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HomeMy WebLinkAboutWQ0001684_2023 Residual Annual Report_20240229 (2)Initial Review Reviewer nathaniel.thorn burg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2023 Permit Number (IR) * WQ0001684 Applicant/Permittee City of Asheboro Email Notifications Does this need review by the hydrogeologist? * Yes U No Regional Office Winston-Salem CO Reviewer Admin Reviewer Wanda Gerald Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Brent Collins Email Address* brent.collins@emaresourcesinc.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 3363993646 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0001684 Has Current Existing permit number Applicant/Permittee Address* PO Box 1106, Asheboro, NC 27204 Facility Name* City of Asheboro Class B Residuals Program Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2023 Asheboro Annual Report - WQ0001684.pdf 12.1 MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/29/2024 It MI. � A, sources, Inc. February 27, 2024 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2023 Annual Report - Asheboro Treatment and Land Application of Residuals Permit No. WQ0001684 Dear Sir or Madam: Enclosed is the 2023 Annual Report for the above referenced land application permit. During 2023 EMA Resources, Inc. land applied 1181.36 dry tons of wastewater residuals to 235.4 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, Z_�Z4;2�_ Brent Collins Director of Technical Services brent.collins(a,emaresourcesinc.com Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 City of Asheboro 2023 Annual Report Residuals Land Application Permit No. WQ0001684 Prepared By: EMA Resources, Inc. Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0001684 County: Randolph Year: 2023 Facility Name (as shown on permit): City of Asheboro Land Application Operator: EMA Resources Inc. Phone: 336-754-1441 Land application of residuals as allowed by the permit occurred during the past calendar year? 23 Yes [.-I No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Total 54 Total number of fields utilized for land application during the year: 18 Total amount of dry tons applied during the year for all application sites: 1181.36 Total number of acres utilizes for land application during the year: 235A Part B - Annual C2MRjanELStatement: Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 621 Yes No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. I ) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached, 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T.] 105(a) or the Pollutant Loading Rates in 15A NCAC 02T.1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T.1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals, Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." .............. . W� ............ Mh 02/26/24 Michael R. Wiseman - Plant Manager 11,,�Hki� Niscinml 01 d'i 1116-�Wl 11,1:� 11) Permittee Name and Title (type or print) Signature of Permittee Date 1/18/2024 Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part. 503.9 (r) and 15A NCAC 02T.1 102 (26) DENR FORM ACF (12/2006) R 2 ct I M— a a R I 9 W 9z I I ct ct k() 00 C` kr) kr) CD kr) kr) to kr) rn Rr) r—i kr) rn r,� C� rn CD 00 kr) kr)r. It kr) kr) rn �t bli bbas—D Qj 14 bli Cd 0 0 " Qj h4 I I C73 QJ CJ I V� * CD C) N ev LL U) U) 0 LL or_ z Lli 0 a I M I a a I I I 2 I CC — — — — — — — — — — — — — — CC 4-4 4j 4j 00 CA 44 u rn 00 kr) 00 00ci bli bfj ct cd bfi 7� 0 PIA cd zi I ■ ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP WQ0001684 Carl Sardi Owner: 23.2 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Carl Sardi Predominant Soil Series: 23.2 Site #: GUO15 Field #: 126.63 EnB 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total D 000000000111H Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11• .. • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 .. • 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11� • 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 •• �1, M� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 ® :. • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 : � • Total ' • •: 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 •: 11 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) o C�7 4t 4t w OC OC � M o N H 0 0 w U O U SE U CZ H O ¢ N O O .-i Uby ..U. O O O N Pr N N N a FC15 N O O O O O O O O O O 0 O 0 U O O O O O O O O O O O p o o N 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 � • • y`�y y Y o0 00 00 a Z Z w r N Ammonia o 0 o Nitrogen E ° N � N a a Y O o O 0 O o O n N C o M D1 Mineralization ry ry ry O N Rate*** o 0 o fr, ry M ti Volatilization C00 1�0 o Rate** o 0 o a O N M a (n Application o 0 Method* o 0 0 0 V V V o a o N N ti 00 � DD � U Q�� •O r O N N u •¢y � � QI QI QI 71 M N � M Q � M N N ,N o W � i o 0 0 "� oo, 4 Q w a U o 0 0 � U U Q Q U w � L- 00 0 0 0 0 0 0 0 0 0 0 'E� ,U, U O ^C$ 00 00 00 `n U a o O �p z UCO N dF N rn -� I t o n u111OW o . zo a112Q o I O Q a 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP Total Dry Tons Applied (Annual): WQ0001684 Cation Exchange Capacity (non 503 only): Steve Fields Owner: Rocking F. Farm Predominant Soil Series: 8.5 Acres Permitted: 8.5 Site #: GUO16 Field #: 20.82 CrB 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11' ': 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ': 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 ' 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 ' • 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1• 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 06 06 O i-i U CZ H O ¢ N O U by O �+ cs N a Q O o O 0 O 0 O 0 O o O O O o O 0 O 0 O 0 O 0 O 0 O 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Z -; a 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0; 0 ri 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 140. Z Z E V r M Ammonia O M Nitrogen E rc-" 00 a a 00 Mineralization ry O oO oO Rate*** � o 0 ti Volatilization Rate** O r. o 0 0 a k, (n Application o 0 0 Method* o 0 0 r ti ti a N Z o 0 0 � U U Qy Q U w D1 0 0 0 0 0 0 0 0 0 0 0 0 M M �O U OCn O 'CS 00 `n U a o z (DCn N a u111OW .10 3112Q o C) Q a 0 0 N N W U- 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Asheboro WWTP WQ0001684 Operator: Ryan Hiatt Owner: Acres Used: 16.29 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): EMH Farms LLC Predominant Soil Series: 16.29 Site #: GU28 Field #: 138.64 EnB 2A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • ' •: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � •: 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 11: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11: • • 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 1�� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.. ®� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O N N � :m :m w OC OC o OC O M E� 0 0 IZ U CZ H O ¢ N O O .—i Uby ..U. O O cs N a Q Q O O O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O O O O O O O O O O O O U O O O O O O O O O O O O - N o 0 0 0 0 0 0 0 0 0 0 Z kn M 'CS .y •�i• y � a1 a1 a Z Z --i w � Ammonia Y M M Nitrogen E a O O O E Mineralization ry ry O Rate*** o o 0 0 0 ti Volatilization O Rate** O O r r.� o o o w (n Application o 0 0 Method* O o o 0 0 aN r a _ V V 0 o N ° o ti 0 ti G a (s 00 �C00 00 Z o 0 0 � U U Qy Q c 00 N 0 0 0 0 0 0 0 0 0 0 0 Cn N M O 0 0 N 0 N 5 o `n U a o v o O OC 11111O M ' O zo 31ra ° o F �4 PL, U PL, P I C) Q a 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Asheboro WWTP WQ0001684 Operator: Ryan Hiatt Owner: Acres Used: 7.06 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): EMH Farms LLC Predominant Soil Series: 7.06 Site #: GU28 Field #: 59.42 EnB 2B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D - Event •. �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • ' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11: • • 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1�� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.. ®® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total '• 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O OC cv :M :M E� 0 0 IZ CZ H O ¢ N O O U by O O cs N a Q Q O O O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O O O O O O O O O O O O U O O O O O O O O O O O O In 00 � o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0�0 D1 kn Z Z E w � Ammonia Nitrogen E a O O O E Mineralization ry ry O Rate*** o o 0 0 0 ti Volatilization O Rate** O O r. O o o w (n Application o 0 0 Method* O o O o Vl ti ti .u, Z o 0 0 � U O 0 0 0 0 o O m v o (D N C w Lo CO M iti ~•,S- QI ^ vCn zO a112Q o I C) Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Asheboro WWTP WQ0001684 Operator: Ryan Hiatt Owner: Acres Used: 12.54 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): EMH Farms LLC Predominant Soil Series: 12.54 Site #: GU28 Field #: 80.93 EnB 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • ® ' •11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • •11 Total ' • •� 1 1 111 1 111 1111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 •� 1 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) Lr' N OC CIA c :M :M H 0 0 w O IZ U CZ H O ¢ N O O .-i Uby ..U. O �+ N O O O O O O O O O O O O O 0 ICD U O O O O O O O O O O O O 0 0 0 0 0 0 0 0 M N Qr V' O O O O O O O O O O O O V' U M 0 0 0 0 0 0 0 0 0 0 0 0 � .--I 'CS � •' «S Y ^ W Z Z E wN Ammonia Y oo o o Nitrogen E a a O Cn E Mineralization O o 0 Rate***o o Z 0 0 ti Volatilization Rate** O r r w (n Application o o Method* O o O o aN QI CC CC Z o 0 � U U Qy Q U w � O O O O O O O O O O O O D1 D1 O `n U a o v o ( a o P� o LO O N U gjuOw o zo a1�Q o U I C) 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Asheboro WWTP WQ0001684 Operator: Ryan Hiatt Owner: Acres Used: 9.94 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): EMH Farms LLC Predominant Soil Series: 9.94 Site #: GU28 Field #: 72.62 EnB 4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1• 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ' 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � 1 1 •• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 •• 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • 1� 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1� 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • Total ' • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O OC N C�7 :M :M H 0 0 w IZ CZ H O ¢ N O O U by O N O O O O O O O O O O O O O 0 ICD U O O O O O O O O O O O O 0 014D kn a v o 0 0 0 0 0 0 0 0 0 0 0 v, M VMl y CC$ 'CS Y � • • E ^ W Z Z w M Ammonia Nitrogen E N N N a ~ O 00 fr, o 0 0 Mineralization ry O Rate*** � o 0 ti Volatilization M Rate** O r. o 0 0 a (n Application o 0 0 Method* O o O o N N _ l ti ti r- U d '� M W 00 CO M r , 00 M Z o 0 0 � U N Qy Q c O A4 O O O M O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 N D1 0 N N O o m v o ( N Cn a ujuOw zo 3112Q ° o I C) Q a 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Asheboro WWTP WQ0001684 Operator: Ryan Hiatt Owner: Acres Used: 16.17 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): EMH Farms LLC Predominant Soil Series: 16.17 Site #: GU28 Field #: 57.81 HhB 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1�� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.. 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1• • �1, M� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® ':� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �:� Total '• 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) OC cv H 0 0 w O Ln rl SE YC O Sr U U H O ¢ Cn N O �+ Tr U Z a N O O O O O O O O O O O O O U O O O O O O O O O O O O O Z a00o 0 0 0 0 0 0 0 0 0 0 0 00 0 0 0 0 0 0 0 0 0 0 0 0 0 �• c� T. 140. Z Z Ammonia Y oo 00 0 Nitrogen E ° N �, O � f, N a a Cn � E wo O O a Mineralization ry O Rate*** O Z o 0 ti Volatilization Rate** O r w Application (nCC o o Method* O o O o N N _ M M ti ti .u, r. p a N Z o 0 � U U Qy Q O o o O m v o ( N o a M U n a u111OW N zo 3112Q a v as o P� I C) Q a 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Asheboro WWTP WQ0001684 Operator: Ryan Hiatt Owner: Acres Used: 10.32 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): EMH Farms LLC Predominant Soil Series: 10.32 Site #: GU28 Field #: 72.62 EnB 6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total D EEMEMENN ININ Event1� 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1• 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ::� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 ::� 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 :1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 :1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • �1, M� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® ' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • Total ' •m 1 111 1 111 1111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �1 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O OC � cv C�7 :M :M E� 0 0 w IZ CZ H O ¢ N O O U by O N O O O O O O O O O O O O O 0 ICD U O O O O O O O O O O O O 0 0 0 0 0 0 o N a o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 M � Z Z w M Ammonia 00 M° Nitrogen E ^" a a O C C) CD 00 E fr, o 0 0 Mineralization ry O M M Rate*** o k" � Z o 0 ti Volatilization C M Rate** O r. o 0 0 a k, Application o 0 0 Method* O O O N 00 r P ry 4 ti 0 ti N Z o 0 0 � U N Qy Q O w l� 0 0 0 0 0 0 0 0 0 0 0 0 N M vi O `n U a o v o ( Cn u111OW o zo Q C) Q a 0 0 N N W U- 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP Total Dry Tons Applied (Annual): WQ0001684 Cation Exchange Capacity (non 503 only): Kimball Markham Owner: Markham Properties Predominant Soil Series: 15.1 Acres Permitted: 15.1 Site #: RD042 Field #: 82.76 BaB 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total D 0000000001111 Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11• ' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 11� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11� • • 1 •1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 •1 • 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' • •• 1111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 •• • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 4t 4t E� 0 0 w O P-i E O E SE ° CZ H O ¢ N ° O U by O O cs N a Q Q O O O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O O O O O O O O O O O O U O O O O O O O O O O O O ¢+ O ur O O O O O O O O O O O V' V a O 01 O O O O O O O O O O O N U00 O O O O O O O O O O O M � y � •• y Y o0 00 a Z Z w r N Ammonia 00°°O 00 o Nitrogen E a a a Mineralization ry ry O M Rate*** O O Z No 00 ti Volatilization Rate** O O a O w Application Method* o 0 0 p 00 M oo a V V Q o N 0 ti M Q � M CZ p p D1 M Z o 0 0 � U N Qy Q U O N N O 0 0 0 0 0 0 0 0 0 0 0 O z U N O CO N N PL, P I C) Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP Total Dry Tons Applied (Annual): WQ0001684 Cation Exchange Capacity (non 503 only): Kimball Markham Owner: Tony Jackson Predominant Soil Series: 8.6 Acres Permitted: 8.6 Site #: RD042 Field #: 34.03 BaB 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total D Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 . • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 � • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 � � 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 � 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1�� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1.. ®® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 06 06 O CZ H O ¢ N O O U by O O cs N a Q Q O O O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 o 0 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 0 0 p N o o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 Y •�i• y :�" y CU 00 00 a 'may Z Z �O r N Ammonia o o Nitrogen E rc-" rc-" ° N M °M° N a a v�i v�i w O O O a Mineralization ry ry O o Rate*** 0 0 Z o o ry M Volatilization O N °M° Rate** O O a O a w Application o Method* O o 0 0 0 0 a N a, v v o N ti N o Q 7� o VN Z o 0 0 � U O `n U a o z (D N a CO N O N CZ N a u111OW C) Q a 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP Total Dry Tons Applied (Annual): WQ0001684 Cation Exchange Capacity (non 503 only): Kimball Markham Owner: Markham Properties Predominant Soil Series: 7.1 Acres Permitted: 7.1 Site #: RD042 Field #: 14.58 BaB 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total D Event 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 •: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 •: �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 � � � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 � 1 1:1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1:1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ®� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' m 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111E -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 4t 4t w E� 0 0 w O E O E SE CZ H O ¢ N O O U by O cs N a Q O o O 0 O 0 O 0 O o O O O o O 0 O 0 O 0 O 0 O 0 O 0 O O O O O O O O U O O O O O O O O O O O O O Z - a 0 o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 00 y y Z Z E w Ammonia Y c o Nitrogen E a Cr Y O v' M 00 a Mineralization ry O o 0 Rate*** O o 0 0 ti Volatilization Rate** O a N o � � a w (n Application o Method* O o 0 0 0 0 P N a, o oq�8 Q U N� o o CC .Vi r U CY N Z 0 0 0 � U N Qy Q U O O O O O O O O O O O O O O O N N O ^c3 00 O �p z U N dF N v Cn Z a ujuOw zo a112(l o CC (3j H O Fr H W Sir � � O W •� o U W O w w o W 0-0 rr Z � H w s. CA O � U � � W o W C s. C o � w .� o w ^W c � x o • o s. W c O �W CA sy O C O W W 40 Ni y 6J W W O C o �., • o U C~C O I C) Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP WQ0001684 Gene Hiatt Owner: 9.25 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Gene Hiatt Predominant Soil Series: 9.25 Site #: RD43 Field #: 48.61 BtB2 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1• 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 �® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 . • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 . • 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ®' 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • 1 Total ' • 1 :� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 :� • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) 11 4t 4t H 0 0 w N C7 O .: I Le N C7 SE CZ H O ¢ N O O U by O N O O O O O O O O O O O O O 0 ICD U O O O O O O O O O O O O 0 0 0 0 0 0 l� a '• Q-i O N O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 � U 0 O O O O O O O O O O O O 0 00 � 'z Z E N o w M Ammonia Nitrogen E " a a O Q ry ry ob Mineralization ry O Rate*** o o 0 o M ti Volatilization C o Rate** O r. o o a k, (n Application o 0 0 Method* O O o O NN Q1 Q1 ti _ o � U Q� �° Q •o V o 0 ti Z o 0 0 � U N Qy Q N w O O O O O O O O O O O O vi N l� O O O O O O O O O O O N O 'CS � `n U a o z (D N 6 a ,� NCn Z a u111OW .10 3112Q C) Q a 0 0 N N W U- 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP WQ0001684 Gene Hiatt Owner: 16.2 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Gene Hiatt Predominant Soil Series: 16.2 Site #: RD43 Field #: 85.07 GbC 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total D 000000000111H Event 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1• 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 1 . • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 . • 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® • •• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • •• Total ' • 1 1: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1: • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O i-i CZ H O ¢ N O U by O N O O O O O O O O O O O O O 0 ICD 0 0 0 0 0 d ' - 00 o0 0 0 0 0 0 0 0 0 0 0 0 0 o0 0o Z N o0 � y y «S 'CS Y � • • Z Z N O w y M Ammonia oO Y o0 Nitrogen E a a O O VZ C/� M C) N N pb L^ E w O O O Mineralization ry O Rate*** O o 0 o M ti Volatilization C I'D � o Rate** O r. o o a k, (n Application C-) Method* O o 0 0 0 0 N N ti 0 0 ti Z o 0 0 � U N Qy Q O N O `n U a o z U N It a u111OW zo 3112(l M ° a U as a, I C) Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP WQ0001684 Gene Hiatt Owner: 6.51 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Gene Hiatt Predominant Soil Series: 6.51 Site #: RD43 Field #: 24.31 BtB2 3A Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 •1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 •1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 �1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 �1 • 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� ® 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 Total '• 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O i-i CZ H O ¢ N O U by O cs N a 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O o O O O O 00 0 0 N 0 0 0 0 0 0 0 0 0 0 0 0 00 DD y y 311 •❑• W W n••I �n �n •�" r O Ammonia N Nitrogen Ed) ~ N a a O O O O � 0 0 0 pip a Mineralization ry ry O N Rate*** 0 0 Z o 0 0 ti Volatilization Rate** 0 0 r. o 0 0 a k, Application o Method* O o 0 0 0 0 aN a i v v P o 0 o N ti � U Q� �° Q Q •° U o 0 0 ti � U a S :Z Z o 0 0 � U N Qy Q O `n U a o z U N v N Cn U Z zo 3112Q ° a v a, I C) Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP WQ0001684 Gene Hiatt Owner: 11.92 Acres Permitted: Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): Gene Hiatt Predominant Soil Series: 11.92 Site #: RD43 Field #: 43.75 BtC2 3b Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1� • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� • 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 . • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 � • 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • • 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1� 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 ®® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' • 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 11 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Z'�e 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O i-i U CZ H O ¢ N U O .-i Uby ..U. O �+ N O O O O O O O O O O O O O 0 ICD 0 0 0 0 0 0 0 0 0 N0 a 0 0 0 0 0 0 0 0 0 0 0 0 o r U o 0 0 0 0 0 0 0 000 0 0 0 •' Y w Z Z E w N Ammonia Y Nitrogen E ° N 'n c�i 0 N a a 00 E w O O O a Mineralization ry C) N o Rate*** O 0 0 o M ti Volatilization C C" o Rate** O r. o 0 0 a k, U) Application CC o 0 0 Method* O o 0 0 aN ti V N 00 o 0 0 ti r. U d U r` 0 0 0 � U U Q Q U w O O O O O O O O O O O O O lC � O 0 O 0 O 0 O 0 O 0 O 0 CD 0 CD 0 CD 0 C) 0 C) 0 C)N 0� C 0 0 CD 0 m O ^c3 00 `n U C a o Cn z (D N a ujuOw M C) Q a 0 0 N N W U- 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Asheboro WWTP Total Dry Tons Applied (Annual): 36.46 Permit #: Operator: Acres Used: WQ0001684 Cation Exchange Capacity (non 503 only): Doug Hensley Owner: Doug Hensley Predominant Soil Series: ApB 13.5 Acres Permitted: 13.5 Site #: RD46 Field #: I Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total• D - Event 1 1 1� • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� • 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 . • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 � • 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 •1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 •1 • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • Total ' •m 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 •: • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O 11 4t 4t Sr i/ SE Yy-1 N U w U CZ H O ¢ N O O .-i Uby ..U. O O N O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 Z O O O O O O O O O O O O U O O O O O O O O O O O O Z -00 o 0 0 0 0 0 0 0 0 0 0 0 1 �n 0 ... 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 o0 � y y � Y � •' ^ E N W Z .Z 40. r Ammonia M Nitrogen E N o N a a a E a Mineralization Rate*** O o 0 0 ti Volatilization O o Rate** O a o M o O a w Application o 0 Method* O o 0 0 0 a 00 N O a O C V ti O Q M OO ti .u, U � DD V1 M Z o 0 0 � U U w O O O O O O O O O O O O D1 N r- 0 N D1 O o C15 `i' U O a o z U U gjuOw U .10 3112Q M ° I U Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Asheboro WWTP Total Dry Tons Applied (Annual): WQ0001684 Cation Exchange Capacity (non 503 only): Doug Hensley Owner: Doug Hensley Predominant Soil Series: 43.2 Acres Permitted: 43.2 Site #: RD46 Field #: 182.30 HeB 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 �: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 �: 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 • • 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • • �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ®� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' •m 1 111 1 111 1111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1� • "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1/19/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) O Yy-1 CZ H O ¢ N O O U by O O O N Pr N O O O O O O O O O O 0 O 0 0 0 0 0 0 0kn 0 0 0 Q.� N O O O O O O O O O O O O D1 O O O O O O O O O O � U M O O O O O O O O O O 0 � � y y «S 'CS Y G1 G1 G1 • • N N N wN r Ammonia o 0 o o Nitrogen E " a a Mineralization ry ry ry O o o Rate*** o 0 0 o 0 0 ti VolatilizationO Rate** o 0 o a O M o 0 a k, (n Application o 0 Method* O o 0 0 0 a V V V ti ti o � BBB � N 00 V) Z o 0 0 � U N Qy Q _ i0-i c 00 l- 7 O ^C$ V1 V1 V1 `i' U CZ a o O �p z U ;R N * N NCO U a a (O O N a u111OW JO alp.Q � F PLI U PL P I C) Q a 0 0 N N LL U) LL 2 O LL z W 0 mil , 1 /13/2023 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 23-005-0052 Client Project Description: Asheboro, NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 1/5/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Way to PM� WRTIA"Wi tMain 901.213.2400 0 Fax u f, www.waypointanalyticaLcom Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00001/23-005-0052 Page 2 of 8 Way lht,(2) PM�TICAL' Sample Summary Table Report Number: 23-005-0052 Client Project Description: Asheboro, NC Lab No Client Sample zo Matrix Date Collected Date Received 89029 Asheboro Solids 01/04K202311:10 01/05/2023 Page 3 of 8 to Way� PA ► x Client: EMA Resources Inc Project: Asheboro, NC Lab Report Number: 23-005-0052 Date: 1 /13/2023 Main 901.213.2400 .41 wwwmaypointanalyticaLcorn CASE NARRATIVE Metals Analysis Method 601 OD Sample 96858 (Miller Pressed Sludge Cake) Analyte: Aluminum QC Batch No: 1-657436/1-657148 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 96858 (Miller Pressed Sludge Cake) Analyte: Potassium QC Batch No: 1-657436/1-657148 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 Way to PM� 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Project Asheboro, NC Information : Report Date : 01/13/2023 Received �.�101/05/2023 - Connie Cook Report Number : 23-005-0052 REPORT OFANALYSIS Project Manager Lab No : 89629 Matrix: Solids Sample ID : Asheboro Sampled: 1/4/2023 11:10 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 81.5 % 1 01/05/23 16:03 FMM SW-DRYWT Ammonia Nitrogen 6430 mg/Kg - dry 86.5 541 1 01/13/23 12:00 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <22.9 mg/Kg - dry 22.9 22.9 1 01/09/23 14:22 ZBD 4500NO3F-2016 Organic N 36270 mg/Kg - dry 86.49 540.5 1 01/12/23 13:00 CALCULATION pH 7.8 S.U. 1 01/11/2310:00 SAR 9045D Total Solids 18.5 % 0.010 0.010 1 01/05/23 16:03 FMM 2540G-2011 Total Volatile Solids 58.5 % 0.010 0.010 1 01/05/23 16:03 FMM 2540G-2011 Total Kjeldahl Nitrogen 42700 mg/Kg - dry 54.1 1350 1 01/12/23 13:00 JPJ ;M-4500-NH3C-TKl` Phosphorus 29100 mg/Kg - dry 14.9 27.0 1 01/07/23 00:51 JTR 6010D Aluminum 57800 mg/Kg - dry 250 270 10 01/09/23 16:23 TJS 6010D Arsenic 9.08 mg/Kg - dry 1.30 2.70 1 01/07/23 00:51 JTR 6010D Cadmium 0.908 mg/Kg - dry 0.108 0.541 1 01/07/23 00:51 JTR 6010D Calcium 17700 mg/Kg - dry 209 270 1 01/07/23 00:51 JTR 6010D Chromium 88.6 mg/Kg - dry 1.28 1.35 1 01/07/23 00:51 JTR 6010D Copper 335 mg/Kg - dry 1.68 2.70 1 01/07/23 00:51 JTR 6010D Iron 25200 mg/Kg - dry 46.1 54.1 1 01/07/23 00:51 JTR 6010D Lead 23.7 mg/Kg - dry 0.972 1.62 1 01/07/23 00:51 JTR 6010D Magnesium 2990 mg/Kg - dry 13.9 27.0 1 01/07/23 00:51 JTR 6010D Manganese 6490 mg/Kg - dry 17.6 27.0 10 01/09/23 16:23 TJS 6010D Mercury 0.5733 mg/Kg - dry 0.0349 0.800 1 01/11/23 13:22 JTR 7471A Molybdenum 35.1 mg/Kg - dry 0.729 1.35 1 01/07/23 00:51 JTR 6010D Nickel 19.1 mg/Kg - dry 0.648 1.35 1 01/07/23 00:51 JTR 6010D Potassium 2040 mg/Kg - dry 33.4 54.1 1 01/07/23 00:51 JTR 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Page 5 of 8 0 Waypoeint2790 "k�u'hitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypoiintanalyticaLcom 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 01/13/2023 755 Yadkinville Rd Information : Received : 01/05/2023 Mocksville , NC 27028 Connie Cook Report Number : 23-005-0052 REPORT OFANALYSIS Project Manager Lab No : 89629 Matrix: Solids Sample ID : Asheboro Sampled: 1/4/2023 11:10 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium 2.92 mg/Kg - dry 1.73 2.70 1 01/07/23 00:51 JTR 6010D Sodium 1290 mg/Kg - dry 70.3 135 1 01/07/23 00:51 JTR 6010D Zinc 914 mg/Kg - dry 4.38 6.76 1 01/07/23 00:51 JTR 6010D Sulfur 11500 mg/Kg - dry 28.0 54.1 1 01/07/23 00:51 JTR 6010D Sodium Absorption Ratio 1.01 Ratio 0.01 0.01 1 01/07/23 00:51 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 6 of 8 l0 Waypoint", J123.8224 Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 23-005-0052 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: T136 Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IMakayla Weaver Date & Time: 01/05/2023 10:02:25 Page 7 of 8 4 I m t rm .0 c CL N (L 0) E E .,E CA, m 0 qll 0 d 0 0 N m m' x Z Z X x = CL 2 o 0 0 C'n nua ax, 0 T. .3 z z Mon "M mom mmom mmm mm mom mm CL A s 300 Ll E d) E SAi CA E E E d H E SPHOS lelOi .... . .. .... ...... . . I'D �,g N,)RAebJ018leJPN �T;7, M 0 1!51 a E E 8luOUJLUV/NNJL 0 C rX w I'm u q, L 2? apsodum()) Aug qej(r)� '*N 2 CO Ou 0 �N 2 u E < t sAaupjuo)jojaqupnN I — 0 S 7-� "I cw� -?r 57 cr U7, 7�) "D Z T Z azu 0 E u 8 Paqe 8 of 8 mil , 4/14/2023 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 23-096-0017 Client Project Description: Asheboro, NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 4/6/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Way to PM� WRTIA"Wi tMain 901.213.2400 0 Fax u f, www.waypointanalyticaLcom Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/29/2024 Arkansas State Program 88-0650 02/07/2024 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 11/14/2025 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 11/14/2025 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2024 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00001/23-096-0017 Page 2 of 8 Way lht,(2) PM�TICAL' Sample Summary Table Report Number: 23-096-0017 Client Project Description: Asheboro, NC Lab No Client Sample ID Matrix Date Collected Date Received 93341 Asheboro Solids 04/05/2023 10:55 04/06/2023 Page 3 of 8 to Way� PA ► x Client: EMA Resources Inc Project: Asheboro, NC Lab Report Number: 23-096-0017 Date: 4/13/2023 Main 901.213.2400 .41 wwwmaypointanalyticaLcorn CASE NARRATIVE Metals Analysis Method 601 OD Sample 93829 (#2) Analyte: Aluminum QC Batch No: 1-675666/1-674801 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 93829 (#2) Analyte: Calcium QC Batch No: 1-675666/1-674801 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Sample 93829 (#2) Analyte: Iron QC Batch No: 1-675666/1-674801 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 93829 (#2) Analyte: Potassium QC Batch No: 1-675666/1-674801 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 93829 (#2) Analyte: Magnesium QC Batch No: 1-675666/1-674801 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 93829 (#2) Analyte: Sulfur QC Batch No: 1-675666/1-674801 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 93833 (San Elijo) Analyte: Mercury QC Batch No: 1-675254/1-674948 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 Way to PM� 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Project Asheboro, NC Information : Report Date : 04/14/2023 Received �.���y04/06/2023 - Connie Cook Report Number : 23-096-0017 REPORT OFANALYSIS Project Manager Lab No : 93341 Matrix: Solids Sample ID : Asheboro Sampled: 4/5/2023 10:55 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 82.9 % 1 04/12/2315:19 JLS SW-DRYWT Ammonia Nitrogen 7370 mg/Kg - dry 93.6 585 1 04/13/23 13:30 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <5.85 mg/Kg - dry 5.85 29.2 1 04/11/23 12:57 ZBD 4500NO3F-2016 Organic N 46670 mg/Kg - dry 93.57 584.8 1 04/13/23 08:00 CALCULATION pH 8.1 S.U. 1 04/11/2311:25 HBT 9045D Total Solids 14.8 % 0.010 0.010 1 04/12/23 14:55 JLS 2540G-2011 Total Volatile Solids 61.7 % 0.010 0.010 1 04/12/23 14:55 JLS 2540G-2011 Total Kjeldahl Nitrogen 54000 mg/Kg - dry 58.5 1460 1 04/13/23 08:00 JPJ ;M-4500-NH3C-TKl` Phosphorus 27300 mg/Kg - dry 16.1 29.2 1 04/11/23 04:57 JTR 6010D Aluminum 47000 mg/Kg - dry 27.0 29.2 1 04/11/23 23:32 JTR 6010D Arsenic 6.67 mg/Kg - dry 1.40 2.92 1 04/11/23 23:32 JTR 6010D Cadmium 0.836 mg/Kg - dry 0.117 0.585 1 04/11/23 23:32 JTR 6010D Calcium 14400 mg/Kg - dry 226 292 1 04/11/23 23:32 JTR 6010D Chromium 62.6 mg/Kg - dry 1.38 1.46 1 04/11/23 23:32 JTR 6010D Copper 316 mg/Kg - dry 1.81 2.92 1 04/11/23 04:57 JTR 6010D Iron 20900 mg/Kg - dry 49.8 58.5 1 04/11/23 04:57 JTR 6010D Lead 25.4 mg/Kg - dry 1.05 1.75 1 04/11/23 23:32 JTR 6010D Magnesium 2980 mg/Kg - dry 15.1 29.2 1 04/11/23 04:57 JTR 6010D Manganese 9120 mg/Kg - dry 19.0 29.2 10 04/11/23 23:27 JTR 6010D Mercury 0.3713 mg/Kg - dry 0.125 1.04 1 04/10/23 14:16 FDS 7471A Molybdenum 53.8 mg/Kg - dry 0.789 1.46 1 04/11/23 04:57 JTR 6010D Nickel 19.5 mg/Kg - dry 0.701 1.46 1 04/11/23 04:57 JTR 6010D Potassium 2220 mg/Kg - dry 36.1 58.5 1 04/11/23 04:57 JTR 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Page 5 of 8 0 Waypoeint2790 "k�u'hitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypoiintanalyticaLcom 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 04/14/2023 755 Yadkinville Rd Information : Received : 04/06/2023 Mocksville , NC 27028 Connie Cook Report Number : 23-096-0017 REPORT OFANALYSIS Project Manager Lab No : 93341 Matrix: Solids Sample ID : Asheboro Sampled: 4/5/2023 10:55 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium 5.51 mg/Kg - dry 1.87 2.92 1 04/11/23 23:32 JTR 6010D Sodium 1350 mg/Kg - dry 76.0 146 1 04/11/23 23:32 JTR 6010D Zinc 778 mg/Kg - dry 4.74 7.31 1 04/11/23 23:32 JTR 6010D Sulfur 11500 mg/Kg - dry 30.3 58.5 1 04/11/23 23:32 JTR 6010D Sodium Absorption Ratio 1.10 Ratio 0.01 0.01 1 04/11/23 04:57 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 6 of 8 l0 Waypoint", J123.8224 Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 23-096-0017 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: T135 Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: lEmily M. Peterson Date & Time: 04/06/2023 09:31:33 Page 7 of 8 a• �m ee o a25. s 4a imam a-� �w wrrMrrrrrr � � ,,. a wL t y db k a *. ........ u' N EJ Sp!los Ieloi f y rw w d' W' F'N L y� / _ g ys;odwo(� t7 GIN EE s.uuaua ejuo jai uigwn nti �a q' r .a• tL q� I,x L+ pip ml � 42'3 du dtl q 1'� w u 0 cn rs col x o ,40 0 co K 0 y .M u w V� ' d k wit , u r Lu !" a Page 8 of 8 mil , 7/28/2023 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 23-192-0034 Client Project Description: Asheboro, NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 7/11/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 9 Way to PM� WRTIA"Wi tMain 901.213.2400 0 Fax u f, www.waypointanalyticaLcom Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/29/2024 Arkansas State Program 88-0650 02/07/2024 California State Program 2904 06/30/2024 Florida State Program - NELAP E871157 06/30/2024 Georgia State Program C044 11/14/2025 Georgia State Program 04015 06/30/2024 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2024 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2024 Mississippi State Program MS 11/14/2025 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2024 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2024 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00001/23-192-0034 Page 2 of 9 Way lht,(2) PM�TICAL' Sample Summary Table Report Number: 23-192-0034 Client Project Description: Asheboro, NC Lab No Client Sample ID Matrix Date Collected Date Received 97972 Asheboro Solids 07/10/2023 10:00 07/11/2023 Page 3 of 9 to Way� PA ► x Client: EMA Resources Inc Project: Asheboro, NC Lab Report Number: 23-192-0034 Date: 7/28/2023 Main 901.213.2400 .41 wwwmaypointanalyticaLcorn CASE NARRATIVE Metals Analysis Method 601 OD Sample 97975 (Shelby WTP) Analyte: Aluminum QC Batch No: 1-693030/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Arsenic QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Calcium QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Chromium QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Copper QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Iron QC Batch No: 1-693030/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Potassium QC Batch No: 1-693030/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 9 to Way� PA ► x Main 901.213.2400 .41 wwwmaypointanalyticaLcorn Sample 97975 (Shelby WTP) Analyte: Magnesium QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Manganese QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Lead QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Sulfur QC Batch No: 1-692735/1-692238 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97975 (Shelby WTP) Analyte: Selenium QC Batch No: 1-692735/1-692238 This analyte was analyzed at a dilution due to IEC interference/matrix interference. Solids Total Mercury Analysis - CVAA Method 7471A Sample 97975 (Shelby WTP) Analyte: Mercury QC Batch No: 1-692588/1-692341 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 Way to PM� 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Project Asheboro, NC Information : Report Date : 07/28/2023 Received �.���y07/11/2023 - Connie Cook Report Number : 23-192-0034 REPORT OFANALYSIS Project Manager Lab No : 97972 Matrix: Solids Sample ID : Asheboro Sampled: 7/10/2023 10:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 79.9 % 1 07/14/23 18:53 KDO SW-DRYWT Ammonia Nitrogen 4980 mg/Kg - dry 79.6 498 1 07/28/23 07:30 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <4.98 mg/Kg - dry 4.98 24.9 1 07/13/23 14:48 CLP 4500NO3F-2016 Organic N 38060 mg/Kg - dry 79.60 497.5 1 07/27/23 10:45 CALCULATION pH 8.1 S.U. 1 07/12/2317:00 CNB 9045D Total Solids 20.1 % 0.010 0.010 1 07/14/23 18:53 KDO 2540G-2011 Total Volatile Solids 52.9 % 0.010 0.010 1 07/14/23 18:53 KDO 2540G-2011 Total Kjeldahl Nitrogen 43000 mg/Kg - dry 49.8 1240 1 07/27/23 10:45 JPJ ;M-4500-NH3C-TKl` Phosphorus 24400 mg/Kg - dry 13.9 24.9 1 07/13/23 23:44 TJS 6010D Aluminum 47000 mg/Kg - dry 116 124 5 07/15/23 00:06 BKN 6010D Arsenic 6.57 mg/Kg - dry 1.24 2.49 1 07/13/23 23:44 TJS 6010D Cadmium 1.11 mg/Kg - dry 0.249 0.498 1 07/13/23 23:44 TJS 6010D Calcium 16700 mg/Kg - dry 193 249 1 07/13/23 23:44 TJS 6010D Chromium 54.7 mg/Kg - dry 1.24 1.24 1 07/13/23 23:44 TJS 6010D Copper 276 mg/Kg - dry 1.49 2.49 1 07/13/23 23:44 TJS 6010D Iron 17400 mg/Kg - dry 42.5 49.8 1 07/13/23 23:44 TJS 6010D Lead 19.9 mg/Kg - dry 0.995 1.49 1 07/13/23 23:44 TJS 6010D Magnesium 3140 mg/Kg - dry 12.9 24.9 1 07/13/23 23:44 TJS 6010D Manganese 4790 mg/Kg - dry 8.71 12.4 5 07/15/23 00:06 BKN 6010D Mercury 0.4853 mg/Kg - dry 0.112 0.930 1 07/13/23 11:16 MRE 7471A Molybdenum 24.4 mg/Kg - dry 0.746 1.24 1 07/13/23 23:44 TJS 6010D Nickel 16.4 mg/Kg - dry 0.746 1.24 1 07/13/23 23:44 TJS 6010D Potassium 1960 mg/Kg - dry 30.8 49.8 1 07/13/23 23:44 TJS 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Page 6 of 9 0 Waypoeint2790 "k�u'hitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypoiintanalyticaLcom 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 07/28/2023 755 Yadkinville Rd Information : Received : 07/11/2023 Mocksville , NC 27028 Connie Cook Report Number : 23-192-0034 REPORT OFANALYSIS Project Manager Lab No : 97972 Matrix: Solids Sample ID : Asheboro Sampled: 7/10/2023 10:00 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium 2.60 mg/Kg - dry 1.74 2.49 1 07/13/23 23:44 TJS 6010D Sodium 1330 mg/Kg - dry 64.7 124 1 07/13/23 23:44 TJS 6010D Zinc 667 mg/Kg - dry 4.23 6.22 1 07/13/23 23:44 TJS 6010D Sulfur 9800 mg/Kg - dry 25.9 49.8 1 07/13/23 23:44 TJS 6010D Sodium Absorption Ratio 1.11 Ratio 0.01 0.01 1 07/13/23 23:44 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 7 of 9 l0 Waypoint", J123.8224 Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 23-192-0034 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: T135 Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: lEmily M. Peterson Date & Time: 07/11/2023 10:11:51 Page 8 of 9 mil , 10/18/2023 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville, NC, 27028 Ref: Analytical Testing Lab Report Number: 23-277-0013 Client Project Description: Asheboro, NC Dear Mr. Brent Collins: Waypoint Analytical, LLC. received sample(s) on 10/4/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a '—'symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Connie Cook Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 9 Way to PM� WRTIA"Wi tMain 901.213.2400 0 Fax u f, www.waypointanalyticaLcom Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/29/2024 Arkansas State Program 88-0650 02/07/2024 California State Program 2904 06/30/2024 Florida State Program - NELAP E871157 06/30/2024 Georgia State Program C044 11/14/2025 Georgia State Program 04015 06/30/2024 Illinois State Program - NELAP 200078 10/31/2024 Kentucky State Program 80215 06/30/2024 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2024 Mississippi State Program MS 11/14/2025 North Carolina State Program 47701 07/31/2024 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2024 South Carolina State Program 84002 06/30/2024 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2024 Virginia State Program 00106 06/30/2024 Virginia State Program - NELAP 460181 09/14/2024 Page 1 of 1 00001/23-277-0013 Page 2 of 9 Way lht,(2) PM�TICAL' Sample Summary Table Report Number: 23-277-0013 Client Project Description: Asheboro, NC Lab No Client Sample ID Matrix Date Collected Date Received 98034 Asheboro Solids 10/03/2023 13:30 10/04/2023 Page 3 of 9 to Way� PA ► x Client: EMA Resources Inc Project: Asheboro, NC Lab Report Number: 23-277-0013 Date: 10/18/2023 Main 901.213.2400 .41 wwwmaypointanalyticaLcorn CASE NARRATIVE Metals Analysis Method 601 OD Sample 98565 Analyte: Aluminum QC Batch No: 1-709473/1-708892 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98565 Analyte: Calcium QC Batch No: 1-709473/1-708892 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98565 Analyte: Potassium QC Batch No: 1-709473/1-708892 This analyte was analyzed at a dilution due to IEC interference/matrix interference. Sample 98565 Analyte: Potassium QC Batch No: 1-710024/1-708892 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98565 Analyte: Magnesium QC Batch No: 1-709473/1-708892 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98565 Analyte: Manganese QC Batch No: 1-709473/1-708892 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98565 Analyte: Sodium QC Batch No: 1-709473/1-708892 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98565 Analyte: Phosphorus QC Batch No: 1-709731/1-708892 Page 4 of 9 to Way� PA ► x Main 901.213.2400 .41 wwwmaypointanalyticaLcorn The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98565 Analyte: Sulfur QC Batch No: 1-709473/1-708892 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 97716 (Annual Sludge) Analyte: Mercury QC Batch No: 1-709569/1-709290 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 9 Way to PM� 46245 EMA Resources Inc Mr. Brent Collins 755 Yadkinville Rd Mocksville , NC 27028 Project Asheboro, NC Information : Report Date : 10/18/2023 Received 1��0yy/04/2023 �.�- Connie Cook Report Number : 23-277-0013 REPORT OFANALYSIS Project Manager Lab No : 98034 Matrix: Solids Sample ID : Asheboro Sampled: 10/3/2023 13:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Moisture 82.4 % 0.010 0.010 1 10/06/23 16:00 CAH SW-DRYWT Ammonia Nitrogen 5600 mg/Kg - dry 90.9 568 1 10/18/23 14:37 JPJ 4500NH3C-2011 Nitrate+Nitrite-N <5.68 mg/Kg - dry 5.68 28.4 1 10/11/23 15:30 CLP 4500NO3F-2016 Organic N 38890 mg/Kg - dry 90.91 568.2 1 10/18/23 10:30 CALCULATION pH 7.5 S.U. 1 10/06/2316:07 CNB 9045D Total Solids 17.6 % 0.010 0.010 1 10/06/23 16:00 CAH 2540G-2011 Total Volatile Solids 57.9 % 0.010 0.010 1 10/06/23 16:00 CAH 2540G-2011 Total Kjeldahl Nitrogen 44500 mg/Kg - dry 56.8 1420 1 10/18/23 10:30 JPJ ;M-4500-NH3C-TKl` Phosphorus 22800 mg/Kg - dry 15.9 28.4 1 10/06/23 23:51 TJS 6010D Aluminum 46400 mg/Kg - dry 26.4 28.4 1 10/06/23 23:51 BKN 6010D Arsenic 6.14 mg/Kg - dry 1.42 2.84 1 10/06/23 23:51 BKN 6010D Cadmium 0.960 mg/Kg - dry 0.284 0.568 1 10/06/23 23:51 BKN 6010D Calcium 17200 mg/Kg - dry 220 284 1 10/06/23 23:51 BKN 6010D Chromium 52.3 mg/Kg - dry 1.42 1.42 1 10/06/23 23:51 BKN 6010D Copper 305 mg/Kg - dry 1.70 2.84 1 10/06/23 23:51 BKN 6010D Iron 15600 mg/Kg - dry 48.6 56.8 1 10/06/23 23:51 BKN 6010D Lead 17.2 mg/Kg - dry 1.14 1.70 1 10/06/23 23:51 BKN 6010D Magnesium 2610 mg/Kg - dry 14.8 28.4 1 10/06/23 23:51 BKN 6010D Manganese 3640 mg/Kg - dry 9.94 14.2 5 10/09/23 14:02 TJS 6010D Mercury 0.4413 mg/Kg - dry 0.124 1.03 1 10/09/23 11:49 MRE 7471A Molybdenum 15.3 mg/Kg - dry 0.852 1.42 1 10/06/23 23:51 BKN 6010D Nickel 15.6 mg/Kg - dry 0.852 1.42 1 10/06/23 23:51 BKN 6010D Potassium 1490 mg/Kg - dry 35.2 56.8 1 10/06/23 23:51 BKN 6010D Qualifiers/ DF Dilution Factor J Estimated value Definitions MQL Method Quantitation Limit Page 6 of 9 0 Waypoeint2790 "k�u'hitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypoiintanalyticaLcom 46245 EMA Resources Inc Project Asheboro, NC Mr. Brent Collins Report Date : 10/18/2023 755 Yadkinville Rd Information : Received : 10/04/2023 Mocksville , NC 27028 Connie Cook Report Number : 23-277-0013 REPORT OFANALYSIS Project Manager Lab No : 98034 Matrix: Solids Sample ID : Asheboro Sampled: 10/3/2023 13:30 Test Results Units MDL MQL DF Date / Time By Analytical Analyzed Method Selenium 3.06 mg/Kg - dry 1.99 2.84 1 10/06/23 23:51 BKN 6010D Sodium 1550 mg/Kg - dry 73.9 142 1 10/06/23 23:51 BKN 6010D Zinc 767 mg/Kg - dry 4.83 7.10 1 10/06/23 23:51 BKN 6010D Sulfur 11300 mg/Kg - dry 29.5 56.8 1 10/06/23 23:51 BKN 6010D Sodium Absorption Ratio 1.21 Ratio 0.01 0.01 1 10/06/23 23:51 CALCULATION Qualifiers/ DF Dilution Factor Definitions J Estimated value Page 7 of 9 l0 Waypoint", J123.8224 Shipment Receipt Form Customer Number: 46245 Customer Name: EMA Resources Inc Report Number: 23-277-0013 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: T99 Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IMakayla Weaver Date & Time: 10/04/2023 09:59:26 Page 8 of 9 CL N LL U) 0 n u El A�! L) no m z m gas 0. 'o E Y' v io C) z C 17 <m'd in. to EE: E SA�'I -0 IV 0 lop E Tz z Td > to ........ ................ E 'SPHOS PlOi LO E (-,'IUOLJJLLI:V/N)4.L c r ......... . .. 7E ce m W011,09) sle'lalLN Z" z 40 < aj�sodlwo(:)) jo qej(D) E �L z (Az)l o3 japti) xlj3eW S cr sjiauileluo:) jo jaqwrIN rcua m m o CY) T) UJ E CO CL F to E E => WY (11� M, < tr) uj 0 x Pars q nf q aceAnalytical° ANALYTICAL REPORT January 17, 2023 EMA Resources Sample Delivery Group: L1572732 Samples Received: 01/05/2023 Project Number: Description: Sludge Report To: Mr. Brent Collins 755 Yadkinville Road Mocksville, NC 27028 Entire Report Reviewed By Reagan Johnson Project Manager Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067and ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy ofthe information provided, and as the samples are received. %yp [Cn Sc ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1572732 01/17/23 17:09 1 of 22 TABLE OF CONTENTS cj'x 11 . c iI M")fle' of Coil 2 Ss: Sample Summary 3 Cn: Case Narrative 4 Sr: Sample Results 5 SS ASHEBORO L1572732-01 5 Fn oc oua�ft)lt bil 111 0 �� S I � 11,11,1111,11,11 a II"" ),It "7 Wet ( IheinnIIstii ),It 'n't Meflhod 9012 "7 1711-1 Ll Wet ( Iheinn�stii ),It 'n't Meflhod 903A1, 9030��1113 77 ....................... Wet ( Iheinnstii ),It :n't Meflhod 9G�15L) 9 Wet ( IheinnIstii ),It :n't Meflhod ���)93/1010A 10 FG Meii 4: 1 � I )t w Meflh�'d 7A170A 11 M et a �� s fl :n't Meflhod 12 .. ...................................... 11111(datflie Oil gaink binniq!)Ourlds (G( YP4S) 'n't Meflhod 82(150����) I II 0 1 firlated Acod Ieii ',)llddes (G( ',nit IIMeflhod 8151A 177-1 ILI :Iesflddes (G( b�it Vlietlhod 808"V:1113 17 Serninii 1111datflie Oil gaink 011,11n11!1Mourids (G( PMS) 'n't Meel hod 82'M: 18 GI: Glossary of Terms 20 AL AccriedftatJoins & d"e'.atJoris 1 Sc: Sample Chain of Custody 22 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1572732 01/17/23 17:09 2 of22 SAMPLE SUMMARY Collected by Collected date/time Received date/time AS[ IEBORO 1 1572732-01 Waste Brent Collins 01/04/23 1110 01/05/23 08 30 ................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................... Method Batch Dilution Preparation Analysis Analyst ............... Location' date/time date/time Preparation by Method 1311 WG1983635 1 01/05/23 13 19 01/05/23 13 19 BTP Mt. Juliet, 1 Preparation by Method 1311 WG1983661 1 01/05/23 12 22 01/05/23 12 22 is Mt. Juliet, TN Wet Chemistry by Method 9012 B WG1983961 1 01/09/23 17 11 01/10/23 14 30 CAT Mt. Juliet, TN III Wet Chemistry by Method 9034-9030B WG1983808 1 01/06/23 15 00 01/11/23 19 30 AW Mt. Juliet, TN Wet Chemistry by Method 9045D WG1984186 1 01/06/23 08 30 01/06/23 10 41 KAD Mt. Juliet, TN Fn Wet Chemistry by Method D93/1010A WG1985101 1 01/09/23 17 34 01/09/23 17 34 WOS Mt. Juliet, TN Mercury by Method 7470A WG1984342 1 01/06/23 10 29 01/06/23 15 10 LAS Mt. Juliet, TN Metals (ICP) by Method 6010D WG1989198 1 01/16/23 09 51 01/16/23 13 55 ZSA Mt. Juliet, TN Ll Volatile Organic Compounds (GC/MS) by Method 8260D WG1984302 1 01/07/23 14 20 01/07/23 14 20 DWR Mt. Juliet, TN Chlorinated Acid Herbicides (GC) by Method 8151A WG1984180 1 01/06/23 20 26 01/11/23 00 45 DLH Mt. Juliet, TN Pesticides (GC) by Method 8081B WG1984981 1 01/09/23 05 58 01/09/23 14 35 RDH Mt. Juliet, TN Semi Volatile Organic Compounds (GC/MS) by Method 8270E WG1984982 1 01/09/23 04 53 01/09/23 15 35 -N-1 Mt. Juliet, TN GI .. ...................................... ) Ll ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1572732 01/17/23 17:09 3 of 22 CASE NARRATIVE All sample aliquots were received at the correct temperature, in the proper containers, with the appropriate preservatives, and within method specified holding times, unless qualified or notated within the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control are within established criteria except where addressed in this case narrative, anon -conformance form or properly qualified within the sample results. By my digital signature below, I affirm to the best of my knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the ................ quality of the data have been identified by the laboratory, and no information or data have been knowingly withheld that would affect the quality of the data. Sr ... r, a% GI Reagan Johnson Project Manager Project Narrative � L All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B. All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-903013. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1572732 01/17/23 17:09 4 of 22 ASHEBORO Collected date/time: 01/04/23 11:10 Preparation by Method 1311 Result Analyte TCLP Extraction TCLP ZHE Extraction - Fluid 1 Initial pH 7.97 Final pH 5.21 Wet Chemistry by Method 9012 6 Result SAMPLE RESULTS - 01 L1572732 Qualifier Prep Batch date / time 1/5/202312:22:55 PM WG1983661 1/5/2023119:09 PM WG1983635 1/5/202312:22:55 PM WG1983661 1/5/202312:22:55 PM WG1983661 1/5/202312:22:55 PM WG1983661 Qualifier RDL Analyte mg/kg mg/kg Reactive Cyanide 0.427 0.250 Wet Chemistry by Method 9034-9030B Result Qualifier RDL Analyte mg/kg mg/kg Reactive Sulfide ND 75.0 Wet Chemistry by Method 9045D Dilution Analysis Batch date / time 1 01/10/202314:30 WG1983961 Dilution Analysis Batch date / time 1 01/11/202319:30 WG1983808 Result Qualifier Dilution Analysis Batch Analyte su date / time Corrosivity by pH 7.67 TC 1 01/06/202310:41 WG1984186 Sample Narrative: L1572732-01 WG1984186: 7.67 at21C Wet Chemistry by Method D93/1010A Result Qualifier Dilution Analysis Batch Analyte Deg. F date / time Ignitability DNI at170 1 01/09/202317:34 WG1985101 Mercury by Method 7470A Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Mercury ND 0.0100 0.20 1 01/06/202315:10 WG1984342 Metals (ICP) by Method 6010D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Arsenic ND 0.100 5 1 01/16/202313:55 WG1989198 Barium 0.107 0.100 100 1 01/16/202313:55 WG1989198 Cadmium ND 0.100 1 1 01/16/202313:55 WG1989198 Chromium ND 0.100 5 1 01/16/202313:55 WG1989198 Lead ND 0.100 5 1 01/16/202313:55 WG1989198 Selenium ND 0.100 1 1 01/16/202313:55 WG1989198 Silver ND 0.100 5 1 01/16/202313:55 WG1989198 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Benzene ND 0.0500 0.50 1 01/07/202314:20 WG1984302 Carbon tetrachloride ND 0.0500 0.50 1 01/07/202314:20 WG1984302 Chlorobenzene ND 0.0500 100 1 01/07/202314:20 WG1984302 Chloroform ND 0.250 6 1 01/07/202314:20 WG1984302 ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1572732 01/17/23 17:09 PAGE: 5 of 22 ASHEBORO SAMPLE RESULTS - 01 Collected date/time: 01/04/23 11:10 L1572732 Volatile Organic Compounds (GC/MS) by Method 8260D Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,2-Dichloroethane ND 0.0500 0.50 1 01/07/202314:20 WG1984302 1,1-Dichloroethene ND 0.0500 0.70 1 01/07/202314:20 WG1984302 2-Butanone (MEK) ND 0.500 200 1 01/07/202314:20 WG1984302 Tetrachloroethene ND 0.0500 0.70 1 01/07/202314:20 WG1984302 Trichloroethene ND 0.0500 0.50 1 01/07/202314:20 WG1984302 Vinyl chloride ND 0.0500 0.20 1 01/07/202314:20 WG1984302 Fn (S) Toluene-dH 103 80.0-120 0110712023 14.20 WG1984302 (S) 4-Bromofluorobenzene 106 77.0-126 0110712023 14.20 WG1984302 (S) 1,2-Dichloroethane-d4 98.9 70.0-130 011071202314.20 WG1984302 Chlorinated Acid Herbicides (GC) by Method 8151A Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 7G1 2,4,5-TP (Silvex) ND 0.00200 1 1 01/11/2023 00:45 WG1984180 2,4-D ND 0.00200 10 1 01/11/2023 00:45 WG1984180 (S)2,4-DichlorophenylAcetic Acid 79.8 14.0-158 011111202300.45 WG1984180 I u Pesticides (GC) by Method 8081B Sc Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time Chlordane ND 0.00500 0.03 1 01/09/202314:35 WG1984981 Endrin ND 0.00500 0.02 1 01/09/202314:35 WG1984981 Heptachlor ND 0.00500 0.0080 1 01/09/202314:35 WG1984981 Heptachlor epoxide ND 0.00500 0.0080 1 01/09/202314:35 WG1984981 Lindane ND 0.00500 0.40 1 01/09/202314:35 WG1984981 Methoxychlor ND 0.00500 10 1 01/09/202314:35 WG1984981 Toxaphene ND 0.0100 0.50 1 01/09/202314:35 WG1984981 (S) Decochlorobiphenyl 41.0 10.0-128 011091202314.35 WG1984981 (S) Tetrochloro-m-xylene 62.4 10.0-127 011091202314.35 WG1984981 Semi Volatile Organic Compounds (GC/MS) by Method 8270E Result Qualifier RDL Limit Dilution Analysis Batch Analyte mg/I mg/I mg/I date/time 1,4-Dichlorobenzene ND 0.100 7.50 1 01/09/202315:35 WG1984982 2,4-Dinitrotoluene ND 0.100 0.13 1 01/09/202315:35 WG1984982 Hexachlorobenzene ND 0.100 0.13 1 01/09/202315:35 WG1984982 Hexachloro-1,3-butadiene ND 0.100 0.50 1 01/09/202315:35 WG1984982 Hexachloroethane ND 0.100 3 1 01/09/202315:35 WG1984982 Nitrobenzene ND 0.100 2 1 01/09/202315:35 WG1984982 Pyridine ND 0.100 5 1 01/09/202315:35 WG1984982 3&4-Methyl Phenol ND 0.100 400 1 01/09/202315:35 WG1984982 2-Methylphenol ND 0.100 200 1 01/09/202315:35 WG1984982 Pentachlorophenol ND 0.100 100 1 01/09/202315:35 WG1984982 2,4,5-Trichlorophenol ND 0.100 400 1 01/09/202315:35 WG1984982 2,4,6-Trichlorophenol ND 0.100 2 1 01/09/202315:35 WG1984982 (S) 2-Fluorophenol 19.8 10.0-120 011091202315.35 WG1984982 (S) Phenol-d5 13.7 10.0-120 011091202315.35 WG1984982 (S) Nitrobenzene-d5 28.6 10.0-127 011091202315.35 WG1984982 (S) 2-Fluorobiphenyl 43.9 10.0-130 011091202315.35 WG1984982 (S)2,4,6-Tribromophenol 91.0 10.0-155 011091202315.35 WG1984982 (S) p-Terphenyl-d14 71.7 10.0-128 011091202315.35 WG1984982 ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1572732 01/17/23 17:09 6 of 22 F- p s o m O1 N E O FFD-l - � � . 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(3 N � N Ln co N rn o � o c O c 0� o 0 0 0 0 c E M o 0 4 a c o o 0 oo0 0 0 0 0 ° s o `o o p o Co 0 0 0 s Q `o c� o o m f0 X X X -6 Ln CO E O t o 0 0 0 0 0 0 0 0 0 0 0 c.i OO ID ID OO OO ID OO IDO O ID O O O O U W N O O O M I� O^ M N M M W CO N V N N 61 c0 O O ^ � ID M IDM IDM ID J E O O O O O O O O O O O O C 0 O E Q M O ID ID ID ID ID ID ID ID ID ID ID IDM om— o 0 0 0 0 0 0 0 0 0 0 0 o Q s cn E 0 0 0 0 0 0 0 0 0 0 0 0 M N rn o o O O co V o O N N m w . w-M � - o - o 0 6 a c n o a w Q o Co o 0 0 0 0 o 0 E 0 0 co `o `o `o `o s Q `o o T V V V V 4 U C QJ QJ QJ Omx Q N = _ = Z d M N d N N N W N a o a co N N0 N LO J v w O a "I E M N U O O O O O O O � o A2 E ID ID 0 OM M M OM M M M N 0 p 0 Y E O O O O O O O M o 0 0 0 o Lo w U N p CO M N N O M N O CO CO Ln co O CO O p� N M M O M O O 6 ^ O O co N O O O N M O M M r O M CO CO ^ O o Ln I� M O M V O (o � Y cc n M � M ID ID M CO L.() n n M p O1 N OM 61 M CO p M M OM (n E O O O O O O Z O O O O O Lo � fn M 61 I.t) M ID O ID 6M N M � E O O O O O O Z O O O O O O O � N M � cc co 0 E Q rn- O O O O O O O O O O O O N - — O O O O O O O O O O O O Q s cn E o 0 0 0 0 0 0 0 0 0 0 0 M N rn O � o N o 0 0 0 0 a a c E 61 M U o 0 o 0 o 0 0 0 0 � T s o 0 0 `o o � `o , 4 o Jc�i c�i >` a :'a a :'a a O N W N a 0 a m N N0 N U) J v w O d 2 Z D =) 0 O � a a � LL GLOSSARY OF TERMS Guide to Reading and Understanding Your Laboratory Report The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not intended as a comprehensive explanation, and ifyou have additional questions please contact your project representative. Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name, Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received. Abbreviations and Definitions MDL Method Detection Limit. ND Not detected at the Reporting Limit (or MDL where applicable). RDL Reported Detection Limit. Rec. Recovery. RPD Relative Percent Difference. SDG Sample Delivery Group. Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and (S) Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be detected in all environmental media. U Not detected at the Reporting Limit (or MDL where applicable). Analyte The name ofthe particular compound or analysis performed. Some Analyses and Methods will have multiple analytes reported. Ifthe sample matrix contains an interfering material, the sample preparation volume or weight values differ from the Dilution standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the result reported has already been corrected for this factor. These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal Limits for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or duplicated within these ranges. Original Sample The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control sample. The Original Sample may not be included within the reported SDG. This column provides a letter and/or number designation that corresponds to additional information concerning the result Qualifier reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and potentially a discussion of possible implications ofthe Qualifier in the Case Narrative if applicable. The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. Ifthere was no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL" Result (Below Detectable Levels). The information in the results column should always be accompanied by either an MDL (Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect or report for this analyte. Uncertainty (Radiochemistry) Confidence level of 2 sigma. A brief discussion about the included sample results, including a discussion of any non -conformances to protocol Case Narrative (Cn) observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report. Quality Control This section ofthe report includes the results ofthe laboratory quality control analyses required by procedure or Summary (Qc) analytical methods to assist in evaluating the validity ofthe results reported for your samples. These analyses are not being performed on your samples typically, but on laboratory generated material. This is the document created in the field when your samples were initially collected. This is used to verify the time and Sample Chain of date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This Custody (Sc) chain of custody also documents all persons (excluding commercial shippers) that have had control or possession ofthe samples from the time of collection until delivery to the laboratory for analysis. This section ofyour report will provide the results of all testing performed on your samples. These results are provided Sample Results (Sr) by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for each sample will provide the name and method number for the analysis reported. Sample Summary (Ss) This section ofthe Analytical Report defines the specific analyses performed for each sample ID, including the dates and times of preparation and/or analysis. Qualifier Description E The analyte concentration exceeds the upper limit ofthe calibration range ofthe instrument established by the initial calibration (ICAL). J2 Surrogate recovery limits have been exceeded, values are outside lower control limits. J3 The associated batch QC was outside the established quality control range for precision. J5 The sample matrix interfered with the ability to make any accurate determination, spike value is high. J6 The sample matrix interfered with the ability to make any accurate determination, spike value is low. J7 Surrogate recovery cannot be used for control limit evaluation due to dilution. P RPD between the primary and confirmatory analysis exceeded 40%. T8 Sample(s) received past/too close to holding time expiration. ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE: EMA Resources L1572732 01/17/23 17:09 20 of 22 ACCREDITATIONS & LOCATIONS !Ninl',71cl I\h ll+"inl l 12065 I cd it I+:+I""I Alabama 40660 Nebraska N E-OS-15-05 Alaska 17-026 Nevada TN000032021-1 Arizona AZ0612 New Hampshire 2975 Arkansas 88-0469 New Jersey—NELAP TNO02 California 2932 New Mexico TN00003 Colorado TN00003 New York 11742 Connecticut PH-0197 North Carolina Env375 Florida E87487 North Carolina' DW21704 Georgia NELAP North Carolina 3 41 Georgia' 923 North Dakota R-140 Idaho TN00003 Ohio—VAP CL0069 Illinois 200008 Oklahoma 9915 Indiana C-TN-01 Oregon TN200002 Iowa 364 Pennsylvania 68-02979 Kansas E-10277 Rhode Island LA000356 Kentucky' 6 KY90010 South Carolina 84004002 Kentucky 2 16 South Dakota n/a Louisiana A130792 Tennessee' 4 2006 Louisiana LA018 Texas T104704245-20-18 Maine TN00003 Texas5 LABO152 Maryland 324 Utah TN000032021-11 Massachusetts M-TNO03 Vermont VT2006 Michigan 9958 Virginia 110033 Minnesota 047-999-395 Washington C847 Mississippi TN00003 West Virginia 233 Missouri 340 Wisconsin 998093910 Montana CERT0086 Wyoming A2 LA A2LA— ISO 17025 1461.01 AIHA-LAP,LLC EMLAP 100789 A2 LA — ISO 17025 5 1461.02 DOD 1461.01 Canada 1461.01 USDA P330-15-00234 EPA—Crypto TN00003 Drinking Water 2 Underground Storage Tanks 3 Aquatic Toxicity "Chemical/Microbiological 5 Mold 6 Wastewater n/a Accreditation not applicable Not all certifications held by the laboratory are applicable to the results reported in the attached report. Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical. ACCOUNT: PROJECT: SDG: DATE/TIME: EMA Resources L1572732 01/17/23 17:09 PAGE: 21 of 22 Ia" 10 T C ul ...... .... AJ 7"7777, MR ZL Awl X, 4w Ad 21 ask "in ILL 2:. At IV co w o :IK 'I ej r3 IW TJ C, w at 61 t t ra ZT Iq tA 00 va Ub RID ain CL Tl Az, 10 00 j IdD qc E rr 'dI w aj w W, U Cl a tn knI ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQOOO 1684 WWTP Name: Asheboro WWTP NPDES Number: NCO026123 Monitoring Period: From 1/1/2023 To 3/31/2023 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) Alt L B (Alk Treatment) 0 Alt. C (Prior Testing)[] == 7RT77iTgen,�s rl]7 Alt.D(NoPriorTesL) Process 7toFurther Reduce Patnogen7gs[3 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying 1:1 Heat Treatment 0 Thermoribilic 0 Beta Ray Gamma Ray Class Alt. (1) Fecal Density �„„ Alt. (2} Process to Significantly Deduce Path®gene ,„";� If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lune Stabilization Air Drying CJ Composting (,r 0 jAerobic Digestion Anaerobic Digestion E3 If applicable to alternative performed (Class A or Class B) complete the following monitoring data: N Parameter Allowable Level Pathogen Density L , MF-er-7 — Excee- Frequency Sample Analytical in Sludge immum Geo. Mean Maximum Units of Analysis Type Tech-nique Mi imum 2x 10tothe Sludge 6th power per gram of Fecal Coliform total solids CFIJ 1701 5779 35651 col/g 0 Quarterly C 1000 mpn per grain of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed: Alt. I (VS reduction) Alt. 2 (40-day bench) [%,�3 Alt. 3 (30-day bench) Ej Alt. 4 (Spec. ()2uptake) L-3 Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) 13 Alt. 8 (Drying - Unstable) E I Alt. 9 (Iniection) El Alt. 10 (Incorporation) [3 No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02'r .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both or the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman - Plant Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 02/26/2z H3 �11) 24;2� 1/19/2024 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (12/2006) CITY OF ASHEBORO Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part 503 (White House Manual) Appendix D Revised 5-28-14 ay Date Moisture and Dry Solids Wt Dish +Wet Solids, g �) . � . 5• � • (Qfh_ 3 � � Wt Dish, g M �Ul1 17. 1 a Wt Wet Solids, g ' .'1 1 d + Wt Dish Dry Solids, g 3� I� w � 5i Wt Dish, g WtDry Solids, g ° - 0 �• i� % Dry Solids " 11 Volatile Solids Wt Dish +Dry Solids, g Wt Dish + Ign Solids, g Wt Ign Solids, g Vol Solids Own i MUM n Aiiolyt ` Checked by ay Da`11te Dish # Wt Dish + Wet Solids, g 24. LniM Wt Dish, g 2 .201 Wt Wet Solids, g '1 : Wt Dish +Dry Solids, g . X'— Wt Dish, g IVt Dry Solids, g 0, % Dry Solids Wt Dish +Dry Solids, g 4 Wt Dish + Ign Solids, g. Wt Ign Solids, g 0, cy jC-J % Vol Solids ii . n Anolt!� Checked by Dish # Wt Dish + Wet Solids, g Wt Dish, g Wt Wet Solids, g Wt Dish +Dry Solids, g Wt Dish, g Wt Dry Solids, g % Dry Solids Wt Dish +Dry Solids, g� Wt Dish + Ign Solids, g IA/4- I-- C-H. , - Moisture and Dry Solids .01e�o . 7 Volatile Solids -1. qb 6 Moisture and Dry Solids Average 1 2,. Average tee, 01 I a 20 Day VSR�.• 4 y .C3 V VIGUIC dvrlW Average 2023 City of Asheboro January Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time Temp. Initials Time Temp. Initials le 15 2 v C�53 q 3 MCA is � � � � 6� � `+ z A� 3 p"ia� 33• V�v 1"G�y�� �31n'�' 4 �� I ��Q , a '� a 3 k 3 3q a Oe� 5 ©07_ 3.3, �'�� �3.6 7 M 15- 3�,� r 0005 33,&v . 9 o s' •o -CJ 3 3 � � (0 D _ 3" I Pew 11 __ p071- '302- 39.5 Aoki a 3S .S 000a 13 DL�f 34) .""(G 14 ©_b�'� is-fo 33,1_ a-3 o 0 33' (6 R 15 N� 3 �G 144QJ 30..E - 33 16 0 (p �i� �� Z, 33 17 01 3. 53 � .. -�W a � , � a33o a 18 ©6� q ���Q "�G ". IDS �_sl_� �33�'" _ 19 iD M 130-1_ 5 A vi_ 20 33�P�► 22 0� �.o 33. � I Sack �� � � c� aso 33- 23 _� ! 30 33 5 �L 24 _— Zs �� � 04 15I � � a 3 3 � 27 -MA-k- 9:S� '�3 % e _ 11 a33 33 28 p (�'44 3i,1 Tc a„i— 3 j 1d 29 A6 y G 13 3 .,q /1 J � 33c _ a� �3 3L1. 0 iq _ . 2023 City of Asheboro February Digester Pilot Plant Temperature Log (Record once per shift) 1 st shift 2nd shift 3rd shi Date Time Temp. Initials Time Temp. Initials Time Temp. Initials 2m�_ _ 930 33.s 1 ° a3oo �3.5 4 0-7 - " ....... -. - 2 6 0�� 33 -�I WOO 3. �E 7 b6S-1 _ �3�� �G 191,5. 33"7 q 7�pO 33. 10 r ► * (t D _ _ �33-� aer � � 3a o 3 11 6.(aSS, 33.3 i Ave1 I �'-! � �3� 1iW+T 23UG J 5 2 0'7O cJ .� A r?n [1 v-) 3 G � Zsoo -:Sz, 13SV 7 (�O 1O `�Rt.�% 14 ���� ten. b. 7 `jC.. ' � W . 3,Lr I � _ ��� a3��3 33.9 fl W 15 BLij" ��i7 1 5 �_ 16 o �s 7 .33, 17 13 �rt3 S 1 33. 3 A(U10 18 bro � _ 33.5 (�� iq � 3 . � e S i �.G �© •? 3. i E__. 20 10� 33 r! ,� 1 Siff 33• ��►T 3` _ 21 105(c 33 s AW y 33 1 Rc,�j a3 a el s 22 15 3 �1 A SQ 3 3 L4 ° _ a �' V 23 j 1 L4LW � 3�• 24 0�7 3�'t uv � s • ! Y�PA, -W _ 25 6 `1 L _ iL' _� 1 33 t v" _ 3 0 0 `33 r ' ,„ 26 fl bH� _ _ ; 27 0'7vi 33.(e I D3dU 2s 29 a 0 o u t m a a� 0 G7 V a N C E �o u d U. E Cftp of Sobeboro Dry Solids for Sludge Hauling Date 31ILA Iz?7 151ti3 3 -11.P 2?j 3 1-1.23 (Analyst Initials iN� b6o ezJ A Dish Number Source Wt. Dish & Wet Solid (g)rj . Wt. Dish (g) S�." �""1.�1 �1 8t4 •% Z �1'I .g3p3 Wt. 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Weight (lb/ft) Operator Initials L �i� �NIN ".CO f` U-)CDIO ti (D � � N CO � t- Lo ,q M. 51 O N CV N N N N M N N N N N N N U)i CD M 00 r M Cq 00 ; N Co 1� U) U) r I� LO M U) N M CD ` CD' O CO O CO C I` ti CD O 00 00 tO 00 00 0 f� Ln N N C l Lo Cl CM N N N € C`M CV 1� I� a0 t` = ti ti N ti, t• ti ti ti ti N Oc J LO 00O :CON Co 'qr 0) �N CA I r r r�N OD1� 0 I� CD I� MOO M�O M CO r li'[ MM N T CD LOLOLOCO�U.) q U)�d ..�d'�`[i [r0vIT M�IT(Y)ce) T� O cc) Or OOO CO 00100 CO O co, O d V � q cer Cd mMMMMMM;MMNN M" co N r r r r r r r r ..'..., I- 0) A a0 O 0)M0TOr0 co 0 00N N MN Nr �.........,O VI— r iNrr N.N N N'NN N NN;N N N N r r A. r N M M' CO [t 00.T Ord �. �f M cco o O N M c- CO M M 00 NM CO O V N CO O M CO U) CD U) qr (M V «) V V' 00 > O I... 4 \ N NININ M!N (M M M M m m co C00 M COM M NIN N N=N N N N co N co 14, N M r r�r r,r'r r r r rlr r�r r r�r r�r,r�r r r...T T T T rr 04 (Mri • CA N CO.. M M M U7 CA.' 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I- M 00 0) co 'IT N 'T I f�M CDOO f- Oti OO 00 Nt` co N N M MN M M MiN MN I N N N LO Z I N r N c)Lo�CO A M (D �M,LO O 0) N I In (D (O N LO 0 i W Nt7 O 0rN O00 - ODM(D LO 0 CA M OD (M I� I�N(D C N LO CA LO O O M O to ArOh r O NM CM � � O N d T [TOAC 1 CO eM (M Cr N CM Iq OM 00 O 14, 8 It O [F Ml0 d)IOU� MpI(VZr6 000000000O0000000000 0 00 U iNLp O016 000 000OOOOOOOOOOi000 r , O 0 0 0 O O O O 0 0 .0 0 0 0 O O O I 0 0 0 0 0 0 lL OOO CD CO ONOON O`CONODO co 00 to ! O T CA 00 O O COO'N� to 0 1 0 M I Ln r CON aD OS N C O 00 I- OD 00 � 0) O)0 0) 00 CA CIO) 00 co CA 100 O co co ti co CD M ,ti S O ,. N O,.,r , M I- N N 1-- 00 00 00 H W [n CA J N M O M (tl� NT M ill 0 M M' co co I� , O to Mq T M O N O O N O CD to I� M co I� LO Il- 00 (O V tC) CA r CO 0) 00 N O a. I I Z J Ln LO I-LON'V M O Nr U)CO f, MOCDN0 ON M Q N M It M O M LO eM M I— CO I1- CAM CO r T O N O 0 CO CD M I,- M N_ I" r U) O O� '. a� 3a CMN CN(NMN ce) hN �LC)NNLO0 VN CO Li I- — N, co r.. I,- M N 1l N M eM N LO N LO LO T ti I- N. (D r to I M r -00 r M Z N 00 N N N 1- 8 LC) M G M I- I- Orr O r OD I` LO LO N M N Cr) N r� q: 0 00 I� N NT (q r M C(OA r LO LO' O CM O (A O t Nr 0L 0r COJOf Or (N/NC cl)�AO W CO O CO C:)I-r ... C) 1— 0') P.- CO(O I,- 1'-000) I� OO TCO f� A W r (DTT r r......r M r-N 0 r 0 r.....T 0r0 O I,- T T r'r.......r MO r NO I� r U) , M lO 00 M CA , N O 00 1 t O O) M I� N� co f� CD f� '�t CO Co O r 00" N N 'q "t I O� j,M - tl0 � p 7,M ��� 0 0.. It �c Ll Lo (O [ L V q_ LO 00�0010000090 0 'IT 'qr0 O 0 � O 00000€OOO(::,OOOO�i00 O d IT v co 00 NC7 0 � � OOOIOi0f0�00000010'0000000 000 C 0 r ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQOOO 1684 WWTP Name: Asheboro WWTP NPDES Number: NCO026123 Monitoring Period: From 4/l/2023 To 6/30/2023 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) Alt L B (Alk Treatment) 0 Alt. C (Prior Testing)[] == 7RT77iTgen,�s rl]7 Alt.D(NoPriorTesL) Process 7toFurther Reduce Patnogen7gs[3 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying 1:1 Heat Treatment 0 Thermoribilic 0 Beta Ray Gamma Ray Class Alt. (1) Fecal Density �„„ Alt. (2} Process to Significantly Deduce Path®gene ,„";� If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lune Stabilization Air Drying CJ Composting (,r 0 jAerobic Digestion Anaerobic Digestion E3 If applicable to alternative performed (Class A or Class B) complete the following monitoring data: N Parameter Allowable Level Pathogen Density L , MF-er-7 — Excee- Frequency Sample Analytical in Sludge immum Geo. Mean Maximum Units of Analysis Type Tech-nique Mi imum 2x 10tothe Sludge 6th power per gram of Fecal Coliform total solidCFIJ 1190 1852 3809 col/g 0 Quarterly C s 1000 mpn per grain of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform weight Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed: Alt. I (VS reduction) Alt. 2 (40-day bench) [%,�3 Alt. 3 (30-day bench) Ej Alt. 4 (Spec. ()2uptake) L-3 Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) 13 Alt. 8 (Drying - Unstable) E I Alt. 9 (Iniection) El Alt. 10 (Incorporation) [3 No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02'r .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both or the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman - Plant Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 02/26/2z H �(l ��11) 24;2� 1/19/2024 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (12/2006) CITY OF ASHEBORO Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part503 (White House Manual) Appendix D Revised 5-28-14 Moisture and Dry Solids iish # ' i.Gl '�O i. . C VVt Dish +Wet Solids, g -i 3 Wt Dish, 9 Wt Wet Solids, g q, " .5Z 1) - Wt Dish +Dry solids, g 11 •, .�2 Wt Dish, g Wt Dry Solids, g .: -101 , , 3o Dry Solids Volatile Solids Wt Dish +Dry Solids, g Wt Dish + Ign Solids, g LA 1 2 , ". Wt Ign Solids, g 2 -1 n. 101 Z n ,nol st s � Checked Vol Solid 3o y by y Dote Moisture and Dry Solids Dish # i 2 Wt Dish + Wet Solids, g Wt Dish. 9 > "� '1_1 `� '"" �� �°• 13 2 Wt Wet Solids, g LL.a -1IJZL. Wt Dish +Dry Solids, g {vy, sby-► S . Z2�Z -7 $ . 3-725 -] 51 `" z, Wt Dish, 9 Wt Dry Solids, 9 2 Z,A... % Dry Solids 'L•cl�J°". �-ISL, QA Volatile Solids Wt Dish +Dry Solids, 9 Wt Dish + Ign Solids, g '&,A . bin LS �• Wt Ign Solids, g 3 LA 5 60, � ?j5 % Vol solids ` „ -71 VI u Analyst " ry Checked by e 3% A,20 Day VSR Day late 2' Moisture and Dry Solids Dish # 2. Wt Dish + Wet Solids, g d Wt Dish, g �• jif'0 I ° g• 8 Wt Wet Solids, g • I a; 0 1' Wt Dish +Dry Solids, g m Wt Dish, g -2 3y r ,' Wt Dry Solids, g Q • (� lD �-I , a .' % Dry Solids 'µOLP .0 Volatile Solids Wt Dish +ry Solids, g ' Wt Dish +Ign Solids, g 1 • . 1 9 r% •� Wt Ian Solids. a "' . I 1 t� (1) . i ,� , "-� . i0.1 � 1 G o • Average Average Average 2023 City of Asheboro April Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time - Temp. Initials Time Temp. Initials 33i AA � 33,_ 'tOa ,� 2 1543 33 ` t 33.07 33. 3 � �� .� s'C& 1943 _33.3 (W4L 3-7, s �E 5 C.,-)I 3 7 �� �qWO )3 .'A6 > 3 a� i 4q Ar g a'7 V-1 �.3 r 441 sw 33 `7 • ,alR,c _ ....... ��, _ 33'l 9�J i 3�� Yip- 000, 33.J E � 10 a141"t <L w 3•s" ri1c� a �oG 3.� fir✓ 1 (a , r 7 _ wNl / �� 30 � —Z I Ll C 12_� L"�� 'S ! 1��� Sd© Lam. 13 0701 .S'' '� f t � 3 230 L. 35 .A0 1 14 0S A 33 .1 t 1 y � 33 IX t 30 .S 3 3 .E AN, ............. SS ry 16 0-1 OC 17 �7 � � 33 ,°1 f ):S-K 331 � , O G , _ 16 07y5 , 3y.0 l-J"� ISIO 31•1 a300 33. P 19 G 74lo 3 3• 454 ISi0_ 33.1 ,A� �ad6 _i�3. � 20 _ 0 7 315 3 3.7 1,7.7 in -7 33. 3 p _ 21 SS 341.1 ,ail' 'I IS (5 33' al Ntiw W30 G 3 22 0G6' 33,9 QE� 1gLIO 33,'6 23 GG 30 . 3 -5 3 3-d 00 24 33.6 r/'1 IS On 32. �'� _ 1K 33• 0 Aw_ 25 U 735 33• �l� 'lSq 1 32• `� m. a3 �� 33 t� 26 0 7 �/� 3 2 • `i D b �Z °1,�� �3 33 fly_ 27 A96 a 30PL 33 3 p 28 p k �3•� ° -� /Soo 3' v ` -ag 01 _ 33•`1 APW 29 ©6S� 3, _Zc ts3S 31.5 3c,o 33. y R:_ 2023 City of Asheboro May Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time Temp. Initials Time Temp. Initials m 1 700 3 3 400 1y 4 I 33.3 1 2Lca � 31.c� n� 2 7bO 33 . � AQj3 3 3a.1 A4W f qqT 32.`� � 4 US% 33.0 " 140 22 j 73{1 � !� C4 5 (o5(D _ 33'1 "4) IyLIO -562'6 6 7"00 3 z• 9 - JI I U4 � &W 33.1 8 c)S 3c .� Ail, 9 _ Oc1s1 36 .o , A oc. i(43�'. 10 0-10 j 3 5.1 4 140 35"Z n 11 j4g3 35�) rr 12 � � � _ � �f�<. )943 SS•0 13 1 1(.l i 3 S' (o J5.1 A W-) 14 123 35-4, A4vd 5 35' fi o+. 16 TE:�j a 17 22 sit 1 3�,g Aws _ 3 o 2300 32.6 23oS �,30 v ,?300 a0� ,Da o 3 �� ago 0 3 Z)3c5o i 3C. 3 9- 00 M 3 C E .O V c� d U. 0 Cf C 0 N C [A DO vo X 4a r wlm.0 Cil to 0 FA .2 s� 0 I\jQD .02 0 000 G) 4 bp co Citp of Ofilbeboro Dry Solids for Sludge Hauling Date 1,3 GJ'A-V2 ? U3 Analyst Initials bb� Sbj 5or ez)A ......- ....... Dish Number -_. ..�. ` slL 0 too Source 51� °l� S�� h Wt. Dish & Wet Solid (g) S 014 • Q1Liq \01. Wt. Dish (g) 1p i3. FS 11 -7 S. -12).b\ 1 k e&11i��J Wt. Wet Solid (g) ��, p�j�j3 �.�E3s� ��.Ib�� .tom-�s� Wt. Dish & Dry Solid (g). 809I BED`l`-� b�. 1r'J�J 3 Wt. Dish (g) %5.11 0) U al . S J 1 QI 1 S. `�45$ �� S� 8cj • 1 I `�S Wt. Dry Solid (g) l0 5q2 C)ce- G`1 ,145ZP .1AU 3 3 •o'2j-� %Dry Solid ��, �� ��,CQ' �(j.bob Z��Z�e I�j•�I% Weight (Ib/ft) SZo.cc> (Operator Initials IOw ` cw Po�-k Q'Cf tp of ROW= Dry Solids for Sludge Hauling Date °1 23 3 Z 3 U (1� C Z� Analyst Initials J Dish Number Q gj0 100 Source slc,d . Wt. Dish & Wet Solid (g) •� 9c9 Wt. Dish (g) .S 03 lTi5- Iq5 Wt. Wet Solid (g) a I.RO(&y 11, 0114 1'-E • 1�I 3'-� Wt. Dish & Dry Solid (g) '60. 5) It C2 g--7. CIS Wt. Dish (g) aU.SI�� U • &II l ��j .IIq� Wt. 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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQOOO 1684 WWTP Name: Asheboro WWTP NPDES Number: NCO026123 Monitoring Period: From 7/l/2023 To 9/30/2023 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) Alt L B (Alk Treatment) 0 Alt. C (Prior Testing)[] == 7RT77iTgen,�s rl]7 Alt.D(NoPriorTesL) Process 7toFurther Reduce Patnogen7gs[3 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying 1:1 Heat Treatment 0 Thermoribilic 0 Beta Ray Gamma Ray Class Alt. (1) Fecal Density �„„ Alt. (2} Process to Significantly Deduce Path®gene ,„";� If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lune Stabilization Air Drying CJ Composting (,r 0 jAerobic Digestion Anaerobic Digestion E3 If applicable to alternative performed (Class A or Class B) complete the following monitoring data: N Parameter Allowable Level Pathogen Density L , MF-er-7 — Excee- Frequency Sample Analytical in Sludge immum Geo. Mean Maximum Units of Analysis Type Tech-nique Mi imum 2x 10tothe Sludge 6th power per gram of Fecal Coliform total solids CFIJ 1109 2326 177936 col/g 0 Quarterly C 1000 mpn per grain of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed: Alt. I (VS reduction) Alt. 2 (40-day bench) [%,�3 Alt. 3 (30-day bench) Ej Alt. 4 (Spec. ()2uptake) L-3 Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) 13 Alt. 8 (Drying - Unstable) E I Alt. 9 (Iniection) El Alt. 10 (Incorporation) [3 No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02'r .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both or the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman - Plant Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 02/26/2z H3 �11) 24;2� 1/19/2024 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (12/2006) laar L/uLc____ Dish # Wt Dish + Wet Solids, g Wt Dish, g Wt Wet Solids, g Wt Dish +Dry Solids, g Wt Dish, g Wt Dry Solids, g % Dry Solids Wt Dish +Dry Solids, g Wt Dish + Ign Solids, g Wt Ign Solids, g % Vol Solids Analyst,M ._ Dish # Wt Dish + Wet Solids, g Wt Dish, g Wt Wet Solids, g Wt Dish +Dry Solids, g Wt Dish, g Wt Dry Solids, g % Dry Solids Wt Dish +Dry Solids, g Wt Dish + Ign Solids, g Wt Ign Solids, g % Vol Solids Analyst X bate Dish # Wt Dish + Wet Solids, g Wt Dish, g Wt Wet Solids, g Wt Dish +Dry Solids, g Wt Dish, g Wt Dry Solids, g % Dry Solids Wt Dish +Dry Solids, g Wt Dish + Ign Solids, g CITY OF ASHEBORO Volatile Solids Reduction Additional Digestion (Option 2) 40 CFR Part 503 (White House Manual) Appendix D Revised 5-28-14 Checked by Moisture and Dry Solids Volatile Solids 9 41 _ '78 w034 5 rZoO. 200 t. 17 pa Q. Q0 Moisture and Dry Solids Volatile Solids Checked by Moisture and Dry Solids ,212' 20 Dav VSR 7.:Z. Sb . ........................... 9.ywv �. Volatile Solids 841. 3 3-7 -,;5 70 q Average Average Average City of Asheboro August Digester Pilot Plant Temperature Log (Record once per shift) 1st shift 2nd shift 3rd shift Date Time Temp. Initials Time I Temp. Initials Time Temp. Initials 1 2 psl 3� 33�' JC I5do :A N jjW 23 �. 64/ �,9 I 36`A 4*JW 3Gr ��- 4 ©L5`- is -A _�s It pew 5 �� . i %)cv 3 _. 6 07oo X • cs I if 42 36.2- mc,4 o?3oc) 35-- 2 R N 1W 8...... U70 �3, - ,�1� I406 35. S , Afl� _ a31� 3% . tom__ _ 9 0 70 q 3t • i ISo2 3!S C Al a3@ NA 10 U7i.5 i� C - � (S61 3 d333 3s.�6 4t7 /7 &5 35,1_ A���_ a3�3 .q 12 A-0 y 5�- 2 3_i S 3 S. 7 wt441) 13 7 3 s, 9 nj; ; 14 15 G s r'f g5. ESL' .23?- 16fi .35.9 a$ ��`�Ave"; 17 18 19 21 22 23 mPTM u x Cftp of zhibebovo Dry Solids for Sludge Hauling Date 3 Tszlt c 2) cl + Z3 Analyst Initials�`-'`��..� c�U� Dish Number 60 100 I Source Sl o,4 %e Wt. Dish & Wet Solid(gjbl�p93. 01 QO `7u� Wt. Dish (g)5 Wt. Wet Solid (g) �' �,� 1 �`{ •� �r`�JV� Wt. Dish & Dry Solid (g) " 1. �lSl�2 S l 'l`7 32 - ^.,1, Wt. Dish (g) � 11 `U� . �" S �S. ( �)2 Wt. Dry Solid (g) Z.0503 Z . c)u n t-o q % Dry Solid Weight (Ib/ft) �J . co Operator Initials W o Ln Nr O� LO 1.0 N M LO (O A T M 00 LO r r— LO 0 O O LO CA O O (0 O LO LO CO 1O C7 LO LO I` LC) (O LO 1 Vi � CO ❑'0LO r-Cl)M r'CO MIIM CV) MMMCl) (MCOmMM T Ct CO 'I` ; 100 10 r-- MOO N M N T Nr LO I— CV r C� I - C) - N O -41(0 ,00 �t CO O M LO ' r �, N , T N M M 'LO m (M d' ,T � LO '00'f� N : r-- r--F- 1` ' N n ti � I` r__ � 1` r__ 1` I, I- r- r- ti Il- � r- � P- ti ti I` ti ti h C O � I C,o O N OO -,;r M 00 O "It r-- O M 0)00 CCO N IICM N 00 N N LO O r r OO M r r T I r LO O to N r 0 C`) LO ;' CM N O't N r Lfj O N d M r r- M CO T O O 00 O r LSO j LO LO LO LO LO M 4 LO LO 6666 LO LO Ct c) - :r LO -;t LO LO CO LO r ❑ U) c E,O 0') 0') 0") O r N r O O Nt M M M N r T r r r r r r 104 E''O O O T T rN �' V' "T M M N r'O O r1r110 r r N N N N N OO N cocoM ('O V' M M M coco- I M M M M COM CO C) M CO CO M CM M M M CO N M r M ❑ N M ti M Lq UL I- LO (. 0 LA 00 r O O r t7 lD r LO O O V- LO O O 00 M cM M O M O co -t N LO M O 1` O LO LO I, ' LO LO 00 LO It LO T LO T LO O r M LO O N d �t M M N r O O r r r `- N N N N N T � 0'M M M1'M M M M� M Cl) C') COIM M C) M M M M (M M',O M co M M M M M co O Ch Qi T T T T r r r r r r r T T r r r T r T T T r r r r r r r r r O M v- r Q O .00 M 00 W I N O fl- O. M rl- N 00 E_ N N N N N (MCI N N 00 N N 1�. N 0) a O� O 00 Lt7 O 00 LO O r N T T r r T r �O T Ocl N LD O W M I O LO O LO LO O LO M M M LS) M O M LO O CO CO 00 CO 00 O CM 00 00 N O E M (M "I 00 O (0 ('M O N CO d) tt ',1- T 0) 00 t- M r O (O V- r,-00 O 0) M M M O 14' O M O T CO O 00 LO r (') LO N Iq1­ LSO O'1;T 00 r-- LO CO N N IT M O 00 I` LO O N O It LO 00 CD LO rl- T-OtisI [I�'V- �0)���'M h0� 001M LO 'O N O (O CO O'N CO 0ILO CO 00 N � M M M M M M M M M LO UON r N O O r r 00 LO N M 1(.0 0) N O LO N r 1• M N N (S) co M CO N CO LO I- N N 1­ r O LO LO 00 � O M CO CO [V CO O (O O �t N Na r 0') J '',r (V r '.r r r r j N T T r T O Z r M V- M M co ct Mqt ('M LO M N ,T O T O 00 N O O N CO N N N r LO mot M1qr 00 (n O O O O 00 r 0 CO 00 (O O 00 - CA r 1,- (0 r (p r (O O O O O ''.. O O O O O r r O O O O M_ M O O h 00 1 t M 00 LO N _O N N r r 0 0 0 O N O 0 0 0 T O O O O O O10 O O O O OO O O O'O O C0 0 0 0 0 0 0 0 O O'O O O O', L O O O Oi0 O O O 010'O O O (.10'O O O 0 O O O O O O a O O oZ O O O O ',O 0 0 0 0 0 O O O 01 O O O O O O O 00 IT 00 IN "q O0 O 00 N N 00 N OD IT q CV 00 E N O 00 LO LO r'T 00 LO � O M O 0)O 1` coIq O 0)N Ct LO r M o0 .(0 00 O I` (O I__ r__Ln (0 00 M (fl 1­(O 1­ M 1­ M M I` I` 0 < W r = COI LO (O c} 0) ; M rl- O IT LO LO M M! O (C) MN MU) CD I m O O 100 1 00 :r I-- M O T m LO 1 r O M NI r 00 00 M O Il LO LLOO N (O 0') N- LN() O CO CO TIr,O T O M O LO M O 00'LO O� 00 00 T O T QJ''� a N r N r r (O :T r r r T r T M m G T Z CD 00 I � � CO r r O �t Co LO CO M lb Z_ J N O 00 � M co,LO O O LO LO u) O (O LO r O0 Ii` O O M (O LO CA 1-QO COLO00(O IN 00 (DLO OO1`M'ct (OLOOMr (D00 Q(D 00 M ct CO N IT co 00 r,-O co00 0) 00 N 0)0 O N 00 00 (M Nt "T M ce) N IT M N r I` N M M d cM C) d 1 � F- OD " r I` M ct N CO 00 t I` I` OD N (O M ;T ;r OD N LO eM r r N CO O 00 1- r O ,;1.rM r CV 00 (O O� 00 0� (O O 00 M r t--00 'ITr 00 N M O I` � O N 1 M I— I` [­ Z U) O Lo N 00 O 00 '- LO 00 00 (O N N I'- r- 00 LO r d' OD (O T LO r O, M N LO O 1` O lb r (M O Cl) I,- r 00 O r- 00 O O V 00 O 00 10 N ti (O O M O N- CM CO co LO OC) J O U) 00 I` CO U) O CO Cr) N O O 00 q d LO r M 00 M O r T r O LC) CO O�C'oOT O� r- N LU 0 000 00 M ti (O O00 NO LO M j r 0) � tia 0000 0000 r 00 00 (OONO 0)j CO LO I` 00 000 10) N 00 � CM 00 O tt 1-- (O 00 O M N O M N M N N LOOT T 00 r r 1 M O _M (' 1 L') O LO LO LO 1.0 M IT LU L0 LLOO L� U CO O O LO LNO O M I "t ! LO 't L0O U.) 0 LO O Oo O'OOOOOOOO'00000�000�00000'O,OOOOO LOO ❑ O O O O O O O O O IO 0 0 0 O O O O O O ,0 O !O 0 0 0 0 T I I _ -- - 44 a 0 0 0 0 0 0 0 0 0 10 O' O O O O' O 1 c] [-] [" 1 f'1 n n r--i F-IN ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: City of Asheboro WQ Permit Number: WQOOO 1684 WWTP Name: Asheboro WWTP NPDES Number: NC00261233 Monitoring Period: From 10/1/2023 To 12/31/2023 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) Alt L B (Alk Treatment) 0 Alt. C (Prior Testing)[] == 7RT77iTgen,�s rl]7 Alt.D(NoPriorTesL) Process 7toFurther Reduce Patnogen7gs[3 If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Heat Drying 1:1 Heat Treatment 0 Thermophilic 0 Beta Ray Gamma Ray Class Alt. (1) Fecal Density �„„ Alt. (2} Process to Significantly Deduce Path®gene ,„";� If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lune Stabilization Air Drying CJ Composting (,r 0 jAerobic Digestion Anaerobic Digestion E3 If applicable to alternative performed (Class A or Class B) complete the following monitoring data: N Parameter Allowable Level Pathogen Density L , mT-er-7 — Excee- Frequency Sample Analytical in Sludge immum Geo. Mean Maximum Units of Analysis Type Tech-nique Mi imum 2x 10tothe Sludge 6th power per gram of Fecal Coliform total solidCFIJ 1019 1068 1125 col/g 0 Quarterly C s 1000 mpn per grain of total solid (dry weight) Salmonella bacteria 3 MPN per 4 grams (in lieu of fecal total solid (dry coliform weight Vector Attraction Reduction (15A NCAC 02T.1107) - Please indicate alternative performed: Alt. I (VS reduction) Alt. 2 (40-day bench) Alt. 3 (30-day bench) Ej Alt. 4 (Spec. ()2uptake) L-3 ::L Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization El Alt 7 (Drying - Stable) 13 Alt. 8 (Drying - Unstable:) d 3 Alt. 9 (Iniection) El Alt. 10 Uncorporation) [3 No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T.1106 and the vector attraction reduction requirement in 15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both or the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Michael R. Wiseman - Plant Manager Brent Collins; Director of Technical Services Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) 02/26/2z H 3 � 11) 24;2� 1/19/2024 Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T. 1102 (26) DENR FORM PVRF 02T (12/2006) Wt Dish, g Wt Wet Solids, g Wt Dish +Dry Solids, g Wt Dish, g Wt Dry Solids, g % Dry Solids Wt Dish +Dry Solids, g Wt Dish + ign Solids, g Wt Ign Solids, g % Vol Solids Analyst Analyst Date I l • 22 2- Dish # Wt Dish + Wet Solids, g Wt Dish, g Wt Wet Solids, g Wt Dish +Dry Solids, g Wt Dish, g Wt Dry Solids, g % Dry Solids Wt Dish +Dry Solids, g Wt Dish + Ign Solids, g Wt Ign Solids, g % Vol Solids Analyst ay ate IL122? Dish # Wt Dish + Wet Solids, g Wt Dish, g Wt Wet Solids, g Wt Dish +Dry Solids, g Wt Dish, g Wt Dry Solids, g % Dry Solids Wt Dish +Dry Solids, g Wt Dish + Ign Solids, g Wt Ign Solids, g 96 Vol Solids ` 14 1 q .I Volatile Solids Checked by n "G( (O Lt. 0 Checked by Moisture and Dry Solids l l . l (D FEZ 2. (p IL. 2�.. 78 ,� °3.2D Volatile Solids 2tp3 -?� i3 08 �78.(n�-22 .-��" o.22z� �._.. Moisture and Dry Solids 1 �� •� �", Volatile Solids y °1s 313 7N O� 1 Checked by �� � VSR = VS,,;g;„ai - VSf,„,, VSoriginal - (VSoriginal X VSfinal) IIIIIIIiwm Average 5 I rn7 Ca y1. (Q 4 1 (e 1 • i'5' lb 20 Day VSR .•i 3 11 Average i ®l 40 Dav VSR 31 1_ `72�3 , 3s.5 I4•v.�.�' )4�y 3�2� � � �3ov �S_� �'� ...... 2 0,�'00 33 ifl o 19 o0 35.0 .� . � 3 3,5 -T 3 GG `� 3Y� Isla j 3� J _ a�a� 3y• 4 V7t5 Z 'c \ !qL4L � Z3C�S 311. 5 0� .3cj. _ ° , 1 Nyl� 3`I• III ` a3oc) Ti �L _ 7 (o5Z. 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C) C14 00 E z03 z03 w C4 E co co L) 0 0 CL a) a) 0 % a C-4 .2 cn (0 .2 In tm S ca F- > Cl) 0 aL) UJ 0 \ C-) C) \ \ , 0 (A 6M4 ca LO LU) 2 m z cn —i uuua g e s Final Audit Report 2024-02-26 Created: 2024-02-26 By: Brent Collins (brent.collins@emaresourcesinc.com) Status: Signed Transaction ID: CBJCHBCAABAAHJzOhQPS986VWSEZinLS3WIgeJifU2yL Document created by Brent Collins (brent.collins@emaresourcesinc.com) 2024-02-26 - 2:44:12 PM GMT- IP address: 206.85.202.26 Document emailed to Mike Wiseman (mwiseman Ca)ci.asheboro.nc.us) for signature 2024-02-26 - 2:44:16 PM GMT Email viewed by Mike Wiseman (mwiseman@ci.asheboro.nc.us) 2024-02-26 - 7:36:57 PM GMT- IP address: 71.2.234.91 Document e-signed by Mike Wiseman (mwiseman@ci.asheboro.nc.us) Signature Date: 2024-02-26 - 7:37:44 PM GMT - Time Source: server- IP address: 71.2.234.91 Agreement completed. 2024-02-26 - 7:37:44 PM GMT