WQ0004268_GW Monitoring_20131214

ouomt I rump
NDWATER QUALITY MONITORING:
ity Name: Allens, Inc. - Turkey
tit Name (if different):
ity Address: 5900 Turkey Highway
key NC 28393-9703 County Sampson
art Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
L ID NUMBER (from Permit): MW-1
Depth: ft,
.1 to Water Level: 18.9 ft. below measuring point
nrinn Point is ft. above land surface
ne of water pumped/bailed before sampling:
10+
Date sample collected: 11/18/13
Well Diameter: in.
Screened Interval: _ft. to .__ft.
Relative M.P Elevation: ft.
'RMIT Number:
Expiration Date: July 31, 2015
m-Discharge WQ0004268
_
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
❑K Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
PH 4.76 units
Spec. C0nd.
Odor
Appearance
Temp. 20 °C DRY at
pMhos time of
a sample analyzed:
Labotatory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
UMETF-RS NOTE: Values should reflect dissolved and colloidal concentrations.
CAD
30.7 mg/I
Nitrite (NO.) as N
mgd
Ph - Lead mg/(
Coliform: MF Ferali_
1100ml
Nitrate (NO3) as N
_ _
7,28 To
Zn - Zinc mgll
Coliform: 10F Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPNmaNud for NgM1ly tma:dsamples)
Orthophosphate_
mgll
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total E.r2
m�'^gll
AI - Aluminum
mgil
PH (when analyzed) __
_units
Ba - Barium
mg/I
TOC _
5.79 mg/I
Ca - Calcium _
'Chloride
147 mg/l
Cd - Cadmium
_mg/I
mgA
Arsenic__
mgll
Chromium: Total-^
mg/I
Grease and Oils
mg/I
Cu - rapper
mgA
ORGANICS: (by GC, GClMS, HPLC)
Phenol _
„ lgil
Fe - Iron
mg/I
(Specify test and method C ATTACH LAB REPORT.)
Sulfate
120 mg/I
- Fig-Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
937 ItMhos
K- Potassium
mgA
VOC , method #
Total Ammonia «mg/I
(Ammoma Nrtrel NH,as N: Ammanla Nitrogen. Total)
Mg -Magnesium
mg/I
,method
Mn - Idanganese
mg/I
,method #
— TKN as N
mg/I
Ni - Nickel
mgA
, method #
Cn•� On--n.e:.. e:...• c...., ram_,.. ,• .. _.
niy,L ce1H9Nt Iota, vuus:
Robert Caldwell, Plant Manager
Penninee for Aathalized Anent) Name and Title- Please print or type
GW-59 Rev. 112007
&OL41

JUumiI r•VKM
UNDWATER QUALITY MONITORING:
PLIANCE REPORT FORM
ity Name: Aliens, Inc. - Turkey
tit Name (if different):
ity Address: 5900 Turkey Highway
key "' NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
L ID NUMBER (from Permit): MW-2 Date sample collected: 11/18/13
Depth: ft. Well Diameter: in.
h to Water Level: 5.10 ft. below measuring point Screened Interval: ft. to ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
the of water pumped/bailed before sampling: 10+gallons
Ass for metals were collected unfiltered: DYES ElNO and field acidified: ❑ YES n No
iRMIT Number:
Expiration Date: July 31, 2015
n-Discharge W00004268
UIC
IDES
Other
'PE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remedialion: Infiltration Gallery
© Spray Field
❑ Remedialion:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 4.97 units
Spec. Cond.
Odor
Appearance
WELL
Temp. 20 eC DRY at
µMhos lime of
e sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
:AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
24.3 mgA
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
0.660 mg/I
Zn - Zinc mgll
Coliform: MF Total
1100ml
Phosphorus: Total as P
mg/I
(Note'Use MPN meOod ferhlgaly tueld samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
226 mgA
AI - Aluminum
mgll
pH (when analyzed)
units
Be - Barium
mg/I
TOC
3.58 mg/I
Ca - Calcium
mgll
Chloride
97.1 mg/I
Cd- Cadmium
mg/l
Arsenic
mg/I
Chromium: Total
mgll
Grease and Oils
mgA
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
9.4 mgA
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
410 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mgA
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHsas N: Ammonia Nitrogen. Total)
Mn - Manganese
mg/I
, method #
TKN as N
mgll
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total-VOCs: mq/L VOC Removal% .
Robert Caldwell, Plant Manager
Pennittee (or Authorized Anent) Name and Title- Please print or type signal a o(Permittee or Aulhodxed Anent)
GW-59 Rev. 112007
k
A

TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
lY "' NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
LID NUMBER (from Permit): MW-3
Depth: ft.
h to Water Level: 11.00.11. below measuring point
Turing Point is ft. above land surface
ne of water pumped/bailed before sampling: _ 10+
Date sample collected: 11118/13
Well Diameter: in.
Screened Interval: _ft. to _ft.
Relative M.P. Elevation: ft.
n-Discharge WQ0004268 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH 5.62 units
Spec. Cond.
Odor
Appearance
Temp. 20 eC DRY at
µMhos time of
t sample analyzed:
LaboratoryName: Microbac Laboratories
Certification No. NC#11 NC#37714
;AMETERS NOTE: Values should
reflect dissolved and colloidal concentrations.
COD
221 mg/I
Nitrite (NO,) as N
ri
Pb - Lead mg/I
Coliform: MF Fecal
/100m1
Nitrate (NOa) as N
0.690 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100m1
Phosphorus: Total as P
mg/l
(Note' Use MPN method for highly tutted
samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
�6Sj'nty/I
Al - Aluminum
mg/l
pH (when analyzed)
units
Ba- Barium
mg/1
TOC
3.38 ri
Ca - Calcium
mg/l
Chloride
128 mg/I
Cd - Cadmium
ri
Arsenic
mg/I
Chromium: Total
ri
Grease and Oils
mg/l
Cu - Copper
mgn
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/1
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
55 mg/1
Hg - Mercury
mgA
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
600 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/I Mg - Magnesium mg/I
(Ammonia Nitrogen; NH>as N; Ammonia Nitrogen, Talon
Mn -Manganese mg/I
TKN as N mgll Ni - Nickel - mg/l
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: _. _ _ mg/L Effluent Total VOCs: mo/L VOC Removal% .
Robert Caldwell, Plant Manager �i� dfJ 41
Permittee for Authorized Apart) Name and Title- Please print or type Sipnalure o ermi ee (or uthoraed Agent) lot
GW-59 Rev. 112007 .. a

runM UN
DWATER QUALITY
ANCE REPORT FO
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
Y NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
!! P
PLING INFORMATION
.LID NUMBER (from Permit): MW-4 Dale sample collected: 11/18/13
Depth: ft. Well Diameter: in.
h to Water Level: 5.90 ft. below measuring point Screened Interval: _ft. to _ft.
curing Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
:RMIT Number:
Expiration Date: July 31, 2015
m-Discharge WQ0004268
UIC -
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remedialion: Infiltration Gallery
® Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 4.35 units
Spec. Cond.
Odor
Appearance
Temp. 21 eC DRY at
µMhos time of
(Date sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
PARANIETERS NOTE; Values should reflect dissolved and colloidal concentrations.
COD
78.7 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100mi
Nitrate (NO3) as N
4.54 mgll
Zn - Zinc mg/i
Coliformi MF Total
/100MI
Phosphorus: Total as P
mg/I
(Note: use MPN method for highly tumid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
84 mg/I
At - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mgA
TOC
4.60 mg/l
Ca - Calcium
mg/l
Chloride
21.5 mg/l
Cd - Cadmium
mg/I
Arsenic
mgll
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mgll
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate_
8.4 mg/I
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
157 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
high
Mg - Magnesium
mg/l
method #
(Ammonia Nitrogen: NI(ras N: Ammonia Nitrogen, ToIaI)
Mn- Manganese
,
mgll
,
,method#
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
moo,.cl,v j, uu,uon\ ,.1.1 vvIb.
Robert Caldwell, Plant Manager
Permittee, (or Authorized Admit Name and Title - Please print or type
GW-59 Rev. 112007
emuent I oral vucs:
VOID

SUBMIT FORM ON YELLOW PAI
QUALITY MONITORING:
PORT FORM
Name: Aliens,Inc.-Turkey
Name (if different):
Address: 5900 Turkey Highway
County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be samoled:
L ID NUMBER (from Permit): R-1 Date sample collected: 11/18/13
Depth: ft. Well Diameter:_in.
h to Water Level: 2.50 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/balled before sampling: 10+ gallons
fRMIT. Number:
Expiration Date: July 31, 2U15
ih-Dischafrge WQ0004268
UIC
)DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑.Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
El Rotary Distributor
❑ Land Application of Sludge
❑`Water Source Heat Pump
❑ Other.
FIELD ANALYSES:
pH 4.45 units Temp. 21 eC
Spec. Cond. µMhos
Odor
Appearance _
a sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714 ,
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 218 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (Noe) as N
1.03 mgA
Zn -Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: use MPN meNod far highly WNW.e Ples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 278 mgA
At - Aluminum
mg/l
pH (when analyzed) units
Be - Barium
mg/I
TOC 9.97 gA
Ca - calcium
mg/I
Chloride 114 mgA
Cd- Cadmium -
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mgA
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.) ,
Sulfate 11 mg/I
_
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance 474 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium.
mg/I
#
(Ammonia NigogM NH�as tF7m W-Nmgen, tToter
Mn - Manganese
mg/l
,method
, method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
Fu1 ncu,carartvri oysreors umy tnaacn rao r<eporTS): mnuent Total VOOs: mg/L . Effluent T,ota6VQCs: _ mg/L VOc Removal%
Robert Caldwell, Plant Manager
Permulee(or Authorized Agent)Nameand Tire- Please print ortype Signal eol Permittea or Aulhoriied Agent)
GW-59 Rev. 1/2007 -
at
of
N
A

s+11 UNl.r
ROUNDWATER QUALITY MONITORING:
DMPLIANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
act Person: Robert Caldwell
Location/Site Name:
LID NUMBER (from Permit): R-2a
Depth: ft.
h to Water Level: 3.30 ft. below measuring point
wring Point is ft. above land surface
Tie of water pumped/bailed before sampling: 10+,
County Sampson
Telephone#: [phone]
No. of wells to be sampled:,
PERMIT Number:
Expiration Date: July 31, 2015:
Non -Discharge WQ0004268
UIC
NPDES
Other
TYPE OF PERMITTED OPERATION BEING.MONITORED
❑ Lagoon
❑ Remedialion: Infiltration Gallery
® Spray Field
❑ Remediation:
❑ Rotary' Distributor
❑ Land Application of Sludge
❑ Water. Source Heat Pump
❑ Other:
Date sample collected: 11/18/13
Well Diameter: in.
Screened Interval: ft. to ft.
Relative M.P. Elevation: ft.
FIELD ANALYSES:
pH 4.20 units Temp. 21 eC
Spec. Cond. µMhos
Odor
Appearance _
l sample analyzed:
Laboratory Name: Microbae Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
<10.0 mg/l
Nitrite (NO2) as N
mg/I
Pb - Lead mg1I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
1.01 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
Tagil
(Note: (Note: Use MPN method(orhighly tumd samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
62.0 mgA
AI -Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOC
2.59 mgll
Ca - Calcium
mgll
Chloride
14.4 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/l
Grease and Oils
Tagil
Cu - Copper
mg1I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB REPORT.)
.Sulfate
17 mg/l
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
114 µMhos
K - Potassium
Trigg
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/l
#
(Ammonia Nitrogen; NH,.. N; Ammonia Nitrogen. Total)
Mn- Manganese
mg/I
,method
,method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
uut, oystuitib viuy lruracn Lae neports(: mnuent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removale/
Robert Caldwell, Plant Manager s
Polarities, (or Authorized Agent) Name and Title - Please pant or type Sign , or Permitle (orAuNonz,itl Agent)
GW-59 Rev. 112007 re
at
of
N
k

SUBMIT FORM ON YFI I OW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
OMs oNOFWATER CuauTMYEaNF RSIC
UNIr
COMPLIANCE REPORT FORM
et7 MA IL8ER1AcSCENTER;RALEI,GHrNC 276997877t Phon6i-'(979)?33a221
FACILITY INFORMATION Please Pnnr ctearryorType
•
PERMIT Number: Expiration Date: July 31. 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey NC 28393-9703 County Sampson
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No, of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
If'.. Permit
SAMPLING INFORMATION
-
If WELL
WELL -ID NUMBER (from Permit): R-3
Date sample collected: 11/18/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
pH 3.67 units Temp. 19 eC
DRY at
Depth to Water Level: 3.10 ft. below measuring point
_in.
Screened Interval: ft.
to
ft. Spec. Cord. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: El
El NO and field acidified: El YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certificatie_n No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 24.3 mg/l
Nitrite (NO,) as N
mgll
Pb - Lead mgA
Colifonn: MF Fecal 1100ml
Nitrate (NO3) as N
2.46 mgA
Zn - Zinc mgll
Coliform: MF Total 1100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method forhighly luNid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 254 mg/l
AI -Aluminum
mgll
pH (when analyzed) units
Be - Barium
mgA
TOC 2.17 mgll
Ca - Calcium
mgll
Chloride 134 mg/I
Cd - Cadmium
mg/I
Arsenic mgll
Chromium: Total
mg/l
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 27 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 583 µMhos
K- Potassium
mg/I
VOC ,method#
Total Ammonia mg/l
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHaas N, Ammonia Nleogen, Totaq
Mn - Manganese
mg/l
, method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mglL Effluent Total VOCs:
Robert Caldwell, Plant Manager
Permiaee (or Authorized AgentiName and Title- Please Print or type
GW-59 Rev. 112007

JubMI I PUKM
UNLY
TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
NC 28393-9703 County Sampson
act Person: Robert Caldwell
Location/Site Name:
Telephone#: [phone]
No. of wells to be sampled: _
PLING INFORMATION -
L ID NUMBER (from Permit): R-4 Date sample collected: 11/18/13
Depth: ft. Well Diameter: in.
i to Water Level: 3.11 ft. below measuring point Screened Interval: _ft. to —ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
¢RMIT Number:
Expiration Date: July 31, 2U15
In -Discharge W00004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other. .
FIELD ANALYSES:
pH 4.08 units
Spec. Cond.
Odor
Appearance
sample analyzed: Laboratory Name: Microbac Laboratories
IAMETERS NOTE: Values should reflect dissolved and'colloidal concentrations.
COD 41.5 mg/I Nitrite (NO,) as N mg/I Pb - Lead
Coliform: MF Fecal /100ml Nitrate (NO3) as N 1.15 mgA Zn - Zinc
Coliform: MF Total /100ml Phosphorus: Total as P mg/I
Nt' U MP
Temp. 22 ac DRY at
µMhos time'of
Certification No. NC#11 NC#37714
mgA
mgA
N
( o e, se meNad roc higNy W,GI samples) Orthophosphate mgA Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 316 mgn AI - Aluminum mg/I
pH (when analyzed) units Be - Barium mgA
TOO 3.57 mg/I Ca - Calcium mg/I
Chloride 146 mg/I Cd - Cadmium mg/I
Arsenic mgA Chromium: Total mg/I
Grease and Oils mg/I Cu - Copper mgll ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1 Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 11 mg/I Hg - Mercury. mgA Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 544 µMhos K- Potassium mg4 VOC , method #
Total Ammonia mgA Mg- Magnesium mg/l , method #
(Ammonia N'igegen; NHoas N: Ammonia Nlrogen. Tolal) Mn- Manganese mgll ,method#
TKN as N mg/1 Ni - Nickel mg/I , method #
For Remodlation
Lab Reports): Influent Total VOCs:
Robert Caldwell, Plant Manager
Permidee (ar Authorized Arienn Name and Title - Please Pdnl or one
GW-59 Rev. 112007
t , I
Effluent Total
r i
)
Removal%
3
For Remodlation
Lab Reports): Influent Total VOCs:
Robert Caldwell, Plant Manager
Permidee (ar Authorized Arienn Name and Title - Please Pdnl or one
GW-59 Rev. 112007
t , I
Effluent Total
r i
)
Removal%
3

,- auomi i ruram UN TI-1urW PAYER ONLY
ROUNDWATER QUALITY MONITORING:
ty Name: Aliens, Inc. - Turkey
it Name (if different):
ty Address: 5900 Turkey Highway
(ey NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
LID NUMBER (from Permit): 13-5—a-
Depth: ft.
h to Water Level: 2.30 ft. below measuring point
Airing Point is ft. above land surface
ne of water pumped/bailed before sampling:
10+
Date sample collected: 11/18/13
Well Diameter: _in.
Screened Interval: _ft. to —ft.
Relative M.P. Elevation: ft.
'RMIT Number:
Expiration Date: July 31, 2015
)n-Discharge WQ0004268
UIC
)DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES: WAS
pH 4.22 units Temp. 21 eC DRY at
Spec. Cond. µMhos time of
Odor sampling,
check
Appearance here: ❑
t sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
:AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
73.8 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/1100ml
Nitrate (NO3) as N
6.04 mg/l
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
rug (Nola: Use MPN method forhly tumid samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
188-mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
- mg/I
TOC
3.32 mgll
Ca - Calcium
mgA
Chloride
29.4 mg/I
Cd- Cadmium
mg/I
Arsenic
mg/l
Chromium: Total
mg/I
Grease and Oils
mgll
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
18 mg/I
Hg- Mercury
mg/I
- Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
226 µMhos
K - Potassium
mgll
VOG , method #
Total Ammonia
mg/l
Mg - Magnesium
mgll
#
(Ammonia Nivogen; NH.as N;Ammonia Nhmgen, Talat)
Mn - Man Manganese 9
mgll
,method
, method #
TKN as N
mgll
Ni - Nickel
mg/I
, method #
.+yam•=nw ..rnr (nuaui t_ou "p""?; innuent Iota? VVGs:
--... .-x r 1 .E ;:•.•. '.tb e. _3�..YiutLt �'Cf:.-EJ. �,: s - �.;� � run�*.V.�S'
Robert Caldwell, Plant Manager
Perminee (or Authorized Apenn Name and Title • Please arm or type
GW-59 Rev. 1/2007
Effluent Total VOCs:
VOC

rumin
:R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
PLING INFORMATION Won PIl
L ID NUMBER (from Permit): R-6 Date sample collected: 11/18/13
Depth: ft. Well Diameter: in.
h to Water Level: 4.10 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne ofwater pumped/bailed before sampling: 10+_gallons
:RMIT Number:
Expiration Date: July 31, 2015
in -Discharge W00004268
UIC
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
©: Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other.
FIELD ANALYSES
PH 6.35 units Temp. 20 ec
Spec. Cond. µMhos
Odor
Appearance
I sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
:AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 26.1 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100m1
Nitrate (NO3) as N
<0.0500 mg/l
Zn - Zinc mg/I
Coliform: MF Total 1100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method forhighly Itstu-..pl..)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 150 mg/I
AI - Aluminum
mg/l
PH (when analyzed) units
Be - Barium
mg/I
TOC �14`3;gp
Ca - Calcium
mg/I
Chloride 43.3 mg/I
Cd- Cadmium
mgA
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mg/I
Cu - Copper
mgA
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 21 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 276 pMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia mgA
Mg - Magnesium
mgA
method #
(Ammonlo Nitrogen; NH,as N: Ammonia Nitrogen, Tow)
Mn - Manganese 9
mg/l
,
,method #
TKN as N mgll
NI - Nickel
mg/I
, method #
Ul 1.=,,,ca,nuou oymeuts vnry tr+¢acn t.ao Kepons): Influent I otal VOGs: ma/L Effluent Tntnl.Vr1Cs• ,. A
Robert Caldwell, Plant Manager
Pennittee (or Authorized Agent) Name and Title- Please Print or type
GW-59 Rev. 1/2007 ,.
at
of

ouoml I -runm
QUALITY MONITORING:
PORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
Y NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be samoled:
L ID NUMBER (from Permit): R-7 Date sample collected: 11/18/13
Depth: ft. Well Diameter: In.
h to Water Level: 11.9 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
7e of water pumped/bailed before sampling: 10+ gallons
iRM1T Number:
Expiration Date: 'July 31, 2015!
n-Discharge WQ0004268
UIC
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 4.74 units
Spec. Cond.
Odor
Appearance
Temp. 21 eC DRY at
µMhos time of
t sample analyzed:
LaboratoryName: Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
50.1 mg/l
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
0.696 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mgll
(Note. Use MPN method roe Nghly tumid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
226 mg/l
Al - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mgll
TOC
8.51 mg/I
Ca - Calcium
mg/I
Chloride
88.6 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/l
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
6.1 mgll
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
365 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/l
, method #
(Ammonia Nitrogen; NH1as N; Ammonia Nimogen. Talal)
Mn- Manganese
mgll
,method #
TKN as N
mg/I
NI - Nickel
mg/I
, method #
rt4 AV111UU1a11V11 OyIeLU N] utey JAIU Gn LaO Kepons): mnUenl Iota) VUGs:
Robert Caldwell, Plant Manager
Permittee (or Authorized Agent) Name and Title -Please Print or type
GW-59 Rev. 1/2007
t
VOC
0

CI1m AlT PnDRA nki VCI I l %AI oAMC o AAll V
GROUNDWATER QUALITY MONITORING:
we
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES 7 T
NISION'OFWATERO/ALITYJNFORM,ATIONPROCE9SINGUNIT i. p tf
COMPLIANCE REPORT FORM
917 MAIL SERVICE CENTER, RALEIGH NC 27689 (9
-1817, Phone ij9J 738aRV. i'
FACILITY INFORMATION Please Pdnt Clearly or Type
PERMIT Number: Expiration Date: JUIy 31. 2015
Facility Name: Allens, Inc. -.Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE, OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey NC 28393-9703 County Sampson
-
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
_
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-8
Date sample collected: 11118/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
in.
pH 4.02 units Temp. 22 °C
DRY at
Depth to Water Level: 5.00 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cord. µMhos
time of
Measuring Point is R. shove land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumped bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 48.0 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
� 376mg/l
Zn - Zinc mg/I
Coliform: MF Total 1100m1
Phosphorus: Total as P
m�g/I
(Note Use NPN method her highly heed samples)
Orthophosphate
mgfl
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 200 mg/I
AI - Aluminum
mg/I
pH (when analyzed) units
Ba - Barium
mg/I
TOC 2.65mg/I
Ca - Calcium
mg/I
Chloride 23.7 mg/I
Cd- Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils Ing/1
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe- Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 22 mgm
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 281 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHsas N. Ammonia Ni"gen, Total)
Mn- Manganese
mg/I
,method#
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent
Robert Caldwell, Plant Manager
Permiltee (or Authorized Agenn Name and Title- Please print or type
GW-59 Rev. 112007
VOC Removal°/

DWATER QUALITY MONITORING:
ANCE REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkev Hiahwav
County Sampson
act Person: Robert Caldwell Telephonem 910-596-0028 I
Location/Site Name: No. of wells to be sampled:
P 1
PLING INFORMATION
L ID NUMBER. (from Permit): R-9 Dale sample collected: 11/18/13
Depth: ft. Well Diameter: in.
I to Water Level: 3.70 ft. below measuring point Screened Interval: ft. to _ft.
airing Point is ft._ above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailedbefore sampling: 10+oallons
:RMIT Number:
Expiration Date: July 31, 2015
ln-Discharge WQ0004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
X❑ Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
PH 4.03 units
Spec. Cond.
Odor
Appearance
Temp. 22 eC DRY at
µMhos time of
sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11. NC#37714
:AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 35.0 mg/I
Nitrite (NO2) as N
mg/1
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
2,87 mg/1
Zn - Zinc mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/l
(Note. Use MPN method for highly WINd samples)
-
Ortho has hate
P P
mgll
Other (Specify, Compounds and Concentration Units):
Dissolved Solids: Total
410 mgA
AI - Aluminum
mg/l
PH (when analyzed)
units
Ba - Barium
mg/I
TOC
3.05 mgA
Ca - Calcium
mg/I
Chloride
35.1 mg/I
Cd - Cadmium
mgA
Arsenic
mgll
Chromium: Total
mg/I
Grease and Oils
mg/1
Cu - Copper
mgA
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
47 mgA
Hg - Mercury
mg/l
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
286 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/1
(Ammonia Nirogen. NHaes 17 Ammonia Nitrogen, Total)
Mg - Magnesium
mgll
,method #
Mn -Manganese
mg/l
,method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports):. Influent
Robert Caldwell, Plant Manager
Permittee (or Authorized ADeotl Name and This - Please Ddot'm type
GW-59 Rev. 112007
Effluent Total VOCs:
Removal%

G'VN-'-59A COMPLIANCE. REPORTFORM Pel•mit#i/iQ00D%2(4
(.Submit oat eueh immirorim periml whir Glf,-57Jnrmsj
1
Enter date monitoring results were due. -) j Will this monitoring report (GW-59 and GW-59A)
1'p"S
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
1
IF the answer to question f or 2 is "YES" list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? tfllre answer is "Yes ". conlact the Regional Ogicejor guidance.
4
Are any monitored constituents equal to or above the established standards?
If the answer to question 4 is 'NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s)
exceeding standards in the space provided below.
/q-6 - Tc-, - 19,3
5
For the constituents identified in question 4 above, have standards'been exceeded previously for the
YE, -
NO
same constituent(s) in the same well(s)in the last two years? ,
If the answer to question 5 is 'NO", skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
12-)9.10 - P4 /l,qi rhy/L 7-aa-13 - R` 33.3 A3/L
11-ig-1l Rb 1').3 My/L
3-)S- 11 -A(- lo,b ns/L
11.13 A 1 ,S m L
Are the monitoring wells lisle in section 5 located at or beyond the review boundary?
1'ES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
VES
O
groundwater quality problem?
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposalsystem is having at the review and compliance
boundaries surrounding this facility Failure to do so may subject the nermittee to a Notice of Violation,
fines, and/or penalties.
g
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this
report (Complian``cerrAReport GW-59A) is true and complete to the best of my knowledge.
4lQGl yj 4) /¢ 13
SigbatTir, of emiittee (or Authorized Agent) Date
l\\-j9\ L'iBP011}

Microbac Laboratories, Inc.
2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Allcns, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Project: M/Wells samples - 3/Yearly
Mw #1
1311371-01
Date Reported: November 30, 2013
Date Received: November 18, 2013
Date Sampled: November 18, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
147
COD, Total
30.7
Conductivity
937
Depth to Water Surface
18.9
Nitrate as N
7.28
pH, Field Test
4.76
Total Dissolved Solids
524
Sulfate as SO4
120
Temperature
20
Analyzed by. Microbac Laboratories, Inc. - Ohio Valley
Total Organic Carbon
5.79
State Certi fications:
NCDNR fit
NCDOH 1137714
USDA 93787
mg/L
11/19/13
17:38
JAW
EPA 300.0, Rev. 2.1 (1993)
mg/L
11/20/13
I I:00
DSK
SM 5220 D-1997
umhos/cm
11/20/13
10:30
DSK
SM 251013- 1997
feet
11/18/13
10:50
Field Measurement
mg/L
11/19/13
17:38
JAW
EPA 300.0, Rev. 2.1 (1993)
PH Units
11/18/13
10:50
Field
mg/L.
11/20/13
10:00
JAO
SM2540C-1997
mg/L
11/19/13
17:38
JAW
EPA 300.0; Rev. 2.1 (1993)
°C
11/18/13
10:50
Field
mg/L
11/24/13
3:01
DiH
E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 1 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Microbac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
io
Allens,.Inc Date Reported: November 30, 2013
Mr. Reid Wells Project: N Wells samples-3/Yearly Date Received: November 18, 2013
5900 Turkey Highway Date Sampled: November 18, 2013
Turkey NC, 28393 Sampled By: Davidson
Mw #2
1311371-02
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
97.1
mg/L
11/19/13
17:54
JAW
EPA 300.0, Rev. 2.1 (1993)
24.3
mg/L
11/20/13
11:00
DSK
SM 5220 D-1997 Al2
410
umhos/cm
11/20/13
10:30
DSK
SM 25 1013- 1997
5.10
feet
11/18/13
10:25
Field Measurement
0.660
mg/L
11/19/13
17:54
JAW
EPA 300.0, Rev.2.1 (1993)
4.97
pH Units
11/18/13
10:25
Field
226
mg/L
11/20/13
10:00
JAO
SM 2540 C-1997
9.4
mg/L..
11/19/13
17:54
JAW
EPA 300.0, Rev. 2.1 (1993). '.
20
°C
11/18/13
10:25
Field
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
Total Organic Carbon 3.58
State Certifications:
NCDNR fill
NCDOH 1137714
USDA 43787
mg/L 11/24/13 3:14 DTH E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 2 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and, environmental site assessments.

Microbac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone] Fax [phone]
Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Microbac- Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
ofAnalysis
Project: M/Wells samples - 3/Yearly
Mw #3
1311371-03
Date Reported: November 30, 2013
Dale Received: November 18, 2013
Dale Sampled: November 18, 2013
Sampled By: Davidson
128
mg/L
11/19/13
18:11
JAW
EPA 300.0, Rev. 2.1 (1993)
221
mg/L
11/20/13
11:00
DSK
SM 5220 D-1997
600
umhos/cm
11/20/13
10:30
DSK
SM 25 1013- 1997
1.00
feet
11/18/13
12:00
Field Measurement
0.690
mg/L
11/19/13
I8:11
JAW
EPA 300.0, Rev. 2.1 (1993)
5.62
pH Units
11/18/13
12:00
Field
568
mg/L
11/20/13
10:00
JAO
SM 2540 C-1997
55
mg/L�.
11/19/13
18:11
JAW
EPA 300.0,Rev. 2:1(1993)
20
°C
11/18/13
12:00
Field
Analyzed by: Microbac laboratories, Inc - Ohio Valley
Total Organic Carbon 3.38
Slat. Certifications:
NCDNR If II
NCDOII 1137714
USDA d3787
at 11/25/13 15:32 DIH E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 3 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Mictobac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone] Fax [phone]
FAYETTEVILLE DIVISION
Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Microbac- Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Project: M/WeOs samples-3/Yearly
Mw #4
1311371-04
Date Reported: November 30, 2013
Date Received: November 18, 2013
Date Sampled: November I8, 2013
Sampled By: Davidson
21.5
mg/L
11/19/13
18:27
JAW
EPA 300.0, Rev. 2.1 (1993)
78.7
mg/L
11/20/13
11:00
DSK
SM 5220 D-1997
157
umhos/cm
11/20/13
10:30
DSK
SM 251OB-1997
5.90
feet
11/18/13
12:35
Field Measurement
4.54
mg/L
11/19/13
18:27
JAW
EPA 300.0, Rev. 2.1 (1993)
4.35
pH Units
11/18/13
12:35
Field
84.0
mg/L
11/20/13
10:00
JAO
SM 2540 C-1997
8.4
mg/L
11/19/13
18:27 L
JAW
EPA 300.0,Rev. 2ah(1993)
21
°C
11/18/13
12:35
Field
Analyzed by: Microbac Laboratories, Inc - Ohio Valley
Total Organic Carbon 4.60
Slate Ceditintions:
NCDNR IfII
NCDOH #37714
USDA #3787
mg/L 11/25/13 15:45 DIH E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 4 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Microbac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Aliens, Inc Date Reported: November 30, 2013
Mr. Reid Wells Project: M/Wells samples - 3/Yearly Date Received: November 18, 2013
5900 Turkey Highway Date Sampled: November 18, 2013
Turkey NC, 28393 Sampled By: Davidson
R-I
1311371-05
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
114
mg/L
11/19/13
18:44
JAW
EPA 300.0, Rev. 2.1 (1993)
COD, Total
218
mg/L
11/20/13
11:00
DSK
SM 5220 D-1997
Conductivity
474
umhos/cm
11/20/13
10:30
DSK
SM 251OB-1997
Depth to Water.. Surface
2.50
feet
11/18/13
15:00
Field Measurement
Nitrate asN
1.03
mg/L
11/19/13
18:44
JAW
EPA 300.0, Rev. 2.1 (1993)
pH, Field Test
4.45
pH Units
11/18/13
15:00
Field
Total Dissolved Solids
278
mg/L
11/20/13
10:00
JAO
SM 2540 C-1997
Sulfate as SO4
11
mg/L
11/19/13
18:44
JAW .
EPA 300.0, Rev. 2.L'(1993)
Temperature
21
°C
11/18/13
15:00
Field
Analyzed by: Microbac Laboratories, Inc. -Ohio Valley
Total Organic Carbon
9.97
mg/L
11/25/13
15:58
DIH
E415.1
State Certifications: Respectfully Submitted
NCDNR 1ll I
DOH 13714
US>I378378
USDA 7
Bonnie K. Sanders, Senior Project Manager
Page 5 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Microbac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC.28306 Phone [phone]
Fax [phone]
PAYE IEVILLE DIVISION
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Aliens, Inc
Date Reported: November 30, 2013
Mr. Reid Wells
Project: M/Wells samples - 3/Yearly Date Received: November 18, 2013
5900 Turkey Highway
Date Sampled: November 18, 2013
Turkey NC, 28393
Sampled By: Davidson
R-2a
1311371-06
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
14.4
mg/L
11/19/13
19:01
JAW
EPA 300.0, Rev. 2.1 (1993).
COD, Total
<I0.0
mg/L
11/25/13
9:10
DSK
SM 5220 D-1997
Conductivity
114
umhos/cm
11/20/13
10:30
DSK
SM 25 1013- 1997
Depth to Water Surface
3.30
feel
11/18/13
13:50
Field Measurement
Nitrate as N
1.01
mg/L
11/19/13
19:01
JAW
EPA 300.0, Rev. 2.1 (1993)
pH, Field Test
4.20
pH Units
11/18/13
13:50
Field
Total Dissolved Solids
62.0
mg/L
11/20/13
10:00
JAO
SM 2540 C-1997
Sulfate as SO4
17
mg/L '
11/19/13
19:01
JAW
EPA 300.0, Rev. 2.1 (1993)
Temperature
21
°C
11/18/13
13:50
Field
Analyzed by: Microbac laboratories, Inc. -Ohio Valley
Total Organic Carbon
2.59
mg/L
11/25/13
16:33 i
OUR
E415.1
State Certifications:
Respectfully Submitted
NCDNR 1111
USDA 43787
Bonnie K. Sanders, Senior Project Manager
Page 6 of 15
Microbac Laboratories, Inc, analyzing water, waste water, food and environmental site assessments.

Midrobac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Aliens, Inc Date Reported: November 30, 2013
Mr. Reid Wells Project: NMells samples-3/Yearly Date Received: November 18, 2013
5900 Turkey Highway Date Sampled: November 18, 2013
Turkey NC, 28393 Sampled By: Davidson
R-3
1311371-07
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Miaobac - Fayetteville Dwislon
,
Chloride
134
mg/L
11/19/13
19:17
JAW
EPA 300.0, Rev. 2.1 (1993)
COD, Total
24.3
mg/L
11/20/13
11:00
DSK
SM 5220 D-1997
Conductivity
583
umhos/cm
I1/20/13
10:30
DSK
SM 2510B-1997
Depth to Water Surface
3.10
feet
11/18/13
14:45
Field Measurement
Nitrate as N
2.46
mg/L
11/19/13
19:17
JAW
EPA 300.0, Rev. 2.1 (1993) Al2
pH, Field Test
3.67
pH Units
11/18/13
14:45
Field
Total Dissolved Solids
254
mg/L
11/20/13
10:00
JAO
SM 2540 C-1997
Sulfate as SO4
27
mg/L
11/19/13
19:17
JAW
EPA 300.0, Rev. 2.1 (1993) Al2
Temperature
19
°C
11/18/13
14:45
Field
Analyzed by: Miaobac tabs stories, Inc. - Ohio Valley
Total Organic Carbon
2.17
mg/L
11/25/13
16:46
D1H
E415.1
State Ccrtilicalions:
Respectfully Submitted
NCDNR Illl
NCDOH 1137714
/ p
USDA #3787
Bonnie K. Sanders, Senior Project Manager
Page 7 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Microbac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.964.1920 Phone
910.864.8774 Fax
of Analysis
Allen, Inc Date Reported: November 30, 2013
Mr. Reid Wells Project: M/1Vells samples - 3/Yearly Dale Received: November 18, 2013
5900 Turkey Highway Date Sampled: November 18, 2013
Turkey NC, 28393 Sampled By: Davidson
R-4
1311371-08
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
146
mg/L
11/19/13 20:40
JAW
EPA 300.0, Rev. 2.1 (1993)
41.5
mg/L
11/20/13 I1:00
DSK
SM 5220 D-1997
544
umhos/cm
11/20/13 10:30
DSK
SM251OB-1997
3.11
feet
11/18/13 13:50
Field Measurement
1.15
mg/L
11/19/1320:40
JAW
EPA 300.0, Rev. 2.1 (1993)
4.08
pH Units
11/18/13 13:50
Field
316
mg/L
11/20/13 10:00
JAO
SM 2540 C-1997
11
mg/L
11/19/1320:40
JAW
EPA300.0,Rev.2.1(1993)
22
oC
11/18/13 13:50
Field
Analyzed by:Miuobac laboratories, Inc. -Ohio Valley
Total Organic Carbon 3.57
State Certifications:
NCDNR lllI
NCDOH 1137714
USDA 43787
mg/L 11/25/13 16:59 DTH E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 8 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Midrobac Laboratories, Inc.
2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
Allen. Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Project: M/Wells samples - 3/Yearly
R-5a
1311371-09
Date Reported: November 30, 2013
Date Received: November 18, 2013
Date Sampled: November 18, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Divlslon
Chloride
29.4
COD, Total
73.8
Conductivity
226
Depth to Water Surface
2.30
Nitrate as N
6.04
pH, Field Test
4.22
Total Dissolved Solids
188
Sulfate as SO4
18
Temperature
21
Analyzed by: Microbac laboratories, Inc. - Ohio Valley
Total Organic Carbon
3.32
State Certifications:
NCDNR fill
NCDOH 937714
USDA #3787
mg/L
11/19/13 20:57
JAW
EPA 300.0, Rev. 2.1 (1993)
mg/L
11/20/13 11:00
DSK
SM 5220 D-1997 Al2
umhos/cm
11/20/13 10:30
DSK
SM 251OB-1997
feet
11/18/13 13:30
Field Measurement
mg/L
11/19/1320:57
JAW
EPA 300.0, Rev. 2.1 (1993)
pH Units
11/18/13 13:30
Field
mg/L
11/20/13 10:00
JAO
SM2540C-1997 Sl
mg/L
11/19/1320:57
JAW
EPA 300.0, Rev. 2.1 (1993)
°C
11/18/13 13:30
Field
mg/L
11/25/13 17:12
DIH
E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 9 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Mi6robac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone] Fax [phone]
FAYETTEVILLE DIVISION
Allens; Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Project: M/1Vells samples-3/Yearly
R-6
x 1311371-10
Date Reported: November 30, 2013
Date Received: November 18, 2013
Date Sampled: November 18, 2013
Sampled By Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
43.3
mg/L.
11/19/1321:13
JAW
EPA 300.0, Rev. 2.1 (1993)
COD, Total
26.1
mg/L
11/25/13 9:10
DSK
SM 5220 D-1997
Conductivity
276
utnhos/cm
11/20/13 10:30
DSK
SM 2510B-1997
Depth to Water Surface
4.10
feet
11/18/13 13:30
Field Measurement
Nitrate as
<0.0500
mg/L
11/19/1321:13
JAW
EPA 300.0, Rev. 2.1(1993)
pH, Field Test
5.35
pH Units
11/18/13 13:30
Field
Total Dissolved Solids
150
mg/L
11/20/13 10:00
JAO
SM 2540 C-1997
Sulfate asSO4
21
mg/L
11/19/1321:13
JAW
EPA 300.0; Rev. 2.1 (1993)
Temperature
20
°C
11/18/13 13:30
Field
Malyzed by: Microbac laboratories, Inc -Ohio
Valley
Total Organic Carbon
14.3
mg/L
11/26/13 13:48
DIH
E415.1
State Certifications:
Respectfully Submitted
NCDNR Yll,
D1137714
3
p'787
378714 US
USDAA
Bonnie K. Sanders, Senior Project Manager
Page 10 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Microbac Laboratories, Inc.
2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
t
Project: MAYells samples - 3lYearly
R-7
1311371-11
Date Reported: November 30, 2013
Date Received: November 18, 2013
Date Sampled: November 19, 2013
Samoled Bv: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
88.6
mg/L
11/19/13 21:30
JAW
EPA 300.0, Rev. 2.1 (1993)
COD, Total
50.1
mg/L
11/25/13 11:20
DISK
SM 5220 D-1997
Conductivity
365
urnhos/cm
11/20/13 10:30
DSK
SM 251OB-1997
Depth to Water Surface
11.9
feet
11/18/13 13:00
Field Measurement
Nitrate as N
0.696
mg/L
11/19/13 21:30
JAW
EPA 300.0, Rev. 11(1993)
PH, Field Test
4.74
pH Units
11/18/13 13:00
Field
Total Dissolved Solids
226
mg/L
11/20/13 10:00
JAO
SM 2540 C-1997
Sulfate as SO4
6.1
mg/L
11/19/13 21:30 -
JAW
EPA300.0, Rev. 2.1 (1993)
Temperature
21
°C
11/18/13 13:00
Field
Analyzed by: Microbac laboratories, Inc. - Ohio Valley
Total Organic Carbon
8.51
mg/L
11/26/13 14:01
DTH
E415.1
State Certifications:
Respectfully Submitted
NCDNR 811
NCDOII 1137714
1�
`'"it1/Ylcl-Q/to�
USDA #3797
Bonnie K. Sanders, Senior Project Manager
Page 11 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

Microbac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
ia
Aliens, Inc Date Reported: November 30. 2013
Mr. Reid Wells , Project: M/Wells samples-3/Yearly Date Received: November 18, 2013
5900 Turkey Highway Date Sampled: November 18, 2013
Turkey NC, 28393 Sampled By: Davidson
R-8
1311371-12
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by:.Microbac- Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
23.7
mg/L
11/19/13 21:47
JAW
EPA 300.0, Rev. 2.1 (1993)
48.0
mg/L
11/25/13 11:20
DSK
SM 5220 D-1997
281
tmthos/cm
11/20/13 10:30
DSK
SM251OB-1997
5.00
feet
11/18/13 12:50
Field Measurement
12.7
mg/L
11/19/13 21:47
JAW
EPA 300.0, Rev. 2.1 (1993)
4.02
pH Units
11/18/13 12:50
Field
200
mg/L
11/20/13 10:00
JAO
SM 2540 C-1997
22
mg/L
11/19/13 21:47
JAW
EPA 300.0,.Rev. 2.1 (1993)
22
°C
11/18/13 12:50
Field
Analyzed by: Microbac laboratories, Inc. - Ohio Valley
Total Organic Carbon 2.65
State Certifications:
NCDNR #11
NCDOIi 1137714
USDA 43787
mg/L 11/26/13 14:14 DIH E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 12 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

J
Microbac Laboratories, Inc. 2592 Hope Mills Road Fayetteville, NC 28306 Phone [phone]
Fax [phone]
FAYETTEVILLE DIVISION
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
of Analysis
Aliens. Inc Date Reported: November 30. 2013
Mr. Reid Wells Project: M/Wells samples - 3/Yearly Date Received: November 18, 2013
5900 Turkey Highway Date Sampled: November 18, 2013
Turkey NC, 28393 Sampled By: Davidson
R-9
1311371-13
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
35.1
mg/L
11/19/13 22:03
JAW
EPA 300.0, Rev. 2.1 (1993)
35.0
mg/L
11/25/13 11:20
DSK
SM 5220 D-1997
286
umhos/cm
11/20/13 10:30
DSK
SM 251OB-1997
3.70
feet
11/18/13 15:05
Field Measurement
2.87
mg/L
11/19/13 22:03
JAW
EPA 300.0, Rev. 2.1 (1993)
4.03
pH Units
11/18/13 15:05
. Field
410
mg/L
11/20/13 10:00
JAO
SM 2540 C-1997
47
mg/L
11/19/13 22:03
JAW
EPA 300.0, Rev. .2.1 (1993)
22
°C
11/18/13 15:05
Field
Analyzed by: Miaobac taboatcaes, Inc - Ohio Valley
Total Organic Carbon 3.05
State Certifications:
NCDNR 1/11
NCDOH 1137714
USDA k3787
mg/L 11/26/13 14:33 DIH E415.1
Respectfully Submitted
Bonnie K. Sanders, Senior Project Manager
Page 13 of 15
Microbac Laboratories, Inc. analyzing water, waste water, food and environmental site assessments.

�iG Up Ni 6>i C R I6g gr V,, Z6y ', v
w� ly `
S t.N
Ltzalit)? Vegetublt`s
5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone]
December 12, 2013
Dept. of Environmental & Natural Resources RE—CE I E ®
Division of Water Quality— Information Processing Unit DEC 18 2013
1617 Mail Service Center
Raleigh. NC 27699-1617
[phone] VVHItt\wumu. � ;;tGIION
AW)P IGTUIN0p0'FSSINi:UNr
RE: Groundwater Quality Monitoring Report
Allens, Inc. — Turkey, NC Facility
Permit # WQ0004268
Enclosed are the original and one copy of the Groundwater Monitoring Report on forms OW-59
and G W-59A, and the lab report for Aliens, Inc — Turkey, NC facility for samples collected in
November. 2013.
If you have any questions or require any additional information, please contact me by
phone at [phone].
Sincerely,
Robert Caldwell
Plant Manager
Aliens. Inc. Turkey facility
CC: Laura Mushinski, Aliens, Inc
Reid Wells. Al lens. Inc —Turkey facility
RECEIVED
DEC 2 3 2013
DENR-FAYETTEVILLE REGIONAL OFFICE

SUBMI F FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
OEP, ATr3ENTOF ENVIRONMENT&'NATURAL RESOURCES
COMPLIANCE REPORT FORM___m
IVISION'OFWATER QUALITYINFORMATION PROCESSING
617MAILSERVICE CENTER. RALEIGHNC27699.1617 Phone.(919)733a221
PERMIT Number: Expiration Date: July 31, 2015
FACILITY INFORMATION Please Pant clean or,Type
Facility Name: Aliens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey '' NC 28393-9703 County Sampson
® Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
(
No. of wells to be sampled: 13
❑ Water Source Heat Pump ❑ Other:
-
Irom Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MWA
Date sample collected: 7/22/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH 5.33 units Temp. 19 °C
DRY at
Depth to Water Level: 7 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cord. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:❑
Samples for metals were collected unfiltered: OYES
❑ NO and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 26.4 mg/I
Nitrite (NO2) as
mg/I
Pb - Lead mg/I
Colifonn: MF Fecal /100m1
Nitrate (NO3) as N 3.51
mg/l
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPNM.Mod1orhJ9h1yturNdsamp1es)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 126 mg/l
Al - Aluminum
mg/I
pH (when analyzed) units
Ba - Barium
mg/I
TOC 6.85 mgA
Ca - Calcium
mg/I
Chloride 18.7 mg/I
Cd - Cadmium
mg/I
Arsenic mgfl
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 23 mgfl
Hg - Mercury
mg/l
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 183 µMhos
K - Potassium
mgA
VOC , method #
Total Ammonia mgfl
Mg - Magnesium
mgfl
, method #
(Ammonia Ni"oen: NH as N: Ammonia Nitrogen. Torah
Mn - Manganese
mg/I
method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
Dui nUmerunrron oysrems unity pvrracn Lao Reports): influent I otal VOGs: mg(L Effluent Total VOCs: me/L VOC Removal°
Robert Caldwell, Plant Manager
Peartittee (or Authorized Agent) Name and Title - Please pint or type
GW-59 Rev. 1/2007

FORM
ONLY
:R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
-
L ID NUMBER (from Permit): MW-2 Date sample collected: 7122/13
Depth: ft. Well Diameter: in. _
1 to Water Level: 4.11 ft. below measuring point Screened Interval: ft. to ft.
Turing Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
:RMIT Number:
Expiration Date: July 31, 2015
on -Discharge W00004268
UIC
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
Il Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 5.90 units
Spec. Cond.
Odor
Appearance
Temp. 20 aC DRY at
time of
Date sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved
and colloidal concentrations.
COD
30.7 mgll
Nitrite (NO2) as N
mgA
Pb - Lead mgll
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
0.706 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/loom1
Phosphorus: Total as P
mg/I
(Nola; Use MPN matters for highly turtoid samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
186 mgA
AI - Aluminum
mgll
pH (when analyzed)
units
Be - Barium
mgA
TOC
6.87 mgA
Ca - Calcium
mg/1
Chloride
86.6 mgA
Cd- Cadmium
mg/I
Arsenic
mgll
Chromium: Total
- mgA
Grease and.Oils
mg/I
Cu - Copper
mg/I '
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
9.8 mgA
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
385 µMhos
K- Potassium
mg/I'
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/l
, method #
(Ammonia Nitration; NH. as N; Ammonia nuagen, Total)
Mn- Manganese
mgA
,method#
TKN as N
mg/l
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports):
Influent Total VOCs:
mg/L. Effluent Total VOCs: -mg/L VOC Removal%
Robert Caldwell, Plant Manager
Perrnittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007

SUBMIT FORM ON
QUALITY MONITORING:
PORT FORM
Name: Allens, Inc. -
Name (if different): _
Address: 5900 Turkey
act Person: Robert Caldwell
Location/Site Name:
County Sampson
Telep hone#: 910-596-0028
No. of wells to be sampled: 13
LID NUMBER (from Permit): MW-3 Date sample collected: 7/22113
Depth: ft. Well Diameter: in.
h to Water Level: 0.900 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumpedibailed before sampling: 10+ gallons
Aes for metals were collected unfiltered: ❑YES ❑ NO and field acidified- M YFS F1 Nn
:RMIT Number:
n-Discharge W00004268
Expiration Date: July 31, 2015
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES
PH 6.33 units Temp. 22 oC
Spec. Cond. µMhos
Odor
Appearance
a sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
71.7 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
1,35 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
WQ:OTgq/I
Al - Aluminum
mg/1
PH (when analyzed)
units
Ba - Barium
mg/I
TOC
2.66 mg/I
Ca - Calcium
mg/I
Chloride
120 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mgA
Cu . Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
55 mgA
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
620 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mg/l
Mg - Magnesium
mgA
, method #
(Ammonia Nitrogen; NH3as N; Ammonia
Nitrogen, Total)
Mn -Manganese
mg/1
,method #
TKN as N
mg/l
Ni - Nickel
mg/I
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Plant Manager
Permmee (or Authorized Anent) Name and Title - Please print or type
GW-59 Rev. 112007
at
of

auoml I runm
QUALITY MONITORING:
Name: Allens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
ty NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 13 I
P ')
PLING INFORMATION
LID NUMBER (from Permit): MW-4 Date sample collected: 712.2/13 .`
Depth: ft. Well Diameter: in.
h to Water Level: 1.50 ft. below measuring point Screened Interval: _ft. to _ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+gallons
:RMIT Number:
m-Discharge W00004268
Expiration Date: July 31. 201b
UIC
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 5.73 units
Spec. Cond.
Odor
Appearance
Temp. 24 eC DRY at
µMhos time of
e sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
:AMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
COD
76 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Coliform: MF Feral
/100ml
Nitrate (NO3) as N
8.10 mg/I
Zn - Zinc mg/I
Coliform: MF Total
Moonlit
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly lurhd samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids; Total
76 mgA
At - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOG
3.21 ni
_ Ca -Calcium-
mg/I
Chloride
19.7 mgA
Cd - Cadmium
mgn
Arsenic
mg/I
. Chromium: Total
mgn
Grease and Oils
mg/I
Cu - Copper
mg/(
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron.
mgn
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
6.6 mg/I
Hg - Mercury
mg/l
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
183 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mgA
Mg - Magnesium
mgn
,method #
(Ammonia Nitrogen; NH3 as N: Ammonia Nitrogen. Total)
Mn - Man Manganese g
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
vulu:
Robert Caldwell, Plant Manager
Permittee(or Authorized Agenn Name and Title- Please print or type - Signature
GW-59 Rev. 112007
enment I otal Vucs:
VOC

QUALITY MONITORING:
PORT FORM
Name: Aliens, Inc. - Turkey `
Name (if different):
Address: 5900 Turkey Highway
Y 1. NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:,
LID NUMBER (from Permit): R-1 Date sample collected: 7/22/13
Depth: ft. Well Diameter. in.
t to Water Level: 2.50 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
:RMIT Number:
Expiration Date: July 31, 2015
m-Discharge WQ0004268
UIC
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 5.84 units
Spec. Cond.
Odor
Appearance
Temp. 23 ec DRY at
µMhos time of
sample analyzed:
Laboratory Name: Mlcrobac Laboratories
Certification No. NC#11 NC#37714
;AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
113 mg/1
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
0.709 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
102 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
.. units
Ba - Barium
mg/I
TOC
3.94 mg/1-
Ca - Calcium
mg/l
Chloride
23 mg/I
Cd - Cadmium
mg/l
Arsenic
. Mg/I
Chromium: Total
mg/l
Grease and Oils
. mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
16 mg/I
Hg - Mercury
mg/1
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
140 µMhos
K - Potassium
- mg/1
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NH3as N: Ammonia Nitrogen, Total)
Mn- Manganese
mgll
- -
,method .#
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
Y. 4 r' 1• ♦•
I certify that, to the bast' my knoMedge and belie/ the Ihfo`rmation subMi ed In this reporjas Inie, accurate and complete(.lantl that the labSratory,analyllcal da(a was produce using approved-rnethoda o(anaysls by,a •'
DWocadifietl Wborat "elamaware that there eresr nigcant nalties'for sudmitling lake Informa(ion,ihdudin`Ihe'ossibdi of fines enrol mment:for know-n vlol11 abons. "C,'•;}5a :,4r
RobertCaldwell,_e
Date)Permittee (or Authorized Agent) Nettle and Title - Please Print or Woe
- rr

ON
=R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc.
Name (if different): _
Address: 5900 Turke
key NC 28393-9703 County Sampson
act Person: RobertCaldwell Telephone#: [phone] j
Location/Site Name: _ No. of wells to be sampled: 13
:RMIT Number:
Expiration Dale: July 31. 2015
n-Discharge WQ0004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION
BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
© Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
WELL ID NUMBER (from Permit): R-2
Date sample collected: 7/22113;
FIELD ANALYSES:
If WELL
WAS
Well Depth: ft.
Well Diameter: in.
pH 5.39 units Temp. 27 eC
DRY at
Depth to Water Level: 2.30 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. µMhos
time of
Measuring Point is ft. above land surface
II
Relative M.P. Elevation: I ft.
Odor
sampling,
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES i❑ NO
❑
sample analyzed: LaboratoryName: Microbac Laboratori(
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
65.2 mg/I
Nitrite (NO2) as N
mg/I
Coliform: MF Fecal
/100m1
Nitrate (NO3) as N
1.02 mg/I
Coliform: MF Total
/loom[
Phosphorus: Total as P
mg/l
(Note: Use MPN method for highly lursid samples)
Orthophosphate
mg/I
Dissolved Solids: Total
42 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Ba - Barium
mg/I
TOC
2.81 mg/I
Ca - Calcium
i mg/I
Chloride
15.1 mg/I
Cd - Cadmium
l mg/I
Arsenic
mg/I.
Chromium: Total
i mg/I
Grease and Oils
mg/I.
Cu- Copper
mg/1
Phenol
mg/1
Fe - Iron
mg/I
Sulfate
26 mg/I
Hg - Mercury
mg/I
Specific Conductance
148 µMhos
K- Potassium
mg/I
Total Ammonia
mg/l
Mg - Magnesium
mg/I
(Ammonia Nitrogen: NHeas N; Ammonia Nitrogen, Total)
Mn- Maneanese
i mo/I
TKN as N mg/I Ni - Nickel
Certification No. NC#11 NC#37714
Pb - Lead mgl[
Zn - Zinc mg/1
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method N. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mo/L Effluent Total VOCs: r.,nn vnc Rpm .io/
Robert Caldwell, Plant Manager
Permittee (or Authorized Adam) Name and Title - Please print or type
GW-59 Rev. 1/2007

SUBMIT FORM ON YFI I nW PAPFR nMl V
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OFjENVIRONMENT8.NATURAL.•RESOURCES, y xv
NISIONOFWATER' QUALITY -INFORMATION PROCESSING UNITt st K
COMPLIANCE REPORT FORM
91'7MAILSERVICECENTERRALEIGH;NC27899N617 Phone:(919)�733-3221 ;;
FACILITY INFORMATION Please Pdnt Clearly or Type f-
-
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING.MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery'
Turkey ' "" NC 28393-9703 County Sampson
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled: 13
❑ Water Source Heat Pump ❑ Other:
(from Per Na
I
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-3
Date sample collected: 7/22113
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in.
pH 5.36 units Temp. 24 oC
DRY at
Depth to Water Level: 3.10 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
sampling,
check
Volume of water pumped bailed before sampling:
10+ gallons
Appearance
here: ElSamples
for metals were collected unfiltered: ❑YES
El and field acidified: ❑ YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:
'
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 56.6 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal I100ml
Nitrate (1,103) as N 3.80
mg/I
Zn - Zinc mg/I
Coliform: MF Total I100ml
Phosphorus: Total as P
Mgt]
(Nat.: Use MPN M.M.d for highly turbidsampl.s(
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 176 mgll
Al - Aluminum
mgll
pH (when analyzed) units
Ba - Barium
mg/l
TOC 3.31 mgfl
Ca - Calcium
mg/I
Chloride 83 mg/I
Cd- Cadmium
mgn
Arsenic mgll
Chromium: Total
mg/I
Grease and Oils mg/1
Cu - Copper
mg/I
ORGANICS: (by GC, GCIMS, HPLC)
Phenol mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 15 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 386 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammne Ningen; NH,as N. Amm.nia Ningen. Tota9
Mn- Manganese
mg/I
,method#
TKN as N mg/I
Ni - Nickel
mg/l
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Plant Manager
Permittee (or Authorized Mean Name and Tdle - Please Print or type
GW-59 Rev. 1/2007
0

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
EPARTMENT OFENVIRONMENT & NATURAL RESOURCES f
DIVISION
COMPLIANCE REPORT FORM
OF WATERQUALITYaNFORMATIONPROCE3SINGUNIT
617MAILSERVICECENTER;RAL'EIGH,NC27699.1617i Phone[phone] =
FACILITY INFORMATION Please Pont Clearly or Type'
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑Remediation: Infiltration Gallery
Turkey INC 28393-9703 County Sampson
-
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other.
Gorr Pmmit
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): R-4
Date sample collected: 7/22113
FIELD ANALYSES:
If WELL
WAS
Well Depth: ft.
Well Diameter:
in.
pH 4.89 units Temp. 26 eC
DRY at
Depth to Water Level: 3.10 ft. below measuring point
Screened Interval:
to
ft. Spec. Cord. µMhos
time of
Measuring Point is ft. above land surface
_ft.
Relative M.P. Elevation:
ft.
Odor
sampling,
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
check
here:
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
❑
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 41.5 mg/l
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
1.33 mg/I
Zn - Zinc mg/l
Coliform: MF Total 1100ml
Phosphorus: Total as P
mg/l
(Note: Use MPN method for highly hiMid samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 180 mg/I
At - Aluminum
mgtI
pH (when analyzed) units
Be - Barium
mg/l
TOC 3.62mg/t
Ca - Calcium
mg/I
Chloride 74 mg/I
Cd- Cadmium
mgll
Arsenic mg/I
Chromium: Total
mgll
Grease and Oils mg/I
Cu - Copper
mgll
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mgh
Fe - Iron
mgll
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 13 mg/I
Hg - Mercury
mgil
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 337 µMhos
K- Potassium
mg/I
VOC ,method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nilrogen; NHnas N; Ammonia Nthogen. Total)
Mn -Manganese
moll
,method #
TKN as N mgll
Ni - Nickel
mg/I
, method #
For Romeatatlon systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Plant Manager
Permittee (or Authorized Apenh Name and Title - Please print or type
GW-59 Rev. 112007

S lnenT FCR"' " o" ,
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF ENVIRONMENTS NATURAL RESOURCES
COMPLIANCE REPORT FORM
DIVISIONOFWATER QUALITY-INFORMATION,PROCESSINGUNITa f
617MAIL sERVICECENTER,RALEIGH;NC27699-i677'--Phono::(919L73"!2 ,
FACILITY INFORMATION Please Print Clearly or Type
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turke- NC 28393-9703 County Sampson
- •
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13 •.
❑ Water Source Heat Pump ❑ Other:
fmm Pemvl
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): R-5a
Date sample collected: 7/22/13
FIELD ANALYSES:
If WELL
WAS
Well Depth: ft.
Well Diameter:
in.
pH 5.46 units Temp. 27 aC
DRY at
Depth to Water Level: 2.10 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cond. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
Samples for metals were collected unfiltered: ]YES
❑ NO and field acidified: OYES
❑ NO
❑
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 104 mgfl
Nitrite (NO2) as N
mgfl
Pb - Lead nt
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
41•84 mg/I
Zn - Zinc mg/1
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: use MPN method for highly lured semples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 122 mgfl
At - Aluminum
mgfl
pH (when analyzed) units
Ba- Barium
mg/I
TOC 3.66 mgfl
Ca - Calcium
mgll
Chloride 22.2 mg/I
Cd - Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mgfl
Grease and Oils mg/l
Cu - Copper
I mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 23mg/I
Hg- Mercury
mg/1
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance 206 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/l
, method #
(Ammania Nitrogen; NHsas N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
method #
TKN as N mg/I
Ni -Nickel
mg/l
, method #
For nemewation systems Onty (Attach Lab Reports): Influent Total VOCS; mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Plant Manager
Pennittee, (or Authorized Agent) Name and Tille- Please print or type
GW-59 Rev. 112007
Signature of e�rmilfei

SI lPRAIT=ODRA rVd VCi 1 Mnr o
GROUNDWATER QUALITY MONITORING:
LDEPARTMENT
OF{ENVIRONMENT S NATURAL' RESOURCES " ,t,
COMPLIANCE REPORT FORM
DIVISION OF WATER 'QUA LITYaNFORMATION PROCESSING UNIT
17 MAIL SERVICE CENTER RALEIGH,NC27699.1617',PhoKo:(919)733-3 21.
FACILITY INFORMATION Please Print clearly or Type
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. -Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey "'-'� NC 28393-9703 County Sampson
`
I
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well LocationlSite Name:
No, of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
from Permit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-6
Date sample collected: 7/22/13 .
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: —
in.
pH 6.18 units Temp. 24 eC
DRY at
Depth to Water Level: 3.60 ft. below measuring point
Screened Interval:
to
Spec. Cond, µMhos
time of
Measuring Point is ft. above land surface
_ft.
Relative M.P. Elevation:
_ft.
ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
❑
LABORATORY INFORMATION
Date sample analyzed:
-
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 117 mg/I
Nitrite (NO,) as N
mg/l
Pb - Lead mg/I
Coliform: MF Feral /100ml
Nitrate (NO3) as N
0.-731 mgll
Zn - Zinc mg/l
Cofform: MF Total /100ml
Phosphorus: Total as P
mgll
(Note: Use MPN melhod for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 178 mg/I
AI - Aluminum
-mg/1
pH (when analyzed). units
Be - Barium
mgh
TOC e4ol:MMign
Ca - Calcium
mg/l
Chloride 31.2 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/1
Grease and Oils mg/I
Cu - Copper
mg/I.
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 12 mgf
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 238 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
,method #
(Ammonia Nitrogen; NHaas N; Ammonia Nitrogen, Teton
Mn-Manganese
mg4
,method#
TKN as N mgA
Ni - Nickel
mg/I
, method At
Robert Caldwell, Plant Manager
Permittee (or Authorized Anent) Name and Tdle- Please print or type
R . Ifluu,

SUBMIT FORM ON Y I I OW PAPER ONLY
.TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
:y """ NC 28393-9703 County Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 13
LID NUMBER (from Permit): R-7 Date sample collected: 7/22/13
Depth: ft. Well Diameter: in.
i to Water Level: 3.00 ft. below measuring point Screened Interval: ft. to ft.
iuring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
IRMIT Number:
Expiration Date: July 31, 2015
n-Discharge WQ0004268
UIC
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
1 Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other: _
FIELD ANALYSES
pH 5.43 units Temp. 23 eC
Spec. Cond. µMhos
Odor
Appearance
sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values
should reflect dissolved and
colloidal concentrations.
COD
63 mg/I
Nitrite (NO,) as N
mg/l
Pb - Lead mg/I
Coliform: MF Fecal
1100ml
Nitrate (NO3) as N
0.861 mg"
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly Wraid
samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
174 mg/l
At - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/l
TOC
`17nTmg/I
Ca - Calcium
mg/I
Chloride
69 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/l
;Grease and Oils
mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iran
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
7.6 mg/I
Hg- Mercury
mg/l
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
300 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia
. mgll
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHras N; Ammenia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N
mg/l
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCsl mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Plant Manager
Permittee (or Authorized Apent) Name and Title- Please print or type Slenalure of
aw-59 Rev. 112007
at
of
N

Al IRM IT Fr1RM Ant VG I rAMI on oco n
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF.ENVIRONMENT'& NATURAL RESOURCES
COMPLIANCE REPORT FORM
r
1,14
IVISION OF WATER CIUALITY;INFORMATION PROCESSING UNIT." .
617MAIL`-SERVI6E'CENTER,RALEIGH„NC27699,1617%PhgriaS(9j9)'733J221.
FACILITY INFORMATION Please Pont cready or Type
PERMIT Number: Expiration Dale: July 31, 2015
Facility Name: Allens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey "" NC 28393-9703 County Sampson
91 Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other.
fmm Pemul
SAMPLING INFORMATION
K WELL
WELL ID NUMBER (from Permit): R-8
Date sample collected: 7122/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in.
pH 4.85 units Temp. 23 °c
DRY at
Depth to Water Level: 2.60 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cord. µMhos
time of
Measuring Point is ft, above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumpedfbailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 26.4 mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N VWIT41m /I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
m /I
(Note: Use MPN method forhlghly turgid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 140 mgn
AI - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mg/I
TOG 3.32 mg/I
Ca - Calcium
mg/I
Chloride 17 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mgll
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 28 mgn
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 262 liMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/l
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen: NHeas N; Ammonia muogen, Tatars
Mn- Manganese
mg/l
,method#
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: _ _ mg/L VOC
Robert Caldwell, Plant Manager Ic u`t � X lbw e
Perloittee(or Authorized Agenl)Name and Title- Please print or type Signature ofP fm'ttee(or Authorized Agenq
GW-59 Rev. 1/2007

ON
TER QUALITY 1140NITORING:
E REPORT FORM
ION OF
MAIL SI
"' ' " "" "' - - -- PERMIT Number: Expiration Date: July 31, 2015
ty Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC
lit Name (if different): NPDES Other
ity Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED
Key NC 28393-9703 County Sampson ❑ Lagoon ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
act Person: Robert Caldwell Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
Location/Site Name: No. of wells to be sampled: 13 ❑ Water Source Heat Pump ❑ Other:
LID NUMBER (from Permit): R-9
Date sample collected: 7/22/13
FIELD ANALYSES:
WAS
Depth: ft.
Well Diameter. — in.
pH 5.36 units Temp. 25 eC
DRY at
T to Water Level: 3.50 ft. below measuring point
Screened Interval: to ft.
Spec. Cond. µMhos
time of
luring Point is ft. above land surface
—ft.
Relative M.P. Elevation: ft.
Odor
sampling,
ne of water pumped/bailed before sampling:
10+ gallons
Appearance
check
here:
for metals were collected unfiltered: DYES
El NO and field acidified: ❑ YES El NO
El
a sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
74.4 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/i 00mi
Nitrate (NO3) as N
1.62 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
234 mg/I
At - Aluminum
mg/I
PH (when analyzed)
units
Ba - Barium
mgll
TOG
4.08 mgn
Ca - Calcium
mg/I
Chloride
17 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/l
Chromium: Total
mg/I
Grease and.0ils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
52 mg/I
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
164 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
,method #
(Ammonia Nitrogen: NH3as N: Ammonia
Nitrogen. Total)
Mn -Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
_ method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: _ mq/L VOC
Robert Caldwell, Plant Manager ( a
Penmttee (or Authanzea Agent) Name and Title- Please print or type Signature f xrmiltee (or
GW-59 Rev, 1/2007

(;W-59A COMPLIANCE REPORT FORM Permit #-wj_jmya6b'
(.Submir one each nwitho irn; period irklr GIP-59 harms.)
I
Enter date monitoring results were due. -3l' I3 ) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
2
Was any required information missing on the GR'-59 report forms?
YES
i
IF the answer to question 1 or 2 is "YES" list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
identification plate, area overgrown, etc.)? IJtheansweris "Yes". contacvthe Regional Ofcejorguidance.
4
Are any monitored constituents equal to or above the established standards?
YES
NO
If the answer to question 4 is 'WO'; skip to section 8..
If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
E
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is "NO" skip to section 8.
If the answer to question 5 is "YES" list in the space provided below, each well with constituent(s) exceeding
standards, concentrations) reported, and sample collection date for each occurrence (forthe last two years).
1a2 IY-lu - R•b //-5 fins%L �5/L
R-G J2 3 eh5/L
3-I1-/3 R b /3.S r ,jjt.
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
1'ES
If the answer is "YES" a groundwater qualityproblem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the permittee implementing previously approved actions required by the Division involving this
-YES(N
groundwater quality problem?
If the answer to question 7 is "YES' describe those actions in the space provided below.
If the answer to question 7 is "NO'; contact the Regional Office within 90 days: an evaluation maV be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation,
fines, and/orpenalties.
8
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this
form with GW-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge that the above information was evaluated and the, information submitted in this
report (Compliance Report GW-59A) is true and complete to the best of my knowledge.
1 u /I3
t ci , , ( e,/Zz-
Sign re of Permittee (or Authorized Agent) Date
(M -�9 N 1214110113

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens. Inc Date Reported: August 03, 2013
Mr. Reid Wells Project: NI/Wells samples -3/\'earl Date Received: July 22, 2013
5900 Turkey Highway Date Sampled: July 22. 2013
Turkey NC. 28393 Sampled By: Davidson
i
Analyzed by: Microbac - Fayetteville Division
Chloride
COD; Total
Conductivity
Depth to Water Surlace
Nitrate as N
pli. Field'Fest
Total Dissolved Solids
Sulfate as SO4
Temperature
Mw 91
1307561-01
18.7
mg/L
7/24/13
1:34
JAW
EPA 300.O.Rev. 2.1(1993)
26.4
mg/L
7/25/13
14:30
DSK
5220 D-1997
183
umhos/cm
7/23h3
15:30
DSK
SM251OB-1997
7.00
feet
7/22/13
9:35
Field Measurement
3.51
mg/L
7/24/13
1:34
JAW
EPA 300.0.Rev. 2.1(1993)
5.33
pH Units
7/22/13
9:35
Field
126
mg/L
1 7/23/13
8:00
JAO
SM 2540 C-1997
23
mg(L
7/24113
1:34
JAW
EPA300.0, Rev.2.1 (1993)
19
°C
7/22/13
9:35
Field
Analyzed by: Mivobac Laboratories, Inc. - Ohio Valley
Total Organic Carbon 6.35
Slate Cenilications:
NCDNR #I I
NCDOII #37714
USDA #3787
mg/L 7/31/13 21:46
BAF SM53 I O-C-2000
Respectfully Submitted
/7 p
Bonnie K. Sanders, Adminlstmovc Assistant
FYI
Page 1 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
L
Aliens, Inc Date Reported: August 08, 2013
Mr. Reid Wells Project M/Nells.samples -3/Yearly Date Received: July 22. 2013
5900 Turkey Ilighway .. Date Samplcd: July 22. 2013
Turkey NC, 28393 Sampled By: Davidson
nlw 92
I307561-02
Analyle Result Units Analyzed .Analyzed By Method Qualifier
Analyzed by: Kcrobac - Fayetteville Division
,Chloride
86.6
COD. Total
30.7
Conductivity
385
Depth to Water Surface
4.11
Nitrate as N
0.706
pH. Field Test
5.90
Total Dissolved Solids
186
Sulfate as SO4
9.8
Temperature
20
Analyzed by: Miorobac Laboratories, Inc. - Ohio Valley
Total Organic Carbon
6.87
Slate Cerlilications:
NCDNR #II
NCDOH #37714
USDA 93787
mg/L
7/24/13
1:51
JAW
EPA 300.0„Rev.2.1(1993)
mg/L
7/25/13
14:30
DSK
5220 D-1997 -
umhos/cm
7/23/13
15:30
DSK
SM 2510B-1997
feet
7/22113
14:54
DSD
Field Measurement
mg/L
7/24/13
1:51
JAW
EPA 300.0, Rev. 2.1 (1993)
pH Units
7/22/13
14:54
DSD
Field
mg/I.
7/23/13
8:00
JAO
SM 2540 C-1997
mg/T. -
7/24/13
ISI
JAW
EPA 300.0. Rev. 2.1 (1993)
°C
7/22/13
14:54
DSD
Field
mg/l.
7/31113
22:10
BAF
SM5310-C-2000
Respectfully Submitted
{7
—iyy1.'A.CL \SLr ke(.L�
Bonnie K. Sanders, Administrative Assistant
Page 2 of 15

Aliens, Inc
Mr. Reid Wells
5900 Turkey I lighway
Turkey NC, 23393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 23306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/W ells samples - 3A'early
Mw 03
1307561-03
Date Reported: August 08, 2013
Date Received: July 22. 2013
Date Sampled: July 22, 2013
Sampled Bp; Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Nioobac - Fayetteville Division
Chloride
COD. Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
120
mg/L
7/24/13
2:07
JAW
EPA 300.0.Rex'.2.1(1993)
71.7
mg/L
7/25/13
1450
DSK
5220 D-1997
620
Umhos/cm
7/23/13
15:30
DSK
SM 2510B-1997
0.900
feet
7/22113
14:55
DSD
Field Measurement
1.35
mg/L
7/24/13
2:07
JAW
EPA 300.0. Rev. 2.1 (1993)
6.33
pH Units
7/22/13
14:55
DSD
Field
600
mg/l.
7/23/13
8:00
JAO
SM 2540 C-1997
55
mg/L
7/24/13
2:07
JAW'
EPA 300.0. Rey. 2.1 (1993)
22
°C
7/22/13
14:55
DSD
Field
Analyzed by: Mivobac Laboratories, Inc - Ohio Valley
Total Organic Carbon . 2.66
Slate Certifications:
NCDNR #I I
NCDOII #37714
USDA 93787
mg/L 7/31113 22:33 BAF SM5310-C-2000
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
Page 3 of 15

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Miuobac- Fayetteville Division
Chloride
19.1
COD, Total
76.(
Conductivity
183
Depth to Water Surface
1.5(
Nitrate as N
8.1(
p1-1. Field Test
5.73
Total Dissolved Solids
76.(
Sulfate as SO4
6.6
Temperature
24
Analyzed by: Microbac laboratories, Inc - Ohio Valley
Total Organic Carbon
3.21
Slate Certifications:
NCDNR 911
NCDOH "37714
USDA "3737
Fayetteville Division
2592 Flope Mills Rd
Fayetteville. NC 28306
910.864 1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples -3/1'early
Mw 94
1307561-04
Date Reported: August 08, 2013
Date Received: July 22, 20
Date Sampled: July 22, 2013
Sampled By: Davidson
mg/L
7/24/13
2:24
JAW
EPA 300.0. Rev.2.1 (1993)
mg/L
7125/13
14:30
DSK
5220 D-1997
umhos/cm
7/23/13
15:30
DSK
SM 251 OB-1997
feel
7/22/13
14:56
DSD '
' Field Measurement
mg/L
7/24/13
2:24
JAW
EPA 300.0, Rev. 2.1 (1993)
pH Units
7/22/13
14:56
DSD
Field
mg/L
7123/13
8:00
JAO
SM 2540 C-1997
mg/L
7/24/13
2:24
JAW
EPA 300.0. Rev.2.1 (1993)
°C
7122/13
14:56
DSD
Field
mg/L
7/31/13
22:56
BAF
SM5310-C-2000
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
a
Page 4 of 15

Allens, Inc
Mr. Reid Wells
5900 Turkey I lighway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples - 3/Yearly
R-I
1307561-10
Date Reported: August 08. 2013
Date Received: July 22, 2013
Date Sampled: July 22, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Kcrobac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
23.0
mg/L
7/24/13
5:10
JAW
EPA 300.0. Rev. 2.1 (1993)
113
mg/L
7/25/13
1430
DSK
5220 D-1997
140
umhos/cm
7/23/13
15:30
DSK
SM 251OB-1997
250
feet
7122/13
14:59
DSD
Field Measurement
0.709
mg/L
7/24/13
5:10
JAW
EPA 300.0, Rev. 2.1 (1993)
5.84
pH Units
7/22/13
14:59
DSD
Field
102
melt
7/23/13
8:00
JAO
SM 2540 C-1997
16
mg/L
7124/13
5:10
JAW
EPA 300.0, Rev. 2.1 (1993)
23
°C
7/22/13
14:59
DSD
Field
Analyzed by: Mit>abac Laboratories, Inc. - Ohio Valley
Total Organic Carbon 3.94
Stale Certification:
NCDNR 911
NCDOH 937714
USDA .3787
mg/L 8/1/13 1:46 BAF SM5310-C-2000
Respectfully Submitte'd'1p.
Bonnie K. Sanders, Administrative Assistant
Page 10 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc Date Reported:. August 08, 2013
Mr. Reid Wells Project: M/Wells samples - 3/1'early Date Received: July 22, 2013
5900 Turkey Highway Date Sampled: July 22, 2013
Turkey NC, 28393 Sampled By: Davidson
R- 2a
1307561-II
Analyze Result Units Analvzed Analyzed By Method Qualifier
Analyzed by: Mioobac - Fayetteville Division
Chloride
COD; Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
15..1
mg/L
7/24/13
5:27
JAW
EPA 300.0, Rev. 2.1 (1993)
65.2
mg/L
7/25/13
14:30
DSK
5220 D-1997
143
umhos/cm
7/23/13
15:30
DSK
SM 251OB-1997
2.30
feet
7/22/13
14:59
DSD
Field Measurement
1.02
mg/L
7/24/13
5:27
JAW
EPA 300.0, Rev. 2.1 (1993)
5.39
pH Units
7/22/13
14:59
DSD
Field
42.0
mg/L
7/23/13
8:00
JAO
SM 2540 C-1997
26
mg/L
7124/13
5:27
JAW
EPA 300.0. Rev. 2.1 (1993)
27
°C
7122113
14:59
DSD
Field
Analyzed by: Mivobzc Laboratories, Ix - Ohio Valley
Total Organic Carbon 1 2.81
State Cerlil ications:
NCDNR #11
NCDOH M137714
USDA #3787
ni 811/13 2:07 BAF SM5310-C-2000
Respectfully Submitted'{p.
Bonnie K. Sanders, Administrative Assistant
SI
Page 11 of 15

G
Allens. Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Micobac - Fayetteville Division
Chloride
83.0
COD. Total
56.6
Conductivity
386
Depth to Water Surface
3.10
Nitrate as N
3.80
III I. Field 'rest
5.36
Total Dissolved Solids
176
Sulfale as SO4 -
15
Temperature
24
Analyzed by: Mitrobac Laboratories, Inc. - Ohio Valley
Total Organic Carbon
3.31
Slate Certifications:
NCDNR CI I
NCDOI 1937714
USDA U787
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: MR\'ells samples - 3/Ycarly
R-3
1307561-12
Date Reported: August 08, 2013
Dale Received: July 22, 2013
Date Sampled: July 22. 2013
Sampled By: Davidson
mg/L
7/24/13
5:43
JAW
EPA 300.0, Rev.2.1 (1993)
mg/L
7/25/13
14:30
DSK
5220 D-1997
umhos/cm
7/23/13
15:30
DSK
SM 251OB-1997
feet
7/22113
1459
DSD
Field Measurement
mg/L
7/24/13
5:43
JAW
EPA 300.0, Rev. 2.1 (1993)
pH Units
7/22/13
14:59
DSD
Field
mg/L
7/23/13
8:00
JAO
SM 2540 C-1997
mg/l.
7/24/13
5:43
JAW
EPA 300.0. Rev.2.1 (1993)
°C
7/22/13
14:59
DSD
Field
mg/L
811/13
2:28
BAF
SM5310-C-2000
Respectfully Submitted
f t��14.ry„a,2. ��J�0,9lz�.Cit.2/
enn,me K. Sanders, Administrative Assistant
Page 12 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 FM
Certificate of Analysis
Aliens, Inc
Mr. Reid Wells Project:. M/R'ells samples-3/1'early
5900 Turkey Highway
Turkey NC. 28393
R-4
1307561-13
Date Reported: August 08. 2013
Date Received: July 22, 2013
Date Sampled: July 22, 2013
Sampled By: Davidson
Analyze Result Units Analvzed Analyzed By Method Qualifier
Analyzed by: Mivobac - Fayetteville Division
Chloride
74.0
mg/L
7/24/13
6:00
JAW
EPA 300.0, Rev. 2.1 (1993)
COD. Total
41.5
mg/L
7/25/13
14:30
DSK
5220 D-1997
Conductivity
337
umhos/cm
7/23/13
1530
DSK
SM 2510B-1997
Depth to Water Surface
3.10
feet
7/22/13
14:59
DSD
Field Measurement
Nitrate as N
1.33
mg/1.
7/24/13
6:00
JAW
EPA 300.0, Rev. 2.1 (1993)
p11. Field Test
4.89
pH Units
7/22/13
14:59
DSD
Field
Total Dissolved Solids
180
mg/L
7/23/13
8:00
JAO
SM 2540 C-1997
Sulfate as SO4
13
mg/L
7/24113
6:00
JAW
EPA 300.0, Rev.2.1 (1993)
Temperature
26
°C
7/22113
14:59
DSD
Field
Analyzed try: Microbac Laboratories, Inc - Ohio Valley
,
'rotalOrganic Carbon
3.62
mJL
8/1/13
2:50
BAF
SM5310-C-2000
State Certifications: Respectfully Submitted
NCDNR CI I
NCDOH 937714
USDA 93787
Bonnie K. Sandcrs. Administrative Assistant
SI
Page 13 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864 8774 Fax
Certificate of Analysis
Aliens. Inc
Mr. Reid Wells Project:. bI/W ells samples - 3/1'early
5900 Turkey Highway
Turkey NC. 28393
R-5a
1307561-05
Date Reported:August O8, 2013
Date Received: July 22, 2013
Date Sampled: July 22. 2013
Sampled Bv: Davidson
Analyle Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: M;aobac - Fayetteville Division
Chloride
22.2
COD. Total
104
Conductivity
206
Depth to Water Surface
2.10
Nitrate as N
4.84
p11. Ficld'fest
5.46
Total Dissolved Solids
122
Sulfate as SO4
23
Temperature
27
Analyzed by. Mitrobac laboratories, Inc - Ohio Valley
Total Organic Carbon
3.66
Stale Certifications'
NCDNR d11
NCDOII 937714
USDA 93787
mg/L
7124/13
2:41
JAW
EPA 300.0, Rev. 2.1 (1993)
rng/I.
7/25/13
14:30
DSK
5220 D-1997
umhos/cm -
7/23/13
15:30
DSK
SM 251 OB-1997
feet
7/22/13
14:59
DSD
Field Measurement
mg/L
7/24/13
2:41
JAW
EPA300.0, Rev. 2.1 (1993)
PH Units
7/22/13
14:59
DSD
Field
mg/L
7/23/13
8:00
JAO
SM 2540 C-)997
mg/L
7/24/13
2:41
JAW
EPA 300.0. Rev. 2.1 (1993)
°C
7/22/13
14:59
DSD
Field
ma/L
7131/13
23:18
BAF
SM5310-C-2000
Respectfully Submitted
Bonnic K. Sanders, Admimstmtive Assistant
Page 5 of 15

Fayetteville Division
2592 Hope. Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Allens, Inc
Mr. Reid Wells Project: MAVells samples-3/Yearly
5900 Turkey Highway
Turkey NC, 28393
R-6
1307561-06
Date Reported: August 08, 2013
Date Received: July 22. 2013
Date Sampled: July 22, 2013
Sampled Bv: Davidson
Analyze Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Micobac - Fayetteville Division
Chloride
31.2
COD, Total
117
Conductivity
238
Depth to Water Surface
3.60
Nitrate as N
0.731
pli. Field Test
6.18
Total Dissolved Solids
178
Sulfate as SO4
12
Temperature
24
Analyzed by: Micobac laboratories, Inc. - Ohio Valley
Total Organic Carbon
33.3
Slate Certifications:
NCDNR kl1
NCDOII k37714
USDA k3787
mg/L
7/24/13
257
JAW
EPA 300.0. Rev. 2.1 (1993)
mg/L
7125/13
14:30
DSK
5220 D-1997
umhos/cm
7/23/13
15:30
DSK
SM 2510B-1997
feet
7/22/13
14:59
DSD
Field Measurement
mg/L
7/24/13
2:57
JAW
EPA 300.0, Rev. 2.1 (1993)
pH Units
7/22/13
14:59
DSD
Field
mg/L
7/23/13
8:00
JAO
SM 2540 C-1997
mg/L
7/24/13
2:57
JAW
EPA 300.0, Rev. 2.1 (1993)
°C
7/22113
14:59
DSD
Field
mg/L
7/31/13
23:40
BAF
SM5310-C-2000
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
Page 6 of 15

Aliens, Inc
Mr. Reid Wells
.5900 Turkey Highway
Turkey NC, 28393
Analyzed try: MiaobaC - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pkl. Field 'rest
Total Dissolved Solids
Sulfate as SO4
Temperature
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: MINVells samples - 3/1'early
R-7
1307561-07
Date Reported: August 08, 2013
Date Received: July 22, 2013
Date Sampled: July 22, 2013
Sampled By: Davidson
69.0
mg/L
7/24/13
3:14
JAW
EPA 300.0, Rev. 2.1 (1993)
63.0
mg/L
7/25/13
14:30
DSK
5220 D-1997
300
umhos/em
7/23/13
15:30
DSK
SM 2510B-1997
3.00
feet
7/22/13
14:59
DSD
Field Measurement
0.861
mg/L
7/24/13
3:14
JAW
EPA300.0, Rev.2.1 (1993)
5.43
pH Units
7/22/13
14:59
DSD
Field
174
mg/L
7/23/13
8:00
JAC
SM 2540 C-1997
7.6
- mg/L
7/24/13
3:14
JAW
EPA 300.0, Rev. 2.1 (1993)
23
°C
7/22/13
14:59
DSD
Field
Analyzed by: Miaobac laboratories, Inc. - Ohio Valley
Total Organic Carbon 17.2
Slate Certifications:
NCDNR 911
NCDOI 1937714
USDA #3787
mg/L 8/1/13 0:43 BAF SM5310-C-2000
Respectfully Submitted tO�
Bonnie K. Sanders, Administrative Assistant
Page 7 of 15

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: NI/Wells samples - 3/1'earh'
R-8
1307561-08
Date Reported: August 08, 2013
Date Received: July 22, 2013
Date Sampled: July 22, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mioobac- Fayetteville Division
Chloride
17.0
mg/L
7/24113
3:31
JAW
EPA 300.0, Rev.2.1 (1993)
COD, Total
26.4
mg/L
7/25/13
14:30
DSK
5220D-1997 AI2
Conductivity
262
umhos/cm
7/23/13
15:30
DSK
SM 251OB-1997
Depth to Water Surface
2.60
feet
7/22113
14:59
DSD
Field Measurement
Nitrate as N
11.4
mg/L
7/24/13
331
JAW
EPA 300.0, Rev.2.1 (1993)
pH. Field Test
4.85
pH Units
7/22/13
14:59
DSD
Field
Total Dissolved Solids
140
mg/L
7/23/13
8:00
JAO
`
SM 2540 C-1997
Sulfate as SO4
28
mg/L
7/24/13
3:31
JAW
EPA 300.0. Rev. 2.1 (1993)
Temperature
22
°C
7/22/13
14:59
DSD
Field
Analyzed by: Microbac Laboratories, Inc. - Ohio Valley
Total Organic Carbon
3.32
mg/l.
8/1/13
1:05
BAF
SM5310-C-2000
state Cenil tcations: Respectfully Submitted
NCDNR 911
NCDOH #37714
USDA 93787��
Bonnie K. Sanders, Administrative Assistant
Page 8 of 15

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/1Vells samples - 3/1'eaily
R-9
1307561-09
I
Date Reported: August 08, 2013
Date Received: July 22, 2013
Date Sampled: July 22, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyred by: Mic obac - Fayetteville Division
Chloride
5.01
mg/L
7/24/13
4:54
JAW
EPA 300.0, Rev. 2.1 (1993)
COD. Total
74.4
mg/L
7/25/13
14:30
DSK
5220 D-1997
Conductivity
164
umhos/cm
7/23/13
15:30
DSK
SM 2510B-1997
Depth to Water Surface
350
feet
7122/13
14:59.
DSD
Field Measurement
Nitrate as N
1.52
mg/L
7/24/13
4:54
JAW
EPA 300.0, Rev. 2.1 (1993)
pH. Field'fest
5.36
pH Units
7/22/13
14:59
DSD
Field
'total Dissolved Solids
234
mg/L
7/23/13
8:00
JAO
SM 2540 C-1997
Sulfate as SO4
52
mg/L
7/24/13
4:54
JAW
EPA 300.0. Rev. 2.1 (1993)
Temperature
25
°C
7/22/13
14:59
DSD
Field
Arelyred by: Microbac Laboratories, Inc. - Ohio Valley
Total Organic Carbon
4.08
mg/L
811/13
1:25
BAF
SM5310-C-2000
State Certifications: Respectfully Submitted
NCDNR 911
NCDOH 937714
USDA 93787
Bonnie K. Sanders. Administrative Assistant
Page 9 of 15

``NO O p S1 F.M ON IES SINCE'
Qu ality Vegetables
5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone]
August 22, 2013
Dept. of Environmental & Natural Resources
Division of Water Quality— Information Processing Unit
1617 Mail Service Center
Raleigh, NC27699-1617 AUG 3
[phone] 302013
WATER QUALITY
RE: Groundwater Quality Monitoring Report tNFORMARdNPROCESSINGUNIT
Aliens, Inc. — Turkey, NC Facility
Permit# WQ0004268
Enclosed are the original and one copy of the Groundwater Monitoring Report on forms G W-59
and GW-59A, and the lab report for Aliens, Inc— Turkey, NC facility for samples collected in
July, 2013.
Monitoring wells # R-6 and R-7 exceeded the 10mg/L limit for TOC as stated in the permit.
These wells have consistently been a little over the compliance limit, but we will resample these and send
the results as soon as they are available.
If you have any questions or require any additional information, please contact me by
phone at [phone].
Sincerely,
Robert Caldwell
Plant Manager
Aliens, Inc. Turkey facility
CC: Laura Mushinski, Aliens, Inc
Reid Wells, Aliens, Inc — Turkey facility
DEN R-FRC
SEP u 9 2013
1

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Off, ©L&
Mtiv 3 RQh "I S�yi�b��i�
i unknown
shc�1 Ly

encsuT I.R.cn
GROUNDWATER QUALITY MONITORING:
DEPARTMENTOF ENVIRONMENT&NATURAL RESOURCES
'1
COMPLIANCE REPORT FORM
��
IVlslot oFwA ERQupuTY41 FORMATIONPROCESSINCUNIT ,'
�BiTMAIL'SERVICECENTERRALEIOHNC27699p1917rPHona:(9�9)733J321r';z?
FACILITY INFORMATION Pease Print Clearly or type
PERMIT Number: Expiration Date: duly 31. 2015
Facility Name: Aliens, Inc. - Turkey
Nan -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
El Lagoon ❑ Remediation: Infiltration Gallery
Turkey '" NC 28393-9703 County.Sampson
��
© Spray Field Remediation:
Contact. Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No, of wells to be sampled:
3
411
El Water Source Heat Pump Other.
rmm ..)
SAMPLING INFORMATION
-
If WELL
WELL ID NUMBER (from Permit): MWA
Date sample collected: 3/11/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
in.
pH 4.94 units Temp. 18 eC
DRY at
Depth to Water Level: 19.0 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cond. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons,
Appearance
here:
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: OYES
El NO
LABORATORY INFORMATION
Date sample analyzed:
-
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 25.7 mg/I
Nitrite (NO,) as N
mg/1
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
C­fi1;Otmg/I
Zn - Zinc mg/I
Coliform: MF Total /1 OOmI
Phosphorus: Total as P
mg/I
'
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg4
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 296 mgn
'AI - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mg4
TOC M3tfngll
Ca - Calcium
mg/I
Chloride 51.7 mgn
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mgn
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC) ,
Phenol mg/I
Fe :Iron
mgn
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate _ 73 mg4
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 526 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia mgA
Mg - Magnesium
mg/l
_ , method #
(Ammonia Nitrogen; NHsas N; Ammmla Nitrogen, TotQ
Mn - Manganese
mg/l
, method #
TKN as N mg/I
Ni - Nickel
mg/1
method #
For Remediation Systems Only (Attach Lati Reports): Influent Total VOCs: mg/L ;Effluent Total VOCs mg/L VOC
Robert Caldwell, Plant Manager
Permlttee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev, 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITYMQNITORING:
DEPARTMENT OFENVIRONMENTBNATORAL RESOURCESry
msloN'oFwaTERnuauTYaNFdRMATIONPROCESSINcuNITr. &,.
COMPLIANCE REPORT FORM"
917 MAIL SERVICE;,OENTER RALEIGH NG 27699,1617 ;Phone [phone]P {',4
FACILITY INFORMATION Please Pant cleallyorType
PERMIT Number: Expiration Date: July 31, 2016
Facility Name: Aliens,. Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different): _- - -
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey "' NC 28393-9703 County Sampson
® Spray Field ❑ Remediation:
Contact Person:' Robert,Caldwell -
Telephone#: [phone]
- ❑ Rotary Distributor ❑ Land Application of Sludge
Well'LocationlSite Name:
No. of wells to be sampled:.
13
❑ Water Source Heat Pump ❑ Other.
SAMPLING INFORMATION - --
-
If WELL
WELL. ID'NUMBER,(from Permit): MW-_:A, "•£ >
Date sa_ rnple collected: 3/11/13-
FIELD ANALYSES:
WAS
Well Depth: ft. ^,:;r.
We'll Diameter:
in.
pH 5.62 units Ternp. 15 eC
DRY at
Depth to Water Level: 5.4 ft. below'measuring point
Screened Interval:
,to _ft.
Spec. Cord. ' µMhos
timef
_ft:
_
P 9 ,
Measuring Point is ft. above land surface
- Relative M.P. Elevation:
_R:
ddor
check
Volume of water pumped/bailed before sampling.
10+ gallons • -
-
Appearance
here: ❑
Samples for metals were collected unfdtered:❑YES
❑ NO and field acidified:_` -❑YES".
❑ NO
LABORATORY INFORMATION • -
Date sample analyzed:
- -. _ - l
Laborato ytJame ' Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should'refleit dissolved and colloidal conoentrations.
COD 25:7• mg/I
- - '.,Nitrite (NO,) as,N
mg/I
Pb - Lead mgll
Coliform: ME Fecal . -/100ml,
. ;, Nitrate (NOA):as N
0.845 mgA
Zn - Zinc mg/I
Coliform: ME Total - /100m1-
Phosphorus: Tofal;as P-
mgA.
(Note: Use Mary meltmC for nignlyhMle samples),
Orthophospli'ate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total :;' 178-:mg/l
Al'=.Aluminum
.-'` mgA
.pH (when analyzed),_ units
Ba-:Barium
mgo-
TOC 3.83 mgll
Ca - Calcium
Chloride 86.1 mgll
Cd- Cadmium
mgA
Arsenic mgll
Chromlum:Total
- mg/l
Grease and Oils mg/I
-Cu - Copper
mgA
ORGANICS: (by GC, GC/MS; HPLC)
Phenol mg/I
" -- ".Fe - Iron
mgA,
"(Specify test and method #:.ATTACH LAB REPORT.)
Sulfate 9.3 mga
Mercury
mg/I
-- Report Attached? ❑ = Yes (1) ❑ No (0)
Specific Conductance 395 µMhos
�:K Potassium
m411
VOC , method #
Total Ammonia mg/I
Mg -Magnesium
mgA
, method ,#
(Ammonia Nitrogen; NH�as N: Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/l
, method #
For Remediation Systems Only (Attach Lab Reports): influent Total VOCs: _ mg/L Effluent Total-VOCs: , mq/L VOC
Robert Caldwell, Plant Manager
Permittee (or Authorized Aqent) Name and Title - Please print or type
GW-59 Rev. 112007

rrr�rt
:R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
Y "''"' NC 28393-9703 county Sampson
act Person: Robert Caldwell Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 13
L ID NUMBER (from Permit): MW-3 Date sample collected: 3/11113
Depth: ft. Well Diameter. in.
h to Water Level: 0.60 ft. below measuring point Screened Interval: ft, to ft.
;wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
ales for metals were collected unfiltered: OYES ❑ NO and field acidified ❑ YES 71 NO
a sample analyzed:
tAMETERS NOTE: Values should reflect dissoly
COD 120 mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /loom)
(Note: Use MPN method for highly herald samples)
Dissolved Solids: Total
388 mgA
pH (when analyzed)
units
TOC
4.30 mgn
Chloride
112 mgA
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
- mgA
Sulfate
57 mgA
Specific Conductance
563 µMhos
Total Ammonia
mgA
(Ammonia Niimgen; NH,as N; Ammonia
Meager. Total)
TKN as N
mall
Robert Caldwell, Plant Manager
Penniltee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007
Date: July 31, 2015
in -Discharge WQ0004268 UIc
)DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon El Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other: _
FIELD ANALYSES
pH 5.97 units Temp. 16 eC
Spec. Cond. µMhos
Odor
Appearance
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
colloidal concentrations.
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Nitrate (NO3) as N
0.806 mgA
Zn -Zinc mg/I
Phosphorus: Total as P
mg,'!
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
At - Aluminum
mg/I
Bat - Barium
mgA
Ca - Calcium
mg/I
Cd- Cadmium
mgA
Chromium: Total
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS; HPLC)
Fe - Iron
mg/I
(Specify test and method MiATTACH LAB REPORT.)
Hg - Mercury
mgA
Report Attached? ❑ Yes (1) ❑ No (0)
K - Potassium
mgA
VOC , method #
Mg - Magnesium
mgA
, method #
Mn - Manganese
mg/I
, method #
Ni - Nickel
mgA
, method #
I Visit VwJ: mnfL vVG
at
of

SURMIT FORM ON VFI I OIAI PAPFR ONI V
GROUNDWATER QUALITY MONITORING:
DEPARTMENTOFENVIRONMENT'BNATURALRESOURCES 4 S y",;+ ✓
IVISIONOFwATERQUALITY4NFDate<TIONPRocEssfNcuNrr k `.{
PROCESSING
COMPLIANCE REPORT FORM
817 MN[ SERVICE CENTER RALERMATIION
Phone (979j 733d12t
FACILITY INFORMATION Pease Font clean or Type
^
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
-
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon EJ Remediation: Infiltration Gallery
Turkey "`g NC 28393-9703 CountySampson
'-�'
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well LocationlSite Name:
No. of wells to be sampled: 13
❑ Water Source Heat Pump ❑ Other. -
fmm Permit
SAMPLING INFORMATION. -
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected: 3/11113
FIELD ANALYSES:
WAS.
Well Depth: ft.
Well Diameter: _in,
pH 5.17 units Temp. 18 aC
DRY at
Depth to Water Level: 6.00 ft. below measuring point
Screened Interval: ft. to
ft. Spec. Cond. µMhos
time of
Measuring Point is ft. above land. surface
Relative M.P. Elevation: ft.
Odor
sampling,
check
Volume of waterpumped/bailed before sampling:
10+ gallons
Appearance _
here: ElSamples
for metals were collected unfiltered: ❑YES
El NO and field acidified: ❑YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 57.8 mgll
Nitrite (NO,) as N
mgA
Pb - Lead mg/I
Coliform: MF Fecal - 1100ml
Nitrate (NO3) as N 2.52
mg/I
Zn - Zinc mgA
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly l dsamples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 74.0 mgA
AI - Aluminum
mg/1
pH (when analyzed) units
Be - Barium
mgA
TOC 4.34 mgll
Ca —Calcium
mgA
Chloride 21.1 mgA
Cd- Cadmium
mgA
Arsenic mgA
Chromium: Total
mg/l
Grease and Oils mg/I
Cu - Copper
mg/i
ORGANICS: (by GC, GCIMS; HPLC)
Phenol mg/I
Fe - Iron
mgA
(Specify test and method MI, ATTACH LAB REPORT.)
Sulfate 16 mgA
Hg - Mercury
mgA
Report Attached? ❑ " Yes (1) ❑ No (0)
Specific Conductance 161 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia mgA
Mg - Magnesium
mgA
, method #
(Ammonia hh"gen; NH... N: Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mq/L VOC
Robert Caldwell, Plant Manager
Pennittee (or Authorized Agent) Name and Title- Please print or type
GW-59 Rev. 1/2007

SUBMIT FORM ON VFI I nVV PAPFR ONI V
GROUNDWATER QUALITY MONITORING:
rDEPARTMENT.,
OF, ENVIRONMENT & NATURAL RESOURCES
IVISIONOFwaTERIWAb*Y4NFORMATIONPROCESSINGUNIT M £
COMPLIANCE REPORT FORM
817,R1AIL`SERVICE CENTER RALEtGH; NC 27698161]- Phon`a (919�7333221,
FACILITY INFORMATION Please Pnnt clearly or Type
-
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. -Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey "" NC 28393-9703 County Sampson
"u '"
-
0 Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land. Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other.
rom Pemil
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-1
Date sample collected: 3/11113
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in.
pH 5.42 units Temp. 15 eC
DRY at
Depth to Water Level: 1.11 ft. below measudng point
Screened Interval:
ft. to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft, above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 111 mg/I
Nitrite (NO2) as. N
mgA
Pb - Lead mg/l
Coliform: MF Fecal 11 Conti
Nitrate (NO3) as N
1.22 mg/1
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/1
(Note: Use MPN metrodforeigNyluraidsamples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 144 mg/I
At - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mgA
TOC 7.26 mg/I
Ca - Calcium
mgA
Chloride 62.9 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mgA
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS.HPLC)
Phenol mgA
Fe - Iron
mgA
(Specify test and method #JkTTACH LABREPORT.)
Sulfate 11 mgA
Hg - Mercury
mg/I
Report Attached? ❑ . Yes (1) ❑ No (0)
Specific Conductance 284 µMhos
K - Potassium
mgA
VOC , method #
Total Ammonia mgA
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NH385N: Ammonia Nitrogen. Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOIDS: mg/L _ Effluent Total VOCs: me/L VOC
Robert Caldwell, Plant Manager
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
QUALITY
EPARTMENTOF ENVIRONMENT& NATURALRESOURCESGROUNDWATER
DIVISION.OF WATER QUALITY-INFORMATIONPROCESSING UNITIF
COMPLIANCE REPORT FORMNITORING:
617 MAIL SERVICE CENT,ERRALEIGH; NC 27699=1617 Phone;t91817J3dR21 i, .,;
FACILITY INFORMATION Please Pant clearly or Type
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
-
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different): -
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey NC 28393-9703 County Sampson
© Spray Field El Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump O Other:
Imm PemJt
SAMPLING INFORMATION
R WELL
WELL ID NUMBER (from Permit): R-2a
Date sample collected: 3/11113
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in.
pH 5.16 units Temp. 15 aC
DRY at
Depth to Water Level: 2.30 ft. below measuring paint
Screened Interval:
ft. to
ft. Spec. Cord. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumped bailed before sampling:
10+ gallons
Appearance
here:❑
Samples for metals were collected unfiltered: El YES
❑ NO and field acidified: 0 YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
"
Laboratory, Name: Microbae Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 30.0 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mgn
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
0.770 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: use MFN memad Tor Nghly Nand samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 40.0 mgn
AI - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mg/I
TOC 2.40 mgn
Ca - Calcium
mgn
Chloride 15.6 mgn
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mgn
Cu - Copper
mgn
ORGANICS: (by GC, GC/MS', HPLC)
Phenol mg/I
Fe - Iron
mgn
(Specify test and method #! ATTACH LAB REPORT.)
Sulfate 28 mlin
Hg - Mercury
mgn
Report Attached? ❑ ` Yes (1) ❑ No (0)
Specific Conductance 144 µMhos
K - Potassium
mg/1
VOC , method #
Total Ammonia mgn
Mg - Magnesium
mg/I
, method #
(Ammonla Nitmgen; NHaas N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/l
,method #
TKN as N mg/I
Ni - Nickel
mgll
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent TotalVOCs: mg/L VOC Removal%_ _
Robert Caldwell, Plant Manager
Permittee (or Authorized Apent) Name and Tdle- Please pant or type
GW-59 Rev. 112007

Q"nRAIT cnoen ON VPF t MAr oeoco OAI v'
GROUNDWATER QUALITY MONITORING:
- -
.UEPARTMENT
OF ENVIRONMENT& NATURAL, RESOURCES';" --
IVISION Op WATER QUALITYdNFORMAT10N PROCESSING UNITK ,.,,;,f +
COMPLIANCE REPORT FORM
617iMAICSERVICE CEF{TER RALEIGF�INC 27699-Seth phpne:,(919)7333221 ;r
FACILITY INFORMATION Please Print Clearly or Type
-
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
El Lagoon ❑Remediation: Infiltration Gallery
Turkey ""°0 NC 28393-9703 County Sampson
""
© Spray Field ❑Remediation:
Contact Person: RobertCaldwell
Telephone#: [phone] ;�.,.
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
Isom Panra
SAMPLING INFORMATION
K WELL
WELL ID NUMBER (from Permit): R-3
Dale sample collected: 3/11113
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter. _in,
pH 3.74 units Temp. 15 eC
DRY at
Depth to Water Level: 3.60 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cone. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
-
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: ❑YES
El NO and field acidified: ❑ YES
El NO
LABORATORY INFORMATION
Date sample analyzed:
-
Laboratory'Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 40.7 mgfl
Nitrite (NO.) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
1.84 mg/I
Zn - Zinc mg/I
Coliform: MF Total 1100ml
Phosphorus: Total as P
mgA
(Note: Use MPN method for highly WroW samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 152 mg/I
Al -Aluminum
mgA
pH (when analyzed) units
Ba - Barium
mgA
TOC 1.67 mgA
Ca - Calcium
mg/I
Chloride 109 mg/I
Cd- Cadmium
mgA
Arsenic mg/I
Chromium: Total
mgA
Grease and Oils mg/I
Cu - Copper
mgA
ORGANICS: (by GC, GC/MS; HPLC) ,
Phenol mg/I
Fe - Iron
-mgA
(Specify test and method #.!ATTACH LAB REPORT.)
Sulfate 25 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ ' Yes (1) ❑ No (0)
Specific Conductance 496 ltMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
,method #
(Ammonia Nitrogen; NH.as N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/l
, method #
TKN as N mg/l
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:, mg/L. - Effluent Total VOCs: : ma/L VOC Removal%
Robert Caldwell, Plant Manager
Pennines (or Authorized Agent) Name and Title- Please print or type
GW-59 Rev. 112007

SUBMIT FORM ON VFI 1 OW PAPFP nNl V
GROUNDWATER QUALITY MONITORING:
EPARTMENT OF ENVIRONMENT 8 NATURAL RESOURCES
ivislOHroFwATERnuALITyaJFORManoNyFRocESstNO uNlr�p�3r` j
COMPLIANCE REPORT FORM
�
" " f
817 MAu;,sERVICE CENTER RALEu3H, NC 27994g81T,FPhone: (918) 7733221�„+'f'i
FACILITY INFORMATION Please Print Cleany or Type -
`
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Allens, Inc. --Turkey
Non -Discharge WQ0004268 UIC
NPDES ' Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey """" NC 28393-9703 County Sampson
© Spray Field ❑Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
fmm PenNt
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-4
Date sample collected: 3/11/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
in,
pH 4.56.units Temp. 14 oC
DRY at
Depth to Water Level: 3.50 ft. below measuring point
Screened Interval:
ft. to
ft. Spec. Cond. µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
Samples for metals were collected unfiltered: ❑YES
El NO and field acidified: ❑ YES
❑ NO
❑
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 40.7 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100m1
Nitrate (NO3) as N
2.73 mg/I
Zn - Zinc mgn
Coliform: MF Total 1100ml
Phosphorus: Total as P
mg/I
(Note: use MPN meMd t rN9hly turbid samples)
.Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 228 mg/l
AI - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mgn
TOC 4.54 mg/I
Ca - Calcium
mg/I
Chloride 129 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mg/I
Cu -Copper
mg/I
ORGANICS: (by GC; GC/MS', HPLC)
Phenol mg/I
I Fe - Iron
mg/I
(Specify test and method #; ATfACH LAB REPORT.)
Sulfate. 6.7 mg/l
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance 505 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia mg/1
Mg - Magnesium
mg/I
,method #
(AmmNitrogen; NH,as N; Ammonia Nibagen, Total)
aneseonia
Mn - Man g
mgll
, method #
TKN as N mgll
Ni - Nickel
mg/I
, method #
For Mememagon Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Robert Caldwell, Plant Manager
Pennittee (or Authorized Aqent) Name and Title- Please print or type
GW-59 Rev. 112007

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
EPART MEW, OF ENVIRONMENTS NATURAL RESOURCES '�'-9 I '*
QUALITYdNFORMATIONPROCESSINGUNIT`
COMPLIANCE REPORT FORM
MsIONOFWATER
MAIL "SERVICE
877 (;ENTERj'R&EIGHi NC 27699,1e 7, Pl ona.,(a,19)7333221
7.. ;
FACILITY INFORMATION Pease Print
Clearly or Type`'
-'
PERMIT Number: Expiration Date: July31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge WQ0004268 ' UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
El Lagoon ❑Remediation: Infiltration Gallery
Turkey NC 28393-9703 County Sampson'
' !7.'
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells. to be sampled:
13
❑ Water Source Heat Pump ❑ Other. -
rmm veme
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-5a
Date sample collected: 3/11 /13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
in.
pH 5.21 units Temp. 17 °C
DRY at
Depth to Water Level: 2.50 ft. below measurin
P g point
Screened Interval:
ft. to
ft. Spec. Cond. Mh os
µ
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 89.9 moll
Nitrite (NO,) as N
mgA
Pb - Lead mgA
Coliform: MF Fecal /looml
Nitrate (NO3) as N
4.95 mg/I
Zn - Zinc mg/I
Coliform: MF Total /loom[
Phosphorus: Total as P
mg/I
(Note: Use MPH megwd rot highly iuNid samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 100 mgA
Al - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mgll
TOC 3.16 mgn
Ca - Calcium
mg/I
Chloride 28.5 mgA
Cd- Cadmium
mg/1
Arsenic mgA
Chromium: Total
mg/I
Grease and Oils mgA
Cu- Copper
mgll
ORGANICS: (by GC, GC/MS; HPLC)
Phenol mgA
Fe - Iron
mg/I
(Specify test and method #.i ATTACH LAB REPORT.)
Sulfate 22 mgA
Hg - Mercury
mgA
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 228 µMhos
K- Potassium
mgA
VOC , method #
Total. Ammonia mg/I
Mg - Magnesium
mg/1
,method#
(Ammonia Niaagen; NHras N; Ammonia Nitrogen, Totel)
Mn- Manganese
mgA
,method#
TKN as N mg/I
Ni - Nickel
mgA
, method #
GW-59 Rev. 112007

SUBMIT nJ
GROUNDWATER QUALITY MONITORING:
EPARTMENTOF ENVIRONMENTBNATURAL RESOURCES 4y u r a v�r
COMPLIANCE REPORT FORM
IVISIONOFwATEtQUALITY4NFORMATIONPRocEss(NGUNrr rr '
sTT61A1L''sERViCECENT'E RALE.lGy Ncrtcse=fe'ti aeona:;jis`j7assxza "�' <.-
FACILITV INFORMATION Please Pnnt cleany or7ype
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Allens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑Lagoon ❑Remediation: Infiltration Gallery•�-
Turkey"'"" NC 28393-9703 Count Sampson County P
•-�
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump El Other.
fmm Pe7N
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): R-6
Date sample collected: 3/11 /13
FIELD ANALYSES:
If WELL
WAS
Well Depth: ft.
Well Diameter: — in.
pH 4.87 units Temp. 15 oC
DRY at
Depth to Water Level: 4.40 ft. below measuring point
Screened Interval:
to
. Spec. Cond. pMhos
time of
Measuring Point is ft. above land surface
_ft.
Relative M.P. Elevation:
_ft.
ft.
Odor
sampling.
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
check
here:
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
❑
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 64.2 mgll
Nitrite.(NOl as N
mg/I
Pb - Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
1.24 mg/1
Zn - Zinc mg/I
Coliform: MF Total 1100mi
Phosphorus: Total as P
mg/I
(Note: Use MPN melhed car highly torliEsampiss)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 82.0 mgA
Al - Aluminum
mgA
pH (when analyzed) units
Be - Barium
. mg/1
TOC -m 11
Ca - Calcium
mgfl
Chloride 42.6 mgA
Cd - Cadmium
mgfl
Arsenic mg/l
Chromium: Tota(
. mg/I
Grease and Oils mgA
Cu - Copper.
mg1l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/1
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 15 mg/l
Hg - Mercury
mgA
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 249 pMhos
K - Potassium
mgA
VOC , method #
Total Ammonia mg/l
Mg - Magnesium
mg/I
#
(Ammonia Nitrogen: NHras N: Ammonia Nigogen, Total)
Mn- Manganese
mg/1
,method
,method#
TKN as N mg/I
Ni - Nickel
mg/I
, method #
Robert Caldwell, Plant Manager
Permittee for Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007

SUBMIT FORM ON YELLQW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
DEPARTMENT OF ENVIRONMENT a NATURALRESOURCESa.
[V]SION'OFWATERQVALITYaNFORMAiION PROCESSING UNIT,f'h�'
COMPLIANCE REPORT FORM
r
61rMAl `sERVICEoENTER M; 9.1e i�Phon.
N RALEIOC276 _. 019)Taa-322
FACILITY INFORMATION Please Print Creamy or Type
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Allens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
El Lagoon ❑Remediation: Infiltration Gallery
Turkey NC 28393-9703 County Sampson
'
X❑ Spray.Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:.
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
rmm Pamm
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-7
Dale sample collected: 3/11/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in.
pH 5.09 units Temp. 16 aC
DRY at
Depth to Water Level: 1.10 ft. below measuring
P g point
Screened Interval:
ft. to
ft. Spec. Cond. " Mhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
sampling,check
Volume of water pumped/bailed before sampling:
1 0+ gallons
Appearance
here: ElSamples
for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
El NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 109 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
0.195 mg/I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Not.: Use MPN method for highly Wtt,id amples)
Orthophosphate -
mg/I
Other(Specify Compounds and Concentration Units):
Dissolved Solids: Total 108 mg/I
AI - Aluminum
mgA
pH (when analyzed) units
Ba - Barium
mg/l
TOC '''42:7 gA
Ca - Calcium
mg/I
Chloride 70:9 mg/I
Cd- Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mgA
Grease and Oils mg/I
Cu - Copper.
mg/I
ORGANICS: (by GC, GC/MS'i HPLC)
Phenol mgA
Fe - Iron
mg/I
(Specify test and method #i ATTACH LAB REPORT.)
Sulfate 7.0 mg/I
Hg - Mercury.
mgA
Report Attached? ❑ Yes.(1) ❑ No (0)
Specific Conductance 296"Mhos
K- Potassium
mg/I
VOC ,method#
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nivagen; NHsas N; Ammonia Nitrogen, Total)
Mn - Manganese
mg/I
, method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC
Robert Caldwell, Plant Manager^ ���� %E�ySll
Permittee(or Authorized Agent)Name and Title- Please print or type Signature Penikfor Authorized Anent) (Date)
GW-59 Rev. 112007

SHRMIT FORM ONYFI I OW PAPFR nNLY
GROUNDWATER QUALITY MONITORING:
EpAR7MENT OF ENVIRONMENTa NATURAL RESOURCES 5 r r. r'v9 v >z5i
nnsroNOFwATERnunLIV4NFORMAt[ONaao—cEssINGUHIT�,;
COMPLIANCE REPORT FORM
,
817 MAILSERVICE CENTER.RALEIGH,�NC,2769- 16174 Phone: (918)733 a22t
FACILITY INFORMATION Please Print Clearly or Type -
-
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon 0 Remediation: Infiltration Gallery
Turkey °""" NC 28393-9703 County Sampson
. - ..
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
rmm Pamvt
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-8
Date sample collected: 3111/13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: _in.
pH 4.74 units Temp. 16 eC
DRY at
Depth to Water Level: 3.20 R. below measuring
P g point
Screened Interval:
ft. to
ft. Spec. Cord. µ Mhos
time of
Measuring Paint is ft. above land surface
Relative M.P. Elevation:
R.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
_
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 40.7 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
`d. 1,1'" /I
Zn - Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly tuned samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 82.0 mga
AI -Aluminum
mg/I
pH (when analyzed) units
Ba - Barium
mg/l
.
TOC 2.65 mg/I
Ca - Calcium
mg/I
Chloride 17.2 mg/I
Cd- Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/l
Grease and Oils mg/I
Cu - Copper.
mg/I
ORGANICS: (by GC, GC/MS! HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #.: ATTACH LAB REPORT.)
Sulfate 24 ri
Hg- Mercury
mg/I
Report Attached? ❑' Yes (1) ❑ No
Speck Conductance 251 µMhos
K- Potassium
Mgt[
VOC ,method#
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHsas N; Ammonia Niuo en. Tole)
Mn - Manganese
mgll
,method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: ma/L VOC Removal%
Robert Caldwell, Plant Manager
Permihee (or Authorized Agent) Name and Title- Please print or type
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
EPARTMENTOFENVIRONMENT& NATURAL RESOURCES 1 °mowy2 r "
msIONOFWATERQuaury4NFORMAnoNPRocEsglNauN1T' t
COMPLIANCE REPORT FORM
atTMAt�sEavacEdEtrT€g Rn�EtGry'Rc27cagt617 Phene,tste);t3asa211,
FACILITY INFORMATION - Please Print clearly or Type'
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
_
Non -Discharge W00004268 UIC
NPDES. : Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
_
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey ""°"' NC 28393-9703 County Sampson
© Spray Field ❑ Remediation:
Contact Person: Robert Caldwell
Telephone#:-910-596-0028-
_ _
-
❑ Rotary Distributor 0 Land Application of Sludge
Well Location/Site Name:
No, of wells to be sampled:
13
❑ Water Source Heat Pump El Other.
from 22=
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-9
Date sample collected: 3/11 /13
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
in.
pH 4.81 units Temp. 16 ac
DRY at
Depth to Water Level: 4.60 ft. below measuring point
—
Screened Interval:
to
ft. Spec. Cord. µMhos
time of
_ft.
-
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of waterpumped/bailed before sampling:
10+gallons
Appearance
here:❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: DYES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 85.6 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mgA
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
2.93 mg/I
Zn - Zinc mgA
Coliform: MF Total /100mi
Phosphorus: Total as P
mgA
(Note: Use MPN metaad for highly t.Mid samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 252 mgA
At - Aluminum
mg/I
PH (when analyzed) units
Be - Barium
mg/l
TOC 3 13 mg/l
Chloride 9.79 gAOK
Ca - Calcium
Cd- Cadmium
mgA
mg/I
Arsenic mg/I
Chromium: Total
mgA
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol _ mg/I
Fe - Iron
mg/l
(Specify test and method MiATTACH LAB REPORT.)
Sulfate 48 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 194 µMhos
K- Potassium
mgA
VOC ,method#
Total Ammonia mgA
Mg - Magnesium
mg/I
, method #
(A hi Nitrogen: NH,,asN:Ammonia Nitrogen. Tatel)
Mn- Manganese
mg/I
,method#
TKN as N mgA
Ni - Nickel
mgA
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: - mg/L Effluent Total VOCs mg/L VOC Removal% _
Robert Caldwell, Plant Manager
Pernittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 1/2007

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fac
Certificate of Analysis
Aliens. Inc
Mr. Reid Wel Is Project: M/W ells samples - 3/)'early
5900 Turkey I iehsvay
Turkey NC, 28393
Mw 91
1303187-01
Date Reported: March 23. 2013
Date Received: March 11, 2013
Date Sampled: March 11, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Miaobac- Fayetteville Division
Chloride
51.7
mg/L
3/12/13
15:22
JLR
EPA 300.0. Rev. 2.1 (1993)
COD, Taal
25.7
mg/L
3/12/13
10:50
DSK
5220 D-1997
Conductivity
526
umhos/cm
3112/13
8:40
DSK
SM 25106-1997
Depth to Water Surface
19.0
feet
3/11/13
1538
DSD
Field Measurement
Nitrate as N
11.0
mg/L
3/12/13
15:22
JLR
EPA 300.0. Rev. 2.1 (1993)
p11. Field rest
4.94
pH Units
3111113
1538
DSD
Field
Total Dissolved Solids
296
mg/L
3/I3113
11:03
JAO
SM 2540 C-1997
Sulrate as SO4
73
mg/L
3/12/13
15:22
JLR
EPA 300.0, Rev. 2.1 (1993)
Temperature
18
C.
3/11/13
1538'
DSD
Ficid
Analysed by: Mlcrobac Laboratories, Inc. - Ohla Valley
i
Total Organic Carbon
16.3
mg/1.
3/18/13
18:44
BAF
SM5310-C-2000
Stale Certifications: Respeeil'ully Submitted
NCDNR #II n
DOH r:37714 US
USDA 93737 1 /
Bonnie K. Sanders. Administrative Assistant
Page 1 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306'
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Allen, hic Date Reported: March 23, 2013
Mr. Reid Wells Project: M/Wells samples -3/1'early Date Received: March 11, 2013
5900 Turkey Highway Date Sampled: March 11, 2013
Turkcy NC, 28393 Sampled By: Davidson
Mw 92
1303187-02
Analyte Result units Analyzed Analyzed By Method Qualifier
Analyzed by:. Microbic - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
'rempemlure
86.1
mg/L
3/12/13
15:38
JLR
EPA 300.0. Rev.2.1 (1993)
25.7
mg/L
3/12/13
10:50
DSK
5220 D-1997
395
umhos/cm
3/12/13
8:40
DSK
SM 25I0B-1997
5.40
feet
3/11113
1538
DSD
Field Measurement
0.845
mg/L
3/IJ13
15:38
JLR
EPA 300.0, Rev.2.1 (1993)
5.62
pH Units
3/11/13
i5:38
DSD
Field
178
mg/L
3/13/13
11:03
JAO
SM 2540 C-I997
9.3
mg/L
3/12/13
15:38
JLR
EPA 300.0. Rev. 2.1 (1993)
15
°C'
3/11?1315:38
DSD'
Field
Analyzed by: Micrubac feboretorws, Inc. - Ohio Valley
Total Organic Carbon 3.83
State Certifications:
NCDNR kl1
NCDOII 437714
USDA #3787
mg/L 3/16/13 17:30 BAF SM5310-C-2000
Respectfully Submitted
Bonnie K. Sanders. Administrative Assistant
Page 2 of 15

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wellssamples-3/1'earh
Mw #3
1303187-03
Dale Reported: March 23. 2013
Date Received: March It, 2013
Date Sampled: March 11, 2013
Sampled Bp: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
112
mg/L
3/12/13
15:55
JLR
EPA 300.0. Rev. 2.1 (1993)
120
mg/L
3/12113
10:50
DSK
.. 5220 D-1997
563
umhos/cm
3/12/13
8:40
DSK
SM 251OB-1997
0.600
feet
3/11/13
15:38
DSD
Field Measurement
0.806
mg/L
3/12/13
15:55
JLR
EPA 300.0. Rev. 2.1 (1993)
5.97
pH Units
3/I1/13
15:38
DSD
Field
388
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997
57
mg/L
3/12/13
15:55
JLR
EPA 300.0. Rev. 2.1 (1993)
16
°C
3/11/13
15:38
DSD
Field
Analyzed by: Mivobac laboratories, Inc - Ohio Valley
'total Organic Carbon 4.30
State Certifications:
NCDNR #II
NCDNR #37714
USDA k3787
mg/L 3/16/13 17:54 BAP SM5310-C-2000
Reysppe2ectfull�ly Submitted 1p,
Bonnie K. Sanders. Administrative Assistant
Page 3 of 15

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: MAVells samples - 3/Yearly
Mw 94
1303187-04
Date Reported: March 23, 2013
Date Received: March 11. 2013
Dale Sampled: March I I, 2013
Sampled By: Davidson
Analyle Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Miaobac - Fayetteville Division
Chloride
21.1
mg/L
3/12113
16:11
JLR
EPA 300.0. Rev. 2.1 (1993)
COD. Total
57.8
mg/L
3/12113
10:50
DSK
5220 D-1997
Conductivity
161
umhos/cm
3/12/13
8:40
DISK
SM 2510B-1997
Depth to Water Surface
6.00
feet
3/I I/13
15:38
DSD
Field Measurement
Nitrate as N
2.52
mg/L
3112/13
16:11
JLR
EPA 300.0. Rev. 2.1 (1993)
pli. Field Test
5.17
pH Units
3/I1/13
15:38
DSD
Field
Total Dissolved Solids
74.0
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997
Sulfate as SO4
16
mg/L
3/12/13
16:11
JLR
EPA 300.0. Rev. 2.1 (1993)
Temperature
18
°C
3/I1113
15:38
DSD
Field
Analyzed by: Microbac Laboaton2s, Inc. - Ohio Valley
Total Organic Carbon
4.34
mg/L
3/I6/13
18:38
BAF
SM5310-C-2000
a
State Certifications, Respectfully Submitted
NCDNR #II
DOH #37714 US
USDA 93787 1
Bonnie K. Sanders. Administativc Assistant
Page 4 of 15

Aliens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 2S306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: MAVells samples-3/1'early
R-1
1303187-05
.. Date Reported: March 23, 2013
Dale Received: March H. 2013
Date Sampled: March 11, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
62.9
COD, Total
111
Conductivity
284
Depth to Water Surface
1.11
Nitrate as N
1.22
pli. Field Teat
5.42
'total Dissolved Solids
144
Sulfate as SO4
1 I
Temperature
15
Analyzed by: Mivobac laboratories, Inc. - Ohio Valley
Total Organic Carbon
7.26
State Certifications:
NCDNR #11
NCDOH #37714
USDA 93787
mg/L
3/12/13
16:28
JLR
EPA 300.0. Rev. 2.1 (1993)
mg/L
3/12/13
10:50
DSK
5220 D-1997
umhos/cm
3/12/13
8:40
DSK
SM 2510B-1997
feet
3111/13
1538
DSD
Field Measurement
mg/L
3/12/13
16:28
JLR
EPA 300.0, Rev. 2.1(1993) Al2
pH Units
3/I1/13
15:38
DSD
Field
mg/L
3/13113
11:03
JAO
SM 2540 C-1997 Si
mg/L
N12/13
16:28
JLR
EPA 300.0. Rev. 2.1(1993) Al2
°C
3/11113
1'5:38
DSD
Field
mg/L
3/16/13
19:01
BAF
SM5310-C-2000
Respectfully Submitted Qp
—i�a'rix.t-f� r�M.r �f.•4a�
Bbdnie K. Sanders, Adminislmlive Assistant
Page 5 of 15

Allen, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax . .
Certificate of Analysis
Project: M/Wclls samples - 3/1'early
R-2a
1303187-06
Date Reported: March 23, 2013
Date Received: March 11, 2013
Date Sampled: March 11, 2013
Sampled By: Davidson
Analyle Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mlaobac- Fayetteville Divisan
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Tempera(ure
15.6
mg/L
3/12113
17:51
JLR
EPA 300.0, Rev. 2.1 (1993)
30.0
all
3112/13
10:50
DSK
5220 D-1997
144
umhos/cm
3/12113
8:40
DSK
SM 25 1013- 1997
2.30
feet
3/11/13
15:38
DSD
Field Measurement
0.770
mg/L
3/12/13
17:51
JLR
EPA 300.0, Rev. 2.1 (1993)
5.16
pH Units
3/11/13
15:38
DSD
Field
40.0
mg/L
3113/13
11:03
JAO
SM 2540 C-1997
28
mg/L
3/12/13
17:51
JLR
EPA 300.0. Rev. 2.1 (1993)
15
°C
3/11/13
15.38
DSD
Field
Analyred by: Microbac Laboratories, Inc. - Ohio Valley
Total Organic Carbon . 2.40
Slate Certifications;
NCDNR#I I
NCDOH #37714
USDA 93787
mg/L 3/16/13 19:23 BAF SM5310-C-2000
Respectfully Submitted
n p
Bonnie K. Sanders, Administrative Assistant
M
Page 6 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc Date Reported: March 23, 2013
Mr. Reid Wells Projects. MAVells samples -3/1'earty Date Received: March 11, 2013
5900 Turkey Highway Date Sampled: March 11, 2013
Turkey NC, 28393 Sampled By: Davidson
R-3
1303187-07
Analyze Result Units Analvzed Analyzed By Method Qualifier
Analyzed by: Mivobac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
109
mg/L.
3112/13
18:08
JLR
EPA 300.0. Rev. 2.1 (1993)
40.7
mg/L
3/12/13
10:50
DSK ,
, 5220 D-1997
496
umhos/cm
3/12/13
8:40
DSK
SM 2510B-1997
3.60
feet
3/11/13
15:38
DSD
Field Measurement
1.84
mg/L
3/12/13
18:08
JLR
EPA 300.0, Rev. 2.1 (1993)
3.74
pH Units
3/11/13
15:38
DSD
Field
152
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997
25
mg/L
3/12/13
18:08
JLR
EPA 300.0, Rev. 2.1 (1993)
15
°C
3/11/13
15:38
DSD
Field
Analyzed by: Mioobac tabonnodes, Inc - Ohio Valley
Total Organic Carbon 1.67
State Certifications:
NCDNR #I I
NCDOH #37714
USDA #3787
mg/L 3116113 19:44 BAF SM5310-C-2000
Respect 1'ul ly Submitted
Bonnie K. Sanders, Administrative Assistant
Page 7 of 15

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. INC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples - 3/1'early
R-4
1303187-08
Date Reported: March 23, 2013
Date Received: March 11, 2013
Date Sampled: March I I, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbar - Fayetteville Division
Chloride
.129
mg/L
3/12/13
18:24
JLR
EPA 300.0. Rev. 2.1 (1993)
COD, Total
40.7
mg/L
3/12/13
10:50
DSK
5220 D-1997
Conductivity
505
umhos/cm
3/12/13
8:40
DSK
SM 2510B-1997
Depth to Water Surface
3.50
feet
3/11/13
1538
DSD
Field Measurement
Nitrate as N
2.73
mg/L
3/12/13
18:24
JLR
EPA 300.0, Rev. 2.1 (1993)
PH, Field" Pest
4.56
pH Units
3/11/13
15:38
DSD
Field
Total Dissolved Solids
228
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997
Sulfate as SO4
6.7
mg/L
3112113
18:24
JLR
EPA 300.0, Rev. 2.1 (1993)
Temperature
14-' '
°C
3/11/13
15:38
DSD
Field '
Analyzed by: Mivobac tabomtories, Inc - Ohio Valley
Total Organic Carbon
4.54
mg/L
3/16/13
20:06
BAF
SM5310-C-2000
Slate Cerlilications:
NCDNR 411
NCDOH 437714
USDA #3737
Respectfully Submitted
,mac
Bonnie K. Sanders, Administrative Assistant
Page 8 of 16

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 23306
910.864.1920 Phone
910.864.3774 Fax
Certificate of Analysis
Aliens, Inc
Mr. Reid Wells Project: M/Welis samples - 3/l'early
5900 Turkey Highway
Turkey NC, 28393
R-5a
1303187-09
Date Repotted: March 23, 2013
Date Received: March 11, 2013
Date Sampled: March 11, 2013
Sampled By: Davidson
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mioobac- Fayetteville D.vision
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
PH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
28.5
mg/L
3/12/13
18:41
JLR
EPA 300.0, Rev. 2.1 (1993)
89.9
mg/L
3/12113
10:50
DSK
5220 D-1997
228
umhos/cm
3/12113
8:40
DSK
SM 251013-1997
2.50
feet
3/11/13
1538
DSD
Field Measurement
4.95
mg/L
3/12/13
18:41
JLR
EPA 300.0,Rev. 2.1(1993)
5.21
pH Units
3/11/13
15:38
DSD
Field
100
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997
22
mg/L
3/12/13
18:41
JLR
EPA 300.0. Rev. 2.1 (1993)
17
°C
3/11/13
15:38
DSD
Field
Analyzed by: Microbac Laboratodes, Inc. - Ohio Valley
Total Organic Carbon 3.16
State Cenilicalions,
NCDNR #I I
NCDDH #37714
USDA 93787
mg/L 3/16/13 20:29 BAF SM5310-C-2000
Respectfully Submitted
Bonne K. Sanders. Administrative Assistant
(9
Page 9 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc Dale Reported: March 23. 2013
Mr. Reid Wells Project M/N'ells samples-3/Yearly Date Received: March 11, 20
5900 Turkey I lip.hrvay Date Sampled: March 11, 2013
Turkey NC, 28393 Sampled By: Davidson
R-6
1303187-10
Analyte Result Units Analyzed Analyzed By Method Qualifier
M3lyzed by: Mic obac - Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
42.6
mg/L.
3/12/13
18:57
JLR
EPA 300.0. Rev.2.1 (1993)
64.2
mg/L
3/12/13
10:50
DSK
5220 D-1997 Al2
249
urrhos/cm
3/12113
8:40
DSK
SM 2510B-1997
4.40
feet
3111/13
15:38
DSD
Field Measurement
124
mg/L
3112/13
18:57
JLR
EPA 300.0, Rev. 2.1 (1993)
4.87
pH Units
3/11/13
15:38
DSD
Field
82.0
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997
15
mg/L
3112/13
18:57
JLR
EPA .300.0.Rev. 2.1 (1993).
15
°C'
3/11/13
15:38
DSD
Field
Analyzed try: Kc obac Laboratories, Inc. - Ohio Valley
Total Organic Carbon 13.5
Stale Certilications:
NCDNR #II
NCDDH 937714
USDA 93787
mg/L 3/16113 20:51 BAF SM5310-C-2000
Respectfully Submitted
Bonnie K. Sanders, Administrative Assistant
Page 10 of 15

Fayetteville Division
2592 Hope Mills Rd
t Fayetteville. NC 28306
910.864.1920 Phone
910 864.8774 Fax
Certificate of Analysis
Allen, Inc -
Mr. Reid Wells Project: M/VVells samples - 3/1'early
5900 Turkey Highway
Turkey NC, 28393
R-7
1303187-11
Date Reported: March 23. 2013
Date Received: March It, 2013
Date Sampled: March 11, 2013
Sampled By: Davidson
Analyle Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mivobac - Fayetteville Division
Chloride
70.9
COD, Total
109
Conductivity
296
Depth to Water Surface
1.10
Nitrate as N
0.915
pH. Field Test
5.09
Total Dissolved Solids
108
Sulfate as SO4
7.0
Temperature
16
Analyzed by: Microbac tabomtories, Inc - Ohio Valley
Total Organic Carbon
42.7
Slate Certifications:
NCDNR k11
NCDOH #37714
USDA B3787
mg/L
3/12113
19:14
JLR
EPA 300.D. Rev. 2.1 (1993)
mg/L
3/12/13
10:50
DSK
5220 D-1997
umhos/cm
3/12113
8:40
DSK
SM 251OB-1997
feet
3111/13
15:38
DSD
Field Measurement
mg/L
3/12/13
19:14
JLR
EPA 300.0. Rev. 2.1 (1993)
pH Units
3/11113
15:38
DSD
Field
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997
mg/L
3/12113
19:14
JLR
EPA 300.0. Rev. 2.1 (1993)
°C
3/I1/13
1538
DSD
Field
mg/L
3/16/13
21:15
BAF
SM5310-C-2000
Respectfully Submitted z
Bonnie K. Sanders. Administrative Assistant
Page 11 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc Date Reported: March 23, 2013
Mr. Reid Wells Project:. M/ll'ells samples-3/Pearl Date Reccived: March 11, 2013
5900 Turkey Highway Date Sampled: March 11, 2013
Turkey NC, 28393 Sampled By: Davidson
R-8
1303187-12
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Microbac- Fayetteville Division
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pl;, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature -
17.2
mg/L
3/12/13
19:31
JLR
EPA 300.0. Rev. 2.1 (1993)
40.7
mg/L
3/12/13
10:50
DSK
5220 D-1997
251
umhos/cm
3/12/13
8:40
DSK
SM 251OB-1997
3.20
feet
3/11/13
1538
DSD
Field Measurement
11.4
mg/L
3/12/13
19:31
JLR
EPA 300.0. Rev. 2.1 (1993)
4.74
pH Units
3/11/13
15:38
DSD
Field
82.0
mg/L
3/13/13
11:03
JAO
SM2540 C-1997
24
mg/L
3112/13
19:31
JLR
EPA 300.0. Rev. 2.1 (1993)
16
°C
3/I1/13
15:38
DSD
Field
Analyzed by: Microbac Laboratories, Inc.- Ohio Valley
Total Organic Carbon 2.65
Slate Cenil[cations:
NCDNR 911
NCDOH Il37714
USDA d3787
mg/L 3/16/13 21:37 BAF SM5310-C-2000
Res/peecllully Submitted
Bonnie K. Sanders, Administrative. Assistant
L,
Page 12 of 15

Allens, Inc
Mr. Reid Wells
5900 Turkey Highway
Turkey NC, 28393
Analyzed by: Miaobac - Fayetteville Diuisian
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH. Field'resl
Total Dissolved Solids
Sulfate as SO4
Temperature
Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 23306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Project: M/Wells samples - 3/1'early
R-9
1303187-13
Date Reported: March 23, 2013
Date Received: March 11, 2013
Dale Sampled: March 11, 2013
Sampled By: Davidson
9.79
mg/L
3/12/13
19:47
JLR
EPA 300.0, Rev. 2.1 (1993) B
85.6
mg/L
3/12/13
10:50
DSK
5220 D-1997
194
umhos/cm
3/12/13
8:40
DSK
SM 25 1013- 1997
4.60
feet
3/11/13
15:39
DSD
Field Measurement
2.93
nig/L
3112/13
19:47
JLR
EPA 300.0, Rev. 2.1 (1993)
4.81
pH Units
3/11/13
15:38
DSD
Field
252
mg/L
3/13/13
11:03
JAO
SM 2540 C-1997 S1
48
mg/L
3/12/13
19:47
JLR ...
EPA 300.0. Rev. 2.1 (1993)
16
°C .
3/11/13
1538
DSD
Field
Analyzed by: Miuobac Laboratories, Inc. - Ohio Valley
Total Organic Carbon 3.13
State Certifications:
NCDNR NI I
NCDOH N37714
USDA 43787
mg/L 3/16/13 21:58 BAF SM5310-C-2000
Respectfully Submitted
Bonnie K. Sanders. Administrative Assistant
Page 13 of 15

Fayetteville Division
2592 Hope Mills Rd
Fayetteville. NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc
Mr. Martin Griess Project: M/Wells samples-3/1'early part 2
5900 Turkey Highway
Turkey NC, 28393
MWHI
1304268-01
Date Reported: April 22, 2013
Date Received: April I I, 2013
Date Sampled: April 11, 2013
Sampled By: R. Wells
Analyze Result Units Analyzed Analyzed By Method Qualifier
Analyzed by: Mimbac laboratories, Inc. - Ohio Valley
Total Organic Carbon 22.6 mg/L 4/19113 10:36 BAF SM5310-C-2000
MW R-6
1304268-02
Analyzed by: Mivobac laboratories, Inc - Ohio Valley
Total Organic Carbon 11.4 mg/L 4/18/13 19:07 BAF
MW R-7
1304268-03
Analyzed by. Microbac Laboratories, Inc. - Ohio Valley
Total Organic Carbon 5.19 mg/L
Notes and Definitions
U Not detected at or above adjusted sample detection limit
Stale Certifications:
NCDNR VI
NCDOII #37714
USDA #3787
4/18/13 19:30 BAF
SM5310-C-2000
SM5310-C-2000
Respectfully Submitted
Jeanne Overstreet, Project Manager
Page 1 of 1

In G U p pl E M OR IHS s INS£
$f'FJ ' ,9z6
i
WW�� rew01
Iles .
5900 To N0-Nw`Sdm 1� 'H CAROLINA, 28393
c� foP�-
April 25, 2013 � il�ssi � one Z rr (Car) ,
Dept. of Environmental & Natural Resources
Division of Water Quality — Information Processing Unit
1617 Mail Service Center
Raleigh. NC 27699-1617
[phone]
RE: Groundwater Quality Monitoring Report
Aliens, Inc. —Turkey, NC Facility- ,
Permit # WQ0004269
t41 Y 13 2013
DENR-FAY'ETTEkLEREGIONAL 9FROU
Enclosed are the original and one copy of the Groundwater Monitoring Reporron-forms GW-59
and G W-59A, and the lab report for Aliens, Inc — Turkey, NC facility for samples collected in
March, 2013. '
Monitoring wells # MW-I, R-6 and R-7 exceeded the 10mg/L limit forTOC as stated in the permit.
These wells were resampled. R-7 is within the permit requirement, but M W-I and R-6 were still slightly
over. We will continue to monitor these closely in the future.
If you have any questions or require any additional information, please contact me by
phone at [phone].
Sincerely,
Robert Caldwell
Plant Manager
Aliens, Inc. Turkey facility
CC: Laura Mushinski, Aliens. Inc
Reid Wells, Aliens. Inc —Turkey facility
MAY - 3 Z013
WATER QUALITY SECTION
INFORMATION PROCESSING UNIT

ro0 U, rr E M O R I E S S INCS I ..
Quality Vegetables
5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA, 28393
PHONE [phone]
FAX [phone]
January 3,2013
Dept. of Environmental & Natural Resources
Division of Water Quality — Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
RE: Groundwater Quality Monitoring Report
Aliens, Inc. — Turkey, NC Facility
Permit # WQ0004268
This letter is in response to the Groundwater Monitoring Report dated December 18, 2012 for the Aliens,
Inc -Turkey, NC facility.
The report showed the TOC level in M W # R-6 exceeded the 10 mg/L limit as specified in the permit.
The well was resampled and the results were within the permit requirements. The result is listed on the
following page.
If you have any questions or require any additional information, please contact me by
phone at [phone].
Sincerely,
Robert Caldwell
Assistant Plant Manager
Aliens, Inc. Turkey facility
CC: Laura Mushinski, Aliens, Inc
Reid Wells, Aliens, Inc —Turkey facility
I
I
i CA g9h al l w2ls
SOt{ wel(3 Q b(�hf9qh no`ioe JtW i
1 Np3 Nwi rhyh-wec-901wjs;V
®ENR-FRO
AN 2Z'2013
r)W0
RECOVER
JAN 11 2013
,,formatiioo�� Sum Unit

2
TER QUALITY MONITORING:
E REPORT FORM
Name: Allens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
ty NC 28393-9703 County Sampson
act Person: Robert Caldwell
Location/Site Name:_
Telep hone#:. 910-596-0028
No. of wells to be samDled: 1
IRMITNumber: Expiration Date: July 31, 2015
n-Discharge WQ0004268 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon.. ❑ Remediation: Infiltration Gallery
© Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
WELL ID NUMBER (from Permit): R-6
Well Depth: ft.
Depth to Water Level: ft. below measuring point
Measuring Point is ft. above land surface
(Volume of water pumped/bailed before sampling:
Samples for metals were collected unfiltered: ❑YES
Date sample collected: 1216112
Well Diameter: _in.
Screened Interval: _ft. to _ft.
Relative M.P. Elevation: ft.
10+ gallons
❑ NO and field acidified:. ❑ YES ❑ NO
FIELD ANALYSES:
pH _units Temp. oC
Spec. Cond. µ
Odor
Appearance
WAS
DRY at
time ofMhos sampling,
check
here: ❑
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD mgA
Nitrite (NO2) as N
mg/l
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
mgA
Zn-Zinc mg/I
Coliform: MF Total 1100ml
Phosphorus: Total as P
mgA
(Note: Use MPN method for Nghly turNd samples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total mgA
AI - Aluminum
mg/I
pH (when analyzed) units
Ba - Barium
mgA
TOC 9.02 mgA
Ca - Calcium
mgA
Chloride mgA
Cd- Cadmium
mg/I
Arsenic mg/1
Chromium: Total
mgA
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mgll
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mgll
Hg- Mercury
.mgA
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance µMhos
K= Potassium
mg/I -
VOC , method #
Total Ammonia mgA
Mg - Magnesium
mg/l
, method #
(Ammonia Nitogen; NH�as N; Ammonia Nitrogen, Total)
Mn- Manganese
mgA
,method#
TKN as N mgA
Ni - Nickel
mg/l
, method #
For Remediation Systems Only; (Attach Lab Reports):. _
_ , ,,Inf1uent-.Total VOCs: <-., ..... _. -
mg/L.: ;Ef luentTotal VCCs:. mg/L , VOC Removal%
Robert Caldwell, Assistant Plant Manager t./yypAf
Penm nittee(orAuthorized Agent) Name and Title -Please print or type - _. .. ..Slgnatureaf Pe Mee(or Authorized Agent)
GW-59 Rev, 1/2007
1

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc
Date Reported: December 18, 2012
Mr. Reid Wells
Project: M/W samples- 3/Yearly, Retest Date Received: December 06, 2012
5900 Turkey Highway
Date Sampled: December 06, 2012
Turkey NC, 28393
Sampled By: R. Wells
M/W - R-6
1212143-01
Analyte Result Units Analyzed Analyzed By Method Qualifier
Analyzed by. Kmbac- Ohio Valley Division
Total Organic Carbon
Stale Certifications:
NCDNR HI I
NCDOH 937714
USDA #3787
9.02 mg/L 12/6/12 0:00 OVD SM 5310C
^Respectfully Submitted
7eanne Overstreet, Project Manager
Pano 1 of l