WQ0004825_2023 Residual Annual Report_20240228 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * W00004825
Applicant/Permittee City of Randleman
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0004825
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
City of Randleman Class B Residuals Program
Please provide comments/notes on your current submittal below.
Submission of the 2023 Annual Report for City of Randleman, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Randleman NC 2023 Annual Report FINAL.pdf 18.45MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tl�
Submission Date 2/28/2024

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 28, 2024
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report for Permit No. WQ0004825
Dear NCDEQ:
SYNAGRO
Synagro is submitting an electronic copy of the above referenced report on behalf of the City of
Randleman, NC.
If you have any questions or need additional information, please do not hesitate to contact Nick
Holcomb at [phone] or Adam Brigman at [phone].
Sincerely,
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Nick Holcomb, City of Randleman
Ryan Copeland, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

CITY OF RANDLEMAN, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0004825
2023 ANNUAL REPORT

City of Randleman, NC
Residuals Land Application Program
2023 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms & Metals Field
Loading Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00004825 County Randolph Year 2023
Facility Name (as shown on permit) City of Randleman WWTP NPDES No. NCO025445
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summary:
Total number of application fields in the permit: 18
Total number of fields utilized for land application during the year: 2
Total amount of dry tons applied during the year for all application sites: 65.37
Total number of acres utilized for land application during the year: 50.78
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .I 105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. l
am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations."
Michael Glass Plant Superintendent
Permittee Nalne and Title (type or print) Ntgnature or rernu ee uaLe
W",- ) -,u :N2/01/2024
Signature of Preparer* Date Si and Uplier Date
(if different from Permittee) (if different fr m Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
DATE RANGE: 1/1/2023 - 12/31/2023
RANDLEMAN,NC
RANDLEMAN, NC RANDLEMAN WWTP LIQUID
MONTH/YEAR
April 2023
July 2023
IEel f1I
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/9/2024 6:18:44 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
266,600.00
G
33.46
D
30.35
254,200.00
G
31.91
D
28.94
520,800.00
G
65.37
D
59.29

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00004825 Laboratory:
Facility Name: RANDLEMAN, NC Waypoint Analytical Virginia Inc.
Residual Source WQ # or
NPDES#: NCO025445
WWTP Name: RANDLEMAN WWTP
Residual Analysis Data
Product Type
LIQ
LIQ
LIQ
Sample or Composite Date
04/11/23
06/15/23
09/28/23
Parameter (mg/kg dry weight)
Ceiling Conc.
Limit
Percent Solids (.°!o)
NA
3.01
72.60
3.04
Arsenic
75
<16.7
<0.5
<16.7
Cadmium
85
53.33
<0.1
<3.33
Copper
4300
383
10.2
97
Chromium
NA
25.2
0.674
38.7
Lead
840
460
12.3
<10
Mercury
57
<6.27
<0.179
<5.77
Molybdenum
75
11.8
0.366
<8.33
Nickel
420
18.3
0.52
13.3
Selenium
100
19.6
<0.5
<16.7
Zinc
7500
447
12.3
407
Total Phosphorus
NA
11100
309
14100
TKN
NA
44300
1730
39000
Ammonia -Nitrogen
NA
3900
128
3900
Nitrate and Nitrite
NA
<167
<5
2190
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
x W/ Z 2-23-21
Signature of Preparer* Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF (12/2006)
Printed: 2/9/2024 6:29:47 PM For: 2027 01

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WO Permit Number:
W00004825
Facility Name:
RANDLEMAN, NC
Residual Source
NPDES # or WQ#:
NCO025445
WWTP Name:
RANDLEMAN WWTP
Residual Analysis Data
Product Type
Sample or Composite Date
Parameters (mg/kg dry weight)
Aluminium
Calcium
Magnesium
pH (s.u.)
Potassium
Sodium
PAN
SAR (Ratio)
Laboratory:
Waypoint Analytical Virginia Inc.
LIQ LIQ LIQ
04/11/23 06/15/23 09/28/23
7730
229
23100
108000
2930
147000
5630
149
3700
10.80
10.00
11.60
2190
59.8
3370
1420
38.1
3240
14246
550
14670
0.1977
0.1583
0.3969
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
=�� 2 2 2�
Signature of Preparer Date
'Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 2/9/2024 6:30:41 PM For: 2027 01 DENR FORM RSSF-B (12/2006)

Waypointo
ANALYTICAL
4/20/2023
Synagro Central LLC/ Randleman
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-102-0002
Project Description: Randleman
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 4/12/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-102-0002
Client Project Description: Randleman
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
61705
Tanker
Solids
61705
Tanker
Solids
61705
Tanker
Solids
61705
Tanker
Solids
61705
Tanker
Solids
61705
Tanker
Solids
61705
Tanker
Solids
61705
Tanker
Solids
61705
Tanker
Solids
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
04/11/2023
08:20
04/12/2023
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

WayPANALYTICAL
46483
Synagro Central LLC/ Randleman Project Randleman
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Number : 23-102-0002 REPORT OFANALYSIS
Report Date : 04/20/2023
Received : 04/12/2023
Brandi Watson
Lab No : 61705
Sample ID : Tanker
Matrix: Solids
Sampled: 4/11/2023 8:20
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
44300
mg/Kg
- dry
8330
1
04/19/23 09:30
JPJ ;M-4500-NH3C-TKI`
Potassium
2190
mg/Kg
- dry
333
1
04/15/23 06:50
BKN
6010D
Calcium
108000
mg/Kg
- dry
1670
1
04/15/23 06:50
BKN
6010D
Magnesium
5630
mg/Kg
- dry
167
1
04/15/23 06:50
BKN
6010D
Sodium
1420
mg/Kg
- dry
833
1
04/15/23 06:50
BKN
6010D
Iron
12600
mg/Kg
- dry
333
1
04/15/23 06:50
BKN
6010D
Aluminum
7730
mg/Kg
- dry
167
1
04/15/23 06:50
BKN
6010D
Zinc
447
mg/Kg
- dry
41.7
1
04/15/23 06:50
BKN
6010D
Nitrate+Nitrite-N
<167
mg/Kg
- dry
167
1
04/18/23 13:28
ZBD
4500NO3F-2011
Chromium
25.2
mg/Kg
- dry
8.33
1
04/15/23 06:50
BKN
6010D
Arsenic
<16.7
mg/Kg
- dry
16.7
1
04/15/23 06:50
BKN
6010D
Mercury
<6.27
mg/Kg
- dry
6.27
1
04/14/23 11:58
FDS
SW-7471B
Molybdenum
11.8
mg/Kg
- dry
8.33
1
04/15/23 06:50
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
pH
10.8
S.U.
1 04/18/2314:52 JJJ
9045D
Lead
460
mg/Kg -
dry
10.0
1 04/15/23 06:50 BKN
6010D
Manganese
427
mg/Kg -
dry
16.7
1 04/15/23 06:50 BKN
6010D
Nickel
18.3
mg/Kg -
dry
8.33
1 04/15/23 06:50 BKN
6010D
Selenium
19.6
mg/Kg -
dry
16.7
1 04/15/23 06:50 BKN
6010D
Qualifiers/
DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 3 of 7

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46483
Synagro Central LLC/ Randleman Project Randleman
Mary Brewer Report Date : 04/20/2023
284 Boger Road Information : Received : 04/12/2023
Mocksville , NC 27028
Brandi Watson
Report Number : 23-102-0002 REPORT OFANALYSIS
Lab No : 61705 Matrix: Solids
Sample ID : Tanker Sampled: 4/11/2023 8:20
Test
Results
Units
MQL
DF Date / Time
Analyzed
By
Analytical
Method
Sulfur
11900
mg/Kg - dry
333
1 04/15/23 06:50
BKN
6010D
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Batch
Moisture
97.0
%
0.010
1 04/17/2315:25
JLS
L676555
Total Solids
Phosphorus
Copper
Ammonia Nitrogen
Organic N
Cadmium
Calcium Carbonate Equivalent
Qualifiers/ DF Dilution Factor
Definitions
3.01
%
0.010
11100
mg/Kg -
dry
167
383
mg/Kg -
dry
16.7
3900
mg/Kg -
dry
3330
40430
mg/Kg -
dry
8333
<3.33
mg/Kg -
dry
3.33
22.2
%
0.1
1 04/17/23 15:25
JLS
SM-2540G
1 04/15/23 06:50
BKN
6010D
1 04/15/23 06:50
BKN
6010D
1 04/20/23 06:00
JPJ
SM-4500-NH3C
1 04/19/23 09:30
CALCULATION
1 04/15/23 06:50
BKN
6010D
1 04/20/23 10:35
DXT
AOAC 955.01
MQL Method Quantitation Limit
Page 4 of 7

Waypoint".0 -
ANALYTICAL
Client: Synagro Central LLC/ Randleman
Project: Randleman
Lab Report Number: 23-102-0002
Date: 4/20/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 96083 (SS-2)
Analyte: Aluminum
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083 (SS-2)
Analyte: Iron
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083 (SS-2)
Analyte: Potassium
QC Batch No: 1-676920/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 96083 (SS-2)
Analyte: Manganese
QC Batch No: 1-676414/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 96083 (SS-2)
Analyte: Lead
QC Batch No: 1-676414/1-676041
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 95708
Analyte: Mercury
QC Batch No: 1-676255/1-676023
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46483
Customer Name: Synagro Central LLC/ Randleman
Report Number: 23-102-0002
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 04/12/2023 09:37:09
Page 6 of 7

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Waypointo
ANALYTICAL
7/5/2023
Synagro Central LLC/ Randleman
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-167-0007
Project Description: Randleman
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 6/16/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-167-0007
Client Project Description: Randleman
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
62329
Lagoon
Tank
Solids
06/15/2023 09:45
06/16/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2011
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46483
Synagro Central LLC/ Randleman Project Randleman
Mary Brewer Report Date : 07/05/2023
284 Boger Road Information : Received : 06/16/2023
Mocksville , NC 27028
Brandi Watson
Report Number : 23-167-0007 REPORT OFANALYSIS
Lab No : 62329 Matrix: Solids
Sample ID : Lagoon Tank Sampled: 6/15/2023 9:45
Test Results Units MQL DF Date / Time By Analytical
Analyzed Method
Moisture
27.4
%
0.010
1
06/20/2316:10
KDO
SM-2540G
Sulfur
344
mg/Kg
10.0
1
06/22/23 00:38
BKN
6010D
Calcium
2930
mg/Kg
50.0
1
06/22/23 00:38
BKN
6010D
Aluminum
229
mg/Kg
5.00
1
06/22/23 00:38
TJS
6010D
Manganese
12.0
mg/Kg
0.500
1
06/22/23 00:38
BKN
6010D
Organic N
1602
mg/Kg
250.0
1
06/25/23 16:00
CALCULATION
Nickel
0.520
mg/Kg
0.250
1
06/22/23 00:38
BKN
6010D
Lead
12.3
mg/Kg
0.300
1
06/22/23 00:38
BKN
6010D
Arsenic
<0.500
mg/Kg
0.500
1
06/22/23 00:38
BKN
6010D
Selenium
<0.500
mg/Kg
0.500
1
06/22/23 00:38
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids
72.6
%
0.010
1 06/20/23 16:10 KDO
SM-2540G
Phosphorus
309
mg/Kg
5.00
1 06/22/23 00:38 BKN
6010D
Copper
10.2
mg/Kg
0.500
1 06/22/23 00:38 BKN
6010D
Total Kjeldahl Nitrogen
1730
mg/Kg
250
1 06/25/23 16:00 JPJ
;M-4500-NH3C-TKI`
Qualifiers/ DF
Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 3 of 7

WayP
�' 7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46483
Synagro Central LLC/ Randleman Project Randleman
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
Report Number : 23-167-0007
REPORT OFANALYSIS
Report Date : 07/05/2023
Received : 06/16/2023
Brandi Watson
Lab No : 62329
Sample ID : Lagoon Tank
Matrix: Solids
Sampled: 6/15/2023 9:45
Potassium
59.8
mg/Kg
10.0
1
06/22/23 00:38
TJS
6010D
Magnesium
149
mg/Kg
5.00
1
06/22/23 00:38
BKN
6010D
Sodium
38.1
mg/Kg
25.0
1
06/22/23 20:08
TJS
6010D
Iron
352
mg/Kg
10.0
1
06/22/23 00:38
TJS
6010D
Zinc
12.3
mg/Kg
1.25
1
06/22/23 00:38
BKN
6010D
Ammonia Nitrogen
128
mg/Kg
100
1
06/29/23 08:25
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<5.00
mg/Kg
5.00
1
06/30/2316:05
CLP
4500NO3F-2011
Cadmium
<0.100
mg/Kg
0.100
1
06/22/23 00:38
BKN
6010D
Chromium
0.674
mg/Kg
0.250
1
06/22/23 00:38
BKN
6010D
Mercury
<0.179
mg/Kg
0.179
1
06/21/2311:18
FDS
SW-7471B
pH
10.0
S.U.
1
06/22/2315:00
CNB
9045D
Molybdenum
0.356
mg/Kg
0.250
1
06/22/23 00:38
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypoint".0
ANALYTICAL
Client: Synagro Central LLC/ Randleman
Project: Randleman
Lab Report Number: 23-167-0007
Date: 7/3/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 88022 (8)
Analyte: Aluminum
QC Batch No: 1-689270/1-688769
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88022 (8)
Analyte: Calcium
QC Batch No: 1-689103/1-688769
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88022 (8)
Analyte: Iron
QC Batch No: 1-689270/1-688769
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 88022 (8)
Analyte: Potassium
QC Batch No: 1-689103/1-688769
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 88022 (8)
Analyte: Potassium
QC Batch No: 1-689270/1-688769
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 88022 (8)
Analyte: Phosphorus
QC Batch No: 1-689103/1-688769
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46483
Customer Name: Synagro Central LLC/ Randleman
Report Number: 23-167-0007
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 06/16/2023 09:12:34
Page 6 of 7

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Waypointo
ANALYTICAL
10/10/2023
Synagro Central LLC/ Randleman
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-272-0005
Project Description: Randleman
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 9/29/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 7

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-272-0005
Client Project Description: Randleman
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
63555
Randleman
Solids
09/28/202316:30
09/29/2023
SM-2540G
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SM-4500-NH3C
WP MTN
9045D
WP MTN
AOAC 955.01
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 7

WayPANALYTICAL
46483
Synagro Central LLC/ Randleman Project Randleman
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Number : 23-272-0005 REPORT OFANALYSIS
Report Date : 10/10/2023
Received : 09/29/2023
Brandi Watson
Lab No : 63555
Sample ID : Randleman
Matrix: Solids
Sampled: 9/28/2023 16:30
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
39000
mg/Kg
- dry
8330
1
10/09/23 13:18
JPJ ;M-4500-NH3C-TKI`
Potassium
3370
mg/Kg
- dry
333
1
10/06/23 01:01
BKN
6010D
Calcium
147000
mg/Kg
- dry
1670
1
10/06/23 01:01
BKN
6010D
Magnesium
3700
mg/Kg
- dry
167
1
10/06/23 01:01
BKN
6010D
Sodium
3240
mg/Kg
- dry
833
1
10/06/23 01:01
BKN
6010D
Iron
8530
mg/Kg
- dry
333
1
10/06/23 01:01
BKN
6010D
Aluminum
23100
mg/Kg
- dry
167
1
10/06/23 01:01
BKN
6010D
Zinc
407
mg/Kg
- dry
41.7
1
10/06/23 01:01
BKN
6010D
Nitrate+Nitrite-N
2190
mg/Kg
- dry
167
1
10/05/23 14:31
CLP
4500NO3F-2016
Chromium
38.7
mg/Kg
- dry
8.33
1
10/06/23 01:01
BKN
6010D
Arsenic
<16.7
mg/Kg
- dry
16.7
1
10/06/23 01:01
BKN
6010D
Mercury
<5.77
mg/Kg
- dry
5.77
1
10/04/23 14:24
JTR
SW-7471B
Molybdenum
<8.33
mg/Kg
- dry
8.33
1
10/06/23 01:01
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
pH
11.6
S.U.
1 10/04/2316:20 CNB
9045D
Lead
<10.0
mg/Kg -
dry
10.0
1 10/06/23 01:01 BKN
6010D
Manganese
1180
mg/Kg -
dry
16.7
1 10/06/23 01:01 BKN
6010D
Nickel
13.3
mg/Kg -
dry
8.33
1 10/06/23 01:01 BKN
6010D
Selenium
<16.7
mg/Kg -
dry
16.7
1 10/06/23 01:01 BKN
6010D
Qualifiers/
DF Dilution Factor
MQL
Method Quantitation Limit
Definitions
Page 3 of 7

WayPANALYTICAL
46483
Synagro Central LLC/ Randleman
Project Randleman
Mary Brewer
284 Boger Road
Information
Mocksville , NC 27028
Report Number : 23-272-0005
REPORT OFAA
Lab No : 63555
Sample ID : Randleman
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Date : 10/10/2023
Received : 09/29/2023
Brandi Watson
VALYSIS
Matrix: Solids
Sampled: 9 / 28/ 2023 16:30
Test
Results
Units
MQL
DF Date / Time
Analyzed
By
Analytical
Method
Sulfur
8070
mg/Kg - dry
333
1 10/06/23 01:01
BKN
6010D
Analytical Method: SM-2540G
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Batch
Moisture
97.0
%
0.010
1 10/03/2316:04
CAH
L708437
Test
Results
Units
MQL
DF Date / Time
By
Analytical
Analyzed
Method
Total Solids
3.04
%
0.010
1
10/03/23 16:04
CAH
SM-2540G
Phosphorus
14100
mg/Kg -
dry
167
1
10/06/23 01:01
BKN
6010D
Copper
97.0
mg/Kg -
dry
16.7
1
10/06/23 01:01
BKN
6010D
Ammonia Nitrogen
3900
mg/Kg -
dry
3330
1
10/10/23 10:02
JPJ
SM-4500-NH3C
Organic N
35100
mg/Kg -
dry
8333
1
10/09/23 13:18
CALCULATION
Cadmium
<3.33
mg/Kg -
dry
3.33
1
10/06/23 01:01
BKN
6010D
Calcium Carbonate Equivalent
24.9
%
0.1
1
10/06/23 14:28
DXT
AOAC 955.01
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 7

Waypoint".0
ANALYTICAL
Client: Synagro Central LLC/ Randleman
Project: Randleman
Lab Report Number: 23-272-0005
Date: 10/10/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 85196 (SS-3, 1'-3')
Analyte: Aluminum
QC Batch No: 1-709315/1-708413
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85196 (SS-3, 1'-3')
Analyte: Iron
QC Batch No: 1-709315/1-708413
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85196 (SS-3, 1'-3')
Analyte: Potassium
QC Batch No: 1-709315/1-708413
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 85196 (SS-3, 1'-3')
Analyte: Manganese
QC Batch No: 1-709158/1-708413
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 85196 (SS-3, 1'-3')
Analyte: Lead
QC Batch No: 1-709158/1-708413
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 5 of 7

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46483
Customer Name: Synagro Central LLC/ Randleman
Report Number: 23-272-0005
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 09/29/2023 09:36:44
Page 6 of 7

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SECTION 3

FACILITY NAME: RANDLEMAN, NC
LAND OWNER: W. HOWARD FIELDS
OPERATOR: W. HOWARD FIELDS
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT M WQ0004825 FIELD#: NC-RD-00018-0-0003-
ANNUAL DRY TONS APPLIED: 33.46 SITE #: NC RD 00018
PREDOMINANT SOIL SERIES: CORONICA
CROP 1 MAX. PAN: 209 CROP 2 NAME:
ACRES UTILIZED: 18.9
ACRES PERMITTED: 18.9
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%"
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
�,
Application
�
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
.0
Amount
UOM
Crop 1
r
Crop 2
Crop 1
Crop 2
4/3/2023
86,800.00
(G)
3.010
0,576
RAL
DRY
-0-<1/2""
SUR
0.5
0.30
44,300.00
3,900.00
167.00
16.424
FSH
4/4/2023
49,600.00
(G)
3.D10
0.329
RAL
DRY
0-<1/2""
SUR
0.5
0.30
44,300.00
3,900.00
167.00
9.385
FSH
4/5/2023
130,200.00
(G)
3.010
0.865
RAL
DRY
0-<1/2""
SUR
0.5
0.30
44,300.00
3,900.00
167.00
24.636
FSH
Apr-23
266,600.00
(G)
Total 1.770
PB
Ibs/acre Applied 0.059
Cumulative Ibs/acre Applied 0,369 1 0.116 1 17.110 1 5.103 1 11.046
Total
HG MO NI SE ZN P
0.022 0.042 D.065 0.069 1.583 39.306
50.445 0.000
Lime Applied
Date Lbs/Ac
Permit PAN Limit (Ibs/acre) 1st Crop, zuy
Federal C.P.L.R. (Ibs/acre)**** 36.6 _ 34.8 1 1,339.0M267.9 15.0 375 0 89.0 2,500.0 `�
RAL = RANDLEMAN, NC RANDLEMAN WWTP LIQUID t
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submittin alse information, including the possibility of fines and imprisonme t for kyowing violations."
S NATURE OFk6WQAVPLIER DA E
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation ***' C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM"
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: RANDLEMAN, NC
Permit #: WQ0004625 Cation Exchange Capacity (non 503 only):
Operator: W. HOWARD FIELDS W. HOWARD FIELDS Predominant Soil Series:
Owner:
Acres Used: 18.90 Acres Permitted: 18.90 Site #: Field #:
NC RD 00018
Residual Analvsis Data fHeaw Metal. and Total Phnsnhnrus use mo/ka. % Solids use Raw Percent ft
3336
CORCUICA
NC RD 00)18 0003
Source
RAL
Sample or
Composite
Date
1
4/11/23
2
3
4
5
6
7
3
9
10
11
12
Solids
3.01
Arsenic
16.700
Cadmium
3.330
Copper
383
Chromium
25.20
Lead
460.00
Mercury
6.270
Molybdenum
11.80
Nickel
18,30
Selenium
1960,
Zinc
447
Total Phosphorus
11100
Annual Heavv Metal Field Loadings (Calculated in Ibs/acrel:
Source
RAL
Total DT/Ac.
/App.Event
1
177
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.059
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Cadmium
0.012
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.012
Copper
1.356
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
1.356
Chromium
0.089
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.089
Lead
1,629
mob
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
omo
0.000
1.629
Mercury
0.022
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.022
Molybdenum
0,042
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.042
Nickel
0.065
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.065
Selenium
0.069
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.069
Zinc
1.583
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
1.583
Total Phosphorus 1
39.306
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
39.306
9 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significant penalties f submitting false information, including the possibility of fines an/d�imp. sonmcnt £otr�knowing violations".
! G %Z
/,%!-7 ,/
Signature rl I a d A6plierl Date DENR FORM MFLSF(12/2006)

FACILITY NAME: RANDLEMAN, NC
LANDOWNER: WESLEY CHARLES DOBBINS
OPERATOR: WESLEY CHARLES DOBBINS
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: WQ0004825 FIELD#: NC-RD-00048-0-0001-
ANNUAL DRY TONS APPLIED: 31.91 SITE #: NC RD 00048
PREDOMINANT SOIL SERIES: BADIN-TARRUS
CROP 1 MAX. PAN: 171 CROP 2 NAME:
ACRES UTILIZED: 31.9
ACRES PERMITTED:31.9
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mglkg
mg/kg
mg/kg
Amount
UOM
Crop 1
Crop 2
Crop 1
Crop 2
7/25l2023
i:6,400.00
(G)
3.010
0.537
RAL
DRY
m 0-<1/2""
SUR
0.5
0.30
44,300.00
3,900.00
167.00
15.301
FSH
7/26/2023
117,800.00
(G)
3,010
0.464
RAL
DRY
0-<112""
SUR
0.5
0.30
44,300.00
3,900.00
167.00
13,215
FSH
Jul-23
254,200.00
(G)
Ibs/acre Applied
Total 1.001 Total 28.516 0.000
0.033
CR J PB HG MO NI SE ZIN
9 .050 1 0.921 0.013 0.024 0 037 030.895
8
Lime
Cumulative Ibs/acre Applied 0.033 0.007 0.767 0.050 0.921 1 0.013 1 0.024 0.037 0.039 0.895
Permit PAN Limit (Ibs/acre) 1st Cropl 171 __._..
Federal C.P L R. (Ibs/acre) * � 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
RAL = RANDLEMAN, NC RANDLEMAN WWTP LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations"
G 22 2-(
S RE OF LAND APPLIER DATE
NR = Not Reported o of Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
* Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: RANDLEMAN. NC 31.91
Permit #: W00004825 Cation Exchange Capacity (non 503 only):
Operator: WESLEY CHARLES DOBBINS WESLEY CHARLES DOBBINS Predominant Soil Series: BADIN-TARRUS
Owner:
Acres Used: 31.88 Acres Permitted: 31.88 Site #: Field #: NC RD 00048 0001
NC RD 00048
Residual Analvsis Data iHeavv Metals and Total Phosahorus use malko. % Solids use Raw Percent #1:
Source
RAL
Sample or
Composite
Date
1
4/11l23
2
3
4
5
6
7
8
9
10
11
12
Solids
3.01
Arsenic
16.700
Cadmium
3.330
Copper
383
Chromium
25.20
Lead
460.00
Mercury
6.270
Molybdenum
11.80
Nickel
18.30
Selenium
19.60
Zinc
447
Total Phosphorus
11100
Annual Heavy Metal Field Loadings (Calculated in Ibslacre):
Source
RAL
Total DT/Ac.
/ App.Event
1
1.00
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.033
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Cadmium
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Copper
0.767
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.767
Chromium
0,050
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.050
Lead
0.921
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,921
Mercury
0.013
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Molybdenum
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Nickel
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0,037
Selenium
0.039
0.000
0.000
0.000
0,000
moo
0.000
0.000
0.000
0.000
0.000
0.000
0.039
Zinc
0.895
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.895
Total Phosphorus
22.218
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
22.218
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ]snowing violations".
Signature of .0F r Date DENR FORM MFLSF (1212006)

SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
ArrzrJy0ca1 Laboralorfas
April 02, 2021
Ryan Copeland
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Randleman WWTP
Dear Ryan Copeland:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 21031812
Summit Environmental Technologies, Inc. received 1 sample(s) on 3/26/2021 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho OH00923, Illinois 200061, Indiana C-OH-13, Kansas
E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988, Minnesota 1780279, Nevada OH009232020-1, New
Hampshire 2996, New Jersey OH006, New York 11777, North Carolina 39705 and 631, North Dakota R-201, Ohio DW, Ohio VAP C1,0052, Oklahoma
2019-155, Oregon OH2O0001, Pennsylvania 011, Rhode Island LA000317, South Carolina 92016001, Texas T104704466-19-16, Utah OH009232020-12,
Virginia VELAP 10381, West Virginia 9957C
Page 1 of 34

SUMMIY Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 WO#: 21031812
Arralyi9cal Laboraloaes TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 4/2/2021
CLIENT: Synagro
Project: Randleman WWTP
WorkOrder Narrative:
21031812: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
21031812-OOIA TCLP-VOC-MSTR 8260D: Corresponding QC exhibited high recovery for Vinyl
chloride. Sample is ND
Analytical Sequence QC Notes:
Pest CCV1 500ppb TCLP-SVOC-CPEST(8081B): P: RPD between confirmation column is greater
than 40%.
CCV VOC-MSTR_NPW(8260): CCV exhibits high recovery for Vinyl chloride. Associated samples
are N.D. for this analyte.
LCS-48669 TCLP-VOC-MSTR TCLP(8260)
Associated samples are N.D. for this analyte.
LCS exhibits high recovery for VInyl chloride.
Original
Page 2 of 34

SUMMIY Summit Environmental Technologies, Inc. Case Narrative
3310 Win St.
ENVIRONMENTAL TEC„HQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 WO#: 21031812
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 4/2/2021
CLIENT: Synagro
Project: Randleman WWTP
LCS-48669 TCLP-VOC-MSTR TCLP(8260): Possible high bias for Vinyl chloride due to high
recovery in CCV.
Original
Page 3 of 34

�� Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
Ekiwlt OMM@N-rALTECHN❑LOG{r,S,INC Cuyahoga Falls, Ohio442� WO#: 21031812
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-446
Wehsite: httn:11www.settek.co Date: 4/2/2021
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GC/MS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low () or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low () or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low () or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low () or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 34

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRCNMEWAL YECHHOLOGNUS, JNC, Cuyahoga Falls, Ohio 44223
Arraly0cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Randleman WWTP
Lab SampleID Client Sample ID
21031812-001 Randleman WWI'P
Tag No Date Collected
3/25/2021 9:10:00 AM
Workorder
Sample Summary
WO#: 21031812
02 Apr-21
Date Received Matrix
3/26/2021 4:00:00 PM Sludge
Page 5 of 34

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES REPORT
ENVIRONMENTAL TECHN❑ L0G1E5, IrJG
Cuyahoga Falls, Ohio 44223
WO#: 21031812
ArWyft cal taboralonas
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
02 Apr-21
Client:
Synagro
Project:
Randleman WWTP
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
21031812-OOIA Randleman WWTP 3/25/2021 9:10:00 AM Sludge Ignitability of Solids (SW-846: 1030)
4/1/2021 11:13:20 AM
pH (SW9045D)
3/29/2021 5:36:55 PM
Reactive Cyanide (9014/7.3.32)-Solid
3/31/2021 2:55:00 PM
Reactive Sulfide (9034)/7.3.42
3/31/2021 2:55:00 PM
TCLP Herbicides by EPA 832113
3/31/2021 4:00:00 PM 4/2/2021 12:54:00 AM
TCLP Mercury Analysis (SW1311/7473/31/2021 4:00:00 PM
4/2/2021 10:25:00 AM 4/2/2021 3:25:00 PM
TCLP Metals Analysis (SW1311/6010:3/31/2021 4:00:00 PM
4/1/2021 1:30:00 PM 4/2/2021 1:30:34 PM
TCLP Pesticides Analysis (SW1311/8(3/31/2021 4:00:00 PM
4/1/2021 11:55:00 AM 4/1/2021 8:55:00 PM
TCLP Pesticides Analysis (SW1311/8(3/31/2021 4:00:00 PM
4/1/2021 11:55:00 AM 4/1/2021 8:55:00 PM
TCLP Semi-Volatiles Analysis 3/31/2021 4:00:00 PM
3/31/2021 12:10:00 PM 4/1/2021 8:26:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
3/31/2021 4:00:00 PM 4/1/2021 7:56:00 PM
Original
Page 6 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVITtONMENTALTECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralories TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 21031812
Date Reported: 4/2/2021
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 3/25/2021 9:10:00 AM
Lab ID:
21031812-OOIA
Project:
Randleman WWTP
Client Sample ID Randleman WWTP
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.0100 mg/L
SW7470A SW7470A Analyst: ERA
1 4/2/2021 3:25:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010D
SW301OA Analyst: DNS
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
4/2/2021 1:30:34 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
4/2/2021 1:30:34 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
4/2/2021 1:30:34 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
4/2/2021 1:30:34 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
4/2/2021 1:30:34 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
4/2/2021 1:30:34 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
4/2/2021 1:30:34 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: SFG
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.500
mg/L
5
4/1/2021 8:26:00 PM
2,4,5-Trichlorophenol
ND
1.25
mg/L
5
4/1/2021 8:26:00 PM
2,4,6-Trichlorophenol
ND
1.25
mg/L
5
4/1/2021 8:26:00 PM
2,4-Dinitrotoluene
ND
0.100
mg/L
5
4/1/2021 8:26:00 PM
Cresols, Total
ND
25.0
mg/L
5
4/1/2021 8:26:00 PM
Hexachloro-1,3-butadiene
ND
0.100
mg/L
5
4/1/2021 8:26:00 PM
Hexachlorobenzene
ND
0.100
mg/L
5
4/1/2021 8:26:00 PM
Hexachloroethane
ND
0.500
mg/L
5
4/1/2021 8:26:00 PM
Nitrobenzene
ND
0.500
mg/L
5
4/1/2021 8:26:00 PM
Pentachlorophenol
ND
1.25
mg/L
5
4/1/2021 8:26:00 PM
Pyridine
ND
1.25
mg/L
5
4/1/2021 8:26:00 PM
Surr: 2-Fluorophenol
65.1
10 - 157
%Rec
5
4/1/2021 8:26:00 PM
Surr: Phenol-d6
74.7
10 - 169
%Rec
5
4/1/2021 8:26:00 PM
Surr: Nitrobenzene-d5
85.2
32.1 - 130
%Rec
5
4/1/2021 8:26:00 PM
Surr: 2,4,6-Tribromophenol
98.9
45.4 - 166
%Rec
5
4/1/2021 8:26:00 PM
Surr: 2-Fluorobiphenyl
79.8
35.7 - 130
%Rec
5
4/1/2021 8:26:00 PM
Surr: p-Terphenyl-d14
103
70 - 145
%Rec
5
4/1/2021 8:26:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound
Limit.
N Tentatively identified
compounds
ND Not Detected
P Second column
confirmation
exceeds
PL Permit Limit
R RPD outside accepted
recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal <MDL
Page 7 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVITtONMENTALTECHNOLOGIE_3,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 21031812
Date Reported: 4/2/2021
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 3/25/2021 9:10:00 AM
Lab ID:
21031812-OOIA
Project:
Randleman WWTP
Client Sample ID Randleman WWTP
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC Analyst: CSS
TCLP PESTICIDES ANALYSIS
(SW1311/8081)
Chlordane, total
ND
0.0250
mg/L
1
4/1/2021 8:55:00 PM
Toxaphene
ND
0.0500
mg/L
1
4/1/2021 8:55:00 PM
Endrin
ND
0.00250
mg/L
1
4/1/2021 8:55:00 PM
gamma-BHC
ND
0.00250
mg/L
1
4/1/2021 8:55:00 PM
Heptachlor
ND
0.00250
mg/L
1
4/1/2021 8:55:00 PM
Heptachlor epoxide
ND
0.00250
mg/L
1
4/1/2021 8:55:00 PM
Methoxychlor
ND
0.00250
mg/L
1
4/1/2021 8:55:00 PM
Surr: TCMX
64.2
10 - 119
%Rec
1
4/1/2021 8:55:00 PM
Surr: DCB
71.6
10 - 119
%Rec
1
4/1/2021 8:55:00 PM
TCLP HERBICIDES BY EPA 8321 B
SW8321
SW1311 M Analyst: TM
2,4-D
ND
0.500
mg/L
50 4/2/2021 12:54:00 AM
2,4,5-TP
ND
0.500
mg/L
50 4/2/2021 12:54:00 AM
Surr: 2,4-Dichlorophenylacetic aci
85.0
70 - 130
%Rec
50 4/2/2021 12:54:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
SW1311M Analyst: MES
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene
ND
0.250
mg/L
50 4/1/2021 7:56:00 PM
1,2-Dichloroethane
ND
0.250
mg/L
50 4/1/2021 7:56:00 PM
MEK
ND
5.00
mg/L
50 4/1/2021 7:56:00 PM
Benzene
ND
0.250
mg/L
50 4/1/2021 7:56:00 PM
Carbon tetrachloride
ND
0.250
mg/L
50 4/1/2021 7:56:00 PM
Chlorobenzene
ND
2.50
mg/L
50 4/1/2021 7:56:00 PM
Chloroform
ND
0.250
mg/L
50 4/1/2021 7:56:00 PM
Tetrachloroethene
ND
0.250
mg/L
50 4/1/2021 7:56:00 PM
Trichloroethene
ND
0.250
mg/L
50 4/1/2021 7:56:00 PM
Vinyl chloride
ND
0.100QC+QL+mg/L
50 4/1/2021 7:56:00 PM
Surr: 4-Bromofluorobenzene
91.3
70 - 130
%Rec
50 4/1/2021 7:56:00 PM
Surr: Di brom ofl uorom ethane
97.6
70 - 130
%Rec
50 4/1/2021 7:56:00 PM
Surr: Toluene-d8
99.1
70 - 130
%Rec
50 4/1/2021 7:56:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound
Limit.
N Tentatively identified compounds
ND Not Detected
P Second column
confirmation exceeds
PL Permit Limit
R RPD outside accepted
recovery limits Original
RL Reporting Detection Limit
U Samples with CalcVal
<MDL
Page 8 of 34

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNQLOGlr,$.IRC Cuyahoga Falls, Ohio44223 (base report)
Arrafyt9caf Laboralorfas TEL: [phone] FAX.- [phone] WO#: 21031812
Website: http://www.settek.com Date Reported: 4/2/2021
CLIENT:
Synagro Tag Number:
Matrix:
SLUDGE Collection Date: 3/25/2021 9:10:00 AM
Lab ID:
21031812-OOIA
Project:
Randleman WWTP
Client Sample ID Randleman WWTP
Analyses Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.490 mg/Kg
1
3/31/2021 2:55:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: KMW
Ignitability nonflammable
mm/sec
1
4/1/2021 11:13:20 AM
RCI
SW9045D
Analyst: ALT
PH (SW9045D)
pH 11.3
s.u.@17.2C
1
3/29/2021 5:36:55 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1
3/31/2021 2:55:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
H
Holding times for preparation or analysis exceeded
MC
Value is below Minimum Compound Limit.
ND
Not Detected
PL
Permit Limit
RL
Reporting Detection Limit
E Value above quantitation range
M Manual Integration used to determine area response
N Tentatively identified compounds
P Second column confirmation exceeds
R RPD outside accepted recovery limits original
U Samples with CalcVal <MDL
Page 9 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Analv n tes Report
ENOROMMEWAL YECHNOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
ArralyVcal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
21031812
Wehsite: http://www.settek.com
02 Apr 21
Client: Synagro
State: NW
Project: Randleman WWTP
Program Name: NC—WW—SCM
Sample ID Matrix
Test Name
Analyte
Status
21031812-OOIA Sludge
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Sludge
pH (SW9045D)
Hydrogen Ion (pH)
A
Sludge
Reactive Cyanide (9014/7.3.32)-Solid
Cyanide, Reactive
U
Sludge
Reactive Sulfide (9034)/7.3.42
Sulfide, Reactive
U
Sludge
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Sludge
TCLP Herbicides by EPA 8321B
2,4-D
A
Sludge
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Barium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Lead
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Sludge
TCLP Metals Analysis (SW1311/6010)
Silver
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Sludge
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Sludge
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Key
Key
NC WW SCM A Accredited
NC WW SCM U Unavailable
Version #2
Page 10 of 34

Summit Environmental Technologies, Inc.
Accreditation
Program
MM'EF
frSU3310 Win St.
Anal�7n tes Report
EMOROMMEWAL IrECHHOL,t
01ES, INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
WO#:
21031812
Wehsite: http://www.settek.com
02 Apr 21
Client: Synagro
State: NW
Project: Randleman WWTP
Program Name: NC—WW—SCM
Sample ID Matrix
Test Name
Analyte
Status
21031812-OOIA Sludge
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Sludge
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Sludge
TCLP Volatiles Analysis
2-Butanone
A
Sludge
TCLP Volatiles Analysis
Benzene
A
Sludge
TCLP Volatiles Analysis
Carbon tetrachloride
A
Sludge
TCLP Volatiles Analysis
Chlorobenzene
A
Sludge
TCLP Volatiles Analysis
Chloroform
A
Sludge
TCLP Volatiles Analysis
Tetrachloroethene
A
Sludge
TCLP Volatiles Analysis
Trichloroethene
A
Sludge
TCLP Volatiles Analysis
Vinyl chloride
A
NC WW SCM A Accredited NC WW SCM U Unavailable
Version #2
Page 11 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48651
Sample ID: 21031750-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 3/31/2021
RunNo: 125936
client ID: BatchQC
Batch ID: 48651
TestNo: SW8270 SW3510C
Analysis Date: 3/31/2021
SegNo: 3281271
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.591
0.200
0.8000
0
73.8
15.2
124
2,4,5-Trichlorophenol
0.821
0.500
0.8000
0
103
30.6
152
2,4,6-Trichlorophenol
0.856
0.500
0.8000
0
107
27.6
150
2,4-Dinitrotoluene
0.813
0.100
0.8000
0
102
58
141
o-Cresol
0.654
0.500
0.8000
0
81.8
26.9
132
Cresols, Total
ND
10.0
1.600
0
88.6
27.6
132
Hexachloro-1,3-butadiene
0.670
0.0400
0.8000
0
83.8
10
156
Hexachlorobenzene
0.757
0.100
0.8000
0
94.7
54.3
142
Hexachloroethane
0.587
0.200
0.8000
0
73.4
1.92
131
Nitrobenzene
0.714
0.200
0.8000
0
89.2
21
135
Pentachlorophenol
0.711
0.500
0.8000
0
88.8
47.4
134
Pyridine
ND
0.500
0.8000
0
52.8
10
130
Surr:2-Fluorophenol
0.846
1.000
84.6
9.77
146
Surr: Phenol-d6
0.878
1.000
87.8
20.7
130
Surr: Nitrobenzene-d5
0.946
1.000
94.6
13.9
156
Surr:2,4,6-Tribromophenol
1.15
1.000
115
27.3
183
Surr:2-Fluorobiphenyl
0.812
1.000
81.2
21.4
153
Surr: p-Terphenyl-d14
1.04
1.000
104
54.8
154
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
m
m
Original
Page 12 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48651
Sample ID: 21031750-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 3/31/2021
RunNo: 125936
client ID: BatchQC
Batch ID: 48651
TestNo: SW8270 SW3510C
Analysis Date: 3/31/2021
SegNo: 3281272
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.592
0.200
0.8000
0
74.1
15.2
124
0.5908
0.270
30
2,4,5-Trichlorophenol
0.761
0.500
0.8000
0
95.1
30.6
152
0.8208
7.59
30
2,4,6-Trichlorophenol
0.723
0.500
0.8000
0
90.4
27.6
150
0.8556
16.8
30
2,4-Dinitrotoluene
0.793
0.100
0.8000
0
99.1
58
141
0.8128
2.49
30
o-Cresol
0.688
0.500
0.8000
0
86.0
26.9
132
0.6540
5.13
30
Cresols, Total
ND
10.0
1.600
0
90.2
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.617
0.0400
0.8000
0
77.1
10
156
0.6704
8.33
30
Hexachlorobenzene
0.721
0.100
0.8000
0
90.2
54.3
142
0.7572
4.87
30
Hexachloroethane
0.608
0.200
0.8000
0
76.0
1.92
131
0.5872
3.48
30
Nitrobenzene
0.690
0.200
0.8000
0
86.2
21
135
0.7140
3.42
30
Pentachlorophenol
0.679
0.500
0.8000
0
84.8
47.4
134
0.7108
4.61
30
Pyridine
ND
0.500
0.8000
0
55.4
10
130
0
0
30 m
Surr:2-Fluorophenol
0.876
1.000
87.6
9.77
146
0
Surr: Phenol-d6
0.878
1.000
87.8
20.7
130
0
Surr: Nitrobenzene-d5
0.880
1.000
88.0
13.9
156
0
Surr:2,4,6-Tribromophenol
1.10
1.000
110
27.3
183
0
Surr:2-Fluorobiphenyl
0.726
1.000
72.6
21.4
153
0
Surr: p-Terphenyl-d14
1.10
1.000
110
54.8
154
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 13 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48651
Sample ID: MB-48651
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 3/31/2021
RunNo: 125936
client ID: PBS
Batch ID: 48651
TestNo: SW8270 SW3510C
Analysis Date: 3/31/2021
SegNo: 3281263
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.100
2,4,5-Trichlorophenol
ND
0.250
2,4,6-Trichlorophenol
ND
0.250
2,4-Dinitrotoluene
ND
0.0500
o-Cresol
ND
0.250
Cresols, Total
ND
5.00
Hexachloro-1,3-butadiene
ND
0.0200
Hexachlorobenzene
ND
0.0500
Hexachloroethane
ND
0.100
Nitrobenzene
ND
0.100
Pentachlorophenol
ND
0.250
Pyridine
ND
0.250
Surr: 2-Fluorophenol
0.783
Surr: Phenol-d6
0.737
Surr: Nitrobenzene-d5
0.835
Surr: 2,4,6-Tribromophenol
1.09
Surr: 2-Fluorobiphenyl
0.733
Surr: p-Terphenyl-d14
0.954
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
1.000
78.3
10
130
1.000
73.7
10
130
1.000
83.5
19
130
1.000
109
10
130
1.000
73.3
22
130
1.000
95.4
34
130
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 14 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48651
Sample ID: LCS-48651
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 3/31/2021
RunNo: 125936
client ID: LCSS
Batch ID: 48651
TestNo: SW8270 SW3510C
Analysis Date: 3/31/2021
SegNo: 3281264
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.578
0.100
0.8000
0
72.3
49.5
130
2,4,5-Trichlorophenol
0.769
0.250
0.8000
0
96.2
63.8
144
2,4,6-Trichlorophenol
0.802
0.250
0.8000
0
100
63.3
149
2,4-Dinitrotoluene
0.772
0.0500
0.8000
0
96.5
70
133
o-Cresol
0.685
0.250
0.8000
0
85.6
56.3
130
Cresols, Total
ND
5.00
1.600
0
86.8
57.3
130
Hexachloro-1,3-butadiene
0.635
0.0200
0.8000
0
79.4
45.2
130
Hexachlorobenzene
0.745
0.0500
0.8000
0
93.2
70
130
Hexachloroethane
0.603
0.100
0.8000
0
75.4
42.1
130
Nitrobenzene
0.670
0.100
0.8000
0
83.8
53.4
130
Pentachlorophenol
0.729
0.250
0.8000
0
91.1
68.8
132
Pyridine
0.381
0.250
0.8000
0
47.6
10
130
Surr:2-Fluorophenol
0.818
1.000
81.8
50.2
130
Surr: Phenol-d6
0.800
1.000
80.0
57.2
130
Surr: Nitrobenzene-d5
0.860
1.000
86.0
54.9
130
Surr:2,4,6-Tribromophenol
1.17
1.000
117
70
154
Surr:2-Fluorobiphenyl
0.742
1.000
74.2
56.3
130
Surr: p-Terphenyl-d14
1.09
1.000
109
70
145
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
m
Original
Page 15 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48669
Sample ID: MB-48669
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date: 3/31/2021
RunNo: 125958
Client ID: PBS
Batch ID: 48669
TestNo: SW8260 SW1311M
Analysis Date: 4/1/2021
SegNo: 3282208
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
ND
0.250
1,2-Dichloroethane
ND
0.250
MEK
ND
5.00
Benzene
ND
0.250
Carbon tetrachloride
ND
0.250
Chlorobenzene
ND
2.50
Chloroform
ND
0.250
Tetrachloroethene
ND
0.250
Trichloroethene
ND
0.250
Vinyl chloride
ND
0.100
Surr: 4-Bromofluorobenzene
2310
Surr: Dibromofluoromethane
2440
Surr: Toluene-d8
2460
2500 92.3 70 130
2500 97.8 70 130
2500 98.4 70 130
QC+
Sample ID: LCS-48669
SampType: LCS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 125958
Client ID: LCSS
Batch ID: 48669
TestNo: SW8260 SW1311M
Analysis Date: 4/1/2021
SegNo: 3282209
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
1.06 0.250
1.00 0 106
64.7
136
1,2-Dichloroethane
1.07 0.250
1.00 0 107
70
130
MEK
ND 5.00
5.00 0 93.8
55.1
149
Benzene
1.05 0.250
1.00 0 105
70
130
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area
response
MC
Value is below Minimum Compound
Original
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 16 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48669
Sample ID: LCS-48669
SampType: LCS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 125958
Client ID: LCSS
Batch ID: 48669
TestNo: SW8260 SW1311M
Analysis Date: 4/1/2021
SegNo: 3282209
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
1.06
0.250
1.00
0
106
70
130
Chlorobenzene
ND
2.50
1.00
0
97.2
70
130
Chloroform
0.972
0.250
1.00
0
97.2
70
130
Tetrachloroethene
0.856
0.250
1.00
0
85.6
70
134
Trichloroethene
0.972
0.250
1.00
0
97.2
62.8
160
Vinyl chloride
2.03
0.100
1.00
0
203
67.1
130
Surr:4-Bromofluorobenzene
2450
2500
98.0
70
130
Surr: Dibromofluoromethane
2380
2500
95.1
70
130
Surr: Toluene-d8
2370
2500
94.6
70
130
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
SQC+
Original
Page 17 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48669
Sample ID: 21031753-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 125958
Client ID: Batch=
Batch ID: 48669
TestNo: SW8260 SW1311M
Analysis Date: 4/l/2021
SegNo: 3282210
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
1.07
0.250
1.00
0
107
13.6
202
1,2-Dichloroethane
1.13
0.250
1.00
0
113
55.7
138
MEK
ND
5.00
5.00
0
96.5
65.3
118
Benzene
1.11
0.250
1.00
0
ill
49.2
145
Carbon tetrachloride
1.07
0.250
1.00
0
107
26.7
156
Chlorobenzene
ND
2.50
1.00
0
101
33.7
159
Chloroform
1.00
0.250
1.00
0
100
48.5
145
Tetrachloroethene
0.856
0.250
1.00
0
85.6
19.2
191
Trichloroethene
1.03
0.250
1.00
0
103
38.4
167
Vinyl chloride
2.08
0.100
1.00
0
208
27.3
161
Surr:4-Bromofluorobenzene
2470
2500
98.7
91.7
109
Surr: Dibromofluoromethane
2460
2500
98.5
75.5
118
Surr: Toluene-d8
2350
2500
94.1
94.1
105
SQC+
Sample ID: 21031753-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 125958
Client ID: Batch=
Batch ID: 48669
TestNo: SW8260 SW1311M
Analysis Date: 4/1/2021
SegNo: 3282211
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1,1-Dichloroethene
0.996 0.250
1.00 0 99.6
13.6
202
1.07 7.05
25
1,2-Dichloroethane
1.08 0.250
1.00 0 108
55.7
138
1.13 4.94
25
MEK
ND 5.00
5.00 0 94.1
65.3
118
0 0
25
Benzene
1.03 0.250
1.00 0 103
49.2
145
1.11 6.89
25
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area
response
MC
Value is below Minimum Compound
Original
ND
Not Detected
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
S
Spike Recovery outside accepted reco
Page 18 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48669
Sample ID: 21031753-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 125958
client ID: BatchQC
Batch ID: 48669
TestNo: SW8260 SW1311M
Analysis Date: 4/1/2021
SegNo: 3282211
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
1.02
0.250
1.00
0
102
26.7
156
1.07
5.19
25
Chlorobenzene
ND
2.50
1.00
0
97.0
33.7
159
0
0
25
Chloroform
0.944
0.250
1.00
0
94.4
48.5
145
1.00
5.89
25
Tetrachloroethene
0.823
0.250
1.00
0
82.3
19.2
191
0.856
3.87
25
Trichloroethene
0.937
0.250
1.00
0
93.7
38.4
167
1.03
9.28
25
Vinyl chloride
1.85
0.100
1.00
0
185
27.3
161
2.08
11.4
25 SQC+
Surr:4-Bromofluorobenzene
2500
2500
100
91.7
109
0
25
Surr: Dibromofluoromethane
2380
2500
95.1
75.5
118
0
25
Surr: Toluene-d8
2370
2500
94.9
94.1
105
0
25
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 19 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48678
Sample ID: MB-48678
SampType: MBLK
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/1/2021
RunNo: 125926
Client ID: PBS
Batch ID: 48678
TestNo: SW6010D SW3010A
Analysis Date: 4/1/2021
SegNo: 3281483
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.500
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.500
TCLP Selenium(Se)
ND
0.0500
TCLP Silver(Ag)
ND
0.500
Sample ID: LCS-48678
SampType: LCS
TestCode: Mtl-TCLP-7(6 Units: mg/L
Prep Date: 4/1/2021
RunNo: 125926
Client ID: LCSS
Batch ID: 48678
TestNo: SW6010D SW3010A
Analysis Date: 4/1/2021
SegNo: 3281484
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.87
0.500
2.000
0
93.5
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
103
80
120
TCLP Cadmium(Cd)
1.99
0.100
2.000
0
99.4
80
120
TCLP Chromium(Cr)
2.09
0.200
2.000
0
104
80
120
TCLP Lead(Pb)
2.03
0.500
2.000
0
102
80
120
TCLP Selenium(Se)
1.99
0.0500
2.000
0
99.6
80
120
TCLP Silver(Ag)
2.08
0.500
2.000
0
104
80
120
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 20 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 21031812
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48680
Sample ID: 21031808-001ams
SampType: MS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/1/2021
RunNo: 125956
Client ID: Batch=
Batch ID: 48680
TestNo: SW8081 SW3510C
Analysis Date: 4/1/2021
SegNo: 3282223
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
0.0184
0.00250
0.0200
0
92.1
70
130
Endrin
0.0100
0.000500
0.0100
0
100
10
224
gamma-BHC
0.00905
0.000500
0.0100
0
90.5
10
192
Heptachlor
0.00991
0.000500
0.0100
0
99.1
10
197
Heptachlor epoxide
0.00936
0.000500
0.0100
0
93.6
10
208
Methoxychlor
0.0104
0.000500
0.0100
0
104
10
251
Surr: TCMX
14.5
20.00
72.5
10
157
Surr: DCB
18.2
20.00
90.8
10
194
Sample ID: 21031808-001amsd
SampType: MSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/1/2021
RunNo: 125956
Client ID: Batch=
Batch ID: 48680
TestNo: SW8081 SW3510C
Analysis Date: 4/1/2021
SegNo: 3282224
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
0.0192
0.00250
0.0200
0
96.1
70
130
0.0184
4.28
30
Endrin
0.0105
0.000500
0.0100
0
105
10
224
0.0100
4.86
30
gamma-BHC
0.00945
0.000500
0.0100
0
94.5
10
192
0.00905
4.25
30
Heptachlor
0.0105
0.000500
0.0100
0
105
10
197
0.00991
5.43
30
Heptachlor epoxide
0.00976
0.000500
0.0100
0
97.6
10
208
0.00936
4.14
30
Methoxychlor
0.0126
0.000500
0.0100
0
126
10
251
0.0104
19.3
30
Surr: TCMX
15.8
20.00
79.1
10
157
0
Surr: DCB
19.8
20.00
98.8
10
194
0
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal)
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected P Second column confirmation exceeds PL Permit Limit Original
R RPD outside accepted recovery limits RL Reporting Detection Limit S Spike Recovery outside accepted reco
Page 21 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48680
Sample ID: LCS-48680
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/1/2021
RunNo: 125956
client ID: LCSS
Batch ID: 48680
TestNo: SW8081 SW3510C
Analysis Date: 4/1/2021
SegNo: 3282227
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
0.0195
0.00250
0.0200
0
97.3
70
130
Endrin
0.0104
0.000500
0.0100
0
104
10
130
gamma-BHC
0.00896
0.000500
0.0100
0
89.6
10
130
Heptachlor
0.0102
0.000500
0.0100
0
102
10
130
Heptachlor epoxide
0.00994
0.000500
0.0100
0
99.4
10
130
Methoxychlor
0.0107
0.000500
0.0100
0
107
10
178
Surr: TCMX
14.6
20.00
72.8
10
130
Surr: DCB
20.1
20.00
100
10
130
Sample ID: MB-48680
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/1/2021
RunNo: 125956
client ID: PBS
Batch ID: 48680
TestNo: SW8081 SW3510C
Analysis Date: 4/1/2021
SegNo: 3282228
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, tot
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor ep
Methoxychlor
Surr: TCMX
Surr: DCB
Qualifiers:
al ND 0.0
ND 0.0
ND 0.00
ND 0.00
ND 0.00
oxide ND 0.00
ND 0.00
14.4
19.4
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
0250
0500
0500
0500
0500
0500
0500
20.00 71.9 10
20.00 97.0 10
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
119
119
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 22 of 34
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
0250
0500
0500
0500
0500
0500
0500
20.00 71.9 10
20.00 97.0 10
E Value above quantitation range
M Manual Integration used to determine area response
P Second column confirmation exceeds
RL Reporting Detection Limit
119
119
H Holding times for preparation or anal)
MC Value is below Minimum Compound
PL Permit Limit
S Spike Recovery outside accepted reco
Original
Page 22 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48680
Sample ID: MB-48680
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 4/1/2021
RunNo: 125956
client ID: PBS
Batch ID: 48680
TestNo: SW8081 SW3510C
Analysis Date: 4/1/2021
SegNo: 3282228
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 23 of 34

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INC
Cuyahoga Falls, Ohio 44223
WO#: 21031812
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
02 Apr-21
Client:
Synagro
Project:
Randleman WWTP
BatchID: 48700
TCLP Mercury ND 0.00200
TCLP Mercury 0.00394 0.00200 0.00400 0 98.5 80 120
TCLP Mercury 0.00434 0.00200 0.00400 0 108 75 125
Sample ID: 21031808-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/2/2021
RunNo: 125982
Client ID: Batch=
Batch ID: 48700
TestNo: SW7470A SW7470A
Analysis Date: 4/2/2021
SegNo: 3283301
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury 0.00427 0.00200
0.00400 0 107 75
125
0.00434 1.63 20
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal)
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 24 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: 48700
Sample ID: 21031808-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 4/2/2021
RunNo: 125982
client ID: BatchQC
Batch ID: 48700
TestNo: SW7470A SW7470A
Analysis Date: 4/2/2021
SegNo: 3283301
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 25 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: R125741
Sample ID: LCS-R125741
SampType: LCS
TestCode: pH_Oil(9045D Units: s.u.@18.1C
Prep Date:
RunNo: 125741
Client ID: LCSW
Batch ID: R125741
TestNo: SW9045D
Analysis Date: 3/29/2021
SegNo: 3274164
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH
7.1
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
7.0 0 101 90 110
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 26 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 21031812
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: R125741
Sample ID: LCS-R125741
SampType: LCS
TestCode: pH_NPW(450 Units: s.u.@18.3C
Prep Date:
RunNo: 125741
Client ID: LCSW
Batch ID: R125741
TestNo: SW9045D
Analysis Date: 3/29/2021
SegNo: 3274154
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 21031858-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@18.8C
Prep Date:
RunNo: 125741
Client ID: Batch=
Batch ID: R125741
TestNo: SW9045D
Analysis Date: 3/29/2021
SegNo: 3274156
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
pH 9.1 9.1 0 5 H
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 27 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: R125903
Sample ID: LCS-R125903
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 125903
Client ID: LCSS
Batch ID: R125903
TestNo: SW1030
Analysis Date: 4/1/2021
SegNo: 3279874
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
7.59
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
7.240 0 105 70 130
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 28 of 34

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INC
Cuyahoga Falls, Ohio 44223
WO#: 21031812
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
02 Apr-21
Client:
Synagro
Project:
Randleman WWTP
BatchID: R125931
Sulfide, Reactive ND 25.0
Sulfide, Reactive 2090 25.0 2310 0 90.5 85 115
Sulfide, Reactive 2160 25.0 2310 0 93.5 80 120
Sample ID: 21031808-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 125931
Client ID: Batch=
Batch ID: R125931
TestNo: SW9034
Analysis Date: 3/31/2021
SegNo: 3281170
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
2270 25.0
2310 0 98.3 80
120
2160 4.97 30
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 29 of 34

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL rECHN❑ Lggir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://`h,-"-m,.settek.com
QC SUMMARY REPORT
WO#: 21031812
02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: R125931
Sample ID: 21031808-001AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 125931
client ID: BatchQC
Batch ID: R125931
TestNo: SW9034
Analysis Date: 3/31/2021
SegNo: 3281170
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 30 of 34

SUMM'T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL rECHN❑ LQgir,-3, INC
Cuyahoga Falls, Ohio 44223
WO#: 21031812
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
02 Apr-21
Client:
Synagro
Project:
Randleman WWTP
BatchID: R125937
Cyanide, Reactive ND 0.490
Cyanide, Reactive 9.53 0.485 10.00 0 95.3 85 115
Cyanide, Reactive 0.527 0.490 0.5000 0 105 65 135
Sample ID: 21031808-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 125937
Client ID: Batch=
Batch ID: R125937
TestNo: SW9014
Analysis Date: 3/31/2021
SegNo: 3281296
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
8.80 0.485
10.00 0 88.0 75
125
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal)
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
ND
Not Detected
P Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL Reporting Detection Limit
S
Spike Recovery outside accepted reco
Original
Page 31 of 34

MM'T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL rECHN❑ LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 21031812
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 02 Apr-21
Client: Synagro
Project: Randleman WWTP BatchID: R125937
Sample ID: 21031808-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 125937
Client ID: Batch=
Batch ID: R125937
TestNo: SW9014
Analysis Date: 3/31/2021
SegNo: 3281296
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 21031808-001AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 125937
Client ID: Batch=
Batch ID: R125937
TestNo: SW9014
Analysis Date: 3/31/2021
SegNo: 3281297
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive 8.67 0.481 10.00 0 86.7 75 125 8.795 1.39 10
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
R RPD outside accepted recovery limits
E Value above quantitation range H Holding times for preparation or anal)
M Manual Integration used to determine area response MC Value is below Minimum Compound
P Second column confirmation exceeds PL Permit Limit
RL Reporting Detection Limit S Spike Recovery outside accepted reco
Original
Page 32 of 34

4i
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E
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0)
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LL
Page 33 of 34

�� � � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIRONMENTALTECHNOLOGiES.lftC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafyacal Laboralnrias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.com
Client Name: SYN-NC-27028 Work Order Number: 21031812 RcptNo: 1
Logged by: Jacqueline Rasile
Completed By: Jacqueline Rasile
Reviewed By: Jennifer Woolf
3/26/2021 4:00:00 PM
3/28/2021 12:06:49 PM
3/29/2021 1:40:05 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition? Yes d❑ No ❑
Custody seals intact on shipping container/cooler? Yes ❑ No ❑ Not Present V
No. Seal Date: Signed By:
5. Was an attempt made to cool the samples? Yes ❑d No ❑ NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C Yes ❑d No ❑ NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No ❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No ❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No ❑
10. Was preservative added to bottles?
Yes
❑
No ❑d NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No ❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No ❑d
13. Does paperwork match bottle labels?
Yes
No ❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑d
No ❑
15. Is it clear what analyses were requested?
Yes
❑d
No ❑
16. Were all holding times able to be met?
Yes
No ❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No ❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
10.6
Goodl
Not Present
Page 34 of 34

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Randleman WWTP WQ Permit Number: WQ 0004825
WWTP Name: Town of Randleman WWTP NPDES Number: NC 0025445
Monitoring Period: From 01/01/2023 To 12/31/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. 1/A (time/temp) Alt. 2B (Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma. Ray Pasteurization
Class B:
Alt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens X
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization X Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Tr -11-.... 1- a..-11------ — ......t..........1 !!'l— A ..« I,]— R\ +i.n fnn,..la..R ennui♦nl inn A.+. -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 6'i'
MPN
MPN/g
Coliform
power per gram
of total solids
CFU/g
CFU
1000 MPN per gram of
MPN/g
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliform)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
0 tion/Alt. 1
Option/Alt.2
Option/Alt. 3 Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) (Spec. 02 pptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt. 8
(I4-DayAerobic)
(Alk Stabilization) X
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Michael Glass Plant Superintendent
Preparer Name and Title ( type or print)
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

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SECTION 6

Agricultural Lime Application Log
Year: 2023
Project: Randleman
Field
(state -county -site -field code)
Soil PHIII
Lime Requirement
(from soil analysis)
Tons/Acre
Applied
Date Applied
RD-18-3
7.6
0.0 tons/ac.
0.00
RD-48-1
5.8
0.0 tons/ac.
0.0

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services Report No. FY24-SL018911
k5i I"14'4+;4,
Client: Howard Fields
Advisor: Ryan Copeland
Predictive
1701 Lynwood Dr
SYNAGRO
°± f'
Greensboro, NC 27406
284 Boger Road
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County : Randolph
_
Soil Testing Section
Sampled: Received: 11/22/2023 Completed: 01/24/2024 Farm: RD-18
Client ID: 435019
Advisor ID: 499503
Sample ID: RD183
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O Mg S Mn Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 0
10 0 0 pH$ 0
0 0
Note: 12 Note: $
2 - Fescue/OGrass/Tim, M 0.0 120-200 0
10 0 0 pH$ 0
0 0
Note: 12 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.18 1.09 25.2 100 0.0 7.6 169 76 89 10
61 974 577 577 365 365
341 0.1 0
North Carolina
Tcbwiv Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services
Report No. FY24-SL018911
Howard Fields
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Ac
exchangeable acidity
Lime
B
boron
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
BS%
% CEC occupied by basic
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 to 75 Ib/1000 sq ft)
Ca%
% CEC occupied by calcium
at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If Mg is recommended and lime is needed, use dolomitic lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Each nutrient recommendation for field crops or other large areas are listed separately in units of lb/acre unless
K-1
potassium index
otherwise specified. Recommendations for N (and sometimes for B) are based on research/field studies for the crop
K20
potash
being grown, not on soil test results. Recommendations for K and P will depend on K-1 and P-1 soil test results and the
Mg%
% CEC occupied by magnesium
crop to be grown. Generally, at K-1 and P-1 values > 50, recommendations will be minimal. If Mg is needed and no lime is
MIN
mineral soil class
recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb/acre alone or in a fertilizer blend will usually
Mn
manganese
satisfy crop needs. Soluble salt levels (SS-1) appear only on reports for diagnostic/problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report in the recommendation section, refer to NCDA&CS
M-0
mineral -organic soil class
$Note: Secondary Nutrients and Micronutrients. Various NCDA&CS crop notes also address lime and fertilizer needs.
N
nitrogen
Na
sodium
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
NO3-N
nitrate nitrogen
the exact fertilizer grade recommended on the report, visit NCDA&CS Fertilizer Substitutions to find information that may
ORG
pH pH
organic soil class
current soil pH
help you choose a comparable alternate. For more information, read NCSU publication,
phosphorus index
A Homeowner's Guide to Fertilizer. In general, homeowners do not need to be concerned about micronutrients.
P-1
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven parameters [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity.
Zn-AI
zinc availability index
The remaining 16 parameters [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I,
NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit NCDA&CS
Understand Your Report for more information.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services Report No. FY24-SL018910
k5i I"14'4+;4,
Client:
Wesley Dobbins
Advisor: Ryan Copeland
Predictive
2246 Banner Whitehead Rd
SYNAGRO
°± f'
Sophia, NC 27350
284 Boger Road
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County : Randolph
_
Soil Testing Section
Sampled: Received: 11/22/2023 Completed: 01/24/2024 Farm: RD-48
Client ID:
475349
Advisor ID: 499503
Sample ID: RD481
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S Mn Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.3 120-200 100
10
0 0 0 0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 100
10
0 0 0 0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class: Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2 Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.41 0.96 7.4 82 1.3 5.8 16 70 56 21
59 710
443 443 99 99
106 0.0
North Carolina
Tcbwim Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/Divisions/Agronomic-Services
Report No. FY24-SL018910
Wesley Dobbins
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Ac
exchangeable acidity
Lime
B
boron
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
BS%
% CEC occupied by basic
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 to 75 Ib/1000 sq ft)
Ca%
% CEC occupied by calcium
at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If Mg is recommended and lime is needed, use dolomitic lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Each nutrient recommendation for field crops or other large areas are listed separately in units of lb/acre unless
K-1
potassium index
otherwise specified. Recommendations for N (and sometimes for B) are based on research/field studies for the crop
K20
potash
being grown, not on soil test results. Recommendations for K and P will depend on K-1 and P-1 soil test results and the
Mg%
% CEC occupied by magnesium
crop to be grown. Generally, at K-1 and P-1 values > 50, recommendations will be minimal. If Mg is needed and no lime is
MIN
mineral soil class
recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb/acre alone or in a fertilizer blend will usually
Mn
manganese
satisfy crop needs. Soluble salt levels (SS-1) appear only on reports for diagnostic/problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-I
manganese index
notations appear on the soil report in the recommendation section, refer to NCDA&CS
M-0
mineral -organic soil class
$Note: Secondary Nutrients and Micronutrients. Various NCDA&CS crop notes also address lime and fertilizer needs.
N
nitrogen
Na
sodium
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
NO3-N
nitrate nitrogen
the exact fertilizer grade recommended on the report, visit NCDA&CS Fertilizer Substitutions to find information that may
ORG
pH pH
organic soil class
current soil pH
help you choose a comparable alternate. For more information, read NCSU publication,
phosphorus index
A Homeowner's Guide to Fertilizer. In general, homeowners do not need to be concerned about micronutrients.
P-1
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven parameters [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity.
Zn-AI
zinc availability index
The remaining 16 parameters [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I,
NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit NCDA&CS
Understand Your Report for more information.