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HomeMy WebLinkAboutWQ0004893_2016 Annual Report_201702132 0 2017 Campbell Soup Supply Company, LLC 2016 Land Application Report Permit #WQ0004893 2120 NC 71 Highway North Maxton, NC 28364 February 13, 2017 North Carolina Department of Environment and Natural Resources Aquifer Protection Section 1.617 Mail Service Center Raleigh, NC 27699-1617 Reference: 2016 Land Application Annual, Report Campbell Soup Supply Company Maxton, North Carolina, Permit No. WQ0004893 Information Processing Unit: Enclosed Campbell Soup Supply Company is submitting all monitoring and reporting information as required in the referenced permit for the facility in Maxton, North Carolina. This report includes: 1) Certification Form, 2) Annual Residual Sampling Summary Form, 3) Annual Metals Field Loading Summary Forms, 4) Annual Land Application Field Summary Form, 5) Residual Analysis Lab Sheets, 6) TCLP Lab Sheets, 7) Pathogen and Vector Attraction Form, 8) Pathogen and Vector Attraction Reduction Documentation, 9) Soils Lab Data, 10) 2016 Application Summary Table, and 11) Application Condition Summaries. This is a non-503 permit that is not required to have pathogen reduction or vector attraction reduction requirements to be met. A total of 656,218 gallons (100,061 dry tons) of industrial residuals were land applied to 56.8 acres. If any further information is required regarding this land application program, please do not hesitate to contact me at (910) 844-1654. Sincerely, Gnus C '� /tic/ J ie C. Collins Environmental Manager (7) TABLE OF CONTENTS I Certification Form II Annual Residual Sampling Summary Form III Annual Metals Field Loading Summary Forms IV Annual Land Application Field Summary V Quarterly Residual Analysis Lab Sheets VI Toxicity Characteristics Leaching Procedure (TCLP) Analysis Report VII Pathogen and Vector Attraction Reduction Documentation Vill Soil Analysis Report IX 2016 Application Summary Table X 2016 Application Condition Summaries Certification Form ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0004893 County: Robeson Year: 2016 Facility Name (as shown on permit): Campbell Soup Supply Company Land Application Operator: Campbell Soup Supply Company Phone: (910) 844-5631 �r Land application of residual solids as allowed by the permit occurred during the past calendar year? -- v❑ Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: 7 Total number of fields land application occurred during the year: 7 Total amount of dry tons applied during the year for all application sites: 100.1 Total number of acres land application occurred during the year: 56.8 Part B: Facility was compliant during calendar year 2016 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. ❑ Yes r❑ Na If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1.Only residuals approved for this permit were applied to the permitted sites. 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 't All other monitoring was performed in accordance with the permit and reported during the year as required l and three (3) copies of certified laboratory results are attached. 6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is; to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing Wildo s." Michael G. Miller - Sr. Dir. Of Operations A A �I 3 Permittee Name and Title (type or print) Signature of Permittee Date Si ture of Preparer* (i different from Permittee) Preparer is defined in 40 CFR Part 503.9 (r) Date Signature of Land Applier Date (if different from Permittee and Preparer) DENR FORM ACF (5/2003) Annual Residual Sampling Summary Form I `r J t ANNUAL RESIDUAL SAM , s,JNG SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: WQ0004893 Laboratory: Facility Name: Campbell Soup Supply Company NPDES # or WQ#: WQ0003626 WWTP Name: Campbell Soup Supply Company - DAF Residual Analvsis Data 1) Waypoint Analytical 2) 3) 4) 5) Sample or Composite Date Ceiling Cone. 1/4/16 4/4/16 9/22/19 11/2/16 Percent Solids NA 2.87 6.61 6.16 0.45 Arsenic 75 3 3 3 3 Cadmium 85 2 2 2 2 Chromium 4,300 NR NR NR NR d Copper NA 25 39 11.7 40 .�, Lead 840 5 5 5 5 9 Mercury 57 0.4 0.6 0.4 0.4 Molybdenum 75 5 5 5. 15 y Nickel 420 22 62 12.6 12.4 Selenium 100 5 5 5 5 Zinc 7,500 216 330 159 395 Total Phosphorus NA 1190 615 1000 3440 TKN NA 25100 14100 13800 30400 Ammonia -Nitrogen NA 2090 1820 1460 17400 Nitrate and Nitrite NA 2 2 6.19 1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." i Si iature of Preparer Date DENR FORM RSSF (512003) ANNUAL RESIDUAL SAI' , �4NG SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Permit Number: W00004893 Laboratory: 1) Waypoint Analytical Facility Name: Campbell Soup Supply Company 2) NPDES # or WQ0003626 3) WQ#: 4) WWTP Name: Campbell Soup Supply Company - DAF 5) Residual Analysis Data ------------ ------------ ------------ "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." if SignArc of Preparer �-F / Date DENR FORM RSSF-B (5/2003) Annual Metals Field Loading Summary Forms ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 22.91175 Permit #: W00004893 Cation Exchange Capacity (non 503 only): >5.0 t ator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company t.... w Used: 5.1 Acres Permitted: 5.1 Site #: S Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1 1/4/16 _2j 1/4/16 3j 4/4/16 4j 9/23/16 5j 9/23/16 a 9/23/16 7 9/23/16 8 9/23/16 9j 0 11 12 %Solids 2.87 2.87 6.61 6.16 6.16 6.16 6.16 6.16 Arsenic 3 3 3 3 3 3 3 3 Cadmiuml 2 2 1 2 1 2 2 1 2 2 1 2 Chrorniuml 0 0 0 28.5 28.5 28.5 28.5 28.5 Copper 25 25 39 11.7 11.7 11.7 11.7 11.7 Lead 5 5 5 5 5 5 5 5 Mercury 0.4 0.4 0.6 0.4 0.4 0.4 0.4 0.4 Molyb- denum 5 5 5 5 5 5 5 5 Nickel 22 22 1 62 1 12.6 12.6 1 12.6 12.6 1 12.6 Selenium 1 5 5 5 5 5 5 5 5 Zinc 216 216 330 159 159 159 159 159 Total Phos- ohorus 1190 1190 615 1000 1000 1000 1000 1000 `ial Heavy Metal Field Loadings (Calculated in lbs/acre): 2 3 4 5 6 7 8 10 11 12 0 y w H m o r � m 0 ^ w D y o 0.3768 0.2477 0.8239 0.7355 0.3004 0.9939 0.2737 0.7406 Arsenic 0.0023 0.0015 0.0049 0.0044 0.0018 0.006 0.0016 0.0044 0 0 0 0 0.027 Cadmium 0.0015 0.001 0.0033 0.0029 0.0012 0.004 0.0011 0.003 0 0 0 0 0.018 Chromitur 0 0 0 0.0419 0.0171 0.0567 0.0156 0.0422 0 0 0 0 0.1735 Copper 0.0188 0.0124 0.0643 0.0172 0.007 0.0233 0.0064 0.0173 0 0 0 0 0.1667 Lead 0.0038 0.0025 0.0082 0.0074 0.003 0.0099 0.0027 0.0074 0 0 0 0 0.0449 Mercury 0.0003 0.0002 0.001 0.0006 0.0002 0.0008 0.0002 0.0006 0 0 0 0 0.0039 Molyb- 0.0038 0.0025 0.0082 0.0074 0.003 0.0099 0.0027 0.0074 0 0 0 0 0.0449 denum Nickel 0.0166 0.0109 0.1022 0.0185 0.0076 0.025 0.0069 0.0187 0 0 0 0 0.2064 Selenium 0.0038 0.0025 1 0.0082 0.0074 0.003 0.0099 0.0027 0.0074 0 0 0 1 0 10.0449 Zinc 0.1628 0.107 0.5438 0.2339 0.0955 0.3161 0.087 0.2355 0 1 0 0 0 1,.7816 Total Phos- 0.8968 0.5895 1.0134 1.471 0.6008 1.9878 0.5474 1.4812 0 0 0 0 8.5879 horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the i:- mation submitted. I am aware that there are significant penalties for submitting false information, i, //ding the possibility of fines and imprisonment for knowing violations" Vggnature of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 2.9022 Permit #: W00004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 8.4 Acres Permitted: 8.4 Site #: S Field #: 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): t 1 11 00000000000 i t t 1 11 0000�000000 t t l • t l 00000000000 ♦ i ... t t 1: 00000000000 t t 1: t 11 00�000�0000 t 11 t t t t 00000000000 i t l t t t 1; 00000000�00 t 11: t l t 00000000000 1 11 ®i t " 00000000000 t 1.. "I certify, under penalty of law, that this document was prepared under mydirection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Applier Date " See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 32.7028 Permit #: W00004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 26 Acres Permitted: 26 Site #: S Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date _jj 1/4/16 1jt 1/4/16 1/4/16 > 1/4/16 > 1/4/16 _1j 1/4/16 Ij 1/4/16 a 4/4/16 _3j 4/4/16 3j 4/4/16 3j 4/4/16 8 [11/3/16 %Solids 2.87 2.87 2.87 2.87 2.87 2.87 2.87 6.61 6.61 6.61 6.61 0.45 Arsenic 3 3 3 3 3 3 3 3 3 3 3 3 Cadmium 2 2 2 2 2 2 2 2 2 2 2 2 Chromiuml 0 0 0 0 0 0 0 0 0 0 0 26 Copper 25 25 25 25 25 1 25 25 39 39 39 39 40 Lead 5 5 5 5 5 5 5 5 5 5 5 5 Mercury 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.6 0.6 0.6 0.6 0.4 Molyb- enum denum 5 5 5 5 5 5 5 5 5 5 5 15 Nickel 22 22 22 22 22 22 22 62 62 62 62 12.4 Selenium 5 5 5 5 5 5 5 5 5 5 5 5 Zinc 1 216 216 216 216 216 216 216 330 330 330 330 395 Total Phos- homs 1190 1190 1190 1190 1190 1190 1190 615 615 615 615 3440 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): { o 0 o' 0.0908 0.0967 0.0279 0.0786 0.0901 0.0489 0.0337 0.1342 0.2101 0.192 0.1948 0.06 Arsenic 0.0005 0.0006 0.0002 0.0005 0.0005 0.0003 0.0002 0.0008 0.0012606 0.0012 0.0012 0.0004 0.0075 Cadmium 0.0004 0.0004 0.0001 0.0003 0.0004 0.0002 0.0001 0.0005 0.0008404 0.0008 0.0008 0.0002 0.005 Chromiunj 0 0 0 0 0 0 0 0 0 0 0 0.0031 0.0031 Copper 0.0045 0.0048 0.0014 0.0039 0.0045 0.0024 0.0017 0.0105 0.0163878 0.015 0.0152 0.0048 0.0852 Lead 0.0009 0.001 0.0003 0.0008 0.0009 0.0005 0.0003 0.0013" 0.002101 0.0019 0.0019 0.0006 0.0126 Mercury 7E-05 8E-05 2E-05 6E-05 7E-05 4E-05 3E-05 0.0002 0.0002521 0.0002 0:0002 5E-05 0.0013 Molyb- 0.0009 0.001 0.0003 0.0008 0.0009 0.0005 0.0003 0.0013 0.002101 0.0019 0.0019 0.0018 0.0138 denum Nickel 0.004 0.0043 0.0012 0.0035 0.004 0.0022 0.0015 0.0166 0.0260524 0.0238 0.0242 0.0015 0.1127 Selenium 0.0009 0.001 0.0003 0.0008 0.0009 0.0005 0.0003 0.0013 0.002101 0.0019 0.0019 0.0006 0.0126 Zinc 1 0.0392 0.0418 0.0121 0.034 0,0389 0.0211 0.0146 0.0886 0.13866rO223 0.1286 0.0474 0.7315 Total Phos- 0.2161 0.2301 0.0664 0.1871 02144 0,1164 0.0802 0.1651 0.25842 0.2396 0.4128 2.4228 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance witha system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possiibiili/tyy of fines and imprisonment for knowing violations" Sigifature of Land Applier Date �- *See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 19.98815 Permit #: W00004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 9.1 Acres Permitted: 9.1 Site #: S Field #: 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1/4/16 1/4/16 1/4/16 4/4/16 9/23/16 9/23/16 9/23/16 11/3/16 11/3/16 11/3/16 11/3/16 1113/16 %Solids 2.87 2.87 2.87 6.61 6.16 6.16 6.16 0.45 0.45 0.45 0.45 0.45 Arsenic 3 3 3 3 3 3 3 3 3 3 3 3 Cadmium 2 2 2 2 2 2 2 2 2 2 2 2 Chromium 0 0 0 0 28.5 28.5 28.5 26 26 26 26 26 Copper 25 25 25 39 11.7 11.7 11.7 40 40 40 40 40 Lead 5 5 5 5 5 5 5 5 5 5 5 5 Mercury 0.4 0.4 0.4 0.6 0.4 0.4 0.4 0.4 0.4 0.4 0.4 0.4 Molyb- denum enum 5 5 5 5 5 5 5 15 15 15 15 15 Nickel 22 22 22 62 12.6 12.6 12.6 12.4 12.4 12.4 12.4 12.4 Seleniuml 5 1 5 1 5 1 5 1 5 5 5 5 5 5 5 1 5 Zinc 216 216 216 330 159 159 159 395 395 395 395 395 Total Phos- horus 1190 1190 1190 615 1000 1000 1000 3440 3440 3440 3440 3440 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): ;+ o ' Y = .j 0 o 0.2524 0.2484 0.0748 0.475 0.348 0.4897 0.1812 0.0381 0.0236 0.0227 0.0035 0.0391 Arsenic 0.0015 0.0015 0.0004 0.0029 0.0021 0.0029 0.0011 0.0002 0.0001 0.0001 2E-05 0.0002 0.0132 Cadmium 0.001 0.001 0.0003 0.0019 0.0014 0.002 0.0007 0.0002 9E-05 9E-05 1 E-05 0.0002 0.0088 hromiu 0 0 0 0 0.0198 0.0279 0.0103 0.002 0.0012 0.0012 0.0002 0.002 0.0647 Copper 0.0126 0.0124 0.0037 0.0371 0.0081 0.0115 0.0042 0.003 0.0019 0.0018 0.0003 0.0031 0.0998 Lead 0.0025 0.0025 0.0007 0.0048 0.0035 0.0049 0.0018 0.0004 0.0002 0.0002 4E-05 0.0004 0.022 Mercury 0.0002 0.0002 6E-05 0.0006 0.0003 0.0004 0.0001 3E-05 2E-05 2E-05 3E-06 3E-05 0.0019 Molyb- 0.0025 0.0025 0.0007 0.0048 0.0035 0.0049 0.0018 0.0011 0.0007 0.0007 0.0001 0.0012 0.0245 denum Nickel 0.0111 0.0109 0.0033 0.0589 0.0088 0.0123 0.0046 0.0009 0.0006 0.0006 9E-05 0.001 0.1131 Selenium 0.0025 0.0025 0.0007 0.0048 0.0035 1 0.00491 0.0018 1 0.0004 0.0002 0.0002 4E-05 1 0.0004 0.022 Zinc 0.109 0.1073 1 0.03231 6.3135l 0.11071 0.15571 0.05761 0.0301 1 0.0186 10.0179 0.0028 0.0309 1 0.9865 Total Phos- 0.6007 0.5912 0.178 0.5843 0.696 0.9794 0.3624 0.2621 0.1624 0.1562 0.0241 0.269 4'.8657 horuS "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" 48�� efz `:.., .2-lazI Sigt ture of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report 11-J Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 3.53396 Permit#: WO0004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 3.4 Acres Permitted: 3.4 Site #: S Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date 1/4/16 1/4116 1/4/16 11/3/17 1113/16 11/3/16 %Solids 2.87 2.87 2.87 0.45 0.45 0.45 Arsenic 3 3 3 3 3 3 Cadmium 2 2 2 2 2 2 Chromium 0 0 0 26 26 26 Copper 25 25 25 40 40 40 Lead 5 5 5 5 5 5 Mercury 0.4 0.4 0.4 0.4 0.4 0.4 Molyb- denum 5 5 5 15 15 15 Nickel 22 22 22 12.4 12.4 12.4 Selenium 5 1 5 5 5 5 5 Zinc 216 216 216 395 395 395 Total Phos- horus 1190 1I90 1190 3440 3440 3440 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): o < a C7 0 m ^ n D o 0.2015 0.2368 0.3895 0.0754 0.0474 0.0888 Arsenic 0.0012 0.0014 0.0023 0.0005 0.0003 0.0005 0 0 0 0 0 0 0.0062 Cadmium 0.0008 0.0009 0.0016 0.0003 0.0002 0.0004 0 0 0 0 0 0 0.0042 hromiunj 0 1 0 0 1 0.0039 0.0025 1 0.00461 0 0 1 0 0 0 1 0 0.011 Copper 0.0101 0.0118 0.0195 0.006 0.0038 0.0071 0 0 0 0 0 0 0.0583 Lead 0.002 0.0024 0.0039 0.0008 0.0005 0.0009 0 0 0 0 0 0 0.0104 Mercury 0.0002 0.0002 0.0003 6E-05 4E-05 7E-05 0 0 0 0 0 0 0.0008 Molyb- 0.002 0.0024 0.0039 0.0023 0.0014 0.0027 0 0 0 0 0 0 0.0146 denum Nickel 0.0089 0.0104 0.0171 0.0019 0.0012 0.0022 0 0 0 0 0 0 0.0417 Selenium 0.002 0.0024 0.0039 0.0008 0.0005 0.0009 0 0 0 0 0 0 0.0104 Zinc 1 0.087 0.1023 0.1683 1 0.05961 0.03741 0.07021 0 0 0 0 0 0 0.5248 Total Phos- 0.4796 0.5636 0.927 0.5188 0.3261 0.6109 0 0 0 0 0 0 3.426 horuS "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Si tature of Land Applier Date ` See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report 0, Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 5.37395 Permit #: W00004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 2.3 Acres Permitted: 2.3 Site #: S Field #: 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): moo, ' ad m9 0 0 o 0.9968 1.3397 Arsenic 0.006 0.008 0 0 0 0 0 0 0 0 0 0 0.014 Cadmium 0.004 0.0054 0 0 0 0 0 0 0 0 0 0 0.0093 Chromival 0.0568 0.0764 0 1 0 0 1 0 1 0 0 1 0 1 0 0 1 0 0.1332 Copper 0.0233 0.0313 0 0 0 0 0 0 0 0 0 0 0.0547 Lead 0.01 0.0134 0 0 0 0 0 0 0 0 0 0 0.0234 Mercury 0.0008 0.0011 0 0 0 0 0 0 0 0 0 0 0.0019 Molyb- 0.01 0.0134 0 0 0 0 0 0 0 0 0 0 0.0234 denum Nickel 0.0251 0.0338 0 0 0 0 0 0 0 0 0 0 0.0589 Selenium 0.01 0.0134 0 0 0 0 0 0 0 0 0 0 0.0234 Zinc 1 0.317 1 0.426 0 0 0 0 0 0 0 0 0 0 0.743 Total Phos- 1.9936 2.6794 0 0 0 0 0 0 0 0 0 0 4.673 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signemre of Land Applier Date " See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report } \_J Facility Name: Campbell Soup Supply Company Total Dry Tons Applied (Annual): 12.645 Permit #: W00004893 Cation Exchange Capacity (non 503 only): >5.0 Operator: Campbell Soup Supply Company Owner: Campbell Soup Supply Company Acres Used: 2.5 Acres Permitted: 2.5 Site #: S Field #: 7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): (� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Sample or Com- posite Date 9/23/16 9/23/16 9/23/16 9/23/16 %Solids 6.16 6.16 6.16 6.16 Arsenic 3 3 3 3 Cadmium 2 2 2 2 Chromium 28.5 28.5 28.5 28.5 Copper 11.7 11.7 11.7 11.7 Lead 5 5 5 5 Mercury 0.4 0.4 0.4 0.4 Molyb- denum 5 5 5 5 Nickel 12.6 12.6 12.6 12.6 Selenium 5 1 5 5 1 5 Zinc 159 159 159 159 Total Phos- horns 1000 1000 1000 1000 -e a o o > EL -i m o 7 c ^ w a 0 1.4387 1.6134 0.8481 1.1578 Arsenic 0.0086 0.0097 0.0051 0.0069 0 0 0 0 0 0 0 0 0.0303 Cadmium 0.0058 0.0065 0.0034 0.0046 0 0 0 0 0 0 0 0 0.0202 Chromiunl 0.082 1 0.092 0.0483 1 0.066 0 0 1 0 0 1 0 0 1 0 1 0 0.2883 Copper 0.0337 0.0378 0.0198 0.0271 0 0 0 0 0 0 0 0 0.1184 Lead 0.0144 0.0161 0.0085 0.0116 0 0 0 0 0 0 0 0 0.0506 Mercury 0.0012 0.0013 0.0007 0.0009 0 0 0 0 0 0 0 0 0.004 Molyb- 0.0144 0.0161 0.0085 0.0116 0 0 0 0 0 0 0 0 0.0506 denum Nickel 0.0363 0.0407 0.0214 0.0292 0 0 0 0 0 0 0 0 0.1275 Selenium 0.0144 0.0161 0.0085 0.0116 0 0 0 0 0 0 0 0 0.0506 Zinc 0.4575 0.5131 0.2697 0.3682 0 0 0 0 0 0 0 0 1.6084 Total Phos- 2.8774 3.2268 1.6962 2.3156 0 0 0 0 0 0 0 0 10.116 horns "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Si azure of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form Annual Land Application Field Summary l ANNUAL LAND APPLICATION r,jZLD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: W00004893 Annual Dry Tons Applied: 22.91167511 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Site #: S Field #: I Acres Utilized: 5.1 Cation Exchange Capacity (non 503): >5.0 Acres Permitted: 5.1 o ,�, °o O Specify Totals per Acre % Solid s Dry Tons Per Acre Residual Sources Summarize (Summarize) 1 e Cond. Dry, Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- till- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 Gal. Cu.Yd. ;:: Report Totals in Gal. Crop 1 Crop 2 Jan 26 16057 3148.4 2.87 0.376801118 DAF Dry 0 S 0.5 0.4 25100 2090 2 ####### 7.72518 Rye Gras 1 Mar 24 10554 2069.4 2.87 1 0.247665131 DAF Dry 0 S 0.5 0.4 25100 1 2090 2 ####### 5.07763 Rye Gras 2 Apr 26 15244 2989 6.61 0.823884398 DAF Dry 0 S 0.5 0.4 14100 1820 2 9.59661 ####### Bermuda 3 Ju129 14,602 2863.1 6.16 0.735459793 DAF Dry 0 S 0.5 0.4 13800 1460 2 8.33717 ####### Bermudal 4 Sep 9 5,964 1169.4 6.16 0.300389139 DAF Dry 0 S 0.5 0.4 13800 1460 2 3.40521 ####### Bermuda 5 Sep 19 19,734 3869.4 6.16 0.993943539 DAF Dry 0 S 0.5 0.4 13800 1460 2 11.2673 ####### Bermuda 6 Sep 20 5,434 1065.5 6.16 0.273694598 DAF Dry 1 0 S 0.5 0.4 13800 1460 2 3.1026 ####### Bermuda 7 Sep 28 14,705 2883.3 6.16 0.7406476 DAF Dry 0 S 0.5 0.4 13800 1460 2 8.39598 ####### Bermuda 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 EEL 120058 0 0 0 0 12 TOTALS: <:i:?::::: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN I PAN 2 Lime A lied Annual Ibs/acre 0.026955 0.01797 0.17351 0.16672 0.04493 0.00392 0.04493 0.20635 0.04493 1.78158 8.58791 44.1049 t2.8028 Date Ibs/ac Current Cumulative Ibs/ac 0.026955 0.01797 0.17351 0.16672 0.04493 0.00392 0.04493 0.20635 0.04493 1.78158 :>::::::::::::: ':: ::::::: :::::::: ... 50 0 Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit I st/2nd Cropl00 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." G`Bim� /e egZ., 1-/3 -lq *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loadina Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1. DENR FORM FSF (5/2003) t ANNUAL LAND APPLICATIO}y,`_ "GELD SUMMARY FORM ' PLEj.a - f`MAKE A COPY OF THIS BLANK FORM TO BE COMP`,, 2ED AND SUBMITTED FOR EACH APPLICATION FIEL-,` PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: WQ000493 Annual Dry Tons Applied: 2.901882984 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Cation Exchange Capacity (non 503): >5.0 Site #: S Field #: 2 Acres Utilized: 8.4 Acres Permitted: 8.4 s a 0 Ca Specify Totals Totals Per Acre %0 Solid s Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry, Wet, Moist Inches Precip. Past 24 Hrs. A li pp cation Meth- od* Vola- tili- zation Rate** Miner- all- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Aug 23 11,297 1344.9 6.16 0.34546226 DAF Dry 0 S 0.5 0.4 13800 1460 6.19 3.91906 ####### Bermuda 1 2 3 4 5 6 7 8 9 10 11 12 TOTALS: 1345 i` :: i : As Cd Cr Cu Pb . Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annual Ibs/acre 0.002073 0.00138 0.01969 0.00808 0.00346 0.00028 0.00346 0.00871 0.00346 0.10987 0.691 3.919061 0 Date Ibs/ac Current Cumulativelbs/ac 0.002073 0.00138 0.01969 0.008081 0.00346 0.00028 0.00346 0.00871 1 0.00346 0.10987:;c::;:;i;ij:..:;;.:i:.:. .. ."" : , . . 299 50 0 Prior Years Cumulative Ibs/ae Permitted C. P. L. R.*** Permit PAN Limit 1 sU2nd Crop p "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Yiimri Z. 1&kg-1 2-/3- /7 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column .# 1. ANNUAL LAND APPLICATIOI�r-, GELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: W00004893 Annual Dry Tons Applied: 32.7053 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Cation Exchange Capacity (non 503): >5.0 Site #: S Field #: 3 Acres Utilized: 26 Acres Permitted: 26 x [ 0 a & q S eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) Site Cond. D Wet' Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN I PAN 2 Must Select Crop I or Crop 2 Gal. Cu.Yd. Report Totals in Gal. Crop 1 Crop 2 Jan 5 19719 758.42 2.87 0.090767315 DAF Dry 0 S 0.5 0.4 25100 2090 2 1.86091 #####4# Pines 1 Feb 18 21016 808.31 2.87 0.096737456 DAF Dry 0 S 0.5 0.4 25100 2090 2 1.98331 ####### Pines 2 Feb 26 6062 233.15 2.87 0.027903619 DAF Dry 0 S 0.5 0.4 25100 2090 2 0.57208 ####### Pines 3 Feb 27 17079 656.88 2.87 0.078615294 DAF Dry 0 S 0.5 0.4 25100 2090 2 1.61177 ####### Pines 4 Mar 8 19573 752.81 2.87 0.090095272 DAF Dry 0 S 0.5 0.4 25100 2090 2 1.84713 ##gig # Pines 5 Mar 17 10628 408.77 2.87 0.048921093 DAF Dry 0 S 0.5 0.4 25100 2090 2 1.00298 ####### Pines 6 Mar 18 7320 281.54 2.87 0.033694242 DAF Dry 0 S 0.5 0.4 25100 2090 2 0.6908 ####### Pines 1 7 May 11 1 12662 1 487.00 6.61 0.134235219 DAF Dry 1 0 S 0.5 0.4 14100 1820 2 1 1.56357 ####### Pines 8 May 26 19820 762.31 6.61 0.210120205 DAF Dry 0 S 0.5 0.4 14100 1820 2 2.44748 ####### Pines 9 Jun 9/2C 36489 1403.42 6.61 0.386835327 DAF Dry 0RO.O013 0.5 0.4 14100 1820 2 4.50586 ####### Pines 10 Oct 17 16836 647.54 0.45 0.612151059 DAF Dry 0 0.5 0.4 30400 17400 2 0.33785 ####### Pines 11 Dec 2-2 66257 2548.35 0.45 0.047819716 DAF Dry 0 0.5 0.4 30400 17400 2 1.32958 ####### Pines 12 TOTALS: 9749 <i:<i>? As Cd Cr Cu PbMo Ni Se Zn P PAN I PAN 2 Lime Applied Annual Ibs/acre 0.0075468 0.00503 0.00312 0.08516 0.01258 0.01378 0.I1268 0.01258 0.73154 2.4228 19.7533 0 Date Ibs/acCurrent Cumulative Ibs/ac 0.0075468 0.00503 0.00312 0.08516 0.01258 0.01378 0.11268 0.01258 0.73154::::::::::::::::::::::::::::::::::::::::::::::::::: .:.................... :; 60 0 Prior Years Cumulative Ibs/ac Permitted C. P. L. R.*** Permit PAN Limit 1st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4 ie�mc0 Z-/3 /% *Application Method: S -Surface, IN -Injection, INC -Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incoraoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so thisinformation needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1. F PLEk� ' MAKE A COPY OF THIS BLANK FORM TO BE COMP c � gl'ED AND SUBMITTED FOR EACH APPLICATION FIEi:L. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: WQ0004893 Annual Dry Tons Applied: 19.99005676 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Cation Exchange Capacity (non 503): >5.0 Site #: S Field #: 4 Acres Utilized: 9.1 Acres Permitted: 9.1 o „ c o OReport S ec fv Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) Site Cond. Dry We,, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo ma- Ni- trogen Ni- trate and Nitrite PAN I PAN 2 Must Select Crop I or Crop 2 Gal. Cu.Yd. Totals in Gal.ict Crop 1 Crop 2 Jan 12 19192 2109 2.87 0.252404326 DAF Dry 0 S 0.5 0.4 25100 2090 2 5.17479 ####### Pines I Feb 2 1 18890 2075.8 1 2.87 1 0.248432562 DAF Dry 0 S 0.5 0.4 25100 1 2090 2 5.09336 4###### Pines 2 Feb 9 5691 625.38 2.87 0.074845405 DAF Dry 0 S 0.5 0.4 25100 2090 2 1.53448 ####### Pines 3 Apr 13 15683 1723.4 6.61 0.475034623 DAF Dry 0 S 0.5 0.4 14100 1820 2 5.5332 ####### Pines 4 Ju17 12329 1354.8 6.16 0.348019218 DAF Dry 0 S 0.5 0.4 13800 1460 2 3.94515 ####### Pines 5 Jul 19 17348 1906.4 6.16 0.489694006 DAF Dry 0 S 0.5 0.4 13800 1460 2 5.55117 ####### Pines 6 Jul21 6420 705.49 6.16 0.181221785 DAF Dry 6 S 0.5 0.4 13800 1460 2 2.05433 ####### Pines 7 Oct 26 18494 2032.3 0.45 0.038136254 DAF Dry 0 S 0.5 0.4 30400 17400 2 1.06034 ###4### Pines 8 Nov 3 1 11458 1259.1 1 0.45 1 0.023627403 DAF Dry 1 0 S 0.5 1 0.4 30400 1 17400 2 10.65694 ####### Pines 9 Nov 9 11029 1212 0.45 0.022742768 DAF Dry 0 S 0.5 0.4 30400 17400 2 0.63234 #4#494# Pines 10 Nov 151 1693 186.04 0.45 0.003491115 DAF Dry 0 S 0.5 0.4 30400 17400 2 0.09707 ####### Pines 11 Nov 23 18942 2081.5 0.45 0.039060069 DAF Dry 0 S 0.5 0.4 30400 17400 2 1.08603 ####### Pines 12 TOTALS: 17271 <<?<::<:: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN I PAN 2 Lime Applied Annuallbs/acre 0.013179 0.00879 0.06468 0.09983 0.02197 0.00195 0.02451 0.11305 0.02197 0.9865 4.86574 32.4192 0 Date Ibs/ac Current Cumulative Ibs/ac 0.013179 0.00879 0.06468 0.09983 0.02197 0.00195 0.02451 0.11305 0.02197 0.9865 >: :;::..:.........•.........:.. 50 0 Prior Years Cumulative Ibs/ac Permitted C. P. L. R.*** Permit PAN Limit Ist/2nd Crop110 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ,�,z� t" /CV,4 2-/✓ 17 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorporation -1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column 9 1. ANNUAL LAND APPLICATIOI(_s 6'>;LD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: WQ0004893 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Site #: S Field #: 5 Acres Utilized: 3.4 Annual Dry Tons Applied: 3.533671344 Cation Exchange Capacity (non 503): >5.0 Acres Permitted: 3.4 o „ e Q> S eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry Wets Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- nation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop I or Crop 2 Gal. Cu.Yd. Totals T Gal. Crop 1 Crop 2 Jan 19 5724 1683.53 2.87 0.201483116 DAF Dry 0 S 0.5 0.4 25100 2090 2 4###### 4.13081 Rye 1 Jan 26 6727 1978.53 2.87 0.236788421 DAF Dry 0 S 0.5 0.4 25100 2090 2 ####### 4.85464 Rye 2 Feb 9 11065 3254.41 2.87 0.389484746 DAF Dry 0 S 0.5 0.4 25100 2090 2 ####### 7.98522 Rye 3 Oct 13655 4016.18 0.45 0.075363551 DAF Dry 0 S 0.5 0.4 30400 17400 2 #4####4 2.09541 Rye 4 Nov 9 8595 2527.94 0.45 0.047436816 DAF Dry 0 S 0.5 0.4 30400 17400 2 ####### 1.31893 Rye 5 Nov 15 16082 4730.00 0.45 0.08875845 DAF Dry 0 S 0.5 0.4 30400 17400 2 ####### 2.46784 Rye 6 0 0 7 0 0 8 0 0 9 0 0 10 0 0 11 0 0 12 TOTALS: 18191 : . ` : As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.0062364 0.0041E 0.011 0.05832 0.01039 0.00083 0.01463 0.04167 0.01039 0.52477 3.42597 0 22.8528 Date Ibs/ac :::: Current Cumulative Ibs/ac 0.0062364 0.00416 0.011 0.05832 0.01039 0.00083 0.01463 0.04167 0.01039 0.52477:;:::::::::::::::::::::::::::::;:::`:<:: 1t0 50 0 Prior Years Cumulative Ibs/ac Permitted C. P. L. R.*** Permi r t PAN Limit lst/2nd Crop P "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 1-10, 1110eZ1_ -4- /3-17 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incornoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loadine Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this informationneeds to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. tr ANNUAL LAND APPLICATIOI' ,� ELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: W00004893 Annual Dry Tons Applied: 5.374019112 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Cation Exchange Capacity (non 503): >5.0 Site #: Field #: Acres Utilized: 2.3 Acres Permitted: 2.3 $ Q S eci Totals per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) 1 e Coe Dry, Wet, Inches Precip. past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- all- zation Rate TKN - Ammo nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 Gal. Cu.Yd. i Report Totals in Gal. Crop 1 Crop 2 Aug 30 8926 3880.9 6.16 0.996886727 DAF Dry 0 S 0.5 0.4 13800 1460 2 11.3007 ####### Bermuda 1 Sep 9 1 11995 1 5215.2 6.16 1 1.339643322 DAF Dry 0 S 0.5 0.4 13800 1460 2 15.1862 ####### Bermuda 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 1 0 1 1 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 l2 TOTALS: 9096 :?<:`z>;:: As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN I PAN 2 Lime A lied Annual lbs/acre 0.014019 0.00935 0.13318 0.05467 0.02337 0.00187 0.02337 0.05888 0.02337 0.74301 4.673 26.4869 0 Date lbs/ac Current Cumulative lbs/ac 0.0I4019 0.00935 0.13318 0.05467 0.02337 0.00187 0.02337 0.05888 0.02337 0.74301 :::5 ....:..........:: ' ::::::... 0 Prior Years Cumulative Ibs/ac Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop 224 50 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." SZ C!n� 2 _/3-/9 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate * * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. 'ff ANNUAL LAND APPLICATIO.. %:ELD SUMMARY FORM t PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Campbell Soup Supply Company Permit #: WQ0004893 Annual Dry Tons Applied: 12.64529482 Owner: Campbell Soup Supply Company Operator: Campbell Soup Supply Company Cation Exchange Capacity (non 503): >5.0 Site #: S Field #: 7 Acres Utilized: 2.5 Acres Permitted: 2.5 o Y „ e O- o S eci Totals Per Acre % Solid s Dry Tons Per Acre Residual Sources (Summarize) t e Cond. Dry, Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Vola- tili- zation Rate** Miner- ali- zation Rate TKN Ammo nia- Ni- trogen Ni- irate and Nitrite PAN 1 PAN 2 Must Select Crop f or Crop 2 Gal. Cu.Yd. >: Report in Gal. Crop 1 Crop 2 Aug 8 14002 5600.8 6.16 1.438688698 DAF Dry 0 S 0.5 0.4 13800 1460 2 16.309 ####### Bermuda 1 Aug 16 15703 6281.2 6.16 1 1.613464406 DAF Dry 0 S 0.5 0.4 13800 1460 2 18.2902 ####### Bermuda 2 Aug 23 8254 3301.6 6.16 0.848088595 DAF Dry 0 S 0.5 0.4 13800 1460 2 9.61393 ####### Bermuda 3 Aug 30 11269 4507.6 6.16 1.157876227 DAF Dry 0 S 0.5 0.4 13800 1460 2 13.1257 ####### Bermuda 4 5 6 7 8 0 9 0 10 0 11 0 12 TOTALS: 19691 :.:.:.:.:.::: As Cd Cr Cu Pb Hg o Ni Se Zn P PAN 1 PAN 2 Lime A lied Annuallbs/acre 0.030348 0.02023 0.28831 0,11836 0.05058 0.00405 0.05058 0.12746 0.05058 1.60844 10.116 57.3388 0 Date Ibs/ac Current Cumulative Ibs/ac 0.030348 0.02023 0.28831 0.11836 0.05058 0.00405 0.05058 0.12746 0.05058 1.60844 ::::::::::'>:::2:::::::::> ::::: :::::::::::::: 0 224 50 0 Prior Years Cumulative lbs/ac 1 Permitted C. P. L. R.*** PermitPAN Limit 1sU2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1. Residual Analysis Lab Sheets \ -I Page: IV 2 Report Number: 16-005-9202 Account Number: 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS, NC 28377 WaY- oint.� ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com project: CAMPBELL DAF SLUDGE 1ST QTR NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/4/2016 09:00:00 Lab Number: 66007 Date Received: 01/05/2016 00:00 Sample Id : M-9 DAF Date Reported: 01/28/2016 Total Solids'" 2.87 28700 100.0 JM 01/05/2016 16:00 SM-254OG Moisture * 97.13 100.0 JM 01/05/2016 16:00 SM-2640G Total Keldahl Nitrogen 2.51 25100 10.0 JM 01/06/2016 08:05 SM-4500-NH3C-TKN Total Phosphorus 0.12 1190 100 KM 01/06/2016 12:31 SW 6010C Total Potassium 0.13 1310 100 KM 01/06/2016 12:31 SW 6010C Total Calcium 0.47 4710 100 KM 01/06/2016 12:31 SW 6010C Total Magnesium 0.06 579 100 KM 01/06/2016 12:31 SW 6010C Total Sodium 0.30 2980 100 KM 01/06/2016 12:31 SW 6010C Total Aluminum 700 100 KM 011061201612:31 SW6010C Total Copper 25 5 KM 01/06/2016 12:31 SW 6010C Total Zinc 216 5 KM 01/06/2016 12:31 SW 6010C Ammonia Nitrogen 0.21 2090 10.0 JM 01/06/2016 08:05 SM-4500-NI3C Organic N 2.30 23010 10.0 01/06/2016 08:05, CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 01/06/2016 08:05 SM-450ONO3F Total Cadmium <2.0 2.0 KM 01/06/2016 12:31 SW 6010C Total NicKel 22 5 KM 01/06/2016 12:31 SW 6010C Total Lead <5 5 KM 01/06/2016 12:31 SW 6010C Total Arsenic <3.0 3.0 KMM 01106/201612:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. A Ourreports andletters are forthe exclusive and confidential use ofourclients, and maynot be reproducedin whole orpart nor may any reference be made to the work; the results, or the companyin any advertising, news release, orotherpublic announcements without obtaining ourpdor written authorization. ` Debbie Holt Page: 2 of 2 Report Number: 16-005-9202 Account Number. 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS, NC 28377 • Waypoi nt 7621 ain 804-7 Road, Richmond, 27 -6446 Main 804-743-9401 0Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com Project: CAMPBELL DAF SLUDGE 1ST QTR NO CERT#257 REPORT OFANA_LYS/S Date Sampled: 1/4/2016 09:00:00 Lab Number: 66007 - Date Received: 01/05/2016 00:00 Sample Id: M-9 DAF ' " Date Reported: 01/28/2016, Total Mercury <0.4 0.4 KMM 01/27/2016 09:00 SW-7471B Total Selenium <5.0 5.0 KMM 01/06/2016 12:31 SW 6010C pH (Standard Units)4.53 2.00 JM 01/06/2016 08:05 SW-9045D Total Molybdenum <5 5 KMM 01/06/2016 12:31 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE MSD WAS OUT OF LIMITS FOR "NH4-N". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Ni". ALL OTHER QC DATA IS ACCEPTABLE. NOTE: "As", "Hg", Wo", AND "Se" ADDED 1/25116 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourreports and letters are for the exclusive and confidenfial use of our clients, and may not be reproduced in whole orpart, nor may any reference be made to the work, the results, or the company in any advertising news release, or other public announcements without obtaining our prior written authorization. Debbie Holt ' Page: 1 cf 2 Report Number. 16-096-9204 Account Number: 00327 ® 7621 Whitepine Road, Richmond, VA 23237 Waypoint_ Main 804-743-9401e Fax 804-271-6446 ANALYTICAL www.waypointanalydcal.com Send To: EHC Inc. project: CAMPBELL SOUP 2ND OTR DAF SLUDGE PO Box 902 NC CERT#257 RED SPRINGS, NC 28377 REPORT OFANALYSIS Date Sampled: 414/201610:00:00 Lab Number: 56541 Date Received: 04ID512616 00:00 Sample Id: DAF Date Reported: 05/12/2016 Total Solids 6.61 66100 100.0 JM 04/05/2016 15:00 SM-2540G Moisture' 93.39 100.0 JM '04/05201615:00 SM-2540G T `al Kjeldahl Nitrogen 1.41 14100 10.0 JM 04/06/2016 08:39 SM4500-NH3C-TKN r` /A Phosphorus 0.06 615 100 KM 04107/201611:01 SW6010C ,,al Potassium 0.02 178 100 KM 04/07/2016 11:01 SW6010C Total Sulfur 0A3 1290 100 KMM 041071201611:01 SW6010C Total Calcium 0.15 1540 100 KM 04107201611:01 SW6010C Total Magnesium 0.02 205 10D KM 041071201611:01 SW6010C Total Sodium 0.08 816 100 KM 041071201611:01 SW6010C Total Iron 3120 100 KMM 04/07201611:01 SW6010C Total Aluminum 818 100 KM 04/07/201611:01 SW6010C Total Manganese 30 5 KMM 04/07/2016'11:01 SW6010C Total Copper 39 5 KM 04/072016 11:01 SW6010C Total Zinc 330 5 KM 04/07201611:01 SW6010C Ammonia Nitrogen 0.18 1820 10.0 JM 041061201608:39 SM4500-NH3C Organic 1.23 12280 10.0 04/061201608:39 CALCULATION Nitrate+Nitrite-N <2.00 2.00 JM 04106/201608:35 SM-450ONO3F Total Cadmium <2.0 2.0 KM '041072016 11:01 SW6010C All values are on a dry weight basis except as noted by asterisk Detecgon limit on all N series is on a Wet basis. mfe Owmpandlef mare lathe mx uslw wdmnfidenfial use Oourcllenfs wdmaymxbereproducedln hme paq mn normaymymtmbe made 'lrtr wo- '' lS fo Mex,k, am.l .us, rcthe ampanyin any c*emtm,, nmw mlemo,, momerpub6c ampuncemmfs withoutobfaining owprfwwr mauNOzwron. Debbie Holt 'Page: 2 of 2 Report Number. 16-096-9204 Account Number: 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS, NC 28377 Lab Number: 56541 Sample Id: DAF • Waypoent_ 7621 ain804-73-9401l-Fax 80,271-6=7 Main 804-743-9401 °Fax 804-271fi446 ANALYTICAL www.waypotntanalydcatcom Project: CAMPBELL SOUP 2ND OTR DAF SLUDGE NO CERT#257 REPORT OFANALYSIS, Date Sampled: 4/4/201610:00:00 Date Received: 04/05/2016 00:00 Date Reported: 05/12/2016 Total Chromium 115 Total Nickel 62 'i tal Lead 5 �1WAmenic 43.0 rebel Mercury 0.6 Total Selenium <5.0 PH (Standard Units) • 4.48 Total Molybdenum <5 Sodium Absorption • 5.17 Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. METALS ADDED 05/04/16 5 KMM 041071201611:01 SW 6010C 5 KM 04107/201611:01 SW 6010C 5 KM 041071201611:01 SW 6010C 3.0 KMM 041071201611:01 SW 6010C 0.4 KMM 051031201609:00 SW-7471B 5.0 KMM 041071201611:01 SW 6010C .2.00 JM 04106/201608:24 SW-9045D 5 KMM 04/07/201611:01 SW 6010C CALCULATION All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. eurrepertsandleders era forth¢ aWacwe and.ffdenff.1 use orour dl.Ws andmayeof Eerepoducedln whole crpart rwrmayanyreferenre hemade N the work, Naresulta, o-the wmpenyln anyacVed eg, newsrelease, crotherpublk sneowcements withoutobleAning curplorwdm avhedieen. Debbie Holt I�/ T_AL I IIII �p pp IIII II'' ''''II A&L Easters II��I���I�I��u II��II������I��IIIIu���uIIIII�IIWI����l��l0 1e< ® 7621 Whitcpinc Road Riclunond VA 23237 TcL• 804-743-9401 EHC Inc. 12:52:43 - - CAWBELL SOUP 2ND OTR DAF SLUDGE Account y Customer Informa - _ Submitted By_ Project ea :21=12aQ Sam le Information Sample'ID Lab Number (Lab Use -- _ _ Collection Information -- - Container Information- Please Check. Desired Tests Only) Type Date Time. Number of Bottles Type Type Volume SL7 SL2Volatile 503 .Nitrogen _ CCE Ag ClCI ile ' Others, Metals Series Solids D _Grab Glass °Z omposite �%�y�/� /O = 2 Plastic —pint qt X _ Grab —OZ Com osite _Glass _ Plastic —pint Grab Glass — O2 Come Plastic G2b _ t _ Glass — °Z Com site _ Plastic —Pint t R in uished.S ; Si nature Date Time^ Recely SI nature ,Date . _Time _ Test Packa a Details - SLI: Total Solids (Moisture) Total KTelmuin Nilmgen, Pbasphunu and Potassium .S Special Instructions or Remarks - SL2: Buie Tot SLI plus Suit", Calcium, Magnesium.Sodium, Iron. Aluminum. Manganese, Copper And Zinc 503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead. Nickel, Selenium. (Copper & Zinc included in SL2) Nitrogen Series: Test KjcldahL Ammonium. Nitrate R Organic Niuog . CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) Page: 1 of 2 Report Number. 16-267-0227 Account Number. 00327 Send To: EHC Inc. PO Box 902 Red Springs • NC 28377 Waypoint.0 ANALYTICAL Project: DAF ,NC Cart #257 7621 Whitepine Road, Richmond, VA Z3237 Main 804-743-9401 ° Fax 804-271-6446 www.waypuintanalydcal.com 3rd. QV. 51J,j,, REPORT OFANALYSIS Date Sampled: 9/22/201612:25:00 Lab Number: 59891 Date Received: 09/23/2016 00:00 Sample Id : DAF Date Reported: 10/05/2016 Total Solids 6.16 61600 100.0 JM 09/23/2016 13:45 SM-254OG Moisture' 93.83 100.0 JM 09/23/201613:45 SM-254OG =�;;lal Kjeldahl Nitrogen 1.38 13800 10.0 JM 09/26/2016 09:50 - SM-0500-NH3C-TKN let Phosphorus 0.10 1000 100 MOS 0929/2016 13:03 6010C total Potassium 0.08 823 100 MOS 09/30/2016 09A6 6010C Total Sulfur 0.08 847 100 MOS 09/29/2016 13:03 6010C Total Calcium 0.11 1120 100 MOS 09/29/2016 13:03 6010C Total Magnesium 0.03 270 100 MOS 09/29/2016 13:03 6010C Total Sodium 0.10 982 100 MOS 09291201613:03 6010C Total Iron 1780 100 MOS 09/30/201609:46 6010C Total Aluminum 669 100 MOS 0929/201613:03 6010C Total Manganese 29.1 5.00 MOS 10/04/201616:39 6010C Total Copper 11.7 5.00 MOS 0929201613:03 6010C Total Zinc 159 5.00 MOS 09130201609A6 6010C Ammonia Nitrogen 0.15 1460 10.0 JM 09261201609:50 SM4500-NH3C Organic 1.23 12340 10.0 09261201609:50 CALCULATION Nitrate+Nitrite-N <6.19 6.19 SJB 091271201615:36 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. unrrer••.•+samrz.-.9n mz rvna rn-ya;nY.w.ala�.'a..•o-re orau.n..:es aRa.Ry'xolmr�ui .,.ru.arvaewPnn mr.,er'amM .m[Rnda ',lI'L(ll�fLOW(,/'f lu C.� rt.v :.«.v 4 n ,v .m •, n m any' a�rt•rtrsny RnrrsrcMa�n w.M1:xrFuElxamvunu•Rru: mlMvu+Etauury.wPenv MT�^s'BW' we.n;n Debbie Holt Laboratory Supervisor Page: 2 of 2. Report Number. 16-267-0227 Account Number. 00327 Send To: EHC Inc. PO Box 902 Red Springs, NC 28377 Lab Number: 59891 Sample Id : OAF Waypoint ANALYTICAL Project: DAF NC Cad #257 REPORT OFANALYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 w.vw.waypuintanalydcal.com Date Sampled: 9122/201612:25:00 Date Received:.09123/2016 00:00 Dale Reported: 10/05/2016 Total Cadmium <2.00 2.00 MOS 09/29/2016 13:03 6010C Total Chromium 28.5 5.00 MOS 09/301201609:46 6010C V'4:al Nickel 12.6 5.00 MOS 09129/201613:03 6010C -al Lead <5.00 5.00 MOS 09/291201613:03 6010C mtalArsenic <3,00 3.00 MOS 09129/201613:03 6010C Total Mercury < A00 0.400 KMM 09282016 11:06 SW-74718 Total Selenium <5.00 5.00 MOS 091301201609A6 6010C pH (Standard Units) 3.48 JM 091261201609:30 SW-9045D Total Molybdenum <5.00 5.00 MOS 0929/2016 13:03 6010C Sodium Absorption' 6.81 CALCULATION Comments: BAR, SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Un.-reM'1p xrar rt':r�:.,a hu,l,� ern,enx a.T1 inM1Ycn1::Y 4»+u'an �mi andmrry m�l6e�ry.re4�Nin W,de wean. rvrmarany r� exa 0emece lu Y:u,rWf, p.ereews_ v Il=o 4�npany n a+ry'ehe+l%srt/ trc,rsrc�h\r. V-OlherpuHx antluuncera.'rl.: rrnMNCblSi4n) n:wjmv �!nr e,rnav,,r.�n+n Debbie Holt Laboratory Supervisor Jn _ SE1M I E:T � EH�����id���l�f g HC�01 DAF 13:12:12 7521 Wbilcpine Road Richmond VA; .i upportaleekaieastem.com Subrniftetl By ; - GhargeTo Copy '. .� To p ( 305kv�� 7at)� Fi-C Am�AAhW4- -rA f AC(,rAA A r t -. ` Lab Number, Collect_lo_ ;SaTple ID ,(Lab'Ose. L L2 UP Grab 1012?51z Type: n Volume '. SLi , SL2- 500 :.Nitrogen - ,. Metals "Series,' PH Glass _Plastic — Oz _pint Glass — oz Plastic —pint t Glass. T— oz Plastic —pint t Glass — pz Plastic —pint 1' _'rRelin 'ishedB .5 Si natdie ,. .:Date, ,- Time r =_ Recetved�B : 5l naturel� •��Date 4 - uuS 7DSlSW1 6%5) i ZZ lb l DO -' rrescracKa e,uelans SLI: Total Solids(Moistum)To KjcldWit Nivocen, Phosphorus and Potassium SL2: Basic Test SL l plus SulfurCalcium, MagnesimgSadium.Iron. Aluminum, Manganese, Copper And Zinc 503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenium. (Copper & Zinc included in SL2) Nitrogen Serick Total Kleldald. Ammonium. \iunlc & Organic Nitrogen, CCE; Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) i FRI.23 SEP 10:30A PRIORITY OVERNIGHT o o'i 7772 8371' 9066 i 't Lkk- M1iG.rim Y AccoWll # I �xj; ow lie G 30 Page: 1 of 2 Report Number. 16-308-0204 Account Number. 00327 Send To: EHC Inc. PO Box 902 Red Springs, NC 2B377 Waypoint_® 7621 644Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804.271-6 ANALYTICAL www.waypolntanalydcal.cum Project: Biosollds NC Cert#257 ' 1Lu. 6—W, REPORT OFANALVS/S Date sampled: 11/22016 10:45:00 Lab Number: 60507 Date Received: 11/032016 00,00 Sample Id: DAF Date Reported: 11/15/2016 Total Solids 0.45 4500 100.0' R D 11103/201615:15 SM-254OG Moisture' 99.54 100.0 R D 11/03/2016 15:15 SM-254OG Total.Keldahl Nitrogen 3.04 30400 10.0 JM 11/09/2016 09:55 SM-4500-NH3C-TKN Total Phosphorus 0.34 3440 100 SJB 111091201611:17 6010C gl Potassium 1.13 11300 100 SJB 11109/201611:17 6010C -,=/! al Sulfur 0.31 3140 100 SJB 11/09/2016 11:17 6010C Total Calcium 0.44 4390 100 SJB 11/092016 11:17 6010C Total Magnesium 0.12 1150 100 SJB 11109201611:17 6010C Total Sodium 1.68 .16800 100 SJB 11/09/201611:17 6010C Total Aluminum 2130 100 SJB 11/09/2016 11:17 6010C Total Manganese 44.0 5.00 SJB 11/092016 11:17 6010C Total Copper 40.0 5.00 SJB 11/09/2016 11:17 6010C Total Zinc 395 5.00 SJB 11/09/201611:17 6010C Ammonia Nitrogen 1.74 17400 10.0 JM 111041201609A5 SM-4500-NH3C Organic N 1.30 13000 10.0 11/04/2016 09:45 CALCULATION NitrateWrinte-N <1.00 1.00 SJB 11104201613:55 450oNO3F-2011 Total Cadmium <2.00 2.00 SJB 111091201611:17 6010C All values are on a dry weight basis except as noted by asterisk Detection limit on all N series is on a wet basis. Owrzpv:cara 4t:es av/a Ne exdv ne a:Conic'zr�auu o: xr C re,. a .Ya 6errroCseeinxMb aP•=" '^aYanyre.Y,trrce .lzmxw /D4/.�/�lc✓�'+-+-� bGb noY, ht rc�.:•a. b:ReepmflnyM e„yefvers+:7 nens re'easa.G omer{rvw annemamxnfa wlMufcalmn�,:v o,epeaxrc:e� amhonrmro� Debbie. Holt Laboratory Supervisor Page: 2 of 2 Report Number. 16-308-0204 Account Number..00327 Wayt�oints 7621 ain807n743-94 1-Fax nd-271- 2 ii 9 E � Maln 804-743-9401 ° Faz 804-271-6666 ANALYTICAL www.waypointanalydcal!com Send To: EHC Inc. Project: Biosolids PO Box 902 NC Cert#257 Red Springs. NC 28377 REPORT OF ANALYSIS Date Sampled: 11/2/201610:45:00 Lab Number: 60507 Date Received: 11/03/2016 00:00 Sample Id: DAF Date Reported: 11/15/2016 Total Chromium 26.0 5.00 SJB 11/09/2016 11:17 6010C I Total Nickel 12.4 5.00 SJB 11/092016 11:17 6010C I Total Lead <5.00 5.00 SJB 111091201611:17 6010C Total Arsenic <3.00 � 3.00 SJB 11109201611:17 6010C at Mercury <0.400 el Selenium 0.400 JM 11/14201610:00 SW-7471B <5.00 5.00 SJB 11/09201611:17 6010C pH (Standard Units) • 3.70 JM 11/04/2016 09:45 SW-9045D ' Total'Molybdenum 15.D 5.00 SJB 11109201611:17 6010C Sodium Absorption58.17 CALCULATION' Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. AJI values are on adry weight basis except as noted by asterisk. Detection limit on all i N series is on a wet basis. (+r°'repass aNr1°'ref53° Iw'am erC+:rx anawr�!CerLa! use am:r c4en5. mWnvrwal6erepodiz:V in ly ' wnde W. rm-meranyrs/a� (-j rm_ r.rvc t�e mw."a aneemmlu°pu: ayrNercrry ngisrerea:e w dfrcrryECcxro<ra artfs wJM:t Wlarrna ov rre m±ae prcr vatm autM.zHm /11N.�ur 7v&e-L- Debbie Holt Laboratory Supervisor 7621 WhiltPrmt Road Richmond VA �cjao. 11��ft 74M-14 -ppod.lOvIonwan.w. y Copy to Eltt'6~1 C 71-L Project 7— "Sam le, InfurrhatiOn e J:a, umber C'U6,lj,, hir.mhation C.rta' iner Inforiiatio!, FLIen. Che5o.md Tests Sample ID �Pb Use�: Ti.. Ilia 503 Nivag Ch f v SL �Jolabilo a Of Battles e 1:1 CE ONers Series SoIlds' VV c-b Compood. Glas. plasuc �ql —crab — Eom.mafi, _Glass 01F —Caab Glass ci! Plas1ii 14 R.rlgDished SI alurep R(mewd 6. fSiq'oaiu-m, e TOSA Lt%/Aj$ 11110214 11boa I N eLI_ a� _ S ecial nstMefinalcr Remarks'-. , ��1� . SU: Mw Tf S1.1 pl. Al.i... Nf.agaao� Cappa Md Zim SOS Metals: Ameat� Cadmium. Chl-mh-. MeMay, Molybdenum, Lead, Mckel. Selenium. 'Jolem. Aj (Copper & Zinc included In SUI Mtro;:c- S-,k. Total Kiddahl. Aam,oai, NJ A oraoi. Ngroca, CCE. CaIQUM Carbonate Equbanlard or Total lreuba5zatlon Vab, (For, Lime Treated Sludge) Toxicity Characteristics Leaching Procedure ,(TCLP) Analysis Report ;_1 "-,*ESC L•A•B 9•C•I•E•N•C•E•B Mr. Thomas Ammons EEC, Inc. PO Box 902 Red Springs, NC 28377 Report Summary Wednesday March 02, 20IG Report Number: L819333 Samples Received: 02/23/16 Client Project: 15-MI-0104-3 12665 Lebanon Rd. Mt. Juliet, IN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 TCLP S1 The analytical results in this report are based upon information supplied by you, the client, and are for your exclusive use. If you have any questions regarding this data package, please do not hesitate to call. Entire Report Reviewed By: 6W►/ Jim4 Hunt , ESC Representative Laboratory Certification Numbers A2LA - 1461-01,1461-02, AIHA - 100789, AL - 40660, CA - 01157CA, CT - PH-0197, FL - E87487, GA - 923, IN - C-TN-01, KY - 90010, KYUST - 0016, NC - ENV375/DW21704/BIOO41, ND - R-140. NJ - TNO02, NJ NELAP - TNO02, SC - 84004, TN - 2006, VA - 460132, WV - 233, AZ - 0612, MN - 047-999-395, NY - 11742, WI - 998093910, NV - TN000032011-1, TX - T104704245-11-3, OK - 9915, PA - 68-02979, IA Lab #364, EPA - TNO02 Accreditation is only applicable to the test methods specified an each scope of accreditation held by ESC Lab Sciences. This report may not be reproduced, 'except in full, without written approval from ESC Lab Sciences. Where applicable, sampling conducted by ESC is performed per guidance provided in laboratory standard operating procedures: 060302, 060303, and 0603041. Page 1 of 13 uESC L•A•B S•C-1•E•N•C•K•S REPORT OF ANALYSIS Mr. Thomas Ammons EHC, Inc. PO Box 902 Red Springs, NC 28377 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02,2016 ESC Sample q.: L819333-01 Date Received February 23, 2016 Description Campbell Soup DAP Sludge (Annual TCLP Sludge) Site ID : MAXTON, NC Sample ID DAP SLUDGE Project : 15-MI-0104-3 Collected By Grady Dobson , Collection Date 02/22/16 10:00 Parameter Result Det. Limit Units Limit Method Date/Time By Dil Corrosivity Non-Corrosiv 9045D 02/25/16 0808 AMC 1 Ignitability DNI at 170 F Deg. F D93/101 02/25/16 0951 JSS 1 PH 3.55 0.100 su 9045D 02/25/16 1055 MAJ 1 Reactive Cyanide BDL 0.250 mg/kg 9012 B 02/29/16 2341 ASK 1 Reactive Sulfide BDL 25.0 mg/kg 9034-90 02/27/16 1114 JSS 1 TCLP Extraction - 1311 02/23/16 2054 LJN 1 Mercury BDL 0.0100 mg/l 0.200 7470A 02/25/16 1816 TRB 1 Arsenic BDL 0.450 mg/l 5.00 6010C 02/25/16 0829 LTB 1 Barium BDL 1.35 mg/1 100. 6010C 02/25/16 0829 LTB 1 Cadmium BDL 0.450 mg/l 1.00 6010C 02/25/16 0829 LTB 1 Chromium BDL 0.450 mg/1 5.00 6010C 02/25/16 0829 LTB 1 Lead BDL 0.450 mg/l 5.00 6010C 02/25/16 0829 LTB 1 Selenium BDL 0.450 mg/l 1.00 6010C 02/25/16 0829 LTB 1 Silver BDL 0.450 mg/1 5.00 6010C 02/25/16 0829 LTB 1 TCLP ZHB Extraction - 1311 02/23/16 1611 LJN 1 TCLP Volatiles Benzene BDL 0.0500 mg/1 0.500 8260B 02/25/16 0223 LRL 1 Carbon tetrachloride BDL 0.0500 mg/l 0.500 8260B 02/25/16 0223 LRL 1 Chlorobenzene BDL 0.0500 mg/1 100. 8260B 02/25/16 0223 LRL 1 Chloroform BDL 0.250 mg/1 6.00 8260B 02/25/16 0223 LRL 1 1,2-Dichloroethane BDL 0.0500 mg/1 0.500 8260E 02/25/16 0223 LRL 1 1,1-Dichloroethene BDL 0.0500 mg/1 0.700 8260B 02/25/16 0223 LRL 1 2-Butanone (MEK) BDL 0.500 mg/l 200. 8260B 02/25/16 0223 LRL 1 Tetrachloroethene BDL 0.0500 mg/l 0.700 8260E 02/25/16 0223 LRL 1 Trichloroethene BDL 0.0500 mg/l 0.500 8260E 02/25/16 0223 LRL 1 Vinyl chloride BDL 0.0500 mg/l 0.200 8260E 02/25/16 0223 LRL 1 Surrogate Recovery Toluene-d8 99.7 % Rec. 114. 8260B 02/25/16 0223 LRL 1 Dibromofluoromethane 93.8 % Rec. 125. 8260E 02/25/16 0223 LRL 1 a,a,a-Trifluorotoluene 98.6 % Rec. 114. 8260B 02/25/16 0223 LRL 1 4-Bromofluorobenzene 94.9 % Rec. 128. 8260B 02/25/16 0223 LRL 1 TCLP Pesticides Chlordane BDL 0.00500 mg/1 0.0300 8081 03/01/16 1029 LKD 1 L819333-01 (PH) - 3.55 at 22.6c Page 2 of 13 �y�;ESC L•A•B S•C-I-E•N•C•E•S REPORT OF ANALYSIS Mr. Thomas Ammons HRC, Inc. PO Box 902 Red Springs, NC 28377 Date Received February 23, 2016 Description Campbell Soup DAF Sludge (Annual TCLP Sludge) Sample ID DAF SLUDGE Collected By Grady Dobson Collection Date 02/22/16 10:00 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) '758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02,2016 ESC Sample # : L819333-01 Site ID : MAXTON, NC Project : 15-MI-0104-3 Parameter Result Det. Limit Units Limit Method Date/Time By Dil andrin BDL 0.00500 mg/1 0.0200 8081 03/01/16 1029 LED 1 Heptachlor BDL 0.00500 mg/l 0.0080 8081 03/01/16 1029 LED 1 Lindane BDL 0.00500 mg/1 0.400 8081 03/01/16 1029 LED 1 Methoxychlor SDL 0.00500 mg/1 10.0 8081 03/01/16 1029 LED 1 Toxaphene BDL 0.0100 mg/l 0.500 8081 03/01/16 1029 LED 1 Surrogate Recovery Decachlorobiphenyl 69.4 $ Rec. 123. 8081 03/01/16 1029 LKD 1 Tetrachloro-m-xylene 71.8 %; Rec. 114. 8081 03/01/16 1029 LED 1 TCLP Herbicides 2,4,5-TP (Silvex) SDL 0.00200 mg/l 1.00 8151A 02/29/16 2138 KLM 1 2,4-D SDL 0.00200 mg/1 10.0 8151A 02/29/16 2138 KLM 1 Surrogate Recovery 2,4-Dichlorophenyl Acetic Acid 83.2 k Rec. 8151A 02/29/16 2138 KLM 1 TCLP Semi-Volatiles 1,4-Dichlorobenzene BDL 0.100 mg/l 7.50 8270C 02/29/16 1753 JF 1 \Y 2,4-Dinitrotoluene SDL 0.100 mg/1 0.130 8270C 02/29/16 1753 JF 1 Hexachlorobenzene SDL 0.100 mg/1 0.130 8270C 02/29/16 1753 JF 1 Hexachloro-1,3-butadiene BDL 0.100 mg/l 0.500 8270C 02/29/16 1753 JF 1 Hexachloroethane BDL 0.100 mg/1 3.00 8270C 02/29/16 1753 JF 1 Nitrobenzene BDL 0.100 mg/l 2.00 8270C 02/29/16 1753 JF 1 Pyridine SDL 0.100 mg/l 5.00 8270C 02/29/16 1753 JF 1 3&4-Methyl Phenol BDL 0.100 mg/1 400. 8270C 02/29/16 1753 JF 1 2-Methylphenol BDL 0.100 mg/1 200. 8270C 02/29/16 1753 JF 1 Pentachlorophenol BDL 0.100 mg/l 100. 8270C 02/29/16 1753 JF 1 2,4,5-Trichlorophenol BDL 0.100 mg/l 400. 8270C 02/29/16 1753 JF 1 2,4,6-Trichlorophenol BDL 0.100 mg/1 2.00 8270C 02/29/16 1753 JF 1 Surrogate Recovery 2-Fluorophenol 46.6 Rec. 87.0 8270C 02/29/16 1753 JF 1 Phenol-d5 29.6 °s Rec. 67.0 8270C 02/29/16 1753 JF 1 Nitrobenzene-d5 64.1 Rec. 120. 8270C 02/29/16 1753 JF 1 2-Fluorobiphenyl 74.5 5 Rec. 122. 8270C 02/29/16 1753 JF 1 2,4,6-Tribromophenol 65.1 5 Rec. 148. 8270C -02/29/16 1753 JF 1 p-Terphenyl-d14 78.4 & Rec. 149. 8270C 02/29/16 1753 JF 1 BDL - Below Detection Limit Det. Limit - Estimated Quantitation Limit(EQL) Limit - Maximum Contaminant Level as established by the US EPA Note: The reported analytical results relate only to the sample submitted. This report shall not be reproduced, except in full, without the written approval from EEC. Reported: 03/02/16 12:06 Printed: 03/02/16 12:44 L819333-01 (PH) - 3.55 at 22.6c Page 3 of 13 Attachment A List of Analytes with QC Qualifiers Sample Work Sample Number Group Type Analyte L819333-01 WG851885 SAMP 2-Sutanone (MHK) WG852188 SAMP Heptachlor Run ID Qualifier R3116188 J6 R3117564 J3 Page 4 of 13 Attachment B Explanation of QC Qualifier Codes �-,-/ Qualifier Meaning J3 The associated batch QC was outside the established quality control range for precision. J6 The sample matrix interfered with the ability to make any accurate determination; spike value is low Qualifier Report Information ESC utilizes sample and result qualifiers as set forth by the EPA Contract Laboratory Program and as required by most certifying bodies including NBLAC. In addition to the EPA qualifiers adopted by ESC, we have implemented ESC qualifiers to .provide more information pertaining to our analytical results. Each qualifier is designated in the qualifier explanation as either EPA or ESC. Data qualifiers are intended to provide the ESC client with more detailed information concerning the potential bias of reported data. Because of the wide range of constituents and variety of matrices incorporated by most EPA methods,it is common for some compounds to fall outside of established ranges. These .exceptions are evaluated and all reported data is valid and useable "unless qualified as 'R' (Rejected)." Definitions Accuracy - The relationship of the observed value of a known sample to the true value of a known sample. Represented by percent recovery and relevant to samples such as: control samples, matrix spike recoveries, surrogate recoveries, etc. Precision - The agreement between a set of samples or between duplicate samples. Relates to how close together the results are and is represented by Relative Percent Differrence. Surrogate - organic compounds that are similar in chemical composition, extraction, and chromotography to analytes of interest. The surrogates are used to determine the probable response of the .group of analytes that are chem- ically related'to the surrogate compound. Surrogates are added to the sample and carried through all stages of preparation and analyses. TIC - Tentatively Identified Compound: Compounds detected in samples that are not target compounds, internal standards, system monitoring compounds, or surrogates. Page 5 of 13 EV C L•A•B S•C•I•E•N-C•E•S BHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level 11 L819333 12065 Lebanon Rd. Mt. Sul et, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02, 2016 Laboratory Blank Analyte Result Units $ Rec Limit Hatch Date Analyzed 1,1-DSchloroethene c .05 mg/1 WG85188S 02/24/16 23:13 1,2-Dichloroethane < .05 mg/l WG851885 02/24/16 23:13 2-Butanone (MEK) < .5 mg/l WGB51885 02/24/16 23:13 Benzene < .05 mg/1 WG851685 02/24/16 23:13 Carbon tetrachloride < .05 mg/1 WGSSI885 02/24/16 23:13 Chlorobenzene < .05 mg/l WG851885 02/24/16 23:13' Chloroform < .25 mg/1 WG851885 02/24/16 23:13 Tetrachloroethene < .05 mg/l WG851885 02/24/16 23:13 Trichloroathene < .05 mg/l WG851885 02/24/16 23:13 vinyl chloride < .05 mg/1 WG851885 02/24/16 23:13 4-Bromofluorobenzene $ Rec. 94.90 80.1-120 WG851885 02/24/16 23:13 Dibromofluoromethane $ Rec. 94.10 79-121 NG851885 02/24/16 23:13 Toluene-d8 % Rec. 99.10 90-115 WG851885 02/24/16 23:13 a,a,a-Trifluorotoluene $ Rec. 98.50 90.4-216 WG851885 02/24/16 23:13 Arsenic < .45 mg/1 WG851901 02/25/16 08:20 Barium < 1.35 mg/1 WG851901 02/25/16 08:20 Cadmium a .45 mg/1 WG851901 02/25/16 08:20 Chromium < .45 mg/1 WG851901 02/25/16 08:20 Lead < .45 mg/1 WG851901 02/25/16 08:20 Selenium < .45 m9/1 WG651901 02/25/16 08:20 silver < .45 mg/1 WG851901 02/25/16 08:20 j rcury < .01 mg/l WG851898 02/25/16 17:44 Reactive Sulfide < 25 mg/kg WG852311 02/27/16 11:14 Reactive Cyanide < .25 mg/kg WG852979 02/29/16 23:36 1,4-Dichlorcbenzene < .1 mg/1 WG852132 02/29/16 11:38 2,4,5-Trichlorbphenol < .1 mg/1 WG852132 02/29/16 11:38 2,4,6-Trichlorophenol < .1 mg/1 WG852132 02/29/16 11:38 2,4-Dinitrotoluene < .1 mg/1 WG852132 02/29/16 11:38 2-Methylphenol < .1 mg/1 WG852132 02/29/16 11:38 364-Methyl Phenol < .1 mg/l WG852132 02/29/16 11:38 Hexachlor0-1,3-butadiene < .1 mg/1 WG852132 02/29/16 11:38 Hexachlorobenzene < .1 mg/l WG852132 02/29/16 11:38 HexaChlOroethane c .1 mg/1 WG852132 '02/29/16 11:39 Nitrobenzene < .1 mg/l WG852132 02/29/16 11:38 Pentachlorophenol < .1 mg/l WG852132 02/29/16 11:38 Pyridine < .1 mg/l W0852132 02/29/16 11:38 2,4,6-Tribromophenol $ Rec. 56.00 11.2-130 WG852132 02/29/16 11:38 2-Pluorobiphenyl $ Rec. 62.50 29.5-131 WG852132 02/29/16 11:38 2-Fluorophenol % Rec. 39.00 10-77.9 WG852132 02/29/16 11:38 Nitrobenzene-d5 $ Rec. 55.50 21.8-123 W0852132 02/29/16 11:38 Phenol-d5 $ Rea. 23.00 5-70.1 WG852132 .02/29/16 11:38 p-Terphenyl-d14 $ Rec. 69.60 29.3-137 WG852132 02/29/16 11:39 2,4,5-TP (Silvex) < .002 mg/1 W0852402 02/29/16 20:58 2,4-D < .002 mg/l WG852402 02/29/16 20:59 2,4-Dichlorophenyl Acetic Acid $ Rec. 80.70 28.2-146 WG852402 02/29/16 20:58 Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 6 of 13 -- ESC L•A•B B•C•1•E•N•C•E•B MC, Inc. Mr. Thomas A=ons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L819333 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02, 2016 Laboratory Blank Analyte Result Units t Rec Limit Batch Date Analyzed Chlordane < .005 mg/l WG852188 03/01/16 09:53 Endrin < .005 mg/1 WG852188 03/01/16 09:53 Lindane < .005 mg/1 WG852188 03/01/16 09:53 Heptachlor < .005 mg/1 WG852188 03/01/16 09:53 Methoxychlor < .005 mg/l W0852188 03/01/16 09:53 Toxaphene < .01 mg/l WG852188 03/01/16'09:53 Decachlorobiphenyl & Rec. 86.70 10-156 WG852188 03/01/16 09:53 Tetrachloro-m-xylene % Rec. 80.20 13.9-137 WG852188 03/01/16 09:53 Duplicate Analyte Units Result Duplicate RPD Limit Ref Samp Batch Corrosivity 0.00 0.00 0.00 10 L819285-01 WG851863 Ignitability Deg. F 0.00 0.00 0.00 10 L819333-01 WGB51812 PH Su 8.67 8.66 0.115 1 L819429-.03 WG851847 PH su 8.01 7.99 0.250 1 L819663-01 WG851847 Reactive Sulfide mg/kg 0.00 0.00 0.00 20 L819333-01 W0852311 -.-.active Cyanide mg/kg 0.00 -0.0215 0.00 20 L819333-01 WG852979 ' �-.:alyte Laboratory Control Sample Units Known Val Result % Rec 'Limit Batch 1,1-Dichloroethene mg/1 .025 0.0252 101. 60.6-133 WG851885 1,2-Dichloroethane mg/l .025 0.0241 96.4 65.3-126 WG851885 2-Butanone (MEK) mg/1 .125 0.0941 75.3 46.4-155 WOBS1885 Benzene mg/l .025 0.0238 95.1 73-122 NG851985 Carbon tetrachloride mg/l .025 0.0247 98.7 70.9-129 WG85IB85 Chlorobenzene mg/l .025 0.0276 110. 79.7-122 WGB51B85 Chloroform mg/1 .025 0.0240 96.1 73.2-125 WG851885 Tetrachloroethene mg/1 .025 0.0267 107. 73.5-130 WG851885 Trichloroethene mg/1 .025 0.0255 102. 79.5-121 WG851885 Vinyl chloride mg/l .025 0.0220 87.8 61.5-134 WG051885 4-Bromofluorobenzene 94.60 80.1-120 WG851885 Dibromofluoromethane 93.40 79-121 WGB51885 Toluene-d8 99.10 90-115 WGGSIS85 a,a,a-Trifluorotoluene 98.70 90.4-116 WGBSI885 Arsenic mg/1 30 9.17 92.0 '80-120 WG851901 Barium mg/1 10 9.20 92.0 80-120 WG851901 Cadmium mg/1 10 9.21 92.0 80-120 WG851901 Chromium mg/1 10 9.23 92.0 80-120 WOBS1901 Lead mg/1 10 9.19 92.0 80-120 WGBS1901 Selenium mg/l 10 9.13 91.0 80-120 WG851901. Silver mg/l 10 9.04 90.0 80-120 WG851901 Corrosivity 6.72 6.70 99.7 98.5-101.5 WG851863 Ignitability Deg. F 82 82.8 101. 93-107 WG951812 • Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 7 of 13 12065 Lebanon Rd. //''�1 Mt. Juliet, TN 37122 ES■ (615) 15) 5858 758- {\v' 1-800-767-5859 FaX (615) 758-5859 L-A•B B•C• I•E•N•C•E•5 Tax I.D. 62-0814289 Est. 1970 BBC, Inc. Mr. Thomas Ammons PO Box 902 Quality Assurance Report Level II Red Springs, NC 28377 March 02, 2016 L819333 Analyte Units Laboratory Control Sample Known Val Result - t Bee Limit Batch PH au 6.31 6.33 100. 98.5-101.5 WG851847 Mercury mg/l .03 0.0294 98.0 80-120 IIGB51898 Reactive Sulfide mg/kg 100 89.2 89.2 70-130 WG852311 Reactive Cyanide mg/kg, 53.9 66.0 122. 50-150 WG852979 1,4--Dichlorobenzene mg/l .05 0.0275 55.0 21-89.4 WG852132 2,4,5-Trichlorophenol mg/1 .05 0.0377 75.5 34.9-112 WG852132 2,4,6-Trichlorophenol mg/l .05 0.0363 72.6 29.8-107 WG852132 2,4-Dinitrotoluene mg/l .05 0.0349 69.7 31.2-105 WG852132 2-Methylphenol mg/1 .05 0.0287 57.4 26.4-86.9 WG852132 364-Methyl Phenol mg/1 .05 0.0305 61.0 27.9-92 WG852132 Hexachloro-1,3-butadiene mg/l .05 0.0290 58.1 16.1-104 WG852132 Hexachlorobenzene mg/1 .05 0.0367 73.4 38.5-116 WG852132 Hexachloroethane mg/l .05 0.0293 58.7 16.5-89.8 WG852132 Nitrobenzene mg/l .05 0.0344 68.9. 31.4-106 WG852132 Pentachlorophenol mg/l .05 0.0343 68.6 30-97.4 WG852132 Pyridine mg/1 .05 0.0120 24.0 13.5-58.9 WG852132 2,4,6-Tribromophenol - 76.50 11.2-130 WG852132 v-Fluorobiphenyl 68.70 29.5-131 WG852132 lY Fluorophenol 44.50 10-77.9 WG852132 E.trobenzene-d5 65.50 21.8-123 WGBS2132 ,enol-d5 28.60 5-70.1 WG852132' p-Terphenyl-d14 72.60 29.3-137 WG852132 2,4,5-TP (Silvex) mg/l .005 0.00422 84.4 46.3-127 WG852402 2,4-D mg/l .005 0.00432 86.4 31.1-136 WG852402 2,4-Dichlorophenyl Acetic Acid 84.20 28.2-146 WG852402 Endrin mg/l .001 0.00102 102. 50.1-131 WG852188 Lindane mg/1 .001 0.000954 95.4 54.7-125 WG852188- Heptachlor mg/l .001 0.000648 64.8 20.7-127 WG852188 Methoxychlor mg/l .001 0.00118 118. 48.2-144 W0852188 Decachlorobiphenyl 76.90 30-156 WG852188 Tetrachloro-m-xylene 94.30 13.9-137 WG852188 Laboratory Control Sample Duplicate Analyte Units Result IRef %Rae Limit RPD Limit Batch 1,1-Dichlorcethene mg/1 0.0253 0.0252 101. 60.6-133 0.570 20 WG851885 1,2-Dichlorcethane mg/l 0.0249 0.0241 100. 65.3-126 3.32 20 WG851885 2-Butanone (MEK) mg/1 0.0924 0.0941 74.0 46.4-155 1.86 20 WG851885 Benzene mg/1 0.0245 0.0238 98.0 73-122 2.82 20 WG851885 Carbon tetrachloride mg/1 0.0248 0.0247 99.0 70.9-129 0.330 20 WG851885 Chlorobenzene mg/l 0.0286 0.0276 114. 79.7-122 3.64 20 WGB51885 Chloroform mg/l 0.0247 0.0240 99.0 73.2-125 2.62 20 WG851885 Tetrachloroethene mg/l 0.0276 0.0267 110. 73.5-130 3.52 20 WG851885 Trichloroethene mg/1 0.0260 0.0255 104. 79.5-121 1.92 20 WG851885 Vinyl chloride mg/1 0.0222 0.0220 99.0 61.5-134 1.17 20 WG851885 4-Bromofluorobenzene 95.50 80.1-120 WG851885 Dibromofluoromethane 94.00 79-121 WG851885 * Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 8 of 13 L-A•B S•C•I•E•N-C•E•S BHC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L819333 Laboratory Control Sample Duplicate 12065 Lebanon Rd. Mt. Juliet, IN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02, 2016 Analyte Units Result Ref %Rec Limit RPD Limit Batch Toluene-d8 99.60 90-115 a,a,a-Trifluorotoluene 101.0 90.4-116 Arsenic mg/1 9.29 9.17 93.0 80-120 1.00 20 WG851901 Barium mg/l 9.31 9.20 93.0 80-120 1.00 20 WG8519dl Cadmium m9/1 9.32 9.21 93.0 80-120 1.00 20 WG851901 Chromium mg/l 9.34 9.23 93.0 80-120 1.00 20 WG851901 Lead mg/1 9.33 9.19 93.0 80-120 1.00 20 WG851901 Selenium mg/1. 9.28 9.13 93.0 80-120 2.00 20 WGB51901 Silver mg/l 9.16 9.04 92.0 80-120 1.00 20 WG851901 Corrosivity 6.71 6.70 100. 98.5-101.5 0.149 10 WG851863 Ignitability Deg. F 83.8 82.8 102. 93-107 1.20 20 WGB51812 PH su 6.33 6.33 100. 98.5-101.5 0.00 1 WG851847 Mercury mg/l 0.0298 0.0294 99.0 80-120 2.00 20 WGBS1898 Reactive Sulfide mg/kg 97.3 89.2 97.0 70-130 8.69 20 WG852311 Reactive Cyanide mg/kg 64.2 66.0 119. 50-150 3.00 20 WG852919 "4-Dichlorobenzene mg/l 0.0299 0.0275 60.0 21-89.4 8.27 32.6 WGB52132 mg/l 0.0410 0.0377 82.0 34.9-112 8.41 23.3 WG852132 _"4,5-Trichlorophenol 2,4,6-Trichlorophenol mg/1 0.0403 0.0363 80.0 29.8-107 10.5 24.1 WG852132 2,4-Dinitrotoluene mg/1 0.0404 0.0349 81.0 31.2-105 14.7 22 WG852132 2-Methylphenol mg/1 0.0313 0.0287 62.0 26.4-86.9 8.64 26.5 NGS52132 3&4-Methyl Phenol mg/1 0.0342 0.0305 68.0 27.9-92 11.3 27 NG852132 Hexachloro-1,3-butadiene mg/1 0.0320 0.0290 64.0 16.1-104 9.57 31.2 WG852132 Hexachlorobenzene mg/1 0.0403 0.0367 80.0 38.5-116 9.30 20.1 WG852132 Hexachloroethane mg/l 0.0323 0.0293 64.0 16.5-89.8 9.45 30.7 WG852132 Nitrobenzene mg/l 0.0369 0.0344 74.0 31.4-106 7.00 25.7 NGS52132 Pentachlorophenol mg/1 0.0390 0.0343 78.0 10-97.4 12.7 35.1 WG852132 Pyridine mg/l 0.0105 0.0120 21.0 13.5-58.9 13.8 32.5 WG852132 2 ,4,6-Tribromophenol 79.80 11.2-130 WG852132 2-Fluorobiphenyl 73.50 29.5-131 WG852132 2-Fluorophenol 45.10 10-77.9 - WG852132 Nitrobenzene-d5 67.50 21.8-123 WG852132 Phenol-d5 31.30 5-70.1 WG852132 p-Terphenyl-dl4 81.30 29.3-137 WG852132 2,4,5-TP (Silvex) mg/l 0.00421 0.00422 84.0 46.3-127 0.170 29.5 W6952402 2,4-D mg/1 0,00429 0.00432 86.0 31.1-136 0.570 28.6 WGSS2402 2,4-Dichlorophenyl Acetic Acid 83.70 28.2-146 WG852402 Endrin mg/l 0.000942 0.00102 94.0 50.1-131 7.60 29.1 WG852188 Lindane 'mg/1 0.000871 0.000954 97.0 54.7-125 9.14 21.1 WG852188 Heptachlor mg/l 0.000684 0.000648 68.0 20.7-127 5.44 30.5 NGB52188 Methoxychlor mg/1 0.00116 0.00118 116. 48.2-144 1.99 27.8 'WG852188 Decachlorobiphenyl 68.30 30-156 WG852188 + Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 9 of 13 �V 12065 Lebanon Rd. Mt. Juliet, TN 37122 ' ( (615) 758-5858 1-800-800-767-5859 Pax (615) 758-5859 L•A•B S•C•I•E•N•C• E•S Tax I.D. 62-0814289 Est. 1970 EHC, Inc. Mr. Thomas Ammons PO Box 902 Quality Assurance Report Level II Red Springs, NC 28377 March 02, 2016 L819333 Matrix Spike Analyte Units ME Res Aef Res TV % Rec Limit Ref Samp Batch Tetrachloro-m-xylene 85.10 13.9-137 Matrix Spike Analyte Units ME Res Ref Res TV t Rao Limit _ Ref Samp Batch 1,1-Dichloroethene mg/1 0.878 0.00 1.25 70.2 48.8-144 LB19333-01 WGSSIB85 1,2-DichlorOethane mg/1 0.963 0.00 1.25 77.0 60.7-132 L819333-01 WG851885 2-Butanone (MEK) mg/l 2.73 0.00 6.25 43.6- 45-156 L819333-01 NGS51885 Benzene mg/1 0.898 0.00235 1.25 71.6 58.6-133 L819333-01 IIGB51885 Carbon tetrachloride mg/1 0.924 0.00 1.25 73.9 60.6-139 L819333-01 WG851885 Chlorobenzene mg/1 1.12 0.00 1.25 89.7 70.1-130 L819333-01 I-IGS51885 Chloroform mg/l 0.939 0.00378 1.25 74.8 66.1-133 L819333-01 NG851885 Tetrachloroethene mg/1 1.04 0.00 1.25 83.1 57.4-141 L819333-01 WG851895 Trichloroethene mg/1 0.991 0.00 1.25 79.3 48.9-148 L819333-01 WG851885 vinyl chloride mg/1 0.823 0.00 1.25 65.8, 44.3-143 L819333-01 WGBSI885 4-Bromofluorobenzene 96.30 80.1-120 WG8S1885 Dibromofluoromethane 93.30 79-121 WGBS1885 Toluene-d8 99.B0 90-115 WG851885 a,a,a-Trifluorotoluene 100.0 90.4-116 WG851885 Arsenic mg/1 9.50 0.0324 30 95.0 75-125 L819333-01 WG851901 Sium mg/1 9.15 0.0625 10 91.0 75-125 L819333-01 WG851901 t+Lmium mg/l 9.30 0.00102 10 93.0 75-125 L819333-01 WG851901 ���:Ominm mg/1 9.38-0.00166 10 94.0 75-125 L819333-01 WG851901 Lead mg/l 9.51 0.0160 10 95.0 75-125 L819333-01 WG951901 Selenium mg/1 9.56-0.0272 10 96.0 75-125 L819333-01 WG851901 Silver mg/1 9.19 o.a0471 10 92.0 75-125 L819333-01 NGS51901 Mercury mg/1 0.0269-0.000426 .03 90.0 75-125 L817719-03 NGS51898 Mercury mg/1 0.0264-0.000370 .03 88.0 75-125 L819285-01 WGSSI898 1,4-Dichlorobenzene mg/1 0.327 0.00 .5 65.5 14-104 L819333-01 WG852132 2,4,5-Trichlotophenol mg/1 0.413 0.00 .5 82.7 30.6-120 L819333-01 WG852132 2,4,6-Trichlorophenol mg/1 0.417 0.00 .5 83.4 19.1-114 L019333-01 WG852132 2,4-Dinitrotoluene mg/l 0.397 0.00 .5 79.4 16.2-135 L819333-01 WG852132 2-Methylphenol mg/1 0.324 0.00 .5 64.7 10-133 L819333-01 WG852132 364-Methyl Phenol mg/l 0.339 0.00 .5 67.7 17.4-100 L819333-01 WG852132 Hexachloro-1,3-butadiene mg/1 0.316 0.00 .5 63.3 15.7-109 L819333-01 WG852132 Hexachlorobenzene mg/1 0.417 0.00 .5 93.5 31.9-135 L819333-01 NGS52132 Nexachloroethane mg/1 0.348 0.00 .5 69.5 10.4-105 L819333-01 IIGB52132 Nitrobenzene mg/1 0.384 0.00 .5 76.7 23.1-121 L819333-01 NGS52132 Pentachlorophenol mg/1 0.437 0.00 .5 87.3 10-108 L819333-01 WG852132 Pyridine mg/1 0.0574 0.00 .5 11.5 10-77.8 L819333-01 TIGS52132 2,4,6-Tribromophenol 80.00 11.2-130 NG852132 2-Fluorobiphenyl 74.30 29.5-131 H0852132 2-Fluorophenol 44.40 10-77.9 WG852132 Nitrobenzene-dS 71.20 21.8-123 WG852132 Phenol-d5 30.80 5-70.1 WG852132 p-Terphenyl-d14 79.90 29.3-137 WG852132 2,4,5-TP (Silvex) mg/1 0.0432 0.00 .05 86.4 46.3-127 L819333-01 WG852402 2,4-D mg/1 0.0443 0.00 .05 88.6 31.1-136 L819333-01 NGS52402 2,4-Dichlorophenyl Acetic Acid 89.90 28.2-146 WG852402 * Performance of this Analyte is outside of established Criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers.' Page 10 of 13 ��ESC L•A•B S-C•I•E•N•C•E•S MC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L819333 Matrix Spike 12065 Lebanon Rd. Mt. Juliet, IN'37122 (915) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02, 2016 Analyte Units MS Res 'Ref Res TV %-Rec Limit Ref Samp Batch Sndrin mg/l 0.00920 0.00 .01 92.0 50.1-131 L819333-01 WG852188 Lindane m4/1 0.00807 0.00 .01 80.7 54.7-125 L819333-01 WG852188 Heptachlor mg/l 0.00596 0.00 .01 59.6 20.7-127 L819333-01 WG852189 Methoxychlor m9/1 0.0105 0.00 .01 105. 48.2-144 L819333-01 WG852188 DecachlorObiphenyl 79.80 10-156 WG852188 Tetrachloro-m-xylene 82.30 13.9-137 WG852188 Matrix Spike Duplicate Analyze Units MSD Ref %Rec Limit RPD Limit Ref Samp Hatch 1,1-Dichlorcethene mg/1 0.937 0.878 75.0 48.8-144 6.54 20 L819333-01 WG851885 1,2-Dichloroethane mg/1 1.03 0.963 92.6 60.7-132 6.96 20 L819333-01 WGB51885 2-Butanone (MEE) mg/l 2.77 2.73 44.3• 45-156 1.53 20.8 L819333-01 WG851885 Benzene mg/l 0.952 0.898 76.0 59.6-133 5.84 20 L819333-01 WG851885 Carbon tetrachloride mg/l 0.998 0.924 79.8 60.6-139 7.67 20 L819333-01 WG851885 Chlorobenzene mg/l 1.20 1.12 96.2 70.1-130 6.97 20 L919333-01 WG851885 Chloroform mg/l 1.01 0.939 80.5 66.1-133 7.25 20 L819333-01 WG851885 _ Tetrachlorcethene mg/1 1.11 1.04 88.9 57.4-141 6.72 20 L819333-01 NG851885 Trichloroethene mg/1 1.05 0.991 84.1 48.9-148 5.93 20 L819333-01 WG851865 vinyl chloride mg/1 0.896 0.823 71.7 44.3-143 8.57 20 L819333-01 WG851885 4-Bromofluorobenzene 98.80 80.1-120 WG851885 -"0romofluoromethane 94.90 79-121 WG851885 ` '�luene-de 100.0 90-115 WG851885 l fh,a-Trifluorotoluene 102.0 90.4-116 W0851885 Arsenic mg/1 9.46 9.50 94.3 75-125 0.00 20 L819333-01 WG851901 Barium mg/l 9.06 9.15 89.9 75-125 1.00 20 L819333-01 WGSS1901 Cadmium mg/l 9.22 9.30 92.2 75-125 1.00 20_ L819333-01 WG851901 Chromium mg/l 9.32 9.38 93.2 _ 75-125 1.00 20 L819333-01 WG851901 Lead mg/1 9.46. 9.51 94.4 75-125 1.00 20 L819333-01 WG851901 Selenium mg/1 9.50 9.56 95.2 75-125 1.00 20 L819333-01 WG851901 Silver mg/1 9.15 9.19 91.5 75-125 0.00 20 L819333-01 NG851901 Mercury mg/l 0.0293 0.0269 99.0 75-125 8.00 20 L817719-03 NG851898 Mercury mg/l 0.0274 0.0264 92.4 75-125 3.00 20 L819285-01 WGB51898 1,4-Dichlorobenzene mg/l 0.323 0.327 64.5 14-104 1.47 36.4 L819333-01 WG852132 2,4,5-Trichlorophenol mg/l 0.402 0.413 80.3 30.6-120 2.83 33.8 L819333-01 WG852132 2,4,6-Trichlorophenol mg/1 0.41a 0.417 82.0 19.1-114 1.64 29.9 L819333-01 WG852132 2,4-Dinitrotoluene mg/l 0.388 0.397 77.6 16.2-,135 2.30 20.6 L819333-01 WG852132 2-Methylphenol mg/1 0.306 0.324 61.2 30-133 5.63 40 L819333-01 W0852132 3&4-Methyl Phenol mg/l 0.327 0.339 65.3 17..4-100 3.57 27.7 L819333-01 WG852132 Hexachlcro-1,3-butadiene mg/1 0.311 0.316 62.2 15.7-109 1.77 37.6 L819333-01 WG852132 Hexachlorobenzene mg/1 0.399 0.417 79.9 31.9-135 4.43 20 L919333-01 WG852132 Hexachloroethane mg/1 0.344 0.348 68.8 10.4-105 1.06 40 L819333-01 WG852132 Nitrobenzene mg/l 0.380 0.384 76.0 23.1-121 0.980 29 L819333-01 WG852132 Pentachlorophencl mg/l 0.440 0.437 87.9 10-108 0.670 40 LB19333-01 WG852132 Pyridine mg/l 0.0555 0.0574 11.1 10-77.8 3.35 38.9 L819333-01 WG852132 2,4,6-Tribromophen0l 79.20 11.2-130 WG852132 2-Fluorobiphenyl 73.20 29.5-131 WG852132 2-Fluorophenol 42.30 10-77.9 WG852132 Nitrobenzene-d5 68.80 21.8-123 WG852132 Phenol-d5 29.10 5-70.1 WG852132 p-Terphenyl-d14 77.70 29.3-137 WG852132 • Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analyzes with QC Qualifiers.' Page 11 of 13 c ESC L•A-II S-C•I•E-N•C•E•S BBC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L819333 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Pax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02, 2016 Matrix Spike Duplicate Analyte Units MSD Ref %Rec Limit BID Limit Ref Sap Batch 2,4,5-TP (Silvex) mg/1 0.0428 0.0432 95.6 46.3-127 0.860 29.5 L819333-01 WG952402 2,4-D mg/l 0.0425 0.0443 85.0 31.1-136 4.15 28.6 L819333-01 WGB52402 2,4-Dichlorophenyl Acetic Acid 82.60 28.2-146 WG852402 Endrin mg/1 0.00970 0.00920 97.0 50.1-131 5.30 29.1 L819333-01 WG852188 Lindane mg/1 0.00833 0.00807 83.3 54.7-125 3.24 21.1 L819333-01 WG852188 Heptachlor mg/1 0.00907 0.00596 90.7 20.7-127 . 41.3• 30.5 L819333-01 WG852188 Methoxychlor mg/1 0.0109 0.0105 109. 48.2-144 3.86 27.8 L819333-01 WG852188 Decachlorobiphenyl 80.40 10-156 WG852188 Tetrachloro-m-xylene 85.90 13.9-137 WG852188 Batch number /Run number / Sample number cross reference WG851530: R3116040: L819333-01 WG851885: R3116188: L819333-01 WG851901: R3116207: L819333-01 WG851625: R3116215: L819333-01 WGB51863: R3116226: L819333-01 WG851812: R3116290: L819333-01 I-GS51847: R3116292: L819333-01 WG851898: R3116414: L819333-01 WG852311: R3116890: L819333-01 WG852979: R3117130: L819333-01 WG852132: R3117275: L319333-01 WGB52402: R3117389: L819333-01 11GS521BB: R3117564: L819333-01 • Calculations are performed prior to rounding of reported values. • Performance of this Analyte is outside of established criteria. For additional information, please see Attachment A 'List of Analytes with QC Qualifiers. - Page 12 of 13 C)ESC L•A•B S•C•I•E•N-C•E•S BRC, Inc. Mr. Thomas Ammons PO Box 902 Red Springs, NC 28377 Quality Assurance Report Level II L819333 The data package includes a Summary of the analytic results of the quality control samples required by the SW-846 or CRA methods. The quality control samples include a method blank, a laboratory control sample, and the matrix spike/matrix spike duplicate analysis. It a target parameter is outside the method limits, every sample that is effected is flagged with the appropriate qualifier in Appendix B of the analytic report. Method Blank - an aliquot of reagent water carried through the entire analytic process. The method blank results indicate if any possible contamination exposure during the sample handling, digestion or extraction process, and analysis. Concentrations of target analytes above the reporting limit in the method blank are qualified with the "B" qualifier. Laboratory Control Sample - is a sample of known concentration that is carried through the digestion/extraction and analysis process. The percent recovery, expressed as a percentage of the theoretical concentration, has statistical control limits indicating that the analytic process is "in control-. If a target analyte is outside the control limits for the laboratory control sample or any other control sample, the parameter is flagged with a "J4" qualifier for all effected samples. Matrix Spike and Matrix Spike Duplicate - is two aliquots of an environmental sample that is spiked with known concentrations of target analytes. The percent recovery of the target analyzes also has statistical control limits. If any recoveries that are outside the method control limits, the sample .that was selected for matrix spike/matrix spike duplicate analysis is flagged with either a "JS" or a "IS". The relative percent difference (tRPD) between the matrix spike and the matrix spike duplicate recoveries is all calculated. If the RPD is above the method limit, the effected samples are flagged with a "J3" qualifier. Page 13 of 13 _f 12065 Lebanon Rd. Mt. Juliet, TN 37122 (615) 758-5858 1-800-767-5859 Fax (615) 758-5859 Tax I.D. 62-0814289 Est. 1970 March 02, 2016 EHC,1W. Billing Information; -` Analysis/ Container I Presemtive ICna;,, cocue `,. Page_ar_ PO Box 9D2 Red Springs, NC 28377 6 2 v v `q v` ,n d U 14 1 016C L,,,-6 5•G•nG•N•C•'=•g 03 31p3tebamnkJ - O 13 v rcisiia zsssv j. c Plwnc ee0767 it'�9 s'R ru: 61L25B•SGT9 O�y$ Report to: - oswo5 Email To: ,//�•I[•ayr+ Project G•�� 6e{� Sau%1 phF S/u/ Description: P / a /}uxrra. C[y� Cftylstata Collected: I D0393 Phone:910-843-4456 Fax: 910.843.5376 Client Project it lob Project is Collected by (print): Site/Faulty 10B P.O.a -r1k Acctnum: ENVHYD Template: 7 ord?"V _ Prelagin: //aa L�rzal a'Ssq, Vr N V V Callettctl (signatu/:e}f Rush? (teh MUST Be Notified) _Same Day------_.-..._...-._2DDft Date Results Needed Immediately Packed on ice N Y,y�- raoR Day ........ -..... ...... -....1W7L _Twa Day _—._.-�..._so% _ Three Day.__._.-___._.25% N of O o k 1J [ TSR: 350• Jimmy Hunt Pa: - Emil? No Yes — — FAX? —No _Yes No. of Sample ID Comp/Grab Matrix ` Depth Date .Time trs Shi pped.Via:.DAF _ _ - Remymnorwou 5amarexpebcarl _ .,. Cal.. ITGL/.'1 v'/�-=I/G /o : Z. - K Matrix: 55 •Soil GW-Groundwater WW-Waste Water DIN -Drinking Water OT-Ocher Remarks: SlvJgx a-Ae pH Temp 1/ v, C Flow ' Other Hold It Relinquishe : (Si �a[uro} Date: 2 z Time: ?2:4!) Received by: (signature) ``re^ , , 1 l:, Samples returned via: ❑ UPS fYFedFx L3Courier ❑_ Condition: (lab use only) �3 µ CDC Seal Intact: _Y N 'DNA PH Checked: NCF: Relinquished by.(Sl naluraT •L- le;44I Relinquished by.(Slpature) y Date: Date: Time: Time: deceived by:(Signarure) rf ��' � Rece I for 11P by. (Signature) - Temp: °C Bottles Received: 2 Date:, f/- Time: Pathogen and Vector Attraction Reduction Documentation The current permit, WQ0004893 does not have vector or pathogen requirements. This is a non -biological wastewater treatment plant and will not require vector attraction reduction. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM Facility Name: Campbell Soup Supply Company Permit Number: WQ0004893 WWTP Name: Campbell Soup Supply Company NPDES Number: WQ0003626 r `mitoring Period: From 1/1/2016 To 12/31/2016 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class A: Alternative 10 Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ ........... If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ElThermophilio ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 10 Alternative 2 ❑ Alternative 3 ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ jAerobic Digestion ❑ Anaerobic Digestion[ .: .... _,.,.:. ""''' If applicable to alternative performed (Class A or Class B) complete the following monito ing data: Parameter Allowable Level, in Sludge g Pathogen Density Number 01 Excee- dences Frequency of Analvsis Sample Type Analytical Tech- ni ue Minimu Geo. Mean Maxim Units Fecal Coliform 2 x 10 to the 6th power MPN per gram of total solids or 2 x 10 to the 6thpower CFU per gram of n \�0 1000 mpn per gram of total solid (dry weight) E Salmonella bacteria (in lieu of fecal coliform 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ 10ption2 ❑ 1 Option 3 ❑ 10ption4 ❑ I Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction were options performed ❑ p CERTIFICATION STATEMENT (please check the appropriate statement) ❑ " I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector' attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." - 'mie C. Collins - Environmental Manager Jamie C. Collins - Environmental Manager Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) gnature of Preparrer Due Signature of Land Applier (if applicable) Date Soil Analysis Report r- s Page 1 0, - i Report hL_-. ir: 16-110-0682 ,r Account Number: 00327 7621 Whitepine Road, Richmond, VA 23237 WMa ypoi nit Main 804-743-9401 ° Fax 804-271-6446 Send To: EHC Inc. ANALYTICAL www.waypointanalytical.com PO Box902 'Every acts... Every year.">;.. Grower: CAMPBELL SOUP RED SPRINGS NC 28377 ANNUAL SOIL SAMPLE SPRAY IRRIGATION SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Lime Index Loss On Ignition Water pH Date Received: 04/19/2016 Date Of Analysis: 04120/2016 Date Of Report: 04/20/2016 OM WN ENR Phosphorus Potassium Magnesium calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number % Soil Ibs/A M3 K M0 Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/1009 meq/1009 FIELDA 11568 2.1 86 145 VH 133 VH 64 M 618 M 75 H 6.7 0.2 4.5 MIN L NOm121 NC=68 FIELD C 2.1 126 VH 73 L 53 L 1124 H 11569 84 64 M 6.4 6.88 0.5 5.5 MIN L NC=105 NC=37 FIELD D 1.0 177 VH 108 H 36 L 487 H 11570 65 64 H 7.2 0.0 3.3 MIN L NC.= 147 NC = 55 FIELD E 2.6 275 VH 155 VH 49 L 876 H 11672 94 68 M 6.5 0.4 5.9 MIN M NO = 229 NC = 79 FIELD F 2.3 475 VH 101 M 103 M 1337 H 11573 84 53 L 6.8 0.2 8.2 MIN L NC=396 NC=52 Percent Base Saturation Nitrate Sulfur Zinc Manganese. Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NON 3 S Zn Mn Fe Cu S SS CI AI ova ova % %ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm FIELD 5 VL 11.2 VH 7 L 0.6 L 7.6 11.9 68.7 7.2 4.4 212 VH 0.7 M NC=10 NC=280.0 NC=44 NC=30.0 FIELD C 6 VL 19.7 VH 5 L 0.9 M 3.4 8.0 74.9 5,1 9.1 183 VH 0.9 M NC=12 NC=492.5 NC=31 NC=45.0 FIELD D 6 VL 18.5 VH 2 VL 0.5 L 8.4 9.1 73.8 8.4 0.0 348 VH 0.7 NC=12 NC=462.5 NC=13 NC=25.0 .M FIELD E 12 L 23.4 VH 37 H 0.9 M 6.7 6.9 74.2 5.0 6.8 329 VH 0.9 M NC=25 NC=585.0 NC=231 NC=45.0 FIELD F 10 L 12.6 VH 19 M 1.1 M 3.2 10.5 81.5 2.8 2.4 292 VH 0.9 M NC=21 NC=315.0 NC=119 NC=55.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent),. ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli-mhas per centimeter), meq/1OOg mawmum of uirty days after testing. by O� IV GOWr H (High), VH (Very High). ENR-Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2= Ibs/A, Soluble Analysis prepared by: Waypoint Analytical Vaginta, Ina r C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Paudc McGroary Page 2 c"K Report 16-110-0682 Account Number:00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received: 04/1912016 Date Of Report: 04/20/2016 r—_ �-Jllb Way oint� ANALYTICAL 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-94010 Fax 804-271-6446 www.waypointa nalytical.com Every acre ... Everyyear. Grower. CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium - Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop veld Goal Lime N PZOs K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A IbfA Ib/A Ib/A 161A IbIA Ib/A MIA Ib/A Ib/A Ib/A FIELDA Berrnudagrass Hay 5 0.0 225 30 86 16 15 0 4 0 1.0 0 FIELD Rye 40 0.0 62 0 14 16 20 0 4 0 1.2 0 FIELD C Rye 40 0.0 62 0 69 27 19 0 4 0 0.9 0 FIELD C Bermudagrass Hay 5 0.5 225 30 162 27 14 0 4 0 0 0 FIELD D Rye 40 0.0 62 0 19 44 19 0 4 0 1.3 0 FIELD D Bermudagrass Hay 5 0.0 225 0 130 44 14 0 4 0 FIELD E Bermudagrass Hay 5 0.0 225 0 40- 31 10 0 0 0 0 0 FIELD E Rye 40 0.0 62 0 23 31 14 0 0 0 0.9 0 FIELD F Rye 40 0.0 62 01 48 0 15 0 3 0 0.7 0 FIELD F Bermudagrass Hay 5 0.0 225 0 137 0 11 0 3 0 0 0 Comments: "The recommendations are based an research data and experience, but NO GUARANTEE or WARRANTY expressed orimplied, concerning crop performance is made." Our reports and letters are for the exclusive and confidentialuse of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the iAaA� work,the results, or the company in any advertising, news. release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 o v — , Repckfv`l; : 16-110-0682 Account Number: 00327 Send To: EHC1nc. PO Box 902 RED SPRINGS NC 28377 Sample(s) : FIELD C Crop: Bermudagrass Hay r Waypoint. ._" ANALYTICAL Apply dolomitic lime to raise pH and improve the magnesium level. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 o Fax 804-271-6446 www.waypointanalytical.com "Every acre... Every year m Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : FIELD C,FIELD D,FIELD E,FIELD F Crop: Bermudagrass Hay Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. Apply N on warm season grass only after late spring when grass starts growing. Sample(s) : FIELD D Crop: Bermudagrass Hay Sodium level is higher than desired, apply gypsum and leaching, with water may be beneficial. Use ammonium sulfate as all or portion of the N requirement to reduce pH. Sample(s) : FIELD D,FIELD E Crop: Bermudagrass Hay Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : FIELD C Crop: Rye Apply, required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : FIELD C,FIELD D,FIELD E,FIELD-F Crop: Rye Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are forthe exclusive and confidential use of our clients„ and may not be reproduced in whole or parR nor may any reference be made to the ?or'. Pc 60w work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977., Pauric McGroary Page 4 O'v-" ReportbL in 16-110-0682 Account Number: 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Waypoint ANALYTICAL "Every acre ... Every year. ",sr SOIL ANALYSIS REPORT Date Received: 04/19/2016 Date Of Analysis: 04/20/2016 Date Of Report: 04/2012016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypolnta nalytica Isom Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION Analytical Method(s): Mehlich 3 Lime Index Loss On Ignition WaterpH OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number % Soil Ihs/A M3 K M 9 Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/1009 meq/100g FIELD G 1.5 275 VH 45 L 34 L 676 H 11574 74 34 L 6.2 6.88 0.5 4.4 MIN L NC=229 NC=23 FIELD H 11575 1.1 68 69 H 104 H 31 L 374 M 70 VH 6.7 0.1 2.8 MIN L NC=57 NC=53 FIELD 1 (1) 2.6 384 VH 216 VH 29 VL 685 M 11576 94 162 VH 6.4 6.88 0.5 5.4 MIN M NC = 320 NO = 110 FIELD I (2) 2.4 401 VH 104 H 42 L 662 H 11577 91 31 L 6.2 6.87 0.6 4.7 MIN L NC=334 NC=53 FIELD J (1) 2.2 199 VH 84 L 62 L 829 H 11578 86 90 H 6.8 0.2 5.5 MIN L NC=166 NC=43 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NON a S Zn .Mn Fe Cu B, SS CI At % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm FIELD G 13 L 13.0 VH 13 M 1.0 M 2.6 2.6 6.4 76.8 3.4 11.4 303 VH 0.8 M NC=27 NC NC=81 NC=50.0 FIELD H 5 VL 4.7 H 5 L 0.9 M 9.5 9.2 66.8 10.9 3.6 249 VH 0.7 M NO = 10 NO = 117.5 NO = 31 NO = 45.0 FIELD 1 (1) 11 L 60.3 VH 4 L 1.2 M 10.3 4.5 63.4 13.0 9.3 327 VH 1.0 M NC=23 NC=1507.5 NC=25 NC=60.0 FIELD 1 (2) 9 VL 23.9 VH 2 VL 0.7 L 5.7 7.4 70.4 2.9 12.8 356 VH 0.8 M NC=19 NC=597.5 NC=13 NC=35:0 FIELD J (1) 7 VL 8.4 VH 44 H 0.6 L 3.9 9.4 75.4 7.1 3.6 164 VH 0.6 M NC=15 NC=210.0 NC=275 NC=30.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies b sample(s) tested. samples ere retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (millfmhos per centimeter), meq/1OOg mazmum or thirty days after testing. by. pod. (hc � � H(High). VH(Very High).ENR- Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2=lbs/A, Soluble Analysis preparetl by. WaypointMalyliwl Virginia, Ina. C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Paude McGroary Page 5OP—ti Repo III,-- r: 16-110-0682 Account Number:00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received:04/19/2016 Date Of Report: 04/20/2016 Wayp®int. Jr, ANALYTICAL "Every acre ... Everyyear. "m 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com SOIL FERTILITY RECOMMENDATIONS Grower. CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION 'Lime Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons T°^s/A Ib/A Ib/A IbIA WA Ib/A Ib/A Ib/A Ib/A MIA Ib/A FIELD G Bermudagrass Hay 5 0.5 225 0 187 46 10 0 4 0 0 0 FIELD G Rye 40 0.0 62 0 72 46 - 13 0 4 . 0 0.8 0 FIELD H Rye 40 0.0 62 30 21 49 20• 0 4 0 0.9 0 FIELD H Bermudagrass Hay 5 0.0 225 30 134 49 15 0 4 0 0 0 FIELD (1) Rye 40 0.0 62 0 0 51 14 0 4 0 0.6 0 FIELD 1 (1) Bermudagrass Hay 5 0.5 225 0 40 51 10 0 4 0 0 0 FIELD 1 (2) Bermudagrass Hay S 0.5 225 0 134 38 11 0 4 0 1.0 0 FIELD 1 (2) Rye 40 0.0 62 0 21 38 16 0 4 0 1.1 0 FIELD J (1) Rye 40 0.0 62 0 62 18 18 0 0 6 1.2 0 FIELD J (1) Bermudagrass Hay 5 0.0 225 0 153 18 13 0 0 0 1.0 0 Comments: 'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients,, and may not be reproduced in whole or part nor may any reference be made to the work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page � qy' Report f�J-._r: 16-110-0682 Account Number: 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Waypoint.. �-J ANALYTICAL Sample(s) : FIELD H,FIELD I (1),FIELD 1(2),FIELD J (1) Crop: Bermudagrass Hay Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. Apply N on warm season grass only after late spring when grass starts growing. 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com "Everyacre...Every year.",., Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION Sample(s) : FIELD H,FIELD I (1),FIELD J (1) Crop: Bermudagrass Hay Sodium level is higher than desired, apply gypsum and leaching with water may be beneficial. Sample(s) : FIELD H,FIELD J (1) Crop: Bermudagrass Hay Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : FIELD I (1),FIELD 1 (2) Crop: Bermudagrass Hay Apply dolomitic lime to raise pH and improve the magnesium level. If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Samples): FIELD H,FIELD I (1),FIELD i (2),FIELD J (1) Crop: Rye Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. Sample(s) : FIELD I (1),FIELD 1 (2) Crop: Rye Apply required magnesium Wth magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made." and Our reports and letters are for the exclusive and confidential use of our Gients„ and may not be reproduced in whale or part,.nor may any reference be made to the flpylcc PAr✓ work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 7 c Report f.-I ar: 16-110-0682 Account Number: 00327 7621 Whitepine Road, Richmond, VA 23237 aypoi nt, Main 804-743-9401 ° Fax 804-271.6446 Send To: EHC Inc. ANALYTICAL www.waypointanalytical.com PO Box 902 "Every acre... Every yearn, Grower. CAMPBELL SOUP RED SPRINGS NC 28377 ANNUAL SOIL SAMPLE SPRAY IRRIGATION SOIL ANALYSIS REPORT AnalyticalMothod(s): Mehlich3 Limelndex LossOnlgnigon WaterpH Date Received: 04/19/2016 Date Of Analysis: 04/20/2016 Date Of Report: 04/20/2016 OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number % Soil Ibs/A M3 K M g Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meg11009 meq/100g FIELD J (2) 3.0 243 VH 134 H 75 L 1016 H 11579 100 119 H 6.5 0.5 7.1 MIN M NC=202 NC=69 FIELD J(3) 1.2 93 H 68 M 37 L 490 H 11580 69 69 H 7.0 0.0 3.2 MIN 1 NC=77 NC=35 FIELD J (4) 2.0 238 VH 89 M 57 L 733 H 11581 83 83 H 6.7 0.2 4.9 MIN L NC=198 NC=46 FIELD J (5) 1.4 64 H 34 VL 112 H 708 H 11583 71 7 VL 6.8 0.1 4.7 MIN L NC=53 NC=17 FIELD J (6) 1.2 93 H 71 M 29 L 385 H 11584 70 47 H 6.8 0.1 2.7 MIN L NC=77 NC=38 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts Chloride Aluminum le ID Field ID K Mg Ca Na H NOaN S Zn Mn Fe Cu B SS Cl Al % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm FIELD J (2) 9 VL 20.3 VH 49 H 0.9 M 4.8 8.8 71.5 1.3 7.1 203 VH 0.8 M NC=19 NC=507.5 NC=306 NC=45.0 FIELD J (3) 5 VL 6.7 H 20 M 0.4 L 5.4 9.6 76.6 9.4 0.0 123 VH 0.5 L NC=10 NC=167.5 NC=125 NC=20.0 FIELD J (4) 6 VL 9.2 VH 63 VH 0.7 L 4.7 9.7 74.6 7.4 4.1 168 VH 0.6 M NC=12 NC=230.0 NC=394 NC=35.0 FIELD J (5) 4 VL 0.9 VL 55 VH 0.5 L 1.9 19.9 75.3 0.6 2.1 188 VH 0.5 L NC=8 NC=22.5 NC=344 NC=25.0 FIELD J (6) 5 VL 7.5 H 13 M 0.4 L 6.7 9.0 71.3 7.6 3.7 88 VH 0.4 L NC=10 NC=187.5 NC=81 NC=20.0 Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (pans per million), Ibs/A This report applies to sample(s) tested. Samples are retained a sod. Rating after each value: VL (Very Low), L(Low), M(Medium), (pounds per acre), ms/cm(milli-mhos per centimeter),meq/1Dag mawmum otteirty days after testing. by fl�oG� H (High), VH (Very High). ENR- Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x2=lbs/A, Soluble Analysis prepared by: WaypointAnalyucal Virginia, Ina ! C:E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Patric McGroary Page 8 c)' Report ! _ Dr. 16-110-0682 Account Number:00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received: 04/19/2016 Date Of Report: 04/20/2016 • Waypoi nt_ 7621 ain 80 -7 Road, Richmond, 27 -6446 Main 804-743-9401 0Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre... Every year.". Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron ple ID F Intended Crop Yield Goal Lime N P205 KZO Mg S Zn Mn Fe Cu d ID Tons Tons0 Ib/A MIA Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A _B Ib/A FIELD J (2) Bermudagrass Hay 5 0.0 225 0 84 5 11 0 0 0 0 0 FIELD J (2) Rye 40 0.0 62 0 27 5 16 0 0 0 0.9 0 FIELD J (3) Rye 40 0.0 62 30 55 43 20 0 3 0 1.4 0.5 FIELD J (3) Bermudagrass Hay 5 0.0 225 80 166 43 15 0 3 0 1.0 0.5 FIELD J (4) Rye 40 0.0 62 0 33 23 19 0 0 0 1.1 0 FIELD J (4) Bermudagrass Hay 5 0.0 225 0 149 23 14 0 0 0 1.0 0 FIELD J (6) Bermudagrass Hay 5 0.0 225 30 199 0 15 2.2 0 0 1.0 0.5 FIELD J (5) Rye 40 0.0 62 30 77 0 20 2.2 0 0 71.3 0.5 FIELD J (6) Rye 40 0.0 62 30 52 51 20 0 4 TO 1.4 0.5 FIELD J (6) Bertnudagrass Hay 5 0.0 225 30 163 51 15 0 4 0 1.0 1 0.5 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or Implied, concerning crop performance is made." p °Gov Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the flpprrc work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 9 c,' ` Report 1 �_ � er: 16-110-0882 J ��...� Account Number:00327 nir23237 Waypoi■ ■ , 7621 Main 804-7 Road, Richmond, 27 -6446 p N Maln 804-743-9401 °Fax 804-271-6446 Send To: EHC Inc. ANALYTICAL www.waypointanalytical.com PO Box902 Every acre... Every year."m Grower: CAMPBELL SOUP RED SPRINGS NC 28377 ANNUAL SOIL SAMPLE SPRAY IRRIGATION Sample(s) : FIELD J (3),FIELD J(4),FIELD J (5),FIELD J (6) Crop: Bermudagrass Hay Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. Apply N on warm season grass only after late spring when grass starts growing. Sample(s) : FIELD J (3),FIELD J (4),FIELD J (6) Crop: Bermudagrass Hay Apply required magnesium with magnesium oxide, Epsom Salts; K-Mag or Sul-PO-Mag. Sodium level is higher than desired, apply gypsum and leaching with water may be beneficial. Sample(s) : FIELD J (3),FIELD J (5),FIELD J (6) Crop: Bermudagrass Hay Boron recommendations are on a broadcast basis. Sample(s) : FIELD J (3),FIELD J (4),FIELD J (5),FIELD J (6) Crop: Rye Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. "The recommendations are based on researchdata and experience, but NO GUARANTEE or WARRANTY expressed or Implied, concerning crop performance Is made." i)° G � Our reports and letters are for the exclusive and confidential use of our clients„ d, and may not be reproduced In whole or panor may any reference be made to the pw;. work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our prior written authorim9on. Copy right 1977. Pauric McGroary Page.10f- `I; Report I er. 16-110-0682 Account Number; 00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 i ' J- T Waypoint, ANALYTICAL "Every acm... Every year. ",r, SOIL ANALYSIS REPORT Date Received: 04/1912016 Date Of Analysis: 04/20/2016 Date Of Report: 04/20/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION Analytical Method(s): Mehlich 3 Lime Index Loss On Ignition Water pH OM Om WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number Soil Ibs/A M3 K M9. Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/1009 meq/100g FIELD J (7) 11585 19 82 203 VH 103 H 54 M 559 M H L MIN NC = 169 NC = 53 69 6.4 6.89 0.4 4.2 FIELD J (8) 11586 1.1 68 77 H 69 M 29 L 402 M L NC=64 NC=35 59- H 6.6 0.2 2.9 MIN FIELLD J (9) 11587 3.0 100 324 VH 149 H 56 L 1110 H 113 H 7.1 0.0 6.9 MIN M NC=270 NC=78 FIELD J (10) 11588 3.3 107 86 H 117 M 62 L 1038 H 107 H 7.0 0.0 6.5 MIN M NC=72 NC=60 FIELD J (11) 1.7 50 M 128 VH 57 M 503 M 11589 79 71 H 6.7 0.2 3.8 MIN L NC=42 NC=65 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID Field ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate mslcm Rate ppm Rate ppm FIELD J (7) 7 VL 13.1 VH 23 H 0.7 L 6.3 10.7 66.5 7.1 9.5 122 VH 0.5 L NC=16 NC=327.5 NC=144 NC=35.0 FIELD J (8) 7 VL 3.5 H 19 M 0.4 L 6.1 8.3 69.3 8.8 6.9 138 VH 0.5 L NC=15 NC=87.5 NC=119 NC=20.0 FIELLD J (9) 7 VL 18.0 VH 25 H 2.1 H 5.5 6.8 80.4 7.1 0.0 305 VH 0.9 M NC=15 NC=450.0 NC=156 NC=105.0 FIELD J (10) 5 VL 10.1 VH 27 H 0.7 L 4.6 7,9 79.8 7.2 0.0 209 VH 0.7 M NC = 10 NC = 252.5 NC = 169 NC = 35.0 FIELD J (11) 7 VL 2.6 M 11 M 0.4 L 8.6 12.5 66.2 8.1 5.3 145 VH 0.5 L NC=15 NC=65.0 NC=69 NC=20.0 Values on this report represenithe plant available nutrients in the Explanation of symbols: %(percent),.ppm (parts per million),Ibs/A This report applies to sample(s) tested. Samples are retained soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. by. POW,, H (High), VH (VeryHigh). ENR- Estimated Nitrogen Release. - (millii-equivalent per 100 grams). Conversions: ppm x2 = Ibs/A, Soluble Analysis prepared by Waypoint Analytical Virginia, Inc G.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Paudc McGroary Page.19( Report L:._ter: 16-110-0682 Account Number:00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received: 04/19/2016 Date Of Report: 04/20/2016 • A _ Waypoint.. ANALYTICAL Everyacre...Every year.". SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE SPRAY IRRIGATION Nitrogen Phosphate . Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yleld Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID Tons Tons/A Ib/A Ib/A Ib/A Ib/A MIA Ib/A Ib/A Ib/A Ib/A Ib/A FIELD J (7) Bermudagrass Hay 5 0.5 225 0 135 26 13 0 3 0 1.0 0.5 FIELD J Cn Rye 40 0.0 62 0 22 26 18 0 3 0 1.1 0.5 FIELD J(8) Rye 40 0.0 62 30 54 51 18 0 3 0 1.4 0.5 FIELD J (8) Bermudagrass Hay 5 0.0 225 30 165 51 13 0 3 0 1.0 0.5 FIEL-D J (9) Rye 40 0.0 62 0 24 24 18 0 3 0 0 0 FIELLD J (9) -- Bermudagrass Hay 5 0.0 225 0 F 40 24 13 0 3 0 0 0 FIELD J (10) Bermudagrass Hay 5 0.0 225 30 117 18 15 0 3 0 1.0 0 FIELD J (10) Rye 40 0.0 62 30 35 18 20 0 3 0 1.1 -0 FIELD J (11) Rye 40 0.0 62 30 15 23 18 0 4 LO 1.4 0.5 FIELD J (11) Bermudagrass Hay 5 0.0 225 31 97 23 13 0 4 0 1.0 0.5 Comments: "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, conceming crop performance is made." pod.Our reports and letters are for the exclusive and confidential use of our clients,. and may not be reproduced in whole or part, nor may any reference be made to the f attar` Par work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977: Pauric McGroary n ° Report,. _,o'ner. 16-110-0682______ _ • r _ ____—�____ _ ___T _ Account Number: 00327 �l1/aypoi nt 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 0 Fax 804-271-6446 Send To: EHC Inc. ANALYTICAL www.waypointanalytical.com POBox 902 "Every acre... Every year. Grower CAMPBELLSOUP RED SPRINGS NC 28377 ANNUAL SOIL SAMPLE SPRAY IRRIGATION Sample(s) : FIELD J (8),FIELD J (11) Crop: Bermudagrass Hay Boron recommendations are on a broadcast basis. Sample(s) : FIELD J (8),FIELLD J (9),FIELD J (10),FIELD J (11) Crop: Bermudagrass Hay Apply additional 65 pounds of nitrogen after every cutting and harvest of hay, Apply N on warm season grass only after late spring when grass starts growing. Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sodium level is higher than desired, apply gypsum and leaching with water may be beneficial. Sample(s) : FIELLD J (9) Crop: Bermudagrass Hay Use ammonium sulfate as all or portion of the N requirement to reduce pH. Sample(s) : FIELD J (8),FIELLD J (9),FIELD J (10),FIELD J (11) Crop: Rye Apply the sulfur recommendation in sulfate form with the spring application.of N. Note: thiosulfate doesn't contain sulfate. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, conceming crop performance is made." p Our reports and letters are for the exclusive and wnfidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the LAwi6 and �°Di' work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 1 of Report N' r: 16-110-0681 _AW Account Number: 00327 � -Waypoint_ Send To: EHC Inc. ANALYTICAL PO- Box .902 "Every acre... Everyyear. "n RED SPRINGS NC 28377 Submitted By: JOSH BASS SOIL ANALYSIS REPORT Date Received: 04/19/2016 Date Of Analysis: 04/20/2016 Date Of Report: 04120/2016 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical.com Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE LAND APPLICATION RESIDUALS Analytical Method(s): Mehllch 3 Lime Index Loss On Ignition WaterpH CM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab Field ID Number �o Soil IbsIA M3 K M 9 Ca Na Soil Buffer H Rate Class ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate pH Index meg1100g meq/1009 SITE-1 11661 1.7 81 124 VH 36 VL 32 M 195 L 8 VL 5.1 6.85 0.8 2.2 MIN L NC=103 NC=18 SITE-2 1.5 104 VH 23 VL 77 H 389 M 11562 76 2 VL 6.3 6.90 0.3 3.0 MIN L NC=87 NC=12 SITE-3 7.7 181 VH 132 H 222 H 1110 M 11563 150 20. VL 6.0 1.4 9.2 MIN VH NC=151 NC=68 SITE-4 2.2 79 H 56 L 92 M 757 M 11564 86 8 VL 6.0 6.84 0.9 5.6 MIN L NC = 66 NC = 29 SITE 5 3.7 234 VH 95 M 147 H 668 M 11565 116 35 L 6.2 6.86 0.7 5.7 MIN M M NC = 195 NC = 49 Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron soluble Salts Chloride Aluminum SamPercent pID le ID Field K Mg Ca Na H N%N S Zn Mn Fe Cu B SS Cl AI % % % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm SITE-1 12 L 4.0 H 20 M 0.9 M 4.2 12.1. 44.3 1.6 36.4 200 VH 0.4 L NC=25 NC=100.0 NC=125 NC=45.0 SITE-2 6 VL 3.7 H 22 H 0.5 L 2.0 21.4 64.8 0.3 10.0 188' VH 0.4 L NC=12 NC=92.5 NC=138 NC=25.0 SITE-3 15 L 4.7 H 99 VH 1.3 M 3.7 20.1 -60.3 0.9 15.2 201 VH 0.5 L NC=31 NC=117.5 NC=619 NC=65.0 SITE-4 8 'VL 5.3 H 19 M 0.5 L 2.6 13.7 67.6 0.6 16.1 108 VH 0.4 L NC=17 NC=132.5 NC=119 NC=25.0 SITES 9 VL 3.4 M 146 VH 1.1 M 4.3 21.5 58.6 2.7 12.3 252 VH 0.6 M NC=19 NC=85.0 NC=913 NC=55.0 Values on this report represent the plant available nutrients in the Explanation of symbols: A(percent), ppm (parts per million), Ibs/A This report applies to samples) tested. Samples are retained soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days aftertest rig. 4 rd/ H (High), VH (Very High). ENR- Estimated Nitrogen Release, (milli -equivalent per 100 grams). Conversions: ppm x2= Ibs/A, Soluble Analysis prepared by: WaypoinlAnalytical Virginia, Inc by: Pd�« IV 60 C.E.C. - Cation Exchange Capacity. Salts rii x 640 = ppm. Paudc McGroary Page 2 of, Report Ntb,:_ r: 16-110-0681—� Account Number:00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received: 04/19/2016 Date Of Report: 04/2012016 �C i Waypoi nt 7621 ain 804-7 Road, Richmond, 27 -W6 Main 804-743-9401 °Fax 804-271-6446 ANALYTICAL www.waypointanalytical.com "Every acre ...Everyyear.",,. Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE Submitted By: JOSH BASS LAND APPLICATION RESIDUALS SOIL FERTILITY RECOMMENDATIONS Nitrogen Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron Sample ID Intended Crop Yield Goal Lime N P205 K20 Mg S Zn Mn Fe Cu B Field ID bu Tons/A Ib/A Ib/A Ib1A MIA Ib/A Ib/A Ib/A Ib/A Ib/A WA SITE-1 Rye 40 1.0 62 0 76 48 14 0 3 0 0.9 0.5 SITE-1 Bennudagrass Hay 5 1.0 225 30 197 48 10 0 3 0 0 0.5 SITE-2 Bermudagmss Hay 5 0.6 225 30 213 3 14 0 3 0 1.0 0.5 SITE-2 Rye 40 0.0 62 0 62 3 19 0 3 0 1.3 0.5 SITE-3 Xmas -Pine 0 0.0 0 22 0 20 0 0 0 0 2.5 SITE-4 Rye 40 0.8 62 30 77 0 17 0 3 0 1.3 0.6 SITE-4 Bermudagrass Hay 5 0.8 225 30 176 0 12 0 3 0 1.0 0.5 SITE 5 Rye 40 0.0 62 0 53 0 16 0 0 0 0.7 0 SITE 5 Bermudagrass Hay 5 0.5 225 0 143 0 11 0 0 0 0 0 Comments: 'The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."�pp m° G Our reports and letters are for the exclusive and confidential use of our clients., and may not be reproduced in whole or part nor may any reference be made to the low,. 0w work,the results, or the company In any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary Page 3 of, Report N', _ : r 16-110-0681 Account Number:00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Sample(s) : SITE-2 Crop: Bermudagrass Hay M .A WaY- - p--oint, -- ANALYTICAL "Every acre... Every year.". Submitted By: JOSH BASS 7621 Whitepine Road, Richmond, VA 23237 - Main 804-743-9401 a Fax 804-271-6446 www.waypointanalVtical.com If dolomitic lime is not used, apply required magnesium with magnesium oxide. Epsom Salts, K-Mag or Sul-PO-Mag. Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE LAND APPLICATION RESIDUALS Sample(s) : SITE-2,SITE-4 Crop: Bermudagrass Hay Boron recommendations are on a broadcast basis. Sample(s) : SITE-2,SITE4,SITE 5 Crop: Bermudagrass Hay Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. Apply N on warm season grass only after late spring when grass starts growing. Sample(s) : SITE-4 Crop: Bermudagrass Hay Apply dolomitic lime to raise pH and improve the magnesium level. Sample(s) : SITE-2 Crop: Rye Apply required magnesium with magnesium oxide, Epsom Salts, K-Mag or Sul-PO-Mag. Sample(s) : SITE-2,SITE4,SITE 5 Crop: Rye Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. Sample(s) : SITE-3 Crop: X'mas- Pine . Apply 1/2 oz. actual N per tree one month after planting. For transplants, incorporate 1/2 Ibs actual N per 400 sq.ft.. prior to planting or two weeks after planting. For the second year, apply 1/2 oz. Actual N per tree in spring. After the second year, apply 1/2 oz. actual N per tree in the Spring and again in the Fall until harvest. " Apply 112 oz. Actual tJ per tree one month after planting. For transplants incorporate 1/2# actual N per 400.sq.ft.. prior to planting or 1/2# actual N peg 400 sq.ft.. two weeks after planting. For Fraser firs after 2nd year apply 1 oz. Actual N per tree 2-4 weeks prior to bud break. For pine Christmas trees apply 1/2 to 1 oz. of actual N per tree 2-4 weeks prior to bud break depending on previous years growth. Boron recommendations are on a broadcast basis. If this soil is organic sand, no lime is needed for soil with pH 5.2 or above. , If the soil pH is lower than 5.2 then apply 1.0 ton per acre. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or Implied, concerning crop performance Is made." me G Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the PAWre °o" work,the results, or the company in my advertising, news release, or other public anauncements without obtaining our prior written authorization. Copy right 1977. Pauric MGGroary Page 4 of; r Report NGmr er: 16-110-0681 °.` r Account Number:00327 Waypoint Send To: EHC Inc. ANALYTICAL PO Box 902 "Every acre ... Every year.'a, RED SPRINGS NC 28377 Submitted By: JOSH BASS SOIL ANALYSIS REPORT IN-.- ns n—r...1— nnrommnaa n=m of Rcnnrt- 171d/7017n1R 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 a Fax 804.271-6446 www.waypointanalytical.com Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE LAND APPLICATION RESIDUALS Analytical Method(s): Mehlich 3 Lime Index Loss On Ignition Water pH OM WN ENR Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab % Soil M3 K Mg Ca Na Soil Buffer H Field ID Number Class Ibs/A Rate Rate Rate Rate ppm Rate ppm Rate ppm Rate PH Index meg1100g meglt00g Rate ppm ppm ppm ppm SITE-6 1.4 119 VH 75 M 103 H 550 M 35 L 7.0 0.0 4.0 11666 72 MIN L NC=99 NC=38 SITE-7 4'6 241 VH 140 H 140 H 687 M 16 VL 5.9 6.83 1.0 6.0 11567 133 MIN M NC=201 NC=72 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron I Soluble Salts Chloride Aluminum' Sample ID K Mg Ca Na H NOaN S Zn Mn Fe Cu B SS Cl Al Field ID % % I "/a % I % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate mslcm Rate ppm Rate ppm SITE-6 4.8 21.5 68.8 3.8 0.0 7 VL 1.7 L 36 H 193 VH 0.7 L 0.5 L NC=15 NC=42.5 NC=225 NC=35.0 SITE-7 13 L 5.2 H 107 VH 236 VH 1.7 H 0.6 M 6.0 19.4 57.3 1.2 16.7 NC=27 NC=130.0 NC=669 NC=85.0 Values an this reportrepresentthe plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to samples) tested. samples are retained a soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days a tertesting. by Prate. IV 601, / H (High), VH (Very High). ENR-Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x2= Iti Soluble Analysis prepared by WaypointAnalylical Virginia, Inc 0 C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Paudc McGroary Page 5 of Report N1,.__`_r: 16-110-0681 Account Number:00327 Send To: EHC Inc. PO Box 902 RED SPRINGS NC 28377 Date Received: 04/19/2016 Date Of Report: 04/20/2016 Waypoint ANALYTICAL "Everyacre...Every year. "TM Submitted By: JOSH BASS SOIL FERTILITY RECOMMENDATIONS 7621 Whitepine Road, Richmond, VA23237 Main 804-743-9401 a Fax 804-271-6446 www.waypointanalytical. corn Grower: CAMPBELL SOUP ANNUAL SOIL SAMPLE LAND APPLICATION RESIDUALS Phosphate Potash Magnesium Sulfur Zinc Manganese Iron Copper Boron eIDYield FFITIT111) Intended Crop Goal LimeNitrogen N P205 16i0 Mg S Zn Mn Fe Cu B Tons Tons/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A Ib/A INA MIA SITE-6 Bermudagrass Hay 5 0.0 225 30 160 0 13 0 0 0 1.0 0.5 SITE-6 Rye 40 0.0 62 0 47 0 18 0 0 0. 1.1 0.5 SITE-7 Bermudagrass Hay 5 0.8 225 0 68 0 10 0 0 0 0 0 SITE-7 Rye 40 0.8 62 0 25 0 13 0 0 0 0 0 Comments: Sample(s) : SITE-7 Crop: Bermudagrass Hay Apply additional 65 pounds of nitrogen after every cutting and harvest of hay. Apply N on warm season grass only after late spring when grass starts growing. Sample(s) : SITE-7 Crop: Rye Apply the sulfur recommendation in sulfate form with the spring application of N. Note: thiosulfate doesn't contain sulfate. The above N recommendation on small grain is the total amount of fall plus spring applications. Apply only 15-20# N in the fall and the balance right before the growth starts in the spring. "The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or Implied; concerning crop performance is made." Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the Tp4r�6 work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977. Pauric McGroary 2016 Application Summary Table r ,, ., Campbell Soup Supply Company Land Applica0on Program Permit NW00004893 2n16 Annncaunn 4nnm- .. � _._f rac Site Field Acres Dates read __.__"..__.._.. Gallons ,Pounds __......_., D Tons/Acre Dry T,4 y Solids i.....,,i CropPAN PAN n, Tons/Acre DryTons amp a eup Supply Company S 1 5.1 1126116 16,057 133.915 0.3768 1.9217 2.87 Rye Grass 7.7252 58.93 4.4925 22.9115 3/24116 10,554 88.020 0.2477 1.2631 2.87 Rye Grass 5.0776 4126116 15244 127132 0.8239 4.2017 6.61 Bermuda 9.5964 7129116 14,602 121,780 0.7355 3.7508 6.16 Bermuda 8.3436 9/9/W 5.964 49.740 0.3004 1.5320 6.16 Bermuda 3.4076 9/19/16 19,734 164,580 0.9939 5.0691 6.10 Bermuda 11.2752 9/20/16 5,434 4 45a2M 0.2737 1.3959 6.16 Bermuda 3.1048 9/28/2016 14,705 122,640 1 0.7406 3.7773 6.16 Bermuda 8.4019 Campbell Soup Supply Company s 2 8.4 8/23/16 11,297 94,220 0.3455 2.9020 0.18 Bermuda 3.9190 3.92 0.3455 2.9020 Campbell Soup Supply Company S 3 26 1/5/16 19.719E153.260 60 0.0908 2.3600 2.87 Pine Trees 1.8610 19.75 1.2679 32.7055 WOMB 21,01670 0.0987 2.5151 2.87 Pine Trees 1.9833 2/26/16 6,0620 0.0279 0.7255 2.87 Pine Trees 0.5721 2127/16 17,07940 0.0788 2.0440 2.87 Pine Trees 7.8178 3/8/18 18,57340 0.0901 2.3425 - 2.87 Pine Trees 1,8471 3/17/16 10,6280 0.0489 1.2720 Z. .Pine Trees 1.0030 W18/2016 7,3200' 0.0337 '0.8761 2.87 Pine Trees 0.6908 5/1112016' 12,66200 0.1342 3,4901 6.61 Pine Trees 1.5636 5/26/2016 19,82000 0.2101 5.4632 8.61 'Pine Trees 2.4475 -6/9/2016 78,11360 0.1920 4.9925 6.61 Pine Trees 2:2387 620/2018 18,37860 0.1948 5.0652 6.87 Pine Trees 2.2692 10/17/2016 15 835 140.410 0.0122 0.3159 0.45 Pine Trees 0.3378 12/2/2016 15 516 129,400 0.0112 0.2912 0.45 Pine Trees 0.3113 12/9/2016 - 19 072 159,060 0.0138 0.3579 0.45 Pine Trees 0,3827 12/16/2018 16,101 134,280 0,0116 0.3021 0.45 Pine Trees 0.3231 12/27/2016 16.568 129.840 0.0112 0.2921 0.45 Pine Trees 0.3124 Campbell Soup Supply Company S 4 9.1 1112/16 19,192 160,060 0.2524 2.2969 2.87 Pine Trees 5,1748 32.43 2.1967 19.9898 2/2/16 18,890 167,540 0.2484 2.2607 2.57 Pine Trees 5.0933 219/16 5 691 47.460 0.0748 0.6811 2.87 Pine Trees 1.5344 4113116 15.683 130,800 0.4750 4.3229 6.61 Pine Trees 5.5334 7/7/78- 12,329 102 820 0.3480 3.1669 6.16 Pine Trees 3.9478 7119/16 17348 144680 0.4897 4A561 6.16 Pine Trees 5.5550 7/21116 6,420 53,540 0.1812 1 1.6490 6.16 Pine Trees 2.0557 10/26/2016 18 494 154,240 0.0381 0.3470 0.45 Pine Trees 1.0603 11/3/2016 11 458 95 560 0.0235 0.2150 0.45 Pine Trees 0.5569 11/9/2016 11029 91980 0.0227 0.2070 0.45 Pine Trees 0.6323 11/15/2016 1,693 14.120 0.0035 0.0318 0.45 Pine Trees 0.0971 11/23/2016 18.942 - 157980 0.0391 0.3555 0.45 Pine Trees 1.0860 Campbell Soup supply Company S 5 3.4 1/19/16 5,724 47,740 0.2015 0.6851 2.87 Rye Grass 4.1310 22.85 1.0393 3.5336 1126116 6,727 56,100 0.2368 0.8050 2.87 Rye Grass 4.8544 2/9/16 - 11,065 -92,280 0.3895 1.3242 2.87 Rye Grass 7.9850 10/5/16 13,655 113,880 0.0754 0,2562 0.45 Rye Grass 2.0952 1119116 8,595 71.680 0.0474 0.1613 0.45 Rye Grass 1.3188 11/15/18 16.082 134.120 0.0888 0.3018 0.45 Rye Grass 2.4676 Campbell Soup WRY Company S 6 2.3 8/30/18 8,926 74,440 0.9968 2.2928 6.15 Bermuda 11.3083 26.51 2.3365 5.3740 919116 11,995 100,040 1.3397 1 3.0812 6.16 Bermuda 16.1972 uppy Company S 7 25 8/8/16 14,002 116,778 3" 6.18 Bermutla8.3207 58CampbellSoup 1 12.6452 , 130,960 14334 67 033fi 616 . Bermuda 18.3027 8/23/2016 8,254 68,840 0.8481 2.1203 5.16 Bermuda 9.6209 8/30/2016 11,269 93,980 1.1578 1 2.8946 6.16 1 Bermuda 13.1345 Numberof Field Applied to: 7 56.8 Campbell Soup Supply Company DAF Sludge, Maaton , NC 656.218 5,472,835 10D.0616 Rye Grass - Jan, Feb, Mar, Apr 100.0616 lstgtr Pan 10251 2nd qtr Pan 5824 3rdgtr Pan 5672 4th qtr Pan 13901 50 lb. limit winter months Bermuda dormant during fall lslgtrsolids 2.87 2nd qtr solids 6.61 3rd qtr solids 6.16 401 qtr solids 0.45 2016 Application Condition Summaries Campbell Soup Supply Company Maxton, North Carolina WQ0004893 1st Quarter DAF Residuals Farmer: Campbell Soup Supply Company 5.1 Site/Tract: S Application Method: Surface Field: I Percent Solids: 2.87 Residual Report No: 16-005-9202 Crop: Winter Rye Grass Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 1/26/2016 1 16,057 Dry Clear 0 3/24/2016 1 10,554 Dry Clear 0 Total Gallons 26,611 r Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company 5.1 Site/Tract: S Application Method: Surface Field: I Percent Solids: 6.61 Residual Report No: 16-096-9204 Crop: Bermuda Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 4/26/2016 1 15,244 Dry Clear 0 Total Gallons 15,244 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company 5.1 Site/Tract: S Application Method: Surface Field:1 Percent Solids: 6.16 Residual Report No: 16-267-0227 Crop: Bermuda Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 7/29/2016 1 14,602 Dry Clear 0 9/9/2016 1 5,964 Dry Clear 0 9/19/2016 1 19,734 Dry Rain 0.1 9/20/2016 1 5,434 Dry Rain 0.2 9/28/2019 1 14,705 Dry Clear 0 Total Gallons 60,439 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company 8.4 Site/Tract: S Application Method: Surface Field: 2 Percent Solids: 6.16 Residual. Report No: 16-267-0227 Crop: Bermuda ' Weather Prev. 24 Hour Date Field No. Gallons Soil Conditions Conditions Rainfall 8/23/2016 2 11,297 Dry Clear 0 Total Gallons 1 1 12,297 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 1st Quarter DAF Residuals Farmer: Campbell Soup Supply Company 26 Site/Tract: S Application Method: Surface Field: 3 Percent Solids: 2.87 Residual Report No: 16-005-9202 Crop: Pine Trees ' Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 1/5/2016 3 19,719 Dry Clear 0 2/18/2016 3 21,016 Dry Clear 0 2/26/2016 3 6,062 Dry Clear 0 2/27/2016 3 17,079 Dry Clear 0 3/8/2016 3 19,573 Dry Clear 0 3/14/2016 3 10,628 Dry Clear 0 3/18/2016 3 7,320 Dry Clear 0 Total Gallons 101,397 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 26 Site/Tract: S Application Method: Surface Field: 3 Percent Solids: 6.61 Residual Report No: 16-096-9204 Crop: 'Pine Trees Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 5/11/2016 3 12,662 Dry Cloudy 0 5/26/2016 3 19,820 Dry Clear 0 6/9/2016 3 18,113 Dry Clear 0 6/20/2016 3 18,376 Dry Clear 0 Total Gallons 68,971 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 4th Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 26 Site/Tract: S Application Method: Surface Field: 3 Percent Solids: 0.45 Residual Report No: 16-308-0204 Crop: Pine Trees Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 10/17/2016 3 16,836 Dry Clear 0 12/2/2016 3 15,516 Dry Clear 0 12/9/2016 3 19,072 Dry Clear 0 12/16/2016 3 _ 16,101 Dry Clear 0 12/27/2016 3 15,568 Dry Clear 0 Total Gallons 83,093 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 1st Quarter DAF Residuals Farmer: Campbell Soup Supply Company 9.1 Site/Tract: S Application Method: Surface Field: 4 Percent Solids: 2.87 Residual Report No: 16-005-9202 Crop: Winter Rye Grass Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 1/12/2016 4 19,192 Dry Clear 0 2/2/2016 4 18,890 Dry Cloudy 0 2/19/2016 4 5,691 Dry Cloudy 0.2 Total Gallons 43,773 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 2nd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 9.1 Site/Tract: S Application Method: Surface Field: 4 Percent Solids: 6.61 Residual Report No: 16-096-9204 Crop: Bermuda Weather Prev. 24 Hour 'Date Field No. Gallons Soil Conditions Conditions Rainfall 4/13/2016 4 15,683 Dry Cloudy 0 Total Gallons 1S,683 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 9.1 Site/Tract: S Application Method: Surface Field: 4 Percent Solids: 6.16 Residual Report No:16-267-0227 Crop: Rye Grass Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 7/7/2016 4 12,329 Dry Clear 0 7/19/2016 4 17,348 Dry Rain 0.7 7/21/2016 4 6,420 Dry Clear 0 Total Gallons 1 36,097 I/J Campbell Soup Supply Company Maxton, North Carolina WQ0004893 4th Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 9.2 Site/Tract: S Application Method: Surface Field: 4 Percent Solids: 0.4S Residual Report No: 16-308-0204 Crop: Rye Grass Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 10/26/2016 4 18,494 Dry Clear 0 11/3/2016 4 11,458 Dry Clear 0 31/9/2016 4 11,029 Dry Clear 0 11/15/2016 4 1,693 Dry Clear 0 11/23/2016 4 18,942 Dry Clear 0 Total Gallons 1 61,616 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 1st Quarter DAF Residuals Farmer: Campbell Soup Supply Company 3.4 Site/Tract: S Application Method: Surface Field: 5 Percent Solids: 2.87 Residual Report No: 16-005-9202 Crop: Winter Rye Grass Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 1/19/2016 5 5,724 Dry Clear 0 1/26/2016 5 6,727 Dry Clear 0 2/9/2016 5 11,065 Dry Rain 0.2 Total Gallons 23,516 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 4th Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 3.4 Site/Tract: S Application Method: Surface Field: 5 Percent Solids: 0.45 Residual Report No: 16-308-0204 Crop: Bermuda Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 10/5/2016 5 13,655 Dry Clear 0 11/9/2016 5 8,595 Dry Clear 0 11/15/2016 5 16,082 Dry Clear 0 Total Gallons 38,332 Campbell Soup Supply Company Maxton, North Carolina WQ0004893 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 2.3 Site/Tract: S Application Method: Surface Field: 6 Percent Solids: 6.16 Residual Report No:16-267-0227 Crop: Bermuda - Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 8/30/2016 6 8,926 Dry Clear 0 9/9/2016 6 11,995 Dry Clear 0 Total Gallons 1 20,921 Campbell Soup Supply Company Maxton, North Carolina. WQ0004993 3rd Quarter DAF Residuals Farmer: Campbell Soup Supply Company Acres: 2.5 Site/Tract: S Application Method: Surface Field: 7 Percent Solids: 0.45 Residual Report No: 16-308-0204 Crop: Bermuda Grass Weather Date Field No. Gallons Soil Conditions Conditions Prev. 24 Hour Rainfall 8/8/2016 7 14,002 Dry Rain 0.1 8/16/2016 .7 15,703 Dry Clear 0 8/23/2016 7 8,254 Dry Clear 0 8/30/2016 7 11,269 Dry Clear 0 Total Gallons 49,228