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WQ0004268_GW Monitoring_20091210
s S�PJ SKO Up S18M O RIES S , & o R 19g6.O • Quality Vegetables 5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA, 28393 PHONE 910-596-0028 FAX 910-596-0127 December 10, 2009 Dept. of Environmental & Natural Resources Division of Water Quality — Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 (919) 733-3221 RE: Groundwater Quality Monitoring Report Allen, Inc. — Turkey, NC Facility Permit# WQ0004268 Enclosed are the original and one copy of the Groundwater Monitoring Report on forms GW-59 and G W-59A, and the lab report for Allens, Inc — Turkey, NC facility for samples collected in November 2009. If you have any question or require any additional information, please contact Reid Wells by phone at (910) 596-0028 ext # 115 or by email at rwells@allens.com. Sincerely, 1 Martin Griess Plant Manager Aliens, Inc. Turkey facility CC: Laura Mnhinski, Allens, Inc Reid Wells, Allens, Inc — Turkey facility RECEIVED DEC 2 9 2009 information Processing Unit DWQIBOG SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: EPARTMENT..OPENVIRONMENT&NATURAL RESOURCES _ OIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 817MAIL SERVICE CENTER, RALEIGH,NC77fi98.1fi17 Phone:(979)T933227 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: 'Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge W00004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon Remediation: Infiltration Gallery Turkey "" ' NC 28393-9703 County Sampson .1 ® Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well LocationlSite Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: mm Perm l SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 1 Date sample collected: 11/2/09 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: in. pH 4.43 units Temp. 18.9 eC DRY at Depth to Water Level: 23.2 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: El YES El NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO,) as N mg/I Pb - Lead mg/I Coliform: ME Fecal /100ml Nitrate (NO3) as N 1,95 mg/I ,Zn - Zinc mg/I Coliform: ME Total /100ml Phosphorus: Total as P mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate mgll Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 3420 mg/l AI - Aluminum mg/l pH (when analyzed) units Be - Barium mg/I TOC 2.4 mg/I Ca - Calcium mgA Chloride 211 mg/I Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/l Grease and Oils mg/I Cu - Copper mgll ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/l Fe - Iron mg/l (Specify test and method A ATTACH LAB REPORT.) Sulfate 27.4 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 1057 µMhos K- Potassium mg/I VOC ,method# Total Ammonia mg/I Mg - Magnesium mg/I ,.method # (Ammenla Nitrogen; NHaes N; Ammonia Nitrogen, Total) Mn - Manganese mg/1 , method # TKN as N mg/I Ni - Nickel mgll , method# For Remediation Lab Reports): Influent Total VOCs: Martin Griess, Plant Manager Permltlee (or Authorized AAent) Name and Title - Please print or type GW-59 Rev. 112007 Effluent Total VOCs: 'ULU of Information Processing Unil O WQ/BOG Removal% /.2 / to SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER; RALEIGH,NO27699-1617 Photie:(919)733.3221' FACILITY INFORMATION Please Plot Crearry or Type PERMIT Number: Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge W00004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkev NC 28393-9703 County Sampson ® Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: eom Pemiil SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 2 Dale sample collected: '11/2/09 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter; in. pH 5.25 units Temp. 17.2 eC DRY at Depth to Water Level: 9.8 ft. below measuring p g point Screened Interval: (l. to ft. Spec. Cond. µMhos time of Measuring Point is, ft. above land surface Relative M.P. Elevation: ft. Odor sampling, check Volume of water pumped/balled before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: [DYES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Datesample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO,) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N <1.00 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid eamples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 252 mgn AI - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 2.4 mg/I Ca - Calcium mg/I Chloride 126 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 4.63 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 689 µMhos K - Potassium mg/I VOC , method # Total Ammonia mg/I Mg - Magnesium mg/I , method # (Ammonla Nitrogen; NHsas N;Ammonia Nitrogen. Total) Mn- Manganese mg/I ,method# TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Lab Reports): Influent Total Martin Griess, Plant Manager Permittee (or Authorized Agent) Name and Title -Please print or type GW-59 Rev. 1/2007 ' Effluent Total VOCs: ,genq 2009 Information Processing Uni: DwC)/BOG VOC /0 / o SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NO 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Pinf Clearly or Type PERMIT Number: Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey `" NC 28393-9703 County Sampson ® Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor. ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: Irom Pemut SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 3 Date sample collected: 11/2/09 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: in, pH 5.86 units Temp. 17.1 ac DRY at Depth to Water Level: 4.0 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. I µMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO,) as N <0.50 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mgll (Note: Use MPN method or hl9Ny lurbld samples) Orthophosphate mg/l Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 333 mg/I AI - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 1 A mg/i Ca - Calcium mg/I Chloride- 57.5 mg/I Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) r Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 68.5 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 285 µMhos K - Potassium mg/I VOC , method # Total Ammonia mg/I Mg - Magnesium mg/I , method # (Ammonia Nirogen; NHras N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/1 , method # For Remediation Lab Reports): Influent Total VOCs: Martin Griess, Plant Manager Pennitlee(or Authorized Agent) Name and Trite- Please print or toe ' GW-59 Rev. 1/2007 Effluent Total VOCs: Information Processing Unit DWQ/BOG VOC Removal% O /0 SUBMIT FORM ON YELLOW. PAPER ONLY DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING; DIVISION OF WATER OUALITY41,11FORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH,No27699.1617 Phone: (919)733-3221 FACILITY INFORMATION Please Pont Clearly or Type PERMIT Number: Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey NC 28393-9703 County Sampson 0 Spray Field ❑ Remediation: Contact Person: Martin Griess. Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ElOther: (from Fero l SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 4 Dale sample collected: 11/2/09 FIELD ANALYSES:- WAS Well Depth: ft. Well Diameter: In. pH 4.23 units Temp. 19.1 eC DRY at Depth to Water Level: 11.6 ft. below measuring point — Screened Interval: to R. Spec. Cord. µMhos time of _ft. sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: " Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO2) as N mgll Pb - Lead mgA Coliform: MF Fecal /100ml Nitrate (403) as N <0.50 mg/1 Zn -Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for hl9Ny turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 92.0 ni At - Aluminum ni pH (when analyzed) units Be - Barium mg/I TOC 1.9mg/l Ca - Calcium mgB Chloride 10.7 mg/I Cd- Cadmium mg/l Arsenic mg/I Chromium: Total - mg/l Grease and Oils ni Cu - Copper mg/I ORGANICS: (by GC, GC/MS; HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 17.1 mg/l Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 191 µMhos K - Potassium mg/I VOC, method # Total Ammonia ni Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NH,as N; Ammonla Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Lab Reports): Influent Total Martin Griess, Plant Manager Pennittee (or Authorized Anent) Name and Title - Please print or type GW-59 Rev. 112007 Effluent Total VOCs: mo/L VOC OEC 2 9 2009 Information Processing Ufw DWO/BOG (L /U SUBMIT FORM ON YEI I QVL PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT L NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1817 MAIL SERVICE CENTER, RALEIGH,NC27699-1617 Phone:(919)779J221 FACILITY INFORMATION Please print pearly or Type PERMIT Number: Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey -' NC 28393-9703 County Sampson ® Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-59670028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: from Pemvl SAMPLING INFORMATION - - If WELL WELL ID NUMBER (from Permit): MW R-1 Date sample collected: 11/2109 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: pH 4.90 units Temp. 18.0 °C DRY at Depth to Water Level: 10.8 ft. below measuring point _in. Screened Interval: ft, to ft. Spec. Cord. µMhos limof - sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LA130RATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should_ reflect dissolved and colloidal concentrations. COD 117 mg/I Nitrite (NOT) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N 6.89 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 98.0 mg/i AI - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 4.6 mg/I Ca - Calcium mg/1 Chloride 17.2 mg/l Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu- Copper mg/l ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 1.52 mg/I Hg- Mercury mg/I Report Attached? ❑ Yes(1) ❑ No Specific Conductance 149 µMhos K - Potassium mg/I VOC , method # Total Ammonia mg/I Mg - Magnesium ni , method # (Ammonia Niu.gen; NHres N; Ammonia Mustier, Told) Mn- Manganese mg/I ,method# TKN as N mgA Ni - Nickel mg/I , method # For Remediation Lab Reports): Influent Total Martin Griess, Plant Manager Permittee (or Authorized Agent) Name and Title - Please Print or type GW-59 Rev. 112007 Effluent Total VOIDS: Information Processing Unit DWQ/BOG VOC Removal% SUBMIT FORM ON YELLQW PAPER ONLY GROUNDWATER QUALITY MONITORING: -DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES OFWATER QUALITY -INFORMATION PROCESSING UNIT ' COMPLIANCE REPORT FORM aDIVISION 1617 MAIL SERVICE CENTER, RALEIGH,NC27699.1617 Phone:(919)733a221 FACILITY INFORMATION Please error Clearly or Type PERMIT Number: Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey "'' NC 28393-9703 County Sampson ` "' ® Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: l No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: Irom Pemtil SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW R-2 Date sample collected: 11/2/09 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: _in. pH 5.86 units Temp. 18.1 eC DRY at Depth to Water Level: 6.10 ft. below measuring point Screened Interval: ft. to Spec. Cond. ItMhos time of _ft. sampling, Measuring Point is ff. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 61.4 mgll Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N <0.50 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/1 Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 96.0mg/I AI -Aluminum mg/1 pH (when analyzed) units Be - Barium mg/I TOC 6.9 mg/I Ca - Calcium mg/I Chloride 7.01 mg/I Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/l Cu - Copper mg/1 ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mgll (Specify test and method A ATTACH LAB REPORT.) Sulfate 11.1 mgll Hg -.Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 93.6 µMhos K - Potassium mg/I VOC , method # Total Ammonia mg/l Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NHsas N;AmmoNa NiVogen. Total) Mn- Manganese mgll ,method# TKN as N mg/I Ni - Nickel mg/l , method # GW-59 Rev. 112007 Information Processing Unit DWO/BOG SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: N DEPARTMENT OF ENVIRONMENT a NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAILSERVICE CENTER, RALEIGH,NC27609-1617 Phone: (019)7334221-, FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: July_31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remedialion: Infiltration Gallery Turkey NC 28393-9703 County Sampson 1 0 © Spray Field ❑ Remedialion: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: rom Perms SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW R-3 Date sample collected: 1112109 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: PH 4.43 units Temp. 16.6 aC DRY at Depth to Water Level: 9.4 ft. below measuring point _in. Screened Interval: ft. to ft. Spec. Cord. pMhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES El NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 40.9 mg/I Nitrite (NO2) as N mgfl Pb - Lead Mg/1 Coliform: ME Fecal /100ml Nitrate (NO3) as N <0.50 mgll Zn - Zinc mgll Coliform: ME Total /100m1 Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other(Specify Compounds and Concentration Units): Dissolved Solids: Total 42.0 mg/l AI - Aluminum Mgt[ PH (when analyzed) units Be - Barium mg/l _ TOC 2.5 mg/I Ca - Calcium mg/I Chloride 6.49 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/l Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 8.67 mg/l Hg- Mercury mg/i Report Attached? ❑ Yes(1) ❑ No Specific Conductance 77.1 pMhos K- Potassium ri VOC ,method# Total Ammonia mg/I _m Mg - Magnesium mgll , method # (A orua Nitrogen; NHsas N; only Nibogan, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Lab Reports): Influent Total Martin Griess, Plant Manager Permiltee (or Authorized Agent) Name and Title - Please Print or Woe GW-59 Rev. 1/2007 Effluent Total VOCs: mglL VOC information Processing Unit DWQ/BOG O SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 7g9-9221', FACILITY INFORMATION Please Print clearly or Type PERMIT Number: Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey INC 28393-9703County SaMpSon Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: mm Pmm SAMPILING .INFORMATION If WELL WELL ID NUMBER (from Permit): MWR-4 Date sample collected: 1.1/2109 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: _in. pH 4.17 units Temp. 16.8 aC DRY at Depth to Water Level: 10.3 ft. below measuring point Screened Interval: to Spec. Cond. ItMhos time of _ft. _ft. sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 27.9 mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N <0.50 mg/I Zn - Zinc mg/I Coliform: MF Total 1100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 123 mg/I AI - Aluminum mgll pH (when analyzed) units Be - Barium mg/1 TOC 0.7 mg/i Ca - Calcium mg/I Chloride 8.42mg/l Cd- Cadmium mg/I Arsenic mg/l Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iran mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 38.0 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 194 µMhos K - Potassium mg/I VOC , method # Total Ammonia mg/l Mg - Magnesium mg/I , method # (Ammonia Nitrogen: NH3 as N;Ammonla Nitrogen, Tobl) Mn- Manganese mg/1 ,method# TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Martin Griess, Plant Manager Pennines (or Authorized Apene Name and Title - Please print or Noe GW-59 Rev. 1/2007 Effluent Total VOCs: Information Processing Unit DWQIBOG VOC SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL'SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (9191733.3221 FACILITY INFORMATION Please Pant Clearly or Type PERMIT Number: Expiration Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey " "' NC ' 28393-9703 County Sampson XI Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#:. 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heal Pump ❑ Other: eem Pemul SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW R-5 Date sample collected: 11/2/09 _ FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: pH 4.20 units Temp. 17.1 eC DRY at Depth to Water Level: 8.8 ft. below measuring point _in. Screened Interval: ft. to ft. Spec. Cord, (tMhos time of Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 31.9 mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /loom[ Nitrate (NO3) as N <1.00 mgll Zn - Zinc mg/I Coliform: MF Total /100m1 Phosphorus: Total as P mg/l (Note: Use MPN method for highly turbid samples) Orthophosphate mg/l Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 196 mg/I AI -Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 0.7 mg/I Ca - Calcium mg/I Chloride 24.0 mg/I Cd- Cadmium mg/i Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 68.4 mg/I Hg - Mercury mg/1 Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 299 NMhos K - Potassium mg/I VOC , method # Total Ammonia mg/I Mg - Magnesium mg/l , method # (Ammonia Nitrogen; NHaas 17,_mrda Nitrogen, Total) Mn- Manganese mg/I ,method# TKN as N ni Ni - Nickel mg/I , method # For Remediation Lab Reports): Influent Total Martin Griess, Plant Manager Permittee (or Authorized Agent) Name and Title -Please print or type GW-59 Rev, 1/2007 Effluent Total VOCs: InEormatlon Processing Unii DWQjBOG VOC Removal% /V AU SUBMIT FORM ONYFLLOW PAPFR ONLY GROUNDWATER QUALITY MONITORING: EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY4NFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM ye 617MAIL SERVICE CENTER, RALEIGH,No27699.1617 Phone:(9191799.6221 FACILITY INFORMATION Pease Print Clearly or Type - PERMIT Number: Expiation Date: July 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge W00004268 UIC NPDES Other _ Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remedlation: Infiltration Gallery Turkey NC 28393-9703 County Sampson 1. � ® Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ •Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other: Irom Pemul SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW R-6 Date sample collected: 11/2109 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: _In. pH 4.17 units Temp. 18.5 eC DRY at Depth to Water Level: 9.11 ft. below measuring point Screened Interval: ft. to Spec. Cond. µMhos time of Measuring Point is ft. above land surface Relative M.P. Elevation: _ft. ft. Odor sampling, check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Mlcrobac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 57.6 mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N 1.88 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/1 (Nob: Use MPN method for highly lurbld samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 148 mg/I Al - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I ' TOC 4.3 mgn Ca - Calcium mg/I Chloride 36.4 mg/I Cd-Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe -Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 52.1 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 219 µMhos K - Potassium mg/1 VOC , method # Total Ammonia mg/l Mg - Magnesium mgll , method # (Ammonia Nitrogen; NHsas N; Ammonia Nitrogen. Total) Mn- Manganese _ mg/l ,method # TKN as N mg/l Ni - Nickel mg/I method # For Rennediation Systems Only • I certify that to the he5l of my4knoµ,lerlpa ar(d belle!+the lnJormati n;pybmdfedlq�ll lszrepor�t °' a cbraWand co.�Iple(g"�angllhel,thelabo'p'lory •alyiical'tlata^yinv'lra luoediisirlr7a pfatied'.'(pASlysls-bye ,. r e:.4, ♦L4111, e. sv "Tq+ 8�-.�! � 'ri Je"tm'C., dy a 9:-i7r+.hTla li"f+.R�.€,r�7'ia• D\NO-carfl6ed:15liSialo 1 11 am/a(vere�tbahthere'erfl s9g'nlflaanL anal ea.fof'sugmTtiiit "ralse`Inrwme ioavincludln the possibhi of=hnes•e d ImptlsoAmep6rdk:kpo nq v ManagerMartin Griess, Plant � e Permillee [orAuthonzedAqenfN-rne and Tire -Please print or type Siqnature of Panthers (or Authorized Agent)- r GW-59 Rev. 112007 Information Processing •:• SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: - EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM �, 617MAIL SERVICE CENTER, RALEIGH,NC27G99-1617 Phone:(919)73JJ221 FACILITY INFORMATION Pease Print clearly or Type PERMIT Number: Expiration Date: July 31. 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon Ll Remediation: Infiltration Gallery Turkey NC 28393-9703 County Sampson -' © Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heat Pump ❑ Other. from Panril SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW R-7 Date sample collected: 11/2/09 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter: _in. pH 3.97 units Temp. 19.9 eC DRY at Depth to Water Level: 10.11 ft. below measuring point Screened Interval: ft, to ft. Spec. Cond. Mhos time of sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+ gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Mlcrobac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 105 mg/I Nitrite (NO2) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N <0.50 mg/1 Zn - Zinc mg/I Coliform: MF Total /100m1 Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 135 mg/I AI -Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 8.5 mg/1 Ca - Calcium mg/I Chloride 21.2 mg/I Cd- Cadmium mgll Arsenic mg/I Chromium: Total mg/l Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/1 Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 51.5 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 276 µMhos K - Potassium mg/I VOC , method # Total Ammonia mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NHsas N;Ammonla Nitrogen. Total) Mn- Manganese mg/I ,method# TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: Effluent Total Martin Griess, Plant Manager Ly`E'_ ` � Q ai or cuu., PermlUse (or Authorized Agent) Name and Title -Please print or type Signature gi Permittee (of Authorized Agent) GW-59 Rev. 112007 information Processing DWQ/BOG VOC Removal% SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 16117 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 733.3221 FACILITY INFORMATION Please Flint Clearly or Type PERMIT Number: Expiration Date: JUly 31, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED TurkeV NC 28393-9703 County Sampson ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: Contact Person: Martin Griess Telephone#: 910-596-0028 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: No. of wells to be sampled: 12 ❑ Water Source Heal Pump ❑ Other: from Pemut SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW R-8 Date sample collected: 11/2/09 FIELD ANALYSES: WAS Well Depth: ff. Well Diameter: in. pH 5.76 units Temp. 16.9 aC DRY at Depth to Water Level: 11.10 ft. below measuring point — Screened Interval: to Spec. Cond. ItMhos time of _fl. —ft. sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 10+gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 22.6 mg/I Nitrite (NO.) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N 23.0 mg/l Zn - Zinc mg/1 Coliform: MF Total /100ml Phosphorus: Total as P mg/1 (Note: Use MPN method for highly tuield samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 226mgn AI - Aluminum mg/I PH (when analyzed) units Be - Barium mg/I TOC 2.3 mg/I Ca - Calcium mg/I Chloride 24.3 mg/l Cd - Cadmium mg/I ' Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 15.4 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 434 µMhos K- Potassium mg/I VOC , method # Total Ammonia mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NH3es N; Ammonia Nilmgen, Total) Mn- Manganese mg/I ,method# TKN as N mg/1 Ni - Nickel mg/l ; method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total Vws;-- * vrrn f— mg/L VOC Martin Griess, Plant Manager_st Permittee (or Authorized Agent) Name and Title -Please print or type Signature of Permitlee for Authprizedp {)processing UoR GW-59 Rev. 1/2007 lrltOrmal� p11Vt]/BOG p Microbac Laboratories, Inc. Page I of 3 FAYETTEVILLE DMSION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVILLE, NC 28306 NC #11 (910) 864-1920 FAX (910) 864-8774 NC #37714 R W. SANDERS, VICE PRESIDENT USDA #3787 http://w .raicrobac.com E-Mail: rsanders@cnicrobac.com WAITER AAIIRR WASTES- FLOOD- P OHARMACEUTICALLS CONSUMER CERTIFICATE OF ANALYSIS Allens, Inc Date Reported: 11262009 Ms. Kathryn Yeager _ Date Received: 11/022009 Post Office Box 250 Order Number: 0911-00219 Siloam Springs, AR. 72761 Invoice No.: 69611 Customer #: A004 Sample Date: 11/022609 Permit EY PLANT Sample Time: 0:00 Samplerr:: Miller iller' Subject: M/Well samples-3/Yearly SKIP Test Method Result Date Time Tech CHLORIDE SM 4500 Q C 211 mg/L 11/05/2009 11:34 ENC COD, SM 5220 D <10 mg/L 11/09/2009 9:00 ENC CONDUCTIVITY SM 2510 B 1057 umhos/ov 11/03/2009 11:45 DCR NITROGEN, NITRATE SM 4500 NO3 E 1.95 mg/L 11/03/2069 13:25 ARS pH, FIELD FIELD 4A3 s.u. 11/02/2009 '10:11 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 3420 mg/L 11/09/2009 10:00 ARS SULFATE SM 15th 426 C 27.4 mg/L 11/03/20D9 13:25 ARS TEMPERATURE FIELD 18.9 deg., C 11/O7j2009 10:11 ROM TOTAL ORGANIC CARBON SM 5310B 2.4 mg/L 11/09/2009 0:00 ECI WATER LEVEL FIELD 23.2 feet 11/02/2009 10:11 ROM 002- M/W'#2. CHLORIDE SM 4500 a C 126 m91L 11/03/2009 13:25 ARS COD SM 5220 D <10 mg/L 11109/2009 9:00 ENC CONDUCTIVITY SM 2530 E 689 umhos/w 11/0312009' 11:45 DCR NIrROGEN,NITRATE SM 4500 NO3 E <3.06 mg/L 11/03/2009 13:25 ARS pH, FIELD FIELD 5.25 s.u. 11/02/2009 10:36 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 2S2 mg/L 11/09/2009 10:00 ARS SULFATE SM 15th 426 C 4.63 mg/L 11/03/2009 13:25 ARS TEMPERATURE FIELD 17.2 deg.,C 11/02/2009 10:36 ROM TOTAL ORGANIC CARBON 5M 53108 24 mg/L 11/09/2009 0:00 ECI WATER LEVEL FIELD 9.8 feet 11/02/2069 10:36 ROM 003 M/W #3 LAB CODES: N/D=None Detected N/F=None Fowd <=Less duct >=Gmacrthaa Fst.=Fstimated Tle4m amalvhdamabmmia'veemms. uiaWcaa�ga^W9 d�a�4 �ae�r mev�ryk(s)amM+elaNcmmm wmne ME�NeErR�w �m�wtenmem e.�am®+w*+Wa•mpan raaa.amuq araeeMV�gM4uNwetlmaB alfimn u:eae�.mr,. �A��pA USM.f➢A-NIOAI TCWI ratl SnOa,bn Convtlmg Umial aE MuoEbMh3l Nah$aM fl6miN P���ll■ Microbac Laboratories, Inc. Page 2of3 FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. FAYE=ILLE, NC 28306 NC #11 (910) 864-1920 FAX (910) 864-8774 NC #37714 R- W. SANDERS, VICE PRESIDENT USDA #3787 http://W .microbar—com E-Mail: rsanders@microbac.com RSRSTS�ODODCETSSNCCALWATEAIWAEEFOOPHARMAUICALLMITRAEUIIS CERTIFICATE OF ANALYSIS Aliens, Inc. Date Reported: 11/26/2009 Ms. Kathryn Yeager Date Received: 11/022009 Post Office Box 250 Order Number: 0911-00219 Siloam Springs, AR 72761 Invoice No.: 69611 . Customer #: A004 Sample Date: 11/022009 NC TURKEY PLANT m Sample Time: 0:00 - Sal Sampler: Miller Subject: M/Wellsamples-3/Yearly SNIP Test Method Result Date Time Tech 603 CHLORIDE SM 4500 CI C 57.5 mg/L 11/03/2009 13:25 ARS COD SM 5220 D <10 mg/L 12/09/2009 9:00 ENC CONDUCTIVITY SM 2510 8 285 umhos/an 11/03/2009 11:45 DCR NITROGEN; NITRATE SM 4500 NO3 E <0.50 mg/L 11/03/2009 13:25 ARS PH, FIELD FIELD 5.86 sm. 11/0Z/2009 10:59 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 333 mg/L 11/09/2009 10:00 ARS SULFATE SM 15th 426 C 68.5 mg/L 11/03/2DO9 13:25 ARS TEMPERATURE FIELD 17.1 deg., C 11102/2D09 10:59 ROM TOTAL ORGANIC CARBON SM 5310B 1.4 mg/L 11/09/2009 0:00 ECI WATER LEVEL FIELD 4.0 feet 11/02/2009 10:59 ROM DDa M/W #4, CHLORIDE SM 4500 a C 10.7 mg/L 11/03/2009 13:25 ARS COD SM 5220 D <10 mg/L 11/09R009 9:00 ENC CONDUCTIVITY SM 2510 B 191 umhos/an 11/03/Z009 11:45 DCR ' NITROGEN, NITRATE SM 4500 NO3 E <0.50 mg/L 11/03/2009 13:25 ARS PH, FIELD FIELD 4.23 su. 11/02/2009 12:40 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 92.0 mg/L 11/09/2009 10:00 ARS SULFATE SM 15th 426 C 17.1 mgfL 11/03/2009 13:2.5 ARS TEMPERATURE FIELD 19.1 deg., C 11/02/2009 12:40 ROM TOTAL ORGANIC CARBON SM S310B 1.9 mg/L 11/09/2009 0:00 Ea WATER LEVEL FIELD 11.6 feet, 11102/2009 12:40 ROM LAB CODES: WD=None I)uw d N/F=Noun Found <=Less than >=Gmarerthan Est—Esdaua d Ile&maemauaam,umm ddandt, anw.� NomieR T®�MEMBER Rt m'Nbl mua s mr mne � wh*. mPmroraC+utwn a WVMr�MhvAw apa m Uc hbV . IRO AilI Tot4 fNAMatvI Cd6WIM1g Omia MbaUblo INalsmaNR®d ��'�a p Microbac Laboratories, Inc. Page 3 of 3 FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVB.LE, NC 28306 NC#11 (910) 864-1920 FAX (910) 864-8774 NC #37714 , R. W. SANDERS, VICE PRESIDENT USDA #3787 http://w .microbar-corn E-Mail: rsanders@rniuobac.com CHEMISTRY • MICROBIOLOGY • FOOD SAFETY - CONSUMER PRODUCTS WATER • AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS CERTIFICATE OF ANALYSIS Allens, Inc. - Date Reported: 11262009 Ms. Kathryn Yeager Date Received: 11/02/2009 Post Office Box 250 Order Number: 0911-00219 Siloam Springs, AR 72761 Invoice No.: 69611 Customer #: A004 Sample Date: 11/022009 Sampler: Miller NC TURKEY PLANT ml - Sample Time: 0:00 Sa Subject M/Well samples-3/Yearly SNIP Tot Method Result ImS7 Date Time Tab RESPECTFULLY SUBMITTED: IT, i'Y �2m�ieM. MICROBAC LABORATORIES, INC. rhankyoufor)vurbostness. Welmireyourfeelb ckonourlevelofsemcetoyom Please contact the faborolory Director, Ron Sander, at 910864-1910, RobertMorgea, COO, at rmorgan@oda,obaccom or Trevor Boyce, CEO, at tboyce@nvcmbaccom with any commenu orsaggestiont. LAB CODES: NA) =Noce Dctead NIF=None Found <=Less than >=Greaterthan E5=Rfi Mod lhdammtlWCLPmnutbnaemhnlm Ns, Mm Waamn9anylnJrbvmsS R.�am'r/tlesampk(s)amlRal a�tlkimGeat WvtM1e MEMBER mnmmn umacraemee,ermmt.dooto-mpartr«ameteuuamv vm�aatwtvnmenaao-wsi rn.n oe aeo-am�t. uSOA-mA-nm515 Tawg loos Saaaatlan raciilt49 �IaN Mumbbglal a,arysnaid nceam A p Microbac Laboratories, Inc. Page I of FAYETTEVILLE DIVISION 2592 HOPE TvIILLS ROAD STATE CERT ID. FAYETTEVILLE, NC 28306 NC#11 (910) 864-1920 FAX (910) 864-8774 NC 07714 R: W. SANDERS, VICE PRESIDENT USDA #3787 http://w .microbac.com I<hfak-rsanders@microbac.com WATERS AIR • WASTES - FOOD FOOD IA RMACEUCICALLS SNNUUTTRRACEOUD PRODUCTS CERTIFICATE OF ANALYSIS Allens, Inc. Date Reported: 111192009 Ms. Kathryn Yeager Date Received: .; 1122009 Post Office Box 250 Order Number: 0911-00220 Siloam Springs, AR 72761 Invoice No.: 69451 Customer#: A004 - Semple Date: 1122009 Permit NC TURKEY PLANT' Sample Time: 0:00 Sampler:r: Miller Subject: M/Well samples -3/Yeady SAIP Test Method Result Date Time Tech 001 M/W Rd CHLORIDE SM 4500 CI C 17.2 mg/L 11/3/2D09 15:45 ARS COD SM 5220 D 117 mg/L 11/9/2009 9:00 ENC CONDUCTIVITY SM 2510 B 149 umhWcrn 11/3/2D09 11:45 DCR NITROGEN, NITRATE SM 45DO NO3 E 6.89 mg/L 11/3/2009 15:45 ARS PH, FIELD FIELD 4.90 s.u. 11/2/2009 15:10 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 98.0 mg/L 11/9/2009 10:00 ARS SULFATE SM 15th 426 C 1.52 mg/L 10/2009 15:45 ARS TEMPERATURE FIELD 18.0 deg., C 11/2/2009' 15:10 ROM TOTAL ORGANIC CARBON SM 5310B 4.6 mg/1- 11/9/2009 0:DO ECI WATER LEVEL FIELD 10.8 feet 11/2/2009 15:10 ROM 002 M/W R_2 CHLORIDE SM 4500 a C 7.01 mg/L 11/312009 15:45 ARS COD _ SM 5220 D 61.4 mg/L 11/9/2009 9:00 ENC CONDUCTIVITY SM 2510 B 93.6 umhosIm 11/3/2009 11:45 DCR NITROGEN, NITRATE SM 4500 NO3 E <0.50 mg/L 11/3/2009 15:45 ARS PH, FIELD FIELD 5.86 s.u. 11/2/2009 24:55 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 96.0 mg/L 11/9/2009 10:00 ARS SULFATE SM 15th 426 C 11.1 mg/L 11/3/2009 15:45 ARS TEMPERATURE FIELD 18.1 deg., C 11/2/2009 14:55 ROM TOTAL ORGANIC CARBON SM 5310B 6.9 mg/L 11/9/2009 0:00 ECI WATER LEVEL FIELD 6.10 feet 11/2/2009 14:55 ROM LAB CODES: MID =None Detected N/F=None Found-<=Lessthm >=Oreatertban Est.=Estmwted meaam «m me uaonnaamommam m oax aaa m�a«nawaars�se,o.�ez,«vem�e«�ry mesan�q:l awymamc meem aaaa we asemeen mtlebn NURKrtbEe��P�m1 �taN«mPartt«at+«mai9«aNe o«o«eswalnuwiots zopwalfi«nmeYmram,s. trsonma moat Tesmq ram smwmn r«s�enq rnmum am nvomes'�miaep-aam Pcmm ® Microbac Laboratories, Inc. Page 2of3 FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVILLE,NC 28306 NC#iI (910) 864-1920 FAX (910) 864-8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA #3787 http://w -rnicrobaccom E-Mal rsauders@microbaccom WATERS AIIR - WASTESIOFOODY P OHARMACEUTICALLS - NUTRAPCEUI'ICALS CERTIFICATE OF ANALYSIS Allens, Inc. Daze Reported: 11/19/2009 Ms. Kathryn Yeager Date Received: 11/2/2009 Post Office Box 250 Order Number: 0911-00220 Siloam Springs, AR 72761 Invoice No.: 69451 Customer #: A004 Sample Date: 1112/2009 Permit NC TORKEY PLANT Sample Time: 0:00 Sampler.r: Miller Subject: M/Well samples - 3/Yearly SNIP Test hletbod Result Date Time Tech 003 M/W R-3 - CHLORIDE SM 4500 CI C 6.49 mg/L 11/3/2009 15:45 ARS COD SM 5220 D 40.9 mg/L 11/9/2009 9:00 ENC CONDUCTIVITY SM 2510 B 77.1 umhcs/uo 1113/2009 11:45 DCR NITROGEN, NITRATE SM 4500 NO3 E <0.50 mg/L 11/3/2009 15:45 ARS pH, FIELD FIELD 4.43 s.u. 11/2/2009 14:25 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 42.0 mg/L 11/9/2009 10:00 ARS SULFATE SM 15m 426 C 8.67 mg/L 11/3/2009 15:45 ARS TEMPERATURE FIELD 16.6 deg.,C 11/2/2G09 14:25 ROM TOTAL ORGANIC CARBON SM 5310D 2.5 mg/L 11/9/2009 0:00 ECI WATER LEVEL FIELD 9.4 feet 11/2/2009 14:25 RDM 004 M/W R-4 CHLORIDE SM 4500 0 C 8.12 mg/L 11/3/2009 15:45 ARS COD SM 5220 D 27.9 mg/L 11/9/2009 9:00 ENC CONDUCTIVITY SM 2510 a 194 umhps/cm 11/3/2009 11:45 DCR NITROGEN, NITRATE SM 4500 NO3 E <0.50 mg/L 11/3/2009 15:45 ARS pH, FIELD FIELD 4.17 sm. 11/2/2009 14:14 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 123 mg/L 11/9/2009 10:00 ARS SULFATE SM Ism 426 C 38.0 mg/L 11/3120M 15:45 ARS TEMPERATURE FIELD 16.8 deg., C I3/2/2009 14:14 ROM TOTAL ORGANIC CARBON SM 5310B 0.7 mg/L 11/9/2009 0:00 ECI WATER LEVEL FIELD 10.3 feet 11/2/2009 14:14 ROM LAB CODES: N/D=None Detected N/F=None Famd <=Less thm, >=Gteaterthan 13L=Fstimated Te �—mft aVaammpairyhg400emtt ogee *ft.n e(s)via,,ar kiv4valu ae MEMBER mam'onu rtak IRA-NIe�gaaJmlwlvirymm Pa QnsWfirq aarc wm�munnmm�aoaw=�em,ue vuo aemy. USD4EPANIe91Ta,6g FmISmNappn UrsuPhg Oe�tloi atl Mvobubg'�INalysesaNae�Ni ® Microbac Laboratories, Inc. Page of FAYETTE' LE DMSION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVE.LE, NC 28306 NC #1I (910) 864-1920 FAX (910) 864-8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA #3787 http://www.microbac-com E-Marsmdem@microbac.com CHEMISTRY • MICROBIOLOGY •FOOD SAFETY CONSUMER PRODUCTS WATER • AIR WASTES • FOOD - PHARMACEUTICALS - NUTRACEUTICALS CERTIFICATE OF ANALYSIS Aliens, Inc. Date Reported: 11/19/2009 Ms. Kathryn Yeager— Date Received: 11/22009 Post Office Box 250 Order Number: 0911-00220 Siloam Springs, AR 72761 Invoice No.: 69451 Customer #: A004 Sample Date: 11/22009 Pemut No. NC TURKEY PLANT Sample Time: 0:00 Sampler: Miller Subject: M/Well samples-3/Yearly SIMP Test Method Result Date Time Tech RESPECTFULLY SUBMITTED: UG_ YI' - Aamrl�An_. MICROBAC LABORATORIES, INC. Tlmnkyouforyourbasiness. Weimiteyourfeedbackonourlevetofsenicetayou Please, contact the Laboratory Dmecmr, Ron Sanders at 910-864-1920, Robert Morgan, COO, at rmorgan@m1crobaccom or Trevor Boyce, CEO, at lboyce a@nucrobaccom with any comment, orsoggesnow. LAB CODFS: N/D=None Detected MF=None Fowd <=Le than >=Greaterthaa Est=Fsfimzmd lbeeapmtlaNaii(mna0'pnar�avlonaW and ran MFMf,£R aoanipa�ryhgamnaes,npaentorcr Ne9nV=1z)arelr+ 1Atl k,ai0aef upon tle mmen w[ahm,mbenompmt wlnptormpaRra*Nvlk'vesmewpos6.atwxmmappwaltmm ee aeordma. ` uSMtPRN1(HIiR6q raodSar,Gtlonfm¢WYq Oim�i3laM niwtlobglml MalysezaN RN ], p Microbac Laboratories, Inc. Page 1 of FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVILLE,NC 28306 NC#I1 (910) 864-1920 FAX (910) 864.8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA #3787 http://ww .raiuobac.com E-Nfail: rsanders@microbac.com ESRRSIOOD0SCIS ODWATRAI• MICROBIOLOGY PHARMAEUTCAL- NUTR4 UTIC� CERTIFICATE OF ANALYSIS Aliens, Inc. Date Reported: 11/192009 Ms. Kathryn Yeager _-Daze Received: 11/7/2009 Post Office Box 250 Order Number: 0911-00639 Siloam Springs, AR 72761 Invoice No.: 69452 .Customer#: - A004 Sample Date: 1IM009 Permit No. NC TURKEY PLANT Sample Time: 0:00 Sampler. Miller _ Subject: M/Well samples - 3/Yearly SNIP Test Method Result Dale Time Tech 001 M/W R-5 CHLORIDE SM 4500 Q C 24.0 mg/L 11/3/2009 16:56 ARS COD SM 5220 D 31.9 mg/L 11/3/20D9 10:47 ENC CONDUCTIVITY SM 2510 B 299 umhos/tm I3/3/2009 11:4S DCR NITROGEN, NITRATE SM 4500 NO3 E <1.00 mg/L 11/3/2009 16:56 ARS pH, FIELD FIELD 4.20 S.U. 11/2/2009 14:00 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 196 mg/L 11/9/2009 10:00 ARS SULFATE SM15th 426 C 68.4 mg/L 11/3/2009 16:56 ARS TEMPERATURE FIELD 17.1 deg., C 11/2/2009 14:00 RDM TOTAL ORGANIC CARBON SM 5310B 0.7 mg/L 11/9/2009 0:00 ECI WATER LEVEL FIELD 8.8 feet 11/2/2009 14:00 ROM 002 M/W R-6. CHLORIDE SM 4500 CI C 36.4 m91L 11/3/2009 16:56 ARS COD SM 5220 D 57.6 mg/L 31/3/2009 10:47 ENC CONDUCTIVITY SM 2510 B 219 umhos/on 11/3/2009 11:45 DCR NITROGEN, NITRATE SM 4500 NO3 E 1.B8 mg/L 11/3/2009 16:56 ARS PH, FIELD FIELD 4.17 s.u. 11/2/2009 13:45 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 148 mg/L 11/9/2009 10:00 ARS SULFATE SM 15th 426 C 5LI mg/L 11/3/2009 16:56 ARS TEMPERATURE FIELD 18.5 deg., C 11/2/2009 13:45 ROM TOTAL ORGANIC CARBON SM 53108 4.3 ng/L 11/9/2009 0:60 Ea WATER LEVEL FIELD 9.11 feel 1r/2/2009 13:45 ROM LAB CODES: N/D=None Detected N/F=None Found <=Lem thaw >-O.eterthan Est -Estimated TMNd NoaelKmmatlonmeavelmtltlp, andoNe a¢nngmmeg mo�aK rt4me[md/NeSanit45)mWR idrtlk icEealtY tlG NEMHEF GNLLTtl Me—bEe rtpmr)m1MioAY4N WkMa'A'vRti9u WCWW Tb6 wdenappoM han ftbb y. } USOAfP OSHTe Iona SantatlonfnmMM f]gnralaM Mbobubg�l Marys¢drO fte=emi� p Microbac Laboratories, Inc. Page 2of3 FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVILLE, NC 28306 NC # I1 (910) 864-1920 FAX (910) 864-8774 NC 437714 R. W. SANDERS, VICE PRESIDENT USDA #3787 http://Vv-microbac.ccm E-Mail: rsanders@niicrobac.com CHEMISTRY WATER • AIR • : MICROBIOLOGY • FOOD SAFETY - CONSUMER PRODUCTS WASTES - FOOD • PHARMACEUTICALS - NUTRACEUTICALS CERTIFICATE OF ANALYSIS Allen, Inc. Date Reported: 11/19/2009 Ms. Kathryn Yeager - _ Date Received: 1122009 Post Office Box 250 Order Number: 0911-00639 Siloam Springs, AR 72761 Invoice No.: 69452 Customer#: A004 Sample Date: 11/22009 Permit NC TURKEY PLANT Sample Time: 0:00 Sampler.r: Miller Subject: MAVell samples-3/Yearly SNIP Test Method Result Date Time Tech CHLORIDE SM 4500 a C 21.2 m9/1- 11/3/2DO9 16:56 ARS COD SM 5220 D 105 mg/L 11/3/20D9 10:47 ENC CONDUCTIVITY SM 2510 0 276 umhos/on 11/3/2009 11:45 DCR NITROGEN, NITRATE SM 4500 NO3 E <0.50 mg/L 11/3/2009 16:56 ARS PH, FIELD FIELD 3.97 sm. 11/2/20D9 13:20 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 135 mg/L II/9/20D9 10:00 ARS SULFATE SM 15m 426 C 51.5 mg/L 11/3/2009 16:56 ARS ...TEMPERATURE FIELD 19.9 deg.,C 11/2/2009 13:20 RDM TOTAL ORGANIC CARBON SM 5310B 8.5 mg/L 11/9/2009 0:DO ECI WATER LEVEL FIELD 10.11 feet il/2/2009 13:20 RDM ON M/W R-8 CHLORIDE SM 4500 CI C 24.3 mg/L 11/3/2009 16:56 ARS COD SM 5220 D 22.6 m9/L 11/9/2009 9:00 ENC CONDUCTIVITY SM 2510 B 434 umhos/nn 11/3/2009 11:45 DCR NITROGEN, NITRATE SM 4500 NO3 E 73.0 mg/L 11/3/2009 16:56 ARS pH, FIELD FIELD 5.76 s.u. 11/I/2009 13:07 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 226 mg/L 11/9/2009 10:00 ARS SULFATE SM 15W 426 C 15.4 mg/L 11/3/2009 16:56 ARS TEMPERATURE FIELD 16.9 deg., C, 11/2/2009 13:07 RDM TOTAL ORGANIC CARBON SM 53108 2.3 mg/L 11/9/2009 0:00 ECI WATER LEVEL FIELD 11.10 feet 11/2/2009 13:07 RDM LAB CODES: MID =None Detected N/F=None Found <=Less than >=Greater Wen Est.=Etimated Tte6aO stl omv4dwmtllonmdaeal m aa5 m0 Wv MEMBER amaRanYt'94ma��4 TCanmM me sanpe(s) arW/[etaN 6 imeeel upon tk mmn� maz a s me m na �rPmema..mnr a m Dart ra aameiml m me P�c�.Am�a.,mm acpwai Aua eia mcaamn. USDA£PANm91 Tati9 faoJSanQatlon UrsWW9 OimYmlvd Ruetiobglml Naryae:aN �rt6 � p Microbac Laboratories, Inc. Page 3of3 FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. TAYETTEVILLE,NC 28306 NC#ll (910) 864-1920 FAX (910) 864-8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA #3787 http://�.microbaccom E-Maih rsanders@microbac.com ATRSRWSRESIO EAI ORETSRUICHEMISTRY • WASTES PHAEUICAL- NUT4CECALS CERTIFICATE OF ANALYSIS Allens, Inc. Date Reported: 11/192009 Ms. Kathryn Yeager Date Received: 1122009 . Post Office Box 250 Order Number: 0911-00639 Siloam Springs, AR 72761 Invoice No.: 69452 • Customer#: A004 Date: 1122009 PennSample NC TURKEY PLANT Sample Time: 0:00 Sampler: Samplerr:: Miller _ Subject: M/Well samples-3/Yearly SJIP Test MetbodResult Date Time Tech RESPECTFULLYSUBMTITED: IIG_ Y/ _ t0 mJann. MICROBAC LABORATORIES, INC. 77=kyvufaryawbwi=a. We tmilejvurfeedbackon our level oftervice toyou. Please conlactthe Laboratory Director, Ron Smtden al 910864d920, Roberl Morgan. COO, alrmorgan&nlcrobaccom or Trevor Sayre, CEO, at tboyce e2tcrobaccom with ony commenu orsuggmfiow. LAB CODES: NID=None Detected NW=None Foaod <=L=ffi. >=Dmaterthaa Est=Estimated �oav mmafu Pe MEM13lR mmaitret'scramm�aremlwhNro-mwnro.aA•atk4g oramvmm��.�uuiaw�mna�rmm me amm.y. IAM£➢PNId+11T Jvq RM Sy�btpn fot5,tl[vy tlmblvtl MoatloYglmlM�dM REnvtl� GW-59A CON PLIANCP REPORT FORM Permit # W A 000 y-268 (Submit one eads monitoring period with G;V--59 forms.) 1 Enter date monitoring results were due. (I 3i'O91 Will this monitoring report (GW-59 and GW-59A) YES be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES IF the answer to question I or 2 is "YES', list in the space provided belowthe well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? Ifthe annver is "Yes", contact the Regional Officefor guidance. 4 Are any monitored constituents equal to or above the established standards? YES O If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? - If the answer to question 5 is "NO" skip to section 8. If the answer to question 5 is "YES'; list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES'; a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMED/ATELYFOR GUIDANCE. If the answer is "NO" monitoring wells may be improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? - If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines. andforpenalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with G W-59 forms for required wells to the address provided at the tap of the current G W-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. c�yl Cq �V %,2//c l0 ( / Signature of Pe ittee r Authorized Agent) Date G1V-59A 12/8/2003 Y `NO ,,, AI ]]IOR16] SIA.00 I] 9gV S6n Quality Vegetables August 31, 2009 Department of Environment & Natural Resources Water Quality Division, Groundwater Section 1636 Mail Service Center Raleigh, NC 27699-1636 919-733-3221 RE: Groundwater Quality Monitoring Report Allens, Inc. — Turkey, NC Facility Permit # WQ0004268 REC S E P 14 20J9 DEAR-FAYMEVUEREG!Mt ORIGE SEp _ � 2009 iniormarion PTocessln9 Vnii ')wQIB0G Enclosed you will find the completed Groundwater Monitoring Report forms GW59 and GW59A and the laboratory report for Allens, Inc. - Turkey, North Carolina facility for samples that were collected in July 2009. The monitoring wells are located around an existing irrigation system (designated as MW-1, etc.) and a planned but not yet used irrigation system (designated as MW-RI, etc.). A new permit was issued to the facility in April 2009. The former permit listed follow-up actions for Total Organic Carbon if the analytical results were greater than 10 mg/l. Other than this parameter, no other limits or parameters with follow-up actions were indicated. The new permit includes limitations for pH, chloride, sulfate, etc. This is the first samples collected under the new permit and several issues with the limitations are noted. Every monitoring well has a pH level below the acceptable range. Consistent with the direction provided by NCDENR during permit drafting, Allens will prepare and request a modification based on regionallbackground pH levels. MW-1, located near Field A (an existing irrigation field), also has exceedances of the standard for nitrate, total dissolved solids, and the sulfate. Reviewing historical data for this well, Allens notes that the depth to groundwater has changed significantly since 2008 versus historical levels and the nitrate levels are higher than historical levels in the last three monitoring events. In contrast, a review of nitrogen loading levels on Field A has shown similar nitrogen loading levels for the last few years. Chloride, a parameter closely tied to vegetable processing wastewater, has variable levels but it is not displaying a clear increasing trend. Allens was also unable to locate groundwater monitoring well elevation information so thet can determine the groundwater flow direction, particularly with the differences in depth to groundwater seen in MW-I. Therefore, the following actions will be taken: o A survey will be conducted of the existing wells when the Rowan Road wells are surveyed so that Aliens can determine groundwater elevation. o Consideration will be given to installing a new monitoring well depending upon the groundwater flow direction. o Further evaluation on MW-1 will be conducted and reported to NCDENR. If you have,any questions or require any additional information, please contact Laura Mushinski by phone at 479-228-0102 or by email at Imushinski@alIens.com.- Sincerely, Martin Griess Plant Manager Aliens, Inc.. CC: Reid Wells, Aliens — Turkey Kathryn Yeager, Aliens File Enclosures t']LUEMli�uiGWPL`\���RU•O�JJJ3COl\`IYi TER QUALITY MONITORING: E REPORT FORM Name: Aliens,Inc.-Turkey Name (if different): Address: 5900 Turkey Highway act Person: Martin Griess Location/Site Name: NC 28393-9703 county Sampson Telep hone#: 910-596-0028 No, of wells to be sampled:. :RMIT Number: Expiration Date: July :31. GU'I'I in -Discharge WQ0004268 ulc )DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: -L ID NUMBER (from Permit): MW 1 Date sample collected: 7/6/2009 FIELD ANALYSES: WAS I Depth: ft. Well Diameter: in. pH 3.85 units "-.�-21 4 °_C DRY at th to Water Level: 21.10 ft, below measuring point Screened Interval: ft, to ft. {Temp Spec. Cond. ° ° �.• p [/Ilum�/(limos time of samplin suring Point Is ft. above land surface Relative M.P. Elevation: ft. Odor (+r check Ime of water pumped/bailed before sampling: 10+ gallons Appearance/ V `t lii here: 1 les for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO n, _ {ORATORY INFORMATION __Inrn ttVlCCE ! • sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories C"TIZ ion N6.LI C3k,T6663771z tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 15.1 mg/I Nitrite (NCz) as N mg/I Pb - Lead mg/l Coliform: MF Fecal /100ml Nitrate (NO3) as N 21.8 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P ni (Note: Use MPN method for highly turbid samples( Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 945mg/l AI -Aluminum mg/l PH (when analyzed) units Be - Barium mg/1 TOC 5.6 mgA Ca - Calcium ni -Chloride 137 mg q� gg �-gg•cadmium Eg.ds• 1E mg/l Arsenic mg%/ E'�1pria rli1 Total mg/I Grease and Oils mgA SEP _ 9 ZOOSCu-copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/l (Specify test and method #. ATTACH LAB REPORT.) Sulfate 291 .mg�r/brmation PrOcessireNnMercury mg/I Report Attached? ElYes (1) ElNo (0) Specific Conductance 2570 pMhos DWQ/gOG K- Potassium mg/l VOC , method # Total Ammonia mg/I Mg - Magnesium mg/1-, method # (Ammonia Nitrogen; NHsas N: Ammonia Nitrogen, Total) Mn- Manganese mgA ,method# TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Martin Griess, Plant Manager 1�� `c�' 3( / 0 free (or Authorized Apent) Name and Title- Please print or Npe Signature of Pertnitlee or Authorized Agent) (D: GW-59 Rev. 112007 Y.11V&WI wilalt[ar0A9:i:1aits] 0IN 0 TER QUALITY MONITORING: TY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: July 31, 2U11 Name: Aliens, Inc. -Turkey Non -Discharge WQ0004268 . UIC Name (if different): NPOES Other Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ,y (slam) NC 28393-9703 County Sampson ❑ Lagoon ❑ Remediation: Infiltration Gallery (OW IMare) (zip) © Spray Field ❑ Remediation: act Person: Martin Griess Telephone#: 910-596-0028 Location/Site Name: No. of wells to be sampled: 12 ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: WELL ID NUMBER (from Permit): MW 2 Well Depth: ft. Depth to Water Level: 9.1 ft. below measuring point Measuring Point is ft. above land surface Volume of water pumped/bailed before sampling: Samples for metals were collected unfiltered: ❑YES Date sample collected: 7/6/2009 Well Diameter: — ft. Screened Interval: _ft. to _ft. Relative M.P. Elevation: ft. 10+ gallons ❑ NO and field acidified: DYES ❑ NO FIELD ANALYSES: pH 4.55 units Spec. Cond. Odor Appearance Temp. 21.5 aC pMhos WAS DRY at time of sampling, check here: ❑ LABORATORY INFORMATION Date sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories Certification No. NC#11, NC#37712 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10.0.mg/I Nitrite (NO,) as N - mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N .13 mgA Zn -Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I Wale: Use MPN method for hig* turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 225 mg/I AI -Aluminum _ mg/I pH (when analyzed) units Ba - Badum mg/I TOC 2.7 mg/I Ca - Calcium mg/I Chloride 118 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I —, - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) ' Phenol mg/I �Cu s ll I I dCogr'r^� mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate <5.0 mg/I SEP Ng - Me curt'" mg/I ReportAttached? ❑ Yes (1) ❑ No (0) Specific Conductance 461 µMhos — K- 049lum mg/I VOC , method # Total Ammonia mg/I information FML9 - Magnesium mg/l , method # (Ammonia Nitrogetr, NHsas N; Ammonia Nitrogen, Total) Ce DtA/Q+rGFa'R6abWe mgA ,method# TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VUCs: mg/L VUc tcemovarra Martin Griess, Plant Manager %� ,'* a,— ����� Perminee(or Authorized Agent) Name and Title -Please print or type Signature of Permin or Authorized Agent) r (Date) GW-59 Rev. 112007 WUN11I hUKM UN -R QUALITY MONITORING: REPORT FORM Name: Aliens,Inc.-Turkey Name (if different): Address: 5900 Turkey Highway :y (stfPeO NC 28393-9703 County Sampson act Person: Martin Griess Location/Site Name: Telep hone#: 910-596-0028 No. of wells to be sampled: 12 LID NUMBER (from Permit): MW 3 Date sample collected: 7/6/2009 Depth: ft. Well Diameter: —in. h to Water Level: 7.2 ft. below measuring point Screened Interval: _ft. to —ft. wring Point is ft. above land surface Relative M.P. Elevation: ft. Tie of water pumped/bailed before sampling: 10+ gallons sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories AMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 14.6 mg/I Nitrite (NO.) as N mg/I Coliform: MF Fecal /loom[ Nitrate (NO3) as N <0,1 mg/1 Coliform: MF Total /looml Phosphorus: Total as P mg/I (Note:. Use MPN method for highly tutlid samples) Orthophosphate mg/I Dissolved Solids: Total 289 mg/I Al -Aluminum Mgt[ pH (when analyzed) units Be - Barium mg/I TOC .7 mg/I Ca - Calcium mg/I Chloride 58.8 mgll Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/l Grease and Oils Mgt[ Cu - Copper mg/I Phenol mg/I Rep'9gj Iran y-,0.0..•FI?._tVla�i{iFP-% mg/I Sulfate 58.1 mg/l mg/l Specific Conductance 380 µMhos SEp K- otassium-,Z—Mgt] mg/I Inforrrlatior"Ar6fy]_a ��'� (Ammoniaal Nitrogen;Hsaas N;Ammonla Nitrogen, Total) mg/I TKN as N mg/I 01/t�Q16��tt 1NI61(itit mg/I iRM1T Number: Expiration Date: July C'I, Zu -I -I in -Discharge WQ0004268 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑K Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other FIELD ANALYSES: pH 5.61 units Spec. Cond. Odor Appearance Pb - Lead Zn - Zinc Temp. 21.7 eC DRY at µMhos time of sampling, check here:❑ Certification No. NC#11, NC#3771z mgA mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GCIMS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L vuc Kerr is Martin Griess, Plant. Manager Permit ee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 112007 Viva t?IrMK VINLI TER QUALITY MONITORING: E REPORT FORM Name: Aliens, Inc. - Turkey Name (if different): Address: 5900 Turkey Highway y (s"Pe9 NC 28393-9703 County Sampson act Person: Martin Griess Location/Site Name: Telephone#: 910-596-0028 No, of wells to be sampled: 12 LID NUMBER (from Permit): MW 4 Date sample collected: 7/6109 Depth: ft. Well Diameter: — in. h to Water Level: 9.10 ft. below measuring point Screened Interval: _ft. to —ft. ng Point is ft. above land surface of water pumped/bailed before sampling: 10+ Number: Expiration Date: harge WQ0004268 UIC_ Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heal Pump ❑ Other: FIELD ANALYSES: pH 3.67 units Spec. Cord. Relative M.P. Elevation: ft. Odor Appearance sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories %METERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10.0 mg/I Nitdte (NOz) as N mg/I Pb - Lead Collform: MF Fecal /10oml Coliform: MF Total /100ml (Note: Use MPN melhod for highly turbid samples) Dissolved Solids: Total 87.5 mg/I pH (when analyzed) units TOC 1.4 mg/I Chloride 34.3 mg/I Arsenic mg/I Grease and Oils mg/I Nitrate (NO3) as N 9.31 mg/I Phosphorus: Total as P mg/I Orthophosphate mg/l AI - Aluminum mg/I Be - Barium mg/I Ca - Calcium _mg/l Cd - Cadmium mg/I roomium: Total mg/I 7J{�gpper mg/l Phenol ri ll — 9 20% - Iron Sulfate Mercury <5.0 n'61prr�aG0n p mg" Specific Conductance 176 µMhos Q(.y- r0cessln K-Potassium mgA Total Ammonia mg/I Q1B 8f�� Mg-T7f�gnesium mg/l (Ammonia Nitrogen; NHsas N; Ammonla Nitrogen, Total) Mn - Manganese mgA TKN as N _ mg/l Ni - Nickel mg/I Zn - Zinc Temp. 19.7 eC DRY at pMhos time of Certification No. NC#11, NC#3771,f mgll mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC . method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mgfL VUU Kemovill Martin Griess, Plant Manager 77 " CU. t Permlttee (or Authodud Agent) Name and Title - Please print or type Signature of Permihee for GW-59 Rev. 1/2007 ouarvui rvmrvi QUALITY MONITORING: PORT FORM Name: Aliens, Inc. -Turkey Name (if different): Address: 5900 Turkey Highway y (slaeo NC 28393-9703 County Sampson act Person: Martin Griess Location/Site Name: L ID NUMBER (from Permit): MW R-1 Depth: ft. i to Water Level: 7.4 ft. below measuring point wring Point is ft. above land surface ne of water pumped/bailed before sampling: 10+ Telephone#: 910-596-0028 No. of wells to be sampled: 12 Date sample collected: 7/6/09 Well Diameter: _in. Screened Interval: _ft. to _ft. Relative M.P. Elevation: ft. RMIT Number: Expiration Date: July 31, 2011 n-Discharge xx WQ0004268 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 3.63 units Spec. Cord. Odor Appearance _ Temp. 22.6 oC DRY at µMhos time of UKM V MnVy sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories Certification No. NC#11, NC#37712 AMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 242 mg/I Nitrite (NO,) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N 1.47 mg" Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/1 (Note: Use NlPN method for highly turbid samples) Orthophosphate mg/l Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 81.4 mg/I At - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 6.3 mg/I Ca - Calcium mg/I Chloride 29.4 mg/I Cd- Cadmium mg/l Arsenic mg/I ."3 P.Chromium: Total mg/I Grease and Oils mg/I 4' �' �(m. Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/l S�p `� �eh�"ir ) mg/I (Specify test and method #. ATTACH LAB REPORT.) El Yes El No Sulfate 53.7 mg/I [I ercu � m9/1 Report Attached? (1) (0) Specific Conductance 133 µMhos / .r,formaryo0� K- t4um mg/I VOC ,method# Total Ammonia mg/l DIZ.plfitg=g�Qne'slium JiN�rri»IIU1art�j'{ebe mg/l ,method # (Ammonia Nitrogen; NHras Ammonia Nitration, Total) N; mg/I method TKN as N _ mg/I Ni - Nickel _ mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent I otal vws_ mgn- onuem I omt V UUb. Martin Griess, Plant Manager Permiftee for Authorized Anent) Name and Title- Please print or type GW-59 Rev. 1/2007 A b1a6L•In�i9:lullL`\'awl IIPIgZ1J�:i9C1Y1 =R QUALITY MONITORING: REPORT FORM Name: Aliens, Inc. - Name (if different): Address: 5900 Turkey Highway y S'reen NC 28393-9703 County Sampson act Person: Martin Griess Telephone#: 910-596-0028 Location/Site Name: No. of wells to be sampled: 12 LID NUMBER (from Permit): MW R-2 Depth: ft. h to Water Level: 6.5 ft. below measuring point Date sample collected: 7/6/09 Well Diameter: in. Screened Interval: _ft. to _ft. curing Point is ft. above land surface Relative M.P. Elevation: __ft. T)e of water pumped/bailed before sampling: 10+ gallons oles for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ N( Number: Expiration Date: July 31, 2011 harge XX W00004268 UIC Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery KI Spray Field ❑ Remedlation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: If WELL FIELD ANALYSES: WAS pH 3.29 units Temp. 21.3 eC DRY at Spec. Cond. µMhos time sampling, Odor check Appearance here: ❑ sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories 4METERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 44.5 mg/l Nitrite (NO2) as N mg/I Pb - Lead Coliform: MF Fecal /loom[ Coliform: MF Total /loom[ (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 183 mg/I pH (when analyzed) units TOC 7.4 mg/I Chloride 13.2 ma/1 Arsenic Nitrate (NO3) as N 6.43 mg/I Zn -Zinc Phosphorus: Total as P Certification No. NC#11, NC#3771Z mg/I mg/I Orthophosphate mgA Other (Specify Compounds and Concentration Units): AI - Aluminum mgA Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Grease and Oils mg/l REC Cau - Copper mg/I Phenol mg/I '"" 9 VC —Iron mg/I Sulfate 108 mg/I SEP , 9 HgnnrtMlercury mg/I Specific Conductance 379 pMhos K = P�assium Inf"nation mg/I TolalAmmonia mg/I PrNdn vlagnesium mg/I (Ammonia Nitrogen; NHsas N;Ammania Nitrogen, Total) DVv (3 rn Q>&rtR�oGgqflfyse MaT mg/l TKN as N mg/I Ni - Nickel mg/I ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes(1) ❑ No method # method # method # method # For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Martin Griess, Plant Manager Permittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 1/2007 SUtlMI I UNLr ROUNDWATER QUALITY MONITORING: oMPLIANCE REPORT FORM Name: Allens, Inc. -Turkey Name (if different): Address: 5900 Turkey Highway ;y iShee1) NC 28393-9703 County Sampson act Person: Martin Griess Location/Site Name: Telephone#: 910-596-0026 No, of wells to be sampled: 12 L ID NUMBER (from Permit): MW R-3 Dale sample collected: 716/09 Depth: ft. Well Diameter: _in. n to Water Level: 9.8 ft. below measuring point Screened Interval: _ft. to _ft. ;wring Point is ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 10+ gallons RMIT Number: Expiration Date: July 31, GU -I "I n-Discharge xx W00004268 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. FIELD ANALYSES pH 3.12 units Temp. 20.6 eC Spec. Cord. µMhos Odor Appearance at of u u ISUKAIURr INCUM grn'N Date sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories Certification No. NC#11, NC#377V PARAMETERS NOTE: Values should reflect" dissolved and colloidal concentrations. COD 141 mg/l Nitrite (NO,) as N mg/I Pb - Lead mg/I Coliform: MF Fecal /100ml Nitrate INC,) as N <0,1 mg/l Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 38.1 mg/l At -Aluminum mg/l pH (when analyzed) units Be - Barium mg/I TOC 1.4 mg/I Ca - Calcium mg/l Chloride 6.9 mg/l Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/l Grease and Oils mg/I Cu- Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mgll (Specify test and method #. ATTACH LAB REPORT.) ❑ Sulfate 13.5 mg/I c. yA-��Iercury mg/l Report Attached? ❑ Yes (1) No (0) Specific Conductance 122 µMhos s,CPj(6 §f A'As,grdsmg/I VOC , method # Total Ammonia mg/I C Mg SM� /gns ui rn' '` Info mg/I , method # (Ammonia Nitrogen; NHsas N; Ammonia Nitrogen, Total( frnat- A n - MaFf4ese mg/I method # TKN as N mg/1 Dyy4ices�)� Nickel mg/I ,method # TM.l%Mr.w ma/L Effluent Total VOCs: - mg/L VOC Removal% Martin Griess, Plant Manager `11K C'✓J�- `- Permiflee (or Authorized Agent) Name and Title - Please print or type signature of Pear iftee for Auth GW-59 Rev, 112007 bubml l ruminn uiN 7 w 1 Lm rrrnm QUALITY MONITORING: PORT FORM Name: Aliens, Inc. - Turkey Name (if different): Address: 5900 Turkey Highway q f51ao) NC 28393-9703 County Sampson Location/Site Person: Martin Griess Telephone#: 910-596-0028 No. of wells to be sampled: 12 L ID NUMBER (from Permit): Depth: ft. to Water Level: 9.3 ft. below measuring point Ting Point is ft. above land surface Date sample collected: 7/6109 Well Diameter: _in. Screened Interval: _ft. to _ft. Relative M.P. Elevation: ft. e of water pumped/bailed before sampling: 10+ gallons Number: Expiration Date: .harge xx WQ0004268 UIC_ Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. FIELD ANALYSES: pH 2.85 units Spec. Cond. Odor Appearance sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories I METERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 114 mg/I Nitrite (NO,) as N mg/1 Pb - Lead Coliform: MF Fecal /100ml Nitrate (NO,) as N .22 mgA Zn - Zinc Colifonn: MF Total /100m1 (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 130 mg/I pH (when analyzed) _ units TOC 1.2 mg/i Chloride- 7.4 mg/l Arsenic mg/1 Grease and Oils Phenol Sulfate Temp. 22 eC µMhos Certification No. NC#11, NC#3771z mg/I mg/I Phosphorus: Total as P mgtl Orthophosphate mg/I Other (Specify Compounds and Concentration Units): AI - Aluminum mg/I -Be - Barium mg/I Ca - Calcium mg/I Cd- Cadmium mg/1 Chromium: Total mg/I ll 4 Cu - Copper mg/I 4 CCc£_cz,j.pR- Icon mg/1 Hg-M mg/l Specific Conductance fnfo 294 pMhos : ` sium mg/I Total Ammonia mg/1 oration c, Mg - Magnesium mg/I to (Ammonia Nitrogen; NHsas N; Ammonia Nitrogen, Total) oIvpor _n�(�S g ['Se mg/I TKN as N mg/I W' ((f�``�OO' Ni - Nickel mg/I ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC ,method# method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L Voc Removal% Martin Griess, Plant Manager PermiHee (or Authorized Anent) Name and Title - Please print or type GW-59 Rev. 1/2007 at of ICI Lei `W➢aallgpARV-M[R .Il`191 :R QUALITY MONITORING: REPORT FORM Name: Allens, Inc. -Turkey Name (if different): Address: 5900 Turkey Highway y ISlreep NC 28393-9703 county Sampson act Person: Martin Griess Location/Site Name: Telephone#: 910-596-0028 No. of wells to be sampled: 12 !RMIT Number: Expiration Date: Jury a-1, ZVI -1 m-Discharge xx W00004268 UIC IDES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery 91 Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other LID NUMBER (from Permit): MW R-5 Date sample collected: 7/6/09 FIELD ANALYSES: WAS Depth: ft. Well Diameter: pH 5.2 units Temp. 19.8 eC DRY at h to Water Level: 13.6 ft. below measuring point tin. Screened Interval: _ft. to _ft. Spec. Cond. µ Mhos time of sampling, Wring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check re of water pumped/bailed before sampling: 10+ gallons Appearance here: ❑ )sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10.0 mg/I Nitrite (NO2) as N mg/I Colifonn: MF Fecal /100ml Nitrate (NO3) as N 0.10 mg/I Coliform: MF Total /100ml Phosphorus: Total as P mgll (Note: Use MPN method for highly turtld samples) Orthophosphate mg/1 Dissolved Solids: Total 85.6mgA AI - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 0.7 mgll Ca - Calcium mg/I Chloride 12.2 m ;-- Cd - Cadmium mg/I Arsenic Total mg/IitC % mg/l Grease and Oils mg)LI,C ,�',y-Chromium: ° SF +,� D - Copper mg/l Phenol mg/I' Fe - Iron - z009 ing/I Sulfate 9'?� rff qrs) Hg - Mercury mg/I Specific Conductance 116 µMS � OOGsI�9 mg/I Total Ammonia moll j gK-Potassium IQ((g-Magnesium mgA (Ammonia Nitrogen; N113as N; Ammonia Nitrogen, Total) Mn -Manganese mg/I TKN as N mg/I Ni - Nickel mg/1 Pb - Lead Zn - Zinc Certification No. NC#11, NC#3771/ mg/I mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes(1) ❑ No VOC ,method# method # method # method # For Remedlatlon Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%e Martin Griess, Plant Manager Permitlee (or Authorized Agent) Name and Title- Please print or Npe Signature of Permitlee (or Authorzed Agent) GW-59 Rev. 112007 O VOIYII I NDWATER QUALITY MONITORING: LIANCE REPORT FORM Name: Allens, Inc. -Turkey Name (if different): Address: 5900 Turkey Highway ty (s"a`° NC 28393-9703 County Sampson ict Person: Martin Griess Telephone#: 910-596-0028 Location/Site Name: No. of wells to be sampled: 12 LID NUMBER (from Permit): MW R-6 Date sample collected: 7/6109 Depth: ft. Well Diameter. _In. i to Water Level: 8.4 ft. below measuring point Screened Interval: _ft. to _ft. curing Point is ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 10+gallons :RMIT Number: Expiration Date: Jury 6 1. tun In -Discharge xx WQ0004268 UIC 'DES Other 'PE,OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 3.53 units Spec. Cond. _ Odor Appearance Temp. 22.1 eC DRY at time of sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories Certification No. NC#11, NC#3771Z '.AMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 67.2 mg/I Nitrite (NO2) as N mg/l Pb - Lead mg/I Coliform: MF Fecal /100m1 Nitrate (NO3) as N 7.39 mg/I Zn -Zinc mg/I Colifonn: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPN method for highly lulbld samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 163 mgll At -Aluminum mg/I pH (when analyzed) units Be - Barium mgA TOC 6.4 mgll Ca - Calcium mg/l Chloride 5.4 mg11 Cd- Cadmium mgA Arsenic mg/l,4'� Chromium: Total mg/I Grease and Oils mg/I v kV c R^^ Gu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mgll '^ �FelIto� Sf P Me(ctfry mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 45.7 mg/1 mg/I Report Attached? ❑ Yes (1) El No (0) SpecificTotal pMh6V 258 orrnellon VOC method # Ammonia mg/I aDW ro M,*r ��Magnesium �� mgll ,method # mm (Ammonia Nitrogen; NHras N; Ammonia Nitrogen, Tots]) - M Ygdnese mg/I , method # TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Martin Griess, Plant Manager Permittee (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. 112007 u ouurvu i vunrvi ury . ru-wv rr ran -R QUALITY MONITORING: REPORT FORM Name: Aliens, Inc. -Turkey Name (if different): Address: 5900 Turkey Highway iy (street) NC 28393-9703 County Sampson act Person: Martin Griess Location/Site Name: Telephone#: 910-596-0028 No. of wells to be sampled: 12 L ID NUMBER (from Permit): MW R-7 Date sample collected: 7/6/09 Depth: ft. Well Diameter. _in. i to Water Level: 8.8 ft. below measuring point Screened Interval: _ft. to _ft. luring Point is ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 10+ gallons :RMIT Number: Expiration Date: July 3I, ZU-1 I in -Discharge xx WQ0004268 UIC 'DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ❑1� Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 3.55 units Spec. Cord. _ Odor Appearance sample analyzed: see attached lab sheets Laboratory Name: Microbiac Laboratories AMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COO 49.6 mg/I Nitrite (NO2) as N mg/I Pb - Lead Coliform: MF Fecal /100m1 Nitrate (NO3) as N <0,1 mgll Zn -Zinc Coliform: MF Total /100ml Phosphorus: Total as P mg/l If WELL Temp. 27.7 eC DRY at ffMhos time of Certification No. NC#11, NC#3771z mg/I mg/I (Nate: Use MPN method for highly turbid samples) Orthophosphate mg/l Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 86.3 mg/1 At - Aluminum mg/I pH (when analyzed) units Be - Barium mgll TOC 7.0 mg/I Ca - Calcium mg/I •Chloride 27.0 mg/I Cd- Cadmium mg/1 Arsenic mg/I p Chromium: Total mg/I Grease and Oils mg/I {,,i 9 C Copper X i``�Iron mgfl ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/1 mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 18.7 ^^A tS'6/j " � 20{�1}�fjq Mercury mg/l Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 134 µmff3ishation p K= PotasslUnl mg/I VOC , method # Total Ammonia mg/I OI.1/0' c_s�'1gY I�ia nestum O0 �/ mg/I , method # (Ammonia Nitrogen; NNses N: Ammonia Nitrogen, Total) Mn - Ma ganese _ mg/l ,method # TKN as N mg/I Ni - Nickel mg/l , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent l otal VUCs: mg/L vuu nemovatio Martin Griess, Plant Manager Permittee (orAuthadzed Agent) Name and Title - Please Print or type GW-59 Rev. 1/2007 IN SUBMIT FORM ON YE1l OW PAPER ONLY TER QUALITY MONITORING: E REPORT FORM Name: Aliens,Inc.-Turkey Name (if different): Address: 5900 Turkey Highway I [o] County Sampson act Person: Martin Griess Telephone#: 910-596-0028 Location/Site Name: No. of wells to be sampled:, LID NUMBER (from Permit): MW R-8 Depth: ft. h to Water Level: 11.1 ft. below measuring point ;uring Point is ft. above land surface me of water pumped/bailed before sampling: 10+ Dale sample collected: 7/6/09 Well Diameter. _in. Screened interval: _ft. to _ft. Relative M.P. Elevation: ft. sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories AMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10.0 mg/1 Nitrite (NO,) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N 22.5 mg/I Coliform: MF Total /100ml Phosphorus: Total as P mg/I (Note: Use MPNmethod for highly turbid samples) Orthophosphate mg/l Dissolved Solids: Total 275 mg/I At -Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 1.4 mgn Ca - Calcium mg/I Chloride 29•4 mg/I S1` Cd- Cadmium mg/I Arsenic mg/I L I:A oym�m: Total mg/I Grease and Oils mg/I S'EP A vt%�u -ry:- oA,per mgll Phenol m /l 11.6 9 Fe - Iron OH9 mg/I Sulfate mgllermation -Mercury p mg/I Specific Conductance 443 µMhos D:,�(/�O 881 - Potassium mg/I Total Ammonia mg/I Mg - Magnesium mg/I (Ammonia Nitrogen; NHoas N; Ammonia Nitration, Total) Mn - Manganese mg/I TKN as N mg/I Ni - Nickel mg/I Number: Expiration Date: harge xx W00004268 UIC_ -DES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other. FIELD ANALYSES: vvAs pH 3.10 units Temp. 22.6 aC DRY at SpMhos time of Spec. Cond. sampling, Odor check Appearance here: ❑ Pb - Lead Zn - Zinc Certification No. NC#11, NC#3771z mg/I mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes(1) ❑ No VOC , method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Martin Griess, Plant Manager Permibee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 1/2007 Signature rI GW-59A COMPLIANCE REPORT FORM Permit # WQ0004268 (Submit one each monitoring period with GW-59 forms.) 9 Enter date monitoring results were due. ( B-31-09 1 Will this monitoring report (GW-59 and GW-59A) be submitted after YES NO the established due date? 2 Was any required information missing on the GW-59 report form? YES NO IF the answer to question 1 or 2 is "YES", list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information, 3 Are any of the monitor wells in need or repair or maintenance (damage casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answeris "Yes", contact the Regional Office forguidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is 'YES" list the affected wells individually with constituent(s) and concentrations(s) exceeding standards in the space provided below: All monitoring wells for pH. MW-1 Nitrate, Total Dissolved Solids, Sulfate. 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituent(s) YES NO in the same well(s) in the past two years? Constituents were not listed on the previous permit. If the answer to question 5 is "NO", skip to section 8. ' If the answer to question 5 is "YES" list in the space provided below, each well with constituents) exceeding standards, concentration(s) reported and sample collection date for each occurrence (for the last two years). 8 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE_ IMMEDIATELY FOR GUIDANCE. If the answer Is "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Istheperrnittee implementing previously approved actions required by the Division involving this groundwater quality YES NO problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines and/or Penalties. 8 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with the GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge. `' €3 ��/o Martin Griess, Plant Manager (Signature of Permiltee or Authorized Agent) Date GW-59A 12/8/2003 U Microbac Laboratories, Inc. ru_c I ut J FAYETTEVILLE DIVISION STATE CERT ID. 2592 HOPE MILLS ROAD FAYETTEVILLE, NC 28306 NC #11 (910) 864-1920 TAX (910) 864-8774 NC 07714 R. W. SANDERS, VICE PRESIDENT USDA #3787 http://%dw%v.niicrobac.com F--Ivlail:rsanders@n3-icrobac.com CER TIFICATE OF ANALYSIS Allens, Inc. Date Reported: 7/23/2009 Ms. Kathryn Yeager Date Received: 7/6/2009 Post Office Box 250 Order Number: 0907-001.08 Siloam Springs, AR 72761 Invoice No.: 66647 Customer #: A004 Sample Date: 7/6/2009 Permit No. NC TURKEY PLANT Sample Time: 0:00 Sampler: Miller Subject: M/Wellsamples -3/Yearly SMP Test alethad Result Date Time Tech CHLORIDE SM 4500 0 C 137 mg/L 7/7/2009 8:00 TDA COD SM 5220 D 15.1 mg/L 7/7/2009 11:00 ENC CONDUCTNITY SM 2510 B 2570 umhos/an 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 21.8 mg/L 7/10/2009 8:10 ARS �pH HELD 3.85 sm. 7/6/2009 10:05 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 945 mg/1- 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 291 mg/L 7/6/2009 15:35 DCR TEMPERATURE FIELD 21.4 deg., C 7/6/2009 10:05 RDM TOTAL ORGANIC CARBON SM 5310B 5.6 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 21.10 feet 7/6/2009 10:05 RDM CHLORIDE SM 4500 CI C 118 mg/L 7/7/2009 8:00 TDA COD SM 5220 D <10.0 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 8 461 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 0.13 mg/L 7/8/2009 8:05 ARS PH FIELD 4.55 s.u. 7/6/2009 10:26 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 225 mg/1- 7/7/2009 13:30 ENC SULFATE SM 15th 426 C <5.0 mg/L 7/6/2009 15:35 DCR TEMPERATURE FIELD 21.5 deg., C 7/6/2009 10:26 RDM TOTAL ORGANIC CARBON SM 5310B 2.7 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 9.1 feet 7/6/2009 10:26 RDM LAB CODES: NID=Nonc Dctcctcd Mr=No=Found <=Lcss than >-Grcaterthan Est.=Bslimatcd The data and o1Mr Infmmadon contaloed an this, and other accompanying daaments, represent only the sample(s) analyzed and is rendered upon the MEMBER tradition that It is not to be reprudua•d -holy or In part for advertising or other puryoses Wldmut Written appreyal hOM the laboratory. A USDA-EPA.M05UTating Food Sanitation Cansuldng Oremd Ml lml and Analyses and Research ® MicrobacLaboratories, Inc. Page 2of3 FAYETTEVILLE DIVISION STATE CERT ID. 2592 HOPE MILLS ROAD FAYETTEVILLE, NC 28306 NC AI I (910) 864-1920 FAX (910) 864-8774 NC 937714 R. W. SANDERS, VICE PRESIDENT USDA 43787 http://xvww.microbac.com E-Mail: isanders@tnicrobac.com WATER • AIR - WASTES • FOOD • PHARMACEUTICALS, NU I RAUEL) I WAL5 CERTIFICATE OF ANALYSIS Allens, Inc. Date Reported: 7/23/2009 Ms. Katliryn Yeager Date Received: 7/6/2009 Post Office Box 250 Order Number: 0907-00108 Siloam Springs, AR 72761 Invoice No.: 66647 Customer #: A004 Sample Date: 7/6/2009 Permit No. NC TURKEY PLANT Sample Time: 0:00 Sampler: Miller Subject: M/Wellsamples -3/Yearly SNIP Test rylethod Result Date Time Tech CHLORIDE SM 4500 0 C 58.0 mg/L 7/7/2009 8:00 TDA COD SM 5220 D 14.6 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 380 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 1500 NO3 E <0.1 mg/L 7/8/2099 8:05 ARS PH FIELD 5.61 s.u. 7/6/2009 10:45 ROM SOLIDS, TOTAL DISSOLVED SM 2510 C 289 mg/L 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 58.1 mg/L 7/6/2009 15:35 DCR TEMPERATURE FIELD 21.7 deg., C 7/6/2009 10:45 ROM TOTAL ORGANIC CARBON SM 53108 0.7 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 7.2 feet 7/6/2009 10:45 ROM _ 004hi�wl:#4 HE -, i.. y i, tl I�ir Oil 0- CHLORIDE SM 1500 Cl C 34.3 mg/L 7/7/2009 8:00 TDA COD SM 5220 D <10.0 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 176 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 9.31 mg/L 7/8/2009 8:05 ARS pH FIELD 3.67 sm. 7/6/2009 9:48 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 87.5 mg/L 7/7/2009 13:30 ENC SULFATE SM 150t 426 C <5.0 mg/L 7/6/2009 15:35 DCR TEMPERATURE FIELD 19.7 deg., C 7/6/2009 9:48 ROM TOTAL ORGANIC CARBON SM 5310B 1.4 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 9.10 feet 7/6/2009 9:48 ROM LAB CODES: N1D=None Detected N/F=None Found <=Less Wan >=Grntcrthan Est.=Estimaled The data and other Information contained on this, and other accom in domments, ra resentbnl the sample(s)anal ed and Is rendered upon the MEMBER pant 9 p Ya .l W condition that Ills not m be tepmduced wholly or In part for ativeNsing or other purposes rNNvut wdden approval from the labomlory. U5DA-EPA4JI05H Tesdng rood 5anilatloo Consulting Uemied and Mlpallologbl Analyses and Resean:n ® Microbac Laboratories, Inc. Page of FAYETTE-VILLE DIVISION STATE CERT ID. 2592 HOPE MILLS ROAD FAYETTEVILLE,NC 28306 NC411 (910) 864-1920 FAX (910) 864-8774 NC 437714 R. W. SANDERS, VICE PRESIDENT USDA'43787 http://u,%vw.microbac.com E-Mail: rsanders@microbaacom WATER CERTIFICATE OFANALYSIS Allens, Inc. Ms. Kathryn Yeager Post Office Box 250 Siloam Springs, AR 72761 Permit No. NC TURKEY PLANT Sampler: Miller Subject: M/Wellsamples -3/Yearly Date Reported: 7/230009 Date Received: 7/6/2009 OrderNumber: 0907-00108 Invoice No.: 66647 Customer #: A004 Sample Date: 7/6/2009 Sample Time: 0:00 SMP Test Method Result Daattee� Time Tech @ / RESPECTFULLY SUBMITTED: Y! . i]aR7.( RA& MICROBAC LABORATORIES, INC. TImnA you far your bnsaress. IYe inriye ym+rfeedback on onr level oJsernice roymt. Please contact Ilia Laboratory Director, Ron Sanders at 910-864-1920, Robert A.lorgon, COO, or nnorganQ+nterobaccom or Trovor Btuco, CEO, at Ibo)'te(aLnicroboc.eont with any connnents or snggastlons. LAB CODES: N/D=None Doweled N/F=None Found <—Lcssthan >=Grealerth:m Est.=Estimated The data and other Information ronrained on this, and other atoompanying documents, represent only the ornple(s) analyzed and Is rendered upon the condition that It L not to be reproduced wholly or In pan for adwtilshg or odrer purposes without written approval from the labem[pry. USDA-EPA-NIDSHTesbng Food5anilabbnC sultlng aemlret and Mlwblologial Analyses and peunuoh MicrobaC Laboratories, Inc. Page I of 3 FAYETTEVILLE DIVISION 2592.HOPE MILLS ROAD STATE CERT ID. FAYETTEVILLE, NC 28306 NC col 1 (910) 864-1920 FAX (910) 864-8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA 93787 http://wivw.microbac.com E-Mail: rsanders@microbac.com CERTIFICATE OF ANALYSIS Allens, Inc. Date Reported: 7/23/2009 Ms. Kathryn Yeager Date Received: 7/6/2009 Post Office Box 250 Order Number: 0907-00462 Siloam Springs, AR 72761 Invoice No.: 66649 Customer #: A004 Sample Date: 09 Permit No. NC TURKEY PLANT Sample Time: 0:00 0:00 Sampler: Miller Subject: M/Well samples - 3/Yearly SMP Test Method Result Date Time Tech 001 -:� .- -- -- - - CHLORIDE SM 4500 Cl C 29.4 mg/L 7/7/2009 8:00 TDA COD SM 5220 D 242 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 133 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 1.47 mg/L 7/8/2009 8:05 ARS ,pH FIELD 3.63 s.u. 7/6/2009 12:25 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 81.4 mg/L 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 53.7 mg/L 7/20/2009 10:45 ENC TEMPERATURE FIELD 22.6 deg., C 7/6/2009 12:25 RDM TOTAL ORGANIC CARBON SM 5310B 6.3 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 7.4 Peet 7/6/2009 12:25 RDM OD2— R 2 c - , 1 II ' CHLORIDE SM 4500 0 C 13.2 mg/L 7/7/2009 8:00 TDA COD SM 5220 D 44.5 ma/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 379 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 6.43 mg/L 7/8/2009 8:05 ARS pH FIELD 3.29 s.u. 7/6/2009 12:17 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 183 mg/L 7/7/2009 - 13:30 ENC SULFATE SM 15th 426 C 108 mg/L 7/20/2009 10:45 ENC TEMPERATURE FIELD 21.3 deg., C 7/6/2009 12:17 RDM TOTAL ORGANIC CARBON SM 5310B 7A mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 6.5 Peet 7/6/2009 12:17 RDM LAB CODES: N/D=None Detected N/F=None Found <=Loss than t,=Greater Wan Est.=Estimated The dab and other Information mntaned on this, and other aanmpznying domments, represent any the sampte(s) analyzed and B rendered upon the MEMBER condition that It is not to be reproduced wholly or In part for adveNsing or other purposes w"out written approval firm the laboratory, y 1150A-EPA-H105H Tx ttng Food sanitation consulting [heMal and Mxroblologiml matyses and Research ® Microbac Laboratories, Inc. Page 2of3 FAYETTEVILLE DIVISION STATE CERT ID. 2592 HOPE MILLS ROAD FAYETTEVILLE, NC 28306 NC 911 (910) 864-1920 FAX (910) 864-8774 NC 937714 R. W. SANDERS; VICE PRESIDENT USDA #3787 bttp://tivww.microbac.com E-Mail: rsanders@tnicrobac.com WATER - AIR • WASTES • FOOD • PHARMACEUTICALS • NUTRACEUTICALS CERTIFICATE OF ANALYSIS Allens, Inc. Date Reported: 7/23/2009 Ms. Kathryn Yeager Date Received: 7/6/2009 'Post Office Box 250 Order Number. 0907-00462 Siloam Springs, AR 72761 Invoice No.: 66649 Customer4: A004 Sample Date: 09 PermitNo. NC TURKEY PLANT Sample'Time: 0:00 0:00 Sampler: Miller Subject: M/Wellsamples -3/Yearly SMP Test Method Result Date Time Tech CHLORIDE SM 4500 a C 6.9 mg/L 7/7/2009 8:00 TDA COD SM 5220 D - 141 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 122 umhos/cm 7/7/2009 . 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E <0.1 mg/L 7/B/2009 8:05 ARS. FIELD ' 3.12 s.u. 7/6/2009 12:05 ROM ,PH SOLIDS, TOTAL DISSOLVED SM 2540 C 38.1 mg/L 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 13.5 mg/L 7/20/2009 30:45 : ENC TEMPERATURE FIELD 20.6 deg., C 7/6/2009 12:05 ROM TOTAL ORGANIC CARBON SM 53103 1.4 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 9.8 feet 7/6/2009 12:05 ROM .. CHLORIDE SM 4500 Cl C 7.4 mg/L 7/7/2009 8:00 TDA COD SM MO D 114 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 294 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 0.22 mg/L 7/8/2009 8:05 ARS PH FIELD 2.85 s.u. 7/6/2009 11:53 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 130 mg/L 7/7/2009 13:30 ENC SULFATE SM SSth 426 C 91.7 mg/L 7/20/2009 10:45 ENC TEMPERATURE FIELD 22.0 deg., C 7/6/2009 11:53 RDM TOTAL ORGANIC CARBON SM 53108 1.2 mg/L 7/14/2609 0:00 ECI WATER LEVEL FIELD 9.3 feet 7/6/2009 11:53 RDM z COD spike did not meet QC requirements. Data is valid, but qualified. LAB CODES: NID=None Detected N/F=None Found <=Lesstban >=Orcaterthan Est. —Estimated The data and olherinfa maInm mntaned on tins, and ether accompanying domme tle, represent only the sampleis) analyzed and B rendered upon the MEMBER � tor6donlhatit is not to be reproduced wholly or in pad for advertising or otherperposes without wdttenapprwal from the laboratory. �a��l� USDA-CFA-MORITesting Food5anitatlon Consulting UemUal and Worobinlogleal Analyses and Research ON ® NJI9Cfi'obac Laboratories, Inc. Page 3 of 3 FAYETTEVILLE DIVISION 2592 HOPE MILLS ROAD STATE CERT ID. FAYETTEVILLE,NC 28306 NC#1I (910) 864-1920 FAX (910) 864-8774 NC R37714 R. W. SANDERS, VICE PRESIDENT USDA43787 http://mwvl.microbac.com E Tvlail rsanders@microbac.com microbac.com TER -AIR • WASTES • FOOD • PHARMACEUTICALS •NUTRACEUTICALS. CERTIFICATE OF ANALYSIS Aliens, Inc. Ms. Kathryn Yeager Post Office Box 250 Siloam Springs, AR 72761 Permit No. NC TURKEY PLANT Sampler: Miller Subject: M/Well samples - 3/Y(mrly SMP Test Method Date Reported: 7/23/2009 Date Received: 7/6/2009 Order Number: 0907-00462 Invoice No.: 66649 Customer #: A004 Sample Date: 7/6/2009 Sample Time: 0:00 Result Date. Time Tech RESPECTFULLY SUBMITTED: 11C _ p/ . 3 afflAdRA& MICROBAC LABORATORIES, INC. 77rankyonforyourbusiness.)Yeiavileyaarf•edbackonourlerelofsenicelo)pou. Please contact the Laboratory Director, Ron Sanders at 910-864-1920, Robert A4organ, COO, al nnorganou rnicrobaacom or Trevor 0grce, CEO, al IbayceQnticrabpccorn milli mry eanunenls arsnggertions. LAB CODES: NID=None Detected N/F=None Found <=Less than >=Greaterthm E•st.=Estimated The data and otherinfmmation contained on Ides, and other accompanying documents, represent only the sample(s) analysetl and is tendered upon the MEMBER condition that It is not to be repmducod wholly or In part for adverating our other purposes without written approval from the laboratory. j ❑MA-Ei mnOSn Tsfing i,nod Sanitaaon Canorlting Oremical and 141aobialoglml Analyses and Researrh ) = _ ® Microbac Laboratories, Inc. ra,e I Ord FAYETTEVILLE DIVISION STATE CERT ID. 2592 HOPE MILLS ROAD FAYETTEVILLE, NC 28306 NC #I I (910) 864-1920 FAX (910) 864-8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA 43787 - -s ' http://iv-ww.nlicrobac.com 1 -Mal: rsanders@microbac.com CHEMISTRY MICROBIOLOGY• FOOD SAFETY• CONSUMER PRODUCTS WATER • AIR • WASTES • FOOD - PHARMACEUTICALS • NUTRACEUTICALS CERTIFICATE OF ANALYSIS Allens, Inc. Date Reported: 7/23/2009 Ms. Kathryn Yeager Date Received: 7/6/2009 Post Office Box 250 Order Number: 0907-00109 Siloam Springs, AR 72761 Invoice No.: 66648 Customer #: A004 Sample Date: 7/6/2009 Permit No. NC TURKEY PLANT Sample Time: 0:00 Sampler: Miller Subject: M/Well samples-3/Yearly SMP Test Method Result Date Time Tech CHLORIDE SM 4500 CI C 12.2 mg/L 7/7/2009 8:00 TDA COD SM 5220 D <10.0 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 116 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 0.10 mg/L 7/8/2009 8:05 ARS PH FIELD 5.20 sm. 7/6/2009 11:40 ROM SOLIDS, TOTAL DISSOLVED SM 2510 C 85.6 mg/L 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 9.75 mg/L 7/20/2009 10:45 ENC TEMPERATURE FIELD 19.8 deg., C 7/6/2009 11:40 ROM TOTAL ORGANIC CARBON SM 5310B 0.7 mD/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 13.6 Feet 7/6/2009 11:40 ROM - .. 00,2-:- M/V✓R. ... .. 1 .. .;;I - _ _. i .'lilila ice.... CHLORIDE SM 4500 CI C 5.4 mg/L 7/7/2009 8:00 TDA COD SM 5220 D 67.2 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 258 umhos/cm 7/7/2009 11:50 TDA NITROGEN, NITRATE SM 4500 NO3 E 7.39 mg/L 7/8/2009 B:05 ARS PH FIELD 3.S3 s.u. 7/6/2009 11:27 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 163 mg/L 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 45.7 mg/L 7/20/2009 10:45 ENC TEMPERATURE FIELD 22.1 deg., C 7/6/2009 11:27 ROM TOTAL ORGANIC CARBON 5M 5310B 5.4 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 8.4 Feet 7/6/2009 11:27 ROM do3_ M/W R:7 = _ LAB CODES: NID=None Detected N/F=None Found <=Lcssthan >=Greaterthan ESL=Estimated The dab and other Information contained on this, and other amompanong domments, represent only the sample(s) analMd and k rendered upon the MEMBER condll..ilia! it H not to be reproducedwholly or in par[ far advediAng or other purposes without written approval fiom the labontury. } usDA-CPA-HID5H Tesgng rood Sanibtinn Consulting ❑iemlcal and Microbiological Analyses and Rhon a=h U 1CIlicrol. ac Laboratories, Inc. FAYETTEVILLE DIVISION STATE CERT 1D, 2592 HOPE MILLS ROAD FAYETTEVILLE, NC 28306 NC #11 (910) 364-1920 FAX (910) 864-8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA 43787 http://wmw.microbac:com E-VIai1: xsandecs@miccobac.com CERTI F'ACATE OF AAIAH YSffS Allens, Inc. Date Reported: 7/23/2009 Ms. Kathryn Yeager Date Received: 7/6/2009 Post Office Box 250 Order Number: 0907-00109 Siloam Springs, AR 72761 Invoice No.: 66648 Customer'r=.: A004 Sample Date: 7/6/2009 Permit No. NC TURKEY PLANT Sample Time: 0:00 Sampler: Miller Subject: M/Well samples-3/Yearly SMP Test Method Result Date Time Tech CHLORIDE SM 4500 CI C 27.0 mg/L 7/7/2009 8:00 TDA COD SM 5220 D 49.6 mg/L 7/7/2009 11:00 ENC CONDUCTIVITY SM 2510 B 134 umhos/cm 7/7/2009 11:50. TDA NITROGEN, NITRATE SM 4500 NO3 E <0.1 mg/L 7/8/2009 8:05 ARS pH FIELD 3.55 s.u. 7/6/2009 11:17 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 86.3 mg/L 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 18.7 mgJL 7/20/2009 10:45 ENC TEMPERATURE FIELD 27.7 deg., C 7/6/2009 11:17 RDM TOTAL ORGANIC CARBON SM 5310B 7.0 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD B.B feet 7/6/2009 11:17 RDM t R. CHLORIDE SM 4500 Cl C 29.4 mg/L 7/7/2009 6:00 TDA COD SM 5220 D <10.0 mg/L 717/2009 11:00 ENC CONDUCTIVITY SM 2510 B 443 umhos/cm 7/7/2009 11:50 TDA' NITROGEN, NITRATE SM 4500 NO3 E 22.5 mg/L 7/10/2009 6:10 ARS PH FIELD 3.10 s.u. 7/6/2009 11:06 RDM SOLIDS, TOTAL DISSOLVED SM 2540 C 275 mg/L 7/7/2009 13:30 ENC SULFATE SM 15th 426 C 11.6 mg/L 7/20/2009 10:45 ENC TEMPERATURE FIELD 22.6 deg., C 7/6/2009 11:06 RDM TOTAL ORGANIC CARBON SM 5310B 1.4 mg/L 7/14/2009 0:00 ECI WATER LEVEL FIELD 11.1 Feet 7/6/2009 11:06 RDM LAB CODES: N/D=None Detected N/F=None Found <=Less than >=Gmaterthan Est.=Estimated The data and other Information contained on this, and other accompanying documents, represent only the sample(s) anaryred and k rendered upon the MEMBER condition that It is not m be reproduced wholly or In part for advernsing or other purposes wMout written approval from the laboratory. /, USDA-ITA-R10SHTesting Pond Sanitatlon Consultinq Ommlcul and 11hmblologicul Analyses and Research Microbac Laboratories mc. -7 { s FAYETTEVILLE DIVISION s a v STATE CERT ID. 2592 HOPE MILLS ROAD FAYETTEVILLE. NC 28306 NC #1 I (910) 864-1920 FAX (910) 864-8774 NC 937714 g R. W. SANDERS, VICE PRESIDENT USDA #3787 http://,%vww.microbac.com E-Tdai1: rsanders@microbac.com CHEMISTRY - MICROBIOLOGY• FOOD SAFETY• CONSUMER PRODUCTS WATER - AIR • WASTES • FOOD • PHARMACEUTICALS •NUTRACEUTICALS CERTIFICATE OF ANALYSIS Allens, Inc. Ms. Kathryn Yeager Post Office Box 250 Siloam Springs, AR 72761 Permit No. NC TURKEY PLANT Sampler. Miller Subject: M/Wellsamples -3/Yearly SMP Test Method Result Date Reported: Date Received: Order Number: Invoice No.: Customer #: Sample Date: Sample Time: Date Time 7/23/2009 7/6/2009 0907-00109 66648 A004 7/6/2009 0:00 Tech RESPECTFULLY SUBMITTED: 0- !'D - A MbA& MICROBAC LABORATORIES, INC. 7Lmrkyotiforyour business. IPe invite yourfeedback on our level ofsenice to you. Please contact the Laboratory Director, Ron Sanders at 910-864-1920, Robert Alforgan, COO, at rmorgan(r@i rnicrobaaconi or Tramr Bowe, CEO, at tboyeeCinicrobac.cotn with mryl commonly or.yaggestions. LAB CODES: NID=None Delecled NIF=None Found <=Less than >=Greaterthan Est,=Estimated The data and utherinfa matron contained on this, and other armmpamying documents, represent only the samples) analyaed and Is rendered upon" MEMBER co,diaon hot It is not to be mprvdumd wholly or In part for advertising or other purposes whhout wrthen approval rmm the laboratory. y USDA-EPA-NIOSHTesnng Foad Sanlatlon rpnsuldng Oiemlal and l4krtblologlal Analyses and nesearth 5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA, 28393 PHONE 910-596-0028 FAX 910-596-0127 April 13, 2009 Department of Environment & Natural Resources Water Quality Division, Groundwater Section 1636 Mail Service Center Raleigh, NC 27699-1636 919-733-3221 RE: Groundwater Quality Monitoring Report Allens, Inc. — Turkey, NC Facility Permit # WQ0004268 Enclosed you will find the completed Groundwater Monitoring Report forms GW59 and GW59A and the laboratory report for Allens, Inc. - Turkey, North Carolina facility for samples that were collected in March 2009. If you have any questions or require any additional information, please contact Kathryn Yeager by phone at 479-524-6431 ext. 296 or by email at kyeager@allens.com. allens.com. Sincerely, C Martin Griess Plant Manager Allens, Inc. CC: Reid Wells, Allens — Turkey Facility Kathryn Yeager, Allens, Inc. File Enclosures M SUBMIT QUALITY MONITORING: FACILITY INFORMATION "" u°"'• °' '+'P" PERMIT Number: Expiration D te: July 39, 2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge xx W00004268 UIC Permit Name (if different): NPDES Other Faciltty Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEiNG7iIONITORED ❑Lagoon sae+m NC 28393-9703 Sampson Turkey County Remedia Ion: Infiltration Gallery (cnn cs�ro) t:q) ® Spray Field ❑ Remedis ion: Contact Person: Martin Grless Telephones: 910-596.0028 ElRotary Distributor ❑ Land Ap Iication of Sludge Well Location/Site Name: No, of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other. mP SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 1 Date sample collected: 3/16/2009 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter in. pH 8.6 units Temp. 1 .4 eC DRY at Depth to Water Level: 17.14 ft. below measuring point Screened Interval: ft, to ft. Spec. Cord. rjI 'I Ahas time Of sampling, Measuring Point is @. above land surface Relative M.P. Elevation: ft Odor check Volume of water pumped/balled befoto sampling: 10+ gallons Appearance here: Samples for metals were collected unfiltered: OYES ❑ NO and field acdiBed: ❑ YES ❑ NO ' LABORATORY INFORMATION Date sample analyzed: see attached lab sheets' Laboratory Name: Microbac Laboratories Certification No. . C#11, NC#3771,t PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 12 mgA Nitrite (NO2) as N mgll Pb - Lead r1r 911 Coliform: MP Fecal /loom[ Nitrate (NOa) as N 17.0 mg/I Zn-Zinc I A Coliform: MF Total /100mi ... Phosphorus: Total as P mgA (Note:utaMPNmthadfor NgNyturbid ramplrr) Orthophosphate mg/I Other (Specify Compound sand'Cbirce trationUnks): Dissolved Solids: Total 398 mgA AI - Aluminum mgA P'1' ^� `�• 4 `� �✓/ fY ')"'y pH (when analyzed) units Be - Barium mg/1nnna TOC 2.6 mg/I Ca - Calcium mgA Chloride 73•4mo Cd-Cadmium mgA Arsenic mgA Chromium: Total mgA rntorrnan,`-; �.;ru'aOG Grease and Oils mgA Cu - Capper mgA ORGANICS: (by GC, GO/MS, HPLC) Phenol fitgA Fe - Iron mgA (Specify test and method A ATTACH LAB REPORT.) Sulfate ' 82.7mgn Hg-,Mercury mg11 Report Attached? ❑ Yas.(1) ❑ No Specific Conductance 629 PMhos K- Potassium mgA VOC - , method# Total Ammonia mgA Mg - Magnesium _mg/I , method # (AmmoNeNeogan;NH,arMAmmamaNluogaa,TOM _ Mn- Manganese mg/I ,method# TM as N mgA ` NI- Nickel mg/I , method # For Remedletion Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Martin Grless, Plant Manager `///I/ O Pamifiee(or Authorized AaeM)Name and Tdie- Plaace pnnt ortype Signalu of Pemlrles for Authanzed Agem) I (Dale) GW-59 Rev. 112007 SUBMIT FORM ON YFI l OW PAPER ONLY r GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILTY INFORMATION Please PON Greatly or Type PERMIT Number: Expiration ate: July 31,2011 Facility Name: Aliens, Inc. - Turkey Non -Discharge xx W00004268 UIC NPDES Other Permit Name (if different): AONITORED tion: Infiltration Gallery Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING ❑ Lagoon ❑ RemewIa Turkey 16tretl0 NC 28393-9703 County Sampson ® Spray Field ❑ Remedi a tion: Contact Person: Martin GrieSS Telephoneit: 910-596-0028 ❑ Rotary Distributor ❑ Land Ap lication of Sludge Well Location/Site Name: No, of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other. Tom Pe SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW 2 Date sample collected: 3/16/2009 FIELD ANALYSES: WAS Well Depth: ft. Well Diameter. in. pH 5.6 units Temp. 3.1 °C DRY at Depth to Water Level: 5.4 ft. below measuring point Screened Interval: ft. to ft Spec. Card. hos irate of sampling,check Measuring Paint Is ft. above land surface Relative M.P. Elevation: ft. Odor Volume of water pumped/balled before sampling: 10+ gallons Appearance ; hare: ❑ S Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: see attached lab sheets Laboratory Name: Microbac Laboratories Certification No. I C#11, NC#3771 e PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. )In COD <10.0 mgll Nitrite (NO2) as N mgA Pb - Lead gA Coliform: MF Fecal /100ml 'Nitrate (NO3) as N <0,1 mgA Zn - Zinc A Coliform: MF Total /100ml Phosphorus: Total es P mgA (Note: Use MPN method torNyily turbid sondes) Orthophosphate mgA Other (Specify Compounds and Conce itration Units): Dissolved Solids: Total 210mgn Al' mgA ,-^+ PH (when analyzed) units Be - Barium mgA v"Z t.- f ' i4" is) i'':t t TOC 2.7 mgA Ca- Calcium mgll Chloride 98.2 mgA Cd-Cadmium mgA kL qI Arsenic mgA Chromium: Total mgA Grease and Otis mgA Cu - Copper mgA ORGANICS: .(by GC; JGC%MS; HPLC) Phenol mgA Fe - Iron mgA (Specify test and method #. ATTACH LAB REPORT.) Sulfate <5.0.mg4 Hg- Mercury mgA Report Attached? ❑ Yes(1) ❑ No Spec Conductance 407 pMhos K-Potassium mgn VOC , method # Total Ammonia mgA Mg - Magnesium mgA , method # (Nrsmnia Mboven; NH°. N; Am(hcam h1 n- , T-A Mn -Manganese _ mg/1 , method # TKN as N mg/I Ni - Nickel mgA , method If For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: rnglL I I VOC Removal% Martin Griess, Plant Manager Penninee ,?Authorized Anent) Name and Title- Please print or type GW-59 Rev. 1/2007 SUBMIT FORM ONYELLOW PAPER ONLY QUALITY MONITORING: Name: Aliens, Inc. - Turkey Name (if different): Address: 6900 Turkey Highway County Sampson act Person: Martin Gdess Telephone#: 910-696-0028 Location/Site Name: No, of wells to be sampled:, LID NUMBER (from Permit): MW 3 Depth: ft. i to Water Level: 4.7 ft. below measuring point luring Point Is ft. above land surface vie of water pumped/balled before sampling: 10+ COD <10.0 mgll Colifonn: MF Fecal /loom] Coliform: MF Total /loom] (Note: Woo MPN method for NgNy hatid samplesl Date sample collected: 3/16/2.009 Well Diameter: _in. ` Screened Interval: _ft. to _ft. Relative M.P. Elevation: ft. ;RMIT Number: Expiratiof m-Discharge )oc W00004268 UIC )DES - Other PE OF PERMITTED OPERATION BEIN ❑ Lagoon ❑ Reme, ® Spray Field ❑ Reme, ❑ Rotary Distributor ❑ Land) ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: _ PH 7.06 units Temp. Spec.Cond. Odor Appearance Laboratory Name: Microbac Laboratories Certification No. colloidal concentrations. Write (N%) as N mgll Pb - Lead Nitrate (NO3) as N <0.1 mgn Zn - Zinc Phosphorus: Total as P mgA Orthophosphate mgn Other (Specify Compounds and Conr is Infiltration Gallery r: ation of Sludge If WELL As 1 aC Y at Ea of NC#3771,e Units): Dissolved Solids: Total 261 mgA AI -Aluminum mglt PH (when analyzed) - units Be - Barium mgA �' ,' .a„�• „i:^"" � - ) . TOC 1.5 mgn Ca - Calcium mg/I _ Chloride 46.3 mg/l Cd-Cadmium mgA Arsenic mgn Chromium: Total mgrl Grease and Oils mgn Cu - Copper mgrl ORGANICS: (by GC, GC%MS;'APLC) Phenol mgA - Fe - Iron mgll (Specify test and method #. ATTAC LAB REPORT.) Sulfate 38.4mgA Hg-Mercury mgA' 1 Report Attached? ❑ Yes(]) ❑ No Specific Conductance 368 µMhos K - Potassium mgll VOC , method # Total Ammonia mg/l Mg - Magnesium mgA , method # (Ammonia Maragam NH.., N; A .la Niboyen, Total) Mn- Manganese mgA .method#� ' TM as N mgll Ni - Nidcei mg1l , method # For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Martin Gress, Plant Manager Penn ttee (orAuthorapd Apant) Name and Title- Please print or type GW-59 Rev. M007 'SUBMIT FORM ONLY QUALITY MONITORING: Name:_ Allens, Inc. - Name (if different): Address: 5900 Turkey Highway ty 6accxt NC 28393-9703 County Sampson act Person: Martin Griess Telephone#:. 910-596-0028 Location/Site Name: No. of wells to be sampled: 4 L.10 NUMBER (from Permit): MW 4 Date sample collected: 3/16/2009 Depth: ft. Well Diameter: _In. It to Water Level: 6.1 ft. below measuring point Screened Interval: _ft. to _ft. ;wring Point is ft. above land surface Relative M.P. Elevation: ft. me of water pumped/bailed before sampling: 10+ gallons MMIT Number: Expiration in -Discharge xX WQ0004266 UIC, )DES _ _ Other xPE OF PERMITTED OPERATION BEIN( ❑ Lagoon ❑ Remed ® Spray Field ❑ Rented ❑ Rotary Distributor ❑ Land A ❑ Water Source Heat Pump ❑ Other:, FIELD ANALYSES: pH 4.16 units Temp. Spec. Cond. Odor Appearance sample analyzed: see attached lab sheets laboratory Name: Microbac Laboratories Certification 4METERS NOTE: Values should reflect dissolved and colloidal concentrations: COD <10.0 mgA Nitrite (NO.) as N mg/I Pb -.Lead Coliform: MF Fecal /100m1 Nitrate (NO3) as N 5.91 mg/I Zn - Zinc Colifonn:MFTotal /t00ml (Note: Uce MPN rn Mod hrhigNy trod eampiee) Dissolved Solids: Total 75.3 mgA pH (when analyzed) units TOC ' <0.5 mgA Chloride 14.4 mgA Arsenic mg/I Grease and OILS mg/I Phenol mg/I Sulfate <5.0 mg/1 Specific Conductance 139µMhos Total Ammonia mg/I (AmmoMe Nlaopen; NH.® N; Anaiwnla Nlt OW. Total) TKN as N mg/I Phosphorus: Total as P mg/I Orthophosphate mg/I AI -Aluminum mg/I Be - Barium - mgA. Ca - Calcium mg/I Cd- Cadmium mgA Chromium: Total mgA Cu - Copper Mgt[ Fe - Iron mgA Hg - Mercury mg/I K- Potassium mgA Mg - Magnesium mgA Mn - Manganese mgA Ni - Nickel _ mgA Other (Specify Compounds and (Specify test and method#: ATTA( Report Attached? ❑ Yes (' VOC , method # method # method # method # Infiltration Gallery on of Sludge Fin eC NC#3771,i Units): LAB REPORT,) ❑ No (0) For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mgA- Effluent Total VOCs: mg/L I I VOC Removalb Martin Griess, Plant Manager1 Permtttee(orAuthorlred ApeM)Name and Title- Please print ortype Stpneture of Petmieee (or uNodzed Apenn -I (Date; GW-59 Rev, 1/2007 CI GW-59A COMPLIANCE REPORT FORM Permit# W00004266 (Submit one each monitoring period with GW-59 forms.) I Enter date monitoring results were due. 4-30-09 Will this monitoring report (GW59 and GW-59A) be submitted after YES NO the established due date? 2 Was any required Information missing on the GW59 report form? YES NO ' IF the answer to question 1 or 2 is "YES' list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells In need or repair or maintenance (damage casing, unlocked or missing cap, missing YES NO Identification plate, area overgrown, etc.)? If the answeris Wes', contact the Regional Office forguidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is 'NO", skip to section 9. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentrations(s) exceeding standards in the space provided below. 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same constituents) YES NO In the same well(s) In the past two years? If the answer to question 51s 'NO", skip to section 6. if the answer to question 5 is "YES" list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). 6 Ara the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO if the answer is "YES", a groundwater qualltyproblem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELYFOR GUIDANCE If the answer is "NO", monitoring wells maybe Improperly located; contact the Regional Otrlce. 7 Is the permittee Implementing previously approved actions required by the Division involving this groundwater quality YES NO problem? if the answer to question 7 is 'YES, describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the Impact the waste disposal system is havina at the review and compliance boundaries surrounding this facility. Failure to do so may subiect the permittee, to a Notice ofylolation. fines, and/or penalties. 6 The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with the GW-59 forms for required wells to the address provided at the top of the current GW-59 forth. I hereby acknowledge that the above Information was evaluated and the information submitted in this report (Compliance Report GWS9A) is We and complete to the best of my knowledge. Martin Griess, Plant Manager (Signature of Permittee or Authorized Agent) Date GW-59A 12/8/2003 WATER • AIR Microbac Laboratories, Inc.. Page I of FAYETTEVILLE DIVISION • STATE CERT ID. 2592 HOPE MILS ROAD FAYETTEVILLE, NC 28306 NC#ll (910) 864-1920 FAX (910) 864-8774 NC #37714 R. W. SANDERS, VICE PRESIDENT USDA #3787i. http://www.microbac.com E-Mail: tsanders@ 1icrobac.cona PHARMACEUTICALS CERTIFICATE OF ANALYSIS Allen, Inc. .Date Reported: 3/31/2009 Ms. Kathryn Yeager Date Received: 3/162009 Post Office Box250 Order Number: 0903-00008 . Siloam Springs, AR 72761 Invoice No.: 64018 Customer#: A004 - Sample Date: 3/162009 PermitNo. NCTURKEYPLANT ' Sample Time: 0:00 Sampler: Miller Subject: M/Wellsamples -3/Yearly SMP Test Method Result Date Time Tech E ,zyrlr3..TX l'-F t001*a=.1M CHLORIDE SM 4500 CI C 73.4 mg/L 3/17/2009 10:15 HAK COD SM 5220 D 12.0 mg/L 3/1812D09 10:30 ENC CONDUCTIVITY SM 2510 B 629 umhos/aR 3/16/2DD9 15:30 HAK NITROGEN, NITRATE SM 4500 NO3 E 17.0 try/L 3/18/2D09 8:35 HAK PH FIELD 8.60 s.u. 3/16/2009 9:55 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 398 mg/L 3/17/2009 9:40 -, HAK SULFATE SM 15th 426 C 82.7 mg/L 3/30/2009 15:30 DCR TEMPERATURE FIELD 16.4 deg.,C 3/16/20D9 0:00 ROM TOTAL ORGANIC CARBON SM 5330E 2.6 rrg/L 3/24/2009 0:00 ECI WATER LEVEL FIELD 17.14 feet 3/16/2009 0:00 ROM CHLORIDE SM 4500 CI C 98.2 mg/L 3/17/2009 10:15 HAK COD SM 5220 D <10.0 mg/L 3/18/2009 10:30 ENC CONDUCTIVITY SM 2516 B 407 umhes/cm 3/16/20D9 15:30 HAK NITROGEN, NITRATE SM 4500 NO3 E <0.1 ng/L 3/18/20D9 8:35 HAK PH FIELD 5.60 s.u. 3/16/2009 0:00 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 210 mg/L 3/17/2009 9:40 HAK SULFATE SM 15th 426 C <5.0 mg/L 3/30/2009 15:30 DCR TEMPERATURE FIELD 13.1 deg.,C 3/16/2009 0:00 ROM TOTAL ORGANIC CARBON SM 5310B 2.7 mg/L 3/24/2009 0:00 ECI WATER LEVEL FIELD 5.4 feet 3/I6/2009 0:00 ROM LAB CODES: NID=None Detected N/F=None Feend <=Lesthm >=Grzeterthan BSL=Estimated MEMBER meam mawcnr aarmmtm mAa as atcamcwmtiin>�.2a�[tl+r meuaeKsl=eaMa+wsmmetwm u� mNion tM ¢ a rt b h rm W ®1 wtv0/ tl M wet (tl aemisbll tl timer aactl�.av<w. um waa'y fmm ee stormy. USnkf IOS1Te960 Ftltl ShcJaVn fdwNng eimazl aitl Mlvahbb9lalAmt/sSWPeevOi Microbac Laboratories, Inc. Page 2 of 3 FAYETTEVILLE DIVISION STATE CER1` ID: 2592 HOPE MII-LS ROAD - FAYETFEVILLE, NC 28306 NC #11 (910) 864-1920 FAX (910) 864-8774 NC #37714 . , . ' R. W. SANDERS, VICE-PRESIDENT USDA-#3787- http-//www.microbac.com E-MaB:is,mders@raicrobac.com ` '- http-//www.riiicrobac.com WATER • AIR • WASTES Allen, Inc. Date Reported: 3/3112009 Ms. Kathryn Yeager Date Received; . , 3/16/2009 '0903-00008 Post Office Box 250 OrdeCNumber: .. Siloam Springs, AR 72761 - InvoiceNo.:. . 64018. Customer#: A004 - Sample Date: 3/16/2009 Permit No. NC TURKEY PLANT Sample Time: 0:00 ' Sampler: Miller Subject:M/Wellsamples -3/Yearly SMP Test Method, Result Date Time Tech 003s-s M�i�i3� �i3 4� c 3a. i' ,'1 £� �-%C.�'y KteT v.". PAy .ram -.fix 1a=c.m- 4 I }'a R '`yt.ss.,. E.. i tae�"kib�} sw'Fi° �.t'LL3C�'L'£ -i ;,.xds435i. CHLORIDE SM 4500 O C 463 mg/L 3/17/2009 _ 10:15 HAK CUD - SM 5220 D <10.0 mg/L 3/18/2009 10:30 ENC CONDUCTIVITY ' SM 2510 B 368 undms/00 3/16/2009 15:30 HAK NITROGEN, NITRATE SM 4500 NO3 E <0.1 mg/L 3/18/2009 8:35 HAK PH FIELD 7.06 s.u. 3/16/2009 0:00 ROM SOLIDS, TOTAL DISSOLVED SM 2540 C 261 Bg/L 3/17/2009 9:40 HAK SULFATE SM 15th 426 C 38.4 Mg/L 3/30/2009 15:30 DCR TEMPERATURE FIELD 11.1 deg., C 3/16/2009 0:00 RDM TOTAL ORGANIC CARBON SM 5310B 1.5 mg/L 3/24/2009 0:00 ECI WATER LEVEL FIELD 4.7 feet 3/1612DO9 0:00 ROM ..,1-*+.•*+iarca�;�4, r�"'.i'�'} -- 7i.t"'"'.-'F�„_ "--.may *vci.�ie"n s✓°"r�:tt ��-�-sL;�;�.^�ra�r-..��'�.i �_��'"*2'�"'��ik'�.",.�`..�3"rsSKKn?l ��'` 'sdM� Wa�4.:%�-,�Rt� �" -! -°' :a...-:= .�h`'"T `yt.Sr..._..^�..� � - - �'�` '� ti=:::•..'�'t.4..2�Y.�' � ...�f -. Vic.. �ir�s'."+.-L,.-� .:s..��'�..d•.^`-'.2 CHLORIDE SM 4500 a 14.4 ng/L 3/17/2009 10:15 HAK CUD SM 5220 D <10.0 mg/L 3/18/2009 10:30 ENC CONDUCTIVITY SM 2510 B 139 umhosloon 3/16/2009 • 15:30 HAK NITROGEN, NITRATE SM 4500 NO3 E 5.91 mg/L 3/18/2009 8:35 HAK pH FIELD 4.16 s.u. 3/16/2DO9 0:00 RUM SOLIDS, TOTAL DISSOLVED SM 2540 C 75.3 mg/L 3/17/2009 BAD HAK SULFATE SM 15th 426 C <5.0 Mg/L 3130/2009 15:30 DCR TEMPERATURE FIELD 123 deg.,C 3/16/2009 0:00 RDM TOTAL ORGANIC CARBON SM 5310B <05 ng/L 3/34/2OD9 0:00 ECI WATER LEVEL FIELD 6.10 feet 3/16/2009 0:00 RDM LAB CODES: N/D-No.. Domed MF=None Foond <= Loss than >=Greater Lhea Psc=Fsdmeted MEMBER lle 4ab ab ma etomum� mnm� m mR, atl pXp a Rvnpanyhp doanves, ,�ecart way me eampk(Q enalyael utl k: rtf deal upon tle .._ - .¢atlebn RalRa MlomnpoM1ml ntM/orNpMfar ae,at6egaaer PRpu�wNul,nRtrnaMeorel(mn ae aOonRry. ®. ISWdAN1091 TeRnp � Cn�i9 l]meclaNMbotdUpeal NelryseM Re�mRa - _ Page 3 of 3 Nflerobac Laboratones, Inc FAYETTEVB,LEDMSION r STA7 2592 HOPE MILLS ROAD FAYETTEVE,LE, NO 28306 EN(910) 864-1920 FAX (910) 864-8774R. W. SANDERS, VICE PRESIDENT http://www.microbaccom E Mail Fsan ers(a3mteiobac cc • MICROBIOLOGY • FOOD SAFETY • CONSUMER PRODUCTS WASTES • FOOD • PHARMACEUTICALS •NUIRACEUTICALS Allen, Inc. Date Reported: 3/312009 Ms. Kathryn Yeager _ Date Received: .. . 3/162009 Post Office Box250 Order Number:., ; ; .0903-00008 - ' Siloam Springs, AR 72761' Invoice No.: ._ ., 64018 - Customer#: A004 - Sample Date: 3/162009 Permit No. NCTURKEYPLANT Sample Time: 0:00. Sampler: Miller ' Subject N/WeRsamples -3/Yearly -• ..SMP Tat Method Result ' Date Time Tech . . .... J� - RESPECTFULLY SUBMITTED: ___/[e. II . .1lan&(16 MICROBAC LABORATORIES, INC. 7hmtkyoafar)aarbmimse Weimircywrfeedbackonmrl verofsmimtoym Pleaeecontact theLabamtotyDirector, RonSondert at910A64.1970, Robert Morgan C00, utrmagan@mlcrabaarom or n cvarBaym, CEO, at tboyce@mimobaacmmwith any commena arsoggesdom. LAB CODES: NID=Noae Dowd NIF=Nova Fomd <—Lesathan >-Gmatm Waa Ea.=Fsumattd MEYaE11 -.. ..-. he aN artlotlrtrtmnaemaomao-el ona4WalvaonrtWm�MawneR namesmYtleu�mktU em!/talaNmrtNaA upon tle meltldi tl�etrt m,umts�maomwmhmmam M1xaMemma>atici�^�AwM14n.apparal fmm tlemOmary. .... mSoA£aAi110511 Tea1q FmESaaatlmt ramWYq rlimimleb mbolbbplmlAmltse eN 0.esmrtl,