WQ0034688_2023 Residual Annual Report_20240228 (2)

Initial Review
Reviewer
nathaniel.thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0034688
Applicant/Permittee Neuse Regional Water and Sewer Authority
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Washington
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0034688
Has Current Existing permit number
Applicant/Permittee Address* 435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name* Neuse Regional WASA Class A Residuals Program
Please provide comments/notes on your current submittal below.
Submission of the 2023 Annual Report for Neuse Regional Water and Sewer Authority, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
NeUse NC 2023 Annual Report FINAL.pdf 4.02MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tl�
Submission Date 2/28/2024

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 28, 2024
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report for Permit No. WQ0034688
Dear NCDEQ:
SYNAGRO
Synagro is submitting an electronic copy of the above referenced report on behalf of Neuse
Regional Water and Sewer Authority, NC.
If you have any questions or need additional information, please do not hesitate to contact
Charlie Colie at [phone] or Matthew Carter at 336-705-9886.
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Charlie Colie, Neuse Regional Water and Sewer Authority
Matthew Carter, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

NEUSE REGIONAL WATER AND SEWER
AUTHORITY
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0034688
2023 ANNUAL REPORT

Neuse Regional Water and Sewer Authority, NC
Residuals Land Application Program
2023 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: WO0034688 County Lenoir Year 2023
Facility Name (as shown on permit) Neuse Regional Water Treatment Plant NPDES No. NC0088111
Land Application Operator S�nagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip PartA, and Part B and proceed to PartC. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: N/A
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 314.49
Total number of acres utilized for land application during the year: 85.00
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water Quality X YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
l . Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the pen -nit and reported during the year as required and three (3 )
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T. I 105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .l 111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11, Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
r
Harold Herring, Executive Director
Permittee Name and Title (type or print) Signature a ennittee ate
Signature of Preparer* Date S nWe of Lard Applier Date
(if different from Pennittee) (if different rom Permittee and Preparer)
*Prepares is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2023 - 12/31/2023
NEUSE REGIONAL WASA, NC
NEUSE REGIONAL WASA, NC WTP LIQUID
MONTH/YEAR
October 2023
TOTAL
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/6/2024 1:21:05 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
2,664,900.00
G
314.49
D
285.24
2,664,900.00
G
314.49
D
285.24

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0034688 Laboratory:
Facility Name: NEUSE REGIONAL WASA, NC Waypoint Analytical Virginia Inc.
Residual Source WQ # or
NPDES#: NCO088111
WWTP Name: NEUSE REGIONAL WASA WTP
Residual Analysis Data
Product Type
Sample or Composite Date
WPL
02/27/23
WPL
04/12/23
WPL
07/18/23
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
2.06
1.51
2.83
Arsenic
75
<23.8
<33.3
<17.9
Cadmium
85
<4.76
<6.67
<3.57
Copper
4300
32
109
128
Chromium
NA
29.1
18.2
18.8
Lead
840
19.1
27.8
12.4
Mercury
57
<8.81
<12.3
<6.79
Molybdenum
75
<11.9
<16.7
<8.93
Nickel
420
15.3
<16.7
14.4
Selenium
100
<23.8
<33.3
<17.9
Zinc
7500
96.7
99.3
88.2
Total Phosphorus
NA
2240
3550
3230
TKN
NA
15700
68700
<8930
Ammonia -Nitrogen
NA
<4760
7000
<3570
Nitrate and Nitrite
NA
<238
<333
<179
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for wing violations."
1*
Signatu of Preparer` Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF (12/2006)
Printed: 2/6/2024 4:42:32 PM For: 1703 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WO Permit Number:
WQ0034688
Facility Name:
NEUSE REGIONAL WASA, NC
Residual Source
NPDES # or WQ#:
NCO088111
WWTP Name:
NEUSE REGIONAL WASA WTP
Residual Analysis Data
Product Type
Sample or Composite Date
Parameters (mg/kg dry weight)
Aluminium
Calcium
Magnesium
pH (s.u.)
Potassium
Sodium
PAN
SAR (Ratio)
Laboratory:
Waypoint Analytical Virginia Inc.
WPL WPL WPL
02/27/23 04/12/23 07/18/23
148000
165000
133000
<2380
<3330
3070
1410
1250
1230
5.80
6.90
6.80
1430
1150
982
<1190
1770
<893
<8902
28501
<5536
0.6829
0.8129
0.5773
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Signature o Preparer' Date
`Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 2/6/2024 4:43:33 PM For: 1703 01 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
3/9/2023
Synagro Central LLC
Matthew Carter
284 Boger Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-059-0002
Project Description: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Matthew Carter:
Waypoint Analytical Virginia, Inc. received sample(s) on 2/28/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-059-0002
Client Project Description: NRWASA
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
61095
NRWASA
Solids
02/27/202310:45
02/28/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

WayPANALYTICAL
46431
Synagro Central LLC
Project NRWASA
Matthew Carter
284 Boger Rd
Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Number : 23-059-0002 REPORT OFANALYSIS
Report Date : 03/09/2023
Received : 02/28/2023
Brandi Watson
Lab No : 61095
Sample ID: NRWASA
Matrix: Solids
Sampled: 2/27/2023 10:45
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.9
%
0.010
1
03/02/2316:00
FMM
SM-2540G
Phosphorus
2240
mg/Kg -
dry
238
1
03/06/23 21:59
TJS
6010D
Sulfur
9240
mg/Kg -
dry
476
1
03/06/23 21:59
TJS
6010D
Calcium
<2380
mg/Kg -
dry
2380
1
03/06/23 21:59
TJS
6010D
Aluminum
148000
mg/Kg -
dry
238
1
03/06/23 21:59
TJS
6010D
Manganese
1200
mg/Kg -
dry
23.8
1
03/06/23 21:59
TJS
6010D
Copper
32.0
mg/Kg -
dry
23.8
1
03/04/23 04:13
JTR
6010D
Zinc
96.7
mg/Kg -
dry
59.5
1
03/04/23 04:13
JTR
6010D
Organic N
15710
mg/Kg -
dry
11900
1
03/07/23 09:30
CALCULATION
Nickel
15.3
mg/Kg -
dry
11.9
1
03/04/23 04:13
JTR
6010D
Lead
19.1
mg/Kg -
dry
14.3
1
03/04/23 04:13
JTR
6010D
Arsenic
<23.8
mg/Kg -
dry
23.8
1
03/06/23 21:59
TJS
6010D
Selenium
<23.8
mg/Kg -
dry
23.8
1
03/06/23 21:59
TJS
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids 2.06 % 0.010 1 03/02/23 16:00 FMM SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

WayPANALYTICAL
46431
Synagro Central LLC
Matthew Carter
284 Boger Rd
Mocksville , NC 27028
Report Number : 23-059-0002
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Project NRWASA
Information :
REPORT OFANALYSIS
Report Date : 03/09/2023
Received : 02/28/2023
Brandi Watson
Lab No : 61095
Sample ID: NRWASA
Matrix: Solids
Sampled: 2/27/2023 10:45
Total Kjeldahl Nitrogen
15700
mg/Kg -
dry
11900
1
03/07/23 09:30
JPJ ;M-4500-NH3C-TKl`
Potassium
1430
mg/Kg -
dry
476
1
03/06/23 21:59
TJS
6010D
Magnesium
1410
mg/Kg -
dry
238
1
03/06/23 21:59
TJS
6010D
Sodium
<1190
mg/Kg -
dry
1190
1
03/06/23 21:59
TJS
6010D
Iron
31800
mg/Kg -
dry
476
1
03/04/23 04:13
JTR
6010D
Ammonia Nitrogen
<4760
mg/Kg -
dry
4760
1
03/07/23 14:00
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<238
mg/Kg -
dry
238
1
03/08/23 15:40
ZBD
4500NO3F-2011
Cadmium
<4.76
mg/Kg -
dry
4.76
1
03/06/23 21:59
TJS
6010D
Chromium
29.1
mg/Kg -
dry
11.9
1
03/04/23 04:13
JTR
6010D
Mercury
<8.81
mg/Kg -
dry
8.81
1
03/02/23 12:35
FDS
SW-7471B
pH
5.8
S.U.
1
03/07/2310:44
SAR
9045D
Total Volatile Solids
36.3
%
0.010
1
03/02/23 16:00
FMM
SM-2540G
Molybdenum
<11.9
mg/Kg -
dry
11.9
1
03/04/23 04:13
JTR
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypointo
ANALYTICAL
Client: Synagro Central LLC
Project: NRWASA
Lab Report Number: 23-059-0002
Date: 3/8/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 92126 (MW2 Soil 10'-12')
Analyte: Aluminum
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Iron
QC Batch No: L667775/L667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Iron
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Potassium
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 92126 (MW2 Soil 10'-12')
Analyte: Selenium
QC Batch No: 1-668064/1-667415
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 93579 (Soil)
Analyte: Mercury
QC Batch No: 1-667310/1-667045
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46431
Customer Name: Synagro Central LLC
Report Number: 23-059-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 02/28/2023 11:36:22
Page 6 of 7

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Page 7of7

Waypointo
ANALYTICAL
4/24/2023
Synagro Central LLC/ Neuse Reg WASA
Marshall Puryear
284 Boger Road
Suite 204
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-103-0009
Project Description: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Marshall Puryear:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/13/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-103-0009
Client Project Description: NRWASA
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
61748
NRWASA
Solids
04/12/202311:00
04/13/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 8

waypANALYTICAL
00454
Synagro Central LLC/ Neuse Reg WASA Project NRWASA
Marshall Puryear
284 Boger Road Information
Suite 204
Mocksville , NC 27028
Report Number : 23-103-0009
Lab No : 61748
Sample ID: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 04/24/2023
Received : 04/13/2023
Brandi Watson
Matrix: Solids
Sampled: 4/ 12/ 2023 11:00
Test
Results
Units
MQL
DF
Date / Time
Analyzed
By
Analytical
Method
Moisture
98.5
%
0.010
1
04/19/23 07:49
CJR
SM-2540G
Phosphorus
3550
mg/Kg -
dry
333
1
04/20/23 03:02
BKN
6010D
Sulfur
10900
mg/Kg -
dry
667
1
04/20/23 03:02
BKN
6010D
Calcium
<3330
mg/Kg -
dry
3330
1
04/20/23 03:02
BKN
6010D
Aluminum
165000
mg/Kg -
dry
333
1
04/20/23 03:02
BKN
6010D
Manganese
2230
mg/Kg -
dry
33.3
1
04/20/23 03:02
BKN
6010D
Copper
109
mg/Kg -
dry
33.3
1
04/20/23 03:02
BKN
6010D
Zinc
99.3
mg/Kg -
dry
83.3
1
04/20/23 03:02
BKN
6010D
Organic N
61670
mg/Kg -
dry
16670
1
04/21/23 13:15
CALCULATION
Nickel
<16.7
mg/Kg -
dry
16.7
1
04/20/23 03:02
BKN
6010D
Lead
27.8
mg/Kg -
dry
20.0
1
04/20/23 03:02
BKN
6010D
Arsenic
<33.3
mg/Kg -
dry
33.3
1
04/20/23 03:02
BKN
6010D
Selenium
<33.3
mg/Kg -
dry
33.3
1
04/20/23 03:02
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids 1.51 % 0.010 1 04/19/23 07:49 CJR SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 8

waypANALYTICAL
00454
Synagro Central LLC/ Neuse Reg WASA Project
Marshall Puryear
284 Boger Road Information
Suite 204
Mocksville , NC 27028
Report Number : 23-103-0009
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
NRWASA
REPORT OFANALYSIS
Report Date : 04/24/2023
Received : 04/13/2023
Brandi Watson
Lab No : 61748
Sample ID: NRWASA
Matrix: Solids
Sampled: 4/12/2023 11:00
Total Kjeldahl Nitrogen
68700
mg/Kg -
dry
16700
1
04/24/23 10:00
CLP ;M-4500-NH3C-TKl`
Potassium
1150
mg/Kg -
dry
667
1
04/20/23 03:02
BKN
6010D
Magnesium
1250
mg/Kg -
dry
333
1
04/20/23 03:02
BKN
6010D
Sodium
1770
mg/Kg -
dry
1670
1
04/20/23 03:02
BKN
6010D
Iron
40300
mg/Kg -
dry
667
1
04/20/23 03:02
BKN
6010D
Ammonia Nitrogen
7000
mg/Kg -
dry
6670
1
04/21/23 13:15
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<333
mg/Kg -
dry
333
1
04/18/23 13:31
ZBD
4500NO3F-2011
Cadmium
<6.67
mg/Kg -
dry
6.67
1
04/20/23 03:02
BKN
6010D
Chromium
18.2
mg/Kg -
dry
16.7
1
04/20/23 03:02
BKN
6010D
Mercury
<12.3
mg/Kg -
dry
12.3
1
04/18/23 12:35
FDS
SW-7471B
pH
6.9
S.U.
1
04/20/2316:20
CNB
9045D
Total Volatile Solids
40.5
%
0.010
1
04/19/23 07:49
CJR
SM-2540G
Molybdenum
<16.7
mg/Kg -
dry
16.7
1
04/20/23 03:02
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 8

Waypoint".0
ANALYTICAL
Client: Synagro Central LLC/ Neuse Reg WASA
Project: NRWASA
Lab Report Number: 23-103-0009
Date: 4/24/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 61926 (SB-1 (19'-20'))
QC Batch No: L677247/L676373
One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are
required.
Sample 61926 (SB-1 (19'-20'))
Analyte: Aluminum
QC Batch No: L677377/L676373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61926 (SB-1 (19'-20'))
Analyte: Iron
QC Batch No: L677377/L676373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61926 (SB-1 (19'-20'))
Analyte: Potassium
QC Batch No: L677377/L676373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 61926 (SB-1 (19'-20'))
Analyte: Magnesium
QC Batch No: L677377/L676373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 61926 (SB-1 (19'-20'))
Analyte: Lead
QC Batch No: L677377/L676373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 61926 (SB-1 (19'-20'))
Analyte: Sulfur
QC Batch No: L677377/L676373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 8

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Sample 61926 (SB-1 (19'-20'))
Analyte: Selenium
QC Batch No: 1-677377/1-676373
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 6 of 8

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 00454
Customer Name: Synagro Central LLC/ Neuse Reg WASA
Report Number: 23-103-0009
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low
F_ Low
concentration EnCore samplers (48 hr)
conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 04/13/2023 09:59:06
Page 7 of 8

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Page
8 of 8

Waypointo
ANALYTICAL
8/4/2023
Synagro Central LLC/ Neuse Reg WASA
Marshall Puryear
284 Boger Road
Suite 204
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-201-0005
Project Description: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Marshall Puryear:
Waypoint Analytical Virginia, Inc. received sample(s) on 7/20/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
& " 0 " -Ab " '� (--, "
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-201-0005
Client Project Description: NRWASA
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
62832
NRWASA
Solids
07/18/202310:00
07/20/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

waypANALYTICAL
00454
Synagro Central LLC/ Neuse Reg WASA Project NRWASA
Marshall Puryear
284 Boger Road Information
Suite 204
Mocksville , NC 27028
Report Number : 23-201-0005
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
REPORT OFANALYSIS
Report Date : 08/04/2023
Received : 07/20/2023
Brandi Watson
Lab No : 62832
Sample ID: NRWASA
Matrix: Solids
Sampled: 7/18/2023 10:00
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
2.83
%
0.010
1
07/25/23 18:22
KDO
SM-2540G
Total Kjeldahl Nitrogen
<8930
mg/Kg -
dry
8930
1
08/03/23 15:00
JPJ ;M-4500-NH3C-TKI`
Phosphorus
3230
mg/Kg -
dry
179
1
07/27/23 01:01
JTR
6010D
Potassium
982
mg/Kg -
dry
357
1
07/27/23 01:01
JTR
6010D
Sulfur
5070
mg/Kg -
dry
357
1
07/27/23 01:01
JTR
6010D
Calcium
3070
mg/Kg -
dry
1790
1
07/27/23 01:01
JTR
6010D
Magnesium
1230
mg/Kg -
dry
179
1
07/27/23 01:01
JTR
6010D
Sodium
<893
mg/Kg -
dry
893
1
07/27/23 01:01
JTR
6010D
Iron
30000
mg/Kg -
dry
357
1
07/27/23 01:01
JTR
6010D
Manganese
3280
mg/Kg -
dry
17.9
1
07/27/23 01:01
JTR
6010D
Copper
128
mg/Kg -
dry
17.9
1
07/27/23 01:01
JTR
6010D
Zinc
88.2
mg/Kg -
dry
44.6
1
07/27/23 01:01
JTR
6010D
Organic N
<8929
mg/Kg -
dry
8929
1
08/02/23 13:00
CALCULATION
Nitrate+Nitrite-N
<179
mg/Kg -
dry
179
1
07/24/23 14:38
CLP
4500NO3F-2016
Nickel
14.4
mg/Kg -
dry
8.93
1
07/27/23 01:01
JTR
6010D
Mercury
<6.79
mg/Kg -
dry
6.79
1
07/26/23 11:37
FDS
SW-7471B
Selenium
<17.9
mg/Kg -
dry
17.9
1
07/27/23 01:01
JTR
6010D
pH
6.8
S.U.
1
07/24/2316:00
ANV
9045D
Total Volatile Solids
37.7
%
0.010
1
07/25/23 18:22
KDO
SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 7

waypANALYTICAL
00454
Synagro Central LLC/ Neuse Reg WASA
Project NRWASA
Marshall Puryear
284 Boger Road
Information
Suite 204
Mocksville , NC 27028
Report Number : 23-201-0005
REPORT OF.
Lab No : 62832
Sample ID: NRWASA
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Date : 08/04/2023
Received : 07/20/2023
Brandi Watson
VALYSIS
Matrix: Solids
Sampled: 7/ 18/ 2023 10:00
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Ammonia Nitrogen
<3570
mg/Kg -
dry
3570
1
08/02/23 13:00
JPJ
SM-4500-NH3C
Aluminum
133000
mg/Kg -
dry
179
1
07/27/23 01:01
JTR
6010D
Arsenic
<17.9
mg/Kg -
dry
17.9
1
07/27/23 01:01
JTR
6010D
Cadmium
<3.57
mg/Kg -
dry
3.57
1
07/27/23 01:01
JTR
6010D
Chromium
18.8
mg/Kg -
dry
8.93
1
07/27/23 01:01
JTR
6010D
Lead
12.4
mg/Kg -
dry
10.7
1
07/27/23 01:01
JTR
6010D
Molybdenum
<8.93
mg/Kg -
dry
8.93
1
07/27/23 01:01
JTR
6010D
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Batch
Moisture
97.2
%
0.010
1
07/25/2318:22
KDO
L694829
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypoint".0
ANALYTICAL
Client: Synagro Central LLC/ Neuse Reg WASA
Project: NRWASA
Lab Report Number: 23-201-0005
Date: 8/3/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 62835 (Kinston WRC)
Analyte: Aluminum
QC Batch No: 1-695278/1-694621
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 62835 (Kinston WRC)
Analyte: Potassium
QC Batch No: 1-695369/1-694621
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 62835 (Kinston WRC)
Analyte: Phosphorus
QC Batch No: 1-695278/1-694621
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 00454
Customer Name: Synagro Central LLC/ Neuse Reg WASA
Report Number: 23-201-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low
F_ Low
concentration EnCore samplers (48 hr)
conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: lBrandi Watson Date & Time: 07/20/2023 11:25:45
Page 6 of 7

Page 7 of 7

SECTION 3

FACILITY NAME: NEUSE REGIONAL WASA, NC
LANDOWNER: SOVEREIGN REAL ESTATE
OPERATOR: MICHAEL GINN
CROP 1 NAME: WHEAT (WH)
RESIDUAL SOURCE(S): *See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT M WQ0034688 FIELD#: NC-1-N-000X6-0-0003-
ANNUAL DRY TONS APPLIED: 73.60 SITE M NC LN 000X6
PREDOMINANT SOIL SERIES: LUMBEE
CROP 1 MAX. PAN: 98 CROP 2 NAME:
ACRES UTILIZED: 26.3
ACRES PERMITTED: 26.3
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type I
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite (lbs/acre)
Application
Month
Solids
Dry TonslAc
Source
Moist
Inches
Method"
Rate—
Rate—
mg/kg
mg/kg
mglkg Crop 1 Crop 2
Amount
UCM
Crop 1
Crop 2 1
10/2312023
214,200.00
(G)
2,830
0,961
NRWASAWPL
SUR
0.5
0.40
8,930,00
3.570.00
179.00 10.641
WH
10/24/2023
308,700.00
(G)
2.830
1.385
NRWASAWPL
SUR
0.5
0.40
8,930.00
3.570.00
179.00 15.336
WH
10/25/2023
100,800.00
(G)
2.830
0.452
NRWASAWPL
SUR
0.5
0.40
8,930,00
3.570.00
179.00 5.008
WH
Oct-23
623,700.00
(G)
Total 2.798 Total 30.985 0,000
AS CD CU CR PB HG MO NI SE ZN P Lime Applied
Ann uallbslacreApplied 0.100 0.020 0.716 0.105 0.069 0.038 0.050 0.081 0.100 0.494 18.079 Date Lbs1Ac
Cumulative Ibslacre Applied 0.386 0.054 27.461 1.549 0.454 0.053 0.243 0.464 0.273 2,448
Permit PAN limit (Ibslacre) 1 st Crop 96
Federal C.P.L.R. (Ibslacre)**** 36.6 34.8 1,339.0 287,9 15.0 375.0 89.0 2,500.0
NRWASAWPL = NEUSE REGIONAL WASA, NC WTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are si an altieyfibmitting false information, including the possibility of fines and imprisonment for knnowing violations"
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, AnaerobicaIly digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation *"" C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ** ** See Site pH & Lime Application Records Section of Report
Printed: 1/3112024 DENR FORM FSF (12/2006)

FACILITY NAME: NEUSE REGIONAL WASA, NO
LANDOWNER: SOVEREIGN REAL ESTATE
OPERATOR: MICHAEL GINN
CROP 1 NAME: WHEAT (WH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0034685 FIELD* NC-LN-00OX6-0-0004-
ANNUAL DRY TONS APPLIED: 240.88 SITE #: NO LN DOOX6
PREDOMINANT 501L SERIES: JOHNS
CROP 1 MAX. PAN: 106 CROP 2 NAME:
ACRES UTILIZED: 58.7
ACRES PERMITTED: 58.7
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page:i
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cord.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
0/0
Residual
Dry, Wet,
Past 24 W&
Application
' €izatiorc
ization
TKN
Nitrogen
and Nitrite
(€bslacre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method"
Rate*"
Rate**'
mg/kg
mglkg
mglkg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
10/23/2023
415,800.00
(G)
2.830
0.836
NRWASAWPL
SUR
0.5
0,40
8,930.00
3,570.00
179.00
9.255
WH
10/24/2023
636,300.00
(G)
2.830
1.279
NRWASAWPL
SUR
D.5
0A0
8,930.00
3,570,00
179.00
14.163
VVH
10/25/2023
856,800.00
(G)
2.830
1.723
NRWASAWPL
SUR
0.5
0.40
8,930.00
3,570.00
179.00
19.070
WH
10/26/2023
132,300.00
(G)
2.830
0.266
NRWASAWPL
SUR
0.5
0.40
8,930.00
3,570.00
179.00
2,945
WH
Oct-23
2,041,200.00
(G)
Total 4.104
AS CD Cu OR PB
lbs/acre Applied 0.147 0.029 1.051 0.154 0.102
five €bslacre Applied 0.551 0.089 32.261 7 2.495 0,551
Total 45.433 0.000
HG MO Ni SE ZN P
0,056 j 0.073 CA18 0.147 f 0724 26.510 [
0.626 1 0,423 1 3.524
Lbs1Ac
Permit PAN Limit{€bslacre) 1st Crop log
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
NRWASAWPL = NEUSE REGIONAL WASA NO WTP LIQUO
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are signific n t' or sub itting false information, including the possibility of fines and imprisonment for knowing violations."
tv.Z! Ay
SIG74ATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required "* Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 *"** See Site pH & Lime Application Records Section of Report
Printed: 113112024 DENR FORM FSF (12/2006)

SECTION 4

SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
January 04, 2024
Matthew Carter
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Nevse Regional WASA
Dear Matthew Carter:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Order No.: 23121878
Summit Environmental Technologies, Inc. received 1 sample(s) on 12/27/2023 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho 01100923, Illinois 200061, Indiana C-011-13,
ISO/EEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988,
Minnesota 1780279, Nevada 011009232020-1, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota
R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon 0112O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina
92016001, Texas T104704466-19-16, Utah 011009232020-12, Virginia VELAP 10381, West Virginia 9957C
Page 1 of 36

SUMMIY Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIFIONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com Date: 1/4/2024
CLIENT: Synagro
Project: Nevse Regional WASA
WorkOrder Narrative:
23121878: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
23121878-00IA TCLP-SVOC-CPEST(808113): Possible high bias for multiple analytes due to high
recovery in bracketed CCV and LCS. Sample is ND for all analytes.
23121878-OOIA Cyanide,Reactive_S(9014): Corresponding MS/MSD exhibited a high RPD, possibly
due to sample matrix. Individually each MS/MSD meet the required criteria.
23121878-OOIA TCLP-SVOC_8270E: CCV demonstrated high recovery for Hexachlorobutadiene.
Sample was ND for this analyte. Possible low bias for Pentachlorophenol due to low recovery in CCV.
Less than 10% of all analytes are outside of acceptable criteria. RLC demonstrates adequate instrument
sensitivity for EPA 8270 requirement.
Original
Page 2 of 36

SUMMIT
Summit Environmental Technologies, In Qualifiers and Acronyms
3310 Win S
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 442� WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- (330) 253-44E
Website: http://www.settek.co; Date: 1/4/2024
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confumation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low () or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 3 of 36

SUMMIEr Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Workorder
Sample Summary
WO#: 23121878
04 Jan-24
CLIENT: Synagro
Project: Nevse Regional WASA
Lab SamplelD Client Sample ID Tag No Date Collected Date Received Matrix
23121878-001 NRWASA 12/26/2023 11:30:00 AM 12/27/2023 9:40:00 AM Sludge
Page 4 of 36

SSummit
Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMENTAL TECHNOLOGIES, INC.
Cuyahoga Falls, Ohio44223
WO#: 23121878
-FEUMMIT
Analytical Laboratories
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
04 Jan-24
Client:
Synagro
Project:
Nevse Regional WASA
Sample ID
Client Sample ID Collection Date Matrix Test Name
Leachate Date Prep Date Analysis Date
23121878-OOIA NRWASA 12/26/2023 11:30:00 AM Sludge Ignitability of Solids (SW-846: 1030)
12/28/2023 10:07:40 AM
Percent Solids by SM2540Mod
12/27/2023 4:50:00 PM
pH (SW9045D)
12/29/2023 2:11:00 PM
Reactive Cyanide (9014/7.3.3.2)-Solid 1/2/2024 11:35:02 AM
Reactive Sulfide (9034)/7.3.4.2
1/2/2024 2:11:53 PM
TCLP Herbicides
12/29/2023 9:18:53 PM
TCLP Mercury
12/28/2023 1:30:00 PM 12/29/2023 7:40:00 AM 12/29/2023 11:27:00 AM
TCLP Metals
12/28/2023 1:30:00 PM 12/29/2023 9:58:21 AM 12/29/2023 2:17:00 PM
TCLP Pesticides
12/28/2023 1:30:00 PM 1/2/2024 9:00:00 AM 1/2/2024 5:52:00 PM
TCLP Semi-Volatiles Analysis
12/28/2023 1:30:00 PM 1/2/2024 11:20:00 AM 1/3/2024 1:41:00 PM
(SW1311/8270)
TCLP Volatiles
12/28/2023 1:30:00 PM 12/29/2023 2:59:00 PM
Original
Page 5 of 36

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Analytical Report
(base report)
WO#: 23121878
Date Reported: 1/4/2024
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/26/2023 11:30:00 AM
Lab ID: 23121878-OOIA
Project: Nevse Regional WASA
Client Sample ID NRWASA
Analyses Result RL Qual Units DF Date Analyzed
FULL TCLP
TCLP MERCURY
TCLP Mercury
FULL TCLP
TCLP METALS
TCLP Arsenic(As)
TCLP Barium(Ba)
TCLP Cadmium(Cd)
TCLP Chromium(Cr)
TCLP Lead(Pb)
TCLP Selenium(Se)
TCLP Silver(Ag)
SW7470A SW7470A Analyst: JJF
ND 0.00200 mg/L 1 12/29/2023 11:27:00 AM
SW6010 SW301OA Analyst: RJE
ND
0.500
mg/L
1
12/29/2023 2:17:00 PM
1.45
1.00
mg/L
1
12/29/2023 2:17:00 PM
ND
0.100
mg/L
1
12/29/2023 2:17:00 PM
ND
0.200
mg/L
1
12/29/2023 2:17:00 PM
ND
0.500
mg/L
1
12/29/2023 2:17:00 PM
ND
0.0500
mg/L
1
12/29/2023 2:17:00 PM
ND
0.500
mg/L
1
12/29/2023 2:17:00 PM
TCLP SEMI-VOLATILES
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
2,4,5-Trichlorophenol
ND
2,4,6-Trichlorophenol
ND
2,4-Dinitrotoluene
ND
Cresols, Total
ND
Hexachloro-1,3-butadiene
ND
Hexachlorobenzene
ND
Hexachloroethane
ND
Nitrobenzene
ND
Pentachlorophenol
ND
Pyridine
ND
Surr: 2-Fluorophenol
80.2
Surr: Phenol-d6
80.8
Surr: Nitrobenzene-d5
73.9
Surr: 2,4,6-Tribromophenol
94.8
Surr: 2-Fluorobiphenyl
78.6
Surr: p-Terphenyl-d14
94.2
SW8270 SW351OC Analyst: SAM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
0.0500
mg/L
1
1/3/2024 1:41:00 PM
0.0250
QC+ mg/L
1
1/3/2024 1:41:00 PM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
0.0250
QC- mg/L
1
1/3/2024 1:41:00 PM
0.0250
mg/L
1
1/3/2024 1:41:00 PM
10 - 130
%Rec
1
1/3/2024 1:41:00 PM
10 - 130
%Rec
1
1/3/2024 1:41:00 PM
10 - 130
%Rec
1
1/3/2024 1:41:00 PM
19 - 151
%Rec
1
1/3/2024 1:41:00 PM
10 - 130
%Rec
1
1/3/2024 1:41:00 PM
20 - 181
%Rec
1
1/3/2024 1:41:00 PM
E Value above quantitation range H Holding times for preparation or analysis exceeded
Qualifiers: M Manual Integration used to determine area response ND Not Detected
PL Pemrit Lint R RPD outside accepted recovery lints
RL Reporting Detection Lint W Sample container temperature is out of lint as specified at testcode
Page 6 of 36 Original

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Analytical Report
(base report)
WO#: 23121878
Date Reported: 1/4/2024
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/26/2023 11:30:00 AM
Lab ID: 23121878-OOIA
Project: Nevse Regional WASA
Client Sample ID NRWASA
Analyses
Result
RL
Qual
Units
DF
Date Analyzed
FULL TCLP
SW8081
SW3510C Analyst: JDB
TCLP PESTICIDES
Chlordane, total
ND
0.0250
mg/L
10
1/2/2024 5:52:00 PM
Toxaphene
ND
0.0500
mg/L
10
1/2/2024 5:52:00 PM
Endrin
ND
0.00500
QC+
mg/L
10
1/2/2024 5:52:00 PM
gamma-BHC
ND
0.00500
QC+
mg/L
10
1/2/2024 5:52:00 PM
Heptachlor
ND
0.00500QC+QL+mg/L
10
1/2/2024 5:52:00 PM
Heptachlor epoxide
ND
0.00500
mg/L
10
1/2/2024 5:52:00 PM
Methoxychlor
ND
0.00500
QC+
mg/L
10
1/2/2024 5:52:00 PM
Surr: TCMX
105
10 - 119
%Rec
10
1/2/2024 5:52:00 PM
Surr: DCB
102
10 - 119
%Rec
10
1/2/2024 5:52:00 PM
FULL TCLP
SW8321
Analyst: MTG
TCLP HERBICIDES
2,4-D
ND
0.500
mg/L
50
12/29/2023 9:18:53 PM
2,4,5-TP
ND
0.500
mg/L
50
12/29/2023 9:18:53 PM
Surr: DCAA
79.0
70 - 130
%Rec
50
12/29/2023 9:18:53 PM
FULL TCLP
SW8260
SW1311
M Analyst: JSH
TCLP VOLATILES
1,1-Dichloroethene
ND
0.100
mg/L
20
12/29/2023 2:59:00 PM
1,2-Dichloroethane
ND
0.100
mg/L
20
12/29/2023 2:59:00 PM
MEK
ND
2.00
mg/L
20
12/29/2023 2:59:00 PM
Benzene
ND
0.100
mg/L
20
12/29/2023 2:59:00 PM
Carbon tetrachloride
ND
0.100
mg/L
20
12/29/2023 2:59:00 PM
Chlorobenzene
ND
1.00
mg/L
20
12/29/2023 2:59:00 PM
Chloroform
ND
0.100
mg/L
20
12/29/2023 2:59:00 PM
Tetrachloroethene
ND
0.100
mg/L
20
12/29/2023 2:59:00 PM
Trichloroethene
ND
0.100
mg/L
20
12/29/2023 2:59:00 PM
Vinyl chloride
ND
0.0400
mg/L
20
12/29/2023 2:59:00 PM
Surr: 4-Bromofluorobenzene
108
70 - 130
%Rec
20
12/29/2023 2:59:00 PM
Surr: Dibromofluorom ethane
107
70 - 130
%Rec
20
12/29/2023 2:59:00 PM
Surr: Toluene-d8
97.8
70 - 130
%Rec
20
12/29/2023 2:59:00 PM
E Value above quantitation range
Qualifiers:
H Holding times for preparation
or analysis exceeded
M Manual Integration used to determine area response
ND Not Detected
PL Pemrit Lint
R RPD outside accepted
recovery lints
RL Reporting Detection Lint
W Sample container temperature
is out of
lint as specified at testcode
Page 7 of 36 Original

SUMMIT
Summit Environmental Technologies, Inc. Analytical Report
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 (base report)
Analytical Laboratories TEL: [phone] FAX.- [phone] WO#: 23121878
Website: http://www.settek.com Date Reported: 1/4/2024
CLIENT: Synagro Tag Number:
Matrix: SLUDGE Collection Date: 12/26/2023 11:30:00 AM
Lab ID: 23121878-OOIA
Project: Nevse Regional WASA
Client Sample ID NRWASA
Analyses
Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: KDH
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive
ND
0.427 QMR mg/Kg
1
1/2/2024 11:35:02 AM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: KDH
Ignitability Non -Flammable
mm/sec
1
12/28/2023 10:07:40 AM
PERCENT SOLIDS BY SM2540MOD
A2540B
Analyst: JPN
Percent Solids
19.7
%
1
12/27/2023 4:50:00 PM
RCI
SW9045D
Analyst: JPN
PH (SW9045D)
pH
7.0
s.u.@19.7C
1
12/29/2023 2:11:00 PM
RCI
SW9034
Analyst: KDH
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive
ND
25.0 mg/Kg
1
1/2/2024 2:11:53 PM
E
Qualifiers: M
Value above quantitation range
Manual Integration used to determine area response
H
ND
Holding times for preparation or analysis exceeded
Not Detected
PL
Pemrit Lint
R
RPD outside accepted recovery lints
RL
Reporting Detection Lint
W
Sample container temperature is out of lint as specified at testcode
Page 8 of 36
Original

SUMMIT summit Environmental Technologies, Inc. Accreditation Program
3310 Win St. Anal tes Report
rt
ENVIRONMENTAL TECHNOLOGIES; INC Cuyahoga Falls, Ohio 44223 y Y
Analytical Laboratories TEL: [phone] FAX.- [phone] WO#: 23121878
Website: http://www.settekcom 04 Jan-24
Client: Synagro
Project: Nevse Regional WASA
State: NW
Program Name: NC WW SCM
Sample ID
Matrix
Test Name
Analyte
Status
23121878-OOIA
Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
Percent Solids by SM2540Mod
Percent Solids
N
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Sludge
TCLP Herbicides
2,4,5-TP
A
Sludge
TCLP Herbicides
2,4-D
A
Sludge
TCLP Mercury
Mercury
A
Sludge
TCLP Metals
Arsenic
A
Sludge
TCLP Metals
Barium
A
Sludge
TCLP Metals
Cadmium
A
Sludge
TCLP Metals
Chromium
A
Sludge
TCLP Metals
Lead
A
Sludge
TCLP Metals
Selenium
A
Sludge
TCLP Metals
Silver
A
Sludge
TCLP Pesticides
Chlordane, total
A
Sludge
TCLP Pesticides
Endrin
A
Sludge
TCLP Pesticides
gamma-BHC
A
Sludge
TCLP Pesticides
Heptachlor
A
Sludge
TCLP Pesticides
Heptachlor epoxide
A
Sludge
TCLP Pesticides
Methoxychlor
A
Sludge
TCLP Pesticides
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
AL
A
Accredited
AL
N Not Accredited
AR
A
Accredited
AR
N
Not Accredited
;A-NELAI
N Not Accredited
CO
U
Unavailable
CT
A
Accredited
CT
N Not Accredited
T,-NELAI
A
Accredited Original#1
,L-NELAI
N
Not Accredited
HI-DW
N pTsl.Aicd�igd cdf
ID
U
Unavailable
L-NELAI
A
Accredited
L-NELAI
N Not Accredited
INDW
U
Unavailable

summit Environmental Technologies, Inc.
Accreditation
Program
3310 Win St.
SUMMIT
ENVIRONMENTAL TECHNOLOGIES; INC Cuyahoga Falls, Ohio 44223
rt
Anal tes Report
y Y
Analytical Laboratories
TEL: [phone] FAX.- [phone]
WO#:
23121878
Website: http://www.settekcom
04 Jan-24
Client: Synagro
State: NW
Project: Nevse Regional WASA
Program Name: NC WW SCM
Sample ID Matrix
Test Name
Analyte
Status
23121878-OOIA Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Sludge
TCLP Volatiles
1,1-Dichloroethene
A
Sludge
TCLP Volatiles
1,2-Dichloroethane
A
Sludge
TCLP Volatiles
2-Butanone
A
Sludge
TCLP Volatiles
Benzene
A
Sludge
TCLP Volatiles
Carbon tetrachloride
A
Sludge
TCLP Volatiles
Chlorobenzene
A
Sludge
TCLP Volatiles
Chloroform
A
Sludge
TCLP Volatiles
Tetrachloroethene
A
Sludge
TCLP Volatiles
Trichloroethene
A
Sludge
TCLP Volatiles
Vinyl chloride
A
AL
A
Accredited
AL
N Not Accredited
AR
A
Accredited
AR
N
Not Accredited
;A-NELAI
N Not Accredited
CO
U
Unavailable
CT
A
Accredited
CT
N Not Accredited
T,-NELAI
A
Accredited Original#1
�L-NELAI
N
Not Accredited
HI-DW
N P *Tsf iYd
ID
U
Unavailable
L-NELAI
A
Accredited
L-NELAI
N Not Accredited
INDW
U
Unavailable

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71661
Sample ID: LCS-71661
SampType: LCS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 177316
Client ID: LCSS
Batch ID: 71661
TestNo: SW8260 SW1311M
Analysis Date: 12/29/2023
SegNo: 4803843
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1, 1 -Dichloroethene
0.0515
0.00500
0.0500
0
103
64.7
136
1,2-Dichloroethane
0.0549
0.00500
0.0500
0
110
70
130
MEK
0.328
0.0250
0.250
0
131
55.1
149
Benzene
0.0506
0.00500
0.0500
0
101
70
130
Carbon tetrachloride
0.0585
0.00500
0.0500
0
117
70
130
Chlorobenzene
0.0471
0.00500
0.0500
0
94.2
70
130
Chloroform
0.0519
0.00500
0.0500
0
104
70
130
Tetrachloroethene
0.0453
0.00500
0.0500
0
90.6
70
134
Trichloroethene
0.0486
0.00500
0.0500
0
97.3
62.8
160
Vinyl chloride
0.0418
0.00200
0.0500
0
83.6
67.1
130
Surr:4-Bromofluorobenzene
54.1
50.00
108
70
130
Surr: Dibromofluoromethane
54.1
50.00
108
70
130
Surr: Toluene-d8
47.1
50.00
94.3
70
130
Sample ID: 23121852-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 177316
Client ID: BatchQC
Batch ID: 71661
TestNo: SW8260 SW1311M
Analysis Date: 12/29/2023
SegNo: 4803848
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1, 1 -Dichloroethene
1.12
0.250
1.00
0
112
13.6
202
1,2-Dichloroethane
1.12
0.250
1.00
0
112
55.7
138
MEK
5.36
1.25
5.00
0
107
65.3
130
Benzene
1.43
0.250
1.00
0.411
102
49.2
145
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 11 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71661
Sample ID: 23121852-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 177316
Client ID: BatchQC
Batch ID: 71661
TestNo: SW8260 SW1311M
Analysis Date: 12/29/2023
SegNo: 4803848
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
1.08
0.250
1.00
0
108
26.7
156
Chlorobenzene
0.983
0.250
1.00
0
98.3
33.7
159
Chloroform
1.07
0.250
1.00
0
107
48.5
145
Tetrachloroethene
0.933
0.250
1.00
0
93.3
19.2
191
Trichloroethene
1.04
0.250
1.00
0
104
38.4
167
Vinyl chloride
0.702
0.100
1.00
0
70.2
27.3
161
Surr:4-Bromofluorobenzene
2800
2500
112
70
130
Surr: Dibromofluoromethane
2650
2500
106
70
130
Surr: Toluene-d8
2380
2500
95.4
70
130
Sample ID: 23121852-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 177316
Client ID: BatchQC
Batch ID: 71661
TestNo: SW8260 SW1311M
Analysis Date: 12/29/2023
SegNo: 4803849
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1, 1 -Dichloroethene
1.11
0.250
1.00
0
ill
13.6
202
1.12
1.39
25
1,2-Dichloroethane
1.13
0.250
1.00
0
113
55.7
138
1.12
1.42
25
MEK
5.53
1.25
5.00
0
ill
65.3
130
5.36
3.09
25
Benzene
1.43
0.250
1.00
0.411
102
49.2
145
1.43
0.315
25
Carbon tetrachloride
1.06
0.250
1.00
0
106
26.7
156
1.08
2.19
25
Chlorobenzene
0.975
0.250
1.00
0
97.5
33.7
159
0.983
0.817
25
Chloroform
1.09
0.250
1.00
0
109
48.5
145
1.07
1.34
25
Tetrachloroethene
0.948
0.250
1.00
0
94.8
19.2
191
0.933
1.60
25
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 12 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71661
Sample ID: 23121852-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 177316
Client ID: BatchQC
Batch ID: 71661
TestNo: SW8260 SW1311M
Analysis Date: 12/29/2023
SegNo: 4803849
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Trichloroethene
1.04 0.250
1.00
0 104
38.4
167 1.04
0
25
Vinyl chloride
0.742 0.100
1.00
0 74.2
27.3
161 0.702
5.54
25
Surr:4-Bromofluorobenzene
2750
2500
110
70
130
0
25
Surr: Dibromofluoromethane
2650
2500
106
70
130
0
25
Surr: Toluene-d8
2360
2500
94.6
70
130
0
25
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 13 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71680
Sample ID: MB-71680
SampType: MBLK
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 12/29/2023
RunNo: 177252
Client ID: PBS
Batch ID: 71680
TestNo: SW7470A SW7470A
Analysis Date: 12/29/2023
SegNo: 4802409
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury ND 0.00200
Sample ID: LCS-71680
SampType: LCS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 12/29/2023
RunNo: 177252
Client ID: LCSS
Batch ID: 71680
TestNo: SW7470A SW7470A
Analysis Date: 12/29/2023
SegNo: 4802410
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00398 0.00200 0.00400 0 99.5 80 120
Sample ID: 23121931-001AMS
SampType: MS
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 12/29/2023
RunNo: 177252
Client ID: BatchQC
Batch ID: 71680
TestNo: SW7470A SW7470A
Analysis Date: 12/29/2023
SegNo: 4802413
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00440 0.00200 0.00400 0 110 75 125
Sample ID: 23121931-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 12/29/2023
RunNo: 177252
Client ID: BatchQC
Batch ID: 71680
TestNo: SW7470A SW7470A
Analysis Date: 12/29/2023
SegNo: 4802414
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00393 0.00200 0.00400 0 98.2 75 125 0.00440 11.3 20
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 14 of 36

summint Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Nevse Regional WASA BatchID: 71680
Won: 23121878
04-Jan-24
Sample ID: 23121931-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 12/29/2023
RunNo: 177252
client ID: BatchQC
Batch ID: 71680
TestNo: SW7470A SW7470A
Analysis Date: 12/29/2023
SegNo: 4802414
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 15 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71685
Sample ID: MB-71685
SampType: MBLK
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 12/29/2023
RunNo: 177248
Client ID: PBS
Batch ID: 71685
TestNo: SW6010 SW3010A
Analysis Date: 12/29/2023
SegNo: 4803387
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
1.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-71685
SampType: LCS
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 12/29/2023
RunNo: 177248
Client ID: LCSS
Batch ID: 71685
TestNo: SW6010 SW3010A
Analysis Date: 12/29/2023
SegNo: 4803391
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.25
0.500
2.000
0
113
80
120
TCLP Barium(Ba)
2.23
1.00
2.000
0
ill
80
120
TCLP Cadmium(Cd)
2.04
0.100
2.000
0
102
80
120
TCLP Chromium(Cr)
2.17
0.200
2.000
0
109
80
120
TCLP Lead(Pb)
2.15
0.500
2.000
0
107
80
120
TCLP Selenium(Se)
2.11
0.0500
2.000
0
105
80
120
TCLP Silver(Ag)
2.15
0.500
2.000
0
107
80
120
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 16 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71685
Sample ID: 23121931-001AMS
SampType: MS
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 12/29/2023
RunNo: 177248
Client ID: BatchQC
Batch ID: 71685
TestNo: SW6010 SW3010A
Analysis Date: 12/29/2023
SegNo: 4803394
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
10.7
2.50
10.00
0
107
70
130
TCLP Barium(Ba)
10.6
5.00
10.00
0.3905
102
70
130
TCLP Cadmium(Cd)
9.17
0.500
10.00
0
91.7
70
130
TCLP Chromium(Cr)
9.83
1.00
10.00
0
98.3
70
130
TCLP Lead(Pb)
9.60
2.50
10.00
0
96.0
70
130
TCLP Selenium(Se)
10.2
0.250
10.00
0
102
70
130
TCLP Silver(Ag)
10.2
2.50
10.00
0
102
70
130
Sample ID: 23121931-001AMSD
SampType: MSD
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 12/29/2023
RunNo: 177248
Client ID: BatchQC
Batch ID: 71685
TestNo: SW6010 SW3010A
Analysis Date: 12/29/2023
SegNo: 4803395
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
10.9
2.50
10.00
0
109
70
130
10.74
1.86
20
TCLP Barium(Ba)
10.7
5.00
10.00
0.3905
103
70
130
10.60
0.957
20
TCLP Cadmium(Cd)
9.24
0.500
10.00
0
92.4
70
130
9.168
0.761
20
TCLP Chromium(Cr)
9.91
1.00
10.00
0
99.1
70
130
9.832
0.831
20
TCLP Lead(Pb)
9.67
2.50
10.00
0
96.7
70
130
9.603
0.737
20
TCLP Selenium(Se)
10.5
0.250
10.00
0
105
70
130
10.24
2.14
20
TCLP Silver(Ag)
10.3
2.50
10.00
0
103
70
130
10.16
1.10
20
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 17 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71723
Sample ID: MB-71723
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/2/2024
RunNo: 177385
Client ID: PBS
Batch ID: 71723
TestNo: SW8081 SW3510C
Analysis Date: 1/2/2024
SegNo: 4805910
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Surr: TCMX
75.0
100.0 75.0 10 119
Surr: DCB
83.4
100.0 83.4 10 119
Sample ID: LCS-71723
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/2/2024
RunNo: 177385
Client ID: LCSS
Batch ID: 71723
TestNo: SW8081 SW3510C
Analysis Date: 1/2/2024
SegNo: 4805913
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
0.169
0.00250
0
0
70
130
Toxaphene
ND
0.00500
0
0
70
130
Endrin
0.100
0.000500
0.100
0
100
10
130
gamma-BHC
0.0921
0.000500
0.100
0
92.1
10
130
Heptachlor
0.124
0.000500
0.100
0
124
10
130
Heptachlor epoxide
0.0872
0.000500
0.100
0
87.2
10
130
Methoxychlor
0.129
0.000500
0.100
0
129
10
178
Surr: TCMX
81.7
100.0
81.7
10
130
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 18 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71723
Sample ID: LCS-71723
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/2/2024
RunNo: 177385
Client ID: LCSS
Batch ID: 71723
TestNo: SW8081 SW3510C
Analysis Date: 1/2/2024
SegNo: 4805913
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Surr: DCB 87.0 100.0 87.0 10 130
Sample ID: 23121878-001AMS
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/2/2024
RunNo: 177385
Client ID: NRWASA
Batch ID: 71723
TestNo: SW8081 SW3510C
Analysis Date: 1/2/2024
SegNo: 4805918
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
0.197
0.0250
0
0
70
130
Toxaphene
ND
0.0500
0
0
70
130
Endrin
0.113
0.00500
0.100
0
113
10
224
QC+
gamma-BHC
0.109
0.00500
0.100
0
109
10
192
QC+
Heptachlor
0.138
0.00500
0.100
0
138
10
197
QC+
Heptachlor epoxide
0.100
0.00500
0.100
0
100
10
208
Methoxychlor
0.152
0.00500
0.100
0
152
10
251
QC+
Surr: TCMX
97.6
100.0
97.6
10
157
Surr: DCB
109
100.0
109
10
194
Sample ID: 23121878-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/2/2024
RunNo: 177385
Client ID: NRWASA
Batch ID: 71723
TestNo: SW8081 SW3510C
Analysis Date: 1/2/2024
SegNo: 4805919
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 19 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71723
Sample ID: 23121878-001AMSD
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/2/2024
RunNo: 177385
Client ID: NRWASA
Batch ID: 71723
TestNo: SW8081 SW3510C
Analysis Date: 1/2/2024
SegNo: 4805919
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
0.194
0.0250
0
0
70
130
0.197
1.80
30
Toxaphene
ND
0.0500
0
0
70
130
0
0
30
Endrin
0.109
0.00500
0.100
0
109
10
224
0.113
3.88
30
QC+
gamma-BHC
0.107
0.00500
0.100
0
107
10
192
0.109
1.64
30
QC+
Heptachlor
0.139
0.00500
0.100
0
139
10
197
0.138
0.430
30
QC+
Heptachlor epoxide
0.0996
0.00500
0.100
0
99.6
10
208
0.100
0.819
30
Methoxychlor
0.145
0.00500
0.100
0
145
10
251
0.152
4.25
30
QC+
Surr: TCMX
98.8
100.0
98.8
10
157
0
Surr: DCB
86.7
100.0
86.7
10
194
0
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 20 of 36

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
WO#: 23121878
04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71737
Sample ID: MB-71737
SampType: MBLK
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/2/2024
RunNo: 177492
Client ID: PBS
Batch ID: 71737
TestNo: SW8270 SW3510C
Analysis Date: 1/3/2024
SegNo: 4808666
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0250
2,4,5-Trichlorophenol
ND
0.0250
2,4,6-Trichlorophenol
ND
0.0250
2,4-Dinitrotoluene
ND
0.0250
Cresols, Total
ND
0.0500
Hexachloro-1,3-butadiene
ND
0.0250
QC+
Hexachlorobenzene
ND
0.0250
Hexachloroethane
ND
0.0250
Nitrobenzene
ND
0.0250
Pentachlorophenol
ND
0.0250
QC -
Pyridine
ND
0.0250
Surr: 2-Fluorophenol
3.78
5.000
75.6
10
130
Surr: Phenol-d6
3.79
5.000
75.8
10
130
Surr: Nitrobenzene-d5
3.68
5.000
73.5
10
130
Surr: 2,4,6-Tribromophenol
4.59
5.000
91.8
19
151
Surr: 2-Fluorobiphenyl
3.89
5.000
77.8
10
130
Surr: p-Terphenyl-d14
4.60
5.000
92.0
20
181
Sample ID: LCS-71737
SampType: LCS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/2/2024
RunNo: 177492
Client ID: LCSS
Batch ID: 71737
TestNo: SW8270 SW3510C
Analysis Date: 1/3/2024
SegNo: 4808667
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: E Value above gtmntitation range H Holding times for preparation or analysis exceeded M Manual Integration iused to deternrine area respons,
ND Not Detected PL Pernt Lint R RPD outside accepted recovery linuts
RL Reporting Detection Lint S Spike Recovery outside accepted recovery lints w Sample container temperature is out of tinut as spec Original
Page 21 of 36

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
WO#: 23121878
04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71737
Sample ID: LCS-71737
SampType: LCS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/2/2024
RunNo: 177492
Client ID: LCSS
Batch ID: 71737
TestNo: SW8270 SW3510C
Analysis Date: 1/3/2024
SegNo: 4808667
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2.57
0.0250
4.000
0
64.2
36.4
130
2,4,5-Trichlorophenol
3.46
0.0250
4.000
0
86.6
31.7
132
2,4,6-Trichlorophenol
3.49
0.0250
4.000
0
87.2
31.1
133
2,4-Dinitrotoluene
4.21
0.0250
4.000
0
105
43.3
130
Cresols, Total
6.22
0.0500
8.000
0
77.8
31.7
130
Hexachloro-1,3-butadiene
3.35
0.0250
4.000
0
83.8
31.4
130
Hexachlorobenzene
3.35
0.0250
4.000
0
83.6
43.1
130
Hexachloroethane
2.34
0.0250
4.000
0
58.6
36.5
130
Nitrobenzene
4.76
0.0250
4.000
0
119
39.5
130
Pentachlorophenol
2.21
0.0250
4.000
0
55.3
34
130
Pyridine
1.79
0.0250
4.000
0
44.6
10
130
Surr: 2-Fluorophenol
4.07
5.000
81.3
10
130
Surr: Phenol-d6
4.37
5.000
87.3
10
130
Surr: Nitrobenzene-d5
4.12
5.000
82.3
10
130
Surr: 2,4,6-Tribromophenol
4.85
5.000
96.9
19
151
Surr: 2-Fluorobiphenyl
4.47
5.000
89.4
10
130
Surr: p-Terphenyl-d14
4.74
5.000
94.7
20
181
QC+
QC -
Sample ID: 23122072-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/2/2024
RunNo: 177492
Client ID: BatchQC
Batch ID: 71737
TestNo: SW8270 SW3510C
Analysis Date: 1/3/2024
SegNo: 4808675
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: E Value above gtmntitation range H Holding times for preparation or analysis exceeded M Manual Integration iused to deternrine area respons,
ND Not Detected PL Pernt Lint R RPD outside accepted recovery linuts
RL Reporting Detection Lint S Spike Recovery outside accepted recovery lints w Sample container temperature is out of tinut as spec Original
Page 22 of 36

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
WO#: 23121878
04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: 71737
Sample ID: 23122072-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/2/2024
RunNo: 177492
Client ID: BatchQC
Batch ID: 71737
TestNo: SW8270 SW3510C
Analysis Date: 1/3/2024
SegNo: 4808675
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2.84
0.0250
4.000
0
70.9
15.2
124
H
2,4,5-Trichlorophenol
3.27
0.0250
4.000
0
81.8
30.6
152
H
2,4,6-Trichlorophenol
3.42
0.0250
4.000
0
85.6
27.6
150
H
2,4-Dinitrotoluene
4.41
0.0250
4.000
0
110
58
141
H
Cresols, Total
6.21
0.0500
8.000
0
77.7
27.6
132
H
Hexachloro-1,3-butadiene
3.71
0.0250
4.000
0
92.6
10
156
HQC+
Hexachlorobenzene
3.45
0.0250
4.000
0
86.2
54.3
142
H
Hexachloroethane
2.60
0.0250
4.000
0
64.9
1.92
131
H
Nitrobenzene
3.61
0.0250
4.000
0
90.3
21
135
m H
Pentachlorophenol
2.70
0.0250
4.000
0
67.5
47.4
134
HQC-
Pyridine
2.05
0.0250
4.000
0
51.2
10
130
H
Surr: 2-Fluorophenol
4.15
5.000
82.9
10
130
H
Surr: Phenol-d6
4.38
5.000
87.6
10
130
H
Surr: Nitrobenzene-d5
4.60
5.000
91.9
10
130
H
Surr: 2,4,6-Tribromophenol
4.62
5.000
92.5
19
151
H
Surr: 2-Fluorobiphenyl
4.84
5.000
96.7
10
130
H
Surr: p-Terphenyl-d14
4.58
5.000
91.6
20
181
H
Sample ID: 23122072-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/2/2024
RunNo: 177492
Client ID: BatchQC
Batch ID: 71737
TestNo: SW8270 SW3510C
Analysis Date: 1/3/2024
SegNo: 4808676
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: E Value above gtmntitation range H Holding times for preparation or analysis exceeded M Manual Integration iused to deternrine area respons,
ND Not Detected PL Pernt Lint R RPD outside accepted recovery linuts
RL Reporting Detection Lint S Spike Recovery outside accepted recovery lints w Sample container temperature is out of tinut as spec Original
Page 23 of 36

summint Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Nevse Regional WASA BatchID: 71737
WO#: 23121878
04-Jan-24
Sample ID: 23122072-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/2/2024
RunNo: 177492
lient ID: BatchQC
Batch ID: 71737
TestNo: SW8270 SW3510C
Analysis Date: 1/3/2024
SegNo: 4808676
knalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
2.82
0.0250
4.000
0
70.4
15.2
124
2.835
0.672
30
H
2,4,5-Trichlorophenol
3.56
0.0250
4.000
0
89.0
30.6
152
3.272
8.49
30
H
2,4,6-Trichlorophenol
3.50
0.0250
4.000
0
87.4
27.6
150
3.422
2.11
30
H
2,4-Dinitrotoluene
4.40
0.0250
4.000
0
110
58
141
4.409
0.0908
30
H
Cresols, Total
6.52
0.0500
8.000
0
81.5
27.6
132
6.213
4.85
30
H
Hexachloro-1,3-butadiene
3.86
0.0250
4.000
0
96.6
10
156
3.706
4.12
30
HQC+
Hexachlorobenzene
3.45
0.0250
4.000
0
86.4
54.3
142
3.448
0.174
30
H
Hexachloroethane
2.64
0.0250
4.000
0
66.1
1.92
131
2.597
1.79
30
H
Nitrobenzene
3.74
0.0250
4.000
0
93.5
21
135
3.612
3.48
30
mH
Pentachlorophenol
2.58
0.0250
4.000
0
64.4
47.4
134
2.700
4.74
30
HQC-
Pyridine
1.83
0.0250
4.000
0
45.8
10
130
2.047
11.1
30
H
Surr: 2-Fluorophenol
4.17
5.000
83.4
10
130
0
H
Surr: Phenol-d6
4.53
5.000
90.5
10
130
0
H
Surr: Nitrobenzene-d5
4.60
5.000
91.9
10
130
0
H
Surr: 2,4,6-Tribromophenol
4.78
5.000
95.5
19
151
0
H
Surr: 2-Fluorobiphenyl
4.74
5.000
94.9
10
130
0
H
Surr: p-Terphenyl-d14
4.43
5.000
88.5
20
181
0
H
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 24 of 36

summint Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
Won: 23121878
04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177129
Sample ID: LCS-R177129
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 177129
Client ID: LCSS
Batch ID: R177129
TestNo: SW1030
Analysis Date: 12/28/2023
SegNo: 4797924
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
7.14
7.240 0 98.6 70 130
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 25 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177170
Sample ID: MB-R177170
SampType: MBLK
TestCode: PctSolid_S(2 Units: %
Prep Date:
RunNo: 177170
Client ID: PBS
Batch ID: R177170
TestNo: A2540B
Analysis Date: 12/27/2023
SegNo: 4800158
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Percent Solids -0.440 0 0
Sample ID: LCS-R177170
SampType: LCS
TestCode: PctSolid_S(2 Units: %
Prep Date:
RunNo: 177170
Client ID: LCSS
Batch ID: R177170
TestNo: A2540B
Analysis Date: 12/27/2023
SegNo: 4800159
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Percent Solids 100
100.0 0 100 90 110
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 26 of 36

summint Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
WO#: 23121878
04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177261
Sample ID: LCS-R177261
SampType: LCS
TestCode: pH_Oil(9045D Units: s.u.@18.9C
Prep Date:
RunNo: 177261
Client ID: LCSW
Batch ID: R177261
TestNo: SW9045D
Analysis Date: 12/29/2023
SegNo: 4802267
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.0
7.0 0 101 90 110
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 27 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177261
Sample ID: LCS-R177261
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@18.8C
Prep Date:
RunNo: 177261
Client ID: LCSW
Batch ID: R177261
TestNo: SW9045D
Analysis Date: 12/29/2023
SegNo: 4802259
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 23121947-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@17.7C
Prep Date:
RunNo: 177261
Client ID: BatchQC
Batch ID: R177261
TestNo: SW9045D
Analysis Date: 12/29/2023
SegNo: 4802261
Analyte
Result
PQL SPK value SPK Ref Val %REC
LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.3
7.2 0.7 5 H
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 28 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177326
Sample ID: RLC 10 PPB
SampType: RLC
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 177326
Client ID: BatchQC
Batch ID: R177326
TestNo: SW8321
Analysis Date: 12/29/2023
SegNo: 4804194
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
ND
0.0100 0.01000
0 55.0
50
150
2,4,5-TP
ND
0.0100 0.01000
0 46.0
50
150 S
Surr: 2,4-Dichlorophenylacetic acid
0.00510
0.01000
51.0
70
130 S
Sample ID: MBLK
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 177326
Client ID: PBS
Batch ID: R177326
TestNo: SW8321
Analysis Date: 12/29/2023
SegNo: 4804195
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 0.0100
2,4,5-TP ND 0.0100
Surr: 2,4-Dichlorophenylacetic acid 0.756 1.000 75.6 70 130
Sample ID: LCS
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 177326
Client ID: LCSS
Batch ID: R177326
TestNo: SW8321
Analysis Date: 12/29/2023
SegNo: 4804196
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.234 0.0100 0.3000 0 78.0 60.5 141
2,4,5-TP 0.216 0.0100 0.3000 0 72.2 68.3 144
Surr: 2,4-Dichlorophenylacetic acid 0.254 0.3000 84.7 70 130
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 29 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177326
Sample ID: LCSD
SampType: LCSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 177326
Client ID: LCSS02
Batch ID: R177326
TestNo: SW8321
Analysis Date: 12/29/2023
SegNo: 4804197
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.251
0.0100 0.3000
0 83.8
60.5
141 0.2339
7.21
30
2,4,5-TP
0.229
0.0100 0.3000
0 76.2
68.3
144 0.2165
5.44
30
Surr: 2,4-Dichlorophenylacetic acid
0.266
0.3000
88.8
70
130
0
0
Sample ID: 23121878-001ADUP
SampType: DUP
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 177326
Client ID: NRWASA
Batch ID: R177326
TestNo: SW8321
Analysis Date: 12/29/2023
SegNo: 4804199
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
2,4-D ND 0.500 0 0 20
2,4,5-TP ND 0.500 0 0 20
Surr: 2,4-Dichlorophenylacetic acid 44.2 50.00 88.4 70 130 0 0
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 30 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177351
Sample ID: MB-R177351
SampType: MBLK
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 177351
Client ID: PBS
Batch ID: R177351
TestNo: SW9034
Analysis Date: 1/2/2024
SegNo: 4804537
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R177351
SampType: LCS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 177351
Client ID: LCSS
Batch ID: R177351
TestNo: SW9034
Analysis Date: 1/2/2024
SegNo: 4804538
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 4920 25.0 5920 0 83.1 14 110
Sample ID: 23121878-001AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 177351
Client ID: NRWASA
Batch ID: R177351
TestNo: SW9034
Analysis Date: 1/2/2024
SegNo: 4804540
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 2950 25.0 5920 0 49.8 10 163
Sample ID: 23121878-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 177351
Client ID: NRWASA
Batch ID: R177351
TestNo: SW9034
Analysis Date: 1/2/2024
SegNo: 4804541
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 3800 25.0 5920 0 64.2 10 163 2949 25.2 30
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 31 of 36

summint Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
QC SUMMARY REPORT
Won: 23121878
04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177351
Sample ID: 23121878-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 177351
client ID: NRWASA
Batch ID: R177351
TestNo: SW9034
Analysis Date: 1/2/2024
SegNo: 4804541
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 32 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177395
Sample ID: MB-R
SampType: MBLK
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 177395
Client ID: PBS
Batch ID: R177395
TestNo: SW9014
Analysis Date: 1/2/2024
SegNo: 4806038
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500
Sample ID: LCS-R
SampType: LCS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 177395
Client ID: LCSS
Batch ID: R177395
TestNo: SW9014
Analysis Date: 1/2/2024
SegNo: 4806039
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 4.73 0.500 10.00 0 47.3 22 110
Sample ID: RLC-R
SampType: RLC
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 177395
Client ID: BatchQC
Batch ID: R177395
TestNo: SW9014
Analysis Date: 1/2/2024
SegNo: 4806040
Analyte
Result
PQL SPK value SPK Ref Val
%REC LowLimit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive ND 0.500 0.5000 0 36.5 14 156
Sample ID: 23121878-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 177395
Client ID: NRWASA
Batch ID: R177395
TestNo: SW9014
Analysis Date: 1/2/2024
SegNo: 4806042
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 1.40 0.362 10.00 0 14.0 10 167 QMR
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 33 of 36

summint Summit Environmental Technologies, Inc. QC SUMMARY REPORT
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC Cuyahoga Falls, Ohio 44223 WO#: 23121878
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 04-Jan-24
Client: Synagro
Project: Nevse Regional WASA BatchID: R177395
Sample ID: 23121878-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 177395
Client ID: NRWASA
Batch ID: R177395
TestNo: SW9014
Analysis Date: 1/2/2024
SegNo: 4806042
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 23121878-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 177395
Client ID: NRWASA
Batch ID: R177395
TestNo: SW9014
Analysis Date: 1/2/2024
SegNo: 4806043
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 2.61 0.403 10.00 0 26.1 10 167 1.399 60.3 10 R
Qualifiers: E Value above quantitation range H Holding times for preparation or analysis exceeded M Manual Integration used to determine area response
ND Not Detected PL Permit Limit R RPD outside accepted recovery limits
RL Reporting Detection Limit S Spike Recovery outside accepted recovery limits W Sample container temperature is out of limit as spec Original
Page 34 of 36

company aulixess Froject Address
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Notes/Comments:
State of Sample Origin:
Check if FOR COMPLIANCE
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White and yellow pages should accompany samples to the laboratory. The
client retains the pink page.
spy

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNOLOGIES, INC. Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Analytical Laboratories TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
Client Name: SYN-NC-27028 Work Order Number: 23121878 RcptNo: 1
Logged by: Anthony W. Britton 12/27/2023 9:40:00 AM C
Completed By: Anthony W. Britton 12/27/2023 2:48:21 PM
Reviewed By: Jennifer Woolf 12/27/2023 3:22:23 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? FedEx
Loa In
3.
Coolers are present?
Yes
No
❑
NA ❑
4.
Shipping container/cooler in good condition?
Yes
❑d
No
❑
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present ❑d
No. Seal Date:
Signed By:
5.
Was an attempt made to cool the samples?
Yes
❑d
No
❑
NA ❑
6.
Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No
❑
NA ❑
7.
Sample(s) in proper container(s)?
Yes
❑d
No
❑
8.
Sufficient sample volume for indicated test(s)?
Yes
❑d
No
❑
g.
Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10.
Was preservative added to bottles?
Yes
❑
No
❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑d
12. Were any sample containers received broken?
Yes
❑
No ❑d
13. Does paperwork match bottle labels?
Yes
❑d
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No ❑
15. Is it clear what analyses were requested?
Yes
❑
No ❑d
16. Were all holding times able to be met?
Yes
❑d
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA ❑d
Person Notified: r Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Logged per previous work orders
Client wrote Herbicide&Pesticide as requested analytical, but writing it that way would indicate total H&P and not TCLP H&P.
Cooler Information
Cooler No
Temp °C
I Condition
Seal Intact
Seal No
Seal Date
Signed By
1
4.2
1 Good
Not Present
Pa e 36 of
6