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WQ0004268_GW Monitoring_20171214
11� GW-59A COMPLIANCE REPORT FORM Permit # WQ0004268 (Submit one each mmriforing period with GIV--59 forms.) I 1 Enter date monitoring results were due. ( eewmber3e•2017) Will this monitoring report (GW-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question I or 2 is "YES" list in the space provided below the well uu, and explain the problems encountered in obtaining the required information. Utl: 2 0 2017 Information Processing UnH 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES identification plate, area overgrown,. etc.)? Ijthe answer is "Yes", contact the Regional Ofcefor guidance. 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is 'NO", skip to section B. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below., 1) pH <6.5 at all monitoring wells; 2) Ammonia-N at MW-R6 = 6.1 mg/L; and Nitrate-N at MW-R8 = 17 mg/L. 5 For the constituents identified in question 4 above, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question 5 is 'NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). Please refer to the data in the attached spreadsheet i Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES", a groundwater quality problem maybe occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer fs "NO", monitoring wells maybe improperly located; contact the Regional Office. 7 Is the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES ;'describe thoseactions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days: an evaluation may be required to determine the impact the waste disposal system is t ev'ew and compliance boundaries surrounding this facility. Failure to do so maysubie a Notice of Violation fines, and/or penalties. ®E JAN 0 B 2018 8 The person completing this. portion (GW-59A) of the moei p� �(�(gA�bftd submit This form with GW-59 forms for required wells to the address r e a e top o{the current GW-59 form. that the _abvomation—was _valuated _nd the informaton submit_e�d- nt_h_shereby acknowledge _.. Lreport (Compliance ReportGW-59A) is true -and complete to the best of my knowledge_ _ 11 RJZ is/14017 Signature of Pernrl (or Authorized Agent) Date GW-59A 12/8/2003 Sample DTW Field Temp. Field pH EC Fecal Coliform I COD NO3N NH3-N Total-P TDS 504 TOC Date ft. °C - Std. Units I umhos/cm MPN/100 mi I -mg1l. .Mar-15 - 21.40 17.0 - 6.5 581 NT <10 0.37 NT NT 222 10.0 8.50 Jul-15 23.10 2010 4.8 '- 91 NT <10 0.63 NT NT 272 10.0 4.98 Nov-15 20.80 --19.0 'S.0- 241 NT <10 0.75 NT NT 280 12.0 9.59 Mar-16 20.40 19.0 65 283 NT i <10 0.23 NT NT 180 7.7 7.94 Jul-16 7.50 20.1 4.6 , NT <3 1 16.0 0.18 0.38 <0.025 170 9.7 3.40 Oct-16 18.00 18.7 _ 3.8 NT 1 118.0 0.22 0.39 <0.025 150 8.3 4.20 Mar-17 24.00 16.3 '4.1 NT <1 113.0 020 0.32 <0.025 180 8.9 3.60 Jul-17 6.00 19.6 4.6 NT <1 113.0 0.21 0.36 <0.025 160 9.2 3.50 Nov-17 27.00 19.7 4.3 NT <1 i <10 .27 0.30 <0.025 150 9.7 3.80 Mean _ 18.69 18.8 4.9 299 <1 j 15 0.34 0.35 <0.025 196 9.5 5.50 Min 6.00 16.3 3.8 91 1 <10 0.18 0.30 <0.025 150 7.7 3.40 Max _ 27.00 20.1 •6.5 581 1 $ 18 D-75 0.39 <0.025 280 12.0 9.59 GWStds. 6.5-8.5 1 10 1.5 500 250 Sample DTW, Field Temp. Field pH EC Fecal Coliform COD NO3 N NH3 N Total-P TDS so, TOC Date ft. °C Std. Units umhos/cm MPN/100 mi !-mg/L----- .Mar-15 3.00 14.0 6.8 723 NT <10 5.20 NT NT 128 22.0 3.33 Jul-15 4.40 22.0 6.1 810 NT I <10 7.12 NT NT 76 4.7 0.98 Nov-15 3.70 19.0 -6.0 870 NT 1 <SO 8.22 NT NT 62 5.5 2.38 Mar-16 4.40 19.0 6.3 826 NT I <10 7.40 NT NT 94 7.9 1.79 Jul-16 _ 4.00 18.9 6.1 NT <1 I SO 9.50 <0.045 <0.025 78 4.1 0.50 Sep-16 NT NT NT NT NT NT NT NT NT NT NT NT Oct-16 4.25 19.6 6.0 NT <10 I <10 10.00 <0.045 <0.025 90 4.0 1.60 Mar-17 4.00 16.1 5.6 NT <3 1150 9.90 <0.045 <0.025 120 3.9 78.00 Jul-17 5.00 19.1 _ 6.4 NT <1 1120 8.30 <0.045 0.031 80 3.6 35.00 Nov-17 _-6.00 19.0 '6.2_-- NT <1 <10 9.20 <0.045 <0.025 100 3.6 0.92 Mean 4.31 18.5 6.2 807 <1 38 8.32 <0.045 0.027 91 6.6 13.83 Min 3.00 14.0 5.6 723 <1 ! <10 150 5.20 <0.045 <0.025 62 3.6 0:50 Max 6.00 22.0 6.8 870 <10 10.00 <0.045 0.031 128 22.0 78.00 GWStds. 6.5-8.5 10 1.5 Sao 250 I Sample DTW Field Temp. "Field pH EC Fecal COD NO3-N NH3-N Total-P TDS SOa TOC Coliform Date ft. °C Std. Units umhos/cm MPN/100 mi ---mg/L----- Mar-15 5.30 16.0 6.9 264 NT 25.9 1 <10 0.54 NT NT 122V7. 11.30 Jul-15 6.00 26.0, 4.7 397 NT 1.47 NT NT 202 1.59 Nov-15 5.60 18.0 , 4.8 177 NT <to 0.38 NT NT 138 3.94 Mar-16. 5.70 17.0 6.9 123 NT <10 I <10 22.0 0.80 NT NT 76 3.31 Jul-16 6.50 21.2 5.5 NT <1 0.60 <0.045 0.04 100 0.92Oct-16 5.25 20.1 5.3 NT <10 0450 <0.045 <0.025 72 1.50 Mar-17 5.00 14.5 5.1 NT <3 <10 34.0 <10 0.088 <0.045 0.029 74 1.50 Jul-17 6.50 20.7 5.4 NT <3 0.39 <0.045 0.74 <50 1.10 .00 19.1 5.1 NT <1 <0.20 <0.045 0.026 50 0.55 Mean 5.98 - 19.2 5.5 240 <1 116.0 <10 0.60 <0.045 0.17 104 10.0 2.86 Min 5:00 14.5 4.7 123 <1 0.09 <0.045 <0.03 <50 5.7 0.55 Max 8.00 26.0 6.9. 397 <10 1 34.0 1.47 <0.045 0.74 202 21.0 11.30 GWStds. 6.5-8.5 1 10 1.5 500 250 NOTES: Red shaded values do not match groundwater standards: ft=feet °C =Degrees Celsius Std. Units=Standard Units umhos/cm = micromhos per centimeter mg/L= parts per million NT = Not Tested DTW = depth to groundwater; Field Temp.= field temperature; EC=electr ' Samples collected and analyzed by Microbac, Fayetteville, NC and EN CO SG Foods, Inc.,, Turkey, NC carbon 1 of Sample �DTW' Field Temp. Field pH EC CFecal oliform +COD NO3N NH3-N Total-P TDS 50a TOC Date ft. °C _ Std. Units I umhos/cm I MPN/SOOmI I-mg/L----- Mar-15 6.60 17.0 6.8 634 NT { 23.0 0.41 NT NT 316 26.0 8.63 Jul-15 6.90 23.0 4.9 495 NT 117.3 0.62 NT NT 116 23.0 3.25 Nov-15 6.30 20.0 4.8 502 NT 112.1 0.38 NT NT 320 4.5 9.41 Mar-16 6.20 18.0 6.7 588 NT 135.9 0.20 NT NT 286 11.0 8.53 Jul-16 6.00 24.1 4.4 NT <1 159.0 0.06 0.07 1.80 140 12.0 9.80 Oct-16 6.50 19.9 4.6 NT 2 1 0.13 0.81 190 9.1 9.70 Mar-17 7.25 14.8 ` ` 3.9 NT <3 <0.025 0.05 0.91 230 13.0 3.00 Jul-17 6.00 21.6 4.5 NT <1 0.084 <0.045 1.20 130 11.0 2.50 50 - 19.4 4.2- NT <3 <0.20 <0.045 1.40 130 16.0 1.50 AS 19:8 5.0 555 1 M43.00.14 0.24 0.07 1.22 206 14.0 6.26 .00 14.8 3.9 � 495 <1 <0.025 <0.045 0.81 116 4.5 1.50 .50 24.1 6.8 634 2 0.62 0.13 1.80 320 26.0 9.80 6.5-8.5- 10 1.5 Soo 250 I Sample DTW Field Temp. Field pH EC ' ifo ColFecalrm 1 COD I NO3N NH3-N Total-P TDS SO4 TOC .Date ft:11 C Std. Units umhos/cm MPN/100 m1 I -mg/L--- Mar-15 4.90 15.0 6.6 202 NT 52.7 0.35 NT NT 264 25.0 23.90 Jul-15 _ 5.80 27.0 4.3 - 164 _ NT j 80.3 0.61 NT NT 210 11.0 36.10 Nov-15 5.30 20.0 .. -4.6 200 NT 1 49.8 0.59 NT NT 354 11.0 75.00 Mar-16 8.70 17.0 6.8 155 NT - j 19.4 0.25 NT NT 326 20.0 11.60 Jul-16 7.00 24.7 4.2 - NT 310 _ i 54.0 0.06 4.0 0.08 310 19.0 16.00 Sep-16 650 25.9 4.3 NT <10 I NT NT 4.5 NT NT NT 13.00 Oct-16 5.25- 22.1 3.9 NT <10 j 100.0 0.10 4.5. 0.15 250 20.0 19.00 Mar-17 6.50 16.8 3.8 NT <3 15.0 0.043 3.2 <0.025 310 30.0 5.20 Jul-17 750 '23.2 -4.5 NT <1' 32.0 <0.@5 4.6 0.04 240 30.0 6.70 Nov-17 7.50 20.6 -4.6- NT _ <1 6.1 0,074 220 29'0 4"0 Mean 6.50 21.2 4.8 180 66 4.480.07 276 21.7 16.11Min 4.90 15.0 3.8 155 <1 =46.10...24 3.20 <0.025 210 11.04.60 Max 8.70 27.0 6.8 202 - .310 6.100.15354 30.0 36.10GW.Stds. 6.5-8.5 1.5 Soo 250 I Sample Date DTW Field Temp. -Field pH EC Fecal Coliform It I COD NO,-N I NHa-N Total-P TDS SO4. TOC ft. .'C Std. Units umhos/cm MPN/100 m1 - mg/L ---- Mar-15 5.20 15.0 - - 6.2 498 NT 1 <10 1 <10 1 <10 1 <10 16.10 NT NT 236 34.0 2.18 Jul -IS 6.50 _ 25.0 _ -4.3 I 450 -NT -21.60 NT NT 106 15.0 2.06 Nov-15 5.40 20.0 4.7 454 NT - 21.40 NT NT 288 12.0 3.05 Mar-16 530 17.0 6.3 374 'NT 18.50 NT NT 180 19.0 1.45 Jul-16 .7.50 - 20.4 .6.2 NT <S 1 29 NT 1 27 24.00 <0.045 <0.036 170 12.0 1.10 Sep -IS NT NT NT NT NT NT <0.045 NT NT NT 2.10 Oct-16 750 20.4 6.2 NT <1 26.00 0.85 0.026 150 11.0 1.20 Mar-17 4.75 13.7 4.2 NT <1 j <10 22.00 0.048 <0.025 220 15.0 0.76 Jul-17 1 8.50 22.8 4.3 NT. <1 54 _ 20.00 <0.045 0.11 1 140 14.0 1.20 Nov-17 9.00 16.8 - 4.2' NT <1 ] 10 17.00 0.150 0.089 120 20.0 1.00 Mean 6.65 19.0 S. 444<1 19 2073. 0.20 0.06 179 16.9 1.61 Min 4.75 13.7 4.2 374 ,<1 <30 16.30 <0.045 <0.025 106 11.0 0.76 Max 9.00 25.0 6.3 498 <1 I 54 26.00 0.85 0.11 288 34.0 3.05 GW Stds. 6.5-8.5 - I SO 1.5 Soo 250 NOTES: Red shaded values do not t ma_ t_ch grodmdwater standards: ft=feet - - °C =_Degrees Celsius Std. Units=Standard Units - - umhos/cm = micromlios per centimeter mg/L=parts per million NT= Not Tested DTW= depth to groundwater; Field Temp.= field temperature; EC=electrical con total organic carbon 'Samples collected and analyzed, by Microbac, Fayetteville, NC and ENCO Laboraf SG Foods, Inc., Turkey, NC 1 2 of 3 Sample DTW Field Temp. Field pH EC Fecal Coliform Date ft. °C Std. Units umhos/cm MPN/100 ml - Mar-15 7.80 18.0 6.2 369 NT Jul-15 7.80 27.0 '4:6 280 _ NT Nov-15 7.50 21.0 '4.3 235 NT Mar-16 5.70 19.0 'S.S 373 ' NT Jul-16 9.00 _ 23.9 .'4.1 NT <10 Oct-16 8.00 21.9 4.3. _ NT <10 - J Mar-17 8.50 15.8 -,3:6 NT <S Jul-17 9.00 25.2 4.4 NT <1 Nov-17 11.50 19.7 4.2 '' NT <1 Mean 8.31 21.3 4.6 314 2Min 5.70 15.8 3.6 235 <1 Max .11.50 27.0� 6.2 373 <10 GW Stds. 6.5-8.5 NOTES: - - i4shaded values do not match groundwater standards. ft =feet •C =Degrees Celsius Sid. Units=Standard Units umhos/cm = micromhos per centimeter mg/L=parts per million NT= Not Tested' DTW = depth to groundwater; Field Temp. = field temperature; EC = electrical condl ' Samples collected and analyzed by Microbac, Fayetteville, NC and ENCO Laboratc :otal organic carbon. SG Foods, Inc., Turkey, NC I 1 3of3 SUBMIT FORM ON YELLOW PAPER ONLY - DEPARTMENT OF ENVIRONMENT& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION ' PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 276994617 Phone:,(919)733.3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon El Remediation: Infiltration Gallery Turkey(Sife.1) NC 28393 County Sampson 'Ov, (siaie) (zip) ❑K Spray Field ❑ Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Plant Site No. of wells to be sampled: 13 ❑ Water Source Heat Pump ❑ Other: Irom Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 11/10/17 FIELD ANALYSES: WAS Well Depth: 30.Oft. Well Diameter: 2 in. pH 4.32 units Temp. 19.7 eC DRY at Depth to Water Level: 27.0 ft. below measuring point Screened Interval: to Spec. Cond. µMhos time of Measuring Point is 3 ft. above land surface —ft. Relative M.P. Elevation: —ft. ft. Odor sampling, check Volume of water pumped/bailed before sampling: 2.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and Feld acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/14 - 12/1 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 25 mg/I Nitrite (NO2) as N <0.017.mg/I Pb - Lead mg/I Coliform: MF Fecal <1 /100m1 Nitrate (NO3) as N 0.53 mg/I Zn - Zinc mg/l Coliform: MF Total /100ml Phosphorus: Total as P 0.045 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mgll Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 330 mg/I At - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 5.4 mg/I Ca - Calcium mg/I Chloride 200 mg/I Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/l Grease and Oils mg/I Cu - Copper mg/l ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate <2.9 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K- Potassium mg/I VOC , method # Total Ammonia <0.045 mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen; N%as N; Ammonla Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/l Ni - Nickel mgA , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal°/ Timothy P. Ruby, Environmental Water Manager IJ Al, n. (-(Aa / a-/ 14- I I ? Permiltee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee for Authorized Agent) (Date) GW-59 Rev. 1/2007 6UbAfiiI rUKIVI UN YU I ()VVr• rCK UNLT _R QUALITY MONITORING: REPORT FORM Name: Sager Creek Vegetable Company Name (if different): Address: 5900 Turkey Highway y (meet) NC 28393 County Sampson act Person: Randall Jarrell Telephone#:919-210-2500 Location/Site Name: Plant Site No, of wells to be sampled:13 IENT OFiENVIRONMENT &NATURAL RESOURCES OF WATER QUALITY-INFORMATION�PROCESSING UNIT PERMIT Number: Expiration Date: olautucl Non -Discharge WQ0004268 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑Remediation: Infiltration. Gallery 0 Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: L ID NUMBER (from Permit): MW-2 Date sample collected: 11/10/17 Depth: 19.75 ft. Well Diameter: 2 in. h to Water Level: 11.0 ft. below measuring point Screened Interval: _ft. to _ft. ;wring Point is 3 ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 10.0 gallons sample analyzed: 11/14 — 12/1 Laboratory Name: ENCO tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO2) as N <0.017 mg/I Coliform: MF Fecal <1 /100ml Nitrate (NO3) as N 0.27 mg/l Coliform: MF Total /100ml Phosphorus: Total as P <0.025 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mgA Dissolved Solids: Total 150 ri AI - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC 3.8 mg/I Ca - Calcium mg/I Chloride 83 mg/I Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate 9.7 ni Hg—Mercury mg/I Specific Conductance µMhos K- Potassium mg/I Total Ammonia 0.30 mg/I Mg- Magnesium mg/I (Ammonia Nitrogen; N%as N; Ammonia Nitrogen, Total) Mn- Manganese mg/I TKN as N mg/I Ni - Nickel mg/I FIELD ANALYSES: pH 5.46 units Spec. Cond. Odor Aooearance WELL Temp. 20.0 eC DRY at µMhos time of Certification No. 591 Pb - Lead mg/I Zn - Zinc mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GCIMS, HPLC). (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method # method # method # method # For Remediation. Systems Only (Attach Lab Reports): Influent Total VOCs: mg1L Effluent Total VOCs: mg/L VOC Removal% Timothy P. Ruby, Environmental Water Manager Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) (Date) GW-59 Rev. 1/2007 N SUBMIT FORM ON YELLOW PAPER ONLY —Im DEPARTMENT OF ENVIRONMENT.& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAIL SERVICE CENTER, RALEIGH;NC27699-1617 Phone: (919) 733-3221 _ FACILITY' INFORMATION Please Print Cleary or Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey Is'me1) NC 28393 County Sampson (City) Istao) (zip) ® Spray Field ❑ Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Plant Site No. of wells to be sampled: 13 ElWater Source Heat Pump ElOther: ("amPermit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-3 Date sample collected: 11/10/17 FIELD ANALYSES: WAS Well Depth: 17.0ft. Well Diameter: 2 in. pH 6.23 units Temp. 19.0 oC DRY at Depth to Water Level: 6.0 ft. below measuring point Screened Interval: ft. to ft. SpecCond. µMhos . time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: — ft. Odor sampling, check Volume of water pumped/bailed before sampling: 10.0gallons Appearance here:❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/14 -12/1 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 29 ni Nitrite (NO2) as N <0.017 ni Pb - Lead mgA Coliform: MF Fecal <1 /100ml Nitrate (NO3) as N 0.049 mg/1 Zn - Zinc mgA Coliform: MF Total /100ml Phosphorus: Total as P 0.33 mg/1 (Note; use MPN.meihod for highly mrbid samples) Orthophosphate mg/1 Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 400 mg/I Al -Aluminum mg/1 pH (when analyzed) units Be - Barium mg/I TOC 2.1 mg/I Ca - Calcium mg/I Chloride 140 mg/I Cd- Cadmium mg/1 Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/1 ORGANICS: (by GC, GC/MS, HPLC) , Phenol mg/I Fe - Iron mg/1 (Specify test and method #. ATTACH LAB REPORT.) Sulfate 57 mg/I Hg - Mercury mg/1 Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mgA VOC , method # Total Ammonia 0.072 mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N ni Ni - Nickel mgA , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: ni Effluent Total VOCs: ri VOC Removal% Timothy P. Ruby, Environmental Water Manager . J L4� P. Kt, / a.:/ 141117 Permittee (or Authorized Agent) Name and The- Please print or type Signature of Permittee t5rAuthorized Agent) (Dale) GW-59 Rev. 112007 SUBMIT FORM ON YELLOW PAPER ONLY _ DEPARTMENT OF ENVIRONMENT & NATURAL' RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearlyor Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑Lagoon ❑Remediation: Infiltration Gallery Turkey$tPeD NC 28393 County Sampson (City) (slate) (Zips ® Spray Field ❑Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/SIte,Name: Plant Site No. of wells to be sampled: 13 ❑ Water Source Heat Pump ❑ Other: from Pertnil SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 11/10/17 FIELD ANALYSES: WAS Well Depth: 30.Oft. Well Diameter: 2'in. pH 4.14 units Temp. 18.9 eC DRY at Depth to Water Level: 13.0 ft. below measuring point Screened Interval: ft. to ft. Spec. Cord. µMhos time of Measuring Point is 3 ft. above land surface — Relative M.P. Elevation: ft. Odor sampling, check Volume of water pumped/bailed before sampling: 12.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: DYES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/10 - 12/1 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO2) as N <0.017 mg/1 Pb - Lead mg/I Coliform: MF Fecal <1 /100ml Nitrate (NO3) as N 9.2 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P <0.025 mg/I (Note: Use MPN method for hlghlytti samples) Orthophosphate mg/1 Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 100 mg/l Al -Aluminum mg/l pH (when analyzed) units Ba - Barium mg/I TOO 0.92 mg/I Ca - Calcium mg/I Chloride 26 mg/I Cd- Cadmium mg/I - Arsenic mg/I Chromium: Total mg/I Grease and Oils _ mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mgA Fe- Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 3.6 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC , method # Total Ammonia <0.045 mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen;NHsas N; Ammonia Nitrogen, Total) Mn - Manganese mg/I. , method# TKN as N mg/l Ni - Nickel mg/I , method# .For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs:. mg/L Effluent Total. VOCs: _ _mg/L VOC Removal% Timothy P. Ruby, Environmental Water Manager Permiltee (or Authorized Agent) Name and Title- Please print or type Signature of Permittee (o Authorized Agent) (Date) GW-59 Rev. 112007 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OFENVIRONMENT;& NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: er DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAIL :SERVICE CENTER, RALEIGH,NC27699�1617 Phone:(919)733-3221 FACILITY INFORMATION Please Print Cleadyor Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC Permit Name (if different): NPDES Other Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED Turkey (s'men NC 28393 County Sampson El Lagoon ElRemediation: Infiltration Gallery (City) (state) (zips ® Spray Field ❑ Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Rowan Site No.. of wells to be sampled: 13 ❑ Water Source Heat Pump ❑ Other: from Permit RAMGI IN(-,INF11RM ATIfIN If WELL LID NUMBER (from Permit): MW-R1 Date sample collected: 11/14/17 Depth: 15.Oft. Well Diameter: 2 in. 1 to Water Level: 8.0 ft. below measuring point Screened Interval: _ft. to _ft. ,wring Point is 3 ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 8.0 gallons sample analyzed: 11/14 - COD 68 mg/I Coliform: MF Fecal <1 /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total. 94 mg/I pH (when analyzed) units TOG 7.5 ri Chloride 56 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/l Sulfate 17 ri Specific Conductance µMh Total Ammonia 0.076 mg/l (Ammonia Nitrogen: NH3es N; Ammonia Nitrogen, Total) TKN as N mg/I Laboratory Name: ENCO colloidal concentrations. Nitrite (NO,) as N 0.13 mg/I Nitrate (NO3) as N <0.20 mg/I Phosphorus: Total as P 3.3 mg/I Orthophosphate mg/I AI - Aluminum mg/I Be - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/1 Cu - Copper mg/1 Fe - Iron mg/I Hg - Mercury mg/I K- Potassium mg/I Mg - Magnesium It Mn- Manganese mg/I Ni - Nickel mg/I FIELD ANALYSES pH 5.11 units Temp. 19.1 eC Spec. Cord. µMhos Odor Appearance Certification No. 591 Pb-Lead mg/1 Zn - Zinc mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal°/ Timothy P. Ruby, Environmental Water Manager -j �. «n � �/ `�/ 19 Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (o Authorized Agent) (Date) GW-59 Rev. 112007 at of n runm VIVLI - DEPARTMENTOF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER'QUALITY-INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAIL SERVICE ,CENTER, RALEIGH,NC27699-1617 Phone:(919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC Permit Name (if different): NPDES Other Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED Turkey NC 28393 County Sampson ❑ Lagoon ❑ Remediation: Infiltration Gallery (City) (slate) (zip) ® Spray Field ❑ Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Rowan Site No. of wells to be sampled: 13 ❑ Water Source Heat Pump ❑ Other: LID NUMBER (from Permit): MW-R2A Date sample collected: 11/14/17 Depth: 15.Oft. Well Diameter: 2in. i to Water Level: 7.5 ft. below measuring point Screened Interval: _ft. to _ft. ,uring Point is -3 ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 7.0 gallons sample analyzed: 11/14 - 12/1 LaboratoryName: ENCO ,AMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO2) as N 0.10 mg/I Coliform: MF Fecal <1 /100ml Nitrate (NO3) as N <0.20 mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0.026 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total 50 mgn AI - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC 0.55 nrl Ca - Calcium mg/I Chloride 39 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron . mg/I Sulfate 1-3 mg/I Hg - Mercury mg/I Specific Conductance µMhos K - Potassium mg/I Total Ammonia <0.045 mg/I Mg - Magnesium mg/I (Ammonia Nitrogen; NHlas N; Ammonia Nitrogen, Total) Mn - Manganese mg/I TKN as N mg/I Ni - Nickel mg/I FIELD ANALYSES: WAS pH 4.62 units Temp. 19.8 eC DRY at Spec. Cond. µMhos time of sampling, Odor check Appearance here: El Certification No. 591 Pb - Lead mg/I Zn - Zinc mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method#. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs; mg/L Effluent Total VOCs: mg/L VOC Removal% Timothy P. Ruby, Environmental Water Manager Permitlee (or Authorized Anent) Name and Title - Please print or type Signature of Permiitee (of Authorized Agent) (Date) GW-59 Rev. 1/2007 SUBMIT FORM ON YELLOW PAPER ONLY _ DEPARTMENT OF ENVIRONMENT S NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAIL SERVICE 'CENTER, ,RALEIGH,NC27699.1617 Phone:'(919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: .Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey (s"s'.t) NC 28393 County Sampson (csy) (State) (zip) ® Spray Field El Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Rowan Site No. of wells to be sampled: 13 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-R3 Date sample collected: 11/10/17 FIELD ANALYSES: WAS Well Depth: 18.Oft. Well Diameter: 2 in. pH 4.19 units Temp. 19.4 aC DRY at Depth to Water Level: 8.5 ft. below measuring point Screened Interval: _ft. to _ft. Spec. Conti. µ Mhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 6.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/10 - 12/1 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO,) as N <0.017 mg/I Pb- Lead mg/I Coliform: MF Fecal <1 /100ml Nitrate (NO3) as N 1.1 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P <0.025 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 250 mg/I Al - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 1.8 mg/I Ca - Calcium mg/I Chloride 120 mg/I Cd - Cadmium mg/1 Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 54 mg/I Hg -. Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC , method # Total Ammonia 0.045 mg/1 Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Mn - Manganese mg/I , method # TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Timothy P. Ruby, Environmental Water Manager Permlltee (or Authorized Agent) Name and Title -Please print or type GW-59 Rev. 1/2007 SUBMIT FORM ON YELI OW PAPER ONLY - DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING, UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, No 27699-1617 Phone:(919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date; 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIO NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey (Sbru.0 NC 28393 County Sampson (City) (Stare) IZp) ® Spray Field ❑Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Rowan Site No. of wells to be sampled:13 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-R4 Date sample collected: 11114/17 FIELD ANALYSES: WAS Well Depth: 15.Oft. Well Diameter: 2 in. pH 4.45 units Temp. 20.5 eC DRY at Depth to Water Level: 7.0 ft. below measuring point .Screened Interval: ft. — to _ft. Spec. Cond. µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 7.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES El NO and field acidified: ❑YES El NO LABORATORY INFORMATION Date sample analyzed: 11/14 - 12/1 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD <10 mg/I Nitrite (NO2) as N 0.16 mg/I Pb - Lead ni Coliform: MF Fecal <1 /100mi Nitrate (NO3) as N <0.20 mg/I Zn - Zinc mg/I Coliform: MF Total /100m1 Phosphorus: Total as P 1.4 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 130 mg/I AI - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 1.5 mg/I Ca - Calcium mg/I Chloride 66 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 16 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia <0.045 mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) Min - Manganese mg/I ,method# TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L. Effluent Total VOIDS: mg/L VOC Removal°/ Timothy P. Ruby, Environmental Water Manager Permiltee (or Authorized Agent) Name and TWe-.Please print ortype GW-59 Rev. 112007 Pennittee /7 SUBMIT FORM ON YFLIOW PAPER ONLY - DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAIL SERVICE CENTER, ;RALEIGH,NC27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey (51iEe0 NC 28393 County Sampson (cuy) (stata) (zip) ® Spray Field ❑ Remediation: Contact Person: Randall Jarrell Telephone#: 919-210-2600 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Rowan Site No. of wells tobe sampled: 13 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION K WELL WELL ID NUMBER (from Permit): MW-R5A Date sample collected: 7/13/17 FIELD ANALYSES: WAS Well Depth: 17.Oft. Well Diameter: 2 in. pH 4.56 units Temp. 20.6 oC DRY at Depth to Water Level: 7.5 ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor sampling, check Volume of water pumped/bailed before sampling: 7.0 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑YES El NO LABORATORY INFORMATION Date sample analyzed: 11114 - 1211 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 17 TV Nitrite (NO,) as N 0.14 mg/I Pb - Lead mgA Coliform: MF Fecal <1 /100ml Nitrate (NO3) as N 2.4 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0.10 mg/I (Note: use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 150 mg/I AI - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 1.7 mg/I Ca - Calcium mg/l Chloride 56 mg/I Cd- Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu- Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 24 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K- Potassium mg/I VOC , method # Total Ammonia <0.045 mg/I Mg - Magnesium mg/I , method # (Ammonia Nitrogen; NHras N; Ammonla Nitrogen, Total) Mn - Manganese mg/l , method # TKN as N mg/I Ni - Nickel mg/I , method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOIDS: mg/L Effluent Total VOIDS: mg/L VOC Removal% Timothy P. Ruby, Environmental Water Manager Permittee (or Authorized Agent) Name and Title- Please, print or type v A'� e . .Signature ofPermittee (or uthor� ized A 17 GW-59 Rev. 112007 JuuwuI rumvi VN T, - wJL rNt"CR VIVLI NDWATER QUALITY MONITORING: LIANCE REPORT FORM Name: Sager Creek Vegetable Company Name (if different): Address: 5900 Turkey Highway y I timme') NC 28393 County Sampson act Person: Randall Jarrell Location/Site Name: Rowan Site LID NUMBER (from Permit): MW-R6 Depth: 18.0 ft. i to Water Level: 9.5.ft. below measuring point Turing Point is 3 ft. above land surface ne of water pumped/bailed before sampling: sample analyzed: 11/16 - COD 12 mg/I Coliform: MF Fecal <1 /100ml Coliform: MF Total 1100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 220 mg/1 pH (when analyzed) units TOC 4.6 mg/I Chloride 120 mg/I Arsenic mg/I Grease and Oils mg/1 Phenol mg/I Sulfate 29 mg/I Specific Conductance µMhos Total Ammonia 6.1 mg/I (Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total) TKN as N mg/I 10.0 Telephone#:919-210-2500 No. of wells to be. sampled: 13 Date sample collected: 11/15/17 Well Diameter: 2 in. Screened Interval: ft. to ft. Relative M.P. Elevation: ft. Laboratory Name: ENCO colloidal concentrations. Nitrite (NO2) as N <0.017 mg/I Nitrate (NO3) as N 0.16 mg/I Phosphorus: Total as P 0.074 mg/I Orthophosphate mg/I AI -Aluminum mg/I Be - Barium mg/1 Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K- Potassium mg/I Mg - Magnesium mg/l Mn- Manganese mg/1 Ni - Nickel mg/I 'ARTMENT OF ENVIRONMENT & NATURAL RESOURCES ISION OF WATER QUALITYdNFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 733-3221 RMIT Number: Expiration Date: 5/31/2021 n-Discharge WQ0004268 UIC DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump El Other.: FIELD ANALYSES: pH 5.13 units Spec. Cord. Odor Appearance WELL Temp. 20.2 eC DRY at µMhos time of Certification No. 591 Pb - Lead mg/I Zn - Zinc mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Timothy P. Ruby, Environmetal Water Manager d Ln� F. wt/may/ / V 14117 Permittee (or Authorized Agent) Name and Title - Please print or Signature of Permlltee (or Afithanzed Agent) a (Date) GW-59 Rev. 1/2007 IN SUBMIT FORM ON YELLOIL PAPER ONLY DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY-MFORMATION,PROCESSING UNIT COMPLIANCE REPORT FORM 1617 MAIL SERVICE CENTER, RALEIGH, No 27699-1617 Phone: (919) 733-3221 FACILITY INFORMATION - Please Print Clearly or Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC NPDES Other Permit Name (if different): Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Turkey is""") NC 28393 County Sampson (CIIv1 (Stata) (Zip) ® Spray Field ❑Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Rowan Site No. of wells to be sampled: 13 ElWater Source Heat Pump ElOther: from Permit SAMPLING INFORMATION if WELL WELL ID NUMBER (from Permit):, MW-R7 Date sample collected: 11/15/17 FIELD ANALYSES: WAS Well Depth: 15.0ft. Well Diameter: 2 in. pH 4.19 units Temp. 16.8 eC DRY at Depth to Water Level: 9.0 ft. below measuring point - Screened Interval: ft. to ft. Spec. Cond. µMhos time of sampling, Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of waterpumped/bailed before sampling: 6.0 gallons Appearance here:.❑ Samples for metals were collected. unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 11/16 - 12/1 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 17 mg/I Nitrite (NO,) as N <0.017 mg/I Pb - Lead mg/I Coliform: MF Fecal <1 /100ml Nitrate (NO3) as N 0.28 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0.15 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 180 mg/I AI - Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 4.2 mgn Ca - Calcium mg/I Chloride 110 mg/I Cd- Cadmium mg/I Arsenic mgh Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate 13 mg/I Hg - Mercury mg/I Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC , method # Total Ammonia 0.061 mg/I Mg - Magnesium mg/I , method # (Ammonia Nltrogen; NH3as N; Ammonia Nitrogen, Total) Mn- Manganese mg/I ,method# TKN as N mg/I Ni - Nickel mg/I , method# For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs:. mg/L VOC Removal°/ Timothy P. Ruby, Environmental Water Manager Permlttee (or Authorized Agent) Name and Title- Please print or type GW-59 Rev. 1/2007 SUBMIT FORM ON YELLOW PAPER ONLY NDWATER QUALITY MONITORING: LIANCE REPORT FORM Name: Sager Creek Vegetable Company Name (if different): Address: 5900 Turkey Highway y (Stm t) NC 28393 County Sampson act Person: Randall Jarrell Telephone#:919-210-2500 Location/Site Name: Rowan Site No. of wells to be sampled: 13 LID NUMBER (from Permit): MW-R8 Date sample collected: 11/15/17 Depth: 18.0% Well Diameter: 2 in. 1 to Water Level: 11.0 ft. below measuring point Screened Interval: ft. to ft. luring Point is 3 ft. above land surface Relative M.P. Elevation: ft. neof water pumped/bailed before sampling: 6.0 gallons Iles for metals were collected unfiltered: DYES ❑ NO and field acidified: DYES ❑ NO sample analyzed: 11/16 - tAMETERS NOTE: Values should reflect dissolved COD 10 mg/I Coliform: MF Fecal <1 /I ooml Coliform: MF Total /loom[ (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 120 mg/I pH (when analyzed) units TOC 1.0 mg/I Chloride 9.6 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate 20 mg/I Specific Conductance µMhos Total Ammonia 0.15 mg/I (Ammonla Nitrogen; NH3as N; Ammonia Nitrogen, Total) TKN as N mg/I Laboratory Name: ENCO colloidal concentrations. Nitrite (NO,) as N <0.017 mg/I Nitrate (NO3) as N 17 mg/I Phosphorus: Total as P 0.089 mg/I Orthophosphate mg/I AI - Aluminum mg/I Ba - Barium mg/I Ca - Calcium mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K- Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I N[ - Nickel mg/I 'ARTMENT OF ENVIRONMENTS NATURAL RESOURCES ISION OF WATER QUALITY -INFORMATION PROCESSING UNIT 7 MAIL SERVICE CENTER, RALEIGH, NC 27699.1617 Phone: (919) 733-3221 !RMIT Number: Expiration Date: 5/31/2021 n-DischargeWQ0004268 UIC IDES Other 'PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remedlatlon: Infiltration Gallery ® Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: pH 4.12 units Temp. 21.0 eC Spec. Cord. µMhos Odor Appearance Pb - Lead Zn - Zinc Certification No. 591 mg/I mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method# method # method # method # at Of GW-59 Rev. 1/2007 SUBMIT FORM ON YELLOW PAPER ONLY - DEPARTMENT OF ENVIRONMENT B NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: DIVISION OF WATER QUALITY -INFORMATION. PROCESSING UNIT COMPLIANCE REPORT FORM 1617MAIL SERVICE 'CENTER, RALEIGH,NC27699-1617 Phone:(919)733-3221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: 5/31/2021 Facility Name: Sager Creek Vegetable Company Non -Discharge WQ0004268 UIC Permit Name (if different): NPDES Other Facility Address: 5900 Turkey Highway TYPE OF PERMITTED OPERATION BEING MONITORED Turkey (51f et) NC 28393 County Sampson ❑ Lagoon ❑ Remediation: Infiltration Gallery (trill I6mle) Or) ® Spray Field ' ❑Remediation: Contact Person: Randall Jarrell Telephone#:919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Rowan Site No. of wells to be sampled: 13 ❑ Water Source Heat Pump ❑ Other: LID NUMBER (from Permit): MW-R9 Depth: 17.Oft. i to Water Level: 11.5 ft. below measuring point ,uring Point is 3 ft. above land surface ne of water pumped/bailed before sampling: sample analyzed: 11/16 - COD 12 mgll Coliform: MF Fecal <1 /100m1 Coliform: MF Total /100ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 180 mg/I pH (when analyzed) units TOC 5.2 mg/I Chloride 59 moll Arsenic mg/I Grease and Oils mg/1 Sulfate 66 mg/1 Specific Conductance µMh Total Ammonia <0.045 mg/I (Ammonla NlUogen; NH,as N; Ammonla Nitrogen, Total) TKN as N mg/1 5.0 Date sample collected: 11/15/17 Well Diameter: 2 in. Screened Interval: ft. to ft. Relative M.P. Elevation: ft. Laboratory Name: ENCO colloidal concentrations. Nitrite (NO,) as N <0.017 mg/I Nitrate (NO3) as N 0.79 mg/1 Phosphorus: Total as P 0.031 mg/I Orthophosphate mg/1 At - Aluminum mg/1 Ba- Barium mg/I Ca - Calcium mg/I Cd - Cadmium moll Chromium: Total mg/1 Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/l K - Potassium _ mg/I Mg - Magnesium mg/l Mn - Manganese mg/I Ni - Nickel mg/I FIELD ANALYSES: pH 4.18 units Temp. 19.7 eC Spec. Cond. µMhos Odor Appearance Certification No. 591 Pb - Lead mg/I Zn - Zinc mg/I Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Timothy P. Ruby, Environmental Water Manager J iyr. Lr 01/A017 Permillee (or Authorized Agent) Name and Title- Please print or type Slgnature of Permittee ( Authorized Agent) (Date) GW-59 Rev. 1/2007 at of J .a.- CO Laboratories Accurate, Tamely, Responsive. Innov atirc, 102-A Woodwinds Industrial Court Cary NC, 27511 Phone: 919.467.3090 FAX: 919.467.3515 Friday, December 1, 2017 WASTEWATER MANAGEMENT, LLC (WA013) Attn: RANDALLJARRELL P.O. Box 578 Pittsboro, NC 27312 RE: Laboratory Results for Project Number: [none], Project Name/Desc: Sager Foods -MWs ENCO Workorder(s): CALS466,CA17316,CA37349 Dear RANDALL JARRELL, Enclosed is a copy of your laboratory report for test samples received by our laboratory between Friday, November 10, 2017 and Wednesday, November 15, 2017. Unless otherwise noted in an attached project narrative, all samples were received in acceptable condition and processed in accordance with the referenced methods/procedures. Results for these procedures apply only to the samples as submitted. The analytical results contained in this report are in compliance with NELAC standards, except as noted in the project narrative. This report shall not be reproduced except in full, without the written approval of the Laboratory. This report contains only those analyses performed by Environmental Conservation Laboratories. Unless otherwise noted, all analyses were performed at ENCO Cary. Data from outside organizations will be reported under separate cover. If you have any questions or require further information, please do not hesitate to contact me. Sincerely, „ Stephanie Franz Project Manager Enclosure(s) FINAL This report relates only to the sample a received by the laboratory, and may only be reproduced In full. I Page 1 Of 39 W W W.encolabsxom SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: MW-1 Lab ID: CA15466-01 Sampled: 11/10/17 10:20 Received: 11/10/17 14:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(g) Analysis Date/Time(.) Colilert 18 NO PREP 11/10/17 18:15 11/11/17 13:29 11/10/17 15:25 11/11/17 11:00 EPA 300.0 NO PREP 12/08/17 11/20/17 16:27 11/20/17 18:31 EPA 350.1 NO PREP 12/08/17 11/17/17 12:10 11/17/17 12:10 EPA 353.2 NO PREP 11/12/17 10:20 11/10/17 17:15 11/10/17 17:15 EPA 353.2 NO PREP 12/08/17 11/18/17 15:19 11/18/17 15:19 EPA 353.2 NO PREP 08/05/20 11/20/17 11:07 11/20/17 12:09 EPA 365.4 Same 12/08/17 11/17/17 11:55 11/20/17 11:50 SM 2540C-1997 NO PREP 11/17/17 11/13/17 16:25 11/13/17 16:25 SM 5220D-1997 Same 12/08/17 11/14/17 17:10 11/14/17 19:45 SM 53308-2000 NO PREP 12/08/17 11/14/17 12:30 11/14/17 12:57 Client ID: MW-1 Lab ID: CA15466-OIRE1 Sampled: 11/10/17 10:20 Received: 11/10/17 14:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date ITime(s) EPA 300.0 NO PREP 12/08/17 11/20/17 16:27 1120/17 18:46 Client ID: MW-2 Lab ID: CA15466-02 Sampled: 11/10/17 09:45 Received: 11/10/17 14:45 Parameter Preparation Hold Date/Time(sl Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 NO PREP 11/10/17 17:40 11/11/17 13:29 11/10/17 15:25 11/11/17 11:00 EPA 300.0 NO PREP 12/08/17 1120/17 16:27 1120/17 19:00 EPA 350.1 NO PREP 12/08/17 11/17/17 12:13 11/17/17 12:13 EPA 353.2 NO PREP 11/12/17 09:45 11/10/17 17:16 -11/10/17 17:16 EPA 353.2 NO PREP 12/08/17 11/18/17 15:21 11/18/17 15:21 EPA 353.2 NO PREP 08/05/20 11/20/17 11:07 1120/17 12:09 EPA 365.4 Same 12/08/17 11/17/17 11:55 1120/17 11:51 SM 2540C-1997 NO PREP 11/17/17 11/13/17 16:25 11/13/17 16:25 SM 5220D-1997 Same 12/08/17 11/14/17 17:10 11/14/17 19:45 SM 5310B-2000 NO PREP 12/08/17 11/14/17 12:30 11/14/17 12:57 Client ID: MW-3 Lab ID: CA15466-03 Sampled: 11/10/17 11:45 Received: 11/10/17 14:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis DateRme(s) Gellert 18 NO PREP 11/10/17 19:40 11/11/17 13:29 11/10/17 15:25 11/11/17 11:00 EPA 300.0 NO PREP 12/08/17 1120/17 16:27 1120/17 19:29 EPA 350.1 NO PREP 12/08/17 11/17/17 12:15 11/17/17 12:15 EPA 353.2 NO PREP 11/12/17 11:45 11/10/17 17:17 11/10/17 17:17 EPA 353.2 NO PREP 12/08/17 11/18/17 13:54 11/18/17 13:54 EPA 353.2 NO PREP 08/05/20 11/20/17 11:07 1120/17 12:09 EPA 365.4 Same 12/08/17 11/17/17 11:55 1120/17 11:53 SM 2540C-1997 NO PREP 11/17/17 11/13/17 16:25 11/13/17 16:25 SM 3220D-1997 Same 12/08/17 11/14/17 17:10 11/14/17 19:45 SM 5310B-2000 NO PREP 12/08/17 11/14/17 12:30 11/14/17 12:57 Client ID: MW-3 Lab ID: CA15466-03RE1 Sampled: 11/10/17 11:45 Received: 11/10/17 14:45 Parameter Preparation Hold Date/rime(s) Prep Date/Time(s) Analysis Date/Time(.) EPA 300.0 NO PREP 12/08/17 11/20/17 16:27 11/20/17 19:14 FINAL Thls report relates only to the sample as received by the laboratory, and may only be reproduced In full. I Page 2 OT 39 WWW.encalabsxomn SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: MW-4 Lab ID: CA35466-04 Sampled: 11/10/17 11:00 Received: 11/10/17 14:45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Anaivsis Date/Time(s) Colilert 18 NO PREP 11/10/17 18:55 11/11/17 13:29 11/10/17 15:25 11/11/17 11:00 EPA 300.0 NO PREP 12/08/17 11/20/17 16:27 11/20/17 19:43 EPA 350.1 NO PREP 12/08/17 11/17/17 12:16 11/17/17 12:16 EPA 353.2 NO PREP 11/12/17 11:00 11/10/17 17:18 11/10/17 17:18 EPA 353.2 NO PREP 12/08/17 11/18/17 13:59 11/18/17 13:59 EPA 353.2 NO PREP 08/05/20 11/20/17 11:07 11/20/17 12:09 EPA 365.4 Same 12/08/17 11/17/17 11:55 11/20/17 11:54 SM 254OC-1997 NO PREP 11/17/17 11/13/17 16:25 11/13/17 16:25 SM'S220D-1997 Same 12/08/17 11/14/17 17:10 11/14/17 19:45 SM 53103-2000 NO PREP 12108117' 11/14/17 12:30 11/14/17 12:57 Client ID: R-3 Lab ID: CA35466-05 Sampled: 11/10/17 12:45 Received: 11/10/17 14.45 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 NO PREP 11/10/17 20:40 11/11/17 13:29 11/10/17 15:25 11/11/17 11:00 EPA 300.0 NO PREP 12/08/17 11/20/17 16:27 1120117 19:57 EPA 350.1 NO PREP 12/08/17 11/17/17 12:22 11/17/17 12:22 EPA 353.2 NO PREP 11/12/17 12:45 11/10/17 17:19 11/10/17 17:19 EPA 353.2 NO PREP 12/08/17 11/18/17 14:03 11/18/17 14:03 EPA 353.2 NO PREP 08/05/20 11/20/17 11:07 11/20/17 12:09 EPA 365.4 Same 12/08/17 11/17/17 11:55 11/20/17 11:55 SM 254OC-1997 NO PREP 11/17/17 11/13/17 16:25 11/13/17 16:25 SM 522OD-1997 Same 12/08/17 11/14/17 17:10 11/14/17 19:45 SM 5330B-2000 NO PREP 12/08/17 11/14/17 12:30 11/14/17 12:57 Client ID: R-3 Lab ID: CA15466-OBREI Sampled: 11/10/17 12:45 Received: 11(10/17 14:45 Parameter Preparation Hold Date/Time(s) Prey Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 12/08/17 11/20/17 16:27 1121/17 09:49 Client ID: R-1 Lab ID: CA17316-01 Sampled: 11/14/17 09:30 _ Received: 11/14/17 13:25 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Timefs) CALC 300.0 NO PREP 08/09/20 11/21/17 11:52 11/21/17 11:52 Colilert 18 NO PREP 11/14/17 17:25 11/15/17 13:29 11/14/17 15:25 11/15/17 10:00 EPA 300.0 NO PREP 11/16/17 09:30 11/14/17 19:38 11/14/17 19:38 EPA 300.0 NO PREP 12/12/17 11/14/17 19:38 11/14/17 19:38 EPA 350.1 NO PREP 12/12/17 11/17/17 12:42. 11/17/17 12:42 SM 254OC-1997 NO PREP 11/21/17 11/20/17 18:15 1120/17 18:15 SM 522OD-1997 Same 12/12/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/12/17 11/21/17 12:00 11/21/17 12:45 Client ID: 11-1 Lab ID: CA17316.01RE1 Sampled: 11/14/17 09:30 Received: 11/14/17 13:25 Parameter Preparation HOW Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 365.4 Same 12/12/17 11/30/17 11:30 12/01/17 09:58 Client ID: R-2a Lab ID: CA17316-02 Sampled: 11/14/17 10:15 Received: 11/14/17 13:25 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) CALC 300.0 NO PREP 08/09/20 11/21/17 11:52 11/21/17 11:52 Colilert 18 NO PREP 11/14/17 18:10 11/15/17 13:29 11/14/17 15:25 11/15/17 10:00 EPA 300.0 NO PREP 11/16/17 10:15 11/14/17 19:53 11/14/17 19:53 EPA 300.0 NO PREP 12/12/17 11/14/17 19:53 11/14/17 19:53 EPA 350.1 NO PREP 12/12/17 11/17/17 12:44 11/17/17 12:44 EPA 365A Same 12/12/17 11/30/17 11:30 12/01/17 09:12 SM 254OC-1997 NO PREP 11/21/17 11/20/17 18:15 11/20/17 18:15, SM 5220D-1997 Same 12/12/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/12/17 11/21/17 12:00 11/21/17. 12:45 FINAL lids report relates onry to the sample as received by the laboratory, and may only be reproduced in full. I Page 3 OP 39 w .encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE ClientID: R-4 Lab ID: CA17316-03 Sampled: 11/14/1711:00 Received: 11/141171325 Parameter Preparation Hold Date/Timefsl Prep Date/Time(s) Analysis Date/Time(s) CALC 300.0 NO PREP 08/09/213 11/21/17 11:52 11/21/17 11:52 CoIllert 18 NO PREP 11/14/17 18:55 11/15/17 13:29 11/14/17 15:25 11/15/17 10:00 EPA 300.0 NO PREP 11/16/17 11:00 11/14/17 20:07 11/14/17 20:07 EPA 300.0 NO PREP 12/12/17 11/14/17 20:07 11/14/17 20:07 EPA 350.1 NO PREP 12/12/17 11/17/17 12:45 11/17/17 12:46 EPA 365.4 Same 12/12/17 11/30/17 11:30 12/01/17 09:13 SM 254OC-1997 NO PREP 11/21/17 11/20/17 18:15 11/20/17 18:15 SM 5220D-1997 Same 12/12/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/12/17 11/21/17 12:00 11/21/17 12:43 Client ID: R-Sa Lab ID: CA17316-04 Sampled: 11/14/17 11:45 Received: 11/14/17 13:25 Parameter Preparation Hold Date/Timefsl Prep Date/Time(s) Analysis Date/Time(s) CALL 300.0 NO PREP 08/09/20 11/21/17 11:52 11/21/17 11:52 Colilert IS NO PREP 11/14/17 19:40 11/15/17 13:29 11/14/17 15:25 11/15/17 10:00 EPA 300.0 NO PREP 11/16/17 11:45 11/14/17 20:21 11/14/17 20:21 EPA 300.0 NO PREP 12/12/17 11/14/17 20:21 11/14/17 20:21 EPA 350.1 NO PREP 12/12/17 11/17/17 12:47 11/17/17 12:47 EPA 365.4 Same 12/12/17 11/30/17 11:30 12/01/17 09:14 SM'254OC-1997 NO PREP 11/21/17 11/20/17 15:40 11/20/17 15:40 SM5220D-1997 Same 12/12/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/12/17 11/21/17 12:00 11/21/17 12:45 ClientID: R-6 Lab ID: CA17349-01 Sampled: 11/15/17 10:35 Received: 11/15/17 11:50 -Parameter Preparation Hold Date/Timefsl Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 NO PREP 11/15/17 18:30 11/16/17 13:04 11/15/17 15:00 11/16/17 09:58 EPA 300.0 NO PREP 12/13/17 11/22/17 13:25 11/22/17 20:58 EPA 350.1 NO PREP 12/13/17 1122/17 09:09 1122/17 11:24 EPA 353.2 NO PREP 11/17/17 10:35 11/16/17 20:19 11/16/17 20:19 EPA 353.2 NO PREP 12/13/17 11/18/17 16:35 11/18/17 16:35 EPA 353.2 NO PREP 08/10/20 11/20/17 11:13 11/20/17 12:32 EPA 365.4 Same 12/13/17 11/30/17 11:30 12/01/17 09:16 SM 254OC-1997 NO PREP 11/22/17 11/21/17 16:20 11/21/17 16:20 SM 5220D-1997 Same 12/13/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/13/17 11/27/17 10:21 11/28/17 11:46 ClientID: R-6 Lab ID: CA17349-OSRE1 Sampled: 11/15/17 10:35 Received: 11/15/17 11:50 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 12/13/17 11/22/17 13:25 1122/17 20:15 Client ID: R-7 Lab ID: CA17349-02 Sampled: 11/15/17 09:45 Received: 11/15/17 11:50 Parameter Preparation Hold Date/Timefsl Prep Date/Time(s) Analysis Date/Time(s) Colilert 18 NO PREP 11/15/17 17:40 11/16/17 13:04 11/15/17 15:00 11/16/17 09:58 EPA 300.0 NO PREP 12/13/17 1122/17 13:25 11/22/17 21:27 EPA 350.1 NO PREP 12/13/17 1122/17 09:09 11/22/17 11:26 EPA 353.2 NO PREP 11/17/17 09:45 11/16/17 20:20 11/16/17 20:20 EPA 353.2 NO PREP 12/13/17 11/18/17 16:35 11/18/17 16:35 EPA 353.2 NO PREP 08/10/20 11/20/17 11:13 11/20/17 12:32 EPA 365.4 Same 12/13/17 11/30/17 11:30 12/01/17 09:17 SM 254OC-1997 NO PREP 11/22/17 1121/17 16:20 11/21/17 16:20 SM 5220D-1997 Same 12/13/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/13/17 11/27/17 10:21 1128/17 11:46 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 4 Of 39 w .encolabs.com SAMPLE SUMMARY/LABORATORY CHRONICLE Client ID: R-7 Lab ID: CA17349-02RE1 Sampled: 11/15/17 09:45 Received: 11/15/17 11:50 Parameter Preparation Hold Date/rime(s) Prep Date/Time(s) Analysis Date/Time(s) EPA 300.0 NO PREP 12/13/17 1122/17 13:25 11/22/17 21:13 Client ID: R-8 Lab ID: CA17349-03 Sampled: 11/15/17 08:50 Received: 11/15/17 11:50 Parameter Preparation Hold Date/Time(s) Prep Date/Time(s) Analvs s Date/Time(s) Colilert 18 NO PREP 11/15/17 16:45 11/16/17 13:04 11/15/17 15:00 11/16/17 09:58 EPA 300.0 NO PREP 12/13/17 1122/17 13:25 1122/17 21:41 EPA 350.1 NO PREP 12/13/17 11/22/17 09:09 11/22/17 11:27 EPA 353.2 NO PREP 11/17/17 08:50 11/16/17 20:21 11/16/17 20:21 EPA 353.2 NO PREP 12/13/17 11/18/17 16:36 11/18/17 16:36 EPA 353.2 NO PREP 08/10/20 1120/17 11:13 1120/17 12:32 EPA 365.4 'Same 12/13/17 11/30/17 11:30 12/01/17 09:18 SM 254OC-1997 NO PREP 11/22/17 1121/17 16:20 11/21/17 16:20 SM 5220D-1997 Same 12/13/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/13/17 11/27/17 10:21 11/28/17 11:46 Client ID: R-9 Lab ID: CA17349-04 Sampled: 11/15/17 08:00 Received: 11/15/17 11:50 - parameter Preparation Hold Date/Time(sl - Prep Date/Time(s) Analvsis Date/ rme(s) Colilert 18 NO PREP 11/15/17 15:55 11/16/17 13:04 11/15/17 15:00 11/16/17 09:58 EPA 300.0 NO PREP 12/13/17 1122/17 13:25 11/22/17 21:56 EPA 350.1 NO PREP 12/13/17 1122/17 09:09 11/22/17 11:32 EPA 353.2 NO PREP 11/17/17 08:00 11/16/17 20:22 11/16/17 20:22 EPA 353.2 NO PREP 12/13/17 11/18/17 16:37 11/18/17 16:37 EPA 353.2 NO PREP 08/10/20 1120/17 11:13 1120/17 12:32 EPA 365.4 Same 12/13/17 11/30/17 11:30 12/01/17 09:20 SM 2540C-1997 NO PREP 11/22/17 11/21/17 16:20 1121/17 16:20 SM 522OD-1997 Same 12/13/17 11/17/17 11:37 11/17/17 16:10 SM 531OB-2000 NO PREP 12/13/17 11/27/17 10:21 1128/17 11:46 FINAL This reportrelates only to the sample as remved by the Iabeatory, and may only be reproduced in full. Page 5 Of 39 SMho w .encolabs.corn SAMPLE DETECTION SUMMARY Client ID: MW-1 Lab ID: CA15466-01 Anala Results Flan MDL Q Units Method Notes Chemical Oxygen Demand 25 10 10 mg/L SM 5220D-1997 Chloride 200 8.7 20 mg/L EPA 300.0 Nitrate as N 0.53 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrate as N 0.53 0.041 0.10 mg/L EPA 353.2 Phosphorus 0.045 3 0.025 0.10 mg/L EPA 365.4 Total Dissolved Solids 330 50 50 mg/L SM 2540C-1997 Total Organic Carbon 5.4 0.34 1.0 mg/L SM 5310E-2000 Client ID: MW-2 Lab ID: CA15466-02 Anala Results Flan MDL 4 Units Method Notes Ammonia as N 0.36 0.045 0.10 mg/L EPA 350.1 Chloride 83 2.2 5.0 mg/L EPA 300.0 Nitrate as N 0.27 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as 0.27 0.041 0.10 mg/L EPA 353.2 Sulfate as SO4 9.7 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 150 50 50 mg/L SM 254OC-1997 Total Organic Carbon 3.8 0.34 1.0 mg/L SM 5310B-2000 Client ID: MW-3 Lab ID: CA15466-03 Anal Results Flag MDL POL Units Method Notes Ammonia as N 0.072 3 0.645 0.10 mg/L EPA 350.1 Chemical Oxygen Demand 29 10 10 mg/L SM 5220D-1997 Nitrate as N 0.049 3 0.025 0.10 mg/L EPA353.2 Nitrate/Nitrite as N 0.049 3 0.041 0.10 mg/L EPA 353.2 Phosphorus 0.33 0.025 0.10 mg/L EPA365.4 Sulfate as SO4 57 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 400 50 50 mg/L SM 2540C-1997 Total Organic Carbon 2.1 t 0.34 1.0 mg/L SM 5310B-2000 Client ID: MW-3 Lab ID: CA15466-031tE3 AnaTyte Results Flag MDL POL Units Method Notes Chloride 140 D 4.4 10 mg/L EPA 300.0 Client ID: MW-4 Lab ID: CA15466-04 Anaa Results Flag MDL POL Units Method Notes Chloride 26 2.2 5.0 mg/L EPA 300.0 Nitrate as N 9.2 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 9.2 0.41 1.0 mg/L EPA 353.2 Sulfate as SO4 3.6 3 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 100 50 50 mg/L SM 2540C-1997 Total Organic Carbon 0.92 3 0.34 1.0 mg/L SM 5310E-2000 Client ID: R-3 Lab ID: CA15466-05 Analyte Results Flan MDL POL Units Method Notes Ammonia as N 0.045 3 0.045 0.10 mg/L EPA 350.1 Nitrate as N 1.1 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 1.1 D 0.20 0.50 mg/L EPA 353.2 Sulfate as SO4 54 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 250 50 50 mg/L SM 2540C-1997 Total Organic Carbon 1.8 0.34 1.0 mg/L SM 5310E-2000 Client ID: R-3 Lab ID: CA15466-OSREI Anala Results Flag MDL 4 Units Method Notes Chloride 120 D 4.4 10 mg/L EPA300.0 FINAL This report relates only to the sample as received by the labomtory, and may only be reproduced in full. Page 6 Of 39 Cam 06co w .encolabs.com SAMPLE DETECTION SUMMARY Client ID: R-1 _ Lab ID: CA17316-01 Anal e - Results Flan MDL 4 Units- MethodNotes Ammonia as N 0.076 3 0.045 0.10 mg/L EPA 350.1 Chemical Oxygen Demand 68 10 10 mg/L SM 5220D-1997 Chloride ' 56 2.2 5.0 mg/L EPA 300.0 Nitrite as N 0.13 - 0.0080 0.10 mg/L EPA 300.0 Sulfate as SO4 17 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 94 50 50 mg/L SM 2540C-1997 Total Organic Carbon 7.5 0.34 1.0 mg/L SM 531OB-2000 QM-07 Client ID: R-1 Lab ID: CA17316-OIRE1 Anale - -. Results Flao MDL PQU Units Method Notes Phosphorus 3.3 D ' 0.050 - 0.20 mg/L. EPA 365.4` Client ID: R-2a 'Lab ID: CA17316-02 Analyte .. -Results Flan MDL EQL Units Method Notes Chloride 39 2.2 5.0 mg/L EPA 300.0 Nitrite as N 0.10 0.0080 0.10 mg/L EPA 300.0 Phosphorus 0.026 3 0.025 0.10 mg/L EPA 365.4 Sulfate as SO4 13 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 50 50 50 mg/L SM 2540C-1997:. - TotalOrganicCarbon 0.55 3 0.34 1.0 mg/L SM 5310E-2000 Client ID: R-4 Lab I0: CA17316-03 Analybe Results FlaFlao IADI, 4, Units Method Notes Chloride 66 2.2 5.0 mg/L EPA 300.0 Nitrite as N 0.16 ,0.0080 0.10 mg/L EPA 300.0 Phosphorus 1.4 .0.025 0.10 mg/L EPA 365.4 Sulfate as SO4 16 2.9' 5.0 - mg/L EPA 300.0 = Total'. Dissolved Solids .130 50 50 mg/L SM 2540C-1997 Total Organic Carbon 1.5 0.34 1.0 mg/L SM 5310E-2000 Client ID: R-Sa Lab ID: CA17316-04 nal - - Results Flea MDI, COL Units erred Notes Chemical Oxygen Demand 17 10 10 mg/L 'SM 522OD-1997 Chloride S6 2.2 5.0 mg/L EPA 300.0 Nitrate as N 2.4 0.20 0.50 mg/L EPA 300.0 Nitrate/Nitrite as N 2.5 0.20 0.50 mg/L CALC 300.0 Nitrite as N 0.14 0.0080 0.10 mg/L EPA 300.0. Phosphorus 0.10 0.025 0.10 mg/L EPA 365.4 Sulfate as SO4 24 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 150 50 50 mg/L SM 2540C-1997 Total Organic Carbon 1.7 0.34 1.0 mg/L SM 5310E-2000 Client ID: R-6 Lab ID: CA17349-01 Analyte Results Flan MDI, 3 Units Method Notes Ammonia as N 6.1 D 0.22 0.50 mg/L EPA 350.1 Chemical Oxygen Demand 12 10 10 mg/L SM 5220D-1997 Nitrate as N 0.16 0.025 0.10. mg/L EPA 353.2 Nitrate/Nitrite as N 0.16 0.041 0.10 mg/L EPA 353.2 Phosphorus 0.074 7 0.025 0.10 mg/L EPA365.4 Sulfate as 504 29 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 220 50 5o mg/L SM 2540C-1997 Total Organic Carbon 4.6 0.34 1.0 mg/L SM 53108-2000 Client ID: R-6 Lab ID: CA37349-01RE3 Analyte Results , Iraq MDL - 12 - -Units ' Method Notes Chloride 120 D 4.4 SO mg/L EPA 300.0 RNAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page 7 Of 39 ENc w .encolabs.com SAMPLE DETECTION SUMMARY Anale - Results Flau MDL Q Units Method Notes Ammonia as N 0.061 I 0.045 0.10 mg/L EPA 350.1 Chemical Oxygen Demand 17 10 10 mg/L SM 5220D-1997 Nitrate asN 0.28 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.28 0.041 0.10 mg/L EPA 353.2 Phosphorus 0.15 0.025 0.10 mg/L EPA 365.4 Sulfate as SO4 13 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 180 50 50 mg/L SM 254OC-1997 Total Organic Carbon 4.2 0.34 1.0 mg/L SM 53103-2000 Client ID: R-7 Lab ID: CA17349-02RE1 Armlyte Results Flan - MDL Pg5 Units Method Notes Chloride 110 D 4.4 10 mg/L EPA300.0 Client ID: R-8 Lab ID: CA17349-03 Analyte Results Flaa MDL PPOL- Units Method Notes Ammonia as N 0.15 0.045 0.10 mg/L EPA 350.1 Chemical Oxygen Demand 10 10 10 mg/L SM 522OD-1997 Chloride 9.6 2.2 5.0 mg/L EPA 300.0 Nitrate as N 17 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 17 D 0.82 2.0 mgJL EPA353.2 Phosphorus 0.089 1 0.025 0.10 mg/L EPA365.4 Sulfate as SO4 20 2.9 5.0 mg/L EPA 300.0 Total Dissolved Scrids 120 50 50 mg/L SM 2540C-1997 Total Organic Carbon 1.0 0.34 1.0 mg/L SM 5330B-2000 Client ID: R-9 Lab ID: CA17349-04 Anala Results Flaa MOIL S Units Method Notes Chemical Oxygen Demand 12 10 10 mg/L SM 5220D-1997 Chlorlde 59 2.2 5.0 mg/L EPA 300.0 Nitrate as N 0.79 0.025 0.10 mg/L EPA 353.2 Nitrate/Nitrite as N 0.79 0.041 0.10 mg/L EPA 353.2 Phosphorus 0.031 1 0.025 0.10 mg/L EPA 365.4 Sulfate as 504 66 2.9 5.0 mg/L EPA 300.0 Total Dissolved Solids 180 50 50 mg/L SM 25QC-1997 Total Organic Carbon 5.2 0.34 1.0 mg/L SM 5310E-2000 FINAL This report relates only to the sample as received by the laboratory, and may onN be reproduced in full. I Page 8 OT 39 ANALYTICAL RESULTS Description: MW-1 Lab Sample ID:CA15466-01 Matrix: Ground Water Sampled: 1111011710:20 Project: Sager Foods-MWs Sampled By: RANDALL JARRELL Classical Chemistry Parameters lvvrw.encolabs.com Received: 11/10/17 14:45 Work Order: CA15466 Analyte ICAS Numberl Results Flao Units DF MDL Q Batch Method Analyzed By Notes Ammonia as N [766441-7]A < 0.045 mg/L 1 0.045 0.10 71<17016 EPA 350.1 11/17/17 12:10 JU Chemical Oxygen DemandA 25 mg/L 1 10 10 7K34031 SM 5220D-1997 11/14/17 19:45 30C Chloride[16887-00-6]A 200 mg/L 4 8.7 20 7K20051 EPA 300.0 11/2011718:31 MKS Nitrate as N [14797-55-8]A 0.53 mg/L 1 0.025 0.10 7K20025 EPA 353.2 11/20/17 12:09 JU Nitrate/Nitrite as NA 0.53 mg/L 1 0.041 mo 71<18014 EPA 353.2 11/18/1715:19 JU Nitrite as N [14797-65-0]A < 0.017 mg/L 1 0.017 0.10 7K10005 EPA 353.2 11/10/17 17:15 JU Phosphams[7723-14-0]A 0.045 J mg/L 1 0.025 0.10 7K17011 EPA 365.4 11/2011711:50 JU Sulfate as 504 [14808-79-e]A < 2.9 mg/L 1 2.9 5.0 71<20051 EPA 300.0 1120/1718:46 MKS Total Dissolved SolidsA 330 mg/L 1 50 50 7K13009 SM 2540C-1997 11/13/1716:25 OMR Microbiological Parameters Analyte ICAS Numberl Coliform, FecalA Chemistry Parameters A-ENmonanaao NWeoa&WJNL 9�a7 Analyte rCAS Numberl Total Organic CarbanA Description: MW-2 Matrix: Ground Water Project: Sager Foods-MWs Classical Chemistry Parameters Analyte ICAS Numberl Ammonia as N [7664-41-7]A Chemical Oxygen Demand' Chloride [16887-00-6]A Nitrate as N [14797-55-B]A Nitrate/Nitrite as NA Nitrite as N [14797-65-0]A Phosphorus [7723-14-0]A Sulfate as SO4 [34808-79-8]A Total Dissolved Solids - Parameters Analyte ICAS Numberl Coliform, Fecal - Results Flaq Units DF POL Batch Method Analwed AM Notes < 1.0 MPN/100 1 1.0 7K13015 Cuffed 18 11/11/17 11:00 RAY mL Results Hari units DF MDL ]Q Batch Method Analwed By Notes 5.4 mg/L 1 0.34 1.0 . 7KI4014 SM 531OB-2000 11/14/17 12:57 SIR Lab Sample ID: CA15466-02 Received: 11/10/17 14:45 Sampled: 11/10/17 09:45 Work Order: CA15466 Sampled By: RANDALL JARRELL Results Flaa units 0.30 mg/L < 10 mg/L 83 mg/L 0.27 mg/L 0.27 mg/L < 0.017 mg/L < 0.025 mg/L 9.7 mg/L ISO mg/L Chemistry Parameters Analyte ICAS Numberl Total Organic CarbanA Results Flan Units < 1.0 MPN/100 not. OF MDL PQL Batch Method Analyzed By Notes 1 0.045 0.10 7K17016 EPA 350.1 11/17/1712:13 ILI 1 30 10 7K14031 SM 5220D-1997 11/14/17 19:45 JOC 1 2.2 5.0 7K20051 EPA 300.0 1120/1719:00 MKS 1 0.025 0.10 7K20025 EPA 353.2 11/20/17 12:09 JU 1 0.041 0.10 7K18014 EPA 353.2 11/18/1715:21 JU 1 0.017 0.10 7K10005 EPA 3S3.2 11/10/1717:16 ILI 1 0.025 0.10 7K17011 EPA 365.4 11/20/17 11:51 JU 1 2.9 5.0 7K20051 EPA 300.0 11/2011719:00 MKS 1 50 50 7K13009 SM 2540C-1997 11/13/17 16:25 OMR DF PPOL- Batch Method Analyzed ey Notes 1 1.0 7K13015 Colilert 18 11/11/1711:00 RAY Results Flaa Units DF MDL ]2 Batch Method Analyzed Bye Notes 3.8 mg/L 1 0.34 1.0 7K14014 SM 5310B-2aoo 11/14/17 12:57 SIR FINAL This report relates Dory to the sample as received "a laboratory, and may my be reproduced In full. Page 9 Of 39 �co y .encolabs.com ANALYTICAL RESULTS Description: MW-3 Lab Sample ID:CA15466-03 Received: 11/10/1714:45 Matrix: Ground Water Sampled: 11110/1711:45 Work Order: CA15466 Project: Sager Foods -MWs Sampled By: RANDALL JARRELL Classical Chemistry Parameters ^ -ENm �ry reralr�anaq Analyte rCAS Numberl Ammonia as N [7664-41-7]A Chemical Oxygen Demand^ Chloride 116887-00-6]A Nitrate as N [14797-55-8]A Nitrate/Nitrite as NA Nitrite as N [14797-65-0]A Phosphorus[7723-14-0]A Sulfate as SO4 [14808-79-8]A Total Dissolved SolidsA ^ -ENCO caryoenni Archie fCAS Numberl Coliform, Fecal - Parameters Parameters ^-ENCOO//dM003'bllEO dlldlyfC (!JC 9[9J Analyte fCAS Numberl Total Organic CarbonA Description: MW-4 Matrix: Ground Water Project: Sager Foods-MWs Classical Chemistry Parameters Analvte FCAS Numberl Ammonia as N [7664-01-7]1 Chemical Oxygen DemandA Chloride[16887-00-6]A Nitrate as N [14797-55-8]A Nitrate/Nitrite as NA Nitrite as N [14797-65-0]A Phosphorus [7723-14-0]A Sulfate as SO4 [34808-79-8]^ Total Dissolved Solids - Parameters Results Flan Units 0.072 J mg/L 29 mg/L 140 D mg/L 0.049 1 mg/L 0.049 1 mg/L < 0.017 mg/L 0.33 mg/L 57 mg/L 400 mg/L DF MDL. 2 Batch Method Analyzed By Notes 1 0.045 0.10 7K17016 EPA 350.1 11/17/17 12:15 JU 1 10 10 7K14031 SM 522OD-1997 11/14/17 19:45 JOE 2 4.4 10 7K20051 EPA 300.0 11/20/1719:14 MKS 1 0.025 0.10 7K20025 EPA 353.2 11/20/17 12:09 JU 1 0.041 0.10 7KI8010 EPA 353.2 11/18/1713:54 ILI 1 0.017 0.10 71<10005 EPA 353.2 11/10/1717:17 JU 1 0:025 0.10 7K17011 EPA 365.4 11/20/1711:53 ILI 1 2.9 5.0 7K20051 EPA 300.0 1112011719:29 MKS 1 50 50 7K13009 SM 254OC-1997 11/13/17 16:25 OMR Results Flaa Units DF POL Batch Method Analyzed _By Notes < 1.0 MPN/100 1 1.0 7KI3015 Calilert l8 11/11/17 11:00 RAY mL Results Fine Units DF MIL PQL Batch Method Analwed By Notes 2.1 mg/L 1 0.34 1.0 7KI4014 SM 531OB-2000 11/14/17 12:57 SIR Lab Sample ID:CA15466-04 Received: 11/10/17 14:45 Sampled: 11/10/17 11:00 Work Order: CA15466 ' Sampled By: RANDALL JARRELL Results Find Units < 0.045 mg/L < 10 mg/L 26 mg/L 9.2 mg/L 9.2 mg/L <0.017 mg/L < 0.025 mg/L 3.6 J mg/L 100 mg/L DF MDL Q Batch Method Analyzed 1 0.045 0.10 7K17016 EPA 350.1 11117/1712:16 1 10 10 7K14031 SM 5220D-1997 11/14/17 19:45 1 2.2 5.0 71<20051 EPA 300.0 11/20/1719:43 1 0.025 0.10 7K20025 EPA 353.2 11/20/17 12:09 10 0.41 1.0 7K38010 EPA 353.2 1111811713:59 1 0.017 0.10 7K10005 EPA 353.2 11/10/17 17:18 1 0.025 0.10 7K17011 EPA 365.4 11/20/17 11:54 1 2.9 5.0 7K20051 EPA 300.0 11/20/17 19:43 1 50 50 7K13009 SM 254OC-1997 11/13/17 16:25 11By Notes ILI JOC MKS Ju ILI Ju JU MKS OMR Analyte rCAS Numberl Results Flan Units DF POLL Batch Method Analyzed By Notes Coliform, Fecal, <1.0 MPN/300 1 1.0 71<13015 Colilert 18 11/11/1711:00 RAY mL Classical Chemistry Parameters ^ - ENCO 0r ndo rerOficda 1?te/NC 4241 Analyte rCAS Numberl Results Flan Units DP MDL Pyh Batch Method Analyzed gy Notes Total Organic CarbonA 0.92 J mg/L 1 0.34 1.0 7K14014 SM 531OB-2000 11/14/1712:57 SIR FINAL Thts report relates only to the sample a rerelved by the labomicry, and may only be reproduced in full. Page 'I O Of 39 Description: R-3 Matrix: Ground Water Project: Sager Foods-MWs Classical Chemistry Parameters Analyte, rCAS Numberl Ammonia as N 17664-41-7]A Chemical Oxygen DemandA Chloride[16887-00-6]A Nitrate as N [14797-55-8]A Nitrate/Nitrite as NA Nitrite as N [34797-65-6]A Phosphorus [7723-14-0]- Sulfate as SO4 [14808-79-8]A Total Dissolved Solids - Parameters ANALYTICAL RESULTS Results Flag Units 0.045 J mg/L < 30 mg/L 120 D mg/L 1.1 mg/L 1.1 D mg/L <0.017 mg/L < 0.025 mg/L 54 mg/L 250 mg/L Lab Sample ID: CA15466-05 Sampled: 11/10/17 12:45 Sampled By: RANDALL JARRELL W .encolabs.com Received: 11/10/17 14:45 Work Order: CA15466 DF MDL 4 Batch Method Analyzed By Notes 1 0.045 0.10 7K17016 EPA 350.1 1111711712:22 JU 1 10 30 7K14031 SM 5220D-1997 11/14/1719:45 30C 2 4.4 10 71<20051 EPA 300.0 11/21/1709:49 MKS 1 0.025 0.10 7K20025 EPA 353.2 1120/1712:09 JU 5 0.20 0.50 7K38030 EPA 353.2 11118/1714:03 JLJ 1 0.017 0.10 7K30005 EPA 353.2 11/10/1717:19 ILI 1 0.025 0.10 7K17011 EPA 365.4 11/20/1711:55 ILI 1 2.9 5.0 71<20051 EPA 300.0 1120/1719:57 MKS 1 50 50 7K13009 SM 254OC-1997 1111311716:25 OMR A-EACO Celyovtre .Mlyfe[NC 59JJ r Analyte rCAS Numberl Results FFI� Units DF PPOL Batch Method Analwed By Notes Coliform, FeolA < 1.0 MPN/100 1 1.0 71(13015 Colilert 18 11/11/17 11:00 RAY mL Chemistry Parameters Analyte rCAS Numberl Results Flag Units OF MDL PQL Batch- Method Analyzed By Notes Total Organic CarbonA 1.8 mg/L 1 0.34 1.0 7K14014 SM 5310B-2000 11/14/1712:57 SIR Description: R-1 Lab Sample ID: CA17316-01 Received: 11/14/1713:25 Matrix: Ground Water Sampled: 11/14/17 09:30 Work Order. CA17316 Project: Sager Foods-MWs Sampled By: RANDALL JARRELL Classical Chemistry Parameters - 6yCO (drya=rtlTirAanaryte [NC S9IJ Analyte 'CAS Numberl Results Flan units Units DF MS POL Batch Method Analwed Ay Notes Ammonia as N [7664-41-7]A O.076 J mg/L 1 0.045 0.10 7K17016 EPA 350.1 11/17/17 12:42 ILI Chemical Oxygen DemandA 68 mg/L 1 10 10 7K17015 SM 5220D-1997 11/17/1716:10 JOC Chloride[16887-00-6]A 56 mg/L 1 2.2 5.0 71(15019 EPA 300.0 11/14/17 19:38 MKS Nitrate as N [14797-55-8]A < 0.20 mg/L 1 0.20 0.50 7K15019 EPA 300.0 11/14/17 19:38 MKS Nitrate/Nitrite as NA <0.20 mg/L 1 0.20 0.50 M1023 CALC 300.0 11/21/1711:52 MKS Nitrite as N [34797-65-0]A 0.13 mg/L 1 0.0080 0.10 7KIS019 EPA 300.0 11/14/17 19:38 MKS Phosphorus 17723-14-0IA 3.3 D mg/L 2 0.050 0.20 7K30008 EPA 365.4 12/01/1709:58 ILI Sulfate as 504 [14808-79-8]A 17 mg/L 1 2.9 5.0 7K15019 EPA 300.0 11/14/17 19:38 MKS Total Dissolved SolidsA 94 mg/L 1 50 50 7K20010 SM 254OC-1997 1120/1718:15 OMR Microbiological Parameters Analyte rCAS Numberl Results Flag Units OF PQL Batch Method Analyzed By Notes Coliform, Fecal- < 1.0 MPNI100 1 1.0 7K20017 Colilert 18 11/15/17 10:00 ASC mL Classical Chemistry Parameters A-ENCO Odando ¢ trH danaly[eINC 4241 , Analvte MAS Numberl Results Fiao Units OF MDL POL Batch Method Analyzed By Notes Total Organic CarbonA 7.5 mg/L 1 0.34 1.0 7KI6013 SM 531013-2000 11/21/1712:45 SIR QM-07 FINAL This report relates only m the sample as received 6y the laboratory, and may only be reproduced in tall. I Page 11 OF 39 ANALYTICAL RESULTS Description: R-2a Lab Sample ID:CA17316-02 Matrix: Ground Water Sampled: 11/14/1710:15 Project: Sager Foods -MWs; Sampled By: RANDALL JARRELL Classical Chemistry Parameters u .encolabs.com Received: 11/14/17 13:25 Work Order: CA17316 Analyte FCAS Numberl Results Fiao Units DF MDL ]Q Batch Method Analyzed AM Notes Ammonla as N [766441-71A < 0.045 mg/L 1 0.045 0.10 7KI7016 EPA 350.1 11/17/17 12:44 JU Chemical Oxygen DemandA < 10 mg/L 1 10 10 7KI7015 SM'5220D-1997 11/17/1716:10 JOC Chloride [16887-00-6]A 39 mg/L 1 2.2 5.0 7K15019 EPA 300.0 11/14/17 19:53 MKS Nitrate as N [34797-55-B]A < 0.20 mg/L 1 0.20 0.50 7KIS019 EPA 300.0 11/14/17 19:53 MKS Nitrate/Nitrite as NA < 0.20 mg/L 1 0.20 0.50 7K21023 CALC 300.0 1121/17 11:52 MKS Nitrite as N [14797-65.0]A 0.10 mg/L 1 0.0080 0.10 7K15019 EPA 300.0 11/14/17 19:53 MKS Phosphorus[7723-14-O]A 0.026 J mg/L 1 0.025 0.10 7K30008 EPA 365.4 12/61/1709:12 JLl Sulfate as SO4 [14808-79-B]A 13 mg/L 1 2.9 5.0 7K15019 EPA 300.0 11/14/17 19:53 MKS Total Dissolved Solid5A 50 mg/L 1 50 50 71<20010 SM 2540C-1997 11/20/1718:15 OMR Microbiological Parameters A -ENCO Carycer fiedanoW[IlC 591] Analyte rCAS Numberl Colifonn, FecalA Chemistry Parameters Analyte rCAS Number Total Organic CarbonA Description: R4 Matrix: Ground Water Project: Sager Foods -MWs Classical Chemistry Parameters A-Eivcv Caryre zwanay Analyte rCAS Numberl Ammonia as N 1766441-7]A Chemical Oxygen DemandA Chloride 116887-00-61A Nitrate as N [14797-55-8]A Nitmte/Nitdte as NA Nitrite as N [34797-65-0]A Phosphorus[7723-14-03A Sulfate as SO4 [14808-79-8]A Total Dissolved Solids - Parameters Analyte rCAS Numberl Coliform, FealA Results Flan Units DF PPOL ,Batch Method Analwed By Notes <1.0 MPN/100 1 .1.0 7K20017 Colilert l8 11/1511710:00 ASC mL Results FLaq Units DF MDI PQL Batch Method Analyzed By Notes 0.55 J mg/L 1 0.34 1.0 7K16013 SM 53108-2000 11121/1712:45 SIR Lab Sample ID:CA17316-03 Received: 11/14/17 13:25 Sampled: 1111411711:00 Work Order: CA17316 Sampled By: RANDALL JARRELL Results Flap Units <0.045 mg/L < 30 mg/L 66 mg/L <0.20 mg/L <0.20 mg/L 0.16 mg/L 1.4 mg/L 16 mg/L 130 mg/L DF MOIL PQL Batch Method Analyzed Ay Notes 1 0.045 0.10 7KI7016 EPA 350.1 11/17/1712:46 JU 1 10 10 7KI7015 SM 5220D-1997 11/17/17 16:10 JOC 1 2.2 5.0 7K15019 EPA 300.0 11/14/17 20:07 MKS 1 0.20 0.50 7KIS019 EPA 300.0 11/14/17 20:07 MKS 1 0.20 0.50 7K21023 CALC 300.0 1121/17 11:52 MKS 1 0.0080 0.10 7K15019 EPA 300.0 11/14/17 20:07 MKS 1 0.025 0.10 7K30008 EPA 365.4 12/01/1709:13 JU 1 2.9 5.0 71(15019 EPA 300.0 11114/1720:07 MKS 1 50 So 7K20030 SM 254OC-1997 1120/17 18:15 OMR Results Flag Units DF PQL Batch Method Analyzed By Notes < 1.0 MPN/100 1 1.0 7K20017 Colilert 18 11/15/17 10:00 ASC mL (Classical Chemistry Parameters A- FNCO Orlando oaaredanal/!a (NC 4241 Analyte rCAS Numberl Results Flan Units DE MCI, PDL Batch Method Analyzed Ay Notes Total Organic CarbonA 1.5 mg/L 1 0.34 1.0 7KI6013 SM 531OB-2000 1121/1712:45 51R FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced In full. Page Z Of 39 Description: R-5a Matrix: Ground Water Project: Sager Foods-MWs Classical Chemistry Parameters ^ - ENCOGry'c,rafiedaWly[NC 591] Analyte, rCASNumberl Ammonia as N [76=-7]A Chemical Oxygen DemandA Chloride[16887-00-6]A Nitrate as N [14797-55-e]A Nitrate/Nitrite as NA Nitrite as N [14797-65-0]A Phosphorus[7723-14-0]A Sulfate as SO4 [34808-79-81A Total Dissolved Solids - Parameters Analyte rCAS Numbed Coliform, FecalA Chemistry Parameters ANALYTICAL RESULTS Lab Sample ID:CA37316-04 Sampled: 11/14/17 11:45 Sampled By: RANDALL JARRELL Results Flan Units < 0.045 mg/L 17 mg/L 56 mg/L 2.4 mg/L 2.5 mg/L 0.14 mg/L 0.10 mg/L 24 mg/L ISO mg/L wwW.encolabs.com Received: 11/14/17 13:25, Work Order: CA17316 DF MDL POL Batch Method Analyzed By Notes 1 0.045 0.10 7K17016 EPA 350.1 11/17/17 12:47 JLl 1 30 10 7K17015 SM MOD-1997 11/17/17 16:10 JOC 1 2.2 5.0 7K15019 EPA 300.0 11/1411720:21 MKS 1 0.20 0.50 7K15019 EPA 300.0 11/14/17 20:21 MKS 1 0.20 0.50 7K21023 CALC 300.0 11/21/17 11:52 MKS 1 0.0080 0.10 7KIS019 EPA 300.0 11/14/1720:21 MKS 1 0.025 0.10 7K30008 EPA 365.4 12/01/1709:14 ILI 1 2.9 5.0 7K15019 EPA 300.0 11/14/1720:21 MKS 1 501 50 7KZ0009 SM 254OC-1997 1120/17 15:40 OMR Results Flaa Units 11_F 4 Batch Method Analwed By Notes < 1.0 MPN/100 1 1.0 7K20017 Colilert 18 11115/1710:00 ASC mL ^-ENro OdaMo o+ionroanaryre[rvc aZa] Analyte rCASNumberl Results Flan Units DF MDL POL Batch Method AnaNzed By Notes Total Organic CarbonA 1.7 mg/L 1 0.34 1.0 7K16013 SM 531OB-2000 1121/1712:45 SIR Description: R-6 Lab Sample ID:CA17349-01 Received: 11/15/1711:50 Matrix: Ground Water Sampled: 11/15/17 10:35 Work Order: CA17349 Project: Sager Foods-MWs Sampled By:RANDALL JARRELL Classical Chemistry Parameters Analyte TAS Numberl , Ammonia as N [7664-41-7]A Chemical Oxygen DemandA Chloride[16887-00-6]A Nitrate as N [14797-55-8]A Nitrate/Nitrite as NA Nitrite as N [14797-6541]A Phosphorus[7723-14-01A Sulfate as SO4 [14808-79-B]A Total Dissolved SOIrdsA Parameters Results Flaa Units 6.1 D mg/L 12 mg/L 120 D mg/L - 0.16 mg/L 0.16 mg/L < 0.017 mg/L 0.074 J mg/L 29 mg/L 220 mg/L BF MDL S Batch Method Analyzed 5 0.22 0.50 7K22009 EPA 350.1 1122117 11:24 1 10 30 7K17015 SM 5220D-1997 11/17/17 16:10 2 4.4 30 71Q2030 EPA 300.0 11/22/17 20:15 1 0.025 0.10 71CO030 EPA 353.2 1120/17 12:32 1 0.041 0.10 7K18015 EPA 353.2 11/18/17 16:35 1 0.017 0.10 7K16U46 EPA 353.2 11/16/17 20:19 1 0.025 0.10 7K300D8 EPA 365.4 12/01/1709:16 1 2.9 5.0 7K22030 EPA 300.0 11/22/17 20:58 1 50 50 71QI025 SM 2540C-1997 1121/1716:20 By Notes MKS JOC MKS ILI ILI MKS ILI MKS OMR Analyte [CAS Numberl Results Rao Units OF 4 Batch Method Analyzed By, Notes Coliform, Fecal^ < 1.0 MPN/S00 1 1.0 7K20022 CoMert 18 11/16/17 09:58 ASC mL Classical Chemistry Parameters ^ -WCO Odande namrad analyre (NC 4241 Analyte rCAS Numberl Results Flaa Units OF MDL POL Batch Method Analyzed Py Notes Total Organic CarbonA 4.6 mg/L 1 0.34 1.0 7K27019 SM 5310B-2000 112811711:46 SIR FINAL This report relates only 0 the sample as reo vived W the laboatory, and may Dory be reproduced In toil. I Page 13 Of 39 El�lCO wwW.encolabs.com ANALYTICAL RESULTS Description: R-7 Lab Sample ID: CA17349-02 Received: 11/15/17 11:50 Matrix: Ground Water Sampled: 11/15/17 09:45 Work Order: CA17349 Project: Sager Foods-MWs Sampled By: RANDALL JARRELL Classical Chemistry Parameters A-ENCO Grycemhm angry Analyte [CAS Numberl Ammonia as N [7664-41-7]A Chemical Oxygen OemandA Chloride[16887-00-6]A Nitrate as N [14797-55-8]A Nitrate/Nitrite as NA Nitrite as N [14797-65-0]A Phosphorus [7723-14-0]A Sulfate as SO4 [34808-79-8]A Total Dissolved SolidsA Parameters ^-ENcl7 Qry refit. Analyte rCAS Numberl Colifdrm, FecalA Chemistry Parameters ^-ENCOO norro Bred aneVe JNC 42#1 Analyte rCAS Numberl Total Organic Carbon^ Description: R-8 Matrix: Ground Water Project: Sager Foods-MWs Classical Chemistry Parameters Analyte rCAS Numberl Ammonia as N [7664-41-7]A Chemical Oxygen DemandA Chloride 116887-00-61A Nitrate as N [14797-55-5]A Nitrate/Nitrite as NA Nitrite as N [14797-65-0]A Phosphorus[7723.14-0]A Sulfate as SO4 [14808-79-B]A Total Dissolved Solids - Parameters Results Flan Units 0.061 ] mg/L 17 mg/L 110 D . mg/L 0.28 mg/L 0.28 mg/L < 0.017 mg/L 0.15 mg/L 13 mg/L 180 mg/L DF MDL 4 Batch Method Analyzed By Notes 1 0.045 0.10 7K22009 EPA 350.1 11/22/17 11:26 MKS 1 10 30 7K17015 SM MOD-1997 11117/1716:10 30C 2 4.4 10 7K22030 EPA 300.0 11/22/17 21:13 MKS 1 0.025 0.10 71CO030 EPA 353.2 11/20/17 12:32 ]L] 1 0.041 0.10 71(18015 EPA 353.2 11/18/1716:35 it] 1 0.017 0.10 71<36046 EPA 353.2 11/1611720:20 MKS 1 0.025 0.10 7K30008 EPA 365.4 12/01/17 09:17 JL1 1 2.9 5.0 7K22030 EPA 300.0 11/22/1721:27 MKS 1 50 50 7K21025 SM 254OC-1997 11/21/17 16:20 OMR Results Flan Units DF 3 Batch Method Analwed By Notes < 1.0 MPN/100 1 1.0 7K20022 Colllert 18 11/I6/17 09:58 ASC mL Results plant Units DF MOL PPOL. Batch Method Analyzed Ay Notes 4.2 moll- 1 0.34 1.0 71C7019 SM 531OB-2000 11/2811711:46 SIR Lab Sample ID: CA17349-03 Received: 11/15/17 11:50 Sampled: 11/15/17 08:50 Work Order: CA17349 Sampled By: RANDALL JARRELL Results Flaa Units 0.15 moll. 10 mg/L 9.6 mg/L 17 mg/L 17 D mg/L <0.017 mg[L 0.089 3 mg/L 20 mg/L 120 M91L DF MDL Q Batch Method Analyzed By Notes 1 0.045 - 0.10 7K22009 EPA 350.1 11122/1711:27 MKS 1 10 10 7K17015 SM 5220D-1997 11/17/17 16:10 30C 1 2.2 5.0 7WO30 EPA 300.0 11/22/17 21:41 MKS 1 0.025 0.10 7K20030 EPA 353.2 11/2011712:32 JL] 20 0.82 2.0 71(38015 EPA 353.2 11/18/17 16:36 JLl 1 0.017 0.10 7KI6046 EPA 353.2 11/16/1720:21 MKS 1 0.025 0.10 7K30008 EPA 365.4 12/01/17 09:18 JU 1 2.9 5.0 71<22030 EPA 300.0 11/22/17 21:41 MKS 1 50 50 7K21075 SM 254OC-1997 11/21/17 16:20 OMR ^-ENLD Gryo'.r8deddNlytelNG 59IJ Analyte rCAS Numbed Results Flao Units DF 4 Batch Method Analyzed epyr Notes Coliform, FeMIA <1.0 MPN/100 1 1.0 7120022 CoMert 18 11/1611709:58 ASC mL Classical Chemistry Parameters ^ -E W Orlando ce2hed anaryfe(NC 4241 Analyte [CAS Numberl Results Flap Units DF MDL 4 Batch Method Analyzed AM Notes Total Organic Carbon- 1.0 mg/L 1 0.34 1.0 7K27019 SM 531OB-2000 11128/1711:46 SIR FINAL This report relates only In the mmple as received by the laboratory, and may only be reproduced In full. Page '� 4 Oj 39 ANALYTICAL RESULTS Description: R-9 Lab Sample ID: CA17349-04 Matrix: Ground Water Project: Sager Foods-MWs Classical Chemistry Parameters ^ -ENCTJ mryt°ra5manaty Analyte rCAS Numberl Ammonla as N [766441-7]^ Chemical Oxygen Demand^ Chloride [16887-00-67A Nitrate as N [14797-SS-8]^ Nitrate/Nitrite as NA Nitrite as N [14797-65-O]^ Phosphorus [7723-14-0]A Sulfate as SO4 [34808-79-8]A Total Dissolved Solids^ Parameters Results Flaa Units < 0.045 mg/L 12 mg/L 59 mg/L 0.79 mg/L 0.79 mg/L < 0.017 mg/L 0.031 1 mg/L 66 mg/L ISO mg/L Sampled: 11/15/17 08:00 Sampled By: RANDALL ]ARRELL ENCO viww.encolabs.com Received:. 11/15/17 11:50 Work Order: CA17349 DF MDL ]Q Batch Method Analyzed By Notes 1 0.045 0.10 71<22009 EPA 350.1 11/22/1711:32 MKS 1 10 10 7K17015 SM MOD-1997 11/1711716:10 ]0C 1 2.2 5.0 71<22030 EPA 300.0 11/2211721:56 MKS 1 0.025 0.10 7K20030 EPA 353.2 11/20/1712iK ILI 1 0.041 0.10 7KI8015 EPA 353.2 11/18/1716:37 ILI 1 0.017 0.10 7K16046 EPA 353.2 11/16/17 20:22 MKS 1 0.025 0.10 7K30008 EPA 365.4 12/01/1709:20 ILI 1 2.9 5.0 71<22030 EPA 300.0 11/22/17 21:56 MKS 1 50 50 7K23025 SM 2540C-1997 11/21/17 16:20 OMR Analyte rCAS Numberl Results flan Units DF PQL Batch Method Analwed By Notes Colifia", Fecal^ <1.0 MPN/100 1 1.0 7K20022 Colilert 18 11/16/1709:58 ASC mL Classical Chemistry Parameters ^ -ENCO odando re fiedanaly[ fNC 4241 Analyte rCAS Numberl Results Flan ' Units BF MDL PQL Batch Method Analwed ]Y Notes Total Organic CarbonA ,5.2 mg/L 1 0.34 1.0 71(27019 SM 5310B-2000 11/2811711:46 SIR FINAL This report relates only to the sample as recieved by the laboratory, and may only be reproduced in full. Page 15 Of 39 FJVCO w .encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7K10005 - NO PREP Blank (7)(10005-BLKS) Prepared: 11/102017 08:05 Analyzed: 11/102017 08:05 Spike Source %REC RPD Analvte gestalt F)aR PD1 units Level Re,sult 0/bREC Limits RPD Limit Notes Nitrite as N 0.017 U 0.10 mg/L LCS (MCDOS-BSI) Prepared: 11/102017 08:10 Analyzed: 11/10/2017 08:10 Spike Source %REC RPD Ana Reim Ela9 E9L. Units Level Result O/ REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L Lod 103 90-110 LCS (7K10005-BS2) Prepared: 11/102017 08:29 Analyzed: 11/102017 08:29 ' Spike Source %REC RPD Analyt Result Eag E91 Units Level Result o/ REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 103 90-110 LCS (71(30005-1153) Prepared: 11/102017 08:39 Analyzed: 11/10/2017 08:39 Spike Source O/OREC RPD Analyt Resul Rag E91, Units Level Resu %REC Limits RPD Limit Notes Nitrite as N 1.0 0.10 mg/L 1.00 101 90-110 Matrix Spike (7K30005-MSl) Prepared:, 11/10/2017 08:34 Analyzed: 11/102017 08:34 Source: CA16688-01 Spike Source %REC RPD Anal vte Rg4RIL flag P91 Unita Level Resul o/•REC Limits RPD Limit Notes Nitrite as N 0.85 0.10 mg/L 1.00 0.10 74 90-110 QM-07 Matrix Spike (7K10005-MS2) Prepared: 11/1012017 08:36 Analyzed: 11/102017 08:36 Source:-CA16693-01 Spike Source OAREC RPD Analvte Resu E)ag E4L Units Level Result OAREC Limits RPD Limit Notes Nitrite as N 0.98 0.10 mg/L 1.00 0.017 U 98 90-110 Matrix Spike Dup (7K10005-MSD7) Prepared: 11/10/2017 08:35 Analyzed: 11/10/2017 08:35 ' Source: CA16688-01 Spike Source %REC RPD Analyze RQUlt flag E9L Um1L4 Level Result %REC Limits RPD Limit Notes Nitrite as N 0.85 0.10 mg/L 1.000.10 75 90-110 0.4 10 QM-07 Batch.M13009 -NO PREP Blank (7K13009-ELK1) Prepared & Analyzed: 11/13/201716:25 Spike Source %REC RPD Attalyt_e ge.5ult Elan PO Unitf Level Result O/OREC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L .. LCS (71(13009-BSI) Prepared &Analyzed: 11113/201716:25 Spike Source %REC RPD Analyze Result Eon EM Liam Level Resml o/.REC Limits RPD Lima Notes Total Dissolved Solids 950 50 mg/L 1000 95 90-130 Dupiiwte (7K33009-DUPS) Prepared &Analyzed: 11113/201716:25 Source: CA15465-01 Spike Source %REC RPD Ana Resu Flag POL Units Level Result O/blti Limits RPD Limit Notes FINAL This report relates Only to the sample asazreceived by the laboratory, and may only be reproduced In full. Page �6Of 39 �co vrPnv.encolalas.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7K13009 - NO PREP - Continued Duplicate (7)(33009-DUPi) Continued Prepared &Analyzed: 11/13/201716:25 - Source: CA15465-01 Spike Source %REC RPD Analvte Result Mq E9L Units Level Result °/ REC Limits RPD Limit 'Notes Total Dissolved Solids 600 50 mg/L 600 03 20 Duplicate (7K33009-DUP2) Prepared &Analyzed: 11/131201716:25 Source: CA15466-01 Spike Source %REC RPD Analv[e Result Elan POL units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 340 50 mg/L 330 4 20 Batch 7K14031 -Same Blank (7K34031-BLK3) Prepared: 11/141201717:10 Analyzed: 11/14/201719:45 Spike Source %REC RPD Anwhite Result Elan PQL Limits Level Result o/ REC Limits RPD Limit Notes Chemical Oxygen Demand 10 U 10 mg/L LCS (7K14031-BSI) Prepared: 11/141201717:10 Analyzed: 11/14201719:45 Spike Source %REC RPD Anal Result Man POL _UJIM Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand - Soo 10 mg/L Soo 100 90-110 Matrix Spike (7K14031-MS1) Prepared: 11/14/2017 17:10 Analyzed: 11/142017 19:45 Source: CA09070-01 Spike Source %REC RPD Anayyte Rg ml Elan P..QS Units, Level Result %REC Limits RPD Limit Notes Chemical Oxygen Demand 560 10 mg/L 526 42 99 90-110 Matrix Spike Dup(7K34031-MSDI) Prepared; 11/14201717:10 Analyzed: 11/14201719:45 ' Source: CA09070-01 Spike Source %REC RPD pir jyig Result Flay PO 11-rit4 Level Result / REC Limits RPO Limit Notes Chemical Oxygen Demand 580 SO mg/L 526 42 102 90-I10 2 10 Batch 7K15019 - NO PREP Blank (7K15019-BLK3) Prepared & Analyzed: 11/14/2017 18:27 Spike - Source o/aREC RPD Anal vte Result EWA EQL IUJIM Level Result o/ REC Limits RPD Limit Notes Chloride 2.2 U 5.0 mg/L Nitrate as N 0.20 U 0.50 mg/L Nitrite as N 0,0080 U 0.10 mg/L Sulfate as 504 2.9 • U 5.0 mg/L LCS (7K35019-1151) Prepared & Analyzed: 11/14/2017 17:29 Anaivte Chloride Nitrate as N Nitrite as N Sulfate as SO4 Spike Source o/aREC RPD Result Elan POL units Level Result /hREC Limits RPD Limit Notes 51 5.0 mg/L 50.0 102 90-110 4.9 0.50 mg/L 5.00 98 90-110 1.0 0.10 mg/L 1.00 103 90-110 52 5.0 mg/L 50.0 104 90-110 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 17 Of 39 CNCO tvLaw.encolalas.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7K16019 - NO PREP - Continued Matrix Spike (7KI5019-MSI) , Prepared & Analyzed: 11/14/2017 20:36 ' Source: CA16972-10 Spike Source %REC RPD Analvte Resu Flag PAL wilts Level Result -/REC Limits RPD 911111 Notes Chloride 18 p. 5.0 mg/L_ 20.0 0.63 89 90-110 QM-07 Nitrate as N 4.9 0.50 mg/L 5.00 0.11 96 90-110 Nitrite as 0.96 0.10 mg/L 1.00 0.0 96 90-110 Sulfate as 504 19 5.0 mg/L 20:0 0.46 93. 90-130 Matrix Spike (7K15019-MS2) Prepared & Analyzed: 11/142017 21:33 Source: CA16969-01 Spike Source °/aREC RPD Anaa Result Man POL units Level Result %REC Limits RPD Limit Notes Chlorlde 25 5.0 mg/L 20.0 5.6 97 90-110 Nitrate as N 7.4 0.50 mg/L 5.00 2.1 105 90-110 Nitrite as N 0.97 0.10 mg/L 1.00 0.038 93 90-110 Sulfate as SO4 19 5.0 mg/L • 20.0 0.55 91 90-110 _. Matrix Spike Dup (7K1S019-MSDI) Prepared & Analyzed: 11/14/2017 20:50 Source: CA16972-10 Spike Source %REC RPD Analvic Resultp3q F- UDLts Level Result o/hREC Limits RPD Limit Notes Chloride 19 5.0 mg/L 20.0 0.63 91 90-110 2 10 Nitrate as N 5.1 0.50 mg/L '5.00 0.11 99 90-110 3 10 Nitrate as N 0.97 0.10 mg/L 1.00 0.0 97 90-110 2 10 Sulfate as 504 19 5.0 mg/L 20.0 0.46 93 90-110 0.9 10 , Batch 7K16046 - NO PREP Blank (71(16046-13LKi) Prepared: 11/162017 19:55 Analyzed: 11/16201719:55 Spike Source 1.REC RPD Analyt Resul Faq P95 Units Level Result °/aREC Limits RPD Limi Notes Nitrite as N 0.017 U 0.10 mg/L LCS (7K16046-BSI) Prepared: 11/162017 20:08 Analyzed: 11/162017 20:08 Spike Source o/aREC RPD .An,Ivt Result Flag PQt units Level Result %REC Limits RPD L11111t Notes Nitrite as N 0.99 0.10 mg/L 1.00 99 90-110 Matrix Spike (7K16046-MS3) Prepared: 11/16/2017 19:57 Analyzed: 11/162017 19:57 , Source: CA15905-01 Spike Source °/aREC RPD Anaivte Resul FFLq P_4S Units Level Result o/ REC Limits RPD Limit Notes Nitrite as N 0.97 0.10 mg/L 1.00 0.017 U 97 90-110 Matrix Spike (7K36046-MS2) :Prepared: 11/162017 20:00 Analyzed: 11/162017 20:00 Source: CA16618-01 Spike Source %REC RPD Anal vte Result Flag P9L Units Level Result of REC Limits RPD Limit Notes Nitrite as N 0.92 0.10 mg/L 1.00 0.017 U 92 90-110 Matrix Spike Dup (7KI6046-MSDS) Source: CASS905-01 An e Nitrite as N Spike Source o/aREC RPD Result Ran PQt Units Level Result o%REC Limits ;RPD Limi 0.95 0.10 mg/L 1.00 0.017 U 95 90-110 2 10 Notes FINAL This report relates any to the sample as received by the laboratory, and may any he reproduced In full. Page' 18 Of 39 CS NCO v7ww.encolabs.corn QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7K16046 - NO PREP - Continued , Matrix Spike Dup (7K36046-MSD2) Prepared: 11/16/2017 20:01 Analyzed: 11/16/2017 20:01 Source: CA16618-01 - Spike , Source %REC RPD Analv[e -Result E149- ROL 4nit5 Level Result %REC Limits RPD Limit Notes Nitrite as N 0.97 0.10 mg/L 1.00 0.017 U 97 90-110 4 10 Batch 7K17011 - Same Blank (7K17011-13LK1) - Prepared: 11/17/2017 11:55 Analyzed: 1120201711:29 Spike Source °/aREC RPD Analvte Result F aq POL 1181155 Level Result °/PREC Limits RPD 'Limit Notes Phosphorus 0.025 U 0.10 mg/L LCS (7917011-BS1) Prepared: 11/17201711:55 Analyzed: 11/20/201711:30 Spike Source %REC RPD Analvte Result EL49 -EPL units Level Result OAREC Limits RPD Limit Notes Phosphoms 1.6 0.10 mg/L 1.60 102 80-120 ' Matrix Spike (7K170ll-MSl) Prepared: 11/172017 11:55 Analyzed: 11/202017 11:33 Source: CA15465-01 Spike Source °/aREC RPD Analvt Resul Ela9 ,PO6 - units Level. Result %REC Limits RPD Limit Notes Phosphorus 12 D 1.0 mg/L 0.640, 11 100 80-120 Matrix Spike Dup (7K17011-MSDS) Prepared: 11/17/2017 11:55 Analyzed: 11/20/2017 11:34 Source: CA15465-01 Spike Source °/aREC RPD 4 Anal vty ReSu Mao POS Units Level .Result °/aREC. Limits RPD Limit Notes Phosphorus 12 D 1.0 mg/L 0.640 1195 80-120 0.3 25 " Batch 7K17015-Same Blank (7K37015-BLK3) Prepared: 11/172017 11:37 Analyzed: 11/17/2017 16:10 Spike Source %REC RPD Anal vte esu Ela9 P_46 Units Level Result a/aREC Limits RPD -Limit Notes Chemical Oxygen Demand 30 U 10 mg/L LCS (7K37035-BSl) Prepared: 11/17/2017 11:37 Analyzed: 11117/201716:10 Spike . Source a/aREC RPD Analvte - Result Ela9 FQL Units Level Result %REC Limits RPD Limit Notes Chemical oxygen Demand 490 10 mg/L Soo 99 90-110 Matrix Spike (7K17015-MS1) Prepared: 11/17/2017 11:37 Analyzed: 11/17/2017 16:10 Source: CA09892-01 - Spike Source %REC RPD Analyt Regul ELq PQL units Level Result %REC Limits RPD. Limit Notes Chemical Oxygen Demand 630 10 mg/L 526 110 99 90-110 Matrix Spike Dup (7K17015-MSD11 Prepared: 11/172017 11:37 Analyzed: 11/17/2017 16: 10 - Source: CA09892-01 Analvte Chemical Oxygen Demand Batch 7K17016 - NO PREP Result Hall POIL O11ikt 650 10 mg/L Spike Source a/aREC RPD Level Result - %REC Limits RPD Limit 526 110 102 90-110 2 10 Notes HNAL Th6 report relates only to the sample as received by the laboratory, and may only he reproduced in full Page 19 Of 39 C.ENCO w .encolabsxom QUALITY CONTROL DATA , Classical Chemistry Parameters - Quality Control Batch 7K17015 - NO PREP - Continued Blank (7K17016-BLKS) Prepared: 11/171201712:01 Analyzed: 11/17/201712:01 Spike Source %REC RPD Analvte Result Elm EQL U13M Level Result %REC Limits RPD Limit Notes Ammonia as N 0.045 'U 0.10 mg/L LCS (7K17016-B51) Prepared: 11117/201712:03 Analyzed: 11/17/201712:03 Spike Source 0/oREC RPD Aualvte Result Elag per, Units Level ResuH /REC Limits RPD hiffift Notes Ammonia as N 1.0 0.10 mg/L 0.989 101 90-110 Matrix Spike (7K17016-MS3) Prepared: 11/17/2017 13:21 Analyzed: 11/17201713:21 Source: CA15465-GIRE1 ' Spike Source °/oREC RPD Anal vte ResUl Ma POL Units Level Result -/oREC Limits RPD Limit Notes Ammonia as N 4.7 0.50 mg/L 1.98 2.9 91 90-110 Matrix Spike (7K37016-MS2) Prepared: 11/17/2017 12:11 Analyzed: 11/172017 12:11 Source: CA3S466-01 .Spike Source 0/dREC RPD Analvte Res"I Elan P26 Units Level Result a/oREC Limits RPD Limit Notes Ammonia as N 0.33 0.10 mg/L 0.385 0.045 U 86 90-110 QM-07 Matrix Spike Dup (7K37016-MSD1) Prepared: 11/172017 13:23 Analyzed: 11/17/201713:23 Source: CA15465.01RE1 - - Spike Source %oREC RPD Analyt Result Elan HQL units Level Result a/oREC Limits RPD Limit Notes Ammonia as N 4.4 0.50 mg/L 1.98 2.9 77 90-110 6 10 QM-07 Batch 7K18010 - NO PREP Blank (7K38010-BLKS) Prepared: 11/182017 13:13 Analyzed: 11/18/2017 13:13 Spike Source %REC RPD nal - Resul Dan - E9S Units Level Result %REC Limits RPD Limit' Notes Nitrate/Nitrite as 0.041 U' 0.10 mg/L LCS (7K18010-BS3) Prepared: 11/18/2017 13:14 Analyzed: 11/18/2017 13:14 Spike Source 0/REC RPD Analvte Result ELan R" units Level Result a/oREC Limits RPD Limit Notes Nitrate/Nitrite as N 13 0.10 mg/L 1.25 102 90-110 r Matrix Spike (7K3801D-MS3) Prepared: 11/182017 13:56 Analyzed: 11/18/201713:56 'Source: CA15466.03 Spike Source %REC RPD AnaAnalyte ResulElect SQL .Units Level Result %REC Limits RPD MMA Notes Nitrate/Nitrite as N 0.54 0:10 mg/L 0.521 0.049 94 90-110 Matrix Spike (71(18010-M52) Prepared: 11/182017 14:01 Analyzed: 11/18/201714:01 Source: CA15466-04 Spike Source%REC RPD Anslvte Result Elan POL Unlu Level - Result %REC Limits RPD Limit Notes Nitrate/Nitrite as 14 1.0 mg/L 5.00 9.2 87 90-110 QM-07 Matrix Spike Dup (71(18010-MSDS) Prepared: 11/18/2017 13:57 Analyzed: 11/18/2017 13:57 Source: CAIS466-03 Spike Source 0%REC RPD Anaa Result Elan P—QL Units Level Result %REC Limits RPD Limit Notes FINAL This report relates only to the sample as received by the labomtory, and may only be reproduced In full. PagE: 20 Of 39 Witco www.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch7KIS010 - NO PREP - Continued Matrix Spike Dup (71(38010-MSD3) Continued Prepared: 11/182017 13:57 Analyzed: 11/18201713:57 - Source: CA15466.03 " ' Spike Source o/aREC RPD Analvte Result FJ34 D" Units Level Result oREC . Limits RPD Limit Notes Nitrate/Nitrite as N 0.59 0.10 mg/L - 0.521 0.049 104 90-110 9 10 Batch 7KIS014 - NO PREP , Blank (7)(18014-e1K1) Prepared: 11/18/2017 13:15 Analyzed: 11/182017 13:15 Spike Source %REC RPD Anal Rewu F19 P9L Un"ts Level Resu t o/aREC Limits RPD Limit Notes Nitrate/Nitrite as 0.041 U 0.10 mg/L - LCS (71(18014-0S1) Prepared: 11/18/201713:16 Analyzed: 11118/201713:16 Spike Source 0/oREC RPD Analyse Result Hag 1191 Umi is Level Result %REC Limits RPD Limit Notes Nitrate/Nitnte as N 13 0.10 mg/L 1.25 101 90-110 Matrix Spike (7K18014-MS3) Prepared: 111181201715:12 Analyzed: 11/182017 15:12 Source: CAL4942-02 Spike Source ^/oREC RPD Analute Result 119 ML Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as 32 2.0 mg/L 10.0 22 103 90-110' Matrix Spike (7K18014-MS2) Prepared: 11/182017 15:17 Analyzed: 11/18/2017 15:17 Source: CA15465-01 ' " Spike Source % REC RPD Analyt, Result L7d9 P4), Units Level Result %REC . Limits RPD Limit Notes Nitrate/Nitrite as 0.051 3 010 1119/1- 0.521 0.055 NR 90-110 QM-07 Matrix Spike Dup (7K38014-MSD3) Prepared: 11/18/2017 15:14 Analyzed: 11/182017 15:14 Source: CA14942-02 - Spike Source %REC RPD Analvte - Resin ELag POL UJ1L Level Result / REC Limits RPD Limit Notes Nitrate/Nitrite as N 33 2.0 mg/L 10.0 22 115 90-110 4 10 QM-07 Batch 7KIS015 - NO PREP Blank (71(38015-131-KI) Prepared: 11/18/2017 15:06 Analyzed: 11/18/2017 15:06 ' Spike Source %REC RPD Analvte Result Ela P01 Units Level Result o/ REC Limits RPD Limit Notes Nitrate/Nitrite as N 0.041 U 0.10 mg/L LCS (7)(18015-11M) Prepared: 11/182017 15:04 Analyzed: 11/18201715:04 Spike Source %REC RPD Ana1vt Resul E)ag E91. Ur RS Level Result o/ REC Limits RPD Limit Notes Nitrate/Nitrite as 1.3 0.10 ri 1.25 102 90-110 Matrix Spike (7K38015-MSS) Prepared: 11/182017 16:00 Analyzed: 11/18/2017 16:00 Source; CA25475-01 Spike Source %REC RPD Analyte Result 099 RSLI Units Level Result / REC Limits RPD Limit Notes Nitrate/Nitrite as.N 51 E 2.0 mg/L 10.0 41 100 90-110 QM-07 FINAL This report relates only to the sample as recalled by the laboratory, and may only be reproduced in full. Page 21 Of 39 www.encolahs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7KIBO15 - NO PREP - Continued Matrix Spike (7K18015-MS2) Prepared: 11/18/2017 16:09 Analyzed: 11/18/2017 16:09 Source: CA16216-01 ' Spike Source %aREC RPD AnaAnalyt Result F1aR P-QL units Level Result o/aREC Limits RPD Limit Notes Nitrate/Nitrite as 76 5.0 mg/L 25.0 55 85 90-110 QM-07 Matrix Spike Dup (7K38015-MSDI) Prepared: 11/18/2017 16:02 Analyzed: 11/18/201716:02 Source: CA15475-01 Spike Source %REC RPD Analyt Result Flan RQL Units Level Result %REC Limits RPD Limit Notes Nitrate/Nitrite as 52 E 2.0 mg/L 10.0 41 109 90-110 2 10 QM-07 Batch 7K2O009 - NO PREP , Blank (71<20009-11M) Prepared & Analyzed: 11/20/2017 15:40 Spike Source %REC RPD Analyte Result Flag P-M units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 m9/L LCS (7K20009-BSI) Prepared & Analyzed: 11/20/2017 15:40 Spike Source °/aREC RPD Analvte Result Ely9 QQS Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 970 50 mg/L 1000 97 90-110 Duplicate (71<20009-DUP1) Prepared & Analyzed: 11/20/2017 15:40 Source: CA16969-01 Spike Source °/aREC RPD Analvte Result F1a9 POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L 62 20 Duplicate (7K20009-DUP2) Prepared &Analyzed: 11/20201715:40 Source: CA16969-02 ' Spike Source - °/aREC RPD Analvte Result F1ao RQL units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 320 s0 mg/L 310 4 20 Batch 7K2O01O - NO PREP Blank (7K20010-BLK3) Prepared & Analyzed: 11/20/2017 18:15 Spike Source o/aREC RPD . AnalYY4 Respl[ Ebb POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L LCS (7K20010-BSi) Prepared &Analyzed: 11/20201718:15 Spike Source %aREC RPD -Analltle Resul Elog POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 960 50 mg/L 1000 95 90-110 Duplicate (7K20010-DUP2) Prepared &Analyzed: 11/20/201718:15 Source: CA16992-01 Spike Source %REC RPD Analvte Result Sall POL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solids 50 U 50 mg/L 50 U 20 Batch 7K2OO51 - NO PREP FINAL I This report relates only to the sample as received by the laboratory, and may only be reproduced In full. P819E: 22 Of 39 QUALITY CONTROL DATA ' Parameters - Quality Control Batch 7K20051 - NO PREP - Continued ENCO www.encolabs.com Blank (7)(20(IS1-BLK3) - Prepared: 11/20/201716:27 Analyzed: 11/20/201717:34 Spike Source %REC RPD Analvte Resul F1a4 p9L 11R115 Level Result %REC Limits RPOLimit Notes Chloride 2.2 U 5.0 mg/L , Sulfate as SO4 2.9 U 5.0 mg/L -. LCS (7K20051-BSI) _ Prepared: 11202017 16:27 Analyzed: 11/20201717:48 ' Spike Source %REC RPD Analvte Result EI4R CQS UBiU Level Result %REC Limits RPD Limit Notes Chloride - 51 5.0 mg/L 50.0 102 90-110 Sulfate as SO4 '52 5.0 mg/L .50.0 105 90-110 .. Matrix Spike (7K20051-MS3) Prepared: 11/20/2017 16:27 Analyzed: 11/202017 18:03 Source: CA15466-01 Spike Source %REC RPD Aualv[e Result Dam PQL i[nm Level Result %REC Limits RPD limit Notes Chloride 280 20 mg/L 80.0 200 99 90-110 Sulfate as SO4 75 20 mg/L 80.0 12 U 94 90-110 Matrix Spike Dup (7K20051-MSD3) Prepared: 1120201716:27 Analyzed: 11202017 18:17 Source: CA15466-01 Spike Source %REC RPD - Analyt Resu Flari POL Units' Level Result °/uREC Limits RPD limit Notes Chloride 290 20 mg/L 80.0 200 104 90-110 1 10 Sulfate as SO4 78 1 20 mg/L - 80.0 12 U 98 90-110 4 10 Batch 7K21O25 - NO PREP Blank (7K21025-BLK1) Prepared &Analyzed: 1121201716:20 Spike Source %REC RPD Anal vte Rest, Elag PQL Units Level Result %REC Limits RPD Limit Notes Total Dissolved Solds so U 50 mg/L LCS (7K21025-BSI) Prepared & Analyzed: 11212017 16:20 Spike Source %REC. RPD Analvte - Resul Elam E91. units Level Result o/ REC Limits RPO Limit` Notes Total Dissolved Solids 980 50 mg/L 1000 98 90-110 Duplicate (7K21025-DUP3) Prepared &Analyzed: 1121/201716:20 Source: CA16618-01 Spike Source %REC RPD Ana R—_sylt 'EiaR E" Units Level Result %REC Limits RPD limit Notes Total Dissolved Solids 120 50 mg/L 120 3 20 Duplicate (7K21025-DUP2), Prepared & Analyzed: 11/21/2017 16:20 Source: CA16618-02 Analyle Total Dissolved Solids Batch 7K22O09 - NO PREP Spike . Source %REC Rasu Elan PQL Units Level Result %REC Limits RPD 140 50 mg/L 130 8 RPD Limit Notes 20 FINAL This report relates only M the sample as received by the laboratory, and may only be reproduced in Poll. Page 23 OF 39 l t .encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Hatch 7K22009 - NO. PREP - Continued Blank (7K22009-BLK3) Prepared: 11/22/2017 09:09 Analyzed: 11/22/2017 10:51 Spike Source %REC RPD Analvte B.e,5411 173R COL 411ite Level -Result %REC Limits . RPD Limit Notes Ammonia as N 0.045 U ,. 0.10 mg/L LCS (7K22009-BS3) Prepared: 11/22/2017 09:09 Analyzed: 11/22/2017 10:53 ' Spike Source %REC RPD Analv[e Rook East E91 units Level Result %REC Limits RPD Limit Notes Ammonia as N 1.0 0.10 mg/L 0.989 101 90-110 Matrix Spike (7K22009-MSI) Prepared: 11/22/2017 09:09 Analyzed: 1122/201710:56 Source: CA14942-02 ' Spike Source %REC RPD Analid Result Haar PQL units Level Result %REC Limits RPD Limit Notes Ammonia as N 038 0.10 mg/L 0.385 0.045 U 98 90-110 Matrix Spike (7K22009-MS2) Prepared: 11222017 09:09 Analyzed: 11/22201712:42 Source: CA15875-01REL Spike Source o/aREC RPD Anelvte Re6_ul pig PQL Units Level Result °/•REC Limits RPD Lima Notes Ammonia as N 110 E 5.0 mg/L 19.8 90 87 90-110 QM-07 Matrix Spike Dup (7K22009-MSD1) Prepared: 11/22/2017 09:09 Analyzed: 11/222017 10:58 Source: CA34942-02 Spike Source %REC RPD Analvte Re_gR ELag EOL Units Level Result %REC Limits RPD Unit Notes Ammonia as N 0A1 0.10 mg/L 0.385 0.045 U 106 90-110 8 10 Batch 7K22030 - NO PREP Blank (7K22030-BLK3) Prepared: 11/22/2017 13:25 Analyzed: 11/22201717:52 Spike Source 0/ REC RPD Anal ResulS Hag POL UDUN Level Result %REC Limits RPD Lama Notes Chloride 21 U 5.0 mg/L Sulfate as SO4 2.9 U 5.0 mg/L LCS (7K22030-BSI) . Prepared: 11/22/2017 13:25 Analyzed: 11/22201718:06 Spike Source %REC RPD AnaIYt£ Re:4P12 EJ39 R" Unila Level Result 0/aREC Limits RPD LiEft Notes Chloride 51 5.0 mg/L 50.0 102 90-I1O Sulfate as SO4 52 5.0 mg/L 50.0 105 90-I10 Matrix Spike (7K22030-MSI) Prepared: 11272017 13:25 Analyzed: 11/222017 18:21 Source: CA16990-01 Spike Source %REC RPD , Analvte Result flag POL Units Level Result %REC Limits RPD Limit Notes Chloride 63 5.0 mg/L 20.0 41 109 90-110 Sulfate as SO4 37 5.0 m9/L 20.0 16 107 90.110 Matrix Spike (7K22030-MS2) Prepared: 11222017 13:25 Analyzed: 11/222017 22:10 Source: CA16992-01 Spike Source %REC RPD Analyt Resulk EL49 £QL Units Level Result 0/REC Limits RPD Limit Notes Chloride 27 5.0 mg/L 20.0 6.3 102 90-110 Sulfate as 504 19 5.0 mg/L 20.0 2.9 U 97 90-110 NNAL This report relates only to the sample u weved by the laboratory, and may only be reproduced in full. Page 24 OF 39 v vnv.encolabs.com QUALITY CONTROL DATA Classical Chemistry Parameters - Quality Control Batch 7K22O3O - NO PREP - Continued Matrix Spike Dup (7K22030-MSDI) Prepared: 11/222017 13:25 Analyzed: 11/22/2017 18:35 Source:. CA16990-01 Spike Source %REC RPD Anaht es Elan 2QL Units Level Resul o/ REC Limits RPD 1111111 Notes Chloride 63 5.0 mg/L 20.0 41 110 90-110 0.3 10 Sulfate as SO4 37 5.0 mg/L 20.0 16 107 90-110 0.07 10 Batch 7K3O008 - Same Blank (7K30008-BLK1) Prepared: 11/30/2017 11:30 Analyzed: 12/012017 08:54 Spike Source %REC RPD A alvt RElul Flg P_QL Units Level Result %REC Limits RPD Limit Notes Phosphorus 0.025 U 0.10 mg/L LCS (7K30008-BSI) Prepared: 11/30/2017 11:30 Analyzed: 12/012017 08:56 Spike Source %REC RPD Analyt Result Elau EQA Units Level Result o/ REC Limits RPD Limi Notes Phosphoms 1.7 0.10 mgp. 1.60 103 80-120 Matrix Spike (7K30008-MS1) Prepared: 11/302017 11:30 Analyzed: 12/012017 08:58 Source: CA16295-02 ' Spike Source /oREC RPD Analyt Result Flao Eu Units Level Result / REC Limits RPD Limit Notes Phosphorus 2.0 0.10 mg/L 0.610 1.3 102 80-120 Matrix Spike DUP (7K30008-MSD1) Prepared: 11/30/2017 11:30 Analyzed: 12/O1/2017 09:00 Source: CA16295-62 Spike Source %REC RPD Anaivte Result Elan 9L Units Level Result 01 REC Limits RPD Limit Notes Phosphorus 2.0 0.10 mg/L 0.640 1.3 103 80-120 0.4 25 Parameters - Batch 7K13O15 - NO PREP Duplicate (7K73015-DUP3) Prepared: 11/102017 15:25 Analyzed: 11/112017 11:00 Source: CA16216-02 Spike Source %REC RPD Analvte Resuft Flan 2Qk Units Level Result o/ REC Limits RPD 1.1mit Notes Coliform, Fecal 1.0 U 1.0 MPN/100 mL 1.0 U 25 Batch 7K2OO17 - NO PREP Duplicate (7K20017-DUP3) Prepared: 11/142017 15:25 Analyzed: 11/152017 10:00 Source: CA14942-03 Spike Source %REC RPD Analyt Result Plan POL Units Level Result %REC Limits RPD Limit Notes Coliform, Fecal 2.0 1.0 MPN/100 ml- 1.0 67 25 QM-12 Oupllwte (7K20017-DUP2) Prepared: 11/14/2017 15:25 Analyzed: 11115201710:00 Source: CA17316-02 Anal Coliforrn, Fecal Batch 7K20022 - NO PREP Spike Source %REC Result Pfau RQL Ur[ts Level Result %RECLimits RPD 1.0 U 1.0 MPN/100 mL 1.0 U RPD Limi Notes 25 FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 25 Of 39 w .encolabs.cam QUALITY CONTROL DATA Microbiological Parameters - Quality Control Batch 7K20022 - NO PREP - Continued Duplicate (7K20022-DUPI) Prepared: 11/15/2017 15:00 Analyzed: 11/16/2017 09:58 Source: CA15914-03 ' Analvte Result flag Caiifonn, Fecal 1.0 U PQL 1.0 Units MPN/100 mL Spike Source %REC Level Result %REC Limits RPD 1.0 RPD Limit Notes 25 Duplicate (7K20022-DUP2) Prepared: 11/152017 ISM Analyzed: 11/16/2017 09:58 Source: CA17349-04 Analyte Result Plan Coliform, Fecal 1.0 U EQl, 1.0 units MPN/100 mL Spike Source %REC Level Result %REC Limits RPD 1.0 U RPD J Limit Notes 25 Classical Chemistry Parameters L Quality Control Batch 7K14014 - NO PREP Blank (71(14014-BLK3) Prepared: 11/14/2017 12:30 Analyzed: 11/14/2017 12:57 Spike Source %REC RPD Aralyt Result Elm E9L Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.34 U 1.0 mill LCS (7K14014-BS1) Prepared: 11/14/2017 12:30 Analyzed: 11/14/201712:57 Spike Source %REC RPD Analyt Result 119 P41. Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 39 1.0 mg/L 40.0 97 85-115 Matrix Spike (7K34014-MS3) Prepared: 11/14/2017 12:30 Analyzed: 11/14/2017 12:S7 Spike Source %REC RPD Analyte Result L7e_4 POL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 47 1.0 mg/L 40.0 5.5 103 85-115 Matrix Spike Dup (7K34014-MSD1) Prepared: 11/14/2017 12:30 Analyzed: 11/14/201712:57 Source: AA08052-01 Spike Source %REC RPD AnaResul Elan EQL units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 46 - 1.0 mg/L 40.05.5 103 85-115 0.3 21 Batch 7K16013 - NO PREP Blank (7K36013-BLK1) Prepared: 1121/201712:00 Analyzed: 11/21/201712:45 Spike Source %REC RPD AnaAnalyte Resu Flag PQL Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 0.34 U 1.0 mg/L LCS (7K16013-BSI) Prepared: 1121201712:00 Analyzed: 1121/201712:45 Spike Source %REC RPD Analid Reesul ELag E01, Units Level Result % REC Limits RPD Limit Notes Total Organic Carbon 42 1.0 mg/L 40.0 106 85-115 ' Matrix Spike (7K16013-MSi) .Prepared: 1121201712:00 Analyzed: 1121201712:45 Source: CA17316-01 Spike Source %REC RPD Analvte Result Fag E91 Units Level Result %REC Limits RPD Limit Notes Total Organic Carbon 44 1.0 mg/L 40.0 7.5 91 85-115 FINAL This report relates only t° the sample as received by the lab°ramry, and may only be reproduced h full. P619E: 26 OF 39 QUALITY CONTROL DATA Batch 7K16013 - NO PREP -,Continued eM www.encolabsxom Source: CA17316-01 Spike - Source %REC RPD Analvte Result EIBg p41f 911ts 'Level Result o/REC Limits RPD imt .Notes Total Organic Carbon 39 110 mg/L 40.0 7.5 79 85-115 12 21 QM-07 Batch 7K27019 - NO PREP Blank (7K27019-BLKI)- Prepared: 11/27/2017 10:21 Analyzed: 11/28/2017 11:46 - :Spike Source ^/oREC RPD Anajyj Resu Flaq .Pyy Units Level Result %REC Limitr RPD Limi Notes Total Organic Carbon 0.34 U 1.0 mg/L - LCS (7K27019-BSI) Prepared: 1127/201710:21 Analyzed:. 11/28/201711:46 Spike Source %REC RPD .ABalvLC Result Elect P91 U^tr Level Result %REC Limits' RPD Notes Total Organic Carbon 34 1.0 mg/L. 40.0 i 86 85-115 Matrix Spike (7K27019-MSS) Prepared: 11/27/2017 10:21 Analyzed: 11/282017 11:46 Source: AA08228-01 .. Spike Source °/oREC RPD Analift ResuftEL5 m Units Level Result %REC .Limits RPD Unlit Notes Total Organic Carbon 36 1.0 mg/L 40.0 036. 89 85-115 Matrix Spike Dup (7K27019-MSDI). Prepared: 11/272017 10:21 Analyzed::11282017 11:46 - Source: AA08228-01 Spike Source %REC RPD Analvte Resul ELaa m Un"ita Level Result %REC Limits RPD Limit Notes Total Organic Carbon 36 1.0 mg/L 40.0 0.36 89 85-115 0.8 21 l FINAL This report relates only to the sample as received by the labomtory, and may only be reproduced In full. Page 27 Of 39 www.encolahs.com FLAGS/NOTES AND DEFINITIONS B The analyte was detected in the associated method blank. D The sample was analyzed at dilution. ] The reported value is between the laboratory method detection limit (MDQ and the laboratory method reporting limit (MRL), adjusted for actual sample preparation data and moisture content, where applicable. U The analyte was analyzed for but not detected to the level shown, adjusted for actual sample preparation data and moisture content, where applicable. E The concentration indicated for this analyte is an estimated value above the calibration range of the instrument. This value is considered an estimate. MRL Method Reporting Limit. The MRL is roughly equivalent to the practical quantitation limit (PQL) and is based on the low point of the calibration curve, when applicable, sample preparation factor, dilution factor, and, in the case of soil samples, moisture content. PQL PQL: Practical Quantitation Limit. N The analysis indicates the presence of an analyte for which there is presumptive evidence (85% or greater confidence) to make a `tentative identification". P Greater than 25% concentration difference was observed between the primary and secondary GC column. The lower concentration is reported. QM-07 The spike recovery was outside acceptance limits for the MS and/or MSD. The batch was accepted based on acceptable LCS recovery. QM-12 Precision between duplicate samples was outside acceptance limits. FINAL This report relates only m the sample as received by the laboratory, and may only be reproduced In full. I Page 28 Of 3g Sample Chain of Custody Form Acct#: WA013 Client WASTEWATER MANAGEMENT, LU Contact: RANDALL JARRELL Ship To: P.O. Box 57B Pittsboro, NC 27312 Report To: P.O. Box 578 Pittsboro, NC 27312 CA15466-01 t\ (.1.a 10 IC MW-1 ------------ -- -1--'--- CA15466-02 1l `to 09%1fMW-2 - - _ . CA15466-03Vyf4l _ Ux-y- MW-3 .. .. ........ .......... ... ... .... CA15466-04 Vl`tx 19U- MW-4 CA15466-05 R-1 CA15466-05 R-2a Prelog M Project#/Reference: Required TAT: CA15466 Sager Foods-MWs 10 ENCO Contact: Stephanie.Franz 102-A Woodwinds Industrial Court Cary, NC 27511 Pittsboro, NC 27312 Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D . FColi , Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2, NOX 353.2 , P , Sulfate 300, TDS SM2540C TOC SM5310B Containers: l-250mLP+H2SO4,2-40mLAV+H3PO4,1-500mLP Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , Nitrate as N 353.2 , Nitrate Cale 3531.2 , Nitrite as N 853.2 , NOX 353.2 , P, Sulfate 300 TDS SM2540C , TOC SM5310B Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV+H3PO4 , 1 - 500ml-P Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2. P , Sulfate 300, TDS SM2540C , TOC SM5310B Containers: 1 - 250mLP+H28O4 ; 2 - 40mLAV+I J3PO4 , 1 - 500mLP Analyses: Nitrate as N 353.2 , Nitrate Cale 353.2 Nitrite as N 353.2 , NOX 353.2 , Ammonia 360.1 , Chloride 300 COD SM5220D , FColi , P, Sulfate 300, TDS SM2540C , TOC SM5310B Containers: l-250mLP+H2SO4,2-40mLAV+M3PO4,1-500mLP Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P, Sulfate 300, TDS SM2540C, TOC SM5310B, Nitrate as N 353.2 , NitrateCale3532 ; Nitrite as N 353.2 , NOX 353.2 Containers`: 1 - 250mLP+H2SO4 , 2 - 40mLAV+HI3PO4 , 1 - 500mLP Analyses: Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 , Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P, Sulfate 300, TDS SM2640C , TOC SM5310B ' Containers: 1-250mLP+H2SO4,2-40mLAV+H3PO4,1-500ml-P Page 29 of 39 �O I I Sample Chain of Custody Form CA15466-07 LL A 1.1. L'L`t3 F2-3 Analyses: Ammonia 350.1 ,Chloride 300 ,COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C, TOG SM5310B, Nitrate as N 353.2 , Nitrate Cale 3512 , Nitrite as N 353.2 , NOX 353.2 Containers: 1-250mLP+H2SO4,2-40mLAV+H3PO4,1-500mLP CA15466-08 CA15466-09 R-4 R-5a ----------------------------------- CA15466-10 R-6 Analyses: Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 , Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C TOG SM5310B Containers: l-250mLP+H2SO4,2-40mLAV+H3PO4,1-50DmLP Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C, TOO SM531013, Nitrate as N 353.2 , Nitrate Cale 353 2 , Nitrite as N 353.2. NOX 353.2. Containers: 1 - 250m.LP+H2SO4 , 2 - 46mLAV+H3PO4 , 1 - 500mLP Analyses: Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 , Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C , TOG SM5310B Containers: l-250mLP+H2SO4,2-40mLAV+H3PO4,1-500ml-P CA15466-11 R-7 Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C, TOG SM5310B. Nitrate as N 353.2 , Nitrate Cale 353:2 , Nitrite as N 353.2 , NOX 353.2 Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV+H3PO4 , 1 - 500mLP ------------------ ------ ----- -- ------ - - - ----- --- - ----------- - - --- --- - - CA15466-12 R-8 Analyses: Nitrate as N 353.2 , Nitrate Cale 35312, Nitrite as N 353.2 , NOX 353.2 , Ammonia 350.1 , Chloride 30D , COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C ,TOG SM5310B I - Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV+H3PO4 , 1 - 500mLP CA15466-13 R-9 Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C, TOC SM531013, Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV+ H 3PO4,1-500mLP ---' ------------------- -- -- -. .__ .. ... .. _ ... ... j. .... --. .- Page 30 of 39 Sample Chain of Custody Form Sampled By Te p: RelingoishedB : DalelTi e: �i(w l' Condition: Acceptable _Unacceptable Receiv d B - DateyTi{ne i Notes: � ! Containers in this sample kit may contain chemical preservatives as required by the EPApmcedu s.Infrmation=mmingMemaledalsmnbefounawe . 00NOT�innsecantainerspriorto use! When filling presented containers, use caution not to inhale vapors that may W caused in the chemical reaction between Me sample and the preservatives. Collect sampll s in a well-venti!ated area or take appmpiizte precautions to avoid exposure to these fumes. See cautions below pertaining to the handling of Mesa materials. It is the shipper's responsibility to ensure that the samples are packed in such a manner to prevent breakage and that any required temperature is maintained during Vans t until receipt at me laboratory. Atemperature blank has been included to measure the ambient temperature of the cooler upon receipt at the lab. Please do not remove this container from the cooler, bu pack along with the samples in a similar manner. This bottle contains deionized water only. 1 The information odow are PRECAUTIONARY STATEMENTS ONLY[ All potential hazards posed by these materials have not been addressed. For additional Information ur assistance,please contact your organizalion's safety professional. ' Cautions a Abbreviations MCI E Hydrochloric Add -STRONG ACID! Avaid skin and eye contact Ifcontad is made. gush affected areas immediatelywithwxter. HN63: Nitric Add- STRONG ACID! STRONG O%IDIZERI Avoid skin and eye contact. ❑ a mad is made, gush affected areas immediately with water. 43PO4 t PhosphoecAcid- STRONGACID! Avoid skin and eye contact. If cardad is made, gush affected areas tmmedialely with water. HYSO4: SulfuricAcid- STRONG ACIDI Avoid skin and eye contact If contact is made, flush eHeded areas immediately with water. Asc Acid[ AsrorbieAdd-Avoitl skin and eye cantacL If canted is made, Rush affected areaiimmedialety with water. ZhAc: ZmcAcelale-Avoid skin and eye contact. If contact is made, flush affected areas immediately with water. P8 2 31 0f 39 NaHSO4: Sodium Thiosulfate- Avoid skin and eye canted It contact is made. Rush affected areas immediatelywith water. 9 NaOH: Sodum Hydroxide -STRONG CAUSTICI Avoid skin and eye contact. Hamad is made, Rush affected areas inmedatelywlthwater. MCOH: Methanol -Avoid skin and eye armed. If carract is made: Rush affected areas immediately with water. Sample Preservation Verification ENCO Cary Work Order: CAI5466 Project: Sager Foods -MWs Client: WASTEWATER MANAGEMENT, LLC (WA013) Project#: [none] Logged In: 10-Nov-17 15:18 Logged By: John C King Preservation Check Performed By: Date/Time: CA15466-01 Cont Type Pres (pH) pH Checked / pH Adjusted Date�me Reagent Used/Co(ments Requirement In•Control Adjusted A 250ml-P+112SO4 <2 / N / NA I Y / I NA CAI5466-02 V i Cont YP Type .. Pres (pH) Requirement pH Checked / In Cdntrol Dal Mme PH Adjusted Adjusted ReagenYUsed/Comments -- A 250mLP+H2SO4 <2 / N 1 NA - Y NA CAI5466-03 Cont' _ ' Type Pres(pH)- Requirement pH Checked? In Control `- DatelTme -_- pH Adjusted Adjusted - -' ,Reagent Used/Comments -- i A 250mLP+H2SO4 <2 - / N / NA I Y / / NA � ` CA15466-04 Cont T e YP Pres (pH) • Requirement pH Checked / In Cdntrol PH Adjusted - - DateTme usted Adjusted Reagent Used/Comments i _ A 250mLP+H2SO4 - • <2 / N / NA I Y I / NA I CAI5466-05 Cont Type Pres(pH) Requirement pH Checked In Control -' Date/Tnie pH Adjusted Adjusted _ Reagent Used/Comments - l -- A, 250ml-P+H2SO4 _ <2 / N / NA Y ! / NA Rea "ent Name ID 1 - 2 pH Strip ID: C:\ELMNT\Print\wko—PreservationCheck.rpt Reagent Name ID 31 15 41 1 6 N_ CCU Sample Chain of. Custody Form Acct#: WA013 Client WASTEWATER MANAGEMENT, LL( Contact: RANDALLJARRELL Ship To: P.O. Box 578 Pittsboro, NC 27312 Report To: P.O. Box 578 Fpittsboro, NC 27312 DateMme Sampled Sample ID CA15466-01 .CA15466-02 - CA15466-03� CA16466-04 CA15466-05 R-1 CA15466-06 ��I lk l� �J R-2a Prelog#: ept6'466- CA-Ofs Project#/Reference: Sager Foods -MWs Required TAT: 10 ENCO Contact: IStephanie Franz Woodwinds Industrial NC 27511 oro, NC 27312 Analyses/Containers Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D, FColi , Nitrate as N 353.2 , Nitrate Cato 353.2 , Nitrite as N 353.2 , NOX 353.2. P , Sulfate 3001, TDS SM2540C , TOC SM5310B Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV+H3PO4 , 1 - 500mLP I - Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 , P , Sulfate 300,, TDS SM2540C , TOC SM53106 Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV+H3PO4 , 1 - 500mLF Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D, FColi , Nitrate as N 353.2 , Nitrate Calc 353.2 , Nitrite as N 353.2 , NOX 353.2 , P , Sulfate 30Q , TDS SM2540C , TOC SM5310B Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV+4H3PO4 , 1 - 500mLP Analyses: Nitrate as N 353.2 , Nitrate Calc 35i 3.2 , Nitrite as N 353.2 , NOX 353.2 , Ammonia 350,1 , Chloride 300, COD SM5220D , FColi , P , Sulfatei 300 , TDS SM2540C , TOC SM5310B t Containers: 1 - 250mLP+H2SO4 , 2 - 40ml-AV+1-13PO4 , 1 - 500mLP Analyses: Ammonia 350.1 , Chloride 300 , COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C. TOC SM5310B. Nitrate as N 353.2 , Nitrate Calc 353.2 , Nitrite as N 353.2 , NOX 353.2 Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV I H3PO4 , 1 - 500mLP Analyses: Nitrate as N 353.2 , Nitrate Calc 353.2 , Nitrite as N 353.2 , NOX 353.2 , Ammonia 350.1 , Chloride 300, COD SM52201), FColi , P , Sulfate 300. TDS SM2540C TOC SM5310B Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV I H3PO4 , 1 - 500mLP Sample Chain of Custody Form CA15466-07 Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C , T6c SM5310B , Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 Containers: 1-250mLP+H2SO4,2-40mLAV+H3PO4,1-500mLP CA15466-08 t i(t v l ISO R-4 Analyses: Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 , Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 300, TDS SM2540C , TOC SM5310B Containers: 1 - 250mLP+H2S64 , 2 - 40mLAV+H,3PO4 , 1 - 500ml-P CA15466-09 t (t y I t y,i R-5a Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , t P Sulfate 300, TDS SM2540C , TOC SM531 oB , , Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 Containers: 1 - 250mLP+H2SO4 , 2 - 40mlAV+H3PO4 , 1 - 50omLP CA15466-10 R-6 Analyses: Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 , Ammonia 350.1 , Chloride 300 , COD SM5220D , FColi , P , Sulfate 300, TDS SM25400 , TOC SM5310B Containers: 1-250mLP+H2SO4,2-40mLAV+H3PO4,1-500mLP CA15466-11 R-7 Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , SM2540C, TOC SM531013 P , Sulfate 300, TDS , Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2 , NOX 353.2 Containers: 1 - 250mLP+H2SO4 , 2 - 40mLAV ;H3PO4 , 1 - 500mLP CA15466-12 R-8 Analyses: Nitrate as N 353.2 , Nitrate Cale 353.2 , Nitrite as N 353.2. NOX 353.2 , Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P , Sulfate 301), TDS SM2540C TOC SM6310B Containers: 1 - 25omLP+H2SO4 , 2 - 40mLAV+H3PO4', 1 - 50omLP CA15466-13 R-9 Analyses: Ammonia 350.1 , Chloride 300, COD SM5220D , FColi , P Sulfate 300, TDS SM2540C, TOC SM5310B , , Nitrate as N 353.2 ; Nitrate Cale 35�1.2 , Nitrite as N 353.2 , NOX 353.2 Containers: 1-250mLP+H2SO4,2-40mLAV+H3PO4,1-500mLP Page 34 of 39 Sample Chain of Custody Form z� Sampled By. Temp: Condition: Acceptable _Unacceptable Containers in this sample hit may named, chemical preserva!ives as required use' k i 4o Date/Time., - il�ia�3 round below. DO NOT rinse wnleiners prior to When pPng preserved containers, use carman not to inhale vapors that may be caused In the chemical reaulon beheen the sample and the prescrvati+ea. Collect samples in a vrell-venblaled area or take appropriate P(emJtlons to avold exposure to these lames: See cautions below pedawng to the hanmtg of these materials , It is the shippers responsibility to ensure Nat the samples are packed in such a manner to prevent breakage and that any required temperature is maintained during bensit until receipt at the laboratory. Atemperature blank has been included to measure the amblent temperature of the water upon receipt at the lab. Please do not remove this container from the water,. but pack along with the samples in a somlarmamaer. This bathe contains daionizedwater only. The information beloware PRECAUTIONARY STATEMENTS ONLY[All potential hazards pond by these materials have not been addressed. For edditiorWinformation or assistance, please contact yaw organization's safely professional. Abbreviations skin and H3PO4: Phosphene Add-STRDNGAUIUt wvam scar MSO4: SulfuricAcid- STRONGACID! Avoid skill an Asa Add: AscorbicAGd -Avoid skin mu eye comas. ZnAc: ZInCAwtam -Avoid skin and eye canted. It a NaHSO4: Sodnun Thiosullme -Avoid ski and eye ce NaOH: Sodium Hydroxide - STRONG CAUSTICI Avo ManH • Methmil -Avoid skin and eve coned. 11 con mart. If wntad is made. flush affected areas immedistetywith water skinandeyewrosta If corded is made, push affected areas immediately with mler. comad. If contact is made, gusb eeded areas imrr-- ,alely wW voter. made. flush effected areas areas immedaLly with water. walef. Immedalely vrilh water. Page 35 of 39 Sample Preservation Verification ENCO Cary Work Order: CA17316 Client: WASTEWATER MANAGEMENT, LLC (WA013) Logged In: 14-Nov-17 13:33 Preservation Check Performed By: CA17316-01 Project: Sager Foods-MWs Project* [none] Logged By: John C King Date/Time: Cont Type Pres(pH) pHChecked! -.DateTme PH Adjusted Used/Comments Requirement In Control AdjustedReagent A _ 250mLP+H2SO4 <2 / N / NA I Y / / NA t CA17316-02 Cont Type Pres (pH) Requirement pH Checked! I In Control DateTme pH Adjusted Adjusted Reagent Used/Comments A 250mLP+H2SO4 <2 / N / NA I Y / I NA , CA17316-03 Cont Type Pres (pH) pH Checked / pH Adjusted DateRme Adjusted Reagent Used/Comments Requirement In Control A 250mLP+H2SO4 <2 /N/NA Y/ /NA I CA17316-04 Cont Type Pres (pH) Requirement pH Checked / In Control Date/Tme pH Adjusted Adjusted Reagent Used/Comments _` A _ 250mLP+H2SO4 _<2 1 / N / NA I Y '/ NA I Rea ent Name ID 1 2 pH Strip ID: 1 b-5Z0 Rea ent Name ID 3 4 i Reagent Name 1 ID 5 � 6 Page 36 of 39 Page 1 of 1 C:1ELM NT1Printlwko_PreservationCheck. rpt 9 min jT? HU711 - P9 - Sample`Chain"Qyl.Custody Form: siim To u bAtwo-'O _4 G 0 ,- '_ * ' - ` jp_; S M2 WC Anglos"Ammonia lO MirgiB 4s N.4 k�X, 2','NOX Can , f A4n70dW354:),1 Mr.- .'. Cbto!' 1� P N 353.2 P' FL904'_i 2 7. A 0 mLF.I. 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Pa.a.. cc^--] eE=s mr'yl:aml wul nib. Sarn re tin P servaii''ri Verification b4COYt2ry MM, CiiznL INA�EWATPR MANAGEMENT; LLC (VYA613) Pfcject [nuns]! L _Qgged bo.L]Red IS PH.C"o I 16 coduol PHAdjpstsd caterr" T Rpac—f USedlCmments4SI AdpjtFd=t R- I N Pra,(pq H, rkedll--- g 1�F jrtco�� H Adj -te P M Ree�lgcnt Usa&Cm,us eMs =,d L Wl C,A17349-fl4 1Coin Type I -pr Ait pR usiod Hdjusled N T I il 46acen'i Name eauent Wia6,, 3 -M `traps C-710820, Page 39 of 39 f 1 �i41t SAM TER QUALITY MONITORING: E REPORT FORM Name: Sager Creek Vegetable Company Name (if different): Address: 5900 Turkey Highway y t$1fet1 NC 28393 County Sampson act Person: Randall Jarrell Telephone#:919-210-2500 Location/Site Name: Rowan Site No. of wells to be sampled: L ID NUMBER (from Permit): MW-R5A Depth: 17.Oft. h to Water Level: 7.5 ft. below measuring point luring Point is 3 ft. above land surface ne of water pumped/bailed before sampling: 7.0 Date sample collected: 11/14/17 Well Diameter: 2 in. Screened Interval: _ft. to _ft. Relative M.P. Elevation: ft. ) sample analyzed: 11/14 - 12/1 Laboratory Name: ENCO tAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 17 mg/I Nitrite (NO2) as N 0.14 mg/I Coliform: MF Fecal <1.0 /100ml Nitrate (NO3) as N 2.4 mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0.10 mg/I (Note: Use MPNmethodfor higNyturhidsamples) Orthophosphate mg/I Dissolved Solids: Total 150 mg/I AI -Aluminum mg/I pH (when analyzed) units Be - Barium mg/I TOC 1.7 mg/I - Calcium mg/I Chloride 56 mg/I pC l��c,C_a REC/1E)1�I W1�,9Sf,�Uadmium RECEIVE- mg/I Arsenic mg/I ®E'L�f167IrY Rum: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mgA JAN 2 9 201,R Fe - Iron mg/I Sulfate 24 nl Hg - Mercury mg/I Specific Conductance µMhos K - Potassium mg/I Total Ammonia <0.04 WOR%L Magnesium �TTEWLLP"':PdP mg/I (Ammonia Nitrogen; NlIos N: Ammonia Nitrogen. Mj'ngan YeE mg/I TKN as N mg/I Ni - Nickel mg/I RESOURCES 'ROCESSING UNIT: 999-1517 Phone:(919) 733-3221 RMIT Number: Expiration Date: blJ'll10L7 n-Discharge WQ0004268 UIC 'DES Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heal Pump ❑ Other: FIELD ANALYSES: pH 4.56 units Temp. 20.6 °C Spec. Cond. µMhos Odor Appearance Certification No. 591 Pb - Lead Zn -Zinc`0 Other (Specify Compou _�/� VI ORGANICS: (by GC, GC/MS?'HPLW (Specify test and method A ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method # method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Timothy P. Ruby, DelMonte Foods, Inc. Pennittee (or Authorized Agent) Name and Title - Please print or type GW-59 Rev. 112007 Signature of Permittee (or Authorized Agent) (Date) at of J UNLI Name: Name (if TER QUALITY MONITORING: E REPORT FORM Creek Vegetable Company Address: 5900 Turkey Highway y (s'roo1) NC 28393 County Sampson Person: Randall Jarrell Telephone#: 919-210-2500 Location/Site Name: Plant Site No. of wells to be sampled: 13 prom Permie PILING INFORMATION LID NUMBER (from Permit): MW-1 Dale sample collected: 11/10/17 Depth: 30.Oft. Well Diameter: 21n. h to Water Level: 27.0 ft. below measuring point Screened Interval: _ft. to _ft. wring Point is 3 ft. above land surface Relative M.P. Elevation: ft. ne of water pumped/bailed before sampling: 2.0 gallons sample COD 25 mg/I Coliform: MF Fecal <1 /100ml Coliform: MF Total A00ml (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 330 mg/I pH (when analyzed) units TOC 5.4 ni Chloride 200 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate <2.9 mg/I Specific Conductance µMhos Total Ammonia <0.045 mg/I (Ammonia Nitrogen; NH>as N; Ammonia Nitrogen. Total) TKN as N mg/I Number: Expiration Date: hargeWQ0004268 UIC_ Other PE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery © Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: FIELD ANALYSES: WAS pH 4.32 units Temp. 19.7 oC DRY at S ec. Cond. µMhos time of p emm�lin Odor Appearance Laboratory Name: ENCO colloidal concentrations. Nitrite (NO,) as N <0.017 mg/l Pb - Lead Nitrate (NO3) as N 0.53 mg/1 Zn - Zinc Phosphorus: Total as P 0.045 mgn Orthophosphate mgll AI - Aluminum mg/l Be - Barium mg/I Ca - Calcium mg/l Cd- Cadmium mg/l Chromium: Total mg/l Cu - Copper mgfl Fe - Iron mq/I Hg - Mercury mgll K- Potassium mg/l Mg - Magnesium mg/I Mn - Manganese mg/I NI - Nickel mg/I Certification No. 591 mg/I Other (Specify Compounds and Concentration Units) wr- .-%If-IN /c: F-? WOMMbon Prccessmg unn ORGANICS: (by GC, GCIMS, 91V t3t�u, (Specify test and method #. ATTACH LAB REPORT.) Report Attached? ❑ Yes (1) ❑ No (0) VOC , method # , method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Timothy P. Ruby, Delmonte Foods, Inc. Permiftee (or Authorized Agent) Name and Title - Please pdnt or type Signature of Pennines (or Authorized Agent) (Date) GW-59 Rev. 1/2007 01