WQ0004268_GW Monitoring_20101222

J 1 NO VR MRMORIRS SINCEl ..
Quality Vegetables
5900 TURKEY HICHWAY, TURKEY, NORTH CAROLINA, 28393�EC�O�ED
PHONE [phone]
FAX A10-SAR-0197 ..
January 12, 2011 FEB 0 9 2011
Dept. of Environmental & Natural Resources DENR-FAYETTEALLE REGIONAL OFFICE
- Division of -Water -Quality - Information Processing Unit
1617 Mail Service Center
Raleieb.NC 27699-1617
[phone]
RE: Groundwater Quality Monitoring- Report ( Resample Report)_
Aliens, Inc. - Turkey, NC Facility
Permit# W00004268
Enclosed are the original, and one copy of the Groundwater Monitoring Report on forms GW-59
and GW-59A, and the lab report for Allens, Inc -Turkey, NC facility for samples collected on
Dec.14.2010.
In the previous report dated Dec 22,2010, the initial result for monitoring well R-6 was 11.9 mg/L
For Total Organic Carbon. Consistent witli the permit requirements, Allens requested that another sample
be taken from this well since the result was greater than 10 mg/L. The results were reported and came back
at 9.1 mg/L, within the permit requirements.
If you have any questions or require any additional information, please contact me by
phone at [phone] ext # 104
Sincerely,
7
Martin Griess
Plant Manager
Allens, Inc. Turkey facility
CC: Laura Mushinski, Allens, Inc
Reid Wells, Allens, Inc - Turkey facility
RECEIVED
JAN 2 0 2011
NjION
nform:Aion processing TUnit
� 8C`IVED
JAN 3 12011
Ea;ei9hRegroeap0(reo

W
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc Date Reported: Jams 06, 2011
Mr. Reid Wells Project: M/W samples- 3/Yearly, Retest Date Received: De ber 15, 2010
Turk Turkey Highway P
Date Sampled: December 14, 2010
Turkey NC, 25393 Sampled By: Miller
M/W - R-6
1012321-01
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
Analyzed by: Miwbac-Chlcagoland Division -
Total Organic Carbon 9.1 mg/L 12/28/10 9:00 JP SM 531013
Qualifier Definitions
State Certifications: Respectfully Submitted
NCDNR #11
NCDOH 937714
USDA 03787 R. W. Sanders, VP/Managing Director
Thank you foryour business. We mvim yonrfe bAack nn our /errf nfterv/¢ la yna. P/eose conlam the LY/Managing Olrccror, Ron Sanders ol9/0A6{-(920. Jnmet Noku, Prcridenl. al
jnuker(Ilmicroboccmn W rrernr 8oyre, C10, al Ibnym n�jniunhac.rom witli anv rommentr arsuggeslians. Page 1 of 1

SUBMIT FORM ON YELLQVV PAPER ONLY
GROUNDWATER QUALITY MONITORING:
PEPARTMENTOF. P.NVIRONMENT&'NATURAL'.RESOURCES
NISION OFIWATER QUALITY -INFORMATION PROCESSING UNITr
COMPLIANCE REPORT FORM
617MAIL-SERVICE,CENTER,RA_LEIGH,`NC276gg-1617�'Phone,(91g)7223221
FACILITY INFORMATION Pease Print Clearly or Type
PERMIT Number: Expiration Date: JUIy131,2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑Remediation: Infiltration Gallery
screen
Turkey NC 28393-9703 County Sampson
i'ut`) (zip)
m Spray Field ❑ Remediation:
Contact Person: Martin Griess
Telephone#: [phone]
❑ Rotary,'Distributor ❑Land Application ofi5ludge
Well Location/Site Name:
No. of wells to be sampled:
❑ WaterSoUrce Heat Pump ❑ Other:
M1nm pirmt
_
SAMPLING INFORMATION
��
If WELL
WELL ID NUMBER (from Permit): R-6
Dale sample collected: 12/14/10
FIELD.'AN%1LYSE5:
AS
Well Depth: ft.
Well Diameter: in.
pH t" ii' units Temp. oC
DRY at
De p g point
Depth to Water Level: ft. below measuring
Screened Interval: ft. to
'
ft. Spec. fiord. µMhos
time of
Measuring Point is ft, above land surface
Relative M.P. Elevation: ft.
Odor . kJ
Sampling,
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here:
Sam des for metals were collected unfiltered: ❑YES
❑ NO and,field acidified: []YES ❑ NO
"
❑
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: MicrobaC LaboratoriesI Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
i
COD mg/I
Nitrite (NO,) as N
mg/l
Pb -iLead mg/I
Coliform: MF Fecal /100ml
Nitrate (NOO as N
mg/I
Zn }Zlnc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mgll
(Nate: Use MPN method for nighty turbid samples)
Orthophosphate
mg/I
Other(Specify Compounds and Concentration Units):
Dissolved Solids: Total mg/I
AI -Aluminum
mg/t
!!
pH (when analyzed) units
Be - Barium
mg/I
TOC 9.1 mgA
Ca- Calcium
mg/I
e t
Chloride mg/l
Cd - Cadmium
mg/I
f,'a
Arsenic mgA
Chromium: Total
mg/I
't
Grease and Oils mg/I
Cu - Copper
mg/1
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/l
Fe -Iron
mg/l
a
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate mg/1
Hg - Mercury
mgll
ReportAttached7 ❑ Yes (1) ❑ No (0)
Specific Conductance µMhos
K- Potassium
mgll
VOC is ,method#
Total Ammonia mg/I
Mg - Magnesium
mgll
-- I8 , method #
(Ammonia Nlimgen; NHoee N; Ammonia Nitrogen, Total)
Mn -Manganese
mgll
'r I,' ,method #
TKN as N mg/l
NI - Nickel
mgll
1 method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VCCs: mg/L Effluent Total VOCs: Ill mg/L ,VOC Removal%.
Martin Griess, Plant Manager 7/(/� AA-'
6bA „
Parminee(or Authorized Agent) Name and Title -Please print or type Sip cure of rmittee(or Authorized Agent) It
GW-59 Rev. 1/2007
•r

�} GW-59A COMPLIANCE REPORT FORM Permit # Itog Obo Llol68'
(Submit one each monitoring period with GW-59 forms.) ,.
1
Enter date monitoring results were due. (/23)' D ) Will this monitoring report (GW59 and GWS9A)
NO
be submitted after the,established due date?
2
Was any required information missing on the GW-59 report forms?
ygS
IF the answer to question 1 or 2 is -YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
O
identification plate, area overgrown, etc)? Ifthe answer is "Yes", contact the Regional Ofcefor guidance.
4
Are any monitored constituents equal to or above the established standards?
YES
If the answer to question 4 is 'NO" skip to section S.
If the answer to question 4 is "YES" list the affected wells individually with constituents) and concentration(s)
exceeding standards in the space provided below:
5
For.the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
,
If the answer to question 5 is "NO', skip to section 8.
If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentraffon(s) reported, and sample collection date for each occurrence (for the last two years)..
l
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES" a groundwater qualify problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE If the answer is "NO", monitoring wells may be improperly
located; contact the Regional Office.
7
Is the perrnittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is 'YES" describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility, Failure to do so may subfect the Permittee to a Notice of Violation,
fines, andforpenalffes.
8
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current G W-59 torte.
I hereby acknowtedge.that.the above -information was evaluated and the` informatiortsubmitted in this,
• -
report.(Compliance, Repo � G_ W59Aj;:isarue'and comp fete:to the best of myknowleJdge: -
Signature of Perm (or Authorized Agent) Date
GW-59A 12/812003

i
Y `p0 Q9 M9tl 00�01 SINCC !9
Quality Vegetables
December 22, 2010
Dept. of Environmental & Natural Resources
Division of Water Quality —Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
RE: Groundwater Quality Monitoring Report
Allens, Inc. — Turkey, NC Facility
Permit# WQ0004268
O :z
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V.zc
ly
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RECEIVED
JAN 13 2011
DENR—FAYEfTEVILLE REGIONAL OMCE
Enclosed are the original and one copy of the Groundwater Monitoring Report on forms GW-59 and G W-59A, and
the lab report for Allens, Inc. (Allens) facility located in Turkey (Sampson County) for samples collected in
November,2010.
The initial result for monitoring well R-6 was 11.9 mg/l for Total Organic Carbon. Consistent with the permit
requirements, Allens requested that another sample be taken from this well since the result was greater than 10 mgtl.
Another sample was collected by our contract laboratory, Microbac, on December 15, 2010. The results for the re-
test are not yet available and•will be submitted once they are available.
There were also some exceedances of the 10 mg/l standard for nitrate — nitrogen. The highest concentration, during
this round, of nitrate — nitrogen was 28.9 mg/l in monitoring well R-8. Monitoring well R-8 also has the highest
groundwater elevation showing that this well is apparently the background well. The higher concentrations of
nitrate —nitrogen in this monitoring well maybe reflective of agricultural practices up -gradient of the site. There
were also nitrate — nitrogen exceedances in monitoring wells R-9 and R-5a, although these concentrations were
lower than those measured in the background well, R-8. The Rowan Road irrigation system, that these monitoring
wells assess, was first put into service in February 2010. Since that time, approximately 99 pounds per acre of plant
available nitrogen have been applied to the coastal Bermuda cover crop via wastewater applications in Zones 13 and
10, which are nearest these wells. Since this application is well within the typical uptake of this cover crop, Allens
does not believe that the nitrate — nitrogen concerns are a reflection of over -application on the irrigation fields.
Finally, the pH level of the groundwater samples in all the groundwater monitoring wells is below the lower range
PH standard of 6.5 standard units. Each well is below this standard, including the background wells. At the Rowan
Road site, the pH level of the groundwater was consistently below this level even before the irrigation site was ever
used. This concern was brought up during the permitting process and Allens was told to monitor for awhile and then
submit a request to modify the permit standard for pH based on what apparently is regional groundwater
characteristic. Allens is preparing summary tables at this point and expects to submit this permit modification
request in the near future.
If you have any questions or require any additional information, please contact me by phone at [phone] ext #
104.

Sincerely,
� All In
Martin Griess
Plant Manager
cc: Laura Mushinski, Allens
Reid Wells, Allens —Turkey
Aliens, Inc
5900 Turkey Hwy
Turkey, NC 28393
910-596-0028

'-R QUALITY MONITORING:
REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkev Hiahwav
County Sampson
act Person: Martin Griess Telephone#: [phone]_ .I
LocalloNSite Name: No..of wells to be sampled:
FLING INFORMATION tm� P mml
LID NUMBER (from Permit): R-1 Q Dale sample collected: 1118/10
Depth: ft. Well Diameter. . In.
g to Water Level: 4.11 ft. below measuring point Screened Interval: ft. to ft.
Turing Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumpedfballed before sampling: 10+gallons
:RMIT Number: Expiration Date: JUIy 31, 2015
m-Discharge W00004268 UIC
IDES Other.
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediatlan: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES: AS
pH 5.28 units Temp. 20 °C [here:
RY at
Spec. Cond. 'µMhos e of
Oder mplin
eck
Appearance _ r
i sample analyzed:
Laboratory Name: Mlcrobac,Laboratories
Certification No. NC#11 NC#37714
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
62.6 mg/I
Nitrite (NO,) as N
hill-
Pb - Lead mg/I
Collform: MF Fecal
1100ml
Nitrate (NO3) as N
2,q1 mgil
Zn - Zinc mg/I
Coliform: MF Total
1100ml
Phosphorus: Total as P
mgll
(Note: Use MPN meltrod far NgNy turbid s.mPles)
Orthophosphate
mgll
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
46.0 mgil
AI - Aluminum
mgn
pH (when analyzed)
unfts
Be - Barium
- inlin
TOC
2.7mg/l
Ca - Calcium,
mg/l
Chloride
10.4 mg/I
Cd- Cadmium
�mg/I '
Arsenic
mg/I
Chromium: Total
mgll
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/l
Fe - Iron
mgll
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
15 mg/I
Hg- Mercury
mg/I
ReportAttached? ❑ Yes(1) ❑ No
Specific Conductance
84.4 µMhos
K - Potassium
mgfI
VOC , method # .
Total Ammonia
mg/I
Mg -Magnesium
mg8
#;
(Ammonia MVopan: NH... N:Amm NftNiba6en, TPla)
Mn- Manganese
mgil
,method
TKN as N
mg/1
NI - Nickel
moil
,method#
mMhM de
• .. •--•^......... -s—... � -"-I tea- r.ey,., ra). nlnuum l olal vucs: /L Enluent Total VOCs'
_ m 9 me/L VOC Removal°
Martin Griess, Plant Manager
Parnell.. for Authadzed Agent) Name antl mile -Please print or type
GW-59 Rev. 1/2007
%,;-�/%/,'0

QUALITY MONITORING:
Name: Aliens, Inc. -
Name (if different): _
Address: 5900 Turkey
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
PLING INFORMATION
,LID NUMBER (from Permit): R-2a Date sample collected: 11/8/10 .
Depth: ft. Well Diameter: —in.
h to Water Level: 4.11 ft. below measuring point Screened Interval: ft. to _
raring Point Is ft. above land surface Relative M.P. Elevation: ft.
me of water pumped/bailed before sampling: 10+gallons
ETERS NOTE: Values should reflect dissolv
COD 74.9 mg/I
Callform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use W14 method far NpNy tarbid samples)
Dissolved Solids: Total
90.0 mgn
pH (when analyzed)
units
TOC
1.0 mg/l
Chloride
14.2 mg/I
Arsenic
mg/l
Grease and Oils
mg/I
Phenol
mg/l
Sulfate
48 mg/i
Specific Conductance
232 µMhos
Total Ammonia
mg/I
(Ammonle Milligan: NHses N: Amnonla
Nimagen, ToNI)
TKN as N mgll
Number: Expiration Date:
Iharge WQ0004268 UIC_
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑Lagoon ❑ Remedlatlon: Infiltration Gallery
® Spray Field ❑ Remedialion:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heal Pump ❑ Other.
FIELD ANALYSES:
pH 4.64 units Temp. 19 °C
ft. Spec. Cond. µMhos
Odor
Appearance _
LaboratoryName: Microbac Laboratories
colloidal concentrations.
Nitrite (NO.) as N mg/l Pb - Lead
Nitrate (NOa) as N 2,06 mg/I Zn - Zinc.
Phosphorus: Total as P mg/1
Orthophosphate
mg/i
AI - Aluminum
mg/l
Be - Barium
mgll
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu- Copper
mgll
Fe - Iron
mg/I
Hg- Mercury
mgll
K- Potassium
mg/l
Mg - Magnesium
mgll
Mn- Manganese
mg/I
NI - Nickel
mg/I
Certification No. NC#11 NC#37714
mg/l
mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes,(1) ❑ No (a)
VOC , method#
method #
method #
method #
FVl ulm1Vu ayarvnia Willy tnuacn Lao neponsf: mrmem ioral VUus: mg/L Effluent Total VOCs: mg/L VOC Removal00/a
Martin Griess, Plant Manager r`,ylo9 p) �Y( ", ' J/j0
Permlltee(or Authorized Attend) Name and Title- Please print or type SIe08 fif PerlrllneI(IAAUIhorized Aoanfl [ (Dale)
GW59 Rev, 1/2007
at
of
1•I

TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. -
Name (if different):
Address: 5900 1
Person: Martin Griess
Location/Site
County Sampson
Telephone#: [phone]
No. of wells to be sampled:
Date:
WQ0004268
'DES Other.
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other.
.L ID NUMBER (from Permit): R-3
Date sample collected: 11/8/10
FIELD ANALYSES:
le
1
Depth: ft.
Well Diameter: — In.
pH 5.25 units Temp.
19 °C
DF
IT to Water Level: 6.80 0. below measuring point
Screened Interval: _ft. to _ft.
Spec. Cond.
µMhos
thin
Paint is ft. above land surface
Relative M.P. Elevation: ft.
Odor
ne of water pumped/bailed before sampling:
10+gallons
Appearance
chi
hei
ales for metals were collected unfiltered: ❑YES
DRATORY INFORMATION
❑ NO and field acidified: ❑ YES ❑ NO
_
sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No.
NC#11 NC#37714
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 57.7 mg/I
Nitrite (NO2) as N mgll
Pb - Lead
mg/I
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N 2.51 mgll
Zn - Zinc
mg/l
Coliform: MF Total /l00ml
Phosphorus: Total as P mgll
(Note: Use MPN method kr highly N,bid eimpies)
.Orthophosphate . mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
26.0 mg/I
pH (when analyzed)
. units
TOO
1.0 mgA
Chloride
9.89 mgA
Arsenic
mg/I
Grease and Oils
mg/l
Phenol
mg/I
Sulfate
- 13 IT
Specific Conductance
72.1 µMhos
Total Ammonia
mg/I
(Ammonle Nitrogen; W,ee N; Ammonia
Nitration. Talon
TKN as N mg/I
AI -Aluminum
mgA
Be - Barium
mgA
Ca - Calcium
mgll
Cd- Cadmium
mgA
Chromium: Total
mg/l
Cu- Copper
mgll
Fe - Iron
mgll
Hg- Mercury
mg/I
K- Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mgll
NI - Nickel
mall
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
ReportAttached? ❑ Yes (1) ❑ No (0)
VOC ,method#
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): . InfluentTotal VOCs:. t_. .- mg/L-, '. Effluent Total VOCs: mg/L VOC Removal%
Martin Griess, Plant Manager
Penalties (or Authorized Agent)Nam. and Title- Please print or type Signature of PermitSe(cr AuthonZed Agent) (Dale) /
GW59 Rev. 112007
at
of
0

Rill 7IT, IY�YOTt1S
---R QUALITY MONITORING:
REPORT FORM
Name: Allens, Inc. - Turkey
Name (If different):
Address: 5900 Turkey Highway
y """° NC 28393-9703 County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: _ _ _ _ _ No. of wells to be sampled:.
L ID NUMBER (from Permit): R-4
Depth: ft.
h to Water Level: 7.40 ft. below measuring point
luring Point Is ft. above land surface
Date sample collected: 11/all0
Well Diameter. in.
Screened Interval: ft. to _ft.
Relative M.P. Elevation: ft.
WQ0004268 UIC;
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other..
FIELD ANALYSES:
pH 4.50 units Temp. 20 eD
Spec. Cond. µMhos
Odor
Ime of water pumped/balled before sampling:
10+ gallons
Appearance
he'.
1ples for metals were collected unfiltered: ❑YES
INFORMATION
❑ NO and field acidified:
❑YES _ ❑ NO
IORATORY
t sample analyzed:
LaboratoryName:
Microbac.Laboratories
Certification No: NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 33.5 mgll
Nitrite (NO,) as N
mgll
Pb - Lead mg/i
Coliform: MF Fecal /100ml
Nitrate (NO,) as N
5.48 mgll
Zn - Zinc mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Nola: Use MPN meNod for highly tMaid samples)
Orthophosphate
mgn
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
53.0 mgll
pH (when analyzed)
units
TOC
0.8 mg/i
Chloride
7.90 mg/I
Arsenic
mgh
Grease and Oils
mgll
Phenol
mg/I
Sulfate
12 mg/I
Specific Conductance
97.4 µMhos
' Total Ammonia
mg/l
(AmmoNa Nllmgen; NHsas N; Ammanle Ninogen. Total)
TKN as N mg/l
AI - Aluminum mgll
Be - Barium mgll
Ca - Calcium mgh
Cd- Cadmium
mg/l
Chromium: Total
mg/I
Cu- Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K- Potassium
mgn
Mg - Magnesium
mgll
Mn- Manganese
mgll
NI - Nickel
mg/l
ORGANICS: (by GC, GC/MS,
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #,
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:. moll ,Effluent Total VOCs: mall.' VOC Removal%
Martin Griess, Plant Manager
Permlllee (or Authorized Agent) Name and'Ple - Please print or tvpe
GW-59 Rev. 1/2007
at
of

:R QUALITY MONITORING:
REPORT FORM
Name: Allens, Inc. -Turkey
Name (if different):
Address: 5900 Turkey Highway
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
- feo P milli
PLING INFORMATION
L ID NUMBER (from Permit): R-5a Date sample collected: 1118/10:..
Depth: ft. Well Diameter. In.
i to Water Level: 5.10 ft, below measuring point Sueened Interval: ft. to ft.
uring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons'
iRMIT Number:
Explratlob Date: July 31, 2015
o-Discharge WQ0004268
UIC
)DES
Other'
'PE OF PERMITTED OPERATION BEING MONITORED
0 Lagoon
❑ Remediatlon: Infiltratlon Gallery
Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other.,
FIELD ANALYSES:
pH 4.43 units Temp. 20 eC
Spec. Cord. .µMhos
Odor
Appearance
t sample analyzed:
Laboratory Name: Microbae Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
97.5 mgA
Nitrite(NO2)as
mgA
Pb - Lead .mgA
Collform: MF Fecal
/100m1
Nitrate (NO3) as N
13.1 mg/I
Zn - Zinc mgA
Collform: MF Total
1100ml
Phosphorus: Total as P
mgA
(Nate: Use MPN trained forN9Ny habld samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
108 mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOC
2.5 mg/I
Ca - Calcium
mg/I
Chloride
16.9 mg/I
Cd- Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu. Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mgA
Fe - Iron
- mgA
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
20 mg/i
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
213 µMhos
K- Potassium
mgA
VOC ,method#
Total Ammonia
mg/I
Mg - Magnesium
mgA
,method #
(AmrtmNa NIVaaen; NHsea N; Ammonia Nivogen, Tow)
Mn- Manganese
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
rur numoulanon oysitems Amy tAuacn i-annepons): Imluent 1 otal vuGs: mg/L.. Effluent Total VOCs: mq/L , VOC Removal
Martin Griess, Plant Manager
Permitlee (or AVlhodud Agent) Name and Title •Please vdnl or type
GW-59 Rev. 112007
at
Of
J

QUALITY MONITORING:
Name: Aliens, Inc. - I UrKey
Name (if different):
Address: 5900 Turkey Highway
!y ""`°" NC 28393-9703
County Sampson
act Person: Martin Griess Telephone#: [phone].
Location/Site Name: No. of wells to be samoled: ......
Number: Exl
haige WQ0004268
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediatlon: Infiltration Gallery
9 Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑Other:._
LID NUMBER (from Permit): R-6 Date sample collected: 11/8/10* FIELD ANALYSES:
Depth: ft. Well Diameter: In. pH 5.71 units
h to Water Level: 7.30 ft. below measuring point Screened Interval: _ft. to —ft. Spec. Cond. _
luring Paint Is ft, above land surface Relative M.P. Elevation: ".ft. Odor
Tie of water pumped/bailed before sampling: 10+gallons Appearance _
Dies for metals were collected unfiltered: ❑YES ..❑ NO and field acidified:.,. DYES -, -❑ NO .
sample analyzed: Laboratory Name: Mlcrobac'Lab"oratories
AMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
Temp. 21 °C
Certification No. NC#11 NC#37714
COD 72.9 mg/I -
Nitrite (NO2) as N
mg/I
Pb - Lead m9 /l
Coliform: MF Fecal 1100ml
Nitrate (NO3) as N
2.10 mg/I
Zn - Zinc mg/I
Coliform: MF Total 1100ml
Phosphorus: Total as P
- mg/I
(Note: Use MPN method far NQNr hubid eemplee)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
131 mgA
pH (when analyzed)
units
TOC
11.9 mgll
Chloride
27.2 mgll
Arsenic
mgA
Grease and Oils
Phenol
Sulfate 21 mg/I
Specific Conductance 213 pMhos
Total Ammonia mg/I
(Ammallo Nitrogen; NHe as N; AsmoNe Nitrogen, Total)
TKN as N mg/I
At - Aluminum
Ba- Barium
mgA
Ca - Calcium
mg/I
Cd- Cadmium
mgA
Chromium: Total
mgA
Cu- Copper
mgll
Fe - Iron
mgA
Hg - Mercury
mgA
K- Potassium
mg/I
Mg - Magnesium
. mgA
Mn - Manganese
mgA
Ni- Nickel
moll
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
ReportAttached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #:
method #'
at
of
For Remediatlon Systems Only (Attach Lab Reports): Influent Total VOCs: .In __ ,Effluent Total VOCs: mg/L % VOC Removal°% _
Martin Griess, Plant Manager
Pennines (or Authodzet Apenn Name analTitle-Please print ortype
GW-59 Rev.112007

TER QUALITY MONITORING:
E REPORT FORM
ity Name: Aliens, Inc. - Turkey
tit Name (if different):
ityAddress: 5900 Turkey Highway
key """0 NC 28393-9703 County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to. be sampled:
Number. Expiration Date:
harge WQ0004268 UIC
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
K Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
L ID NUMBER (from Permit): R-7
Date sample collected: 11/81.10
FIELD ANALYSES:
WAS
Depth: ft.
Well Diameter. —in.
pH 4.67 units Temp.
19 °C
DRY at
h to Water Level: 4.11 ft, below measuring point
Screened Interval: to _fi.
Spec. Cord.
ItMhos
time of
;wring Point is ft. above land surface
_ft.
Relative M.P. Elevation: ft.
Odor
samplin
no of water um ed/bailed before sampling:
P P p g:
10+ gallons
-
Appearance
check
here:
for metals were collected unfiltered: ❑YES
ORATORY INFORMATION
. ❑ NO and field acidified: ❑YES ❑ NO
L
sample analyzed:
LaboratoryName: Microbac Laboratorles
Certification No.
NC#11 NC#37714
4METERS NOTE: Values should reflect dissolved and colloidal concentratlons.
COD 49.8 mg/I
Nitrite (NO3) as N mgn
Pb - Lead
mgn
Colifonn: MF Fecal 1100ml
Nitrate (NO3) as N 2.29 mgn
Zn - Zinc
mgn
Coliform: MF Total /loom]
INole: NSe MPN mae,a,I fir M1InM1N M1nAIA..m.l.a
Phosphorus: Total as P mg/I
Dissolved Solids: Total
78.0 mg/1
pH (when analyzed)
units
TOC
8.8 mg/I
Chloride
20.7 mg/I
Arsenic mg/l
Grease and Oils
mg/l
Phenol
mg/I
Sulfate
10 mg/I
Specific Conductance
147 µMhos
Total Ammonia
mg/I
(Ammon. Nitragan: NHraa N; AmmaNe
Nitrogen, Toter
TKN as N
mall
Martin Gress, Plant Manager
Permltoe (ar Authorhaid Agent) Name and Title- Please print or type
GW-59 Rev. V2007
Orthophosphate
mg/I
AI - Aluminum
mgn
Be - Barium
mg/I
Ca - Calcium
mg/I
Cd- Cadmium
mg/I
Chromium: Total
mgn
Cu- Copper
mg/I
Fe - Iron
mgn
Hg - Mercury
- mgn
K- Potassium
mg/I
Mg - Magnesium
mgll
Mn- Manganese
mg/I
Ni- Nickel
ma/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method A ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
nl,n,onl I Wdl vws. mgn, emuent 1 otal VUcs: mglL . VOC Removal°%_

UNL7
QUALITY MONITORING:
PORT FORM
Name: Allens, Inc. - Turkey
Name (if different):
Address:
NC
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
L ID NUMBER (from Permit): R-8 Date sample collected: 1118110
Depth: ft. Well Diameter: in.
h to Water Level: 8.50 ft. below measuring point Screened Interval: ft. to ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
Number: Expiration
harge W00004268 UIC
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediatlon: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES: IWAS
PH 4.23 units Temp. 22 eC DRY at
Spec. Cond. µMhos time of
Odor samplir
check
Appearance here:(—
tmple analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
DETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 33.5 mgA
Ndrlte (NO,) as N
mg/I
Pb - Lead mgA
Coliform: MF Fecal /looml
Nitrate (1,103) as N
28.9 mg/I
Zn - Zinc moll
Coliform: MF Total /loom[
Phosphorus: Total as P
mg/I
(Nate: free MPN melhed for hlatJy habidaampNQ
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
221 mg/I
pH (when analyzed)
units
TOC
0.9 mg/I
Chloride
21.2 mg/I
Arsenic
mg/I
Grease and Oils
rno/I
Phenol
mgll
Sulfate
13 mg/I
Specific Conductance
358 µMhos
Total Ammonia
mg/l
(Pmmonla Nine,, NH,.. N: AmmaNe
Niboaen. Tota11
TKN as N mg/I
At - Aluminum
Be - Barium
mg/I
Ca - Calcium
mg/I
Cd- Cadmium
mgA
Chromium: Total
mgA
Cu- Copper
mg/I
Fe - Iron
mgA
Hg - Mercury
mg/I
K- Potassium
mg/I
Mg - Magnesium
mgA
Mn - Manganese
mg/I
Ni- Nickel
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method A ATTACH LAB REPORT.)
Report Attached? ❑ Yes-(1) ❑ No (0)
VOC , method s#
method #
method #
method #
ror numuaianon oysrems umy fAuacn Lao Keportsl: Influent Total VOCs: _ mg/L . Effluent Total VOCs: mgA. VOC Removal%
Martin Griess, Plant Manager
Perrnlltee (or Authorized Agent) Name and Tllle- Please print or type
GW-50 Rev, 112007

QUALITY
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
IY ``""' NC 28393-9703 County Sampson
act Person: Martin Gress Telephone#: 910=596-0026 I
Location/Site Name: No. of wells to be sampled:,__ P 11
PLING INFORMATION
L ID NUMBER (from Permit): R-9 Date sample collected: 11/8110
Depth: ft. Well Diameter: in,
h to Water Level: 7.90 ft. below measuring point Screened Interval: ft. to ft.
;wring Point is ft. above land surface Relative M.P. Elevation: _ ft.
Tie of water pumped/bailed before sampling: 10+ gallons
COD 80.7 mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total 1100ml
(Nate: Uw MPN methnd(or Nghly nm,14 sample.)
Dissolved Solids: Total
176 mgll
PH (when analyzed)
units
TOG
3.4 mgn
Chloride
12.4 mgll
Arsenic mgn
Grease and Oils mg/I
Phenol ma/I
Sulfate 51 mg/I
Specific Conductance - 272 µMhos
Total Ammonia mgn
(Ammonle Nllmyen; NHses N; A *Ns Nllmaen. Tolao
TKN as N moll
Martin Griess, Plant Manager
Pemlltlee (or Aulhodzed Alien 1) Name and Mile - Please pdnl or type
GW-59 Rev. V2007
WQ0004268
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedialion: Infiltration Gallery
® Spray Field ❑ Remedialion:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heal Pump ❑ Other:
FIELD ANALYSES:
PH 4.26 units Temp. 20 `C
Spec. Cond. µMhos
Odor
Appearance
Laboratory Name:. Mlcrobad.Laboratodes - Certification No. NC#11 NC#37714
colloidal: concentrations:
Nitrite (NO,) as N, � mg/I Pb - Lead mg/I
Nitrate (NO3) as N 15.1 mg/I Zn - Zinc mg/I
Phosphorus: Total as P mg/I
Orthophosphate
mg/I
AI - Aluminum
mg/I
Be - Badum
mg/I
Ca - Calcium
mg/I
Cd-_Cadmium
mgll
Chromium: Total
mg1I
Cu- Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
_mg/I
K- Potassium
mgA
Mg - Magnesium
mg/I
Mn- Manganese
mg/I
Ni - Nickel
mo/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
ld
at
of

ONLY
ROUNDWATER QUALITY MONITORING:
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
Y (S,w) NC 28393=9703 County Sampson
act Person: Martin Guess Telephone#: [phone] I
Location/Site Name: No. of wells to be sampled:
(fro P nN 1
FLING INFORMATION
L ID NUMBER (from Permit): MW-1 Date sample collected: 11/8110
Depth: ft. Well Diameter: in.
h to Water Level: 24.6 ft. below measuring point Screened Interval: _ft. to _ft.
luring Point Is ft. above land surface Relative M.P. Elevation: ft.
lie of water pumped/bailed before sampling: 10+ gallons
Number: Expiration Date:
Marge WQ0004268 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedialion: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES: [WAS
pH 4.61 units Temp. 24 °C DRY at
Spec. Cond. .µMhos time of
Odor sampling,
check
Appearance - here: ❑
) sample analyzed: Laboratory Name: Microbac Laboratories
WMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 39.6 mg/I Nitiite.(NOZ) as N mg/I Pb - Lead
Coliform: MF Fecal 1100ml Nltrate (NOj) as N 8.18 .mg/I Zn - Zinc
Certification No. NC#11 NC#37714
mg/I
mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
570 mg/I
AI - Aluminum
mgll
pH (when analyzed)
units
Be - Barium
milli
_
' TOC
4.3 mgn
Ca - Calcium
mg/I
Chloride
98.7 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Capper
mg/I
ORGANICS: (by GC, GC1MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
210 mg/i
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
1000 µMhos
K.- Potassium
mg/I
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium'
mg/I
, method #
(Ammonia Nmooen; NH, as N; Ammonla Nitrogen, Total(
Mn - Manganese
mg/I
, method #
TKN as N
mg/I
NI - Nickel
mg/I
, method #,
For Remedlatlon Systems Only (Attach Lab Reports):.
_ Influent Total VOCs:
mg/L. Effluent Total VOCs: mg/L, VOC Removal%
Martin
or type
GW-89 Rev. 112007

QUALITY MONITORING:
(PORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address:
County Sampson
act Person: Martin Griess Telephone#: 910-596=0028 I
Location/Site Name: No, of wells to besampled:
feo P 'a
PILING INFORMATION
LID NUMBER (from Permit): MW-2 f Date sample collected: 1.116110' -
Depth: ft. Well Diameter: in.
h to Water Level: 8.60 ft. below measuring point Screened Intervalr_ft. to —ft.
luring Point Is ft. above land surface Relative M.P. Elevation: ff.
ne of water pumped/balled before sampling: 10+ gallons
Number: Expiration Date:
harge WQ0004268 UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedlation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land;Application of Sludge
❑ Water Source Heat Pump ❑ Other: _
FIELD ANALYSES: Z WAS
pH 5.41 units Temp. 19 oC DRY at
Spec. Cond. µMhos time of
sampling,
Odor _ check
Appearance here: ❑
ample analyzed: Laboratory Name: Microbac. Laboratories Certification No. NC#11 NC#37714
METERS NOTE: Values should reflect dissolved and colloidal concentrations. ..
COD 37.7 mgll Nitrite (NO2) as N mg/I Pb - Lead mg/I
Coliform: MF Fecal /100ml Nitrate (NO3) as N 2;02 mg/1 Zn - Zinc , mg/I
Coliform: MF Total /100ml Phosphorus: Total as P mg/I
(Note: Use MPN method for hlahly Nrbld samples) Orthophosphate_ mo/I Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
209 ni
pH (when analyzed)
units
TOC
2.3 mg/i
Chloride
11.7 mgA
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/l
Sulfate
8.1 mg/I
Specific Conductance
427 µMhos
Total Ammonia
mgA
(Ammunla Nitrogen; 14%as N; A
NitNltmgen, Total)
TKN as N ri
For Remedlation Systems
Martin Griess, Plant Manager
Pennittes (er Authorized Agent) Name and Title - Please print or type '
GW-59 Rev. 112007
AI - Aluminum
.mgA
Be - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
moll
Chromium: Total
mg/I
Cu- Copper
mgPo
Fe - Iron
mg/I
Hg - Mercury
mg/I
K- Potassium
mgll
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
NI - Nickel
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #,
method #

ON
DWATER QUALITY MONITORING:
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkev Hiahwav
County Sampson
act Person: Martin Griess Telephone#: [phone] I
Location/Site Name: No, of wells to be sampled:
If P ')
PLING INFORMATION
LID NUMBER (from Permit): MW-3 - Date sample collected: 11/8/10
Depth: ft. Well Diameter: _in,
i to Water Level: 3.90 ft. below measuring point Screened Interval: —ft. to —ft.
uring Point is ft. above land surface Relative M.P. Elevation:
ne of water pumped/bailed before sampling: _ 10+ gallons
COD 34.5 mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
306 mg/I
pH (when analyzed)
units
TOC
0.8 mgA
Chloride
9.02 mg/I
Arsenic
mg/I
Grease and Oils
mg/l
- Phenol
mg/I
Sulfate
60 mg/I
Specific Conductance
415 µMhos
TotalAmmonia -
mg/I
(Ammonle Nitrogen; NH, as N; Ammonia
Nitrogen, Total)
c
TKN as N
ma/1
:RMIT Number: . Expiration Date: July 31, 2015
n-Discharge WQ0004268 UIC
IDES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedlation: Infiltration Gallery
® Spray Field ❑ Remedlation:
❑ Rotary Distributor ❑ Land''Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES: WAS
pH 5.91 units Temp. 19 oC DRY at
Spec. Cond. µMhos time of
Odor sampling,
check
Appearance here: ❑
Laboratory Name: Microbac.Laboratories
Certification No. NC#11 NC#37714
colloidal concentrations.
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Nitrate (NOp) as N
2.03 mgll
Zn - Zinc mg/I
Phosphorus: Total as P
mgll
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
AI -Aluminum _
mgn
Be - Barium
mg/I
Ca - Calcium
mg/1
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mgA
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron
mg/I
(specify test and method A ATTACH LAB REPORT.)
Hg - Mercury
mgA
Report Attached? ❑ Yes (1) ❑ No (0)
K- Potassium
mg/I
VOC , method #i
Mg - Magnesium
mg/1
, method #,
Mn - Manganese
mgll
, method #,.
Ni - Nickel
mg/l
_ , method #
..,,,y n I; uuwem I oval vUcs: mg/L etiluent Total VOCs: mg/L; VOC Removal%
Martin Griess, Plant Manager
PermlIts (orAuthorized Apem)Name and Title- Please print or type
GW59 Rev.112007

SUBMIT
ER QUALITY MONITORING:
REPORT FORM
Name: Aliens
Name (if different):
Address: 59001
County Sarripson
act Person: Martin Griess Telephone#: [phone],
Location/Site Name: No. of wells to be sampled:
10
M W-4
Depth: ft.
i to Water Level: 4.10 ft. below measuring point
luring Point Is ft. above land surface
ne of water pumped/bailed before sampling:.
sample
COD
34.4 mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
/100ml
(Note: Use MPN method for Nghly turbid samples)
Dissolved Solids: Total
74.0 mg/I
PH (when analyzed)
units
TOC
<0.5. mg/I
Chloride
11.1 mg/I
Arsenic
_ mg/I
Grease and Oils -
- mg/I
Phenol
mg/I
Sulfate
3.0 mg/I
Specific Conductance
149:µMhos
Total Ammonia _
mg/I
(Ammonia Nitrogen; Wise N; Ammania Nitrogen, Total)
TKN as
0+
Date:
. WQ0004268
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon . ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediatlon:
❑ Rotary Distributor ❑ Land'Application of Sludge
❑ Water Source Heat Pump ❑ Other:
Date sample collected: 11/8/10-.
FIELD ANALYSES: -Wj
Well Diameter. _in.
pH 4.25units Temp.
22°C
OF
Screened Interval: _ft.
to _ft.
Spec. Cond. -!
µMhos
fim
Relalive'M:P.Elevation:.,.
. ft. -
Odor
sal
chi
)allons
Appearance
he
JO and field acidified: ❑ YES
❑ NO
Laboratory Name: MicrobacCaboratories
Certification No.
NC#11 NC#37714
colloidal concentrations.
Nitrite (NO2Jas N
mg/I
Pb - Lead
mg/I
Nitrate (NO3) as N
10.0 mg/I
Zn - Zinc
mg/I
Phosphorus: Total as P
mg/l
Orthophosphate
'mg/I
Other (Specify Compounds and Concentration Units):
AI - Aluminum
mg/I
Be - Barium
mg/l
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/l
Hg- Mercury
.. mg/1
_
K-Potassium_
`-mg/l
Mg - Magnesium
mg/I
Mn- Manganese
mg/I
Ni - Nickel
mg/I
ORGANICS: (by GC,. GC/MS, HPLC)
-(Specify test and method M ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method
method #i
method #
method #,.
For Remediation Systems Only (Attach Lab.Reports): : Influent TotaI,-VOCs; ' mg/L Effluent Total;VCCs:.. .` mg/L)_ VOC Removal°/a
Martin Griess, Plant Manager
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59. Rev, 112007 _
at
of
INS

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc
Mr. Martin Griess Project: M/Wells samples-3/Yearly Date Reported: November 30,2010
5900 Turkey Highway Date Received: November 08. 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: November 08.2010
Mw #1
1011177-01
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: Microbac - Fayetteville
Division
Chloride
98.7
ni
11/9/10 10:36
TDA
EPA 300.0
B
COD, Total
39:6
mg/L
1119110 14:20
ARS
SM 20th Ed. 5220 D
A4
Conductivity
1000
umhos/cm
11/15/10 16:00
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
24.6
feet
11/8/10 18:45
RDM
Field Measurement
Nitrate as N
8.18
mg/L
11/9/10 10:36
TDA
EPA 300.0
PH, Field Test
4.61
pH Units
11/8/10 18:45
RDM
—Field
Total Dissolved Solids
570
mg/L
11/9/10 14:30
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
210
mg/L
1119110 1036
TDA
EPA 300.0
A 12
Temperature
24
aC
11/8110 18:45
RDM
Field
Mw #2
1011177-02
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: Microbac - Fayetteville Division
Chloride
11.7
mg/L
11/9/10 10:36
TDA
EPA 300.0
B
COD, Total
37.7
mg/L
11-19/10 14:20
ARS
SM 20th Ed. 5220 D
A4
Conductivity
427
umhos/cm
11/15/10 16:00
ARS -
SM 20th Ed. 2510 B
Depth to Water Surface
8.60
feet
11/8/10 12:05
RDM
Field Measurement
Nitrate as N
2.02
mg/L
11/9/10 10:36
TDA
EPA 300.0
PH, Field Test
5.41
IiH Units
11/8/10 12:05
RDM
Field
Total Dissolved Solids
209
ni
11/9/10 14:30
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
8.1
mg/L
11/9/10 10:36
TDA
EPA 300.0
Temperature
19
aC
1118/10 12:05
ROM
Field
Mw #3
1011177-03
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: Mlaobac - Fayetteville Division
Chloride
9.02
ing/L
11/9/10 10:36
TDA
EPA 300.0
B
State Certifications:
Respectfully Submitted
NCDNR #11
NCDOH #37714
tu- iv_
USDA #3787
R. W. Sanders, VP/Manaaino Director
Thank you for your business. We•inrim rmmfirr/hnc'k nn
mar ln•ehfrerrin rn/nn. Pleacernnt.. the l'Ph/vnagirg
Uirxnnr, Ron Smrdecr al'Jf0.yl.{.I yZn„/rrnrea Nakep Pre knr,nl
Pnd,V....u. borc'e. CrU m rbnP¢Lbuirrubar.eom vvirR aqr cumuuntr' nr.vu uxrimrr.
Page I of 3

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.364.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Allens. Inc
Mr. Marlin Griess Date Reported: November 30, 2010
Project: M/Wells samples-3/Yearly 5900 Turkey Highway Dale Received: November08,2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: November 08,2010
Mw #3
1011177-03
Analyte
Result
Unit
Analysis Date/Time
Analyst
. Method Qualifier
Analyzed by: Microbac - Fayetteville Division
-
COD, Total
34.5
mg/L,
11/9/10
14:20
ARS
SM 20th Ed. 5220 D A4
Conductivity
415
umhos/cm
11/15/10
16:00
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
3.90
feet
I1/8/10
12:40
RDM
Field Measurement
Nitrate as N
2.03
mg/L
11/9/10
10:36
TDA
EPA 300.0
pH, Field Test
5.91
pH Units
11/8/10
12:40
RDM
Field
Total Dissolved Solids
306.
mg/L
l 119/10
14:30
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
60
mg/L
I1/9/10
10:36
TDA
EPA 300.0
Temperature
19
°C
I1/8/10
12:40
RDM
Field
Mw #4
1011177-04
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
Chloride
11.1
mg/L
11/9/10
10:36
TDA
EPA 300.0 B
COD, Total
34.4
mg/L
11/9/10
14:20
ARS
SM 20th Ed. 5220 D A4
Conductivity
149
unahos/cm
11/15/10
16:00
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
4.10
feet
I I/8/10
13:15
RDM
Field Measurement
Nitrate asN
10.0
mg/L
11/9/10
10:36
TDA
EPA 300.0
pH, Field Test
4.25
pH Units
11/8/10
13:15
RDM
Field
Total Dissolved Solids
74.0
mg/L
11/9/10
14:30
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
3.0
mg/L
11/9/10
10:36
TDA
EPA 300.0 -
Temperature
22
°C
11/8/10
13:15
RDM
Field
Slate Certifications: Respectfully Submitted
NCDNR #11
NCDOH #37714 6V- W- + �
USDA #3787 R. W. Sanders, VP/Managing Director
Thank you for your business. We• im•ire ywrrfmdback nn nnr level aJ.vervice m ymr. Pleene coulacl lire IT Alunaging Direcmq Ran Sunckrx of 910404-19211. James Nnkex Prc ir4•nr.
jnnkcrQmiertrhae.2nm nr %'revnr Bnyx'¢, CGO, m rhnyxcQmilruhnernm u•ilb ony cnnun¢uty nr.vrggeninnr'. Page 2 of',

Fayetteville Division
2592 Hope Mills Rd
Fayetteville,NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens. Inc
Mr. Martin Griess Date Reported: November 30,.2010
Project: M/Wells samples=3/Yearly
5900 Turkey Highway Date Received: November 08, 2010
Turkey NC. 28393 - Sampled By: Robin Miller DW Sampled: November 08, 2010
Qualifier Definitions
I
B Detected in the associated Method Blank
A4 CCV was outside acceptance limits. Data is valid but qualified.
Alt MS/MSD fail recovery, but the LCS passes criteria.
State Certifications: Respectfully Submitted
NCDNR #11
NCDOH #37714 f.>_ W_ Zmoi Siena.
USDA #3787 R. W. Sanders, W/Minasing Director
Thank you for your business. We invite• wnr ficJback nn my level ofevmice tn)vnl. Vfeare enntn<t Jre r'VMmraging lJlreemq Rnn Snnders al Ylf/-RGJ-/J20, Jnmea NoAeq Prxxidunl, nt
Jnnkcrlamicmhac. cone nr''l'rvvar Hmrc•, CLO, or rhny'ce nmicrnbvc.cnm or suggestions. Page 3 of 3

Environmental Chemists, Inc.
6602 Windmill Way - Wilmington, NC28405-
?
[phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL &CONSULTING
[phone]
- CHEMISTS
NCDENR: DWQ CERTIFICATE 094. DLS CERTIFICATE #37729
Microbac Laboratories - Fayetteville
Date of Report: Nov 19, 2010
2592 Hope Mills Road
Customer PO #:
Fayetteville NC 28306
Report #: 2010-11358
Attention: Bonnie Sanders
Report to: Bonnie Sanders
ProjectlD: 1011177
Lab ID Sample ID:
Collect Datelrime Matrix Sampled by
10-28597 Site: 1011177-01
11/8/2010 11:45 AM Water Client
Test
Method Results Date Analyzed
Total Organic Carbon (TOC)
SM 5310 B
4.3 mg/L 11/16/2010
Lab ID Sample ID:
_Collect Date/Time
Matrix Sampled by
10-28598 Site:1011177-02
11/8/2010 12:05 PM
Water Client
Test
Method
Results 'Date Analyzed
Total Organic Carbon (TOC)
SM 5310 B
2.3 mg/L 1111612010
Lab ID Sample ID:
Collect Daterrime
Matrix Sampled by
10-28599 Site: 1011177-03
11/8/2010 12:40 PM
Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
SM 5310 B
0.8 mg/L 11/16/2010
Lab ID Sample ID:
Collect Datelrime
Matrix Sampled by
10-28600 Site:1011177-04
11/8/2010 1:15 PM
Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
SM 5310 B
<0.5 mg/L 11/16/2010
Comment:
Reviewed by:
/7
Report #.:- 2010-11358 Page 1 of i

,local)
MONITORING:
Name: Aliens,Inc.-Turkey
Name (if different): _
Address: 5900 Turkev Hiqhwav
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to be samoted
Date:
W00004268
rPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
ELL ID NUMBER (from Permit): R-14a
Date samplecollecled:i 11/8/10 �:,,:
FIELD ANALYSES:
If WELL
WAS
Well Depth: ft.
Well Diameter: . in.
pH 5.28 units
Temp. 20 aC
DRY at
Depth to Water Level: 4.11 ft. below measuring point
Screened Interval: _ft. - to ft.
Spec. Cond.
'µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
,-
sampling,
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
i
check
here:
Samples for metals were collected unfiltered: ❑YES
LABORATORY INFORMATION
❑ NO andfield ack ified:. ❑YES. ..❑.NO
❑
Date sample analyzed:
Laboratory Name:-MicrobaD L•aboratorles
"
Certification No. NC#11-NC#37714
PARAMETERS NOTE: Values should reflect dissolved'and colloidal concentrations.
COD 62 1
Kn.• k -
6 mg/ {N oteOz) as N mg/I Pb - Lead mg/I
Coliform: MF Fecal /100ml Nitrate (NO3) as N 2.41 mg/I Zn - Zinc mg/I
Coliform: MF Total /100ml
(Now, use MPN method for highly lurhid samples)
Dissolved Solids: Total
46.0 mg/I
pH (when analyzed)
units
TOC
2.7 mgn
Chloride
10.4 mg/I
Arsenic
mg/I.
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
15 mg/I
Specific Conductance
84.4 µMhos
TotalAmmonia
mg/I'
(Ammanla Nitrogen; NH, as N; Ammonia
Nitmgen• Total)
TKN as N
. mall
Phosphorus: Total as P
rur �wP�. wr• ,,,,,.DILL
Orthophosphate
mg/I
AI - Aluminum
mg/I
Be - Barium
- _.mgn
Ca - Calcium
-`.-mg/l
Cd - Cadmium
`"'•mg/l
Chromium: Total
mg/I
Cu - Copper
mg/I
- Fe -Iron
mg/I
Hg - Mercury
mg/I
K- Potassium
mg/I
Mg - Magnesium
mg/I
Mn- Manganese
mg/I
Ni - Nickel
-mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
tanuent i oral
method #
method #
method #
VOC Removal%
Martin Griess, Plant Manager
Fe ia..(or Authorized Agent)Name and Title- Please print or type Signature o1 Penmities (or Authorized Agent) (Date)
GW-59 Rev. 112007

oucarva l rVRrvl UN yr L Lv rAr=K UNLT
r EPARTMENT OF:ENVIRONMENT B NATURAL. RESOURCES '
TER QUALITY MONITORING: e r VISION OF WATER QUALITY.INFORMATIONIPROCESSING UNIT
c 000ner rneur r ,:_ _.
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
(Street) )y _ NC 28393-9703 county Sampson
act Person: Martin Griess Telephone#: [phone]
Locatlon/Site Name: No. of wells to be sampled:
LID NUMBER (from Permit); R-2a Date sample collected: 11/8/10
Depth: ft. Well Diameter: _in.
h to Water Level: 4.11 @, below measuring point - Screened Interval: _ft. to —ft.
luring Point Is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/balled before sampling: 10+ gallons
fRMIT Number: Expirat(on Date: July 31, 2016
in -Discharge WQ0004268 UIO
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedlation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH 4.64 units Temp. 19 oC
Spec. Cond. µMhos
Odor
Appearance
f sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
'
COD
74.9 mg/I
Nitrite (NO,) as N -
mg/I
Pb - Lead mg/1
Coliform: MF Fecal
/100ml
Nitrate (NOa) as N
2,06mg/1
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mg/I
'
(Note: Use MPN method for highly lurhld eamplee)
Orthophosphate
mgll
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
90.0mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOC
1.0 mg/I
Ca - Calcium _
mg/I
Chloride
14.2 mg/I
Cd - Cadmium
mg/1
Arsenic
mg/I
Chromium: Total
mgll
Grease and Oils
mg/l
Cu - Copper
mgll
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/l
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
48 mg/I
Hg - Mercury
mg/l
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
232 µMhos
K- Potassium
mg/I
VOC , method #
Total Ammonia
mg/l
Mg - Magnesium
mg/I
- ,method #
(Ammonia Nitrogen; NH, as N; AmmoNe Nlirogen, Total)Mn
- Manganese
mg/I
,method#
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
For Remedlatlon
Lab RenorlRle InRuanf Tnfal VrH:e-
Martin Griess, Plant Manager
Penittee (or Authodzed Apent) Name and mile - Please print or type
GW-59 Rev. 1/2007
CRhienf T.JoI \/nn.
VOC Removal%
(Date)
at
of
701

FORM
MONITORING:
Il,I T eYrUMNIA11UIV ..____...... _......y ... ayv ...
ity Name: Aliens, Inc. - Turkey
it Name (if different):
ity Address: 5900 Turkey Highway
key `a"Be0 NC 28393-9703 county Sampson
(city) (Sul.) (zip?
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
IRMIT Number:
Expiration Date: duly 31, 2015
n-Discharge WQ0004266
UIC
IDES
Other'
'PE OF PERMITTED OPERATION BEING MONITORED
El Lagoon
ElRemedeiation: Infiltration Gallery
® Spray Field
❑ Remeillation:
ElRotary Distributor
(
❑ Land Appllcation of Sludge
❑ Water Source Heat Pump
❑ Other:"
L ID NUMBER (from Permit): R-3 Date sample collected: 11/8/10 FIELD ANALYSES:
Depth: fl. Well Diameter; In. pH 5.25 units Temp. 19 -°C
h to Water Level: 6.80 ft. below measuring point Screened Interval: _ft. to _ft. Spec. Cond. 'ftMhos
luring Point Is ft. above land surface Relative M.P. Elevation: ft. Odor
ne of water pumped/bailed before sampling: 10+ gallons Appearance
) sample analyzed:
Laboratory Name: MierobacLaboratories
Certification No.: NC#11 NC#37714
WMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
57.7mg/I
Nitrite (NOg)asN
mg/I
Pb - Lead mg/I
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
2.51 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P -
mg/I
(Note: Use MPN method for highly turbid. samples)
Orthophosphate
_ mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
26.0 mgn
AI - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOD
1.0 mg/l
Ca -Calcium
mgll
Chloride
9.89 mg/I
Cd- Cadmium
_ mg/I.
Arsenic
mg/I
Chromium: Total
mg/i
Grease and Oils
mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC),
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
13 mg/I
Hg -Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance.
72.1µMhos
K- Potassium
mg/I
VOC .,method#,
Total Ammonia
mg/I
Mg - Magnesium
mg/I
, method #
(Anw°nla Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method # i.
vut:
Martin Griess, Plant Manager
Permlttee(or Authorized Anent)Name and Title- Please print or type
GW-59 Rev. 1/2007
at
Of

SUBMIT FORM ONYELLOW PAPER ONLY
• .
DEPARTMENT OF ENVIRONMENT & NATURAL'AESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION 00 WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
7
1617 MAIL SERVICE QENTER, RALEIGH, NC 27699 161T; Phone: [phone];',"
Please Print Clearly or Type - ""
FACILITY INFORMATION �
- '`-
PERMIT Number: ExpiratioriDate: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
Non -Discharge WQ0004268 UICi
NPDES Otherl
Permit Name (If different): -....
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
Turkey (st`eq NC 28393-9703 County;Sampson
❑ Lagoon ❑Remediation:Infiltration Gallery
(0rh (Slate) (zip) 1
® Spray Field ❑Remediation:
Contact Person: Martin GrIeSS
Telephone#: [phone]
❑Rotary Distributor ❑Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled::
"
❑ Water Source Heat Pump ❑ Otherj `
rrom PemN
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-4
Date sample collected: 11181'TO
` FIELD ANALYSES: '.
WAS
Well Depth: ft.
Well Diameter:
pH 4.50 units Temp. ` 20 eC
DRY at
Depth to Water Level: 7.40 ft. below measuring point
_In.
Screened Interval: _ft.
to _ft.
Spec. Cond. ;µMhos
.
time of
sampling,
Measuring Point Is ft. above land surface
RelativeM.P. Elevation:
-ft.
Odor
check
Volume of water pumped/balled before sampling:
10+gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
El NO and field acidified: ❑ YES "
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbaci-aboratcries Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentratlons.
COD 33.5 mg/l
Nitrite (NO,) as N
- mgll
Pb - Lead mg/1
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
5.48.111911
Zn - Zinc - mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Nate; Use MPN method for highly takid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 53.0mg/I
AI -Aluminum
mg/I
'
pH (when analyzed).. units
Be - Barium _
mg/l
TOC 0.8 mg/I
Ca - Calcium
mg/I
Chloride 7.90 mg/1
Cd - Cadmium
Mgt[
Arsenic mgA
Chromium: Total
mgll
Grease and Oils mgll
Cu - Copper
mgll
ORGANICS: (by GC, GC/MS,.HPLC)
Phenol mg/I
Fe - Iron
- mgtl
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 12 mg/I
Hg - Mercury,
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 97A µMhos
K- Potassium
mg/I
VOC , method #
' Total Ammonia mg/I
Mg - Magnesium
mg11
, method #
(Ammonla Nitrogen; NHsas N; Ammonia Nitrogen, Total)
Mn-'Manganese
mg/I
,method #:
TKN as N mg/I
Ni - Nickel
mg/I
method #
For Remediatlon Systems Only (Attach Lab Reports): Influent Total VOCs: " mg/LEffluent Total VOCs: mg/L ; VOC Removal%
Martin Griess, Plant Manager
Parrattee(or Authorized Anent)Name and Title- Please print or type
GW-59 Rev. 112007

Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc
Mr.. Martin Griess Project: M/Wells samples - 3/Yearly Date Reported: November 30, 2010
5900 Turkey Highway Date Received: November 08.2010
Turkey NC. 28393 Sampled By:. Robin Miller Date Sampled: November 08, 2010
R-1
I011178-01
I Analyte Result Unit Analysis Date/Time Analyst Method Qualifier I
Chloride
10.4
mg/L
COD, Total
62.6
mg/L
Conductivity
84.4
umhos/cm
Depth to Water Surface
4.11
feet
Nitrate as N
2.41
mg/L
pH, Field Test
5.28.
pH Units
Total Dissolved Solids
46.0
mg/L
Sulfate as SO4
15
mg/L
Temperature
20
oC
11/9110 10:36
11/9/10 14:20
11/15/10 16:00
I1/8/10 15:30
1119110 10:36
11/8/10 15:30
11/9/10 14:30
11/9110 10:36
11/8/10 15:30
R-2x
1011178-02
TDA
EPA 300.0
ARS
SM 20th Ed. 5220 D
ARS
SM 20th Ed. 2510 B
RDM
Field Measurement
TDA
EPA 300.0 .
RDM
Field
AMM
SM 20th Ed. 2540 C
TDA
EPA 300.0
RUM
Field
B
A4
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier I
Chloride
14.2
mg/L
.COD, Total
74.9
mg/L
Conductivity
232
umhos/cm
Depth to Water Surface
4.11
feet
Nitrate as N
2.06
mg/L
pH, Field Test
4.64
pH Units
Total Dissolved Solids
90.0
mg/L
Sulfate as SO4
48
mg/L
Temperature
19
oC
11/9/10 10:36
11/9/10 14:20
11/15/10 16:00
11/8/10 15:15
11/9110 10:36
11/8/10 15:15
I1/9/10 14:30
11/9/10 10:36
11/8/10 15:15
R-3
1011178-03
TDA
EPA 300.0
ARS
SM 26th Ed. 5220 D
ARS
SM 20th Ed. 2510 B
RDM
Field Measurement
TDA
EPA 300.0
RDM
Field
AMM
SM 20th Ed. 2540 C
TDA
EPA 300.0
ROM
Field
B
A4
Analyte Result - Unit Analysis Date/Time Analyst Method QualifierI
Analyzed by: Kaiibac - Fayetteville Division
Chloride 9.89 mg/L II/9/10 10:36 TDA EPA 300.0 B
State Certifications: Respectfully Submitted
NCDNR #11 .
NCDOH #37714
USDA #3787 R. W. Sandcrs, VP/Managing Director
Thank you for your business. We!titre yourfeedbaci an onr ln•cl ojremler m gnu.. Please contact the FP Managing Director, Ran Sanders of 910464-1920../unrer NoAcr. President, ul
junAea'. @micmhoccnnr ur Trevur B.)-re. CEO. oI IGnyce rt rrrlcrnGoc. mm virh vny cnmmentr nr snggenions. Page l of 3

01
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fae
Certificate of Analysis
Allen, Inc
Mr. Martin Griess Project: M/Wells samples-3/Yearly Date Reported: November 30, 2010
5900 Turkey Highway Date Received: November O8, 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: November O8, 2010
R-3
1011178-03
Analyse
Result
Unit
Analysis, Date/Time
Analyst
Method Qualifier
Analyzed by: Mirzohac - Fayetteville Division
COD, Total
57.7
'mg/L
1119110
14:20
ARS
SM 20th Ed. 5220 D A4
Conductivity
72.1
umhos/cm
11/15/10
16:00
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
6.80
feet
11/8/10
15:00
RDM
Field Measurement
Nitrate as N
2.51
mg/L
1119/10
10:36
TDA
EPA 300.0
pH, Field Test
5.25
pH Units
11/8110
15:00
RDM
Field
Total Dissolved Solids
26.0
mg/L
1119110
14:30
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
13
mg/L
11/9/10
10:36
TDA
EPA 300.0
Temperature
19
°C
11/8/10
15:00
RDM
Field
R-4
1011178-04
Analyte Result Unit Analysis Date/Time Analyst - Method Qualifier
Chloride
7.90
mg/L
11/9/10
10:36
TDA
EPA 300.0 B
COD, Total
33.5
mg/L
11/9/10
14:20
ARS
SM 20th Ed. 5220 D A4
Conductivity
97.4
umhos/cm
11/15/10
16:00
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
7.40
feet
11/8/10
14:50
ROM
Field Measurement
Nitrate as N
5.48
mg/L
11/9/10
10:36
TDA
EPA 300.0
pH, Field Test
4.50
pH Units
11/8/10
14:50
RDM
Field
Total Dissolved Solids
53.0
mg/L
11/9/10
1430
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
12
mg/L
11/9/10
10:36
TDA
EPA 300.0
Temperature
20
°C
II/8/10
14:50
RDM
Field
State Certifications: Respectfully Submitted
NCDNR #11
NCDOH #37714 W- CW- 1&0W6Q&Vb&
USDA #3787 R. W. Sanders, VP/Managing Director
Thank you for your business. WUnlrr Amrrftedhpr
p.A,o.v@..iernbnetcom nr Trcrnr HrHxe. CEO. .NGgr¢r n nrirrnhunenm vilh ony cnrnmenis nrsngg.funrc. Page 2 of 3

0
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens, Inc
Mr. Martin Griess Project: M/Wells samples-3/Yearly Date Reported: November 30. 2010
5900 Turkey Highway Date Received: November O8.2010
Turkey NC, 28393- Sampled By: Robin Miller Date Sampled: November 08, 2010
Qualifier Definitions
B Detected in the associated Method Blank
A4 CCV was outside acceptance limits. Data is valid but qualified.
State Certifications: Respectfully Submitted
NCDNR #11
NCDOH #37714 6u- CW>< �
USDA #3787 R.W. Sanders. VP/Managing Director
Thank you for your business. We niviie ynnrfeedboc'k on onr Ievcl ufservim In ynu. Pleasx contact Ibe IP.A-lanngrog Direcron Ron Sanders or 910-864-19211, Jm Nnkes. Pre.vdwv. of '
jooArv@uWcrnboewio or 7) owr Bek=,.CEO. of lbnycer@ndcroboccnor wish any corn L'O or suggestions. Page of.3
L

Environmental, Chemists, hie.
_s
6602 Windmill Way • Wilmington, NC 28405 _
- _
SM
[phone] (lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL 8 CONSULTING
[phone]
CHEMISTS
NCDENR: DWQ CERTIFICATE #94.. DIS CERTIFICATE #37729
Microbac Laboratories - Fayetteville
Date of Report: Nov 19, 2010
2592 Hope Mills Road
Customer PO #:
Fayetteville NC 28306
Report#: 2010-11357
Attention: Bonnie Sanders
Report to: Bonnie Sanders
ProjectlD: 1011178
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
10-28592 Site:1011178-01
11/8/2010 3:30 PM
Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
SM5310 B
2.7 mg/L 11/16/2010
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
10-28593 Site: 1011178-02
11/8/2010 3:15 PM
Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
SM5310B
1.0 mg/L 11/16/2010
Lab ID Sample ID:
Collect Dateirime
Matrix Sampled by
10-28594 Site: 1011178-03
11/8/2010 3:00 PM
Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon '(TOC)
SM5310B
1.0 mg/L 11/16/2010
Lab ID Sample ID: Collect Daterrime Matrix Sampled by
10-28595 Site: 1011178-04 11/8/2010 2:50 PM Water Client
Test Method Results Date Analyzed
Total Organic Carbon (TOC) SM5310 B 0.8 mg/L 11/16/2010
Comment
Reviewed by:
u
Report#.: 2010-11357 Page 1 of i

For
TER
Name: Aliens, Inc. - Turkey.
Name (if different): _
Address: 5900 Turkey Highway
act Person: Martin`Griess Telephone#:[phone]
Location/Site Name: No::of wellstobe sampled:
WQ0004268
'RE OF PERMITTED OPERATION BEII
❑ Lagoon - ❑ Remi
® Spray Field ❑ Rem,
❑ Rotary Distributor . ❑'Land
❑ Water Source Heat Pump 0 Othe
L ID NUMBER (from Permit): R-5a - Date sample collected: 11/8/10 ' - FIELD ANALYSES:
Depth: ft. - _ "Well Diameter. In. "
Sp 4.. units
h to Water Level: 5.10 ft. below measuring
paint � ScrBened'lnterval: _ft: to —ft. Spec. Cond.
luring Point is ft. above land surface Relative"M.P. Elevation: ft. Odor
ne of water pumped/bailed before sampling: f0+ gallons Appearance
COD ..97.5 mgll
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
108 mg/I
pH (when analyzed)
units
TOG
'2.5 mg/I
Chloride
16:9 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
20 mg/I
Specific Conductance
213 µMhos
Total Ammonia
mg/1
(Ammonla Nitrogen; NHses N; Ammenle
Nihogen, Total)
TKN as N mg/I
Systems Only (Attach LabReport-
Microbac Labdeitories -
Nitrite (NO2) as.N
_ mgn
Nitrate (NO,) as N
.13.1 mg/1
Phosphorus: Total as P
mg/I
Orthophosphate
- mg/I
AI - Aluminum
mg/I
Be - Barium
—Mgt]
be - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mgn
Cu - Copper
mg/I
Fe - Iron
- mg/I
:Hg - Mercury
- mg/I
`K- Potassium
mg/I
Mg - Magnesium
mg/I
Mn- Manganese
mg/I
Ni - Nickel
me/1
Martin Griess,.Plant Manager
Penniftee.(orAUNodzed Agent) Name and Title - Please print or type - slgnature of Permittee (or Al
GW-59 Rev. 112007 -
Date:
MONITORED
Ition: Infiltration Gallery
Temp. 20 QC
IGMhos -
of Sludge
Certification No.,= NC#11 NC#37714
Pb - Lead ,.mg/I
Zn - Zinc ';mg/I
Other (Specify Compounds and Concentration Units):
OR (by GC, GC/MS, HPLC);
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method # s
method #
method #
method #'
at

SUBMIT FORM ONYELI OW PAPER.ONLY
DEPARTMENT .OKENVIRONMENT'&NATURAURESOURCES'� -' - - --q
GROUNDWATER QUALITY MONITORING:
DIVISIONOFWATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCEREPORTFORM
-
fell MAILSERVICE 6ENTER, RALEIGH, NC 27099"1317 Phone;,(819)733.3P21,_q.
FACILITY INFORMATION
Pease Pdnt Cleady or Type
-` ' -
PERMIT Ntintlier: ExpiratioA Date: July 31, 2015
FacilityName: Aliens, Inc. -Turkey
Non=Disctiarrge W00004268 UIC
NPDES - Other?
Permit Name (If different): _ '
Facility Address: 6900Turkey Highway
—
TYPE OF PERMITTED OPERATION BEING MONITORED
❑Lagoon ❑ Remediatlon: Infiltration Gallery
ahe°g
Turkey NC 28393-9703 .County Sampson
ca47
(state) Izrol
® Spray Field ❑ Remedlation:
Contact Person: Martin Griess
Telephone#: [phone]-
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
.. No. of wellstobe sampled:
....
• ❑Water Source Heat Pump ❑ Other:f
-
ham PenNt '.
SAMPLING INFORMATION
_
K WELL .
WELL ID NUMBER (from Permit): R-6
:Date sample collected; 1118/10 -'
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: In.
"pH 5.71 units Temp. 21 °C
DRY at
Depth to Water Level: 7.30 ft. below measuring point
Screened Interval: R.
to
ft., Spec. Cond. ;µMhos
time of
sampling,
Measuring Point Is ft. above land surface
: Relative M.P. Elevation:
.:ft.
Odor
check
Volume ofwater pumped/bailedbefore sampling:
10+:gallons
Appearance
here:
❑
Samples for metals were collected unfiltered: OYES
i❑'NO and field acidified:- ❑YES...
ONO
LABORATORY INFORMATION
Date sample analyzed:
.Laboratory"- Name:' .Microbac:LBboratories Certification No.:-. NC#ll NC#37714
PARAMETERS NOTE: Values should reflect dissolved'and colloidal concentrations.
COD
72.9 mg/I
Nitrite (NO.) as N
mg/I
Pb - Lead .' mgll
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
2A 0 mgll
Zn - Zinc mgl[
Coliform: MF Total
/loom]
Phosphorus: Total as P
mg/l
(Note: Use NIPN method for highly habld samples)
Onhophosphate
- mgll
Other (Specify Compounds .and Concentration Units):
Dissolved Solids: Total
131 mg/I
AI - Aluminum
Mgt]
pH (when analyzed)
units
Be - Barium
mg/I
TOC
11.9 mgn
Ca- Calcium
mg/I
Chloride
27.2 mgll
Cd - Cadmium
mg/l
Arsenic
mg/I
Chromium: Total
mgli
Grease and Oils
mg/I
Cu - Copper
mgli
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
21 mgn
Hg - Mercury
mgn
Report Attached? - ❑ Yes (1) ❑ No (0)
Specific Conductance
213 µMhos
K - Potassium _
mgll
VOC , method #`
Total Ammonia
Mgt]
V Mg - Magnesium
. mglI
, method
(Ammonlo Nllrogen;NH°ao N;Ammonla Nitrogen, Total)
Mn.-Manganese
mg/I
,method#:
TKN as N
mgll
-Nf - Nickel
Mgt]
, method # -
For Remedlatlon Systems Only (Attach Lab Reports): , Influent Total VOCs: 'mg/L, Effluent Total VOCs: mg/L i VOC Removal%
Martin Griess, Plant Manager
Permlltee(or Authorized Agent)Name and Title- Please print or type - _ Ipneture or Permiltee.(a
GW59 Rev. 112007

SNRMIT-FORM ON YECLOW PAPER nNLY,
GROUNDWATER QUALITY MONITORING:
• .
DEP@RTMENTOF ENVIRONMENT& NATURAL'RESOURCES;,?
IVISION OF WATERC4uAu7Y-INFORMAnON-agacesswc UNIT r
COMPLIANCE REPORT FORM
1617',MAIL SERVICE ,CENTER, RALEIGN. NC 27888.181.1 Phone: t919) 733 322ti,
FACILITY INFORMATION Pease Pdnt,,Cleaty or Type
�"=>
PERMIT Number: Expiration Date: July 31, 2015
Facility Name: Aliens, Inc. - Turkey
-
Non -Discharge W00004268 UICr
Permit Name (if different): -
..
NPDES Other'
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION'BEING MONITORED
ElLagoon ElRemediatlon: Infiltration Gallery
Turks rs"`°° NO 28393-9703 County Sampson
;rent tus'.) izipt
® Spray Field ❑ Remediatlon:
Contact Person: .Martin Griess
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No::of wells to be sampled:.''
...'.
❑Water Source Heat Pump ❑Other:.
.. _ .. .- ....,.-
.'.... e
SAMPLING INFORMATION
"' ..
'-'--
i
If WELL
WELL ID NUMBER (from 'Permit): R-7
Date sample collected: 1 IIAMO, 7`: -.
-- FIELDANALYSES:-
WAS
Well Depth: fl.
Well Diameter: ' In.
pH 4.67 units Temp. 19 eC
DRY at
Depth to Water Level: 4.11 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond. -µMhos
time of
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
'
Odor
check
Volume of water pumped/bailed before sampling:
1.0+gallons-
Appearance
here:❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: _❑YES
❑ NO
_
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No; NC#11 NC#37714.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations..
€
COD 49.6 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead . mgll
CDliform: MF Fecal /100ml
Nitrate (NO3).as N '
-2.29 mg/I
Zn -Zinc ' mg/1
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 78.0mg/I
M-Aluminum
mg/1
pH (when analyzed) units
Be - Barium
mg/I
TOC 8.8 mg/l
Ca - Calcium
mg/I
Chloride 20.7 mg/I
Cd - Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)-
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method A ATTACH LAB REPORT.)
Sulfate 10mg/I
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance 147 µMhos
K - Potassium
mg/I
VOC , method #
Total Ammonia mg/1
Mg - Magnesium
mg/I
, method #,
(Ammonia Nitrogen; NHsas N;Ammonia Nitrogen, Totel
Mn-Manganese
mg/I
,method#
TKN as N mgll
Ni - Nickel
mg/I
, method #
For Remedlatlon Systems Only (Attach Lab,Reports): Influent Total VOCs: mg/L-- Effluent Total VOCs: mg/L i VOC Removal%
Martin Griess, Plant Manager
Permittee (or Authorized Apenn Name and Title -Please print or type
GW-59 Rev. 1/2007

JUCIVIII run Nl
QUALITY MONITORING:
Name: Allens, Inc. - Turkey
Name (if different): _
Address: 5900 Turkey Highway
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No, of wells to be sampled:
Ihom Pemtitl
PLING INFORMATION
L ID NUMBER (from Permit): R-8 Date sample collected: 11/8/10
Depth: ft. Well Diameter: _in.
h to Water Level: 8.50 ft. below measuring point Screened Interval: _ft. to _ft:
luring Point Is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/balled before sampling: 10+ gallons
Date:
WQ0004268 UIC
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Rem edlation: Infiltration Gallery
Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other: _
FIELD ANALYSES: WAS
pH 4.23 units Temp. 22 eC DRY at
Spec. Cond. µMhos time of
Odor sampling,
check
Appearance here: ❑
sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
\METERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 33.5 mg/I Nitrite (NO,) as N mg/I Pb - Lead mg/I
Coliform: MF Fecal /100ml Nitrate (NO3) as N 28.9 mg/I Zn - Zinc mg/I
Coliform: MF Total /100ml Phosphorus: Total as P mgn
(Nola: Use MPNmethod for highly Wmldsamples) Q h h h
Dissolved Solids: Total
221 mg/I
pH (when analyzed)
units
TOC
0.9 mg/I
Chloride
21.2 mg/I
Arsenic
.. mg/I
Grease and Oils
mg/I
Phenol
Sulfate 13
Specific Conductance 358,4Mhos
Total Ammonia mg/I
(Ammonia Nitrogen; NHsas N; Ammonia Nitrogen, Total)
TKN as N mg/I
rt op osp ate
mg/I Other (Specify Compounds and Concentration Units):
AI - Aluminum
mg/I
Be - Barium
mg/I
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni - Nickel
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method A ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
ror memectauon aystems umy tAu;acn Lao neportsl: , ulriuen[ i otal vuts: mg/L _-_ _ Effluent Total VOCs: _ me/L VOC Removal%
Martin Griess, Plant Manager
Perri (or Authorized Agent)Name and This- Please print or type
GW-59 Rev. 1/2007

QUALITY MONITORING:
PORT FORM
Name: tkilens, Inc. - I urKey
Name (if different):
Address: 5900 Turkey Highway
y 'at ° NC 28393-9703 County Sampson
act Person: Martin Griess Telephone#: 910=596-0028
Location/Site Name: No. of wells to be sampled:..
LID NUMBER (from Permit): -R-9
Depth: ft.
h to Water Level: 7.90 ft. below measuring point
wring Point is ft, above land surface
ne of water pumped/balled before sampling:
sample
COO 80'.7 mg/l
Collform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note; Use MPN method for highly turbid samples)
Dissolved Solids: Total
176 mgll
pH (when analyzed)
units
TOC
3.4 mg/I
Chloride
12.4 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
51 mg/I
Specific Conductance
272 µMhos
Total Ammonia
mg/I
(lvnmonla Nitrogen: NHsea N; Ammonla
Nitrogen, Total)
TKN as N
mg/I
1
Date sample collected: 11/8/10 _.
Well Diameter: In.
Screened Interval: ft. to ft.
Relative M.P. Elevation: d ft.
:onolaai concentrations;
- -
Nifrit—(NOz)"'ea N -
.moll
Nitrate (NO3) as N
15.1 nigh
Phosphorus: Total as P
mg/I
Orthophosphate
mg/I
AI - Aluminum
_ .mg/I
Be - Barium
nig/I
Ca - Calcium
mg/I
-Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu- Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mgll
K- Potassium
mg/I
Mg - Magnesium.
_ mg/I
Mn-'Manganese
mgli
Ni - Nickel
.ma/I
m-Discharge WQ0004268 UICi
DDES Other=.
'PE OF PERMITTED OPERATION BEING MONITORED
El Lagoon ElRemediation: Infiltration Gallery
®"Spray Field ❑ Remediatlon:
❑ Rotary Distributor ❑ Land Applicationrof Sludge
❑ Water Source Heal Pump ❑ Other::
FIELD ANALYSES:
PH 4.26 units_ Temp. ; 20 eC
Spec. Cond. µMhos
Odor
Appearance
Certification No.�NC#11 NC#37714
Pb - Lead `mg/I
Zn - Zinc ;mg/I
,Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GCIMS, HPLC)'
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method # :.
method #
method #
method #
For Remedlatlon Systems Only (Attach Lab Reports): I Influent Total VOCs: .. mg/L_-Effluent Total"VOCs: me/L j VOC Removal%
Martin Griess, Plant Manager
Permittee(or Authorized Agent)Name and'Tltle- Please print or type Sipn reb Pe i ee.(or Ai
GW-59 Rev. 112007
) a/i>116
at
of

Fayetteville Division
2592 Hope Mills Rd
' Fayetteville, NC 28306
910.864.1920 Phone
910.864.9774 Fax
Certificate of Analysis
Aliens. Inc
Mr. Martin Griess Project: M/Wells samples-3/Yearly Date Reported: November30,2010
5900 Turkey Highway Date Received: November 08. 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: November 08, 2010
Analyze
Result Unit
Total Organic Carbon
2.5
Analyzed by: Mimbac- Fayetteville Divislon
Chloride
16.9
COD, Total
97.5
Conductivity
213
Depth to Water Surface
5.10
Nitrate as N
13.1
pH, Field Test
4.43
Total Dissolved Solids
108
Sulfate as SO4
20
Temperature
20
mg/L
mg/L
mg/L
umhos/cm
feet
mg/L
pH Units
mg/L
mg/L
aC
R-5a
1011179-01
Analysis Date/Time
11/8/10 14:40
11/9/10 10:36
11/9/10 14:20
11/15/10, 16:00
11/8/10 14:40
11/9/10 10:36
11/8/10 14:40
11/9110 14:30
1119110 10:36
1118110 14:40
R-6
1011179-02
Analyst Method
RP SM 5310B
TDA
EPA 300.0
ARS
SM 20th Ed. 5220 D
ARS
SM 20th Ed. 2516 B
RDM
Field Measurement
TDA
EPA 300.0
RDM
Field
AMM
SM 20th Ed. 2546 C
TDA
EPA 300:0
RDM
Field
Qualifier
B
A4
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
Total Organic Carbon
11.9
Analyzed by: Microbac - Fayetteville Divislon
Chloride
27.2
COD, Total
72.9
Conductivity
213
Depth to Water Surface
730
Nitrate as N
2.10
pH, Field Test
5.71
Total Dissolved Solids
131
Sulfate as SO4
21
Temperature
21
mg/L
mg/L
mg/L
umhos/cm
feet
mg/L
pH Units
mg/L
mg/L
aC
11/8/10 14:40
1119/10 10:36
11/9/10 14:20
11/15/10 16:00
11/8/10 14:30
1119110 I0:36
11/8/10 14:30
11/9/10 14:30
1119110 10:36
11/8/10 14:30
R-7
1011179-03
RP SM 5310B
TDA
EPA 300.0
ARS
SM 20th Ed. 5220 D
ARS
SM 20th Ed. 2510 B
RDM
Field. Measurement
TDA
EPA 300.0
RDM
Field
AMM
SM 20th Ed. 2540 C
TDA
EPA 300:0
RDM
Field
B
A4
State Certifications: Respectfully Submitted
NCDNR #11
NCDOH #37714. 6R- W- s%ju r�
USDA #3787 R: W. Sanders, VP/Managing Director
Thank you for your business. Weim•itCynar(•edhockrriuniNerelrfren•iceiayoo. Plean, contact the rTMnihnging Director, Ran Sanders of 910464-1920. daoievNnkec. Pm,iNen( of
p4a, n)..rrahw cneh nr rotor Rgece. CEO• tnibmrce(il, nmrob.e n nh vblh om•=...toms or xgwWianr. I Page 1 of 3

(.I i'
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Fax
Certificate of Analysis
Aliens. Inc
Mr. Martin Criess Project: M/Wells samples - 3/Yearly Date Reported: November 30, 2010
5900 Turkey Highway Date Received: November 09, 2010
Turkey NC. 28393 Sampled By: Robin Miller Date Sampled: November 08, 2010
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Analyzed by: ECI
Total Organic Carbon .,
8.8
mg/L
11/8/10 14:40
RP
SM 5310B
Analyzed by: Mimbac- Fayetteville
Division
-
Chloride
20.7
mg/L
11/9/10 10:36
TDA
EPA 300.0
B
COD, Total
49.6
Ing/L
11/9/10 14:20
ARS
SM 20th Ed. 5220 D
A4
Conductivity
147
umhos/cm
11/15/10 16:00
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
4.11
feet
11/8/10 14:20
RDM
Field Measurement
Nitrate as N
2.29
mg/L
1119/10 10:36
TDA
EPA 300.0
pH, Field Test
4.67
pH Units
11/8/10 14:20
RDM
Field
Total Dissolved Solids
78.0
mg/L
1119110 14:30
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
10
mg/L
1119110 10:36
TDA
EPA 000.0
Temperature
19
°C
I118/10 14:20
RDM
Field
R-8
1011179-04
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
Total Organic Carbon
0.9
mg/L
11/8/10
14:40
RP
SM 5310B
Analyzed by: Microbac- Fayetteville Division
Chloride
21.2
mg/L
11/9/10
10:36
TDA
EPA 300.0 B
COD, Total
33.5
mg/L
11/9/10
14:20
ARS
SM 20th Ed. 5220 D A4
Conductivity
358
umhos/cm
11/15/10
16:00
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
8.50
feet
11/8/10
14:10
RDM
Field Measurement
Nitrate as N
28.9
mg/L
1119110
10:36
TDA
EPA 300.0
pH, Field Test
4.23
pH Units
11/8/10
14:10
RDM
Field
Total Dissolved Solids
221
mg/L
11/9/10
14:30
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
13
mg/L
1119110
10:36
TDA
EPA 300.0
Temperature
22
°C
II/8/10
14:10
RDM
Field
R-9
1011179-05
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
State Certifications: Respectfully Submitted
NCDNR #11.
NCDOH #37714
USDA #3787 R W. Sanders, VP/Managing Director
Thank you for your business. We invite ynnrfeedback na nnrlevel ofservim to ynrt. Please ctm1aa the IPSlsorogmg D)reel°r, Ron Sanders al 91046J-1920, Jana= Nnkm Pmwfmil, 01
jnnkes(rramicrob°ceom nr7.rnr Bnyre, CEO, n1 tboycen rricrvba .. ,with any mmm¢nls nrsoggertiwrs. Paget of 3

f !=c D
J
Fayetteville Division
2592 Hope Mills Rd
Fayetteville, NC 28306
910.864.1920 Phone
910.864.8774 Far
Certificate of Analysis
Aliens. Inc
Mr. Martin Griess Project: M/Wells samples - 3/Yearly Date Reported: November 30. 2010
5900 Turkey Highway Date Received: November 08, 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: November 08, 2010
gnclyL ey: eCl
Total Organic Carbon
3.4
Malyied by: Microbac - Fayettevine Division
Chloride
12.4
COD, Total
80.7
Conductivity
272
Depth to Water Surface
7.90
Nitrate as N
15.1
pH, Field Test
4.26
Total Dissolved Sblids
176
Sulfate as SO4
51
Temperature
20
mg/L
11/8/10
14:40
RP
SM 531013
mg/L
1119110
10:36
TDA
EPA 300.0
B
mg/L
1119110
14:20
ARS
SM 20th Ed. 5220 D
A4
umhos/cm
11/15/10
16:00
ARS
SM 20th Ed. 2510 B
feet
11/8110
15:45
RDM
Field Measurement
mg/L
1119110
10:36
TDA
EPA300.0
Si
pH Units
11/8/10
15:45
RDM
Field
mg/L
11/9/10
14:30
AMM
SM 20th Ed. 2540 C
mg/L
1119110
10:36
TDA
EPA300.0
SI
°C
11/8/10
15:45
RDM -
Field
Qualifier Definitions
S I Relative Percent Difference (RPD) outside accepted recovery limits
B Detected in the associated Method Blank
A4 CCV was outside acceptance limits. Data is valid but qualified.
State Certifications: NCDNR #11 Respectfully Submitted
NCDOH #37714 X. eW_ Aoiradeye,
USDA #3787 R. W. Sanders, VP/Managing Director
Thank you for your business. We invileynurfeedboekunour1c Jofcernice toyvn. Pieove contonthe 1P.Monogiog Din ior, Ron Sandersat910461-1920, Jomev Noke. Pns)d<o' of
jnokenQjoicroboecront or 7nror Bnyre. CEO. of tboyco@n icrobor.conr with onv rommenev orsuggestions Page 3 of 3

: Environmental Chemists, Inc.
6602 windmill Way • Wilmington, NC 28405
+ - ® [phone] (Lab) • [phone] (Fax)
M
710 Bowsertown Road • Manteo, NC 27954
1252) 473-5702
ANALYTICAL & CONSULTING
CHEMISTS NCDENR: DWQ CERTIFICATE #94.-DLS CERTIFICATE #3772.9
Microbac Laboratories - Fayetteville Date of Report: Nov 19, 2010
2592 Hope Mills Road Customer PO #:
Fayetteville , NC 28306 Report#: 2010-11355
Attention: Bonnie Sanders Report to:,. Bonnie Sanders
Project10: 1011179
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
10-28587 Site:1011179-01 11/8/2010 2:40 PM Water Client
Test Method Results Date Analyzed
Total Organic Carbon (TOC)
Lab ID Sample ID:
10-28588 Site:1011179-02
Test
SM 5310 B
Method
Collect Datefrime Matrix
11/8/2010 2:30 PM Water
2.5 mg/L 11/16/2010
Sampled by
Client
Results Date Analyzed
Total Organic Carbon (TOC) SM6310B 11.9'mg/L 11/16/2010
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
10-28589 Site:1011179-03 11/8/2010 2:20 PM Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
SM5310B
8.8 mg/L 11/16/2010
Lab ID Sample ID:
Collect DateTime
Matrix Sampled by
10-28590 Site:1011179-04
11/8/2010 2:10 PM
Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
SM5310B
0.9•mg/L 11/16/2010
Lab ID Sample ID:
Collect Date/Time
Matrix Sampled by
10-28591 Site:1011179-05
11/8/2010 3:45 PM
Water Client
Test
Method
Results Date Analyzed
Total Organic Carbon (TOC)
SM5310B
3.4 mg/L 11/16/2010
Comment:
by: 7�e
.Reviewed w
Report7t.: 2010-11355 Page 1 of 1

I ,: -- "
,NO Up MEMORIES SI NeR
Quality Vegetables
5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA,
PHONE [phone]
FAX [phone]
August 20, 2010
Dept. of Environmental & Natural Resources
Division of Water Quality —Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
RE: Groundwater Quality Monitoring Report
Allens, Inc. — Turkey, NC Facility
Permit # W00004268
28393
0-J
Enclosed are the original and one copy of the Groundwater Monitoring Report on forms GW-59
and GW-59A, and the lab report for Allens, Inc — Turkey, NC facility for samples collected in
July, 2010.
If you have any questions or require any additional information, please contact me by
phone at [phone] ext # 104
Sincere
hYp"AMartin Griess
Plant Manager
Allens, Inc. Turkey facility
CC: Laura Mushinski, Allens, Inc
Reid Wells, Allens, Inc — Turkey facility
` kot0a"6\10 OG

SUBMIT FORM
TER
Name: Aliens, Inc. -
Name (if different): _
Address: 5900 Turkev
act Person:
Location/Site
MONITORING:
L ID NUMBER (from Permit): MW-1
Depth: ft.
h to Water Level: 21.2 ft. below measuring point
curing Point is ft, above land surface
ne of water pumped/balled before sampling: 1
COD 20.3 mg/l
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
551 mg/l
pH (when analyzed)
units
TOC
4.2 mgA
Chloride
84.2 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
180 mg/l
Specific Conductance
920'µMhos
Total Ammonia
mg/I
(Ammonia Nitrogen; NH3 as N; Ammonia
Nitrogen, Total)
TKN as N mgll
County Sampson
Telephone#: [phone]
No. of wells to be sampled:
Date sample collected: 7/19/10
Well Diameter: in.
Screened Interval: ft. to ft.
Relative M.P. Elevation: ft.
iRMIT Number:
Expiration Date: July 31, 2011
,n-Discharge WQ0004268
UIC
IDES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
® Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES:
pH 4.62 units
Spec. Cc Ind.
Odor
Appearance
Temp. 26 aC DRY at
time of
_i: laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
Tend colloidal concentrations.
Nitrite (NO2) as N
mgA Pb - Lead mg/I
Nitrate (NO3) as N
12.2 mgA Zn - Zinc mgA
Phosphorus: Total as
ril l
Orthophosphate
mg/l Other (Specify Compounds and Concentration Units):
AI - Aluminum
mg/I
mg/l
C=
RECE+
mg/I
d gg ddmmium
tP �C omlum: Total
mg/I
mg/I
Procg9siQ4IN
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
mtormation
DWQ/BOGFe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
K- Potassium
mgA
VOC ,method#
t Mg - Magnesium
mgll
,method#
Mn - Manganese
mg/I
, method #
Ni - Nickel
mg/i
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VCCs: mg/L Effluent Total VOCs: - _- mall. VOC Removal%
Martin
GWS9 Rev. 1/2007
n

TER QUALITY MONITORING:
E REPORT FORM
ity Name: Aliens, Inc. - Turkey
IitName (if different):
ty Address: 5900 Turkey Hi-ghway
<ey e" `g NC 28393/,9703 County Sampson
(pM1 Istalel (ZIP) i
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No, of wells to be sampled:
Number: Expiration Date:
harge W00004268 UIC- ..
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
PLING INFORMATION _
LID NUMBER (from Permit): MW-2 Dale sample collected: 7/19/10 FIELD ANALYSES:
Depth: ft. IWell Diameter: — In. pH 5.24 units:. Temp. 22 eC
i to Water Level: 8.90 ft. below measuring point Screened Interval: _ft. to _ft. Spec. Cond. µMhos
,uring Point is ft. above land surface Relative M.P. Elevation: ft. 'Odor
ne of water pumped/bailed before sampling: 10+ gallons Appearance
a sample analyzed:
Laboratory Name: Microbac Laboratories
.Certification No. NC#11 NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
<10.0 mgll
Nitrite (NO2) as N
mg/l
Pb - Lead mg/I
Coliform: MF Fecal
/loom]
Nitrate (NO3) as N
<0.0200 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/loom]
Phosphorus: Total as P
mg/I
(Nate: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
172mg/I
Al -Aluminum
mg/l
pH (when analyzed)
-
units
Be - Barium
mg/I
TOC
2.6 mgn
Ca - Calcium
mg/I
Chloride
124 mg/l
Cd - Cadmium
mg/I
at
of
Arsenic mg/I
Chromium: Total
mgn
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/l
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 11 mg/I
Hg- Mercury
mg/I
ReportAftached9 ❑ Yes(1) ❑ No,(0)
Specific Conductance 375 µMhos
K - Potassium _
mg/I
VOC , method #
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen: NHsas NI Ammonia Nitrogen, Total)
Mn -Manganese
mg/I
,method #
TKN as N mg/I
Ni - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports):
_ Influent Total VOCs:
mg/L Effluent Total VOCs: mg/L VOC Removal%
Martin Griess, Plant Manager
Permittee(or Authorized Agent)Name and Title- Please print or type _
GW-59 Rev.112007

TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. -
Name (if different): _
Address: 5900 Turkev
County Sampson
act Person: Martin Griess Telephone#: [phone] I
Location/Site Name; No. of wells to be sampled:
- ffmm PemNl
PLING INFORMATION '
LID NUMBER (from Permit): MW-3 Date sample collected: 7/19/10
Depth: ft. Well Diameter: _In.
i to Water Level: 4.80 ft. below measuring point Screened Interval: _ft. to _ft.
,uring Point Is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+7 gallons
sample
COD <10.0 mg/I
Coliform: MF Fecal /looml
Collform: MF Total /10oml
(Note; Use MPN method for highly turbid samples)
:RMIT Number: Expiration'Date: July 31, 2011
n-Discharge WQ0004268 UIC
'DES Other
PE OF PERMITTED OPERATION BEING. MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
pH 6.98. units Temp. 28 °C
Spec. Cond. µMhos
Odor
Appearance
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
colloidal concentrations. -
Nitrite (NO,) as N mg/I Pb - Lead mg/I
Nitrate (NO3) as N <0.0200 mg/I Zn - Zinc mg/I
Phosphorus: Total as P mg/I
Orthophosphate mg/I Other (Specify Compounds and Concentration Units):
at
Of
Dissolved Solids: Total
287mg/I
At - Aluminum
mg/I
pH (when analyzed)
units
Be - Barium
mg/I
TOC
1.0 mg/I
Ca - Calcium
mg/I
Chloride
70.7mg/I
Cd- Cadmium
mgfl
Arsenic
mgfl
- Chromium: Total
mg/1
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Suffate
68 mg/I
Hg - Mercury
mgll
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
355 µMhos
- _ K - Potassium
mgfl
VOC , method #
Total Ammonia
mg/I
- Mg - Magnesium
mg/l
, method #
(Ammonia Nitrogen; NHsas N; Ammonia
Nitrogen, Total)
Mn- Manganese
mgll
_
,method#
TKN as N
mg/I
Ni - Nickel
mgll
, method #
For Remedlatlon Systems Only (Attach Lab Reports):
Influent Total VOCs:
mglL . Effluent Total VOCs: mglL VOC.Removal%
Martin Griess, Plant Manager
Permittee (or Authorized Anent) Name and Title - Please print or type
GW-59 Rev. 112007
-,d0 -/O

ONLY
TER QUALITY MONITORING:
E REPORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkev Hiahwav 1
County Sampson
act Person: Martin Griess Telephone* 910-596-0028
Location/Site Name: No. of wells to be sampled:
ID NUMBER (from Permit): MW-4 Date sample collected: 7/19/10
Depth: ft. Well Diameter: _in.
to Water Level: 7.10 ft. below measuring point i Screened Interval: ft. to ft.
firing Point is ft, above land surface Relative M.P. Elevation: ft.
a of water pumped/bailed before sampling: 10+'gallons
Number: Expiration Date:
harge WQ0004268 UIC_
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ RotaryDistributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD.ANALYSES- WAS
PH 4.08 units Temp. 25 eb DRY at
Spec. Cond. µMhos time of
Odor samplin
check
Appearance here: r
sample analyzed: Laboratory Name: Microbao Laboratories Certification No. NC#1.1 NC'#37714
'METERS .NOTE: Values should reflect dissolved and colloidal concentrations.
COD <10.0 mgn j Nitrite (NO2) as N mg/I Pb - Lead mg/I
Colitorm: MF Fecal /100m1. i Nitrate (NO3) as N 10,3 mg" Zn - Zinc mg/I
Coliform: MF Total /100ml j Phosphorus: Total as P mg/I
(Note: Use MPN method for highly turbid samples) Orth In h I
Dissolved Solids: Total
79.0 mg/I
pH (when analyzed)
units
TOC
<0.5 mg/I
Chloride
20.2 mg/I
Arsenic
mg/I
Grease and Oils
mg/1
Phenol
mg/I
Sulfate
3.2 mg/I
'Specific Conductance
137 µMhos
Total Ammonia
mg/I
(Ammonia Nitrogen: NH, as N; Ammonia
Nitrogen, Total)
TKN as N mg/I
For Remedlatlon Systems Only (Attach Lab
Martin Griess, Plant Manager
Permlttee (or Authorized Agent) Name and Title -.Please print or type
GW-59 Rev. 112007
op osp a e
mg,
AI -Aluminum
mg/I
Be - Barium
mgA
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg-..Mercury
_mg/I
K- Potassium _
mg/I
Mg - Magnesium
mg/I
Mn- Manganese
mgA
Ni- Nickel
mg/I
Other (Specify Compounds and Concentration Units)
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method A ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
lal VOCs: mg/L VOC Removal%
-o /v

TER QUALITY MONITORING:
Name: Allens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y sr en NC 21
IGfll (Slate) (<
act Person:
Location/Site
PERMIT Number: Expiration Date: July 31, 2011
Non -Discharge W00004268 UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
County Sampson ❑ Lagoon ❑ Remediation: Infiltration Gallery
RI Spray Field ❑ Remediation:
Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
No. of wells to be sampled: ❑ Water Source Heat Pump ❑ Other.
LID NUMBER (from Permit): R-1 tDate sample collected: 7/19/10
Depth: ft. Well Diameter: in.
i to Water Level: 5.30 ft. below measuring point Screened Interval: _ft. to _ft.
wring Point is fl. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailedbefore sampling: 10+'gallons
sample
IAMETERS NOTE: Values should reflect dtssolv,
COD 61.5 mg/I
Collform: MF Fecal /100ml
Coliform: MF Total /looml
(Note: Use MPN method for highly turbid Samples)
Dissolved Solids: Total
54.0 mg/I
pH (when analyzed)
units
TOC
4 mg/I
Chloride
1.92 Mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
2.3 mg/I
Specific Conductance
80.3µMhos
Total Ammonia
mg/I
(Ammonia Nitrogen; NH3 as N; Ammonle
Nitrogen, Total)
TKN as N mg/I
FIELD ANALYSES:
pH 4.73 units Temp. 28 °C
Spec. Cond. µMhos
Odor
Appearance
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
t colloidal concentrations.
Nitrite NO N
( :) as mgll Pb - Lead mg/I
Nitrate (NOa) as N 0.278 mg/I Zn -Zinc mgfi
Phosphorus: Total as P mg/I
Orthophosphate mg/I Other (Specify Compounds and Concentration Units):
AI -Aluminum
mgll
Be - Barium
mg/I
. Ca - Calcium
mg,1
Cd - Cadmium
mg/I
Chromium: Total
mgll
i Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Hg - Mercury
mg/l
Report Attached? ❑ Yes (1) ❑ No (0)..
K- Potassium
mg/l
VOC ,method#
Mg -Magnesium
mg/I
, method #
Mn - Manganese
mg/I
, method #
NI - Nickel
mg/I
,method #
For Remedlation Systems Only (Attach Lab Reports): Irifluent Total VOCs: ,mg/L Effluent Total VOCs: mp/L VOC Removal%
Plant
GW-59 Rev. 112007
i
at
Of

Fillil T FnPftg nM VFI I n1Al .Aoa:o nen v
GROUNDWATER QUALITY MONITORING:
EPARTMEN'POF,ENVIRONMEN7g`NATURAL RESOURCES e. ,r
wl3tohbF WATER QUALITY INFORMATION PROCESSING UNl7
COMPLIANCE REPORT FORM
a77MAIL SIiRVIC�EyCENTERIRALEIGH NG 17699=je17 9121L�,s
Phopat!_(919)7Jg
FACILITY INFORMATION Please Print Creasy or Type
PERMIT Number: Expiration Date: Jul 31, 2011
Facility Name: Aliens, Inc. -Turkey
-
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different): i -
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑Lagoon ❑Remediation: Infiltration Gallery
sa&eq
Turkey NC 28393-9703 County Sampson
arnl r51a19) (zip)
® Spray Field ❑ Remediation:
Contact Person: Martin GrieSs
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
I No. of wells to be sampled:
❑ Water Source Heat Pump ❑ Other:
I
ham Peanil
$AMP' ING'QLjMAT10N
WELL ID NUMBER (from Permit): R-2a
j '
Date sample collected: 7119/10
FIELD ANALYSES:
If WELL
WAS
Well Depth: ft.
Well Diameter: —
in.
pH 4.72 units Temp. 28 ac
DRY at
Depth to Water Level: 5.70 ft. below measuring point
Screened Interval:
to
Spec. Cord, µMhos
time of
Measuring Point is ft. above land surfaceRelative
_ft.
M.P. Elevation:
_ft.
ft.
Odor
sampling,
Volume of water pumped/bailed before sampling:
10+ gallons
E
Appearance
check
here:
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑YES
❑ NO
❑
LABORATORY INFORMATION
Date sample analyzed:
i ,
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved ;ii colloidal concentrations.
COD 83.8 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
0.468 mg"
Zn -Zinc mg/I
Collform: MF Total /100ml
Phosphorus: Total as P
mg/I
Wale: Use MPN malnad for highly Mreld Samples)
Orthophosphate
mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 91.0 mg/I
AI - Aluminum
mg/I
pH (when analyzed) units
- Be - Barium
mg/I
TOC 2.2 mg/I
Ca - Calcium
mg/I
Chloride 12.1 mg/l
Cd- Cadmium
mg/I
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils n i
Cu - Copper
mgll
ORGANICS: (by GC, GCIMS, HPLC)
Phenol mg/I
I Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 45 mg/I
Hg- Mercury
mg/1
ReportAttached? ❑ Yes(1) ❑ No
Specific Conductance 204 pMhos
K- Potassium
mg/I
VOC ,method#
Total Ammonia mg/I
Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NHsae N; Ammania Nitrogen, Totes)
I Mn - Mahganese
mgll
,method #
TKN as N mg/l
Ni - Nickel
mg/l
, method #
For Remediation Systems Only (Attach Lab
Martin Grless, Plant Manager
Pernittee WAuthonzed Agent) Name and Title -Please print or type ,
GW-59 Rev. 112007
VOC Removal%

QUALITY MONITORING:
Name: Aliens,Inc.- Turkey
Vame (if different): _
Address: 5900 Turkey Highway
act Person: Martin Griess
Location/Site Name:.
LID NUMBER (from Permit): R-3
Depth: ft.
i to Water Level: . 7.00 ft. below measuring point
uring Point is ft, above land surface
ne of water pumped/balled before sampling: 10+'c
COD 16.4 mg/i
Coliform: MF Fecal /looml
Coliform: MF Total /loom[
(Note: Use MPN method ror highly turbid samples)
Dissolved Solids: Total
28.0 mgn
pH (when analyzed)
units
TOC
1.3 mg/I
Chloride
8.32 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
17 mg/I
Specific Conductance
68.8 µMhos
Total Ammonia
'mgn
(Ammonia Nitrogen; NHsae N; Ammonla
Nitrogen, Total)
TKN as N mgll
County Sampson
Telephone#: [phone]
No. of wells to be sampled:
Number: Expiration Date:
harge W00004268 UIC_
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedtatlon: Infiltration Gallery
® Spray Field ❑ Remediatlon:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other: _
-Date sample collected: 7/19/10 FIELD ANALYSES: WAS
Well Diameter: _in. pH 4.19 units Temp. 26 eC DRY at
Screened Interval: _ft. to _ft. Spec. Con;. µMhos time of
sampiin
Relative M.P. Elevation: ft. Odor check
�s Appearance here: r
and field acidified: ❑ YEB El NO - L
Laboratory Name: Microbac Laboratories Certification No. NC#11: NC#37714
idal concentrations.
Nitrite (NO2) as N
mg/I
Pb - Lead mg/l
Nitrate (NO3) as N
0.933 mg/I
Zn - Zinc mgll
Phosphorus: Total as P
mgll
Orthophosphate
Fri
Other (Specify Compounds and Concentration Units):
AI - Aluminum
mg/I
Be -Barium -
mg/I
Ca - Calcium
mg/l
Cd - Cadmium
m9/1
Chromium: Total
mg/I
Cu - Copper mg/I
Fe - Iron mg/I
Hg - Mercury mg/I
K- Potassium mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni- Nickel
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method M ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0),
VOC , method #
method #
method #
method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L _ Effluent Total VOCs: mg/L VOc Removal%
Martin Griess, Plant Manager �Q t` �__
ties (or Authorized Agent) Name and Title- Please print or type ` Signature of Permigee (OF Aufhodzetl Agent)
GW-59 Rev. 112007

SUBMIT FORM ON YE1 I OW PAPER ONLY
MONITORING:
REPORT
TY INFORMATION neasa rnnr uaenyor type —
Name: Aliens,Inc.-Turkey
Name (if different): '
Address: 5900 Turkey Highway
�y a""" NC 28393-9703 County Sampson
act Person: Martin Griess
Location/Site Name:
Telephone#: [phone]
No. of wells to be samoled:
L ID NUMBER (from Permit): R-4 - Date sample collected: 7/19110
Depth: - ft. Well Diameter: in.
h to Water Level: 7.80 ft. below measuring point Screened Interval: _ft. to ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
IAMETERS NOTE: Values should reflect dissoly
COD <10.0 mg/I
Coliform: MF Fecal /100ml
Coliform: MF Total /100ml
(Note: Use MPN method for highly turbid samples)
IRMIT Number:
Expiration Date: July 31, 2011
n-Discharge W00004268
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITClRED
❑ Lagoon
❑ Remediation: Infiltration Gallery
® Spray Field
❑ Remediation:
❑ Rotary Distributor.
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES: - AS
pH 4.04 units Temp, 30 `C '[he
RY at
Spec. Cond. µMhos e of
mpling,
Odor eck
Appearance re: ❑
Laboratory Name: Microbac Laboratories Certification No. NC#11`NC#37714
(,colloidal concentrations.
Nitrite (NO.) as N mg/I Pb - Lead mg/I
Nitrate (NO3) as N 4.85 mg/I Zn - Zinc mgn
Phosphorus: Total as P mg/I
Orthophosphate mg/i Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
58.0mg/I
AI - Aluminum
mg/I
pH (when analyzed)
units
- Be - Barium
mg/l
TOC
0.6 mg/I
Ca- Calcium
mg/I
Chloride
27.8 mg/I
Cd- Cadmium
mg/I
Arsenic
-
mg/I
Chromium: Total
mg/I
_
Grease and Oils
mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
16mga
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance
103 PMhos
_ K- Potassium
mg/I
VOC ,method#
Total Ammonia
mg/I
- Mg - Magnesium
mg/I
, method #
(Ammonia Nitrogen; NH,aa N; Ammsma
Morgan. TotalMo'-
Manganese
mg/l•.
method #
TKN as N
mg/I
Ni - Nickel
mgll
, method #
For Remedlatlon Systems Only (Attach Lab Reports):
Influent Total VOCs:
_ma/L .Effluent Total VOCs mo/L VOC Removal%
Martin Griess, Plant Manager
Permittee (or Authorized Agent) Name and Title. Please print or type
GW-59 Rev. 112007

ONLY
ROUNDWATER QUALITY MONITORING:
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:,
RMIT Number: Expiration Date: July 31, ZOt'I
n-Discharge WQ0004268 UIC
'DES Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
RI Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
-
If WELL
WELL ID NUMBER (from Permit): R-5a
_
Date sample collected: 7/19/10
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
pH 4.03 units Temp.
33 DC
DRY at
Depth to Water Level: 6.40 ft. below measuring point
_In.
Screened Interval: ft. to ft.
Spec. Cond.
µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance.
here: ❑
Samples for metals were collected unfiltered: DYES
❑ NO: and field acidified: DYES ❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Mierobao Laboratories
Certification No.
NC#11_NC#37714
PARAMETERS NOTE: Values should reflect dissolved and, colloidal concentrations.
COD 39.9 mg/I
Nitrite (NO.) as N mg/I
Pb - Lead
mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N 9.25 mg/I
Zn -Zinc
mgll
Coliform: MF Total
/100ml
: Phosphorus: Total as P
mg/I
(Note: Use MPN method for hlghly turbld samples)
Orthophosphate
mg/I Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
116mg/I
AI -Aluminum
mg/I
pH (when analyzed)
units
Be— Barium.
mg/l _
TOO
2.3 mg/I
-. Ca - Calcium
mg/l
Chloride
9.21 mg/l
- Cd - Cadmium
mg/I
Arsenic
mg[1
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
23 mg/I
Hg -Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
160µMhos
K- Potassium
mg/I
VOC ,method# _
Total Ammonia
mg/l
Mg - Magnesium
mg/I
,method#
(Ammonia Nitrogen: NH3 as Nt Ammome
Nitrogen, Total)
Mn- Manganese
mg/I
,method#
TKN as N
mg/I
NI - Nickel
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L _ Effluent Total VOCs: mg/L VOC Removal%_
Martin Griess, Plant Manager
tee (or Authodzed Agent) Name and Title - Please pant or type
GWS9 Rev.112007

MONITORING:
REPORT
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkev Hiahwav
County Sampson
act Person: Martin Griess Telephone#: [phone] I
Location/Site Name: No. of wells to be sampled:
foam Pe 'p
PLING INFORMATION
L ID NUMBER (from Permit): R-6 Date sample collected: 7/19110
Depth: ft. Well Diameter: in.
i to Water Level: 7.20 ft. below measuring point Screened Interval: _ft. to ft.
wring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+ gallons
or: Expiration Date:
WQ0004268 UIC_
Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary• Distributor El Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES: AS
PH 5.05 units Temp. 30 oC. DRY at
Spec. Cond. µMhos time of
Odor _
Appearance
sample analyzed: Laboratory Name: Microbac Laboratories Certification No. NC#1 PNC#37714
%METERS NOTE: Values should reflect dissolved and'colloidal concentrations.
COD 54.1 mg/I Nitrite (NO,) as N mg/I Pb - Lead mg/I
Coliform: MF Fecal /100ml Nitrate (NO3) as N 1.66 mg/l Zn -. Zinc mg/I
Coliform: MF Total /100ml ', Phosphorus: Total as P mg/I
(Nob: Use MPN method for highly turbid samples)
Dissolved Solids: Total
112 mg/I
PH (when analyzed)
units
TOC
9:7 mg/I
Chloride
23.4 mg/l
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
25 mg/I
Specific Conductance
163 µMhos
Total Ammonia
mg/1
(Ammonia Nitrogen; NHsas N; Ammonia
Nitrogen, Totep
TKN as N mg/1
Orthophosphate
mg/I
AI - Aluminum
mg/I
Be - Barium
mgA
Ca - Calcium
mga
Cd - Cadmium
mg/l
Chromium: Total
mg/1
Cu- Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K- Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mgA
Ni- Nickel
mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
For Remedlatlon Systems Only (Attach Lab Reports): Iriguent Total VOCs: mgI Effluent Total VOCs: mg/L VOC Removal%
Martin Griess, Plant Manager of 1, O
'Permigas (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (or Authorized Agent)
GW-59 Rev.112007

SUBMIT FORM ON
QUALITY MONITORING:
,PORT FORM
Name: Aliens, Inc. - Turkey
Name (if different):
Address: 5900 Turkey Highway
y ts""" NC 28393-9703 County Sampson
Person: Martin Griess
Location/Site
Telephone#: [phone]
No, of wells to be sampled:
Number: Expiration Date:
:harge W00004268 UIC_
Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
® Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
-L ID NUMBER (from Permit): R-7
Date sample collected: 7119/10
FIELD ANALYSES:
WAS
I Depth: ft.
Well Diameter: _in. -
pH 4.11 units Temp.
27 oC
DRY at
th to Water Level: 6.00 ft. below measuring point
Screened Interval: ft. to ft.
Spec. Cond.
µMhos
time of
isuring Point is ft. above land surface
Relative M.P. Elevation: ft.
Odor
sampling,
check
Ime of water pumped/bailed before sampling:
10+'gallons
Appearance
here: ❑
I les for metals were collected unfiltered: ❑YES
❑,:NO - and field acidified: ❑ YES ❑ NO
IORATORY INFORMATION
:sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No.
NC#11NC#37714
tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 17.7 mg/I
Nitrite (NO,) as N mg/I
Pb - Lead
mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N 0.551 mg/I
Zn - Zinc
mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P mg/I
(Note: Use MPNmethod for highly tudridsamples)
Orthophosphate mgll
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
73.0 mg/I
pH (when analyzed)
units
TOC
4.6 mg/I
Chloride
29.8 mg/I
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
mg/I
Sulfate
9.4 mg/i
Specific Conductance
125 µMhos
Total Ammonia
mg/I
(Ammonia Nitrogen; NH3 as N: Ammonia
Nitrogen, Total)
TKN as N mg/I
AI -Aluminum
mg/I
Be - Barium
mgll
Ca - Calcium
mg/I
Cd - Cadmium
mgll
Chromium: Total
mg/l
Cu - Copper
mgli
Fe - Iron
mg/I
Hg - Mercury
mg/I
K - Potassium
mg/I
Mg - Magnesium
mg/I
Mn- Manganese
mg/I
NI - Nickel
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg1L Effluent Total VOCs: mg/L VOC Removal%_
Martin Griess, Plant Manager
Permiltee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.112007

�rmrer<UNLT
DWATER QUALITY MONITORING:
ANCE REPORT FORM
Name: Aliens
Name (if different):
Address: 59001
Inc. -
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No. of wells to be sampled:
feo P mtll
PLING INFORMATION
L ID NUMBER (from Permit): R-8 Date sample collected: 7/19110
Depth: ft. Well Diameter. In.
i to Water Level: 6.40 ft. below measuring point Screened Interval: ft. to _ft.
,uring Point is ft, above land surface Relative M.P. Elevation: ft.
ne of water pumped/bailed before sampling: 10+gallons
:RMIT Number:
n-Discharge W00004268
Expiration Dale: July 31, 2011
UIC
'DES
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon
❑ Remediation: Infiltration Gallery
® Spray Field
❑ Remediation:
❑ Rotary Distributor
❑ Land Application of Sludge
❑ Water Source Heat Pump
❑ Other:
FIELD ANALYSES: WAS
pH 3.80 units Temp. 30 e0 DRY at
Spec. Cond. {tMhos time of
Odor sampling,
check
Appearance here: ❑
a sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
2AMETERS NOTE: Values should
reflect dissolved andlcollotdal concentrations.
COD
<10.0 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mgA -
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
35,9 mg/I
Zn - Zinc mg/I
Coliform: MF Total
/100m1
Phosphorus: Total as P
mg/I
(Note: Use MPN method for Mghly luNid samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
259 mg/I
At - Aluminum
mgll
pH (when analyzed)
units
Be - Barium
mg/1
TOC
0.7 mg/I
Ca - Calcium
mg/I
Chloride
35.9 mg/I
Cd - Cadmium
mg/I
Arsenic
mg/I
Chromium: Total
mg/I
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol
mg/I
Fe - Iron
mgll
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
20 mg/i
Hg - Mercury
mg/i
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance
363 µMhos
K - Potassium
mg/1
VOC , method #
Total Ammonia
mg/I
Mg - Magnesium
mg/I
#
mmethod
(Ammonia Nitrogen: NH3NH3as Nmm : Aonla Nitrogen, Total)
Mn - Man Manganese 9
mg/I
, method #
TKN as N
mg/I
Ni - Nickel
mg/I
, method #
.., no,r,cururrorr oyssrans Willy (nuacn}ao rceporrs): mnuent i otai vacs: mg/L , Effluent Total VOCs: ma1L VOC Removals/
Martin Griess, Piant Manager1�����
PermiHas for Authorized Agent) Name and Title - Please print or type Signature of Permlttee for Authorized Agent) (Date)
GW-59 Rev. 112007

SUBMIT FORM ON YELL QW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
DEPARTMENLOF ENVIRONMENT.&'IA' URAL'RESOURCES ::°, - ` •'
COMPLIANCE REPORT FORM
IV1810H2OF WATER OUALITY.INEORMA710N PROCESSING UNIT'
6....
7 MA ILSERVICE;CENTER RAL'EIOH NC Y78Be-1817= Phone:(e1e) 7d3J221
FACILITY INFORMATION Pease Print Clearly
PERMIT Number: Expiration Date: July 31, 2011
Facility Name: Allens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑'Lagoon ❑ Remedlatidn: Infiltration Gallery
Turkeys"° " NC 28393-9703 Count Sampson
Y
iL rl (1WO (zip)
© Spray Field ❑ Remediatlon:
Contact Person: Martin Griess
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
ElWater Source Heat Pump ❑ Other:
som Pemut
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): R-9
-
Date sample collected: 7/19110
FIELD ANALYSES:
If WELL
WAS
Well Depth: ft.
Well Diameter: in,
pH 3.98 units Temp. 30 °c
DRY at
Depth to Water Level: 7.60 ft. below measuring point
Screened Interval: ft.
to
Spec. Cond. µMhos
time of
Measuring Point is ft, above land surface
Relative M.P. Elevation:
_ft.
ft.
Odor
sampling,
check
Volume of water pumped/bailed before sampling:
10+gallons
Appearance
here:
Samples for metals were collected unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
❑
LABORATORY INFORMATION
Date sample analyzed:
iLaboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and`collotdal concentrations.
COD 58.6 mg/I
Nitrite (NO,) as N
mg/1
Pb - Lead mg/I
Coliform: MF Fecal /100m1
Nitrate (NOp) as N
1.79 mg/I
Zn - Zinc mgll
Coliform: MF Total /loom)
Phosphorus: Total as P
mgll
(Note: Use MPN method for highly turbid samples)
Orthophosphate
mg/I
Other(Specify Compounds and Concentration Units):
Dissolved Solids: Total 295mg/I
AI - Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mg/I
TOC 5.3 mg/I
Ca - Calcium
mg/1
Chloride 11.6 mg/I
Cd - Cadmium
mg/l
Arsenic rit
Chromium: Total
mg/I
Grease and Oils mgh
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC) -
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method A ATTACH LAB REPORT.)
Sulfate 130 mg/I
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 411 µMhos
K- Potassium
mg/I
VOC ,method#
Total Ammonia mg/I
Mg - Magnesium
mg/I
,method#
(Ammonla Nitrogen; NHsas N; Ammo NiNitrogen, Total)
Mn - Manganese
hit
,method #
TKN as N ni
Ni - Nickel
mg/l
, method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L ,Effluent Total VOCs: mg/L VOC Removal%
Martin Griess, Plant Manager 7 ya y` -
Permithee (or Authorized Agent) Name and Title - Please print or type Signature of Pennittea (or Authgdzetl Apenq to
GW-59 Rev. V2007

Fayetteville Division
2592 Hope Mills Rd 8-11 Wendy Court
Fayetteville, NC 28306 Greensboro, NC 27409
910.864.1920 Phone [phone] Phone
910.864.8774 Fax [phone] Fax
Certificate of Analysis
Allens, Inc
Mr. Martin Grim Pmject: M/Wellssamples-3/Yearly Date Reported: August4,2010
5900 Turkey Highway Date Received: July 19, 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: July 19, 2010
MW #1
1007539-01
Analyse
Result
Unit
Analysis Date/Time
Analyst
Method Qualifier
Arolym1 or. M
Total Organic Carbon
4.2
mgL
7/22/10 0:00
ECI
SM 5310B
Anatrzed by: Kcrobac- FayelRviTe CWbon
Chloride
84.2
mg/L
7/20/10 9:48
TDA
EPA 300.0
COD, Total
20.3
mg/L
7121/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
920
umhos/cm
727/10 14:56
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
21.2
feet
7/19/10 10:30
RDM
Field Measurement
Nitrate as N
12.2
mg/L
720/10 16:17
TDA
EPA 300.0
pH, Field Test
4.62
pH Units
7/19/10 10:30
RDM
Field
Total Dissolved Solids
551
mg/L
721/10 9:45
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
180
mg/L
722110 17:39
ENC
EPA 300.0
Temperature
26
°C
7119/10 10:30
RDM
Field
Mw #2
1007539-02
Analyse
Result
Unit
Analysis Date/rime
Analyst
Method Qualifier
Ma" by. to
Total Organic Carbon
2.6
mg/L
722/10 0:00
ECI
SM 5310B
Analvral W. Mmaac - Fayetne ille dWsbn
Chloride
124
mg/L
720/10 9:27
TDA
EPA 300.0
COD, Total
<10.0
mg/L
721/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
375
umhos/cm
727/10 14:56
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
8.90
feet
7/19/10 10:45
RDM
Field Measurement
Nitrate as N
<0.0200
mg/L
7/20/10 16:17
TDA
EPA 300.0
pH, Field Test
5.24
pH Units
7119/10 10:45
RDM
Field
Total Dissolved Solids
172
mg/L
720/10 11:20
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
11
mg/L
7/21/10 10:48
TDA
EPA 300.0
Temperature
22
°C
7/19/10 10:45
RDM
Field
Mw #3
1007539-03
State Cefcations: Respectfully Submitted
NCDNR 011.#693
NCDOH #37714, #37795
USDA 43787 R. W. Sanders, VP/Mwa&g Director
Tn youraryoerbusiness. We ymircyourJereb°ckw ourh.</oJnniae royou. P/rare mrtmcuhe VPM°vgirg Direaoq Ron S+mkrs ar9/Odb/-/9S0,J vNwtra,PreriAene or
jnokrr(dmirmb°emmorTre.vr Byar, CEO.9uboyrr(djnicmk°erom virh yeanmenu orroggesdam.
Page 1 of3

Fayetteville Division
2592 Hope Mills Rd 8-B Wendy Court
Fayetteville, NC 28306 Greensboro, NC 27409
910.864.1920 Phone [phone] Phone
910.864.8774 Fax [phone] Fax
Certificate of Analysis
Allen, Inc
Mr. Martin Grim Project: M/Nellssamples-3/Yearly Date Reported: August4,2010
5900 Turkey Highway Date Received: July 19, 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: July 19, 2010
Analyse
Result
Unit
Analysis Datefrime
Analyst
Method Qualifier
aawel by. �
Total Organic Carbon
1.0
mg/L
7/22/10 0:00
ECI
SM 5310B
MaWai by. NOvdac- Fayettedle DMon
Chloride
70.7
mg/L
7/21/10 10:48
TDA
EPA 300.0
COD, Total
<10.0
mg/L
7/21/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
355
umhos/cm
727/10 14:56
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
4.80
feet
7/19/10 I1:00
RDM
Field Measurement
Nitrate as N
<0.0200
mg/L
720/10 16:17
TDA
EPA 300.0
pH, Field Test
5.98
pH Units
7/19/10 11:00
RDM
Field
Total Dissolved Solids
287
mg/L
721/10 9:45
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
68
mg/L
7/21/10 10:48
TDA
EPA 300.0
Temperature
28
°C
7/19/10 11:00
RDM
Field
Mw N4
1007539-04
Analyte
Result,
Unit
Analysis Dateirime
Analyst
Method Qualifier
a Wr by: rfl
Total Organic Carbon
<0.5
mg/L
722/10 0:00
ECI
SM 531013
M vmd by. N6nobac- Fayetuniie olNsbn
Chloride
20.2
mg/L
721/10 10:48
TDA
EPA 300.0
COD, Total
<10.0
mg/L
721/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
137
umhos/cm
727/10 14:56
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
7.10
feet
7/19/10 11:30
ROM
Field Measurement
Nitrate as N
10.3
mg/L
720/10 16:17
TDA
EPA 300.0
pH, Field Test
4.08
pH Units
7/19/10 11:30
RDM
Field
Total Dissolved Solids
79.0
mg/L
721/10 9:45
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
3.2
mg/L
721/10 10:48
TDA
EPA 300.0
Temperature
25
°C
7/19/10 11:30
RDM
Field
State Certifications:
Respectfully Submitted
NCDNR #11. #693
1
NCDOH 437714,#37795
USDA #3787
R- W. Senders, VP/Managing Director
Thank you for your business. We imire}wr/edbad on °nrleel o/rervire rolvu
Pleme mnmrnhr iP/Afmugirg Dirrer°gR°nS.mhrz or 910.86.E-/910, J°mn N°kes, PreriJene, ar
jrokes a}mirr°bac.rom orlYrwrBolee, CEO, a
rEoyce�mJnlrr°5°grom xirR wycanmrnrt °rsuggenlou'
Page 2 of3

Fayetteville Division
2592 Hope Mills Rd
8-B Wendy Court
Fayetteville, NC 28306
Greensboro, NC 27409
910.864.1920 Phone
336.856.9710 Phone
910.864.8774 Fax
336.856.9711 Fax
Certificate of Analysis
Allen, Inc
Mr. Martin Griess Project: IVI/Wellssampla-31Yearly Date Reported: August4,2010
Turk Turkey Highway
Date Received: July 19, 2010 Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: July 19, 2010
Qualifier Definitions
State Certifications: Respectfully Submitted
NCDNR #11. 9693
NCDOH 037714,#37795 i.[�� �'��. s�u-reR3u.•5.
USDA #3787 R. W. Sanders, VP/Managing D'aector
Thank you for your business. We imireyamJeedbaek on ourinrl aJservice royou Pleose mnexr de PP/Mamrgirrg Dirceror, Ron Sam/ers ar 9/0.961-/930, Janes NoMs. PrcsiJem, ar
jnakes(edmieroboerom ar 7reror 8o)n, CEO, auboyre(amrerabac.rom nlrh arty eoarmenuormggeniom.
Page of3

Fayetteville Division
2592 Hope Mills Rd
8-B Wendy Court
Fayetteville, NC 28306
Greensboro, NC 27409
910.864.1920 Phone
336.856.9710 Phone
910.864.8774 Fax
336.856.9711 Fax
Certificate of Analysis
Allens, Inc
Mr. Martin Griess Project M/Wellssamples-3/Yearly Date Reported:
5900 Turkey Highway Date Received: July l9, 2010
Turkey NC, 28393 Sampled By: Robin Miller
Date Sampled: July 19, 2010
R-1
1007541-01
Analyte
Result
Unit
Analysis DateiTime
Analyst
Method Qualifier
gnarysa by: ra
Total Organic Carbon
4
mg/L
7/22/10 0:00
ECI
SM 5310B
Analyrel by: Krnabac- FayetteNk Darision
Chloride
1.92
mg/L
7120110 9:48
TDA
EPA 300.0
COD, Total
61.5
mg/L
7/21/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
80.3
umhos/cm
7/27/10 14:56
ARS
SM 20th Ed. 2510B
Depth to Water Surface
5.30
feet
7/19/10 13:00
RDM
Field Measurement
Nitrate as N
0.278
mg/L
7/20/10 16:17
TDA
EPA 300.0
Nitrite as N
0.278
mg/L
7/20/10 9:48
TDA
EPA 300.0
pH, Field Test
4.73
pH Units
7/19/10 13:00
RDM
Field
Total Dissolved Solids
54.0
mg/L
7/20/10 11:20
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
2.3
mg/L
7/20/10 9:48
TDA
EPA 300.0
Temperature
28
°C
7/19/10 13:00
REIM
Field
R-2m
1007541-02
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
Analyzed by: M
Total Organic Carbon
AaMed W. Dtioobac- Fayeneville WN on
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
Nitrite as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
2.2
mg/L
722/10 0:00
ECI
SM 5310B
12.1
mg/L
720/10 9:48
TDA
EPA 300.0
83.8
mg/L
721/10 11:05
ENC
SM 20th Ed. 5220D
204
umhos/cm
727/10 14:56
ARS
SM 20th Ed. 2510 B
5.70
feet
7/19/10 12:50
RDM
Field Measurement
0.468
mg/L
7/20110 16:17
TDA
EPA 300.0
<0.0300
mg/L
7/20/10 9:48
TDA
EPA300.0
4.72
pH Units
7/19/10 12:50
RDM
Field
91.0
mg/L
720/10 11:20
AMM
SM 20th Ed. 2540 C
45
mg/L
7/20/10 9:48
TDA
EPA 300.0
State Certifications: Respectfully Submitted
NCDNR 011. #693
NCDOH #37714,#37796 iR�� �'��. >91u.rr.�{.ci •±.
USDA #3787 R. W. Sanders, VP/Maragin6 Director
Thank you for your business. Weimire/av JeJback on °w/em!°Jxe.dee m/va Plmre ronracnhe VPBdawgixgOtrenon Ran Sanders ar 9/0.B6I-/910, James Nokex, Presirlenp ar
Jnokes(djnicmbac.com or rrerOfB )'ce. CEO, artDak'ee(ami°r°baarom airh any rmnmersrs or suggeariam.
Page 1 of

Fayetteville Division
2592 Hope Mills Rd 8-B Wendy Court
Fayetteville, NC 28306 Greensbom, NC 27409
910.864.1920 Phone [phone] Phone
910.864.8774 Fax [phone] Fax
Certificate of Analysis
Allen, Inc
Mr. Martin Griess Project: MlWellssamples-3/Yearly Date Reported:
5900 Turkey Highway Date Received: July 19, 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: July 19, 2010
R-2
1007541-02
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
Pnelytel by: Mcrobac-Fayette0e tM Wn
Temperature 28 oC 7/19/10 12:50 RDM Field
R-3
1007541-03
Analyte Result Unit Analysis Date/rime Analyst Method Qualifier
Total Organic Carbon
1.3
mg/L
7122110 0:00
ECI
SM 5310B
Mxiyied by: Kaobac- FayetteWle DMsan
Chloride
8.32
mg/L
7/21/10 10:48
TDA
EPA 300.0
COD, Total
16.4
mg/L
7/21/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
68.8
umhos/cm
7/27/10 14:56
ARS
SM 201h Ed. 2510 B
Depth to Water Surface
7.00
feet
7/19/10 12:40
RDM
Field Measurement
Nitrate as N
0.933
mg/L
7/20/10 16:17
TDA
EPA 300.0
Nitrite as N
<0.0300
mg/L
721/10 10:48
TDA
EPA 300.0
pH, Field Test
4.19
pH Units
7119/10 12:40
RDM
Field
Total Dissolved Solids
28.0
mg/L
720/10 11:20
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
17
mg/L
7/21110 10:48
TDA
EPA 300.0
Temperature
26
eC
7/19/10 12:40
RDM
Field
R-4
1007541-04
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method Qualifier
Total Organic Carbon
M Wed by: Kciobac-FayeltevneD n
Chloride
COD, Total
Conductivity
Depth to Water Surface
0.6 mg/L 722110 0:00 ECI SM 5310B
27.8
mg/L
720/10 9:48
TDA
EPA 300.0
<10.0
mg/L
721/10 11:05
ENC
SM 20th Ed. 5220 D
103
umhos/cm
7/27/10 14:56
ARS
SM 20th Ed. 2510 B
7.80
feet
7/19/10 12:30
RDM
Field Measurement
State Cenilications: Respectfully Submitted
NCDNR #11.#693
NCDOH #37714,#37795 ieC�-
USDA #3787 R. W. Sander, VP/Managing Director
Thank you foryour business. We ire teJurfealbackon ourlewl ofremce o,oa Pimre ronmcr the WMw�atgad for. Ron Soeden m 91aa64-1920, Jam,,Nobq PrcddIM(
Jnok,,(dmicmhoceam orTrewrB.,v. CBO, at r6 e(ynicrobac.eom with mry mmmener orrvggestioru.
Page 2 of

Fayetteville Division
2592 Hope Mills Rd 8-B Wendy Court
Fayetteville, NC 28306 Greensboro, NC 27409
910.864.1920 Phone [phone] Phone
910.864.8774 Fax [phone] Fax
Certificate of Analysis
Aliens, Inc
Mr. Martin Griess Project: NMellssamples-3/Vearly Date Reported:
Turk Turkey Highway
Date Received: July 19, 2010 Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: July 19, 2010
R-4
1007541-04
Analyte
Result
Unit
Analysis Date/lime
Analyst
Method Qualifier
Mxlymd by: Moroba[ -Feyet eLWteGn
Nitrate as N
4.85
mg/L
7/20/10 16:17
TDA
EPA 300.0
Nitrite as N
<0.0300
mg/L
7/20/10 9:48
TDA
EPA 300.0
pH; Field Test
4.04
pH Units
7/19/1012:30
RDM
Field
Total Dissolved Solids
58.0
mg/L
7/20/10 11:20
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
16
mg/L
7120/10 9:48
TDA
EPA 300.0
Temperature
30
°C
7/19/10 12:30
RDM
Field
Qualifier Definitions
State Certifications: Respectfully Submitted
NCDNR #11. 9693
NCDOH #37714,#37795 "��_ ICJ'
USDA 93787 R. W. Sandms, VP/Monaging Director
Thank you toryour business. Weimime urfaedbackonovrlewlofser eeto/m,. P/evsemnmcuhe VP/Mamgilg�iren°q Ron Sanders m9l0dW-T9TB, Jamer Nokex, Psesidem, or
jnokn(gmicrvDac.rom or T ,o,Bxe,CEO,
Page 3 of3

Fayetteville Division
2592 Hope Mills Rd
8-B Wendy Court
Fayetteville, NC 28306
Greensboro, NC 27409
910.864.1920 Phone
336.856.9710 Phone
910.864.8774 Paz
336.856.9711 Fax
Certificate of Analysis
Allens, Inc
Mr. Martin Gress Date Reported: August 4, 2010
Project: MlNells samples-3/Yearly Date Received: July 19,2010
5900 Turkey Highway y
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: July 19, 2010
R-5a
1007545.01
Analyte Result Unit Analysis Datetrime Analyst Method Qualifier
nns cay:c
Total Organic Carbon
2.3
mg/L
7/22/10 0:00
ECI
SM 5310B
Ar Wal or. htiaobac- FayeUawre Oivlsion
Chloride
9.21
mg/L
7/20/10 9:48
TDA
EPA 300.0
COD, Total
39.9
mg/L
7/21/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
160
umhos/cm
7/27/10 14:56
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
6.40
feet
7119/10 12:20
RDM
Field Measurement
Nitrate as N
9.25
mg/L
7/20/10 16:17
TDA
EPA 300.0
pH, Field Test
4.03
pH Units
7/19/10 1220
RDM
Field
Total Dissolved Solids
116
mg/L
7/20/10 11:20
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
23
mg/L
7/20/10 9:48
TDA
EPA 300.0
Temperature
33
°C
7119/10 12:20
RDM
Field
R-6
1007545-02
Analyte Result Unit Analysis Date/Time Analyst Method Qualifier
An W. .
Total Organic Carbon
9.7
mg/L
7/22/10 0:00
ECI
SM 5310B
7aWyzed by: hllaobac- Fayetteville Dv on
Chloride
23.4
mg/L
7/21/10 10:48
TDA
EPA 300.0
COD, Total
54.1
mg/L
7/21/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
163
umhos/cm
7/27/10 14:56
ARS
SM 2I11h Ed. 2510 B
Depth to Water Surface
7.20
feet
7/19/10 12:10
RDM
Field Measurement
Nitrate as N
1.66
mg/L
7/20/10 16:17
TDA
EPA 300.0
pH, Field Test
5.05
pH Units
7/19/10 12:10
RDM
Field
Total Dissolved Solids
112
mg/L
7121/10 9:45
AMM
SM 20th Ed. 2540 C Sl
Sulfate as SO4
25
mg/L
7/21/10 10:48
TDA
EPA 300.0
Temperature
30
°C
7/19/10 12:10
RDM
Field
R-7
1007545-03
State Certifications: Respectfully Submitted
NCDNR #11,#693
NCDOH #37714,#37795
USDA #3787 R. W. Sanders, VP/Managing Director
Thank you for your trusiness. We izrvirq°urJeeJback on our /eey oJzeniceroyvu. Pleaze conracr the VY/Almngirg Dyrenor. Ron Saarlenar 9/0.86J-1910,J es Notre; YresiJent ar
jmke.ArymcwMc.conr or Trewr Boyce. CEO. a rbo)<xQnricrobac.rom nirh arty rommenu °rrvgyesriam.
Page 7 of 3

Fayetteville Division
2592 Hope Mills Rd
8-13 Wendy Court
Fayetteville, NC 28306
Greensboro, NC 27409
910.864.1920 Phone
336.856.9710 Phone
910.864.8774 Fax
336.856.9711 Fax
Certificate of Analysis
Aliens, Inc
Mr. Martin Grim Project: M/Wellssamples-3/Yearly Date Reported: August 4, 2010
5900 Turkey Highway Date Received: July 19, 2010
Turkey NC, 28393 Sampled By: Robin Miller
Date Sampled: July 19.2010
Analyte
Result
Unit
Analysis Date/Time
Analyst
Method
Qualifier
M Weae: ra
Total Organic Carbon
4.6
mg/L
7/22110 0:00
ECI
SM 5310B
Malytai by: M crobac- Fayetteville wsbn
Chloride
29.8
mg/L
721110 10:48
TDA
EPA 300.0
COD, Total
17.7
mg/L
721/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
125
umhos/cm
7/27/10 14:56
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
6.00
feet
7/19/10 12:00
RDM
Field Measurement
Nitrate as N
0.551
mg/L
720/10 16:17
TDA
EPA 300.0
pH, Field Test
4.11
pH Units
7/19/10 12:00
RDM
Field
Total Dissolved Solids
73.0
mg/L
721/10 9:45
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
9.4
mg/L
7/21/10 10:48
TDA
EPA 300.0
Temperature
27
°C
7/19/10 12:00
RDM
Field
R-S
1007545-04
Analyte
Result
Unit
Analysis Date/fime
Analyst
Method
Qualifier
A Wecl by: ra
Total Organic Carbon
0.7
mg/L
722/10 0:00
ECI
SM 5310B
M Wed try: Kcrobac- FayMteviOe omsbn
Chloride
35.9
mg/L
721/10 10:48
TDA
EPA 300.0
COD, Total
<10.0
mg/L
721/10 11:05
ENC
SM 20th Ed. 5220 D
Conductivity
363
umhos/cm
727/10 14:56
ARS
SM 20th Ed. 2510 B
Depth to Water Surface
6.40
feet
7/19/10 11:50
RDM
Field Measurement
Nitrate as N
35.9
mg/L
7/20/10 16:17
TDA
EPA 300.0
pH, Field Test
3.80
pH Units
7/19/10 11:50
RDM
Field
Total Dissolved Solids
259
mg/L
721/10 9:45
AMM
SM 20th Ed. 2540 C
Sulfate as SO4
20
mg/L
721/10 10:49
TDA
EPA 300.0
Temperain a
30
°C
7/19/10 I1:50
ROM
Field
R-9
1007545-05
Analyte
Result
Unit
Analysis Date/rime
Analyst
Method
Qualifier
State Cefcabons:
Respectfully Submitted
NCDNR #11. #693
_s
:rC- �'�
NCDOH 937714, #37795
_ r91r-4rt.c.Y•'t/.•5.
USDA #3787
R. W. Sanders, VP/Managing Director
Thank you for your business. Weimiieyvurfe mkonourkwlofsernarro .
Please roman the WWamgiMl ton Rona en at 910,86 1920, J=n Nokes. Prcside4 at
jnoke.C.�mismba<.mm or TmrorBokay. CEO. a
Page 2 of3

Fayetteville Division
2592 Hope Mills Rd
8-B Wendy Court
Fayetteville, NC 28306
Greensboro, NC 27409
910.864.1920 Phone
336.856.9710 Phone
910.864.8774 Fax
336.856.9711 Fax
Certificate of Analysis
Allen, Inc
Mr. Martin Griess Project: MflVellssamples-311irm ly Date Reported: August 4, 2010
5900 Turkey Highway Date Received: July 19, 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: July 19, 2010
AWWW W. EQ
Total Organic Carbon
M Vzed br. Kco c-Faytlten9e eiriJon
Chloride
COD, Total
Conductivity
Depth to Water Surface
Nitrate as N
pH, Field Test
Total Dissolved Solids
Sulfate as SO4
Temperature
5.3
mg/L
7/22/10 0:00
ECI
SM 5310B
11.6
mg/L
7/20/10 9:48
TDA
EPA 300.0
58.6
mg/L
7/21/10 11:05
ENC
SM 20th Ed. 5220 D
411
umhos/cm
7/27/10 14:56
ARS
SM 20th Ed. 2510 B
7.60
feet
7/19/10 11:25
RDM
Field Measurement
1.79
mg/L
7/20/10 16:17
TDA
EPA 300.0
3.98
pH Units
7/19/10 11:25
ROM
Field
295
mg/L
7/21/10 9:45
AMM
SM 20th Ed. 2540 C
130
mgfL
7/22110 17:53
ENC
EPA 300.0
30
°C
7/19/10 11:25
RDM
Field
Qualifier Definitions
SI Relative Percent Difference(RPD) outside accepted recovery limits
State Certhcabons: Respectfully Submitted
NCDNR #11. M93
NCDOH #37714. #37795 A?. Rim. r�r-e reaYu.5.
USDA #3787 R. W. Sanders, VP/Mmaging Director
Thank you foryour business. Wr imireyovrJeedhack on aurinsl aJser.ia to ° Please roman Cher WornginglNrecroq Ron Samkrsar. 91086t-19I0,JamesNAo, President.
jre.trr!ymicmbac.rom or 7nmrHoe,CW, ar rbayce(a/nicmhac.rom with°nyc=mrou orsoggesdoos.
Page 3 of

GW-59A COMPLIANCE REPORT FORM Permit #W0 W qq6,?
(Submit one each monitoring period with GW-59 jorms.)
I
Enter date monitoring results were due. (£f- 3 -) o ) Will this monitoring report (GW59 and GW59A)
YES
NO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
O
IF the answer to question 1 or 2 is 'YES ; list in the space provided below the well identification numbers) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
identification plate, area overgrown, etc)? Ifthe answer is "Yes", contact the Regional Office for guidance.
4
Are any monitored constituents equal to or above the established standards?
ES
NO
If the answer to question 4 is 'NO", skip to section B.
Ifthe answerto question 41s "YES"list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.
IhW d# l T55 _ 55) M311 mw3+y - Nitr4k _ 10.3 ri,5#-
mtu 4 I Ni-ka% _ )a.a m5 jL iv,4rale
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
If the answer to question 5 is 'NO', slip to section 8.
If the answer to question 5 is "YES" list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
A 8 - vi+rJe— leveh hi5i% 5inc� tuel( insfa/l .0 -
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
O
If the answer is "YES" a groundwater quality problem maybe occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. if the answer is "NO", monitoring wells maybe improperly
located; contact the Regional Office.
7
Is the pennittee implementing previously approved actions required by the Division involving this
YES
O
groundwater quality problem?
If the answer to question 7 is 'YES; describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days: an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Wo/adon,
fines, andfor penalties.
g
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge. that the above information was evaluated and the. information submitted in this
report (Compliance Repori G,W-59A) is true and complete to the best of my knowledge. ,.
I �fc)
S�ignature of Pennittee (or Authorized Agent) Date
GW-59A 12/3/2003

Li
r
O dY MEN O RIB SIIV Cg
Quality Vegetables • Q
0 5900 TURKEY HIGHWAY, TURKEY, NORTH CAROLINA'"`'_83
PHONE [phone] /
PAX 910—..596-0127 Uj 1xb
April 30, 2010 () Q
Dept. of Environmental &Natural Resources
6S.
Division of Water Quality — Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
[phone]
RE: Groundwater Quality Monitoring Report
Allen, Inc. — Turkey, NC Facility
Permit # W00004268
Enclosed are the original and one copy of the Groundwater Monitoring Report on forms GW-59
and GW-59A, and the lab report for Allen, Inc — Turkey, NC facility for samples collected in
March, 2010..
If you have any question or require any additional information, please contact Reid Wells by
phone at [phone] ext # 115 or by email at [e-mail].
m Sincerely c �(
*Martin Griess
Plant Manager
Aliens, Inc. Turkey facility
CC: Laura Mnhinski, Aliens, Inc
Reid Wells, Aliens, Inc — Turkey facility
a
DENR-FAYEMLLEREGIONAL 04;0i

SUBMIT FORM ON YELLOW PAPER ONLY
..
OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING;
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
,.DEPARTMENT
!
617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
t Cl e Pd snee e
FACILITY INFORMATION Plea - M orT �
PERMIT Number. Expiration Date: JUIy'31„ 2011
Facility Name: Aliens; Inc. -Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remedialion: Infiltration Gallery
Turkey '(c""') NC 28393-9703 County SaITIPSOn
(fitly) (LI]Yei (Zip)
® Spray Field ❑ Remediation:
Contact Person: Martin Griess
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/SiteName:
No. of wells tobe sampled:.. 13
❑ Water Source Heat Pump ❑ Other:
'cam Penh
SAMPLING INFORMATION
-
_
If WELL
WELL ID NUMBER (from Permit): MW-1
Date sample collected:. 3/1/10
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: - in.
pH 5.20 units Temp. 19.1 eC
DRY at
Depth to Water Level: 20.8 ft. below measuring point
Screened Interval: _ft.
to _ft,
Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/bailed before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO andfield acidified: ❑ YES'.
❑ NO
LABORATORY INFORMATION.
Date sample analyzed: -
-
Laboratory Name: Mierobac Laboratories _ Certification No. NC#11 NC#37714
PARAMETERS NOTE:'. Values should reflect dissolved and colloidal concentrations.
COD 11 mg/I
Nitrite (NO2) as N
mg/I
Pb - Lead mgll
Coliform: MF Fecal /loom)
Nitrate (NO3) as N
.12.m9A
Zn- Zinc mg/I
Coliform: MF Total /100ml
Phosphorus:. Total as P
mg/I
(Note; Use MPN method car highly turbid aarwae)
Orthophosphate
mg/t
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total <25.0,mgll
AI -Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mg/I
�'� _ <. I V -�-,
TOC 1.7 mgn
Ca - Calcium -
mg/I
Chloride 18.3mg/I
Cd- Cadmium -
mg/I
_MAY�ntn
Arsenic mg/l
Chromium: Total
mg/I
Grease and Oils mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC%M �LoLr �'e;ac'rig. llnit
V M fir..
Phenol mgA
Fe -Iron
mg1l
(Specify test and method #. ATTACH LABREPORT.)
Sulfate 29.3mgn
Hg- Mercury
mg/I
Report Attached? ❑ Yes(1) ❑-No(0)
Specific Conductance 313µMhos
K- Potassium
mg/I
VOC ,method# _
Total Ammonia _ moll
Mg - Magnesium
mg/I
,method#
(Ammonia Nitrogen; NH3as N; Ammona Mtragen, Total)
Mn- Manganese
mg/I
,method#
TKN as N mg/I
Ni - Nickel
mgA
, method #
For RemedlationSystems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: _ mg/L VOC Removal%
Martin Griess, Plant Manager
Pennines, (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007
P.

EPARTMENT OF ENVIRONMENT 6 NATURAL RESOUR
TY MONITORING: NISION OF WATER QUALITY -INFORMATION PROCESf
FORM 1117 MAIL SERVICE CENTER, RALEIGH, NC 276204 till
Name: Aliens; Inc. - Turkey _
Name (if different)_:
Address: 5900 Turkey Highway
q (m,d) NC 28393-9703 County Sampson
act Person: Martin Griess Telephone#: [phone] I
Location/Site Name: - No. of wells to be sampled: 13
from Pemrel
PILING INFORMATION
LID NUMBER (from Permit): MW-2 Date sample collected:: 311/10
Depth: ft. Well Diameter: _in.
h to Water Level: 8.2 ft. below measuring. point Screened Interval: ft. to _ft.
luring Point is -ft. above land surface Relative M.P. Elevation: ft.
Tie of water pumped/bailed before sampling: 1 D+ gallons
er: Expiration Date:
WQ0004268 UIC_
Other
PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑,Remediation Infiltration Gallery
® Spray Field ❑ Remedistion:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:'
FIELD ANALYSES:
pH 5.38 units Temp. 15.0 aC
Spec. Cond: µMhos
Odor
Appearance
nple analyzed: Laboratory Name:. Microbac Laboratories
ETERS NOTE: Values Should reflect dissolved and colloidal concentrations.
COD <%o mg/I Nitrite (NO2) as N mg/I Pb - Lead
COliform: MFFecal /loom] Nitrate (NO3) as N 13 mg/I Zn - Zinc
Coliform: MF Total
/100ml
(Note: Use MPN method for highly turbid samples)
Dissolved Solids: Total
249 mgn
pH (when analyzed)
units
TOb
2.6 mgll
Chloride
161 mg/I
Arsenic
mg/I
Grease and Oils
mgn
Phenol
mg/I
Sulfate
4.18. mg/I
Specific Conductance
511 µmhos
Total Ammonia
mg/I
(AmmoNa Ntrogen; NH, as N; Ammonia Nitrogen; Total)
TKN as N mg/I
Phosphorus: Total as P
mg/I
Orthophosphate
mg/I
AI - Aluminum
mg/I
Be - Barium
mgn
Ca - Calcium
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mgA
Fe - Iron
mg/I
Hg - Mercury
mg/I
K- Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
NI - Nickel
mg/I
Certificatlon No. NC#11 NC#37714
mg/I
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS,. HPLC)
(Specify test and method ,#. ATTACH LAB REPORT.)
Report Attached? ❑ Yes.(1). ❑ No
yOC , method #
method #
method #
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs:.. mg/L VOC Removal%a
Martin Griess, Plant Manager
Permlttee (or Authorized Agent) Name and. Title - Please print or type
GW-59 Rev. 112007
at
Of

auemn r�nm ury �r•_.yr w� n+rert urv�r
MONITORING:
Aliens, Inc. -Turkey
Address:
County Sampson
act Person: Martin Griess Telephone#: [phone]
Location/Site Name: No, of wells to be sampled: 13
prom Pem n
PLING INFORMATION
L 10 NUMBER (from Permit): MW-3 Date sample collected:. 311110
Depth: ft. Well Diameter: _in.
i to Water Level: 3.7 fl.'below measuring point Screened Interval: —ft. to —ft.
luring Point is ft. above land surface Relative M.P. Elevation: ft.
ne of water pumped@ailed before sampling:. 10+ gallons
MAIL SERVICE CENTER. RALEIGH, No 27699-1 a17
Number: Expiration Date:.
.harge WQ0004268 'UIC_
Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon❑Remediation::Infiltration Gallery
® Spray Field ❑ Remedialion:,
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES: WAS
PH ..6.0 units Temp. 12.0 eC DRY at
Spec. Cond. µMhos time of
Isarrinfin
Odor _
Appearance
sample analyzed: _ Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714 `
%METERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD <10.0mg/l Nitrite (NOg)as.N mgA Pb - Lead mg/I
Coliform: MF Fecal /100m1 Nitrate (NO3) as N <0A mg/I Zn- Zinc -Mg/1
Coliform: MF Total
/100ml
(Note: Use MPN method terhlghly areld samples)
Dissolved Solids: Total
246 mgA
PH (when analyzed),
units
TOC
2.3 mgA
Chloride-
15.6 mgA
Arsenic
mg/I
Grease and Oils
mg/I
Phenol
_ mg/l
Sulfate
57.5 mgn
Specific Conductance
378µMhos
Total Ammonia
.. _mgA
(Ammonia Nitrogen; NH,os N; Ammonia Nitrogen, Total)
TKN as N mgA
Phosphorus: Total as P
mgA
Orthophosphate
mg/I
Al -Aluminum
mgA
Be - Barium
mgA
Ca -Calcium
mgll
Cd- Cadmium
Mg/I
Chromium: Total
mg/I
Cu- Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K-_Potassium
mg/l
Mg - Magnesium
mg/l
Mn - Manganese
mg/l
Ni- Nickel
mg/1
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LABREPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method #
method #
method #
method #
For Remedlatlon Systems Only (Attach Lob Reports): Influent Total VOCs: mg/L. Effluent Total VOCs mg/L VOC Removal%
Martin Griess, Plant Manager
Perminee (or Authorized Agent) Name and Title - Please limit or type
GW-59 Rev. 112007
7

SUBMIT FORM ONYELL12W PAPER ONLY
•DIVISION
DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:'
OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27690.1617 Phone: (919)73gJ221
FACILITY INFORMATION - Please Pont Clearly or Type -
PERMIT Number: Expiration Date: I duly 31, 2011
Facility Name: Allens„Inc. - Turkey
_ _.
Non -Discharge WQ0004268 UIC
Permit Name (if different):
-
NPDES Other
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
_
Turkey" NC 28393-9703 County Sampson
_
❑ Lagoon ❑ Remediation' Infiltration Gallery
lG3l rant=7. l4)
®.Spray Field ❑ Remedialicn:
Contact Person: Martin Griess
Telephone#: [phone]
❑ RotaryDistributor ❑.Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
Rom PemN
SAMPLING INFORMATION
- - -
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected: 311/10
FIELD ANALYSES: -
AS
Well Depth: IL
Weil Diameter:
pH 4.46 units Temp. 151 aC.
DRY at
Depth to Water Level: 5.9 ft; below measuring point
Screened Interval: ft.
—
to
ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft: above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/balled before sampling:
10+gallons
Appearance
here: ❑
Samples for metals were collected. unfiltered: DYES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Mierobao' Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD <10.0 mg/I
Nitrite (NO,) as N
mg/I
Pb -.Lead mg/I
Coliform: MF Fecal NOOm[
Nitrate (NOO as N
7.43 mg/I
Zn - Zinc mg/l
Coliform: MFTotal /loom!
Phosphorus: Total as P
mg/I
(Note: Use. MPN melt it for highly tumid eamplw)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved' Solids: Total 68.0mg/I
AI - Aluminum
mgA
pH (when analyzed) .units
Be - Barium
mg/I
_
TOC 0.6 mgA.
Ca- Calcium -
mg/l
Chloride 16.2 mgA
Cd - Cadmium
mg/I
Arsenic mgA
Chromium: Total
mg/I
Grease and Oils mg/I
Cu - Copper
mgA
ORGANICS: (by GC/MS', HPLC)
Phenol mgA
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 2.34 mgll
Hg - Mercury
mg/I
Report Attached? ❑ Yes (i) ❑ No (0)
Specific Conductance 149µMhos
K- Potassium
mg/I
VOC ,method#
Total Ammonia mgA
Mg - Magnesium;
mg/I
-, method #
(Ammonia Nitrogen; NNsas tZ Ammonia Nitrogen; Total)
Mn- Manganese;
mg/I
,method .#
TKN as: N mgA
Ni - Nickel
mg/I
, method #
For Remedtatlon Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/LVOC Removal%
Marlin Griess; Plant Manager
Permiftee (or Authorized AgenO Name and Title- Please, print or type
GW-59 .Rev. 112007

SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT & NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phonr._(9191 797J221
FACILITY INFORMATION
Please Print Clearlyor type -
PERMIT Number: Expiration Date: July 31, 2011
Facility Name: Allens, Inc. - Turkey
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
Turks fstme)
NC 28393-9703 County. Sampson
❑ Lagoon❑.Remediation:Infiltration Gallery
(Ot')
(z"t") 00
©. Spray Field ❑ Remediation:
Contact Person: Martin Griess
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site.Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump D Other:
tram Pmmit
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): R-1
Date sample collected: 3/1110
FIELD ANALYSES:
WAS
Well Depth: ft..
Well Diameter:
pH 5.30 units Temp. 11.6oG
DRY at
Depth to Water Level: 5.4 ft.'below measuring point
_in.
Screened Interval:
to
Spec. Cond. µMhos
time of
_ft.
—ft.
sampling,
Measuring Point is ft, above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumpedibailed before sampling:
10+gallons
Appearance
here:❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed: -
- -
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
GOD
45.9 mg/I
Nitrite (NO,) as N
mgn
Pb - Lead mgA
Coliform: MF Fecal
/loom]
Nitrate (NO3) as N
0.35 mgA
Zn - Zinc ni
Coliform: MF Total
/loom)
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly turbid samples)
Orthophosphate.
mg/l
Other (Specify Compounds. and Concentration Units):
Dissolved Solids: Total.
61.0mgn
AI -Aluminum
mgA'
pH (when analyzed).
units
Be - Barium
ni
TOC
6.7' mg/l
Ca —Calcium
mgA
Chloride
8.61_ mgA
Cd - Cadmium
mgA
Arsenic
mg/l
Chromium: Total.
mg/l
Grease and Oils
mgA
Cu - Copper
mgA
ORGANICS: (by GC, GC/MS„HPLC)
Phenol
mgA
Fe - Iron
mgA
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate
12.7 ni
Hg - Mercury
mg/I
Report Attached? ❑ Yes (1) ❑. No (0)
Specific Conductance
90.0 AMhos.
K.- Potassium
mg/l
VOCmethod #
Total Ammonia -.
mg/I
Mg - Magnesium
mgA
, method #
(Ammonia Nitrogen; N%os N; Anunsnia Moogen, Tow) -
Mn - Manganese
mgA
; method #
TKN as N
mgA
Ni - Nickel
mglt
, method #
For RemedlatiomSystems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Totel'VOCs: _ mg1L VOC Removal"s%
Martin Griess, Plant Manager
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev. 112007

SUBMIT FORM ONYELI.OW PAPER ONLY
DEPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER OUALITY4NFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM _
917 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 732a221
FACILITY INFORMATION Pease Print Clearly or Type
PERMIT Number: Expiration Date;. JUI 31,'.201-1
Facility Name: Aliens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES. Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediationi Infiltration Gallery
Turkey 15"'l) NC 28393-9703 County Sampson
Ply) asp:-1 Ie,P)
© Spray Field ❑ Remediation:
Contact Person: Martin Grless
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other: -
lromPamN
SAMPLING INFORMATION
-
If WELL
WELL ID NUMBER (from Permit): R-2a
Date sample collected: 3/1/10
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
pH 5.17 units Temp. 11.6 aC
DRY at
Depth to Water Level: 5.9 ft. below measuring point
_in.
Screened Interval:. ft.
—
to
-ft. Spec. Cond. µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/bailed.before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑YES
❑ NO
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values shouldreflect dissolved_ and colloidal concentrations.
COD 106 mg/I
Nitrite (NO2) as N
mgA
Pb - Lead mg/I
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
0.69 mg/l
Zn - Zinc mgn
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for hIghly habld Naples) -
.Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 94.0mgn
Al -Aluminum
'mgA
pH (when analyzed) units
Ba -Barium
mgA
TOC 5.3 mg/I
Ca - Calcium
mgA
Chloride 8.88 mg/I
Cd- Cadmium
mg/I
Arsenic mg/I
Chromium: Total
mg/I
Grease and Oils mg/l
Cu- Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 45.3 mg/i
Hg - Mercury .
_mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance. 174 µMhos
K - Potassium
mg/l
VOC , method #
Total Ammonia mgA
Mg - Magnesium
mgA
, method #
(Ammonla Nitrogen; NHrei N: Ammonia Nitrogen, Total)
Mn- Manganese
mgA
,method#
TKN as N mg/I
Ni - Nickel
mgA
, method #
For Remedlatlon Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Martin Griess, Plant Manager
Pennitlee (or Authorized Anent) Name and Title - Please Print or type Signature of Pennittee (or Authorized Agent) (Date)
GW-59 Rev. 112007

'SUBMIT FORM ON YELLOW PAPER ONLY
EPARTMENT OF ENVIRONMENT 6 NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
, , ,DIVISION
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number:.. Expiration Date: July 31, 2011
Facility Name: Aliens, Inc.-Turkey
Non-Discharge WQ0004268 UIC
NPDES Other
Permit .Name (if dif(erent):,
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration. Gallery
Turkey l€""') _ NC 28393-9703 County Sampson
(ce;)
Is�:n lLP1
® Spray Field ❑ Remediation:
Contact Person: Martin Gdess
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Sfte Name:
No. .of wells to be sampled: 13
❑ Water Source Heat Pump El Other
from Pamn
SAMPLING INFORMATION.
if WELL
WELL ID NUMBER (from Permit): R-3
_ _
Date sample collected: 311/10
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH 4.53 units. Temp. 10.1 °C
DRY at
Depth to Water Level: '7.3 ft.. below measuring point
Screened Interval: ft.
to
ft. Spec. Cond, µMhos
time of
sampling,
Measuring Point is ft. above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/bailed before sampling:'
10+ gallons
Appearance
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑:NO and field acidified: ❑ YES
ONO'
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac. Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD
13.6 mg/l
Nitrite (NO2) as N
mg/I
Pb - Lead mgA
Coliform: MF Fecal
/100ml
Nitrate (NO3) as N
1.84 mg/1
Zn -.Zinc mg/I
Coliform: MF Total
/100ml
Phosphorus: Total as P
mgA
(Notes Use MPN method for highly turbidsemplas)
Orthophosphate
mg/i
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
34.0 mg/l
AI -Aluminum -
mgp
pH (when analyzed)
units
- Be -Barium,
mgA
TOC
0.8 mg/l
Ca -Calcium
mg/I
Chloride
5.20 mgA
Cd - Cadmium
mgA
Arsenic
mgA
Chromium: Total
mgA
Grease and Oils
mg/I
Cu - Copper
mg/t
ORGANICS: (by GC, GC/MS', HPLC)
Phenol
mg/l
Fe -Iron
mgA
(Specify test and method #. .ATTACH LAB REPORT.)
Sulfate
11.4mgA
Hg-Mercury
mgA
Report Attached? ❑ Yes(1) ❑ No,(0)
Speck Conductance
82.8 µMhos
K - Potassium
mg/l.
VOC , method #
Total Ammonia
mg/l
Mg - Magnesium -
mgA
, method #
(Ammanie Nio-ogm NHsas N:Ammcnla Ndragen, Tow)
Mn - Manganese.
mg/l
, method #
TKN as N
mgh
Ni - Nickel
mg/I
method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOCRemoval%
Martin Griess, Plant Manager
Families (or Authorized Agent) Name and Title -Please, print or type
GW59 Rev. 112007

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
.•
EPARTMENT OF ENVIRONMENT &NATURAL RESOURCES
NISION OF WATER QUALITYdNFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
,
817 MAIL SERVICE CENTER, RALEIGH, NO 27699.1617 Phone: [phone]
FACILITY INFORMATION
Please Pdnt Curdy or Type
PERMIT Number: Expiration Dale:. July'31,2011
Facility Name: Aliens, Inc. - Turkey
Non -Discharge W00004268 UIC
NPDES. Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Turkey 1e1e0 NC 28393-9703 County SaMPSOR
1Gmr
(-'1=) (")
® Spray Field ❑ Remediation:
Contact Person: Martin Griess
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No. of wells to be sampled:
- 13
❑ Water Source. HeatPump ❑ Other.,
Imm Pemd
SAMPLING' INFORMATION
-
-
If WELL.
WELL to NUMBER (from Permit): R-4
Date sample collected: 3/1/10
FIELD ANALYSES:
WAS -
ell Depth`: ft.
Well Diameter:
pH 4.46 units Temp. 10.1 QC
DRY at
Depth to Water Level: 7.4 ft. below measuring paint
_in.
Screened Interval:
ft. to
ft. Spec,. Cond. µMhos
time of
-
sampling,
Measuring Point Is ft. above land surface
Relative M.P. Elevation:'
ft.
Odor
Volume of water pumped[bailed before sampling:
10+ gallons
Appearance
here: ❑
Sam les for metals were collected unfiltered: OYES
❑ NO and field acidified: ❑YES
❑ NO.
LABORATORY' INFORMATION
Date sample analyzed:
- --
Laboratory Name: Microbac Laboratories Certification No, NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved'. and colloidal concentrations.
_
COD
<10 mg/I
Nitrite (NO2) as N
mg/I
Pb-Lead mod
Coliform: ME Fecal
/loom]
Nitrate (NO3) as N _
3,32 mg/l
Zn -Zinc mgA
Coliform: ME Total
/loom]
Phosphorus: Total as P
mgA
(Nate;: Use MPNmeamdrorHgNYMbldeamples)
Orthophosphate
mgA
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total
66.0 mg/I '
Al -Aluminum
mg/]
pH (when analyzed)
units,
Be - Barium _
mg/1
TOC
0.7 mg/I
Ca - Calcium
mgA
Chloride
5.94 mg/l
Cd - Cadmium
mgA
Arsenic
mg/I
Chromium: Total
mg/1
Grease and Oils
mg/I
Cu - Copper
mg/I
ORGANICS: (by GC, GCIMS, HPLC)
Phenol
mg/I
Fe - Iron
mgA
(Specify test and method #. ATTACH LABREPORT.)
Sulfate
29.2 mg/I
Hg - Mercury.
mg/I
Report Attached?' ❑ Yes (1) ❑ No (0)
Specific. Conductance
145.pMhos
K- Potassium
mgn
VOC. , method #
TotalAmmonta.
mg/I
Mg -Magnesium
mg/I
, method #
(Ammonia Nitrogen;NN,ae N:A-0nia Nieopan,TotWI
Mn- Manganese
mgA
,method#
TKNasN.
mg/I
Nt- Nickel
mg/I
,method#
For Remedlatlon Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mall . VOC Removal%a
Martin Griess, Plant Manager
Permlttee.(or Authorized Agent) Name and Title -Please print or type
GW-59 Rev. 1/2007

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF ENVIRONMENT&NATURAL .RESOURCES
GROUNDWATER QUALITY MONITORING:
OFWATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
,DIVISION
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Pont Clearly or Type
PERMIT Number: Expiration Dater duly 31, 2011
Facility Name: Aliens, Inc., -Turkey
'
Non -Discharge W00004268 UIC -
Permit Name (if different):
NPDES Other _
Facility Address: 590.0_ Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
Turkey Sve_li NC 28393-9703 County Sampson
❑ Lagoon ❑ Remediation: Infiltration Gallery
(C:d) fela!pk (up1.
® Spray Field. ❑Remediation:
Contact Person:. Martin Griess
Telephone#. [phone]
❑ Rotary Distributor ❑ Land, Application of Sludge
Well LocatiaNSite Name:
No, of wells to be sampled:
13.
❑ Water Source Heat Pump ❑ Other:
F. Pem,i
SAMPLING INFORMATION'
-
If WELL
WELL ID NUMBER (from Permit): R-5a
Date sample collected:
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter:
in.
pH 4.48 units Temp. 10.8 "C
DRY at
Depth to Water Level: 5.9 ft. below measuring point
Screened Interval: —
ft. to
ft. Spec. Cond. µMhos
time. of
sampling,
Measuring Point is ft, above land surface
Relative M.P. Elevation:
ft.
Odor
check
Volume of water pumped/bailedbefore sampling:
gallons
Appearance
here: ❑
Samples for metals were collected. unfiltered: DYES
El NO and field acidified:. ❑YES
❑NO.
LABORATORY INFORMATION
Date sample analyzed:
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should_ reflect dissolved
and colloidal concentrations.
COD 75.6 mg/I
Nitrite (NO2)as N
mg/I
Pb - Lead mg/1-
Coliform: MF'Fecal Mooing]
Nitrate (NO3) as N
8.67 mg/I
Zn-Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPNmethod for highly turbid mursolea)
Orthophosphate
. mg/l
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 111 mgli
AI -Aluminum
mg/I
pH (when analyzed) units
Be - Barium
mgll
TOC 2.4 mg/I
Ca. -Calcium
mgn
Chloride 11.0 mg/I
Cd - Cadmium
mgll
Arsenic mg/I
Chromium: Total
mgll
Grease and Oils mg/l
Cu -Copper
mg71
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mgli
(Specify test and method #. ATTACH LAB REPORT.).
Sulfate. 17.2 mgn
Hg-Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance. 213 µMhos
K - Potassium _
_
mg/I
VOC , method #
Total Ammonia mgll
Mg - Magnesium
mgA
, method #
(Ammenla Nmogen;NH.as N(Ammonia Nitmgen.Total)
Mn-Manganese
mg/I
.,method#
TKN as N mg/l
Ni - Nickel
mg/I
, method #
For Remediatlon Systems Only (Attach Lab Reports): Influent Total VOCs: mq/L Effluent Total VOCs: mall. VOC Reril l9a
Martin Griess, Plant Manager
Pennlhee (or Authorized Agent) Name and Title - Please pint or type
GW-59 Rev. 112007

3R QUALITY
REPORT FO
Name: Aliens, Inc. - Turkey
Vame (if different):.
Address: 5900 Turkey Highway
ki 10]
County
act,Personr Martin Griess Telephone#: [phone]
Location/Site Name: _ _ No. of wells to be sampled:.
XSSING UNIT
617 Phone:
Date: _July
WQ0004268 - UIC
)DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
UK Spray Field ❑ Remediation:
❑ Rotary,Distributor ❑ Land Application of Sludge
❑ Water Source. Heat Pump ❑ Other:
-L ID NUMBER (from Permit): R-6
Date sample collected:
FIELD ANALYSES:
WAS
Depth: ft.
Well Diameter:
in,
pH 4.96 units Temp. 11.9 oC
DRY at
th to Water Level: 7.30 ft. below measuring. point
Screened Interval:
ft, to _ft.
Spec. Cond. µMhos
timeof
samplin
suring Point is ft. above land surface
RelativeM.P. Elevation.
ft.
Odor
check
ime of water pumped/bailed before sampling:
gallons
Appearance
here: r
i'lesfor metals were collected unflltered:DYES
El NO and. field. acidified: DYES
❑.NO
-
L
N
!ORATORY INFORMATION
) sample analyzed:
Laboratory Name: Microbac Laboratories
Certification No. NC#11 NC#37714
IAMETERS NOTE: Values should .reflect dissolved
and colloidal concentrations.
COD, 51.9 mg/1
Nitrite (NO2) as N
Mg/1
Pb -Lead mg/I
Coliform:MF Fecal /100ml
Nitrate (NO3) as N
5.51 mg/l
Zn-Zinc mg/I
Coliform: MF Total /100ml
Phosphorus: Total as P
_ Mg/1
(Nola: Use MPN method for highly Wield samples)
Orthophosphate
mg/1
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 118 mgA
AI -Aluminum
.mgA
pH (when analyzed) units
Be - Barium
mg/l
_
TOG 6.3 mg/l
Ca - Calcium
mg/l
Chloride 2.91 mg/l
Cd- Cadmium
mg/1
-
Arsenic mg/I
Chromium: Total
mg/l
'
Grease and Oils _ mg/I
Cu - Copper
mg/1
ORGANICS: (by GC,: GCIMS, HPLC)
Phenol mg/l
Fe - Iron
mg/1
(Specify test and method#. ATTACH LAB REPORT.)
Sulfate 32.8mg/l
Hg- Mercury,
mgA
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance 240 µMhos.
K-Potassium
mg/1
VOC , method #
Total Ammonia mgA
Mg- Magnesium
mgA
, method #
(Ainmonla Nitrogen; NH3 aS N;Anmoma Mtrogan. Total)
Mn- Manganese
mg/I
,method#
TKN as N 'mg/I
Ni - Nickel
mg/l
, method #
For Remedlation Systems Only (Attach Lab Reports): Influent TotalVOCs: mg/L Effluent Total VOCs: mg/L VOC RemovaP/o
Martin Griess, Plant Manager
Permlttee (or Authorized Agent)'. Name and Title • Please print or type
GW-59 Rev. 1/2007

SUBMIT FORM ONYELLOW. PAPER ONLY
GROUNDWATER QUALITY MONITORING:
.•
EPARTMENT OF ENVIRONMENT &.NATURAL RESOURCES
VISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
,.
1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone. [phone]
FACILITY INFORMATION. Please Print clearly or Type
PERMIT Number: Expiration Date: July 31,.2011
Facility Name:_ Allens, Inc, - Turkey
_
Non -Discharge WQ0004268 UIC
NPDES Other
Permit Name (if different):
Facility Address: 5900 Turkey Highway
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
(6tmet)
Turks NC 28393-9703 County Sampson
Ic@Y t"1e1 (2,P)
® Spray Field ❑ Remediatlon:
Contact Person: Martin Griess
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name:
No, of wells to be sampled:
13
❑ Water Source Heat Pump ❑ Other:
Ram PemJl
SAMPLING INFORMATION
-
If WELL
_ WELL ID NUMBER (from Permit): R-7
Date sample collected:. 3/1/10
FIELD ANALYSES:
WAS
Well Depth: ft.
Well Diameter: in.
pH 4.58 units Temp. 12.0PC
DRY at
Depth to Water Level 5.5 ft. below measuring point
Screened Interval: ft.
to
ft. Spec. Cord. µMhos
time
sampling,
Measuring Point is ft. above land surface
Relative M,RElevatton:
ft..
Odor
check
Plume of water pumped/balled before sampling:
10+ gallons
Appearance
here: ❑
Samples for metals were Collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
❑ NO
LABORATORY INFORMATION
Date sample. analyzed:
-
Laboratory Name: Microbac Laboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should. reflect. dissolved and colloidal concentrations.
COD 11.3 mg/I
Nitrite (NO,) as N
mg/l
Pb=Lead mg/l
Coliform: MF Fecal /100ml
Nitrate (NO3) as N
1.78 mg/l
Zn - Zinc mg/I
Coliform: MF Total /100m1
Phosphorus: Total as P
mg/I
(Note: Use MPH method for Nghly turbid samples).
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total. 73.0 mg/I
AI - Aluminum
mg/I
pH.(when ,analyzed) - .units
Be - Barium
mg/I
TOC -3.5 mg/l
_
Ca - Calcium
mg/l
Chloride 27.6 mg/I
Cd - Cadmium.
mg/l
Arsenic rng/l
Chromium: Total
mg/I
Grease and Oils _ mg/l
Cu - Copper
mg/I
ORGANICS: (by GC, GC/MS, HPLC)
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 9.58 mg/l
Hg • Mercury
mg/I
Report Attached? ❑ Yes (1) ❑ No (0)
Specific Conductance 154µMhos
K- Potassium
mg/l
VOC ,method ,#
Total Ammonia mg/I
Mg— Magnesium
mg/I
, method #
(Ammonia Nitrogen; NH.ae 17Ammonl9Nitrngen, 76
Mn- Manganese
mg/l
,method#
TKN as N mg/I
Ni - Nickel
mg/1'
,.method #
For Remediation Systems Only (Attach Lab Reports):. Influent Total VOCs: mg/L Effluent Total VOCs: _ _ _molt. VOC Removal%. _
Martin Griess, Plant Manager
Permittee (or Authorized Anent) Name and Tile- Please Print or We
GW-59 Rev. 112007

SUBMIT FORM ON YELLOW PAPER ONLY
'
. .DEPARTMENT
OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM
16117 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: [phone]
FACILITY INFORMATION Pease Prfnt C/eady or Type -
PERMIT Number: Expiration Date:. July 31, 2011
Facility Name: Aliens„ Inc. - Turkey
Non -Discharge WQ0004268 UIC
Permit Name (if different):
NPDES Other
Facility Address: 5900_Turkey Highway
TYPE OF PERMITTED OPERATION. BEING MONITORED
El Lagoon El Remediation: Infiltration Gallery
_
Turkey ("',eQ NC 28393-9703 County_ Sampson
Ic,yl (cute) (Lp)
® Spray Field ❑ Remediation:
Contact Person: Martin Griess
Telephone* 910-596-0028
❑ Rotary Distributor ❑ Land. Application of Sludge
Well Location/Site Name:
No. of wells. to be sampled:
13
❑. Water Source Heat Pump ❑ Other:
-
hom PemN
SAMPLING INFORMATION
- - -
-
-
If WELL
WELL ID NUMBER (from Permit): R-8
Date sample collected: 3/1110
FIELD ANALYSES:,
WAS
Well. Depth: ft.
Well Diameter:
pH 4.49 units Temp. 12.0 eC
DRY at
Depth to Water Level: 5.3 ft. below measuring paint
_in,
Screened Interval: _ft.
to
ft. Spec. Cond. µMhos
time of
sampling,
MeasuringPoint is ft. .above .land surface
Relative M.P. Elevation:.
8.
Odor
check
Volume of waterpumped/bailed before sampling:. 10+ gallons
Appearance.
here: ❑
Samples for metals were collected unfiltered: ❑YES
❑ NO and field acidified: ❑ YES
NO
LABORATORY
Date sample analyzed:
Laboratory Name: MicrobacLaboratories Certification No. NC#11 NC#37714
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD <10.0 mg/I
Nitrite (NO,) as N
mg/I
Pb - Lead mg/l
Conform: MF Fecal /100ml
Nitrate (NO3) as N
30.7 mg/i
Zn - Zinc mg/l
Coliform: MF Total /100ml
Phosphorus: Total as P
mg/I
(Note: Use MPN method for highly Wrold samples)
Orthophosphate
mg/I
Other (Specify Compounds and Concentration Units):
Dissolved Solids: Total 222mgn
AI -Aluminum
mg/I
pH (when analyzed) .units
Be - Barium
_ mg/I
_
TOC 0.7mg/I
Ca- Calcium
mg/I
Chloride _ 18.9 mg/1
Cd - Cadmium
'mg/I
Arsenic. mg/I
Chromium: Total _
mg/l
Grease and Oils mg/I
Cu - Copper
mg/l
ORGANICS: (by GC, GC/MS, HPLC),
Phenol mg/I
Fe - Iron
mg/I
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 12.7mg/i
Hg- Mercury
mgll
Report Attached? ❑ Yes(1) ❑ No
Specific Conductance, _ 379 lWhos
K- Potassium
mg/1
VOC ,,method#
TotalAmmonia mg/l
Mg - Magnesium
mg/I
..,method#
(Ammonia Nitrogen: NH,a N; Ammonia Ningon, Total)
Mn-Manganese,
mg/I
method #
TKN as N. mgA
'Ni - Nickel;
mg/I
, method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg7L VOC Removal%,
Martin Griess, Plant Manager
Permittee (orAutharized Agent) Name and Title • Please print or type
GW-59 Rev. 1/20D7

liq iul
ONLY
DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES
GROUNDWATER QUALITY MONITORING: ,DIVISION OF WATER OUALITY-INFORMATION PROCESSING UNIT
COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: [phone]
FACILITY INFORMATION Please Print Clearly or Type .PERMIT Number: Expiration Date: July 31, 2011.
Facility Name: Aliens, Inc. - Turkey Non -Discharge WQ0004268 UIC'
Permit Name (if different):. NODES Other
FacilityAddress: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED
Turk: (sv0L0 NC 28393-9703 County Sampson ❑ Lagoon ❑ Remedlation: Infiltration Gallery
(cnn - ggyarm (zp)
®Spray Field ❑.Remedlation;
Contact Person: Martin Griess Telephone#: [phone] ❑ Rotary Distributor ❑ Land Application of Sludge
ell Location/Site Name: No, of wells to be sampled: 13 ❑. Water Source Heat Pump ❑ Other:
LID NUMBER (from Permit): R-9 Datesample collected:
Depth: ft. Well Diameter: —in.
i to Water Level: 8.50 ft. below measuring point Screened Interval: _fit to _ft.
wring Point is ft, above land surface Relative M.P. Elevation: ft.
ne of waterpumped/bailed before sampling:. gallons
COD
56.8 mg/I
Coliform: MF Fecal
/100ml
Coliform: MF Total
hooml
(Note: Use. MPN method for highly tumid samples)
Dissolved Solids: Total
148 mg/I
pH(when 'analyzed) ._
units
TOC
2.7 ni
Chloride
4.18 mgll
Arsenic
mg/I
Grease and Oils
mgll
Phenol
mg/I
Sulfate,
47.3 mg/I
Specific. Conductance
251 µMhos
Total Ammonia
- 'mg/I
(Ammonla Nitrogen; NHsas IT; Ammonla Nitrogen. Total)
TKN..as N mg/1
FIELD ANALYSES:
pH 4.44 units Temp. 12 °C DRY at
Spec..Cond. µMhos time of
eamolin
Odor _
Appearance
Laboratory Name: Microbac Laboratories-
colloidal concentrations.
Nitrite. (NO2) as N mg/I Pb - Lead
Nitrate (NO3) as. N 12.3 mgll Zn - Zinc
Phosphorus: Total as.P mg/I
Orthophosphate
mg/I
AI - Aluminum
mg/I
Be - Barium
mgA
Ca -Calcium
_
mg/I
Cd - Cadmium
mg/I
Chromium: Total
mg/I
Cu - Copper
mg/I
Fe - Iron
mg/I
Hg - Mercury
mg/I
K-.Potassium
mg/I
Mg - Magnesium
mg/I
Mn - Manganese
mg/I
Ni-'Nickel
mg/I
Certification No. NC#11 NC#37714
mgll
Other (Specify Compounds and Concentration Units):
ORGANICS: (by GC, GC/MS', HPLC)
(Specify test and method #. ATTACH LAB -REPORT.)
Report Attached? ❑ Yes (1) ❑ No (0)
VOC , method
method #
method #
method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total'VOCs. mglL. VOC Removal%
Martin Griess, Plant Manager
Perminee (or Authodwel A9en0 Name and Title - Please print or type.
GW-59 Rev. 112007

1YucrUDac ;Lta00raY0neS, Inc.
-
FAYETTEVILLE DIVISION
STATE CERT 1D.
2592 HOPE MILLS ROAD
FAYETTEVILLE,NC 29306
NC911
[phone] FAX [phone]
NC 937714
R. W. SANDERS, VICE PRESIDENT
USDA 93717
http://wvm,.microbac.com E-]Mail: [e-mail]
WATER -AIK •
WA:'I'HS • FOOD
• PHARMACEUTICALS • NUTRACELITICALS
CERTIFICATE OF ANALYSIS
—1
Allens, Inc.
Date Reported:
03/24/2010
Post Office Box 250
Date Received:
03/01/2010
Siloam Springs, AR 72761
Order Number.
1003-00011
Invoice No.:
72193
Customer #:
A004
Sample Date:
03/01/2010
Permit No. NC TURKEY PLANT
Sample Time:
0:00
Sampler. Miller
Subject: M/Well samples - 3/Yearly
SNIP Test
Aletbod
Result
Date
Time
Tech
gg RE
CHLORIDE
SM 4500 O C
18.3 mg/L
03/02/2010
16:24
DCR
COD
SM 5220 D
11 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
SM 2510 B
313 umhos/an
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
0.12 mg/L
03/02/2010
16:24
DCR
pH, FIELD
FIELD
5.20 s.u.
03/01/2010
0:00
RDM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
<25.0 mg/L
03/02/2010
16:30
ARS
SULFATE
SM IM 426 C
29.3 mg/L
03/04/2010
9:32
DCR
TEMPERATURE
FIELD
19.1 deg., C
03/01/2010
0:00
RDM
TOTAL ORGANIC CARBON
SM 5310B
1.7 mg/L
03/09/20}0
0:00
ECI
WATER LEVEL
FIELD
20.8 feet
03/01/2010
0:00
RDM
CHLORIDE
SM 4500 Cl C
161 mg/L
03/04/2010
9:32
DCR
COD
SM 5220 D
<10.0 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
'SM 2510 B
511 umhoslan
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
0.13 mg/L
03/02/2010
16:24
DCR
PH, FIELD
FIELD
5.38 sm.
03/01/2010
0:00
RDM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
249 mg/L
03/02/2010
16:30
ARS
SULFATE
SM 15th 426 C
4.1B mg/L
03/02/2010
16:24
DCR
TEMPERATURE
FIELD
15.0 deg., C
03/01/2010
0:00
RDM
TOTAL ORGANIC CARBON
SM 5310B
2.6 mg/L
03/09/2010
0:00
Ea
WATER LEVEL
FIELD
8.2 feet
03/01/2010
0:00
RDM
TECH INITIALS: CHI-Microbac, Chicitpland; PIT-Micmbac, Pittsburgh; CMP-Micmbac, Camp Hill; BAP/AJF-Micmbac Greensboro;
All other initials are Micmbac, Fa)rtteyille except as noted.
LA13CODES: N/D=None Detected N/F=None Found <=Less than >=Grcaterthan ESL=Estimated
The data and offier Wormaaon cmtamra an this, and obis accompanylog doanants, n ommtcdy the amplets) analyaei aM is rendered upon the MEMBER
mncMan that it is nom be reov&icut whoiy or in part foradmdsng or odwpmpgY3 W o"wdden appmat from the tabamtmy,
USDA-EPA-mOSH Tes" Food SiNlabon CmexOng Qianbl and MiooRologlal Malyses aM Researth •

Microbac Laboratories, Inc.
-' -- -
r{' FAYETTEVILLE DIVISION
2592 HOPE MILLS ROAD
STATE CERT 1D.
FAYETTEVILLE,NC 28306
NC#Ll
® ®
® [phone] FAX [phone]
NC #37714
R. W. SANDERS, VICE PRESIDENT
USDA #3787
http://wv.m�crobac.com E-Mail rsandm@,mirrobac.com
microbaeeom
CHEM IS[ ICY ' MIl.11l.Ut5IULUUY ' 1•01JIJ SAYEIY • UUNSUMEK PKUUUCIJ
WATER •AIR
WASTES -PUUD- PHARMACEUTICALS- NUIRACEUTICALS
CERTIFICATE OF ANALYSIS
Allen, Inc.
Date Reported:
03/24/2010
Post Office Box 250
Date Received:
03/01/2010
Siloam Springs, AR 72761
Order Number:
1003-00011
Invoice No.:
72193
Customer #:
A004
Sample Date:
03/01/2010
Permit No. NC TURKEY PLANT
Sample Time:
0:00
Sampler: Miller
Subject: M/Wellsamples -3/Yearly
SMP Test Method Result Date Time Tech
CHLORIDE
SM 450D a C
15.6 mg/L
03/02/2010
16:24
DCR
COD
SM 5220 D
<10.0 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
SM 2510 B
378 umhos/cm
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
<0.1 mg/L
03/02/2010
16:24
DCR
pH, FIELD
FIELD
6.0 s.u.
03/01/2010
0:00
ROM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
246 mg/L
03/02/2010
16:30
ARS
SULFATE
SM 15th 426 C
57.5 mg/L
03/04/2010
9:32
DCR
TEMPERATURE
FIELD
12.0 deg., C
03/01/2010
0:00
ROM
TOTAL ORGANIC CARBON
SM 5310E
2.3 mg/L
03/09/2010
0:00
ECI
WATER LEVEL
FIELD
3.7 feet
93/01/2010
0:00
ROM
CHLORIDE
SM 4500 Cl C
16.2 mg/L
03/02/2010
16:24
DCR
COD
SM 5220 D
<10.0 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
SM 2510 B
149 umhos/an
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
7.43 mg/L
03/04/2010
9:32
DCR
pH, FIELD
FIELD
4.46 s.u.
03/01/2010
0:00
ROM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
65.0 mg/L
03/02/2010
16:30
ARS
SULFATE
SM 15th 426 C
2.34 mg/L
03/02/2010
16:24
DCR
TEMPERATURE
FIELD
15.7 deg., C
03/01/2010
0:00
RDM
TOTAL ORGANIC CARBON
SM 53108
0.6 mg/L
03/09/2010
0:00
ECI
WATER LEVEL
FIELD
5.9 feet
03/01/2010
0:00
ROM
TECH INITIALS: CHI-Microbac, Chicagoland;
PIT-Microbac, Pittsburgh;
CMP-Microbac, Camp Bill;
BAP/A1F-Ivlicrobx. Grcensboro;
All other initials are Microbac, Fayetteville except as noted.
LAB CODES: N/D=None Detected N/F=None
Found <=Lessthan
>=Grealerthan Est.=Estimated
The dab and other hdmmatim contained on Mk and other a®rapanying doer n% represent only to sample(s) anahad and is serdaed upon the
=dtlon loth is not to be n podued wfmoy Orin Fart for adverdshg or otherpurynses velaour mRtm aaphoval Gam the hlnramry.
MEMBER
USDAFPA-11105HTesdog
Food Sanlmtianrnnsulang
Ohmibl and ldloabblogbl Amlyseswd
Research

Microbac Laboratories, Inc.
FAYETTEVILLE DIVISION
STATE CERT 1D.
2592 HOPE MILLS ROAD
FAYETTEVILLE, NC 28306
NC #11
[phone] FAX [phone]
NC #37714
R. W. SANDERS, VICE PRESIDENT
USDA 93787
http://w%vw.microbar-com E-Afail: [e-mail]
WATER • AIR - WAS I*ES • FOUL) . PHARMACEUTICALS • NUIRACEUTICALS
CERTIFICATE OF ANALYSIS
Allens, Inc.
Date Reported:
03/24/2010,
Post Office Box 250
Date Received:
03/01/2010
Siloam Springs, AR 72761
Order Number:
1003-00011
Invoice No.:
72193
Customer #:
A004
Sample Date:
03/01/2010
Permit No. NC TURKEY PLANT
Sample Time:
0:00
Sampler. Miller
Subject M/Wellsamples -3/Yearly
SMP Test Method Result Date Time Tech
RESPECTFULLY SUBMITTED: R. i7 - Awn&4at
MICROBAC LABORATORIES, INC.
71=43roufor your business. lPe bruite ymrrfeedback on our level ofsernice 1o)'ou. Please contact the Laboratory Director, Ron Sanders at 910.861-1920. Robert A&gon,
COO, at nnorgan a m1arvbaacmn or Trevor Bose, CEO, at fboycv@nfierobaacom Wilt cull, crommener or suggestions.
TECH INITIALS: CHI-Micmbac, Chieagoland; PIT-Microbae, Pittsburgh; CMP-MiaobaS Camp Hill, HAP/AW-Microbac, Grecnsbom;
All other initials arc Micmbac, Fayeaevillc ccceptas noted.
LAB CODES: N1D=None Detected NIF=None Found <=Lesslhan >=Owalcrthnn Fsl.=Estimated
The data orb oUw tNarmatbn mntab� on Ws, and other aam penybg dommmtsf w4ae ra my the samplets) analyml aml Is rendered upon Ne MEMBER
conom that R is not m be reproduced wholly or In part ra admt[s'vy a ad oparpores wlahout Written appmval hom the Hbaut qy
ISUMPA-mOSH Teting Food sanitation Camuaing Mmkzl and fRloohblogld Arelyses and Research

t, Microbac Laboratories, Inc.
`ar. t "t'
FAYETTEVILLE DIVISION
STATE CERT ID-
2592 HOPE MILLS ROAD
FAYETTEVILLE,NC 28306
INC911
[phone] FAX [phone]
NC #37714
R. W. SANDERS, VICE PRESIDENT
USDA 43787
http://wvkm,.microbac.com E-Mail: rsanders@microbac-com
WATER • AIR • WASTES • FUUU • PHARMACEUTICALS • NUTRACEU"11CALS
CERTIFICATE OF ANALYSIS '
Aliens, Inc.
Date Reported:
0324/2010
Post Office Box 250
Date Received:
03/01/2010
Siloam Springs, AR 72761
Order Number.
1003-00012
Invoice No.:
72194
Customer #:
A004
Sample Date:
03/012010
Permit No. NC TURkEY PLANT
Sample Time:
0:00
Sampler: Miller
Subject: M/Wellsamples -3/Yearly
SMP Test
Method
Result
Date
Time
Tech
E.
CHLORIDE
SM 4500 O C
8.61 mg/L
03/02/2010
16:24
DCR
COD
SM 5220 D
45.9 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
SM 2510 B
90.0 umhos/an
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
0.35 mg/L
03/02/2010
16:24
DCR
pH, FIELD
FIELD
530 S.u.
03/O1/2010
0:00
RDM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
61.0 mg/L
03/02/2010
16:30
ARS
SULFATE
SM IM 426 C
12.7 mg/L
U3102/2010
16:24
DCR
TEMPERATURE
FIELD
11.6 deg., C
03/01/2010
0:00
ROM
TOTAL ORGANIC CARBON
SM 5310B
6.7 mg/L
03/04/2010
0:00
ECI
WATER LEVEL
FIELD
5.4 feet
03/01/2010
0:00
ROM
CHLORIDE
SM 4500 CJ C
B.BB mg/L
03/02/2010
16:24
DCR
COD
SM 5220 D
106 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
SM 2510 B
174 umhos/cm
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
0.69 mg/L
03/02/2010
16:24
DCR
pH, FIELD
FIELD
5.17 s.u.
03/01/2010
0:00
ROM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
94.0 mg/L
03/02/2010
16:30
ARS
SULFATE
SM 15th 426 C
45.3 mg/L
03/05/2010
11:25
OCR
TEMPERATURE
FIELD
11.6 deg., C
03/01/2010
0:00
ROM
TOTAL ORGANIC CARBON
SM 5310B
5.3 mg/L
03/04/2010
0:00
ECI
WATER LEVEL
FIELD
5.9 feet
03/O112010
0:00
ROM
TECH INITIALS: CHI-Microbac, Cbicagoland: PIT-Microbac, Pittsbureh; CMP-Microbac, Camp Hill; BAP/A1F-Microbac, Greenshom;
All other initials arc Microbac, Fayetteville except as noted.
LAB CODES: N/D=None Detected N/F=None Found <=Less than >=Gmalcrthan ESL=Estimated
The data and other fnf Uon =Wnel an tt%s, and outer loam , represent anly the saopiats) aMped ame is rendered upon the MEMBER
m
eannan that It is not to be repvdumd nho@/ or in part for advedldn9 or other wnosas w awt veQten approval from the bborAn.
USDA-EPMMC!al `r s g Food San'MW- rnnsul[Inp Ch kal and M W014CM Analyses and Researoh
..................................... ...... _.. ..... ..... ... ..... ....... I .. _,......................... ............................... I.... I .... I .... .. .

Microbac Laboratories, Inc.
FAYETTEVILLE DIVISION
STATE CERT ID.
2592 HOPE MILLS ROAD
FAYETTEVILLE,NC 28306
NC411
[phone] FAX [phone]
NC 937714
R. W. SANDERS, VICE PRESIDENT
USDA 93787
http://www.niicrobac.com E-Mail: tsanders@rnierobaeeom
WATER • AIR
- WASTES • FOUL) • PHARMACEUTICALS - NUI'RACEUTICALS
CERTIFICATE OF ANALYSIS
Aliens, Inc.
Date Reported:
03(_)4/2010
Post Office Box 250
Date Received:
03/01/2010
Siloam Springs, AR 72761
Order Number.
1003-00012
Invoice No.:
72194
Customer/r:
A004
Sample Date:
03/01/2010
Permit No. NC TURKEY PLANT
Sample Time:
0:00
Sampler: Miller
Subject: M/Well samples - 3/Yearly
SMP Test Method Result Date Time Tech
CHLORIDE
SM 4S00 Cl C
5.20 mg/L
03/02/2010
16:24
DCR
COD
SM 5220 D
13.6 mg/L
03/04/2010
11:00
ENC
CONDUCT1VTlY
SM 2510 B
82.8 umhw/an
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
1.84 mg/L
03/02/2010
16:24
DCR
pH, FIELD
FIELD
4.53 s.u.
03/01/2010
0:00
ROM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
34.0 mg/L
03/02/2010
1630
ARS
SULFATE
SM 15th 426 C
11.4 mg/L
03/02/2010
16:24
DCR
TEMPERATURE
FIELD
10.1 deg., C
03/01/2010
0:00
ROM
TOTAL ORGANIC CARBON
SM 5310B
D.8 mg/L
03/04/2010
0:00
ECI
WATER LEVEL
FIELD
7.3 feet
03/01/2010
0:00
RDM
- , .. i.: r I f.- -c
oi4 R 4MRS
CHLORIDE
SM 4500 O C
5.94 mg/L
03/02/2010
16:29
DCR
COD
SM 5220 D
<10.0 mg/L
03/04/2010
11:00
ENC
CONDUCTIVIN
SM 2510 8
145 umhos/cm
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
3.32 mg/L
03/02/2010
16:24
DCR
pH, FIELD
FIELD
4.46 sm.
03/01/2010
0:00
RDM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
66.0 mg/L
03/02/2010
16:30
ARS
SULFATE
SM 15th 426 C
29.2 mg/L
03/05/2010
11:25
DCR
TEMPERATURE
FIELD
10.1 deg., C
03/01/2010
0:00
ROM
TOTAL ORGANIC CARBON
SM 5310B
0.7 mg/L
03/04/2010
0:00
ECI
WATER LEVEL
FIELD
7.4 feet
03/01/2010
0:00
ROM
TECH INITIALS: CHI-Microbac, Chicogoland; PIT-Microbac, Pittsburgh:
CMP-Microbac, Camp Hill;
BAP/AIF-Microbac, Greensboro;
All outer initials are Microbac, Fayetteville
except as noted.
LAB CODES: NID -None Detected
N/F-None Found <=Lessthan
>-Gteaterthan EsL=Estimated
M�EM6�ER�
Information End other Infoation contained on this, and o0w accompanying d000ner , reo,esent only the sampiefs) awlyml aM Is rendered upon the
oandiron that nis not to be reproduced wh* or in Part for advonsng orather purposes without wdden apprum from Me laboratory.
�IAr�IYI�
USDA -EPA -NOSH Testing road Sanimtbn CunsuliMg
rhemial and HiwGalogicol Matyses
and Heseardt
w®

Microbac Laboratories, Inc.
FAYETTEVILLE DIVISION
STATE CERT ID,
2592 HOPE MILLS ROAD
FAYETTEVILLE,NC 28306
NC#I1
[phone] FAX (910) 8"8774
NC #37714
R. W.SANDERS, VICE PRESIDENT
USDA #3787
http://www.nticrobac.com E-Mail- rsandersQlnicrobae.com
WATER • AIR. WASTES • FOUL) • PHARMACEUTICALS • INU7RAC;EUIIC:ALS
CERTIFICATE OF ANALYSIS
Aliens, Inc. Date Reported: 0324/2010
Post Office Box 250 Date Received: 03/01/2010
Siloam Springs, AR 72761 Order Number. IG03-00012
invoice No.: 72194
Customer #: A004
Permit No. NC TURKEY PLANT Sample Date: 0 : 01/2010
Sampler: Miller . Sample Time: 000
Subject: M/Wellsamples -3/Yearly
SMP Test Method Result Date Time Tech
Sample did not meet recommended spike recovery for Chloride, Nitrate or Sulfate analysts.
RESPECTFULLY SUBMITTED: UG_ rl , .+CJt
MICROBAC LABORATORIES, INC.
]bank yotrforyour business. lPe imdte ymtrfeedback on our level ofservice to you. Please contact the Laboratory Director, Ron Sanders at 910-864-19207, Robert dlorgan,
COO, at rmorganoa micraboacom or Trevor Bore. CEO, at Iboyee&Wcrobac.com vYth mry comments orsuggestions.
TECH BJRIAI S: CHI-Micmbac, Chicagoland; PIT-MicmbaS Pittsburgh; CMP-Mivobac, Camp Hill; BAPIAIF-Micmboc, Gmasboro;
All other initials are Micmbac, Fayetteville except as noted.
LAB CODES: NID=Non Detected NIF=None Found <=Less than >=Greaterthan Est. —Estimated
The dam and curer tnfarmatiam mnbined an this, and miner aunmpa%mv doovnenrs, mpresem anN the samplels, anaNa'a and is rendered upon the MEMBER
mu5t1on that It It not to be reproduced MoM1/ min part for 8dreNsry m aMe purposes wtftm wman apprand tam the Wa,,dmy.
LIMA-EPA-14051 Testing rood 5ammtimr Cansutarq Chmdcl and Mcnablologkal Anabses and Research

le
1V1IefuDi3l: Lin LlU1*211 LUI'1CS1111C.
v
FAYETIEVILLE DIVISION
STATE CERT ID.
)g
2592 HOPE MILLS ROAD
FAYE7TEVILLE, NC 28306
NC #11
®
A
[phone] FAX [phone]
NC 937714
R. W. SANDERS, VICE PRESIDENT
USDA 93787
http://ww%.microbac.cotn L-\fail: [e-mail]
UHtMIN I KY
' MIUKUI3IULUU Y ' YUUU SAYY:1 Y • CUNSUMtK YKUUUCI S
WATER • AIK •
WASTES • F'UUU • PHARMACEUTICALS • NUI'RACEU 1CALS
CERTIFICATE OF ANALYSIS
Allens, Inc.
Date Reported:
03/242010
Post Office Box 250
Date Received:
03101/2010
Siloam Springs, AR 72761
Order Number.
1003-00013
Invoice No.:
72195
Customer #:
A004
Sample Date:
031012010
Permit No. NC TURKEY PLANT
Sample Time:
0:00
Sampler. Miller
Subject: M/Well samples-3/Yearly
SNIP Test
Method Result
Date
Time Tech
CHLORIDE
SM 450D CI C 11.0 mg/L
03/02/2010
16:24 DCR
COD
SM 5220 D 75.6 mg/L
03/04/2010
11:00 ENC
CONDUC rVrrY
SM 2510 B 213 umhos/cm
03/08/2010
11:35 DCR
NITROGEN, NITRATE
SM 4500 NO3 E 10.5 mg/L
03/04/2010
9:32 DCR
pH, FIELD
FIELD 4.48 sm.
03/01/2010
15:06 ROM
SOLIDS, TOTAL DISSOLVED
SM 2540 C Ili mg/L
03/02/2010
16:30 ARS
SULFATE
SM 15th 425 C 17.2 mg/L
03/02/2010
16:24 DCR
TEMPERATURE
FIELD 10.8 deg., C
03/01/2010
15:06 RDM
TOTAL ORGANIC CARBON
SM 53103 2.4 mg/L
03/09/2010
0:00 ECI
WATER LEVEL
FIELD 5.9 feet
03/01/2010
15:06 RDM
002' 6.
_..;:..L7_.... ........ __
CHLORIDE
SM 4500 0 C 2.91 mg/L
03/02/2010
16:24 DCR
COD
SM 5220 D 51.9 mg/L
03/04/2010
11:00 ENC
CONDUCTIVITY
SM 2510 B 240 umhos/an
03/08/2010
112S DCR
NITROGEN, NITRATE
SM 4500 NO3 E 5.51 mg/L
03/04/2010
9:32 DCR
pH, FIELD
FIELD 4.96 sm.
03/01/2010
13:14 RDM
SOLIDS, TOTAL DISSOLVED
SM 2540 C 118 mg/L
03/02/2010
16:30 ARS
SULFATE
SM 15th 426 C 32.8 mg/L
03/04/2010
9:32 DCR
TEMPERATURE
FIELD 11.9 deg., C
03/01/2010
13:14 RDM
TOTAL ORGANIC CARBON
SM 5310B 11.4 mg/L
03/09/2010
0:00 ECI
WATER LEVEL
FIELD 7A feet
03/01/2010
13:14 RDM
TECH INITIALS: CHI-Microbac, Chicaoolond; PIT-Microbac, Pittsburgh; CMP-Microbac, Camp Hill; BAP/AIF-Microbuc, Greensboro;
All other initials are Microbac, Fayetteville escepL as noted.
LABCODES: NID-None Detected NIF—None Found <=Lmsthan >=Greaterthan rsL=Estimated
The dart aM oMer wormadon tnntamed on MH, and other accompanying documents, rerxesernt only the simples) astral and Is rendered upon tt a MEMBER
j
mm rdaan Mat it is not to be repmdul whodotry lbaor M part for adverustrm or oder pumoses withmn written appt l from the laboromry. Lt61J.i=.
LWA-EPA-140SHTestlrg FoSanwn Consu�rg Oienfral and Mvabblagitat ArOyses and Remamh

c
WATER
Aliens, Inc.
Post Office Box 250
Siloam Springs, AR 72761
Permit No. NC TURKEY PLANT
Sampler: Miller
IMLICCUUitC Lauur211.1.1 , JLHC.
-
FAYETTEVILLE DIVISION
STATE CERT ID.
2592 HOPE MILLS ROAD
FAYETTEVILLE,NC 28306
NC411
[phone] FAX [phone]
NC #37714
IUSDA#1711
R. W. SANDERS, VICE PRESIDENT
http://wwvt,.microbac,com E-Mail: [e-mail]
W ASI'ES - FOUL)
CERTIFICATE OF ANALYSIS
Date Reported:
03/24/2010
Date Received:
03/0112010
Order Number.
1003-00013
Invoice No.:
72195
Cmtomer4:
A004
Sample Date:
03101/2010
Sample Time:
0:00
Subject: M/Wellsamples -3/Yearly
SMP Test Method Result Date Time Tech
CHLORIDE
SM 4500 Cl C
27.6 mg/L
03/04/2010
9:32
DCR
COD
SM S220 D
113 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
SM 2510 B
154 umhos/an
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
1.78 mg/L
03/02/2010
16:24
DCR
PH, FIELD
FIELD
4.58 s.u.
03/01/2010
13:59
RDM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
73.9 mg/L
03/02/2010
16:30
ARS
SULFATE
SM 15th 426 C
9.58 mg/L
03/02/2010
16:24
DCR
TEMPERATURE
FIELD
17-0 deg., C
03/01/2010
13:59
RDM
TOTAL ORGANIC CARBON
SM 53108
3.5 mg/L
03/09/2010
0:00
ECI
WATER LEVEL
FIELD
5.5 feet
03/01/2010
13:59
RDM
CHLORIDE SM 45110 Cl C
18.9 mg/L
03/02/2010
16:24
DCR
COD SM 5220 D
<10.0 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY SM 2510 B
379 umhos/cm
03/08/2010
11:35
DCR
NITROGEN, NITRATE SM 4500 NO3 E
30.7 mg/L
03/04/2010
9:32
DCR
pH, FIELD FIELD
4.49 s.u.
03/01/2010
12:43
RDM
SOLIDS, TOTAL DISSOLVED SM 2540 C
222 mg/L
03/02/2010
46:30
ARS
SULFATE SM 15th 426 C
12.7 mg/L
03/02/2010
16:24
DCR
TEMPERATURE FIELD
12.0 deg., C
03/01/2010
12:43
RDM
TOTAL ORGANIC CARBON SM 5310B
0.7 mg/L
03/09/2010
0:00
ECI
WATER LEVEL FIELD
5.3 feet
03/01/2010
12:43
RDM
'TECH INITIALS: CHI-Microbac, Chimeoland; PIT-Microbac, Pittsburgh;
CMP-Microbac, Camp Hill; BAP/A1F-Microbac, Greensboro;
All other initials are Microbac, Fayetteville except as noted.
LAB CODES: N/D=None Detected N/F=None Found <=Less than
—Grealerthan Est. -Estimated
MEMBER
The data and atha Infamtation ovnalned on this, and other armmpanring daaunents, represent only the samples) analyzed and is rendemd upon ate
mnddfon that It is not to be reproduced wholly or hi pan for advertising or cow poposes vdthout meten approval from the raborotary.
USDA-EPA4dOSH Testing Food Sanitallon Consulting
Oremaaridl aPllaoblobgl al AnalyseM a
ReseanT
G�i.1.L

Microbac Laboratories, Inc.
rage a °t'
FAYETTEVILLE DIVISION
STATE CERT ID.
2592 HOPE MILLS ROAD
FAYETTEVILLE, NC 28306
NC #I I
[phone] FAX [phone]
NC 07714
R. W. SANDERS, VICE PRESIDENT
USDA#3787
http://www.microbac-com E-1Viail:[e-mail]
WATER • AIR • WASTES - FOUL) • PHARMACEUTICALS • NU RACEUTICALS
CERTIFICATE OF ANALYSIS
Aliens, Inc.
Post Office Box 250
Siloam Springs, AR 72761
Permit No. NC TURKEY PLANT
Sampler. Miller
Subject: M/Well samples-3/Yearly
SMP Test Method
Date Reported: 03/24/2010
Date Received:
03/01/2010
Order Number:
1003-00013
Invoice No.:
72195
Customer#:
A004
Sample Date:
03/O1/2010
Sample Time:
0:00
Result Date Time Tech
CHLORIDE
SM 4500 Cl C
4.16 mg/L
03/02/2010
16:24
DCR
COD
SM 5220 D
56.8 mg/L
03/04/2010
11:00
ENC
CONDUCTIVITY
SM 2510 B
251 umhos/cm
03/08/2010
11:35
DCR
NITROGEN, NITRATE
SM 4500 NO3 E
123 mg/L
03/04/2010
9:32
DCR
pH, FIELD
FIELD
4.44 s.u.
03/01/2010
16:16
ROM
SOLIDS, TOTAL DISSOLVED
SM 2540 C
146 mg/L
03/02/2010
16:30
ARS
SULFATE
SM 15th 426 C
47.3 mg/L
03/04/2010
9:32
DCR
TEMPERATURE
FIELD
11.8 deg., C
03/01/2010
16:16
RDM
TOTAL ORGANIC CARBON
SM 5310B
2.7 mg/L
03/09/2010
0:00
ECI
WATER LEVEL
FIELD
7.6 feet
03/01/2010
16:16
RDM
RESPECTFULLY SUBMITTED: R r► - 1C umd &
MICROBAC LABORATORIES, INC.
77tank inn for your business. We invite yourfeedbuck on our level afservice to you. Please contact the Laboratory Director. Ron Sanders at 910-864-1920. Robert tbforgon,
COO, at rnmrgannnderobaeconi or Trevor Hoge, CEO, at tbgvice@,nfcrabaecom will, any contenents or suggestions.
TECH INITIALS: CHI-Microbac, Chicaeoland; PIT-Micmbac, Pittsburgh; CMP-Microbac, Cmp Hill; BAP/AJF-Micmbac.Greensboro;
All other initials are Microbac, Fa)eneville except as noted.
TAB CODES: N/D = None Detected NIF—None Found <= Less than > = Grater than ESL = Estimated
The dab aM other Infomutbn oantahed an th6, and other acmmpanybig doam eots, represent any the sample(s) an tnusl and is rendered new the MEMBER
�
aatldlon ftat it is not to be reproduced whW or In part for advertistrg or other purposes svldmu[ wdnen approval from the lab wq. LiV.L
16DA-FDA-m0SHTeshg FoDd SanitatbnransWCn9 0a=k mdFDw1eob_ral MalysesaMneseanh
..................................................................................................................................... I......................... ....... ..

1
Fayetteville Division
2592 Hope Mills Rd
8-B Wendy Court
Fayetteville, NC 28306
Greensboro, NC 27409
910.864.1920 Phone
336.856.9710 Phone
910.864.8774 Fax
336.856.9711 Fax
Certificate of Analysis
Inc Mr. R Date Reported: ApnI29, 2010
Mr. Reid Wells Project: M/W samples- 3/Yearly, Retest
5900 Turkey Highway Date Received: Apri120, 2010
Turkey NC, 28393 Sampled By: Robin Miller Date Sampled: April 20, 2010
DRAFT: NW - R-5a
1004582-01
Analyte Result
Unit
Analysis Datelfime
Analyst
Method
Qualifier
Analyzed by: Maobac- Fay9LvNe gH9on
Depth 6.30
fen
420/1016:25
RDM
Field Measmem®t
Nitrate as N 8.67
mg/L
421110 16:13
ARS
EPA 300.0
DRAFT: NW -R-6
1004582-02
Analyte Result
Unit
Analysis Daterfime
Analyst
Method
Qualifier
AnaWed by: M
Total Organic Carbon 5.3
mg/L
4/28/10 0:00
Ea
SM 5310C
Mayrel by: Kiaotuc- Faretlevlle 0irisbn
Depth 7.30
fen
42011016:35
RDM
Field Mettoameat
DRAFT: MM - R-9
1004582-03
Analya Result
Unit
Analysis Dnerrime
Analyst
Method
Qualifier
Ar�atyml by: Kc obac- Fayette+itle Dnaslon
Depth 8.50
fact
42011016:45
RDM
Field Measuremeot
Nita. as 12.3
mgtL
421110 16.13
ARS
EPA 300.0
Notes and Definitions
State Cessations: Respectfidly Submitted
NCDNR 911,#693
NCDOH 937714,037796 a �- tl'��. s9ium.ciry •±.
USDA #3787 R. W. Sandy% VP/Managing Director
Thank you for your business. Weimircpurkedbmkon mnlenl Jsemre ro yov. Pycax roan the ITWanaging Dimcro4 Ron Sanden at 91""-1920, James Nam, Preadenr, ar
jnokm(e�mieabae.eom or TrewrRoyar, CEO, ar rbayce(rym'embac.rom virh anyeanmenv orsuggerNmar.
Page 1 of I

+• `� S GoW-59A COMPLIANCE REPORT FORM Permit # Wo00 ya(�b�
(Submit one each monitoring period with GIV-59 forms.)
�I
I
Enter date monitoring results were due. - 10 Will this monitoring report (GW-59 and GW-59A)
YES
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
YES
IF the answer to question t or 2 is `YES; list in the space provided below the well identification numbers) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing
YES
identification plate, area overgrown, eta)? Ifthe answer is "Yes", contact the Regiomal OJfhcefor guidance.
4
Are any monitored constituents equal to or above the established standards?
S
NO
If the answer to question 4 is 'NO", skip to section 8.
If the answer to question 4 is "YES" list the affected wells individually with consfituent(s) and concentration(s)
exceeding standards in the space provided below:
R-T A)h+r-+e = 36. `7 fne/4-
R-`P4. w4m4e- = !a?. a thf3/L
5
For the constituents identified in question 4 above, have standards been exceeded previously for the
YES
same consfituent(s) in the same well(s) in the last two years?
If Me answer to question 5 is 'NO; skip to section B.
If the answer to question 5 is "YES", list in the space provided below, each well with consfituent(s) exceeding
standards, concentrations) reported, and sample collection date for each occurrence (for the last two years).
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
If the answer is "YES" a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELYFOR GUIDANCE If the answer is "NO" monitoring wells may be improperly
located; contact the Regional Office.
7
Is the pernittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
If the answer to question 7 is 'YES" describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 days; an evaluation may be
required to determine the impact the waste disposal system is having at the review and compliance
boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation
fines. and(orpenaltfes.
8
The person completing this portion (GW-59A) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to the address provided at the top of the current G W-59 form.
hereby acknowledge that the above information was evaluated and the information submitted in this j
report (Compliance Repoli G -59A) is true and complete to the best of my kin/owledge. J
-'
,2?-10
signature of Perndtee or Authorized Agent) Date
GW-59A 12/812003