers
Location/Site Name:
Telephone#: [phone]
No. of wells to be sampled:
IRMIT Number: Expiration Date: July 31, 201b
n-Discharge WQ0004268 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
WELL
WELL ID NUMBER (from Permit): MW-3
Dale sample collected: 8/23/12
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter.
pH I
Temp. or.
DRY at
Depth to Water Level: ft. below measuring point
_in.
Screened Interval: ft. to
—
ft.
_units
Spec. Cond.
µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead
mgA
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mgll
Zn - Zinc
mgA
Coliform: MF Total 1100ml
Phosphorus: Total as P
mgll
(Note: Use MPN method for highly tmeid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 416 mg/I
AI - Aluminum
mgll
pH (when analyzed) units
Be - Barium
mgll
TOC mg/I
Ca - Calcium
mg/I -
Chloride mgfl
Cd - Cadmium
mgfl
Arsenic mgn
Chromium: Total
mgA
Grease and Oils mgA
Cu - Copper
mgn
ORGANICS: (by GC, GC/MS; HPLC)
Phenol mg/I
Fe - Iron
mgll
(Specify test and method #! ATTACH LAB REPORT.)
Sulfate mg/I
Hg- Mercury
mgA
ReportAttached7
❑: yes (1) ❑ No
Specific Conductance µMhos
K- Potassium
mg/I
VOC
, method #
Total Ammonia mgA
Mg - Magnesium
mgA
, method #
(Ammonia Nitrogen; NHsas N;Ammonia Nitrogen, Total)
Mn- Manganese
mgA
,method#
TKN as N mg/I
Ni - Nickel
mg/I
, method # '
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent.Total VOCs: mglL VOC Removal%a
Tim Browers, Plant Manager,—
Permidee(or Authorized Anent)Name and Title- Please print or type. Signature of Feral (or Authorized Aql
GW-59 Rev, 1/2007

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/W samples - 3/Yearly, Retest
M/W - 401
1208560-01
Date Reported: September 07, 2012
Date Received: August 23, 2012
Date Sampled: August 23, 2012
Sampled By: R. Wells
Analyze Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Morobac laboratories, Inc - Ohio Valley
Total Organic Carbon 5.62 mg/L 8/30/12- 18:01 DIH A5310B
MW:#3
1208560-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Total Dissolved Solids 416 mg/L
Notes and Definitions
U Not detected at or above adjusted sample detection limit
" [Undefined]
Slate Ccnificalions:
NCDNR till
NCDOH #37714
USDA #3787
8/27/12 13:40 JAO SM 20th Ed. 2540 C
Respectrufy Submitted
Bonnie K. Sanders, Administrative Assistant
Page 1 of 1

SLIRMIT Fr1PM r1N VFI I MAI PAPFP'r1NI V
b
0
D
c
so c
ID -p ua
Do o
Om
L)y ❑
to ~
C
GROUNDWATER;QUALITYMONITORING:
I'
!
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES s
wlsloNOFwATER'6UAurv4NFORNAnoNPaocEsslNcuNr?��"t�r�,
COMPLIANCE REPORT FORM
j
617 MAIL'SERVICEOENTER RALEIGH; NC 276691617r Phone,(919)733,3221q`,�
.r... :'.
t Cl Please Print or Type
FACILITY INFORMATION PlI � �
""''"-"
- : Jul
PERMITNumber: Expiration Date: y 31, 2015
Facility Name: Alleris, Inc. -Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different): _.
Facility Address: 5900 Turkey Highway
- -
-
TYPE OF PERMITTED "OPERATION BEING MONITORED
El Lagoon El Remediation: Infiltration Gallery
Turkey ' I`""' NC 28393-9703 County Sampson
Spray Field ❑ Remediation:
Contact Person: Tim Browers
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name:
No. of wells to be- sampled:
13
❑ Water, Source Heat Pump El
from Pemul
SAMPLING INFORMATION
If WELL ,
WELL ID NUMBER (from Permit): MW-1
Date sample'collected: 7/9/12
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in,
pH 3.35 units Temp. 26 °C
DRY at
Depth to Water Level: 21 ft, below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. µMhos
time of
—
-
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples focmetals were collected unfiltered: DYES
❑ NQ and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and,cohoidal concentrations.
. COD 201 mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /1 OOml
Nitrate (NO3) as N
5.73 mg"
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Nora: Use MPN method for Highly NNidsempies)
Orthophosphate:
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 458 mgn
AI - Aluminum
mg/I
pH (when analyzed) units
.Ba -.Barium
mg4
TOC24:4mgll
Ca - Calcium
mg4
Chloride 199 mg/I
- Cd,-Cadmium
mg/I
I
Arsenic mg/I
Chromium:.Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg4
ORGANICS: (by GC, GC/MS, HP.LC)
Phenol mg/I
F Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 42 rri
Hg - Mercury
mg4
Report. Attached? ❑ Yes (1) ❑ No (0)
Conductance 808. µMhos
K - Potassium
mg/l
VOC , method #
Jpecific
Total Ammonia mg4
(Ammonia Nitrogen; NH3a6 N; Ammonia Nitrogen, Total)
i Mg - Magnesium
mg1I
, method #
Mn - Manganese
mg/I
method #
TKN as N mg/l
i Ni = Nickel
mg/I
method #
For Remediation Systems Only (Attach
Plant Manager
,rized Agent) Name and Title - Please print or type Signature of Peaoittee (or Authorized Agent)'
Rev. 1 /2007 : r
?v I)
(Date)

SUBMIT FORM ON YELLOW PAPER ONLY
OEPARTMENTOFENVIRONMENTti NATURALRESOURCESr
GROUNDWATER QUALITY MONITORING:
IVIs1oNOFwATEanuaury NFORMAnoNPRocEsslNcunlT
COMPLIANCE REPORT FORM
Mill N
677 MAILSERVICE$,CENTER RALEIGH;`NC 276B9187T sPhane (e19)7337421
FACILITY INFORMATION - Please Pont Cleady or Type -
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey "" NC 28393-9703 County Sampson
1'n'0 t'`"
© Spray Field ❑ Remediation:
Contact Person: Tim Browers
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No, of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 7/9/12
FIELD ANALYSES:
WAS
Well Depth: R.
Well Diameter. in.
pH 3.70 units Temp. 24 aC
DRY at
Depth to Water Level: 7.7 ft. below measuring point
Screened Interval:
to
R. Spec. Cond: µMhos
time of
_ft.
sampling,check
Measuring Point Is R. above land surface
Relative M.P. Elevation:
R.
Odor
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Dale sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 102 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mgll
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
0.632 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN molhad for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 222 mg/I
_ At - Aluminum
mg/I
pH (when analyzed) units
Ba-Barium
mg/I
TOC 5.15 al
_ Ca - Calcium
mg/I
Chloride 83.5 mg/I
Cd- Cadmium
mg/l
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe - Iron
mg/1
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 7.8 nr ll
Hg - Mercury
mgll
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 363 µMhos
K - Potassium
mg/l
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
,method #
(Amma,Je Nlwgen: NH3 as N: Ammaaia Niwgen, total)
Mn - Manganese
mg/I
method #
TKN as N mg/l
Ni - Nickel
mg/I
, method #
For Remedlation Systems Only •
I cedify that, to the best of my kno ,,,e and belief; the Information submieed in this report Is true; accurate, and complete, and that the liberate analytical data was produced us)ng approved methods of analysts bqa
DWO-certified laboralo , ml in re that there ere si nifica'nt enaNles fofsubmitting false information, Including the cssitilll 'or ones ands im risonn lfor 4wriri ,violations:
Tim Browers, Plant ManagerPemnittee Car Authorized Agent) N.nne and Title -Please print or type Signature of Peniftee (orAuthorized Agent) �!
s.

FORM
ONLY
NDWATER QUALITY MONITORING:
LIANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y "°'"'' NC 28393-9703 County Sampson
act Person: Tim Browers Telephone#: [phone]
Location/Site Name: ! No, of wells to be sampled: 13
L ID NUMBER (from Permit): MW-3 Dale sample collected: 719112
Depth: ft. Well Diameter: in.
1 to Water Level: 5.1 ft. below measuring point Screened Interval: ft. to ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
ties for metals were collected unfiltered: ❑YES ❑ NO and field acidified ❑ YFS M Nn
ETERS NOTE: Values should reflect dissolv
COD 116 mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total
/100ml
(Nate; Use MPN method for highly tuebld samples)
Dissolved Solids: Total
IC-526"nuril
pH (when analyzed)
units
TOC
2.53 mg/I
Chloride
104 mall
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
53 mg/I
Specific Conductance
500 µMhos
Total Ammonia
mg/1
(Ammonia Nitrogen; Nils es N; Ammonia Nitrogen, Total)
TKN as N
For Remediation
Lab
:RMIT Number:
m-Discharge W00004268
Expiration Date: July 31, 2015
UIC .
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 5.81 units
Spec. Cond.
Odor
Appearance
Temp. 27 ac DRY at
µMhos time of
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
colloidal concentrations.
Nilrite.(NO2) as N
mg/I
Pb - Lead mg/I
Nitrate (NO3) as N
0.616 mg/I
Zn - Zinc mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
AI - Aluminum
mg/I
• Be - Barium
mg/I
Ca - Calcium
mg1l
Cd - Cadmium
mg/1
Chromium: Total
mg/1
Cu -Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC) ,
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
K - Potassium
mg/I
VOC , method #
Mg - Magnesium
mg/1
, method #
Mn - Manganese
mg/I
, method #
Ni - Nickel
mg/I
, method #
Tim Browers, Plant Manager
Permitlee (or Authorized Agent) Name and Tdle- Please print or type
GW-59 Rev. 112007 ,
Total
iomplete, and that gpJaboratoryanalytical data
the- dssihitit y of fines and'Im risdnment'for knt
Signature of Pennittee (or Authorized Aqent�
VOC

UNLY
:R QUALITY MONITORING:
REPORTFORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
act Person: Tim Browers
Location/Site Name:
L ID NUMBER (from Permit): MW-4
Depth: ft.
1 to Water Level: 10.5 ft. below measuring point
.uring Point is ft. above land surface
ne of water pumped/bailed before sampling: 10+
)lea for metals were collected unfiltered: ❑YES ❑
County Sampson
Telephone#: [phone]
No. of wells to be sampled: 13
Date sample collected: 7/9/12
Well Diameter: in.
Screened Interval: _ft. to _ft.
Relative M.P. Elevation: ft.
:RMIT Number:
m-Discharge WQ0004268
Expiration Date: July 31, 2015
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 4.17 units
Spec. Cond.
Odor
Appearance
Temp. 26 eC DRY at
µMhos time of
l sample analyzed:
Laboratory Name: Mlcrobac Laboratories
Certification No. NC#11 NC#37714
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
48.6 mg/l
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NOa) as N
4.87 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly lureld samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
110 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba- Barium
mg/I
TOC
2.58 mgfI
Ca - Calcium
mg/I
Chloride
24.8 mg/I
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
3.8 mgll
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
174 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Ammaola Nitrogen: NM,as PT, mmonla Nltmgen, TotaQ
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: _mg/L Effluent Total VOCs: mglL VOC Removal%
Tim Browers, Plant Manager V oter g1l ")-6
Permiftee (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (or Authorized Agent) (Date)
GW-59. Rev. 112007

SUBMIT FORM ON VFI I OVI PAPER nNi V
GROUNDWATER QUALITY MONITORING:
DEPARTMENTOF ENVIRONMENTS NATURALRESOURCES
IVISION OF WATER QUALITY4NFORMATION PROCESSING UNITr+�.k'.x
COMPLIANCE REPORT FORM
617 MAIL SERVICE OE_NTEft RALEIGH; NC E3
Z76991617 Phono (919))1a 7P21
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Allens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey """' NC 28393-9703 County Sampson
r� `It'll
© Spray Field ❑ Remediation:
Contact Person: Tim Browers
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
(From Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-1
- Date sample collected: 7/9/12
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in,
pH 4.19 units Temp. 29 eC
DRY at
Depth to Water Level: 7.50 ft. below measuring
P g point
Screened Interval: ft.
to
ft. Spec. Cond. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 349 mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mgh
Coliform: MF Fecal /100m1
Nitrate (NO3) as N
0.672 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN meNOC for highly lurhiaeomples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 112 mg/I
Al - Aluminum
mg/I
pH (when analyzed) units
Ba -'Barium
mg/I
TOC 2.11 mg/I
Ca - Calcium
mg/l
Chloride 35.1 mg/I
Cd- Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mg/l
Grease and Oils mg/l
Cu - Copper
mgll
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 10 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 169 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen: Nikes N;Ammonia Nitrogen. Total)'
Mn-Manganese
mg/I
,method#
TKN as N mg/l
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mD/L VOC Removal°/
Tim Browers, Plant Manager
Permiaee (or Authorized Agent) Name and Title- Please print or type
GW-59 Rev. 112007

FORM
NDWATER QUALITY MONITORING:
LIANCE REPORT FORM
ty Name: Aliens, Inc. - Turkey
iit Name (if different):
ty Address: 5900 Turkey Highway
<ey NC 28393-9703 County Sampson
act Person: Tim Browers Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 13
L ID NUMBER (from Permit): R-2a Date sample collected: 719/12
Depth: ft. Well Diameter: in.
1 to Water Level: 7.50 ft. below measuring point Screened Interval: ft. to ft.
•uring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
:lea for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES 11 Nn
:RMIT Number:
Expiration Date: July 31, 2015
m-Discharge W00004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 3.35 units
Spec. Cond.
Odor
Appearance
Temp. 30 eC DRY at
....,._- time of
a sample analyzed:
Laboratory Name:
Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved andcolloidal concentrations.
COD
26.2 mgA
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
4.79 mgn
Zn - Zinc mg/I
Coliform: MF Total
/100m1
Phosphorus: Total as P
mg/I
(Note: Use MPN melnod for hlgNy lurbltl samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
68 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/l
TOC
1.00 mg/I
Ca - Calcium
mg/I
Chloride
12.8 mg/l
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mgll
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
7.6 mgll
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
134 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/l
Mg - Magnesium
mg/I
, method #
(Ammonia Nibogen; NH3 as N; Ammonia Nitrogen, Total)
Mn- Manganese
mg/I
,method#
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L - Effluent Total VOCs: _ mq/L VOC Removal%
Tim Browers, Plant Manager
Permittee (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (or Authorized Agent)
GW-59 Rev. 1/2007

'u
ROUNDWATER QUALITY MONITORING:
OMPLIANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y NC 28393-9703 County Sampson
ad Person: Tim Browers
Location/Site Name:
Telephone#: [phone]
No. of wells to be sampled: 13
L ID NUMBER (from Permit): R-3 Date sample collected: 7/9/12
Depth: ft. Well Diameter: in.
i to Water Level: 9 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
:RMIT Number:
Expiration Date: July 31. 2015
�in-Discharge WQ0004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 3.43 units
Spec. Cond.
Odor
Appearance
Temp. 25 aC DRY at
time of
sample
analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
116 mg/I
Nitrite (NOO as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
1.65 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN meeNcd forhighly tumid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
170 mg/I
Al - Aluminum
mg/I
pH (when analyzed)
units
Be -Barium
mg/I
TOC
1.40 mg/l
Ca - Calcium
mg/I
Chloride
70.5 mg/I
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
17mg/I
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
369 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHsas N; Ammoma Nilragen, Total)
Mn - Manganese
mg/I
method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remediation Svstems Only (Attach Lab Reports): Influent Total VOCs: ma/L Effluent Total VOCs: ma/L VOC Removal%
Tim Browers, Plant Manager SS/ao
Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent)
GW-59 Rev, 112007

RI IRnnIT FnORA non VFI I r IAI DADCD nut v
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF ENVIRONM"NT Z, NATURAL
IVISIONdKIRATERQUALITY-INFORMATIONPROCEsslNcUNIT.
COMPLIANCE REPORT FORM
z•• '1 `•�: ,
6771MAIL SERVICE'CENTER'RALEIOFi NC Y769851et7 Phona'(9791733a2?7l ij�' ... ..
FACILITY INFORMATION Please Pdnt
Cleady or Type
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
El Lagoon agoon ❑Remediation: Infiltration Gallery
Turkey j9A",nj NC 28393-9703 County Sampson
❑X Spray Field ❑ Remediation:
Contact Person: Tim Browers
' Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
from Pertnil
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-4
Date sample collected: 7/9/12
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
pH 3.62 units Temp. 28 eC
DRY at
Depth to Water Level: 8 R, below measuring point
_in.
Screened Interval:
to
Spec. Cond. µMhos
time of
Measuring Point is R. above land surface
_ft.
Relative M.P. Elevation:
_R.
R.
Odor
sampling.
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
check
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No, NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 26.2 mg/l
Nitrite (NOz) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
1.15 mg/I
Zn - Zinc mg/I
Coliform: MF Total 1100ml
Phosphorus: Total as P
mg/l
(Note: Use MPN mooned for highly tursid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 142 mg/I
Al - Aluminum
mg/l
pH (when analyzed) units
Be - Barium
mg/l
TOC 1.36 mg/I
Ca - Calcium
mg/I
Chloride 33.5 mg/I
Cd - Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GCIMS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 29 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 229 µMhos
K- Potassium
mg/l
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHeas N; Ammame Nitrogen, Tolal)
Mn -Manganese
mgll
,method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Tim Browers, Plant Manager —�cjl act I
Permittee for Authorzed Agent? Name and Title - Please print or type Signature of Pentaftee (or Authorized Agent) (Date
GW-59 Rev. 112007

SUBMIT FORM
TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. -
Name (if different): _
Address: 5900 Turkey
Sampson
act Person: Tim Browers Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 13
L ID NUMBER (from Permit): R-5a
Depth: ft.
h to Water Level: 7 ft, below measuring point
luring Point is ft. above land surface
ne of water pumped/bailed before sampling: 10+
PERMIT Number:
Expiration Dale: July 31, 2015
Non -Discharge WQ0004268
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
R1 Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
Date sample collected: 7/9112
Well Diameter: in.
Screened Interval: ft. to ft.
Relative M.P. Elevation: ft.
FIELD ANALYSES
pH 3.65 units Temp. 29 aC
Spec. Cond. µMhos
Odor
Appearance
e sample analyzed:
Laboratory, Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved colloidal concentrations.
COD
179 mgA
Nitrite (NOr) as N
mg/I
Pb - Lead mg/I
Coliform: IMF Fecal
/100ml
Nitrate (NO3) as N
6.28 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Nola: Use MPN melhod for highly turbid samples)
Orthophosphate
ri
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
120 mgll
At - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOC
1.53 mg/l
Ca - Calcium
mg/I
Chloride
20.7 mgA
Cd- Cadmium
mg/I
Arsenic
mgA
Chromium: Total
mg/I
Grease and Oils
mg/l
Cu - Copper.
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB :REPORT.)
Sulfate
19 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
194 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method # .
(Ammonia Nitrogen; NHsas N; Ammanla
Nitrogen, Total)
Mn - Manganese
mg/l
, method # _
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs::. mg/L, _ Effluent Total VOCs: mg/L VOC Removal%
Tim Browers, Plant Manager 1�
Permittee (or Authorized Agent) Name and Title- Please print or type Signature of Permiftee (or
GW-59 Rev. 112007
at
of

ON
ROUNDWATER QUALITY MONITORING:
DMPLIANCE REPORT FORM
Name: Aliens, Inc. -
Name (if different): _
Address: 5900 Turkey
act Person: Tim Browers
Location/Site Name: '
L ID'NUMBER (from Permit): R-6
Depth: ft.
h to Water Level: 8 ft. below measuring point
luring Point is ft. above land surface
ne of water pumped/bailed before sampling: 10+
county Sampson
Telephone#: [phone]
No, of wells to be sampled: 13
Date sample collected: 7/9/12
Well Diameter: in.
Screened Interval: ft.
Relative M.P. Elevation:
to _ft.
ft.
'RMIT Number:
Expiration Date: July 31, 2015
m-Discharge WQ0004268
UIc
'DES
Other
'PE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
EI Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 4.44 units
Spec. Cond.
Odor
Appearance
Temp. 28 oC DRY at
µMhos time of
sampling,
check
here: ❑
e sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
84.4 mgfl
i Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3yas N
1.25 mg/I
Zn - Zinc mg/I
Coliform: MF Total
1100ml
Phosphorus: Total as P
mg/I
(Note: use MPN menmd for highly tumid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
136 mg/I
Al - Aluminum
mg/I
pH (when analyzed)
units
Ba-- Barium
mg/I
TOC
5.15 mg/I
_ Ca - Calcium
mg/I
Chloride
44.7 mg/l
Cd- Cadmium
mg/l
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu'- Copper
mg/I
ORGANICS: (by GC, GC/MS,'HPLC)
Phenol
mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
18 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
262 µMhos
K - Potassium
mg/l
VOc , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
,method #
(Ammonia Nitrogen; NHras N; Ammonia
Nitrogen, Total)
Mn - Manganese
mg/l
, method #
TKN as N
mg/I
Ni - Nickel
mg/l
-- , method #
For Remediation Systems Only; (Attach Lab Reports,): Influent Total VOCs:: mg/L —Effluent Total VOCs:
Tim Browers, Plant Manager
Permiltea (or Authorized Agent) Name and Title - Please prinfor type
GW-59 Rev. 112007

TER QUALITY MONITORING:
E REPORT FORM
ity Name: Aliens, Inc. - Turkey
lit Name (if different):
ityAddress: 5900 Turkey Highway
key """ NC 28393-9703 County Sampson
(c1y ,fma1 1-"dd i
act Person: Tim Browers Telephoned: 910-596-0028
Location/Site Name: No. of wells to be sampled: 13
LID NUMBER (from Permit): R-7 Date sample collected: 7/9/12
Depth: ft. - Well Diameter: —in.
h to Water Level: 8 ft. below measuring point Screened Interval: _ft. to _ft.
luring Point is ft, above land surface Relative M.P. Elevation: ft.
Tie of water pumped/bailed before sampling: 10+ gallons
ales for metals were collected unfiltered: OYES ❑ NO and field acidified: ❑YES ❑ NO
a sample analyzed: Laboratory Name: Microbac Laboratories
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
111 mgA
Nitrite (NO.) as N
mg/I
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
0.604 mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P'
mg/I
(Note: Use MPN roamed for highly turbld samples)
Orthophosphate
mg/I
Dissolved Solids: Total
134 mgA
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba- Barium
mg/I
TOC
6.76 mgA
Ca - Calcium
mg/l
Chloride
46.4 mgA
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/1
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
5.6 mg/I
Hg - Mercury
mg/I
Specific Conductance
198 µMhos
K- Potassium
mg/I
Total Ammonia
mg/I
Mg - Magnesium
mg/I
(Ammonia Nitrogen: NHS as Nl Ammonia Nitrogen,
Total)
Mn- Manganese
mg/I
TKN as N
mg/I
Ni - Nickel
mg/I
:RMIT Number:
Expiration Date: July 31, 2015
m-Discharge W00004268
UIC
)DES
Other
'PE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other.
FIELD ANALYSES:
pH 4.35 units
Spec. Cond.
Odor
Appearance
Temp. 26 °C DRY at
µMhos time of
Certification No. NC#11 NC#37714
Pb - Lead mg/I
Zn - Zinc mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.')
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
ror memeolatlon systems manly lAttacn Lao Kepprts): Inriuent total VUCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Tim Browers, Plant Manager
Permittee (or Authorized Anent) Name and Title - Please Print or type
GW-59 Rev. 112007

TER.QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. -
Name (if different): _
Address: 5900 Turkey
v i`lec:l
County Sampson
act Person: Tim Browsers Telephone#: [phone]
Location/Site Name: No, of wells to be sampled: 13
PERMIT Number:
Expiration Date: July 31, 2015
Non -Discharge WQ0004268
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
L ID NUMBER (from Permit): R-8 Date sample collected: 7/9112
Depth: ft. Well Diameter: in.
h to Water Level: 9 ft. below measuring point Screened Interval: ft. to ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
)lea for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO
FIELD ANALYSES:
pH 4.15 units Temp. 29 aC
Spec. Cond, µMhos
Odor
Appearance
a sample analyzed:
Laboratory Name: Mlcrobac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD
115 mg/I
Nitrite (NO2) as N
mgA
Pb - Lead mgll
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
13.9 Ill
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
ri
(Note: Use MPN memoal for highly tu`ald samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
172 mgA
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba -.Barium
mg/I
TOC
1.05 mgA
Ca - Calcium
mg/I
Chloride
23.6 mgA
Cd- Cadmium
mg/I
Arsenic
mg/1
Chromium: Total
mgA
Grease and Oils
mg/I
Cu -,Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
31 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
285 µMhos
K'- Potassium
mg/I
VOC method #
Total Ammonia.
mgA
Mg - Magnesium
mg/I
-method#
(Ammonia Nitrogen; Wass N: Aeanoda Nitrogen, Total
Mn- Manganese
mg/I
,method#
TKN as N
mgA
Ni - Nickel
mg/l
, method #
ror memeaianon ayscems Amy tAttacn Lao KeporrS): intment (oral VULS: mg/L ,Lttluent Total VOOs: mg/L VOC Removal%
Tim Browers, Plant Manager
Permitteefor Authorized Agent)Name and Title- Please print or type - signature of Petmittee.(ar Authorized Agent)
GW-59 Rev. 112007 r
at
of

FORM
Y
TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. - I urKey
Name (if different):
Address: 5900 Turkey Highway
:y 'x."tril NC 28393-9703 county Sampson
act Person: Tim Browers
Location/Site Name:
Telephone#: [phone]
No. of wells to be sampled: `13
LID NUMBER (from Permit): R-9 Date sample collected: 7/9/12
Depth: ft. Well Diameter: in.
h to Water Level: 9 ft, below measuring point Screened Interval: _ft. to _ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
Tie of water pumped/balled before sampling: 10+ gallons
:RMIT Number: Expiration Date: July 31, ZU15
In -Discharge W00004268 UIC
)DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedialion: Infiltration Gallery
© Spray Field ❑ Remedialion:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH 3.73 units
Spec. Cond.
Odor
Appearance
Temp. 30 eC DRY at
µMhos time of
sample analyzed:
, Laboratory,Name:
Microbac Laboratories
Certification No. NC#11 NC#37714
AMETERS NOTE: Values should reflect dissolved and. colloidal concentrations.
COD 241 mgA
Nitrite (NOz) as N
mgA
Pb - Lead mg/I
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
_ 4.80 mgA
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mgll
(Note: Use MPN matinee for highly turtle samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
184 mgn
Al - Aluminum
mg/I
pH (when analyzed)
units
Be -Barium
mg/I
TOC
- 1.88 mgA
Ca - Calcium
mg/I
Chloride
8.75 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mgA
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
43 mg/I
Hg - Mercury
mgll
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
188 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Amnanid Nitrogen; NH3 as T. Ammonia
Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N
mg/1
Ni - Nickel
mg/I
, method #
o-
For Remediatlon Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L .Effluent Total VOCs: mg/L VOC Removal% _
Tim Browers, Plant Manager
c
Pemlittee Car Authorized Agent) Name and Title - Please print or type Signature of Permlttee(or AuNonzed Anent)
GW-59 Rev. 1/2007
i

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc
Date Reported: August 15, 2012
Mr. Reid Wells
Project: M/Wells samples -3/learly Date Received: July 09, 2012
5900 Turkey Highway
Date Sampled: July 09, 2012
Turkey NC, 28393
Sampled By: Derek Davidson
Mw #1
1207159-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Miaobac - Fayetteville Division
,
Chloride
199
mg/L
7/10/12
1:21
JAW
EPA300.0
COD, Total
201
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
Conductivity
808
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
21.0
feet
7/9112
15:45
DSD
Field Measurement
Nitrate asN
5.73
mg/L
7/10/12
1:21
JAW
EPA300.0
pH. Field Test
3.35
pH Units
7/9/12
15:45
DSD
Field
Total Dissolved Solids
458
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2540 C.
Sulfate as SO4
42
mg/L
7/10/12
1:21
JAW
EPA 300.0
Temperature
26
°C
7/9/12
15:45
DSD
Field
Analyzed by: Mbobzc laboratories, Inc. - Ohio Valley
'
Total Organic Carbon
24.4
mg/L
7/17/12
10:43
DIH
A5310B
State Certifications:
Respectfully Submitted
NCDNR #II
D714
s,.Jll
USDAA #3783787
US
1 J
Bonnie K. Sanders, Administrative Assistant
Page 1 of 13

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Mlaebae- Fayetteville Division
Chloride
83.5
COD; Total
102
Conductivity
363
Depth to Water Surface
7.70
Nitrate as N
0.632
pH, Field Test
3.70
Total Dissolved Solids
222
Sulfate as SO4
7.8
Temperature
24
Analyzed by: Mioobac laboratories, Inc. - Ohio Valley
Total Organic Carbon
5.15
State Certifications:
NCDNR NI I
NCDOH 437714
USDA 43787
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples -3JYeariy
Mw #2
1207159-02
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
mg/L
7/10/12
3:01
JAW
EPA300.0
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 25I0 B
feet
7/9/12
15:48
DSD
Field Measurement
mg/L
7/10A2
3:01
JAW.
EPA300.0
pH Units
7/9/12
I5:48
DSD
Field
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2540 C.
mg/L
7/10112
3:01
JAW
EPA300.0
°C
7/9/12
15:48
DSD
Field
mg/L
7/16/12
19:13
DIH
A5310B
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
Page 2 of 13

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville,NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples - 3Nearly
Mw 93
1207159-03
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyze Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac - Fayetteville Division
Chloride
COD. Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
104
mg/L
7/10/12
3:17
JAW
EPA300.0
116
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
500
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
5.10
feet
7/9/12
15:49
DSD
Field Measurement
0.616
mg/L
7110/12
3:17
JAW
EPA300.0
5.81
pH Units
7/9/12
15:49
DSD
Field
526
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2540 C
53
mg/L
7/10/12
3:17
JAW
EPA300.0
27
°C
7/9/12
15:49
DSD
Field
Analyzed by: Micnobac laboratories, Inc. - Ohio Valley
Total Organic Carbon 2.53
State Certifications:
NCDNR #II
NCDOH #37714
USDA #3787
mg/L 7/16/12 19:40 D1H A5310B
Respectfully Submitted p
Bonnie K. Sanders, Administrative Assistant
Page 3 of 13

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc
Date Reported: August 15, 2012
Mr. Reid Wells
Project: MAWells samples - J/Yearly Date Received: July 09, 2012
5900 Turkey Highway
Date Sampled: July 09, 2012
Turkey NC, 28393
Sampled By: Derek Davidson
Mw N4
1207159-04
Analyzed by: Miaobac - Fayetteville Division
Chloride
24.8
mg/L
7/10112
1:38
JAW
EPA300.0
COD, Total
48.6
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
Conductivity
174
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
10.5
feet
7/9112
15:50
DSD
Field Measurement
Nitrate as N
4.87
mg/L
7/10/12
1:38
JAW
EPA 300.0
pH, Field Test
4.17
pH Units
7/9/12
15:50
DSD
Field
Total Dissolved Solids
110
mg/L
7/10/12
15:19
JA ,
SM 20th Ed. 2540 C
Sulfate as SO4
3.8
mg/L
7/10/12
1:38
JAW
EPA 300.0
Temperature
26
°C
7/9/12
15:50
DSD
Field
Analyzed try: Microbac laboratories, Inc - Ohio Valley
.
Total Organic Carbon
2.58
mg/L
7/16/12
20:27
DIH
A53IOB
State Certifications: _
Respectfully Submitted
NCDNR #II
NCDOH #37714
USDA 93787
Bonnie K. Sanders, Administrative Assistant
Page 4 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Far
Certificate of Analysis
Project: M/Wells samples - 3/1 early
R-1
1207159-05
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyle Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
35.1
mg/L
7/10/12
3:34
JAW
EPA300.0
COD, Total
349
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
Conductivity
169
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
7.50
feet
7/9/12
15:51
DSD
Field Measurement
Nitrate as N
0.672
mg/L
7/10112
3:34
JAW
EPA 300.0
pH, Field Test
4.19
pH Units
7/9/12
15:51
DSD
Field
Total Dissolved Solids
112
mg/L
7110/12
15:19
JAO
SM 20th Ed. 2540 C
Sulfate as SO4
10
mg/L
7/10/12
3:34
JAW
EPA 300.0
Temperature
29
°C
7/9/12
15:51
DSD
Field
Analyzed by: Miaobac Laboratories, Inc - Ohio valley
Total Organic Carbon
2.11
mg/L
7/16/12
20:54
DIH' ' "
A5310B
State Certifications:
NCDNR NI I
NCDOH #37714
USDA #3787
Respectfully Submitted
Bonnie R. Sanders, Administrative Assistant
Page 5 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fae
Certificate of Analysis
Project: M/Wells samples - 3/Yearly
R-1a
1207159-06
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
12.8
mg/L
7/10/12
3:50
JAW
EPA300.0
26.2
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
134
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
7.50
feet
7/9/12
15:52
DSD
Field Measurement
4.79
mg/L
7/10/12
3:50
JAW
EPA300.0
3.35
pH Units
7/9/12
15:52
DSD
Field
68.0
mg/L
7/10/12
15:I9
JAO
SM 20th Ed. 2540 C
7.6
mg/L
7/10/12
3:50
JAW
EPA300.0
30
°C
7/9/12
15:52
DSD
Field
Analyzed by: Miaobac Laboratories, Inc - Ohio Valley
Total Organic Carbon 1.00
State Certifications:
NCDNR #II
NCDOH #37714
USDA 93787
mg/L 7/16/12 21:18 DIH A5310B
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
Page 6 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Far
Certificate of Analysis
Project: M/Wells samples - 3/1'early
R-3
1207159-07
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyzed by: Miaobac - Fayetteville Division
Chloride
70.5
mg/L
7/10/12
4:07
JAW
EPA300.0
COD, Total
116
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
Conductivity
369
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
9.00
feet
7/9/12
15:53
DSD
Field Measurement
Nitrate asN
1.65
mg/L
7/10/12
4:07
JAW
EPA300.0
pH, Field Test
3.43
pH Units
7/9/12
15:53
DSD
Field
Total Dissolved Solids
170
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2540 C
Sulfate as SO4
17
mg/L
7/10/12
4:07
JAW
EPA300.0
Temperature
25
°C
7/9/12
15:53
DSD
Field
Analyzed by: Miaubac taboatorie's, Im - Ohio Valley
Total Organic Carbon
1.40
mg/L
7/16/12
21:40
DIH
A5310B
State Certifications:
Respectfully Submitted
NCDNR 911
NCDOH #37714
�. •.J'
USDA B3787
— ' - ^"^' /""'n-aQ/i.n�
Bonnie K. Sanders, Administrative Assistant
Page 7 of 13

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC.28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: Mf Wel Is samples - 3/1'early
R-4
1207159-08
Date Reported: August 15, 2012
Dale Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Miaobac - Fayetteville Division
Chloride
33.5
mg/L
7110/12
4:57
JAW
EPA300.0
COD, Total
26.2
mg/L
7/10/12
14:18
DSK
SM 20thEd. 5220 D
Conductivity
229
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
8.00
feet
7/9/12
15:54
DSD
Field Measurement
Nitrate as N
1.15
mg/L
7/10/12
4:57
JAW
EPA300.0
pH, Field Test
3.62
pH Units
7/9/12
15:54
DSD
Field
Total Dissolved Solids
142
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2540 C
Sulfate as SO4
29
mg/L
7/10112
4:57
JAW
EPA300.0
Temperature
28
oC
7/9/12
15:54
DSD
Field
Analyzed by: Miaobac Laboratories, Inc - Ohio Valley
Total Organic Carbon
1.36
mg/L
7/16/12
22:03
DIH
A5310B
r
State Certifications:
Respectfully Submitted
NCDNR kll
NCDOH #37714
USDA k3787
Bonnie K. Sanders, Administrative Assistant
Page 8 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples - 3/Yearly
R-5a
1207159-09
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed try: Mivobac - Fayetteville Division
Chloride
20.7
mg/L
7/10/12
5:13
JAW
EPA300.0
COD; Total
179
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
Conductivity
194
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
7.00
feet
7/9/12
15:59
DSD
Field Measurement
Nitrate as N
6.28
mg/L
7/10/12
5:13
JAW
EPA300.0
pH, Field Test
3.65
pH Units
7/9/12
15:59
DSD'
Field
Total Dissolved Solids
120
mg/L
7/10112
15:19
JAO
SM 20th Ed. 2540 C
Sulfate asSO4
19
mg/L
7/10/12
5:13
JAW
EPA300.0
Temperature
29
°C
7/9/12
15:59
DSD
Field
Analyzed by: Miaobac Laboratories, Inc - Ohio Valley
Total Organic Carbon
1.53
mg/L
7/16/12
22:28
DIH
A5310B
State Certifications:
NCDNR NII
NCDOH 937714
USDA 43787
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
Page 9 of 13

Alleas, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope MillsRd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fact
Certificate of Analysis
Project: M/Wells samples-3/Yearly
R-6
1207159-10
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
44.7
COD, Total
84.4
Conductivity
262
Depth to Water Surface
8.00
Nitrate as N
1.25
pH. Field Test
4.44
Total Dissolved Solids
136
Sulfate as SO4
18
Temperature
28
kelyzed by: Miaobac Labomtodes, Inc - Ohio Valley
Total Organic Carbon
5.15
State Certifications:'
NCDNR #II
NCDOH 937714
USDA 93787
mg/L
7/10112
5:30
JAW
EPA300.0
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
umhos/cm
7/10112
9:30
DSK
SM 20th Ed. 2510 B
feet
7/9/12
16:00
DSD
Field Measurement
mg/L
7/10112
5:30
JAW
EPA300.0
pH Units
7/9/12
16:00
DSD
Field
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2540 C
mg/L
7/10/12
5:30
JAW
EPA300.0
°C
7/9/12
16:00
DSD
Field
mg/L
7/16/12
22:53
DIH
A5310B
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
Page 10 of 13

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd -
Fayetteville, NC 28306
910,864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples - 3/Yearly
R-7
1207159-11
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by., Micrabac - Fayetteville Division
Chloride
46.4
COD, Total
III
Conductivity
198
Depth to Water Surface
8.00
Nitrate as N
0.604
pH, Field Test
4.35
Total Dissolved Solids
134
Sulfate as SO4
5.6
Temperature
26
Analyzed by: Mivobac Laboratories, Inc. - Ohio Valley
Total Organic Carbon
6.76
State Certifications:
NCDNR #II
NCDOH 437714
USDA #3787
mg/L
7/10/12 6:20
JAW
EPA300.0
mg/L
7/10/12 14:18
DSK
SM 20th Ed. 5220 D
umhos/cm
7/I0/12 9:30
DSK
SM 20th Ed. 2510 B
feet
7/9/12 16:01
DSD
Field Measurement
mg/L
7/10/12 6:20
JAW'
EPA300.0
pH Units
7/9/12 16:01
DSD
Field
mg/L
7/10/12 15:19
JAC
SM 20th Ed. 2540 C
mg/L
7/10/12 6:20
JAW
EPA300.0
°C
7/9/12 16:01
DSD
Field
mg/L
7/16/12 23:20
DIH
A5310B
Respectfully Submitted
A
Bonnie K. Sanders, Administrative Assistant
Page 11 of 13

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fav
Certificate of Analysis
Project: M/Wells samples - 3/Yearly
R-8
1207159-12
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac- Fayetteville Division
Chloride
COD. Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
23.6
mg/L
7110/12
6:36
JAW
EPA300.0
115
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
285
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2310 B
- 9.00
feet
7/9/12
16:02
DSD
Field Measurement
13.9
ang/L
7/10/12
6:36
JAW
EPA300.0
4.15
pH Units
7/9/12
I6:02
DSD
Field
172
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2340 C
31
ni
7/10112
6:36
JAW
EPA300.0
29
°C
7/9/12
16:02
DSD
Field '
Analyzed by: Mierobac tabomtories, Inc - Ohio Valley
Total Organic Carbon 1.05
Slate Certifications:
NCDNR #II
NCDOH #37714
USDA #3787
ni 7/16/12 23:46 DIH A5310B
Respectfully SubmitteddA /C p � �
Bonnie K. Sanders, Administrative Assistant
Page 12 of 13

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Allen, Inc
Mr. Reid Wells Project: M/Wells samples - 3/Yearly
5900 Turkey Highway
Turkey NC, 28393
R-9
1207159-13
Date Reported: August 15, 2012
Date Received: July 09, 2012
Date Sampled: July 09, 2012
Sampled By: Derek Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac - Fayetteville Division
Chloride
8.75
COD; Total
241
Conductivity
188
Depth to Water Surface
9.00
Nitrate as N
4.80
pH, Field Test
3.73
Total Dissolved Solids
184
Sulfate as SO4
43
Temperature
30
Analyzed by: Miaobac laboratories, Inc - Ohio Valley
Total Organic Carbon
1.88
Notes and Definitions
mg/L
7/10/12
6:53
JAW
EPA300.0
mg/L
7/10/12
14:18
DSK
SM 20th Ed. 5220 D
umhos/cm
7/10/12
9:30
DSK
SM 20th Ed. 2510 B
feet
7/9/12
16:03
DSD
Field Measurement
mg/L
7/10/12
6:53
JAW
EPA300.0
pH Units
7/9/12
16:03
DSD
Field
mg/L
7/10/12
15:19
JAO
SM 20th Ed. 2540 C
mg/L
7/10/12
6:53
JAW
EPA300.0
°C
7/9/12
16:03
DSD.
Field
mg/L 7/17/12 0:10
U Not detected at or above adjusted sample detection limit
SI Relative Percent Difference (RPD) outside accepted recover limits
State Certifications:
NCDNR #II
NCDOH 937714
USDA #3787
DIH A5310B
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
S1
Page 13 of 13

GW-59A COMPLIANCE REPORT FORM Permit 9 WO Dag
(Submit ane each nlonitariu; period %*h G'IP-59jorms.)
1
Enter date monitoring results were due. -31�13 Will this monitoring report (GW59 and GW-59A)
YES
O
be submitted after the established due date?
2
Was any required information missing on the G`V-59 report forms?
YES
i'
IF the answer to question 1 or 2 is "YES'; list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
identification plate, area overgrown, etc.)? Dim annver is "Yes ", contact the Regional O9icejor guidance.
4
Are any monitored constituents equal to or above the established standards?
YE
NO
If the answer to question 4 is "NO" skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
mw-1 — -row aq.L) M5A
mw-3 — rDs Sa6 Mg/4
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
E
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO" skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
mw-/ l oc so.a ris/L
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answeris "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
YES
� O
groundwater quality problem?
If the answer to question 7 is "YES" describe those actions in the space provided below.
If the answer to question 7 is "NO'; contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subiecf the nermiflee"to a Notice of Violation,
fines, and/or penalties.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form.
Ihereby acknowledge that ,the:above:information:was,evaluated,apd the information submitted in this
report:,(Compliance ReporttGW-59A),is. true and complete,to:the hest of:my.knowiedge.
Signature of Pennittee (or Authorized Agent) Date
(AV-59A 12!S!20113

Ws L4)1 ar
40f _
kI
_M5 h' X3
w3k It of -
Mwnod al 9/K ,
Intl 4D&
M)F'o vI So>eO(L diural Resources
plpg6�j --Information Processing Unit
1617 Mau Serva..
Raleigh, NC 27699-1617
[phone]
NG Up TS r.M OR I ES SINOG
Quality Vegetables
HIGHWAY, TURKEY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone]
(P
RE: Groundwater Quality Monitoring Report
Aliens, Inc. —Turkey, NC Facility
Permit # WQ0004268
Enclosed are the original and one copy of the Groundwater Monitoring Report on forms GW-59
and GW-59A, and the lab report for Aliens, Inc —Turkey, NC facility for samples collected in
July,2012.
Monitoring well # M W-1 exceeded the 1 Omg/L limit for TOC as stated in the permit.
Monitoring well # M W-3 exceeded the 500mg/L limit for TDS as stated in the permit.
These wells will be resampled and results submitted as soon as possible.
If you have any questions or require any additional information, please contact me by
phone at [phone] ext # 104'
Sincerely,
Tim Browers
Plant Manager
Allens, Inc. Turkey facility
CC: Laura Mushinski, Aliens, Inc
Reid Wells, Aliens, Inc —Turkey facility
®Ell it RR —FRO
SPP 0 4 2012
0WC)
Pc E' Vpt)
AUG 3 0 2012
lnformation Processing Unit
DWQ/BOG

�y q1i
V��O � dal &oi(.�,(
h TO
,-�Ni}�a�% re dW r
h�iv' — �edotol lia,
in Y51f�lf� titiDi-{�-,
CQ�� t70hn�ki'
64V `nG Vp MEMORIES SIN08 ry
I
i
Quality Vegetables
,:
5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLZNA, 28393
PHONE [phone]
FAX [phone]
DENR—FRO
JU14 1 1 2012
Dwo
May 24, 2012
Dept, of Environmental & Natural Resources RECEIVED
Division of Water Quality -Information Processing Unit �U 2012
1617 Mail Service Center
Raleigh, NC 27699-1617 Inft=26+w+ ProcewkV Va
[phone] DWOMM
.RE: Groundwater Quality Monitoring Report
Allen, Inc. - Turkey, NC Facility
Permit # WQb004268'
This letter is in response to the Groundwater Monitoring Report dated April 20, 2012 for the Aliens, Inc. -
Turkey, NC facility.
The report showed the TOC levels in Monitoring Wells R-6 and R-7 exceeded the 10 mg1L limit as
specified in the permit.
The two wells were resampled and the results were within the permit requirements. The results are listed on
the following pages.
If you have any question or require any additional information, please contact me by
phone at [phone] ext # 104
Sincerely, - - - - -
Tim Browersf
Plant Manager t 1� To -
Aliens, Inc. Turkey facility �C
CC: Laura Mushinski, Allen, Inc
Reid Wells, Allen, Inc -Turkey

AJ9u lmasiz ,
ONLY
QUALITY MONITORING:
Name: Aliens, Inc. - Turkey
Name (if different):
Address:
NC 28393-9703 County Sampson
act Person: Tim Browers Telephone#: [phone]
Location/Site Name: No.. of wells to be sampled: 2
�rvmcnr a rvXmrrllL nCOVMtt4'Ee
ION OF WATER QUALITY -INFORMATION PROCESSING UNIT ,
MAIL'SERVICE CENTER, RALEIGH, NC 276904817, Phone: (019) 731
',MIT Number: Expiration Date: July 31, 20•
-Discharge W00004268 UIC
3DES Other
TE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Spray field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
LID NUMBER (from Permit): R-6
Date sample collected: 4123/12
FIELD ANALYSES:
AS
Depth: ff.
Well Diameter: _in,
pH Temp.
°C
DRY at
h to Water Level: ft. below measuring point
Screened Interval: ft. to
_units
Spec. Cond.
µMhos
time of
luring Paint is ff. above land surface
_ft.
Relative M.P. Elevation: ff.
Odor
sampling,check
ne of water pumped/bailed before sampling:
gallons
Appearance
here:❑
Ass for metals were collected unfiltered: ❑YES.
❑ NO and field acidified: ❑YES ❑ NO
ORATORY INFORMATION
sample analyzed:
Laboratory Name: Microbae Laboratories
Certification No.
NC#11 NC#37714
4METERS NOTE: Values should reflect dissolved
and colloidal concentratlons.
COD mg/I
Nitrite (NO2) as N mg/I
Pb - Lead
mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N mg/I
Zn - Zinc
mg/I
Coliform: MF Total /100ml
(Note: Use MPH met sifter highlytereidsanplee)
Dissolved Solids: Total
pH (when analyzed)
- units
TOC
7.45 mg/I
Chloride
mg/I
Arsenic
mg/I'
Grease and Oils
mgA
Phenol
mgA
Sulfate_
mq/1
Specific Conductance pMhos
Total Ammonia mg/1
(Ammonla Nllrogen; NHeae N; AmmoNe Nftaen, Total)
TKN as N mg/I
Phosphorus: Total as P
Orthophosphate
mgA
AI -Aluminum
mg/I
Be - Barium'
mgA
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu- Copper
mgA
Fe - Iron
mg/I
Hg - Mercury
mgA
K - Potassium
mgA
Mg - Magnesium
mg/I
Mn-.Manganese
mg/I
Ni - Nickel
mq/I
Other (Specify Compounds and Concentration Units)
JLliy V9 PnI2
info
ORGANICS: (by GC, 44E$ 9 Unit
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method If
method At
. ul• 1111JUCrll I umr vuis: mg1L emuem l oral vUCs: mg/L VOC Removal°
Tim Browers, Plant Manager—,`
Parmlllee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or
GW-59 Rev: V2007

auonnii runny
L.J91W
")I
QUALITY MONITORING:
Name: Allens, Inc. - Turkey
Name (If different):
Address: 5900 Turkey Highway_
It®g
)3 County Sampson
act Person: Tim Browers Telephone#: [phone] I
Location/Site Name: No. of wells.to be sampled: 2
- _ - Iham PemJa
FLING INFORMATION
L ID NUMBER (from Permit): R-7 Date sample collected: 4/23/12
Depth: ft. Well Diameter: In.
h to Water Level: ft. below measuring point Screened Interval: ft. to ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of waterpumped/bailed before sampling: gallons
IF WATER OUALITKINFORMATION PROCESSING UNIT, ,
SERVICE CENTER, RA[EIGH, NC Z7999-461T .P.hone: (919
Number: Expiration Dale: July 31,
harge WQ0004268 UIC
)DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑. Lagoon ' ❑ Remediation: Infiltration Gallery
®-Spray Field ._. _ _� Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump Q Other: -
FIELD ANALYSES:
AS
pH Temp. eC
RY at
_units
Spec. Cond. µMhos
e of
[check
mplin
Odor
Appearance
re:r
Date sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD
mgfl
Nitrite (NO2) as N
mg/I
Pb - Lead _ mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
,mg/I
(Note: Use MPN method for highly tumid samples)
Orthophosphate
mgfl
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
mgfl
AI -Aluminum.
mgfl
pH (when analyzed)
units
Be - Barium
mgfl
TOC
3.69 mg/I
Ca- Calcium
mgA
Chloride
mgfl
Cd- Cadmium
mgfl
Arsenic
mg/I
Chromium: Total
mgfl
Infarryindion
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC,08mM1811 L
Phenol
mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
mg/I
Hg- Mercury
mg/l
Report Attached? ❑ Yes(1) ❑ No(0)'
Specific Conductance
µMhos
K - Potassium
mg/l
VOID , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHsea N:Ammonia NlWgen, Tot¢9
Mn- Manganese
mg/I
,method#
TKN as N
mg/I
Ni -Nickel
mgfl
, method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L Effluent Total VOCs: mo/L VOC Removal%
Tim Browers, Plant Manager
Permutes (or Authorized Anent) Name and Title - Please print or type
GW-59 Rev. 1/2007

e
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc IDate Reported: May 22, 2012
Mr. Martin Griess Project: M/W samples - 3/Yearly, Retest Date Received: April 23, 2012
5900 Turkey Highway__ Date Sampled: April 23, 2012
Turkey NC, 28393 Sampled By: R. Wells
M/W - R-6
1204429-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc -Ohio Valley
Total Organic Carbon 7.45 mg/L 4/30/12 20:51 DiH A5310B
M/W - R-7
1204429-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
Total Organic Carbon 3.69 mg/L 4/30112 21:13 DIH
Notes and Definitions
U Not detected at or above adjusted sample detection limit
Stale Certifications:
NCDNR #11
NCDOH #37714
USDA #3787
A5310B
RECEIVED
JUN $ 2012
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistanl
Page 1 of 1
r

SUBMIT FORM ON YEL Lci PAPER'ONLY- '. .
EPARTMENTOFENVIRONMENt 6N4&1014 RESOURCES
GROUNDW TER QUALITY"MONITORING:
;
NIs10NOF WATER QUALINdNF.ORMQTION PROCESSING UNR -
COMPLIAN E REPORT FORM
017rMAIL SERVIbE CENTER, RABEIGH, NC2785-0617 •leonergS79)7Ja 7P21 * '
RMATION Pease Pnnt Cleady or Type
PERMIT Number. Expiration Date: July 31, 2015
Facility Name:
I Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name ( f different):
Facility Address 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediatlon: Infiltration Gallery
Turkey ig"°`g NC 28393-9703 County Sampson
fc�bl (slam) MP)
Spray Field ❑ Remedlation:
Contact Persoi : Tim Browers
Telephone#: [phone],
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Nile Name:
No. of wells to be sampled: 13
❑Water Source Heal Pump El Other:
ham PonMl
SAMPLING IN -ORMATION
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected: 3/15/12
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH W,09 units Temp. 25 °C
DRY at
Depth to Watei Level: 27 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. µMhos
time of
Measuring Poi`t is ft, above land surface
Relative M.P. Elevation: ft.
Odor
sampling,
check
Volume of watt•r pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for m tals were -collected unfiltered: ❑YES
❑ NO and.field acidified: ❑ YES ❑ NO
LABORATOR"
INFORMATION
Laboratory Name: Mlcrobac Laboratories Certification No. NC#11 NC#37714
Date sample analyzed:
PARAMETER.
NOTE:'Values should reflect dissolved and colloidet concentratlons.
coo 122 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Colifor
: MF Fecal /100ml
Nitrate (NO3) as N 4.04
mg/I
Zn - Zinc mg/l
Colifor
MF Total /100ml
Phosphorus: Total as P
mgA
(Note: Ue
MPN method for highly Ndtid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved
olids:Total 435mg/I
AI - Aluminum
mgA
pH (when
analyzed) units c Be - Barium
mg/I
TOC 4.32 mg/I
r� Calcium
��Od-v`,Oafimjum
mg/I
Chloride 207mg/l
Arsenic
PR
5
mg/I
b° Diu Cooppper
Gre
1710mg/l
se and Oils mP'rorrgarion Pr L>u
mgA
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mgA
r
Ow U Fe - Iron
QQG
mg/I
(Specify test and method M ATTACH LAB REPORT.)
_
Sulfate 39 mg/I
Hg 3rtercury
mgA
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
812 µMhos
K - Potassium
mg/I
VOC , method #
Tot
I Ammonla mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia
1hogen; 14143ea N; AmmoNa Nitrogen, Total)
Mn -Manganese
mg/1
,method #
TKN as N mg/I
NI - Nickel
mg/I
, method #
4

For
MONITORING:
Name:' Aliens,Inc.-Turkey
Name (If different):
Address: 5900 Turkey Highway
5geetl
:Y NC 28393-9703 County Sampson
act Person: Tim Browers TelephoneM 910-596-0028
Location/Site Name: No, of wells to be sampled: 13'
1
(from Pemin
PLING INFORMATION
LID NUMPER (from Permit): MW-2 Date sample collected: 3/15112
Depth: ft. Well Diameter: In.
h to Water Level: 8.5 ft. below measuring point Screened Interval: _ft. to _ft.
luring Point is ft. above land surface Relative M.P. Elevation: _ ft.
me of water pumped/bailed before sampling: 10+ gallons
sample
COD
113 mg/I
Coliform: MF Fecal
/100ml
Coliforp: MF Total
/100ml
(Nola: Use MPN method for highly turbid samples)
Dissolved Solids: Total
206 mg/I
pH (when analyzed)
units
TOO
4.54 mg/1
Chloride
90.3 mg/I
Arsenic
mg/1
_
Grease and Oils _
mgA
Phenol
mgA
Sulfate
9.2 mgA
Specific Conductance
I
399 µMhos
Tot$I Ammonia
mg/I
(Ammonla longer; NNeas N; AmmoNa Nitrogen. Total)
TKN as N mgA
Plant
:RM1T Number: Expiration Date: VUly :5„_
in -Discharge WQ0004268 UIC
?DES Other I
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Applicati Dn of Sludge
❑ Water Source Heat Pump ❑ Other:.
FIELD ANALYSES:
pH %% its Temp. 25
Spec. Cond. .µMho,
Odor
Appearance
Laboratory Name: Microbac Laboratories
Certification No. NC#111
NC#37714
colloidal concentrations.
Nitrite (NOz) as N
mg/I
Pb - Lead mg/I
Nitrate.(NO3) as N
1.14 mg/I
Zn - Zinc mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mg1l
Other (Specify. Compounds and Concentratio
i Units):
AI -Aluminum
mg/I
Be - Barium
mgA
Ca - Calcium
mg/I
Cd - Cadmium
mg/1
Chromium: Total
mg/1
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
I -
.. 'Fe - Iron
mgA
(Specify test and method #. ATTACH LAB
Hg -'Mercury
_ mg/1
111REPORT.)
Report Attached?. ❑ Yes (1) ❑
No (0)
K - Potassium
mg/I
VOC , method #
Mg - Magnesium mgA
Mn - Manganese mg/I
NI - Nickel mgA
method #
method #
method #
at
Of
.nF
GW59 'Rev. 112007

t
SubMITFORM ONYELI 01K PAPER ONLY. - <-
GROUNDWATER QUALITY MONITORING:
� .
EPARTMENT t1E.ENYIRQIjNENTrS, NATURAL RESOURCE
COMPLIANCE REPORT FORMu
ee
nnsloR�,�nTE�bnLm�t141oRaedtloNh�ocEss7N�u�t�t
tiq� seRulcB LteR,�(nieioHxxc'stsee+sar P
o�ertsgetrsaa7gt , _e
FACILITY INFORMATION Please Print /eady or Type
PERMIT Number: Expiration Date: IJuly`
31, 2015
Fatuity Name: i Aliens, Inc. -Turkey
Non -Discharge WQ0004268 UIC
Permit Name (if different):
NPDES Other
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
w)
Turke st,NC 28393-9703 County Sampson
❑ Lagoon El Remediation:
nfiitration Gallery
(cM)t ts,�iet 00 -
® Spray Field ❑ Remediation:
of Sludge
Contact Person: Tim Browers Telephone#: [phone]
❑ Rotary Distributor ❑ Lend Application
ell Location/Stle Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
Rom Pemtlr
SAMPLING INFORMATION
I
If WELL
ELL 10 NUN BER (from Permit): MW-3
Dale sample collected: 3/15112
FIELD ANALYSES:
AS
Well Depth: ft.
Well Diameter:
pH TA9-1untts Temp. 26
1 C
DRY at
Depth to Wate(.Level: 4 ft. below measuring point
_in.
Screened Interval:
_ to
Spec. Cond. µMhos
time
_ft.
_ft.
sampling,
Measuring Poi0t is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumpediballed before sampling:
10+9allons
Appearance
here:❑
Sam Ies for metals werecollected unfiltered: ❑YES
❑ NO and: field acidified: ❑YES
❑ NO
LABORATORY INFORMATION
-
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11
NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 100 mg/I
Nitrite (NOZ) as N
mg/I
Pb -Lead mg/I
Coliforin:MFFecal /100ml
Nitrate .(NO3).asN
0.713mgA
Zn-Zinc - mgil
'
Coliform: MF Total /loom]
Phosphorus: Total as P
mg/]
(Note: Ue4 MPNmathotlfor hipNy turbid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentratio
i Units):
Dissolved Solids: Total 361 mg/I
AI - Aluminum
mgll
-
pH (whin analyzed) units
Be -Barium
mg/l
-
TOO 2.87 mgll
Ca - Calcium
mg A
Chloride 94.2 mg/I
Cd - Cadmium
mg/i
Arsenic mgA
Chromium: Total
mgA
Grease and Oils mg/I
Cu - Copper
_. mgA
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iran
mg/I
(Specify test and method #. ATTACH LAB
EPORTJ
Sulfate'. 55 mgll
Hg - Mercury
mgA
Report Attached? ❑ Yes (1)
qo (0)
Specific Clonductance 496 µMhos
K- Potassium
mgA
VOC , method#
Tot;l Ammonia mgll
Mg - Magnesium
mgA
, method #T
(Ammonia Ilmpen: NMrea N; Ammonia NlRopan, Toteq
Mn - Manganese
mgA
, method #
TKN as N. mg/1
Ni - Nickel
mg/I
—TI
, method #
--
I
For Remediat(on,SystemsOnty (Attach Lab Reports):... Influe1. nt TotaI;VOCs: -_ mall. .Effluent Total VOCs: ma/L VOCIRernoval%
Tim Browerg, Plant Manager �,,,., \54d,,,,v 112zI I2
GW-59 Rev. 1/2007

GROUNDWATER QUALITY MONITORING: e
COMPLIANCE REPORT FORM
tpjsroHnArrquulry�NoRrwATroNPoessMuyT
et%f�Ai�sitRYtcNtER,paF7cH;Noiiaf> t41r,Pong
�xfi
(alsjvaia:ia x:
FACILITY INFORMATION Please Pdnt C)eady or Type _
Facility Name:' Aliens, Inc. - Turkey
PERMIT Number: Expiration Date:
Non -Discharge WQ0004268 UIC
WU1y 31, 2015 _
Permit Name (if different):
NPDES Other
Facility Address: 5900 Turkey Highway
TurkeyNC 28393-9703 County Sampson
-- :cMr - ISiate) lost -
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation:
®.Spray Field -❑ Remediation:
nflitration Gallery
Contact Person: Tim Browers Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application
of Sludge
Well Location/ its Name: No. of wells to be sampled: 13
❑ Water Source Heat Pump ❑ Other:
ham PenNl
SAMPLING IN�ORMATION
WELL ID NUMBER (from Permit): MW-4 Date sample collected: 3115/12 FIELD ANALYSES:
If WELL
WAS
Well Depth: ft. Well Diameter: _in. pH Q5V8J- Il nfts Temp. 24
Depth to Walel Level: 9 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. µMhos
Measuring Poiet is ft.. above land surface .Relative M.P. Elevation: — _ ft. Odor
Volume of water pumped/bailed before sampling: 10+gallons Appearance
Samples for metals were.collected unfiltered: OYES ❑ NO and field acidified: ❑ YES ❑ NO
C
I
DRY at
time of
sampling,
check
here: ❑
Date sample is talyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#1j1
NC#37714
PARAMETERS. NOTE: Values should reflect dissolved
and colloidal concentrations.
COD
114 mg/I
Nitrite (NO2) as N
mgA
Pb -Lead mg/I
Coliform: MF Fecal
/loom[
Nitrate (NO3) as N
4.84 mgll
- Zn - Zinc mgA
Coliform: MF Total
/looml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly lmEld samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentratio
i Units):
DissolvedSolids:Total
100.mg/I
AI - Aluminum
mgA
pH (when analyzed)
units
Be -Barium
mg/l
TOO
4.94m9A
Ca - Calcium
mg/I
Chloride
24.5 mgA
Cd - Cadmium
mg/l
I
Arsenic—mgA
Chromium: Total
mgA
Grease and Oils
mgA
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/l
.. Fe - Iron
mgA
(Specify test and method #. ATTACH LAB
�L`EPORT.)
Sulfate.
5.4 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑
No (0)
Specific Conductance
170 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mgA
method # �—
(AmmaNe�ihogen: NHaea tTAmmonle Nitrogen, Total)
,
Mn - Manganese
mg/1
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remedlation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L.: Effluent Total VOCs: _ moll. VOCIRemoval%
TmimBower$,dPdlant Manager
ittAuth Agent) Name and Title- Please print or type
GW-59 Rev. 1/2007

7-
,SUBMIT FORM 'ON YELLOW PAPER ONLY
DEPIARTMENTPOEENVIRONMENTv&'NATURAQFtESOURCES;
'I,'
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
t$1Z,.MAfLSW1RVICE CENTER RACEIGH,'96476994817- Phone:
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date:
July 31, 2015
Facility Name: Aliens. Inc. -Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (I! different):
infiltration Gallery
Facility Addresp: 590OTurke y Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
El Lagoon 11 Remediation:
sVocq - NC 28393-9703 County Sampson
Turks
KI Spray Field 0 Remediation:
I on of Sludge
Contact Persoq: Tim Browers Telephone* 910-596-0028
El Rotary Distributor 11 Land Applicati
Well Location/Site Name:
I
No. of wells to be sampled;
13
❑ Water Source Heat Pump El Other:
7—mp,mtlo
SAMPLING INFORMATION
It WELL
WELL ID NUM BER (from Permit): R-1
Date sample collected: 3/15112
FIELD ANALYSES:
WAS
'
Well Depth: ft.
Well Diameter:
In.
pH `6�_12units Temp. 26
Ic
DRY at
Depth to Water Level: 5 ft. below measuring point
Screened Interval:
ft. to
ft. Spec.Cond. AMhos
time of
sampling,
Measuring Point Is -ft. above land surface
Relative M.P. Elevation:
-ft.
Odor
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals werebollected unfiltered: EIYES
11 NO and field acidified: EIYES
El NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#111
NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 276 mgfl
Nitrite (1,102) as N
mg/I
Pb - Lead mg/I
Coliforrn: MF Fecal /100ml
Nitrate (NO3) as N
0.830 mg/1
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentratic
i Units):
Dissolved Solids: Total 83 mg/i
AI -Aluminum
mgn
pH (when analyzed) units
Be - Barium
mgn
TOC 6:30 ni
Ca - Calcium
mgn
Chloride 15.5 mgll
Cd - Cadmium
ing/I
Arsenic mg/I
Chromium: Total
mg/i
Grease and Oils. mg/I
Cu - Copper
ing/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method A ATTACH LAB
REPORT.)
Sulfate 12 mgn
Hg - Mercury _mg/I
Report Attached? El Yes (i) El
0(0)
Specific Conductance' 102 IiMhos
K - Potassium
-mg/I
VOC method#
Total Ammonia _mg/I
Mg - Magnesium
mgn
method #
(Ammonia Nluoijen; '113as N; Ammonia 1,11mgen, Total)
Mn - Manganese _mg4
method #
TKN as N mgn
Ni - Nickel
mgA
method #
For Remedlietion Systems Prily (Attach Lab Reports): _. Influent TqtalVOqs: _mg/L Effluent Total VOCs: mg/ I - Reports): 1 L VOCIRemoval%
Tim Browers, Plant Manager
Pormiltee (Or Auth ' prized Agent) Name and Title - Please print or type
GW-59 Rev. 112007

„SUBMIT FORMON'YELIS%WrPAP,ER ONLY - .+ - -.-S :..
-'
GROUNDWTER QUALITY MONITORING:isirFYAreRaupuzabtzt+ATmNocessw�um
"`�`--"'"”? .
EPARTp1ENT OF ENVI)tONMENI;-b NA7URALRE50URCE5� � ,, 7
COMPLIANCE,REPORT FORM1+AILaERycEttTRRRYAEI0f1Tlh27cssaetnb3(ataf>>32�t
?�
PERMIT Number: Expiration Date: Uul" 31, 2015
FACILITY INFORMATION Please Pdnt Clearly or Type --
Facility Name: Aliens, Inc. -Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Addresa: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
s rears
TurkeyNC 28393-9703 County Sampson
❑ Lagoon ❑ Remediation: nfiltration Gallery
1
(SW.) Opt
® Spray Field ❑ Remediation:
Contact Person: Tim Browers
Telephone#: [phone]
❑ Rotary Distdbutor El Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled: 13
❑ Water Source Heat Pump ❑ Other:
I
ham PenNl
SAMPLING INFORMATION
If WELL
WELL ID NUMPER (from Permit): R-2a
Date sample collected: 3115112
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
pH g4189�units Temp. 25
C
DRY at
Depth to Water Level: 5 ft. below measuring point
— ft.
Screened Interval: _ft. to
_ft.
Spec. Cord. µMhos
time of
n
sampling,
P g,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of watelr pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were.collected unfiltered: DYES
El NO and field acidified: ❑ YES ❑ NO
-
LABORATORY INFORMATION
NC#1I1
NC#37714
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No.
PARAMETER NOTE: Values should reflect dissolved and colloidal concentrations.
COD 31.7 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Colifo7: MF Fecal /100ml
Nitrate (NO3) as N 0.686
mg/I
Zn - Zinc mg/1
ColifwIn: MF Total /100ml
Phosphorus: Total as P
mgA
(Note: Use, MPNe»tnodfor his* turbid samples) -
Orthophosphate
mgA
_Other(Specify Compounds and Concentratio
i Units): -
Dissoived Solids: Total 88 mgA
At - Aluminum
mgA
pH (when analyzed) units
Be - Barium
mgA
TOC 1.92 irl
Ca - Calcium
mgA
Chloride 10.4 mg/I
Cd - Cadmium
mgA
Arsenic mgll
Chromium: Total
mgA
_ _
Grease and Oils mgll
_
Cu - Capper
mg/1
ORGANICS: (by GC, GC/MS,-HPLC)
Phenol mgll
-Fe - Iron
mgA
(Specify test and method #, ATTACH LAB
EPORT.)
Sulfate 37 mg/I
Hg - Mercury
mgA
Report Attached? ❑ Yes (1) El�o
(0)
Specific Conductance 155 µMhos
K - Potassium
mgA
VOC , method #
Tot I Ammonia mg/I
Mg - Magnesium
mgA
, method #
(Alnmaala�itmgen:NH,aaN,AmmohiaNitrogen, Total)
Mn- Manganese
mgA
,method#
TKN as N . mg/I
NI - Nickel
mgA
, method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs,,mg/L
Effluent Total VOCs: - mglL VOCIRemovai%
I certify hal, tolhe'bcsl of my knovledge and belief, the irdonnal6n submitled
DWO-cerblied laboratory. I ainaware that there are enlniboant ponanies
in 1111S report is true, accurate, and complete, and that the
far SUbIldring false inforninflon.inchiding 1he possibilityof fines
laboratory
and
analytical data was produced tisilig approved inefilods of analysis
lint,ftonment for knonving violations.
by a
V
2-
GW-5a 'Rev. 1/2007

�,'iSUBtd1T FORM ON�YELLOW PAPER ONLY_;
I
GROUNDWATER QUALITY MONITORING-
. .
EP TMENTOF„£'Nyl o MENT14 NAhm—BOURCE
tikw!AT lA�rv,4�FQR�Anbigij r4i4
b
� �
�A910
COMPLIANCE REPORT FORM
a1�nat9EBvlc£o LATER ruLrot+;e;2taes+,afzt phonelata}zaaas7
FACILITY INFORMATION. Please Print Clearly or Type
PERMIT Number: Expiration Date:
JUI"31, 2015
Facility Name:! Aliens,Inc.- Turkey
Non -Discharge W00004268 UIC
Permit Name (if different):
NPDES Other
FacilityAddress: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MON'TORED
Turke tseeeg NC- 28393=9703 County Sampson
El Lagoon ❑ Remediation: Infiltration
Gallery
Spray Field' ❑ Remediation:
n of Sludge
Confect Person: Tim BroWerS Telephone#: [phone]
❑ Rotary Distdbutor ❑ Lend Applicati{
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
ea PonNt
SAMPLING INFORMATION
If WELL
WELL IDNUM .BER (from Permit): R-3
Date sample collected: 3/15/12
FIELD ANALYSES:
WAS
Well Depth: ' ft.
Well Diameter:
in.
pH 5 1 units Temp. 26
C
DRY at
Depth to Water Level: 6.6 ft. below measuring
p g point
Screened Interval:
ft. to
- Mhos
ft. Spec. Cond. µ
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P.,Elevation:
ft.
Odor
check
olumaofwater pumped/balled before sampling:
10+gallons
-
Appearance
here:❑
Sam les for metals were collected unfiltered: ❑YES
❑ NO and: field acidified:. ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
- Laboratory Name: Microbac Laboratories Certification No: NC#11
NC#37714
PARAMETERS NOTE( Values should reflect dissolved and colloidal concentrations.
COD 123 mgn
Nitrite (NO.)as N
mg/I
Pb- Lead mgn
Coliform: MF Fecal /loom]
Nitrate (NO3) as N
0.742 mg/I
Zn - Zinc mg/1
Coliforjn: MF Total /loom[-
Phosphorus: Total as P
mg4
-
(Note: use tnPN moUoafor highly wmla samples)
Orthophosphate,
mg/I
Other (Specify Compounds and Concentration
Units):
Dissolved Solids: Total 92 mg/1
At - Aluminum -
mg/I
..
pH (when analyzed) units
Be - Barium
mg/I
TOC 1.45mgn
Ca - Calcium
mg/I
Chloride 45.3 mg/1
Cd-Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mgn
Greiise and Oils _ mg/I
Cu - Copper
mg4
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg4
(Specify test and method #. ATTACH LAB
EPORT.)
Sulfate 17mg/I
Hg- Mercury -..
mg/l
Report Attached? ❑ Yes,(1) ❑
o(0)
Specific Conductance 222 µMhos
K - Potassium
mgA
VOC , method #
Toti I Ammonia mg/I
Mg - Magnesium
mgn
, method #
(Ammonie;llaogen; NH,as N: Ammonia Nitrogen, Total
Mn- Manganese -
mgn
,method#=
TKN as N mg/I
Ni - Nickel
mgn
, method #
For
Tim
OW-59 Rev. 112007

SOBMIT FORM ONYELL0INPAPER,ONBY
.-t1;11111ES1=
IMPAI ITMENTOFENVIRONMENT�NNATOMLRESOURCES�'
GROUNDWATER QUALITY MONITORING:
DIVISIOtiOF, rxATERQUALITvgNEORMATIONPROFasINIT
COMPLIANCE REPORT FORM
elf MAILSERVICE(919173a4Z2 CENTER,RALEiQNNczigsatetT:Pbono:1I
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: � Aliens, Inc. -Turkey
Non -Discharge ' W00004268 UIC
NPDES Other
Permit Name (If different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon El Remediation: Infihration Gallery
Turks (Strvc' NC 28393-9703 County Sampson
rcm(Sm.) (Do -
® Ell,.
Spray Field Remediation:
Contact Person: Tim BroWers
Telephone#: [phone]
❑ .Rotary Distributor ❑ Land Applicatii n of Sludge
Well LocatlonTte Name:
No. of wells to be sampled:
13
El Water Source Heat Pump ❑ Other:
Tom P.11
IDN
If WELL
ELL ID NU BER (from Permit): R-4
Date sample collected: 3/15/12
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
pH .80 unfts Temp. 25
C
DRY at
Depth to Water Level: 7 ft. below measuring point
_In.
Screened Interval: _ft.
to _ft.
Spec. Cond. µMhos
time ofsampling,
Measuring Point is ft. above land surface
Relative M.P.-Elevation:
ft.
Odor
check
Volume of water pumped@ailed before sampling:
10+ gallons
Appearance
I
here:
for In were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
ElSamples
LABORATORY INFORMATION
Date sample analyzed.
Laboratory Name: Microbac Laboratories Certification No. NC#1I1
NC#37714
PARAMETER NOTE: Values should reflect dissolved and colloidal concentrations.
COD 96.1 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal llooml
Nitrate (NO3) as N
3.72 mg/I
Zn - Zinc mg/1
Coliform: MF Total -/loom[
Phosphorus: Total as P
_ mgll
(Note: Uea MPN method for hipNyluNitl samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentratlor_Units):
Dissolved Solids: Total 164 mg/I
At -Aluminum
mg/I
i
pH (whyn analyzed) units
Be - Barium
mgA
I
TOC 3.52 mg/l
Ca - Calcium
mgA
Chloride 49.3 mg/I
Cd- Cadmium
mg/I
Arsenic mgA
Chromium: Total
mgA
Grepse and Oils mgA
Cu - Copper
mgA
ORGANICS: (by GC, GCIMS, HPLC)
Phenol mg/I
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB
Sulfate 18mg/I
Hg-Mercury
mgA
Report Attached? ❑ Yes.(1) ❑
rRRr--eePORT.)
Plo(o)
Specific Conductance 279 µMhos
K - Potassium
mgA
VOC , method #
Tot I Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Ptmgen; NH°as N; AmmoNo Nitrogen, Total)
Mn- Manganese
mg/I
,method#
TKN as N mg/I
Ni - Nickel
mgll
, method #
For Remedlatjon Systems -Only (Attach Lab Reports):
InfluentTolal VOCs:
mg/L Effluent Total VOCs: mgA- VOC
Removal%
I ce, Iffy that, 1. thobest of any knowledge and beliefi it ie information submilled
owacarthiedlab&atory. I ain maire Ilia there an, sionlricaril r)enajt;es
In [his opot I is latoi accurate, and complete,
for subunming false 41formition, fincludino tile possibility
slid that tile lAboralory
of fine.% and Imprisonment
analytical dala vras produced tieung opproved nnelhods of analysis by a
for knowiral violatio.s.
Tim Browers, Plant
GW-59 Rev. 112007

MONITORING:
Names Aliens; Inc. -
Name (if different):
Address: 5900 Turkey Highway
y , (SeeB) NC 28393-9703 County Sampson
act Person: Tim Browers Telephone#: [phone] I
Location/Sits Name: No. of wells to be sampled: 13
(hom PertNg
L ID NU BER (from Permit): R-5a Date sample collected: 3/15/12
Depth: ft. Well Diameter: _in.
h to Wale( Level: 5 ft, below measuring point Screened Interval: —ft. to —ft.
wring Point is ft.•above land surface Relative M.P. Elevation: _ ft.
ne of watgr pumped/bailed before sampling: 10+ gallons
Number: Expiration Dale:
;harge W00004268 UIC
Other
'PE OF PERMITTED OPERATION BEING MOD
El Lagoon ❑ Remediation:
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ land Applica
❑ Water Source Heat Pump ❑ Other: _
FIELDANALYSES:
pH D?u_Ils Temp.
Spec. Cond.
Odor
Appearance
Gallery
of Sludge
ymple ahayzed: Laboratory Name: Microbac Laboratories Certification No. NC#111 NC#37714
AETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 82.8 mgll Nitrite (NO2) as N mg/I Pb - Lead mg/1
Colifor/n: MF Fecal /100m1 Nitrate (NO3) as N 6.82 mg/I Zn - Zinc mg/I
Colifop: MF Total /100ml Phosphorus: Total as P mgA.
(Note: Us? MPNmethodforhighly turbid eemplea) Orthophosphate mgA Other (Specify Compounds and Concentraft Units):
Dissolved Solids: Total
126 mgn
pH (when analyzed)
units
TOO
3.52 mg/l
Chloride
17.6 mg/I
Arsenic. _
mgA
Grasse and Oils
mgA
Phenol
mg/I
Sulfate
-23 mg/l
Specific Conductance
201 µMhos
Total Ammonia
mgA
(Ammonia �Itmgen; NHeas N; Ammanle Nitrogen, TOW
TKN as N mg/I
For
Tim Browers. Plant
AI - Aluminum
mg/I
- Be -Barium
mgA
Ca - Calcium
mg/I
Cd- Cadmium
mg/l
Chromium: Total
mgll
_
Cu- Copper
mgA
Fe - Iron
mgA
Hg- Mercury
mgA
K- Potassium
mg/I
Mg - Magnesium
mg/l
Mn - Manganese
mgll
Ni - Nickel
mgll
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB EPO
Report Attached? ❑ Yes (1) ❑ o (0)
VOC , method #
method #
method #
method #
at
of
GW-59 Rev. 1/2007

For
TER
Name: Aliens
Name (if different):
Address: 5900 1
TY MONITORING:
FORM
Inc. -
County Sampson
act Person: Tim Browers Telephone#: [phone]
Location/Site Name:. No. of wells to be sampled: 13
!RMIT Number:
Expiration Date:
m-Discharge W00004268
UIC_
IDES
Other _
'PE OF PERMITTED OPERATION BEING MW
❑ Lagoon
❑ Remediation:
® Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Applica'
❑ Water Source Heat Pump
❑ Other: _
L ID NUMBER (from Permit): R-6 Date sample collected: 3/16/12 FIELD ANALYSES:
Depth: ft. Well Diameter: — in. pH ' d JQriils Temp. 24
h to Water Level: 7 ft. below measuring point Screened Interval: _ft. to _ft. Spec. Cond. µMho,
luring Point is ft. above land surface Relative M.P. Elevation: ft. Odor
ne of water pumped/bailed before sampling: 10+ gallons Appearance
COD 125 mg/I
Coliform: MF Fecal _ /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
156 mg/I
pH (when analyzed)
units
TOC
k1AG mgll
Chloride
38.8 mgA
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/l
Sulfate
26 mg/I
Specific Conductance
233 µMhos
Total Ammonia
mg/I
(Ammonia Nitrogen; NHras N; Ammonia Nitrogen, Total)
TKN as N
ri l
Lab
Laboratory Name: _ Microbac Laboratories
colloidal concentrations.
Nitrite (NO2) as N
mg/I
Nitrate (NOa) as N
1.20 mg"
Phosphorus: Total as P '
mgA
Orthophosphate
mg/I
AI - Aluminum
mg/I
Be - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mgA
Cu - Copper
mgA
Fe - Iron
mgA
Hg - Mercury
mg/I
K - Potassium
mgA
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni- Nickel
mgA
Gallery
of Sludge
Certification No. NC#11 NC#37714
Pb - Lead mg/I
Zn - Zinc mg/l
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB EPO
Report Attached? ❑ Yes (1) ❑ o(0)
VOC , method #
method #
method #
method #
Tim Browers, Plant Manager
Penalties (or Authodzed Agent) Name and Title - Please print or type Signature of Permlttee (or Authorized Agent
GW-59 Rev. 112007
at
of
n

SUBMIT FORM ON YELLQipL PAPER ONLY_:L-
'OF�E�VIRCxMENT&F1ATU(ZntS.RE$OURCE�,
GROUNDWATER QUALITY MONITORING:
ivstbNoFwn itti6ttraNFoarirlOxtocEsf�
�xrc
COMPLIANCE REPORT FORM
d±tttpmLSavic@N„T,Ea,t}Ai�cHrrxs"ilea"ietr, pon'a`•(easy
FACILITY INFORMATION Please Pdnt Cleady or Type _
PERMIT Number: Expiration Date:.
Oui" 31, 2015
Aliens, Inc. - Turkey Facility Name:- Y
Non -Discharge W00004268 UIC .�
Permit Name (If different):
NPDES Other
RED
llration Gallery
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONjTnfi
❑ Lagoon El Remedialion:
Turke rs1eB0 NC 28393-9703 County Sampson
(cry), (sia,a) (ZIP)
® Spray Field ❑ Remediatian:
Contact Persor+: Tim Browers
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application
of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
El Water Source Heat Pump El Other:
rom 6m
SAMPLING INFORMATION
If WELL
WELL ID NUM .PER (from Permit): R-7
Dale sample collected: 3/15112
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
pH c4_I7 Its Temp. 25
C
DRY at
Depth to Water Level: 7 ft. below measuring point
_in.
Screened Interval:
ft. to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
-Odor
check
Volume of water pumped/bailed before sampling:
10+ gallons
_ _
Appearance
here: ❑
Samriles for metals were collected unfiltered: ❑YES
❑ NO and field acidified: OYES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
"
Laboratory Name: Microbac Laboratories Certification No. NC#11
NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 163 mg/I
Nitrite (NO,) as N
mgA
Pb - Lead mg/l
Colifor(n: MF Fecal /100ml
Nitrate (NO3) as N
1,02 mg/I
Zn - Zinc mgA
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Il MPN method for highly turbid mmpies)
Orthophosphate
mgA
Other (Specify Compounds and Concentratio
i Units):
Dissolved Solids: Total 141 mg/I
AI -Aluminum
mgA
PH (whin analyzed) units
Be - Barium
mgA
TOC [i—
Ca - Calcium
mg/I
Chloride 47.9 mg/1
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mgA
Cu - Copper
_ _.. mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1
Fe -.Iron
mgA
(Specify test and method #. ATTACH LAB
EPORT.)
Sulfate 7.8 mgA
Hg - Mercury
mg/l
Report Attached? ❑. Yes (1) ❑
o (0)
Specific Conductance 208 µMhos
K - Potassium
mgA
VOC , method #
Total Ammonia mgll
Mg - Magnesium
mg/I
method #
(Ammonia �Itropen; NH, es N. AmmoNs Nitrsaen, Tatee
Mn -Manganese
mg/l
,
,method #
�
TKN as N mg/l
NI - Nickel
mgA
, method #
For
GW-59 'Rev. 112007

TY MONITORING:
FORM
Name:' Aliens, Inc. -
Name (if different):
Address: 5900 Turkey Highway
:y a"°`0 INC 28393-9703 county Sampson,
Person: Tim Browers Telephone#: [phone]
:ation/Site Name: No. of wells to be sampled: 13
Number: Expiration Date:
harge . WQ0004268 UIC_
'DES . Other —
PE OF PERMITTED OPERATION BEING MOh
❑ Lagoon ❑Remediation:
® Spray Field. ❑ Remediation:
❑ Rotary Distributor ❑ Land Applical
❑ Water Source Heat Pump ❑ Other: _
L ID NUMPER (from Permit): R-8
Date sample collected:
3/15/12
FIELD ANALYSES:
Depth: ft.
Well Diameter:
_in.
pH 'Vig'un1ts Temp. 26
h to Water; Level: 8 ft. below measuring point
Screened Interval:
_ft. to
_ft. Spec. Cond. µMhos
ng Point is ft. above land surface
of water pumped/balled before sampling: 10+
Relative M.P. Elevation: ft.
Odor _
Appearance
Gallery
of Sludge
at
of
Date sample analyzed: V
Laboratory, Name: Microbac Laboratories
Certification No. NC#1
NC#37714
PARAMETERS NOTE: Values should reflect dissolved
and colloidal: concentrations.
COD
147 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/loom[
Nitrate (NO3) as N
„ 16 mg/I
Zn - Zinc mg/I.
Coliform: MF Total
/loom[
Phosphorus: Total as P
mg/l
(Nate: UaejMPN meMedfor highly Wrbitlsemples)
_
Orthophosphate
mgA
Other (Specify Compounds and Concentration
Units):
Dissolved Solids: Total
180mgn
AI -Aluminum
mgA
pH (when analyzed)
units
Be -'Barium
mg/l
TOC
2.90 mgA
Ca - Calcium
mgA
Chloride
18 mgA
Cd - Cadmium
mgA
Arsenic
mgA
Chromium: Total
mgA
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB
REPORT.)
Sulfate
19 mgA
Hg - Mercury
mgA
Report Attached? ❑ Yes (1) ❑
No (0)
Specific Conductance
270 µMhos
K- Potassium
mgA
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mgA
, method #
(Ammonie Mibcgen; N%es N;AmmoNe Nltmgen, To[a9
Mn- Manganese
mgA
;method #
TKN as N
mgA
Ni - Nickel
mgA
, method #
For Remedlatlon Systems Only (Attach.LabReports):
Influent Total VOCs:
mg/L __ -Effluent Total VOCs: mg/L, VOC
Removal%
Tim Browers, Plant Manager ­1Z 4hA I(rz
Permittee(or Authorized Agent) Name and Title- Please prinlgr type Signature of Permlltee(or Authorized Agent) - (late)
GW59 Rev. 112007 .

SU6MIT FORM ONYEu.od[PAPER ONLY=
ee
EPARTMEt(TOF ENy1RONMENI`6 iURALRE56URCE9,.�
't
GROUNDWATER QUALITY MONITORING:
-1
>v%sl64i)FW i�a611AU 40'-taArror Pr�ocesaw00rvr
�
COMPLIANCE REPORT FORM
�e
e
lraae�i FtyylCeoEN1EdRato�t�yi7s�g`tearroo;tais)7aaezi„�,�
FACILITY INFORMATION Please Print Cleady or Type -
PERMIT Number: F_upiration Date:
Oul31, 2015
Facility Name:' Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
Permit Name (if different):
NPDES Other
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
TurkeyNC 28393-9703 County Sampson
❑ Lagoon ❑ Remedlatipn:
nfiltration Gallery
ish0c) - (zc)
® Spray Field. ❑ Remediation:
_
Contact Person: Tim Browers-
= Telephone#:. [phone]
❑ Rotary Distributor ❑ Land Applicati6n
of Sludge
Well Location/Site Name:
No, of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
from PemN
SAMPLING INFORMATION
I
If WELL
ELL ID NUM)BER (from'Permit): R-9
Date sample collected: 3115/12
FIELD ANALYSES:
AS
Well Depth: ft.
Well Diameter:
pH 443-units Temp. 24
1 C
DRY at
Depth to Water, Level: 8.7 ft. below measuring point
_in,
Screened Interval: _ft.
to _ft.
Spec. Cond: µMhos
-
time of
sampling,
Measuring Pofr?t is _ ft. above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
El
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑YES
❑ NO
LABORATORY INFORMATION
Date sample jayzed:
- -
Laboratory Name: Microbac Laboratories Certification No. NC#1I1
NC#37714
PARAMETER, NOTE: Values should reflect dissolved and:eolloldal'eoncentratlons.
COD 409 mgA
Nitrite (NO.) as N
mgn
Pb - Lead mg/I
Colifor(n:-MF Fecal 1100ml
Nitrate (NO3) as N
4.34 mg/i
Zn - Zinc mg/I
Coliforp: MF Total /loom[
Phosphorus: Total as P
mgA
(Note: Uee MPN method for highly turbid samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentratiop
Units):
Dissolved Solids; Total 129mg/I
AI -Aluminum
mg/l
pH (wh7n analyzed) units
Be - Barium
mgn
TOC 3.61.mgn
Ca - Calcium
mg/I
_
Chloride 6.31 mg/l
Cd- Cadmium
mg/I
_
Arsenic mg/I
Chromium: Total
mgA
Grease and Oils mg/i.
Cu - Capper
_
_ mgA
ORGANICS: (by GC, GC/MS,.HPLC)
Phenol _ mg/l
-
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB
Sulfate 51 mgll
Hg - Mercury
. mg/I
Report Attached? ElYes (1) ❑
�EPORT.)
o (0)
Specific Conductance 201 pMhds
K- Potassium
mgA
VOC , method #
Total Ammonia - - mg/I
Mg - Magnesium
mg/1
, method #
(Ammonia Nitrogen; NH3 as IT, Ammonia Nitrogen, Totae
Mn -Manganese
mgll
,method #
�
TKN as N mgA
NI - Nickel
mgll
, method #
For Remediation Systen s 0nly (Attach Lab Reports):
.,fnfluard TotCUOCs: -
mg/L Effluent Total VOCs; .. rpglL VOC
Removal%
I certify that, to lhL best ot any knowledge and befiel, the information submined
fa this reimi is true, accurate. and complete,
and that tile laboratory
analytical thao was produced using aupproved methods of analysis by a
GW-59 Rev. 1/2007

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864 9774 Fax
Certificate of Analysis
Alters, Inc
Mr.
59 Martin00 Turkey Highway Project: Mhyells samples - 3/Yearly Date Re orted: March 29, 2012
Date Received March 15, 2012
59
Turkey NC, 28393 Sampled By: Oglesby Date Sampled March 15, 2012
Mw #1
120336I-01
Analyte
Result
Unit
Analysis Date/fhne
Analyst
Method
Qualifier
An Wed by: Miaotoc- Fay9teWlk DWm
Chloride
207
mg/L
3/16/12 16:46
JAW
EPA300.0
B
COD, Total
122
mg/L
3/17/12 15:00
DSK
SM 20th Ed. 5220 D
Conductivity
812
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 25 10 B
Depth to Water Surface
27.0
feet
'3/16/12 17:55
BO
Field Measurement
Nitrate as N
4.04
mg/L
3/16/12 16:46
JAW
EPA300.0
pH, Field Test
5.09
pH Units
3/15/12 11:40
BO
Field
Total Dissolved Solids
435
mg/L
3/16112 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
39
mg/L
3/16/12 16:46
JAW
EPA300.0
B
Temperature
25
°C
3/15/12 11:40
BO
Field
Analyzed by: M law taboramries, Inc -Ohb
Valley
Total Organic Carbon
4.32
mg/L
3/23/12 1:09
DIH
E415.1
Mw 02
1203361-02
Analyte
Result
Unit
Analysis DatetTime
Analyst
Method
Qualifier
Waled by.M bac- Fayeoxnue Oman
Chloride
90.3
mg/L
3/16/12 17:03
JAW
EPA300.0
B
COD, Total
113
mg/L
3/17/12 15:00
DSK
SM 20th Ed 5220 D
Conductivity
399
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 251013
Depth to Water Surface
8.50
feet
3/16/12 17:55
BO
Field Measurement
Nitrate as N
1.14
mg/L
3/16112 17:03
JAW
EPA300.0
pH, Field Test
5.46
pH Units
3/15/12 11:50
BO
Field
Total Dissolved Solids
206
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
9.2
mg/L
3/16/12 17:03
JAW
EPA300.0
B
Temperature
25
°C
3/15/12 11:50
BO
Field
Analyael by: Mk bao Ubordtadea, Me - Ctuo
Valley
Total Organic Carbon 4.54 mg/L 3/23/12 1:22 DIH E415.1
Mw N3
1203361-03
State Certifications:
Respectfully Submitted
NCDNR-#11 ... .... __ .. ..... ......... _..._ _.... .._ _.... ...... _..
NCDOH #37714
Robert Denver
USDA 43787
Robert Dermer, Diyisiov Manager
Thankyouforyour Wsiness. Weimiie oufeedb°r mmrynxloJ.rtftw.wu P(eose ronrou thelByirionMam¢er.R°hen Permerar9/Od60-y910. Jamer NoW. Pre file tm
j°meaiu4.rt7a rmiemb°cc°m or7mor Bya. CEO. °r rmorah mry mmmenvarevggnrionr.
Page 1 of

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.R64 R774 Fax
Certificate ofAnalysis
Aliens, Inc Date Reported: March 29, 2012
5900 Turkey Highway Martin Oriess Project: M/Wells samples-3Nearly Date Received; March 15, 2012
590
Turkey NC, 28393 Sampled By: Oglesby Date Sampled: March 15, 2012
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
Chloride
94.2
COD, Total
100
Conductivity
496
Depth to Water Surface
4.00
Nitrate as N
0.713
pH, Field Test
6.19
Total Dissolved Solids
361
Sulfate as SO4
55
Temperature
26
An WW by: Miaobw Iabaarodes, Inc - Ohio
Valley
Total Organic Carbon
2.87
mg/L
3/16112 17:19
JAW
EPA 300.0 B
mg/L
3/17/12 15:00
DSK
SM 20th Ed. 5220 D Al2
umhostem
3/16112 10:00
DSK
SM 20th Ed. 2510 B
feet
3/16/12 17:55
BO
Field Measurement
mg/L
3/16/12 17:19
JAW
EPA300.0
PH Units
3/15/12 11:30
BO
Field
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
mg/L
3/16/12 17:19
JAW
EPA300.0 B
aC
3/15/12 11:30
BO
Field
mg/L 3/22/12 13:13 DIH E415.1
Mw H4
1203161-04
Analyte Result Unit Analysis DaterIlime Analyst Method Qualifier
Anar oy: wivoaz-raY� pie �rviswn
Chloride
24.5
mg/L
3/16/12 17:36
JAW
EPA300.0 B
COD, Total
114
mg/L
3/19/12 14:45
DSK
SM 20th Ed. 5220 D
Conductivity
170
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
9.00
feet
3/16/12 17:55
BO
Field Measurement
Nitrate asN
4.84
mg/L
3/16/12 17:36
JAW
EPA300.0
pH, Field Test
5.61
pH Units
3115/12 11:20
BO
Field
Total Dissolved Solids
100
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate asSO4
5.4
mg/L
3/16/12 17:36
JAW
EPA300:0 B
Temperature
24
aC
3115/12 11:20
BO
Field
Pn Wal by: Mivobac labaramria, Inc - Ohio Valley
Total Organic Carbon
4.94 mg/L 3/22/12 13:28
DIH E415.1
R-1
1203361-05
Analyte
Result Unit Analysis Date rime
Analyst Method Qualifier
Stare Certifications:
Respectfully Submitted
NCDNR"#11._„
..
NCDOH #37714
Robert Dermer
USDA #3787
Robert Deraner. Division Manaeer
Thank you for your business. WeinWey urfeedbxkmourlewlof,eMre, gym. Please conracuhe DiWnonMawger, Robert Dermerm 916844-191a, James Nakes, Pnsurnt.at
james.nokes(a3micwbae.m or lkwrll m. CEO, aumwehn,x 2micwb c.wm with my env orm,,stimu.
Pa¢e2 of

f
Fayetteville Division
2592 Hope Nhlls Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.964 9774 Fax
Certificate of Analysis
Mr. Martin, Inc Daze Re orted: March 29, 2012
590Tuk y Hig Project: MlWells samples-3Nearly Date Received: March 15, 2012
5900 Turkey Highway
Turkey NC, 28393 Sampled By: Oglesby Date Sampled: March 15, 2012
Analyrel by: Mkmbao- FayetteMe OM9on
Chloride
15.5
mg/L
3/16112 17:53
JAW
EPA300.0
COD, Total
276
mg/L
3/19112 14:45
DSK
SM 20th Ed. 5220 D
Conductivity
102
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
5.00
feet
3/16/12 17:55
BO
Field Measurement
Nitrate as N
0.830
mg/L
3/16/12 17:53
JAW
EPA 300.0
pH, Field Test
5.12
pH Units
3/15/12 15:10
BO
Field
Total Dissolved Solids
83.0
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
12
mg/L
3/16/12 17:53
JAW
EPA 300.0
Temperature
26
°C
3/15/12 15:10
BO
Field
Analyze] by: Mioubac 14baaterlea, Im - Cob
Valtey
Total Organic Carbon
6.30
mg/L
3/22/12 13:41
DIH
E415.1
R-2a
1203361-06
Analyte
Result
Unit
Analysis DateTime
Analyst
Method
Analyzed by: Mksolec- Faye ten0e(M Van
Chloride
10.4
mg/L
3/16/12 18:09
JAW
EPA300.0
COD, Total
31.7
mg/L
3/19/12 14.45
DSK
SM 20th Ed. 5220 D
Conductivity
155
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
5.00
feet
3/16/12 17:55
BO
Field Measurement
Nitrate as N
0.686
mg/L
3/16/12 18:09
JAW
EPA 300.0
pH, Field Test
4.89
pH Units
3/15/12 14:50
BO
Field
Total Dissolved Solids
88.0
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
37
mg/L
3/16/12 18:09
JAW
EPA 300.0
Temperature
25
°C
3/15/12 14:50
BO
Field
Analyzed by: Miaobac tabwafOrles, ix - Ohio Way
Total Organic Carbon
1.92
mpfL
3/22112 13:54
DIH
E415.1
R-3
1203361-07
10
Qualifier
Analyte Result Unit Analysis DateyTime Analyst Method Qualifier
State Certifications:
Respectfully Submitted
NCDNR-#11_-- _ .. _.__._.......... ..... .. .. __..____.... -.<.. _...__ _..._ _... ..
_
NCDOH #37714
Robert Demmer
USDA #3787
Robert Derma. Division Manages
Thank you foryour business. Weimireyoarfeeao aaourtn afzznlmw,u PleasermaraetO MvbimM ger,Aoben&mera9l"F 1920,J=Cs Nokes, Preridmat
Jamexnokesa.ke bac. or Tma,Bo . CEO, ar onn,,&,eQmkz b.o .ram wtthm co.a=orrvggertiom.
Page 3 of

Fayetteville Division
2592 Hope Mills Rd
Favetteville. NC 28306
910.864.1920 Phone
910 RM 9774 Far
Certificate of Analysis
Allen, Jae
Mr. Martin Griess Project: M/Wells samples-3/Yearly Date Reported March 29, 2012
5900 Turkey Highway Date Received: March 15, 2012
Turkey NC, 28393 Sampled By: Oglesby Date Sampled: March 15, 2012
R-3
120336t-n7
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method Qualifier
Analyiel by: Kmbac-Fay9RtiAe DIvWm
Chloride
45.3
mg/L
3/16/12 18:59
JAW
EPA 300.0 B
COD, Total
123
mg/L
3/19/12 14:45
DSK
SM 20th Ed. 5220 D
Conductivity
222
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
6.60
feet
3/16/12 17:55
BO
Field Measurement
Nitrate as N
0.742
mg/L
3/16/12 18:59
JAW
EPA 300.0
pH, Field Test
5.11
pH Units
3/15/12 14:35
BO
Field
Total Dissolved Solids
92.0
mg/L
3/16112 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
17
mg/L
3/16/12 18:59
JAW
EPA 300.0
Temperature
26
°C
3/15/12 14:35
BO
Field
AroWiby: Mko tabw�, Nc-eWo WNW
Total Organic Carbon
1.45
mgfL
3/22/12 14:07
DIH
E415.1
R-4
12n3361-OR
Analyte Result Unit Analysis Date2me Analyst Method Qualifier
Chloride
49.3
mg/L
3/16/12 19:15
JAW
EPA300.0
COD, Total
96.1
mg/L
3/19/12
14:45
DSK
SM 20th Ed. 5220 D
Conductivity
279
umhos/cm
3/16/12
10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
7.00
feet
3/16112
17:55
BO
Field Measurement
Nitrate as N
3.72
mg/L
3/16/12
19:15
JAW
EPA 300.0
pH, Field Test
4.80
pH Units
3/15112
14:15
BO
Field
Total Dissolved Solids
164
mg/L
3/16/12
11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
18
mg/L
3116/12
19:15
JAW
EPA 300.0
Temperature
25
°C
3115/12
14:15
BO
Field
Malyzed by: Ml Ioac tabwa des, Ina -ONo Valley
Total Organic Carbon
3.52
mg/L
3/22/12
14:19
DIH
E415.1
R-5a
1203361-09
State Certifications:
Respectfully Submitted
NCDOH 037714
Robert Dermer
USDA #3787
Robert Dezner, Division Manager
Thank you foryour business. Weimiewurfeedb am° invwwl iaz°wu Pleax m^,,..•the Divlrion Mam¢er. Ro6ertDezmerw 9/0.Y6t-/PIO.J ee Noker. PreeWa.
j°mer.mk iooh°v ram orlkvorbayee,CEO.°zzrewrhjveP°ia°4°°.mm
Page 4 of

Fayetteville Division
2592 Hope Mills Rd
Fayetteville- NC 28306
910.864.1920 Phone
910 R64 9774 Fay
Certificate of Analysis
Alters, Inc Dace Re orted: March 29, 2012
5900 Turkey HigMartin ighway Project: MlWells samples-3/Yearly Date Received: March 15, 2012
59
Turkey NC, 28393 Sampled By: Oglesby Date Sampled: March 15, 2012
Analyte
Result
Unit
Analysis Daterrime
Analyst
Method
Qualifier
AneWed by: Mkmbac- Faye eMlle Divition
Chloride
17.6
mg/L
3/16/12 19:32
JAW
EPA 300.0
Al2
COD, Total
82.8
mg/L
3/19/12 14:45
DSK
SM 20th Ed. 5220 D
Conductivity
201
umhos/cm
3/16112 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
5.00
feet
3/16/12 17:55
BO
Field Measurement
Nitrate as N
6.82
mg/L
3/16/12 19:32
JAW
EPA 300.0
Al2
pH, Field Test
5.03
pH Units
3115/12 1350
BO
Field
Total Dissolved Solids
126
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
23
mg/L
3/16/12 19:32
JAW
EPA 300.0
Al2
Temperature
25
oC
3/15/12 13:50
BO
Field
Aneyea1 by: Mkmbac tabaamna, Inc - Ohio
Valley
Total Organic Carbon
3.52
mg/L
3/22112 14:54
DIH
E415.1
R-6
12n3761-10
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifer
Anayael by: Mioobac-Fayemmlle rieWw
Chloride
38.8
mg/L
3/16/12 20:22
JAW
EPA300.0
COD, Total
125
mg/L
3/19/12 14:45
DSK
SM 20th Ed. 5220 D
Conductivity
233
lunhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
7.00
feet
3/16/12 17:55
BO
Field Measurement
Nitrate as N
1.20
mg/L
3/16/12 20:22
JAW
EPA 300.0
pH, Field Test
4.74
pH Units
3/15/12 13:35
BO
Field
Total Dissolved Solids
156
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
26
mg/L
3/16/12 20:22
JAW
EPA 300.0
Temperature
24
'C
3/15/12 13:35
BO
Field
Analyzed by. Mioobac taboralxx es, Inc - Ohio Valley
Total Organic Carbon
10.6
mg/L
3/22112 15:07
DIH
E415.1
R-7
19.03161-11
Analyte Result Unit Analysis Date/1-ime Analyst Method Qualifier
State Certifications: Res ectfidl Submitted
........I .........__.. _._..._... ..... _._ _.. .1... ..—_. P... Y------ - -...
NCDOH #37714 Robert Dermer
USDA #3787 Robert Darner. Division Maaaea
Thank ywforywrbusiness. Weimie7 vrfeermrc mmrle W.fservi .e . Plear. ronracr Jre DiWsianM gen RobertOermerae 910.461-1930, Jmner Notre; President err
jmnernohs(aJmicmbaerom or]ie,nr aoyee, CEO, aelmvrAo7ee(aJmicro6oe.mm with wy rommenu or ru�ernom. Pape 5 of 7

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910 9" 9774 Far
Certificate of Analysis
Mr. Martin, Inc Date Re orted: March 29, 2012
59Turkey
Project: M/Wells samples-3/Yearly Date Received: March 15, 2012
5900 Turkey Highway
Turkey NC, 28393 Sampled By: Oglesby Date Sampled: Mar h 15, 2012
Malyzel by: Mia°ht - Fay6[evme DtvWm
Chloride
47.9
mg/L
3/16/12 20.39
JAW
EPA300.0
COD, Total
163
mg(L
3/19/12 14:45
DSK
SM 20th Ed. 5220 D
Conductivity
208
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
7.00
feet
3/16/12 17:55
BO
Field Measurement
Nitrate as N
1.02
mg(L
3/16112 20:39
JAW
EPA300.0
pH, Field Test
4.71
pH Units
3/15/12 13:20
BO
Field
Total Dissolved Solids
141
mg/L
3/16112 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
7.8
mg/L
3/16/12 20:39
JAW
EPA 300.0
Temperature
25
°C
3/15/12 1320
BO
Field
Malyial by: Miaobac tapwaNnes, Inc - Ohio
Valley
Total Organic Carbon
13.7
mg/L
3/22/12 15:21
DIH.
E415.1
R-8
1203i61-».
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
AWWW by: KKmiec- FayeW.viue Divislm
Chloride
18.0
mg/L
3/16/12 20:55
JAW
EPA300.0
COD, Total
147
mgIL
3/19/12 14.45
DSK
SM 20th Ed. 5220 D
Conductivity
270
umhos/cm
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
8.00
feet
3/16/12 17:55
BO
Field Measurement
Nitrate asN
16.0
mg/L
3/16/12 20:55
JAW
EPA300.0
pH, Field Test
5.40
pH Units
3/15/12 12:50
BO
Field
Total Dissolved Solids
180
mg/L
3116/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
19
mg/L
3/16/12 20:55
JAW
EPA 300.0
Temperature
26
°C
3/15/12.12:50
BO
Field
Malyret by: Mk bac Labaatoties, Inc -Ohio Valley
Total Organic Carbon
2.90
mg/L
3/22/12 15:34
DIH
E415.1
R-9
17.03761-11
Qualifier
Analyte Result Unit Analysis DateTme Analyst Method Qualifier
MaWel or. Kluotmc- FayefteAOe Divisbn
State Certfications:
Respectfully_ Submitted_
NCDNR#ll
NCOOH N37714
Robert Dermer
USDA #3787
R°bvt Dener.Division Mavaeer
Thank you foryourbusinem Weimael°srfeeaark°n°arfnvlcf nic toy°a Pleaneanma JrcO onMawger,ftoben Oermerm9l"A 1920.Jmnes N°.trr. Frcndem.ae
jamea.fmlzr(Jmycmbacmm or Tmmr B°ps, CEO, alymwnbalee('ymim°baecam wirh arrymmmenv arruggeanay.
Paee 6 of7

Fayetteville Division
2592 Hope Mats Rd
Faveaeville. NC 28306
910.864.1920 Phone
910 R64 R774 Fax
Certificate of Analysis
Allen, Inc
Mr. Martin Grim Project: M/Wells samples - 3/Yearly Date Reported: March 29, 2012
5900 Turkey Highway Date Received March 15, 2012
Turkey NC, 28393 Sampled By: Oglesby Date Sampled: March IS, 2012
R-9
1203161-13
Analyte
Result
Unit
Analysis DateJl-une
Analyst
Method Qualifier
Malyied by; Miaobc- rayelhrine lavislon
-
Chloride
6.31
mg/L
3/16/12 21:12
JAW
EPA300.0
COD. Total
409
mia/L
3/19/12 14:45
DSK
SM 20th Ed. 5220 D Al2
Conductivity
201
umhos/em
3/16/12 10:00
DSK
SM 20th Ed. 2510 B
Depth to Water Surface
8.70
feet
3116/12 17:55
BO
Field Measurement
Nitrate as N
4.34
mPJL
3/16/12 21:12
JAW
EPA 300.0
PH, Field Test
4.43
pH Units
3/15/12 15:30
BO
Field
Total Dissolved Solids
129
mg/L
3/16/12 11:01
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
51
mgJL
3116/12 21:12
JAW
EPA 300.0
Temperature
24
0C
3/15/12 15:30
BO
Field
MaWal by: Mlaa[ac tab9rdbnies, Inc - OND Valle/
TotalOrganiaCarbon -
3.61
mpJL
322112 15:46
DIH
E415.1
Qualifier Definitions
U Not detected at or above adjusted samule detection limit
B Detected in the associated Method Blank
Alt MSIMSD fail nxoverv. but the LCS passes criteria.
State CertFications:
Respectfully Submitted
NCDOH #37714
Robert Derrner
USDA #3787
Robert Deaner, Divivi. Manager
Thank you tnrvour business We invite wurlecdbackon mrr level o/rervirero wa Plrvsemrtvcti.MpN nM=oer.RobeHDewier.9l"64-1920.✓ sNekes. President.
j.no.mM.s(aJmicwba<.eom or7knrBoytt, C£O, of rn:rnnbolce(d�niewb..mm wbh mryrammenu.suggesdane
Paee 7 of7

Mill
p GW-59A COMPLIANCE REPORT FORM Permit # iyQ a0t)Vbg
(Submit one each monitoring period with GW--59 forms.)
1
Enter date monitoring results were due. - o ^ Will this monitoring report (GW-59 and GW59A)
YES
QjO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
co
IF the answer to question f or 2 is 'YES" list in the space provided below the well identification numbers) and
explain the problems encountered in obtaining the required intimation.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
O
identification plate, area overgrown, etc.)? Ythe answer is "Yes", contact the Regional Ofceforguidance.
4
Are any monitored constituents equal to or above the established standards?
NO
If the answer to question 4 is 'NO", skip to section B.
If the answer to question 4 is "YES" list the affected wells individually with constituent(S)r and concentration(s)
exceeding standards in the space provided below:
R- 6 — '70C 10.16 mg)L
R 7 — -roc- /3.7 m5lL
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
ONO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO" skip to section 8.
If the answer to question 5 is "YES" list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
— )?-G Tx /).3 rh5IL
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is NO" monitoring wells maybe improperly
located; contact the Regional ice.
7
Is the pernittee implementing previously approved actions required by the Division involving this
YES
groundwater quality problem?
If the answer to question 7 is 'YES", describe those actions in the space provided below.
If the answer to question 7 is `NO" contact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines. and/orpenaltjes.
8
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby ackgowledge that the above,information was evaluated and tits'•infornation,submitted.in'this
report (Compliance ReporNGW59A) is true and complete'to'-ttie16est of my knowledge. ' ' '` - V
I
Signature of Permittee (or Authorized Agent) Date
GW-59A 121812003

j �tNG V V MHMO AT S S.':$Itp CB 79
I 56¢
Quality Vegetables -
5900 TMU(EY HIGHWAY, TORHEY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone]
April 20, 2012
Dept. of Environmental & Natural Resources
Division of Water Quality — Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
RE: Groundwater Quality Monitoring Report
Allen, Inc. — Turkey, NC Facility
Permit# WQ0004268
Enclosed are the original and one copy of the -Groundwater Monitoring Report on forms GW-59
and GW-59A, and the lab report for — Turkey, NC facility for samples collected in
March, 2012. f
Monitoring � .�11IiU'oj \ h�/ \ mg/L limit for TOC as stated in the permit.
These wells c i �J , T15 (Y1 1 ` -.d as soon as possible.
If you have an C00 ill Jvo- \information, please contact me by
phone at (910)1 n� g a Q
Sincerely,
Tim Brewers
Plant Manager
Allens, Inc. Turkey facility
CC: Laura Mushinski, Allens, Inc
Reid Wells, Allens, Inc —Turkey facility,
tntO�ma�\0���
®ENR—FRO
APR 3 0 2012

. N G Up MEMORIES S I N O B
• Quality Vegetables
5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone] -.
February 7, 2012
Dept of Environmental & Natural Resources
Division of Water Quality - Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
(9 9) 733-3221-
RE 1°/j �= ,om'toring Report
�a 6� NC Facility
e
T � •: to the Groundwater Monitoring Report dated December 21, 2011 for the Allens,
In"
fits on _ -
- T, t �p�rL TOC levels in MW-I, MW-2, and R-6 ex eeded the l0mg limit as specified in
fl;
i e resampled and the results were within the permit requirements. The results are listed
a, ees.
1 f,4uestions or require any additional information, please contact me by phone at (910) 596-
0;
Sincerely,
72L
Martin Griess
Plant Manager
Allens, Inc. Turkey facility
CC: Laura Mushinski, Allens, Inc
Reid Wells, Allens, Inc -Turkey facility
FEB 13 2012
DVV
C 1
FEB It 9 2012
Information Processing Unit
DWO/BOG

SR QUALITY MONITORING:
REPORT FORM
Name:I Aliens, Inc. - Turkey
Name (If different):
5900 Turkey Highway
(5h0G1) NC 28393-9703 County Sampson
Martin GNess Telephone#: [phone]
Name: No, of wells to be sampled:.
LID NU BER (from Permit): MW-1 Date sample collected: 1/23/12
Depth: ft. Well Diameter: in.
i to Wale Level: ft. below measuring point Screened Interval: _ft. to _ft.
,wring Poi t is ft. above land surface Relative M.P. Elevation: fl.
ne of walyr pumped/bailed before sampling: gallons
-RMIT Number:
Expiration Date: July 31 2015
an -Discharge WQ0004268
UIC
3DES
Other
(PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remedialion: Infiltration Gallery
RI Spray Field
❑ Remedialion:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH _units Temp. °C
Spec, Cond. µMhos
Odor
Appearance
at
of
Date sample ahalyzed:
Laboratory Name: Mlerobae Laboratories
Certification No. NC#11 NC#37714
PARAMETER" NOTE: Values should reflect dissolved
and colloidal concentrations.
COD
mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
MF Fecal
/100ml
Nitrate (NO3) as N
mgll
Zn - Zinc mg/I
�Coliform:
X Colifol�m: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Us MPN maNatl for highlytu�old samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
^Dissolved Solids: Total
mg/I
At - Aluminum
mg/I
pH (why n analyzed)
units
Be - Barium
mg/I
TOO
5.10 mg/I
Ca - Calcium
mg/I
Chloride
mg/I
Cd- Cadmium
mg/I
mg/I
Chromium: Total
mg/I
GrelArsenic
se and Oils
mg/l
Cu - Copper
mg/I
ORGANICS: (by GC,,GC/MS, HPLC)
„ Phenol
mg/I
Fe - Iron
mg/l
(Specify test and method M ATTACH LAB REPORT.)
Sulfate
mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Oonductance
I
µMhos
K- Potassium
mg/I
VOC ,method#
To I Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Anunonla Iaogen: NH°as N:Ammonle Nitrogen, Totap
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remedial on Systems Only (Attach Lab Reports):
Influent TotaI.VOCs:
mg/L.. Effluent Total VOCs: mg/L VOC. Removal%
�best of my knowledge and belief, [lie
rabury; t a. aware that there are significant
Information submitted
penalties for
!it this remort is title, accurate, and complete,
submitting (alse inlormalioni including rie
and that file laboratory
possibility of fines and Imprisonment
analytical data was produced using appfov.d plethoric of analysis by a
for knowinq violations,
_Martin Grietfs, Plant Manager
Parmittea (or Authorized Anent) Name and Title - Please print or type
Signature of Pennitlae (or Authorized ApenO (Dal
GW-59 I Rev. 1/2007

N
QUALITY MONITORING:
Name: l Aliens,Inc.-Turkey
Name (yf different):
Griess
County Sampson
Telephone#: [phone]
No. of wells to be sampled:
LID NUMBER (from Permit): MW-2 Date sample collected: 1/23/12
Depth: ft. Well Diameter: in.
h to Wale Level: ft. below measuring point Screened Interval: ft. to _ft.
luring Poillt is ft. above land surface Relative M.P. Elevation: ft.
ne of wahI:r pumped/bailed before sampling: gallons
sample
(Note: Us
Dissolved
pH (wh
Specific
lyzed:
Laboratory Name: 'Microbac Laboratories
NOTE: Values should reflect dissolved and colloidal concentrations.
COD
mg/l
Nitrite (NO,) as N
mg/I
MF Fecal
/100MI
Nitrate (NO3-) as N
mg/I
MF Total
/100ml
Phosphorus: Total as P
mg/I
PN method for highly forbid samples)
Orthophosphate
mg/I
ilids:Total
mg/I
AI - Aluminum
mg/I
analyzed)
units
Be - Barium
mg/I
TOC
6.34 mg/I
Ca -.Calcium
mg/I
Chloride
mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
e and Oils
mg/I
Cu - Copper
mg/I
Phenol
mg/I
Fe - Iron
mg/I
Sulfate
mg/I
Hg - Mercury
mg/I
nductance
µMhos
K- Potassium
mg/I
Ammonia
mg/I
Mg - Magnesium
mg/I
vgen; NHsas N; AmmoNa Nitrogen, Total)
Mn- Manganese
mg/I
TKN as N
mg/I
NI - Nickel
mg/I
I certify that, to the best of my knowledge and belief, the. ii
DWD-certified lab ratory. I am aware that there are signi
.r-
Pennittee (or Authprized Agent) Name and Title - Please
GW-59 IRev. 112007
!RMIT Number: Expiration Date: July 31, 2015
n-Discharge W00004268 uIC
-DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑, Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH _units Temp.
Spec. Cord. µMhos
Odor
Appearance
oC DRY at
time of
Certification No. NC#11 NC#37714
Pb - Lead mg/I
Zn - Zinc mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
Effluent Total VOCs:
VOC

TER QUALITY MONITORING:
E REPORT FORM
FACILITY INF(7RMATIDN PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey Non -Discharge W00004268 UIC
Permit Name ( f different): NPDES Other
Facility Address : 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED
Turkey i 5i""'} NC 28393-9703, County Sampson El Lagoon ❑ Remediation: Infiltration Gallery
icryij (stale) (LP) ® Spray Field ❑ Remediation:
Contact Persalti: Martin Griess Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
ell.Location/)dite Name: No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other:
L ID NUMBER (from Permit): R-6 Date sample collected: 1/23112
Depth: - ft. Well Diameter: in.
hto Wate`` Level: ft. below measuring point Screened Interval: _ft. to _ft.
luring Poi t is ft. above land surface Relative M.P. Elevation: ft.
ne of wat r pumpedfbailed before sampling: gallons
sample
COD
mg/I
Coliforin: MF Fecal
/100ml
Coliform:.MF Total
/100ml
(Note: Us IMPN method for highly turbid samples)
Dissolved Polids: Total
mg/I
pH (whom analyzed)
units
TOC
6.41 mg/I
Chloride
mg/I
Arsenic
mg/I
Grekse and Oils
mg/I
Phenol
mg/I
Sulfate
mg/I
Specific Conductance
juMhos
Tot l Ammonia
mg/I
(Ammonia Itrogen; N%.. N; Ammonla Ngmgen, Total)
TKN as N
ma/I
FIELD ANALYSES:
PH _units Temp. °C
Spec. Cond. µMhos
Odor
Appearance
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
colloidal concentrations.
Nitrite (NO,) as N
mg/I Pb - Lead mg/I
Nitrate (NO3) as N
mg/I Zn - Zinc mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mg/l Other (Specify Compounds and Concentration Units):
AI - Aluminum
mg/I
Be - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron
mg/I
(Specify test and method A ATTACH LAB REPORT.)
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
K - Potassium
mg/I
VOC , method #
Mg - Magnesium
mgfl
, method #
Mn - Manganese _
mg/I
, method #
Ni- Nickel
mg/I
,method#
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCg: mg/L.. ,Effluent Total VOCs: _, _ ma/L VOC Removal%
Martin
07 - %-/.)--
at
of
GWS9 IRev. 1/2007

Fayetteville Division
2592 Hope Mills Rd ,
Fayetteville, NC 28306
910.864.1920 Phone
910.964.9774 Fax
Certificate of Analysis
Allens, Inc
Mr. Martin Griess Project: M/Rr samples - 3/Yeady, Retest Date Reported: February 06, 2012
Date Received: January23, 2012
5900 Turkey Highway Date Sampled January23, 2012
Turkey NC, 28393 Sampled By: Mr. Reid Wells
M/W - #01
1201400-01
Analyte - Result
Unit
Analysis DateTime
Analyst -
Method
Qualifier
Anatyrad by: Mkmtac UOorato ies, Inc -ONo Vala
Total Organic Carbon 5.10
nag/L
1/27/12 2:08
DIH
A5310B
MW:#2
1201400-02
Analyte Result
Unit
Analysis DateTme
Analyst
Method
Qualifier
Matyzet by: Mkmbx labaarodes, Inc - Ohio Vale/
Total Organic Carbon 6.34
mg/L
1/27/12 2:32
DIH
A5310B
M/W - R-6
1201400-03
Analyte Result
Unit
Analysis Date/rime
Analyst
Method
Qualifier
kwWe0 by: Mimbae law am 0, Inc - Ohlo vane,
Total Organic Carbon_ 6A1
mg/L
1/27/12 2:57
DIH
A5310B
Qualifier Definitions
U Not detected at or above adjusted sample detection limit
State Certifications:
Respectfully Submitted
NCDNR #11
NCDaH 037714
Robert.Dermer
USDA 03787
Robert Derma, Division Managa
Thank you for yourbusiness. Preddem.m
Jmnesrmkes irmbarmm or7iewrBga, CBO,ar rm.orbojregmirmbaae wlrh yro menu orrvag Baru.
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