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HomeMy WebLinkAboutWQ0036561_2023 Residual Annual Report_20240229Initial Review Reviewer nathaniel.thorn burg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2023 Permit Number (IR) * WQ0036561 Applicant/Permittee City of Danville Email Notifications Does this need review by the hydrogeologist? * Yes U No Regional Office CO Reviewer Admin Reviewer Wanda Gerald Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Brent Collins Email Address* brent.collins@emaresourcesinc.com Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 3363993646 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0036561 Has Current Existing permit number Applicant/Permittee Address* 279 Park Avenue, Danville, VA 24541 Facility Name* City of Danville Class B Residuals Program Please provide comments/notes on your current submittal below. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2023 Danville Annual Report - WQ0036561.pdf 16.58MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 2/29/2024 City of Danville 2023 Annual Report Residuals Land Application Permit No. WQ0036561 Prepared By: EMA Resources, Inc. Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 It MI. � A, sources, Inc. February 27, 2024 DENR/Water Quality Section Non -Discharge Compliance Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Re: 2023 Annual Report — City of Danville, VA Treatment and Land Application of Residuals Permit No. WQ0036561 Dear Sir or Madam: Enclosed is the 2023 Annual Report for the above referenced land application permit. During 2023 EMA Resources, Inc. land applied 454.22 dry tons of wastewater residuals to 220.48 acres of private farmland. Please contact Brent Collins - Director of Technical Services if you have any further questions regarding this report. Sincerely, Brent Collins Director of Technical Services brent.collinsLemaresourcesinc.com Phone 336975191441 — Fax 336975191442 755 Yadkinville Rd — Mocksville, NC 27028 ANNUAL LAND APPLICATION CIUMFIC/U105i RMANM : INQ Id"atrmnrwdi N:, VWQ00365M County: Puusylrranpa County,, VA 'eat-:: 2023 pw acihly Naaine ( �w shown on Ilp permit): City of p tairivifle, I wartpnaadwde II lhl land ppmppa'Iddiapaa ;maaunA gyllpanm"«:at;maur:; h:,p 4 pCw �awwa:nrwaw aw pynw;. d''IlkaAaauGnA�:; r�u.��Tr p land d aallp'plwpl cat;p mnc or remwdiaduuaaldat a:as aadldaawed. by tfiie permit awceturre d (hundumpg the post caada� n de r year? Ed yes C3 No - pNt'' lea, spinriilpi Part A,and Part Bond III'muCroaam:.m^anad WWI C AlmNirresidualswere pgenw ante d but not land aplallp'He d, IlpaWase aata:sch an an ppwlllamaadamunc on 11114OW Ville ransi d.unaadw wire llhnaauuadl.d dd., d wataad mnuarrmidbwi abd ai(.p adnw autuw:a n du p p n ern �Ihn �, nnnn�' 6 Tow! wd nnunnnndbw n or news umtn w ad dwan p innrd apapppiw alionu during the yw,nn 7 �FoZ,apnrriounQnf(hy Ums hnNd anniiIthe, year dbn�upa,pr i ar-I " 1`1 2 � ....�.. WJ nundwn o acres utdkos Cpan Qubnpicatibn the ywar22(h4. LiipL um�ian iu 111 :°��� yiiiy uau ;mmnunn nmo�:n pw`n'aaciphicty was conrmmppalddiaaurmtduit-II nc araatlemn daaaI 2023 wwxpc b aaplpl e moncCddifloirrns of t.11he land a apmpp'heaatadcannrrn Ipmerncmmdit. Oncm°IDmium�uC g but not plucm�up��:muay to i1m.einns 1-1 betlaw' r) n«wmaumnd pkmyr�dii , Division of Wateir Qm.iunmplpity�. Yes 0 No dt''n o Ilpalllenu.aaaa, ppanrnaw�i de as written mdescripput.daanrm lyy tll e Facility Was not a ornmppmddaannct;, the adauhm, and explain conrnnaa e aacHwanma taken., k.euan„ p ( Or dy residuals, approved p(br Chia p-awarrrndt, wwcre aap'plpapdw d to the p errnndtta,wp sites, 2(Sodp IA wu s aajuuste d as n spajdhe d in to p erunndt and ppnrrnw '4wms aapropwdda.;nd or nw;u;npe dd to anchua.; T aa. mAl pap -p oral 4*0 CdA or the ➢'drwdt, sppwaa,pdde d dmn the ppernnin- :h( A nunin d soHs aanaap sis wwamw, pe dwamrrrne d on each stings nu.,wx1ving uw°aannduu ds during the. past caapw;rirdaa yc;aar and t.prc (.h( colppuca„ of paaboraatabn y rwstflts are attached. `) Annual "IC"C; 1) analysis (dd equudrrwnad( was qno dwbmrrie d and tdnrce (:d( copies wbd w°atmt'ddde d llayd or'.1>G0ry iw,.auudtar "Arwa att.aawapnwnwd. p ) AN other rrnwbmidtwarnripp vaibb Ippondwbrrrmiew in accordance wvdt n to ppormmidt and wprwamtew a u.umirny, the year aua°,a required Qania t'pnirwnwr (d( coppics wbd e rtdd'' e d daboraAA'Ory rrw,tauadtwa acre aatilarChe d. 6) The Why y added not a;waaeed n:ny aap'd-re Pappdaa4,uaA y;anru mi-itram4ion dWE in p 5A 7" CAC, 02.1" . II l05(aa) or the, pyandpuutaarnt': p.,wbaaadnunpp Wass in p .` A INC AC:; tDv. .d p 05(pb( (aapappOnad-de to 40 C"FR Illaart; 503 iegu hated 1,a dpdtics). 7( AN genCrrap requuire nnentaa in an.S specified in the p_i miad App:ppdw;aatdwbma Permm h were w;wwunupplldedl wwd,h (aipappd'dw°drb1lw, to dO (°d'R d'"anrt 503 rwguullaat.wd Wntdwno. ( AN nwuoraptorprnpy and reporting requu.drwriennts in d 5A 1" CAC: 02T .d p p d wow r,wanrrnp lied with (a.p:ppppuw;W to ddd 011 Part, 503 rwjuupaat.wnwd MWO. 9( .AN wbpperaauuwpnna"a and nrrrraallrut, it arw e requanrua naMrin in We ppa.,irrrnat, ww m complied wit wbr, in we t",aaa'uw wpd as deviation, pprnwnr aautVn ykaatdwbrn was naxeivend mom the p ddwtdaaon apd'` & w r Quuaap , pCt( No w°-w�:wd auve nt:daani o (hound NO= Quanpdty Suiriwdaarwdta occurred at as manonnpt.wbrunny aneH or wnxpapllau.nnautpw:annw„ abd° violations arc auAL'I.w;dnead to mcluuwde a a.daprwapaprd�'Ia.w, auw°t.dw: ns aa.mnwd rerne dlaationns,, p d "w<"w etaaaive pwer wwass mnnaa � pt p � g " pb � "". � p� rest du:a11ris., aas d. mm�lf�apn'nw",m' ran'n rd'D;pR,m �;rC�b. n�Va8mnad .�&;TMnumw;mnt"�1&0 b w"r7�w,bml�n&;TMm' wamn w"�L�; n „nt,w" rw";�;w;mm� . specified in the ppe nnn'ut. p y( No naanawd'd orrw adwpuaais dirabrrnn We application sntw,a onto aawpow°-w,m pbrabppett;y or ruw,aa:rday suarface voters has occurred, p 3) .All pnunllhr requupmwiinnwnntw as aupp&dhw a:d on the pmpennU vxrwi maintained during each a apppwpdw°,aatpwbnn wbt nwtskiuuaahs. I% rt: C - d Tm tmt` ca.t;daaunc a aay ana:M j, under ]d ein aaltt,y aut' Itaaww, that the above idurrnt"aauurmnwmaaUaauur is, to tllhire best of' iney Ilkinnaaw%rda dge and p efiiel', true, accurate, aanncad a°auannnllpuldan at, tl -an; as same that Chere are sipgnncditI Ip enaadtaies t'hrunr wuiullkam it,tdiurrnp"g d`aalllse mnradaunrucamaatiourm, including the plaausMpkroaphhy of tiuirrma;s and iianmpl risaumnutmne nt For knowing Matdonnnaa.," Al.nniJolhnson- Divi;„ionnDuoettorot'Wi(cr&Wiscve4cr'�roatnnona A�nnhi n �A�1 2!®1i24J24 Perrnnntt,w,c, Naarrruwi and "Il"ntde (type, nwn print) Signature, of p erinndttee, p utw, ni �" d /7" d /2024 ------------------------------------------------------------------------------------------------------------------------------------------ awdpunatuure u:DCdnrcjraa.rcra" Date, d"tdpaiiautu:ure o h_,annwd Ap;ppplier Dale (dd`wddddwtmwtmrrt: mom Ihn- midi ce) (dd wpdd'dbrennt Rom d"w°mMdt.ce and IIIDnw;paui r) ,V p'repp«arer is wdatdhrrn A in 40 C'p R dn' a 5031 (0 aeons] 15A NC AC:, 02 h" .1 102 (26( I)ENR p"'Olf'M ACF- 2006) 11 —4 m 11 --- ------- .............. .... .... .............. -- ...... .. .. ...... ...... .... .... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... ...... -------------- ------ ------ ------ ------ ------ ------ ------ ------ ------ ------ ------ ------ ------ ------ ------ all ....... ....... ....... ....... ....... ....... ....... ....... ....... ....... ...... ...... ...... 5 lC.r.b CV) 11 fl"b o 'It" cn lr.b 7"t Ir, r': I[— t CA ---------- ('?'d ! . .. .. -------------- ---------------------------------------------------------- . . f � Rel .............. ...... ...... ...... ...... ...... ...... cl, ...... oc ...... C, ...... ...... 11,­b ...... CZ) ...... �= ...... CZ) CZ) ...... C,'� ...... cn , C_ � I lf`� ("� ('�) in r, lit 00 i—o C>0 v� lry in cg� it., , : j C, SI! .... .. .... ...... ...... ...... ...... ...... ...... ...... ...... lit ...... ...... ...... ...... ...... (DI ------- --- ---------------------------------------------------------------------- I P CA CD xi /I x /I ---------------------- ------ ------- ------- ------- ------ ------ ------- ------ ------ ------ ------ ------ ------ ------ ------ 4`2 ----------- CD CC.) (114 I U Icy C.Y .............. ---- -------- .............. ...... ....... ...... ...... ...... ...... ...... ....... ...... ....... ...... ....... ...... ...... ...... ...... ...... ...... ...... ...... ...... ....... ...... ...... ...... ...... ...... ---------------- -------------------------- --- -------------- ------- ------- ------ ------ ------ ------ ------ ------ ------- ------ ------- ------ ------ ------ 0 PL, - CPp --- --- ----- .............. ...... ....... ...... ...... ...... ...... ...... ...... ...... ...... ....... ...... ...... ...... U ND CA �Z_D , �'A �'A I[,,- cz� i'' a .7t' 1[". C Cl I[ ',- M C, ------- ----- ---- --- --------- rl .............. ...... ....... ...... ...... ...... ...... ...... ...... ...... ...... ....... ...... ...... ...... CA ------- ----- ---- --- ----- ---- ----- ---- ----- --- i—C or .............. ...... ....... ...... ...... ...... ...... ...... ....... ...... ....... ...... ....... ...... ...... 00 lC— (DI 7t, IM (DI Ell �yyE-I 14 ---------- CN CN ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 50.70 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: Nettie Blackwell Predominant Soil Series: FbB2 Acres Used: 20.33 Acres Permitted: 20.33 Site #: CS06 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1. • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1� • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1� 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1� 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • • 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� • �1, M� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• Total ' • 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ; e. e 4 � 2�- Signature of Land Applier 1/21/2024 Date DENR FORM MFLSF (12/2006) O U O O d zP� v w w Q cs N a Q Q O O O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 o Z Z o 0 0 0 0 0 0 0 0 0 0 o 0 0 0 0 0 0 0 0 0 0 a O N O O O O O O O O O O U00O O O O O O O O O O E N N w o Ammonia N N M Nitrogen E C Ay�l N M N a E w O O O a Mineralization M M Rate*** N o ry 0 0 ti Volatilization Rate** 0 0 r r. C o 0 0 k, (n Application o 0 0 Method* O o 0 0 O a i V V ti 00 ti C. U a «S � � Z Z Z o 0 � U U Qy Q O o C O O C) 'CS 'CS O 0 00 C) N z (D N U U N Z a ujuOw3112 I C) Q a 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 119.77 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: Nettie Blackwell Predominant Soil Series: FbB2 Acres Used: 45.87 Acres Permitted: 45.87 Site #: CS06 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • • 1 1� • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� • • 1 � 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ®� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ; e. e 4 � 2�- Signature of Land Applier 1/21/2024 Date DENR FORM MFLSF (12/2006) C` OC Cn C` OC Cn O ZP� U w w w w a N --i DD Vl M M � � 00 00 0 0 0 0 0 0 0 0 7 M cC 'CS Y l� t` t` t` • • Z N N N N r Ammonia J N N N N io0 Nitrogen Er. M M M M N N r. r-, 00 a Mineralization 0oo `' Rate*** o 0 0 0 o N N M ti Volatilization o Rate** o 0 0 o a C O o 0 a k, fr; Application 0 Method* O o O V U' V1 V1 V1 V1 V1 l-- M 00 00 a V V V \ O a O N O N ti r. O d '-' M M O N � N 1.0 �C Z Z Z Z Z o 0 0 � U N Qy Q N 00 � 01 01 0 0 0 0 0 0 0 0 �O M 01 o Cn U CZ O O O O O O 'LS 'CS O N "C3 U U N Cn Z 3 U 7 11111OWJO F PLI U PL P I C) Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 69.05 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: James Blackwell Owner: Nettie Blackwell Predominant Soil Series: FbB2 Acres Used: 26.89 Acres Permitted: 26.89 Site #: CS06 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • • 1 1�: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1�: • 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ; e. e 4 � 2�- Signature of Land Applier 1/21/2024 Date DENR FORM MFLSF (12/2006) C1 OC N C1 OC N O U CZ H O ¢ U N O O .—i Uby ..U. Pr O O O U N N N a FC15 cs N a Q Q Q o 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 0 O O O O O O O O N 7 U m 00 00 � y y «S 'CS � Y l- � � •❑• y O r7-+ N N N 2i W r7-+ w r Ammonia N N N 00 00 0O Nitrogen E M M M a Y O O O O O O � vi vi a Mineralization 0 � � Rate*** o 0 0 o 0 o M ti Volatilization o o Rate** o 0 o a O O O a k, Application CI,CC o o Method* O o O o � N N No V, V V V O o N ti p a O O U �r. v N BBB N Z Z Z- Z O O � U w N vi O O O O O O O O O vi vi N 0 U NCn U O cs p o 0 0 O o U U N Z '� zo 3112Q � � o I U Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: Margaret Hatchett Owner: Margaret Hatchett Predominant Soil Series: Acres Used: 27.76 Acres Permitted: 27.76 Site #: CS12 Field #: 16.18 ToC 2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total D 0000000001118 Event 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 1 . • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 � • 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 11 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11 � 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �� 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ®® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ; e. e 4;:; � �1- 1/21/2024 Signature of Land Applier Date DENR FORM MFLSF (12/2006) IN cv :M :M w I'D OC o � d N �4 w O a U bq O U 0 s. IZ YC L^+ O Sr U U CZ H O ¢ N O O .-i Uby ..U. O �+ N O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 U O O O O O O O O O O O O d a O O O O O O O O o 0 o r a o o 0 0 0 0 0 0 0 0 0 0 U M O O O O O O O O O O O M M CC$ 'CS Y � •' Z Z N �' N Ammonia � 00 00 O Nitrogen E a O CIO O O O OOp a Mineralization M 0 Rate*** o Z o o 0 0 ti Volatilization . ) Rate** O r. o o 0 0 0 0 a k, (n Application CC o Method* O o 0 0 0 0 aN V O a O In N O O O ti O 'CS U 00 CO Q U Q O y O O vMi O O ti .u, r- U OY 00 M U Z Z o 0 0 � U U Q Q N 00 O O O O O O O O O O O In N r 00 O O O O O O O O O O O 'CS 0 � M C N U Z O U 0) O O dF v° o (D U U N Cn Z a u111OW I N Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 36.69 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: William Hatchett Owner: W.H. Hatchett Predominant Soil Series: FbB2 Acres Used: 17.47 Acres Permitted: 17.47 Site #: CS12 Field #: 5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D - Event 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • • 1 1� 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 •• 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 ®' 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • 1 Total ' • • •:1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • •:1 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ; e. e 4 � 2�- Signature of Land Applier 1/21/2024 Date DENR FORM MFLSF (12/2006) O IN OC OC IZ U H O ¢ U Cn N O O CZ cs N a Q Q O O O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 .O. O Z Z O O O O O O O O O O O U O O O O O O O O O O O 00 Z Z c w r Ammonia N N 0 Nitrogen E N c! O a Mineralization M M O O �C � Rate*** fr, ry o0 o M ti Volatilization C Rate** 0 0 r. o o 0 M 0 a k, (n Application O M n Method* O o 0 0 N n n o r a i V V p o N ti a C N N p U a w Z Z Z a 0 O 0 O 0 O M U Qy Q O pp O ^C$ o 00 00 N U CZ U (n O O O 00 o o o O U cs FBI � o CZ U U U N Z .� I U Q 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 141.33 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: David Sartin Owner: David Sartin Predominant Soil Series: ToB Acres Used: 75.78 Acres Permitted: 75.78 Site #: CS14 Field #: 1 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� 1 11• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 11• �® 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 1 :1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 :1 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 •• 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1• 1 1� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1� ® • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • Total ' • : : 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ; e. e 4 � 2�- Signature of Land Applier 1/21/2024 Date DENR FORM MFLSF (12/2006) OC C` Cn C` OC C` Cn C` O ZP� U w w w w w a N o O O O O O O O O Z Z Z Z Z o 0 0 0 0 0 0 0 Z Z N N N N N r Ammonia ..... N Nitrogen �� M M M M M A, N 00 N O a Mineralization M M M M M O o o Rate*** CC L+ Volatilization o Rate** o 0 0 0 o a C O o O a Application Method* O o 0 0 N N O M a v v v v v ti V V ct3 '� M 00 M Z Z Z Z Z Z o 0 0 � U N Qy Q U O N r N M 0 0 0 0 0 0 0 Cn O M 0 O o G1 G1 G1 G1 G1 M M M M M C Cn U CZ O O O O O O o O o o 0 0 N 'CS (D N N OC . CZ N o CZ U U U N Cn Z CZ - v T��UO� I C) Q a 0 0 N N LL U) LL 2 O LL z W 0 ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Danville Total Dry Tons Applied (Annual): 20.50 Permit #: WQ0036561 Cation Exchange Capacity (non 503 only): Operator: David Sartin Owner: David Sartin Predominant Soil Series: FbB2 Acres Used: 6.38 Acres Permitted: 6.38 Site #: CS14 Field #: 3 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- phorus Annual Heavv Metal Field Loadings (Calculated in lbs/acre): Total• D Event 1 1: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1: 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 • 1 1• 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1• 1 1 • 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 • • 1 1 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1 •• �� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1: 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 1: ®� 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 Total ' • �1 • 1 111 1 111 1111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 1 111 �1 • • -I certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". ; e. e 4 � 2�- Signature of Land Applier 1/21/2024 Date DENR FORM MFLSF (12/2006) OC M M OC M :M :M N �4 w O a O Sr O s. ij OC OC SE yc O Sr U U CZ H O ¢ U N O O U by O �+ N O o O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 O 0 U O O O O O O O O O O O O d ' 00 00 '• O O O O O O O O O O O O � N � Y 1 � •' E N _ ^ Z Z w Ammonia Nitrogen E Cr Z w O O � a Mineralization M O .-1 Rate*** O Z o O o M CC L+ Volatilization ) o o Rate** O a O o O a k, Application o 0 Method* O o 0 o O aN a O N v o ti 0 ti M � U w Z Z o 0 0 � U N M_ O O O O O O O O O O O vi O O O O O O N DD N O � 'CS 0 � N U CZ U (� 00 O O O N U NS'r z (D N U U U N Cn Z a ujuOw zo 3112Q � o I U Q 0 0 N N LL U) LL 2 O LL z W 0 mil , 4/19/2023 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 23-094-0014 Project Description: VPDES Permit# VA0060593 Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 4/4/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Brandi Watson Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 14 (2) Waypoeint7621 Whitepine Load, Richmond, VA 23237 Main 804-743-94010 Fax 8 4-271-6446 ANALYTICAL wo, w,waypointanalyticaLc m Sample Summary Table Report Number: 23-094-0014 Client Project Description: VPDES Permit# VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 9045D WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-2320 B WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 6010D WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 4500NO3F-2011 WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SW-7471B WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-4500-NH3C WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-4500-NH3C-TKN WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-2540G WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 SW-9045C WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 SW-7.3.4 WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 SW-7.3.3 WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 ASTM D93-80 WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 SW-1311 (ZHE) WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 SW-1311 WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8270C WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8260B WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8151A WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8081A WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 7470A WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 6010D WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61588 Matrix: Solids Sample ID : LTS A -Basin 23-1245 A Sampled: 4/3/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Potassium 3980 mg/Kg - dry 250 1 04/07/23 06:51 BKN 6010D Magnesium 3550 mg/Kg - dry 125 1 04/07/23 06:51 BKN 6010D Sodium 17700 mg/Kg - dry 625 1 04/07/23 06:51 BKN 6010D Iron 30300 mg/Kg - dry 250 1 04/07/23 06:51 BKN 6010D Zinc 2390 mg/Kg - dry 31.3 1 04/07/23 06:51 BKN 6010D Ammonia Nitrogen 22400 mg/Kg - dry 2500 1 04/06/23 05:50 JPJ SM-4500-NH3C Nitrate +N itrite-N <125 mg/Kg - dry 125 1 04/11/23 12:44 ZBD 4500NO3F-2011 Cadmium <2.50 mg/Kg - dry 2.50 1 04/07/23 06:51 BKN 6010D Chromium 43.3 mg/Kg - dry 6.25 1 04/07/23 06:51 BKN 6010D Mercury <4.70 mg/Kg - dry 4.70 1 04/07/23 11:40 FDS SW-7471B pH 7.3 S.U. 1 04/10/2311:30 HBT 9045D Molybdenum 9.78 mg/Kg - dry 6.25 1 04/07/23 06:51 BKN 6010D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 60800 mg/Kg - dry 2500 1 04/11/23 09:45 TKM SM-2320 B Total Solids 3.97 % 0.010 1 04/10/23 14:09 JLS SM-2540G Aluminum 29300 mg/Kg - dry 125 1 04/07/23 06:51 BKN 6010D Selenium <12.5 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Sulfur 12900 mg/Kg - dry 250 1 04/07/23 06:51 BKN 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 14 ,�f�AL4'�i ICAL Wayp to 79434 Inframark Project A/P Northside WWTP Information 229 Northside Drive Danville , VA 24540 Report Number : 23-094-0014 . Lr PII 0 . 7 �� Tp• Main 43444 www.waypointanalyticaLcom VPDES Permit# VA0060593 REPORT OFANALYSIS Report Date : 04/19/2023 Received : 04/04/2023 Brandi Watson Lab No : 61588 Sample ID : LTS A -Basin 23-1245 A Matrix: Solids Sampled: 4/3/2023 8:05 Moisture 96.0 % 0.010 1 04/10/2314:09 JLS SM-2540G Total Kjeldahl Nitrogen 71000 mg/Kg - dry 6250 1 04/07/23 11:00 CLP ;M-4500-NH3C-TKlN Phosphorus 22500 mg/Kg - dry 125 1 04/07/23 06:51 BKN 6010D Calcium 16500 mg/Kg - dry 1250 1 04/07/23 06:51 BKN 6010D Manganese 900 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Copper 440 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Organic N 48600 mg/Kg - dry 6250 1 04/06/23 05:50 CALCULATION Nickel 55.0 mg/Kg - dry 6.25 1 04/07/23 06:51 BKN 6010D Lead 48.5 mg/Kg - dry 7.50 1 04/07/23 06:51 BKN 6010D Arsenic < 12.5 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Total Volatile Solids 52.1 % 0.010 1 04/10/23 14:09 JLS SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61589 Matrix: Solids Sample ID : LTS A -Basin 23-1245 B Sampled: 4/3/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sulfide (Reactivity) <25.3 mg/Kg 25.3 1 04/13/23 10:30 CNB SW-7.3.4 Cyanide (Reactivity) <0.125 mg/Kg 0.125 1 04/12/23 10:30 CNB SW-7.3.3 Ignitability >96 degrees C 1 04/12/23 04:45 JFM ASTM D93-80 pH Qualifiers/ DF Dilution Factor Definitions 1 04/17/2317:03 CNB SW-9045C MQL Method Quantitation Limit Page 5 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61590 Matrix: TCLP Sample ID : LTS A -Basin 23-1245 C Sampled: 4/3/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP Metals Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP Pesticide Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP SVOC Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP VOC ZHE Extraction Combined 1 04/10/23 13:00 ALM SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L675452 04/11/23 13:52 Prep Method: 3015A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 04/11/23 19:04 JTR L675662 TCLP Barium <0.250 mg/L 0.250 1 04/11/23 19:04 JTR L675662 TCLP Cadmium <0.0500 mg/L 0.0500 1 04/11/23 19:04 JTR L675662 TCLP Chromium <0.100 mg/L 0.100 1 04/11/23 19:04 JTR L675662 TCLP Lead <0.100 mg/L 0.100 1 04/11/23 19:04 JTR L675662 TCLP Selenium <0.500 mg/L 0.500 1 04/11/23 19:04 TJS L675662 TCLP Silver <0.0500 mg/L 0.0500 1 04/11/23 19:04 JTR L675662 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 6 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61590 Matrix: TCLP Sample ID : LTS A -Basin 23-1245 C Sampled: 4/3/2023 8:05 Analytical Method: 7470A Prep Batch(es): L675539 04/12/23 07:55 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 04/12/23 13:42 FDS L675724 Analytical Method: 8081A Prep Batch(es): L676046 04/13/23 17:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Endrin <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP gamma-BHC <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP Methoxychlor <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP Toxaphene <0.006000 mg/L 0.006000 10 04/14/23 16:58 VIC L676321 TCLP Chlordane <0.004000 mg/L 0.004000 10 04/14/23 16:58 VIC L676321 TCLP Heptachlor Epoxide <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP Heptachlor <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 Surrogate: Decachlorobiphenyl 64.86 Limits: 36-116% 10 04/14/23 16:58 VIC L676321 Surrogate: Tetrachloro-m-xylene 60.58 Limits: 25-123% 10 04/14/23 16:58 VIC L676321 Analytical Method: 8151A Prep Batch(es): L676065 04/14/23 18:00 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 04/17/23 23:29 VIC L676737 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 04/17/23 23:29 VIC L676737 Surrogate: DCAA 65.80 Limits: 20-120% 1 04/17/23 23:29 VIC L676737 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 7 of 14 Waypoeinto ANALYTICAL 79434 Inframark Project A/P Northside WWTP Information 229 Northside Drive Danville , VA 24540 Report Number : 23-094-0014 7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 www,waypointa nalyticaLcom VPDES Permit# VA0060593 REPORT OFANALYSIS Report Date : 04/19/2023 Received : 04/04/2023 Brandi Watson Lab No : 61590 Matrix: TCLP Sample ID : LTS A -Basin 23-1245 C Sampled: 4/3/2023 8:05 Analytical Method: 8260B Prep Batch(es): L676130 04/13/23 08:23 Prep Method: 5030B Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Carbon Tetrachloride <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Chlorobenzene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Chloroform <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP 1,4-Dichlorobenzene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP 1,2-Dichloroethane <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP 1,1-Dichloroethene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Methyl Ethyl Ketone (MEK) <0.200 mg/L 0.200 1 04/13/23 13:07 ASH L676139 TCLP Tetrachloroethene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Trichloroethene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Vinyl Chloride <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 Surrogate:4-Bromofluorobenzene 92.2 Limits:71-137% 1 04/13/23 13:07 ASH L676139 Surrogate: Dibromofluoromethane 90.0 Limits: 70-128% 1 04/13/23 13:07 ASH L676139 Surrogate: 1,2-Dichloroethane - d4 116 Limits: 63-136% 1 04/13/23 13:07 ASH L676139 Surrogate: Toluene-d8 93.8 Limits: 70-130% 1 04/13/23 13:07 ASH L676139 Analytical Method: 8270C Prep Batch(es): L675936 04/13/23 11:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP 3&4 Methylphenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP 2,4-Dinitrotoluene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 8 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61590 Sample ID : LTS A -Basin 23-1245 C Matrix: TCLP Sampled: 4/3/2023 8:05 Analytical Method: 8270C Prep Batch(es): L675936 04/13/23 11:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobenzene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Hexachlorobutadiene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Hexachloroethane <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Nitrobenzene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Pentachlorophenol <0.0500 mg/L 0.0500 1 04/13/23 20:12 VBW L676114 TCLP Pyridine <0.0500 mg/L 0.0500 1 04/13/23 20:12 VBW L676114 TCLP 2,4,5-Trichlorophenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP 2,4,6-Trichlorophenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 2,4,6-Tribromophenol 65.0 Limits: 42-102% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 2-Fluorobiphenyl 57.5 Limits: 24-86% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 2-Fluorophenol 27.3 Limits: 13-37% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 4-Terphenyl-d14 75.0 Limits: 30-122% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP Nitrobenzene-d5 60.0 Limits: 25-78% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP Phenol-d6 17.1 Limits: 9-27% 1 04/13/23 20:12 VBW L676114 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 9 of 14 to Way� PA ► x �... , Main .04.40, Fax 04,,4, www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES Permit# VA0060593 Lab Report Number: 23-094-0014 Date: 4/18/2023 Separatory Funnel Extraction 8081 Method 3510C Sample 61590 (LTS A -Basin 23-1245 C) QC Batch No: L676046/L676046 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction 8270 Method 3510C Sample 61590 (LTS A -Basin 23-1245 C) QC Batch No: L675936/L675936 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis Method 601 OD Sample 61588 (LTS A -Basin 23-1245 A) Analyte: Aluminum QC Batch No: L674758/L674295 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 61588 (LTS A -Basin 23-1245 A) Analyte: Iron QC Batch No: L674758/L674295 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 61588 (LTS A -Basin 23-1245 A) Analyte: Potassium QC Batch No: L674758/L674295 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 10 of 14 Way A.4, k L.. Main 804,d "q 44.. •' Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 23-094-0014 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IDavid Lennon Date & Time: 04/04/2023 13:16:47 Page 11 of 14 N. ..... .... . . ..IM Page 1�1'1'1').f 14 LunuapqAj%N wnivapS Ain ojo..- .)�Uasjv peal P13N ujnit,uo.jqD wniLupeD Duq asaueguevq —'. ujriutwniv — MOM WnIpos on" Lunisauft�Ni jnjjnS wn'SSP10d snjo4dsOI4d (uopejn:)je3) Ua2OJIN:)'UL'SJO1 E? m Ca se IPIN + alOJIN Ua3OJI!N-eRJOWWV - NNII SISZSI Oj v SWI -",EZ u1seq V Srj- :aIdweS (VIEVU juno3:)V VA 4uiodAeM) dIMM VA'alIjAue(I njetuej;ul A01 sisal SpIlosoig pajinba)j Page 13 of 14 1LE80 I III 1AMV01. /V\ gwl' (YI & I:").1. wt'g1 ugwyGw�I u�si���r.naw;k ACT (H luum pnq l 011'gl),,I.l.la� 11gwl.�.r '� I ;,1� 4���1 "Pttlw"ICI lraaalrl w4wgVfgw'°�� RIu7 "+kllw (,","919,1v P N N S L 11NI � ._ .... M1,S LIsHM I)u,V ,")gj Y 01 d1 M(M1R,�..I Bql,� fiq a �d10N. 1� lglll I y lips Y, q q a, q I .... w 1 I.I Icltigiq'" q a>pq ,, E a, Iga � .���.... { � aI citej iq lua.I I %'11ata' I G^�G�ll'_P_._.— Y �lq _ �1 tire°,w� a,z�w IN A N � ov ass P V L iI glyI fl I ,gabsso� <I �I I g�qa il;, dl �' I sei 1r�a1 ... puag7, I�qlllgq[ q aowr A11Z _.. 11�1S1w,G A0! "1"I'a��^� 91 I. I .� 'q�q�.lQ�. .wd, I � To-, � �y �..—. P r 'b 11 l 11 .` i all 1 1 �4�1 Nnloigq� II CI1 01 ".Iq' 'j ql�� RwG�I kl a� f1 � tt1 1 141 R �r Mu l I;aiw MIN Vwu Iy�I i a y li"laq P klr'aa1 l"„.01 f Ik@ill.l )O IV-1 Mkj 1f4'kN I III,Ca p a PI'%I,. �W!1r7�t�a l ��4+ jjd ....... _.... _.... �I1�. yw IM d: °k �r��� o a��H ���a��M� x ar %l �r�Aq,�fw�rrcroa V1� ��i�ai�������� ;:��'a�gp�rp�1wl�arrlt�r Page 14 of 14 Danville 4/3/23 mg/kg mg/L Equiv Weight Milli Equiv Sodium 17700 702.69 23 30.55174 Calcium 16500 655.05 20 32.7525 Magnesium 3550 140.935 12 11.74458 Percent Solids 3.97 SAR 6.48 SAR Na+ a (Ca2+ + M92+) 30.55174 '',::: 0.5( 32.753 2 + 11.74458 2 ) mil , 4/27/2023 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 23-109-0007 Project Description: VPDES Permit # VA0060593 Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 4/19/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Brandi Watson Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 (2) Waypoeint7621 Whitepine Load, Richmond, VA 23237 Main 804-743-94010 Fax 8 4-271-6446 ANALYTICAL wo, w,waypointanalyticaLc m Sample Summary Table Report Number: 23-109-0007 Client Project Description: VPDES Permit # VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 61824 LTS A -Basin 23-1298 Solids 04/18/2023 08:05 04/19/2023 SM-2540G WP MTN SW-7471B WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SM-4500-NH3C WP MTN 9045D WP MTN SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 8 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit # VA0060593 A/P Report Date : 04/27/2023 Northside WWTP Information : Received : 04/19/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-109-0007 REPORT OFANALYSIS Lab No : 61824 Matrix: Solids Sample ID : LTS A -Basin 23-1298 Sampled: 4/18/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 96.0 % 0.010 1 04/25/2316:30 JLS SM-2540G Sulfur 10200 mg/Kg - dry 250 1 04/22/23 03:10 TJS 6010D Calcium 13600 mg/Kg - dry 1250 1 04/22/23 03:10 TJS 6010D Manganese 733 mg/Kg - dry 12.5 1 04/22/23 03:10 TJS 6010D Zinc 1930 mg/Kg - dry 31.3 1 04/22/23 03:10 TJS 6010D Nickel 44.8 mg/Kg - dry 6.25 1 04/22/23 03:10 TJS 6010D Lead 38.8 mg/Kg - dry 7.50 1 04/22/23 03:10 TJS 6010D Arsenic <12.5 mg/Kg - dry 12.5 1 04/22/23 03:10 TJS 6010D Selenium <12.5 mg/Kg - dry 12.5 1 04/22/23 03:10 TJS 6010D pH 7.4 S.U. 1 04/25/2316:30 CNB 9045D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 56500 mg/Kg - dry 2500 1 04/24/23 09:20 AMS SM-2320 B Organic N 67050 mg/Kg - dry 6250 1 04/24/23 12:00 CALCULATION Total Solids 4.01 % 0.010 1 04/25/23 16:30 JLS SM-2540G Phosphorus 19200 mg/Kg - dry 125 1 04/22/23 03:10 TJS 6010D Copper 348 mg/Kg - dry 12.5 1 04/22/23 03:10 TJS 6010D Magnesium 3000 mg/Kg - dry 125 1 04/22/23 03:10 TJS 6010D Molybdenum 7.50 mg/Kg - dry 6.25 1 04/22/23 03:10 TJS 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 8 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit # VA0060593 A/P Report Date : 04/27/2023 Northside WWTP Information : Received : 04/19/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-109-0007 REPORT OFANALYSIS Lab No : 61824 Matrix: Solids Sample ID : LTS A -Basin 23-1298 Sampled: 4/18/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sodium 17100 mg/Kg - dry 625 1 04/22/23 03:10 TJS 6010D Total Kjeldahl Nitrogen 79000 mg/Kg - dry 6250 1 04/25/23 09:30 CLP ;M-4500-NH3C-TKlN Potassium 3650 mg/Kg - dry 250 1 04/22/23 03:10 TJS 6010D Iron 24400 mg/Kg - dry 250 1 04/22/23 03:10 TJS 6010D Aluminum 23500 mg/Kg - dry 125 1 04/22/23 03:10 TJS 6010D Ammonia Nitrogen 12000 mg/Kg - dry 2500 1 04/24/23 12:00 CLP SM-4500-NH3C Nitrate+Nitrite-N <125 mg/Kg - dry 125 1 04/20/23 14:35 ZBD 4500NO3F-2011 Cadmium <2.50 mg/Kg - dry 2.50 1 04/22/23 03:10 TJS 6010D Chromium 36.0 mg/Kg - dry 6.25 1 04/22/23 03:10 TJS 6010D Mercury <4.53 mg/Kg - dry 4.53 1 04/20/23 12:53 FDS SW-7471B Total Volatile Solids 52.0 % 0.010 1 04/25/23 16:30 JLS SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 8 to Way� PA ► x �... , Main .04.40, Fax 04,,4, www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES Permit # VA0060593 Lab Report Number: 23-109-0007 Date: 4/26/2023 Metals Analysis Method 6010D Sample 98538 (TOCSOSB0320-24) Analyte: Aluminum QC Batch No: 1-678073/1-677142 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98538 (TOCSOSB0320-24) Analyte: Aluminum QC Batch No: 1-678312/1-677142 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98538 (TOCSOSB0320-24) Analyte: Iron QC Batch No: L677789/L677142 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98538 (TOCSOSB0320-24) Analyte: Potassium QC Batch No: L677789/L677142 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 8 Way A.4, k L.. Main 804,d "q 44.. •' Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 23-109-0007 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IDavid Lennon Date & Time: 04/19/2023 12:40:38 Page 6 of 8 -u S n� 0 Cn 71 V (oil -Mu > Z, m 011 > L 14 C) > cn 0 3 cc' v < 0 a) Ol F6 >< 3 o 1p Ln 9 Cr 3 (0 q Number of Containers -4 Cr 3 --1 C C Cr MatrIN (Refer to x0y) M ;:� JG)rab of (C)omposfte E3 3 Cr 0 Cc z See attached list hi R, ir rows 0 m 0 3 3 Cn! 3 ISOR mo 's, --4 (D (1) 3 > 3 V (n Cr 2 (D (D (D tu MI Z' S Cn E5 Cr r, 4"MmIlAA NJ 0 r4 (D C) 4 0 0) < CL m Ocr, CO Page 7 of 8 M Required Blosoild's Tests for Inframark Danville, VA WWTP (Waypoint VA Account 79434) Sample: LTS A Basin 23 PO: 152575 p�H Alkalinity Ammoni,a-Nitrogen Nitrate + Nitrite as Nitrogen Organlic Nitrogen, (calculation) Phosphorus Potassium Sulfur Calcium Magnesium Sodium: iron Alumnurn Manganese Zinc "'-"Cadmium Nickei Lead Arsenic Mercury Selenium Molybdenum Page 8 of 8 Danville 4/18/23 mg/kg mg/L Equiv Weight Milli Equiv Sodium 17100 685.71 23 29.81348 Calcium 13600 545.36 20 27.268 Magnesium 3000 120.3 12 10.025 Percent Solids 4.01 SAR 6.90 SAR Na+ a (Ca2+ + M92+) 29.81348 '',::: 0.5( 27.268 2 + 10.02500 2 ) mil , 5/10/2023 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 23-122-0006 Project Description: VPDES Permit #: VA0060593 Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 5/2/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Brandi Watson Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 (2) Waypoeint7621 Whitepine Load, Richmond, VA 23237 Main 804-743-94010 Fax 8 4-271-6446 ANALYTICAL wo, w,waypointanalyticaLc m Sample Summary Table Report Number: 23-122-0006 Client Project Description: VPDES Permit #: VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 61897 LTS A -basin 23-1332 Solids 05/01/2023 08:00 05/02/2023 SM-2540G WP MTN SW-7471B WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SM-4500-NH3C WP MTN 9045D WP MTN SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 8 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit #: VA0060593 A/P Report Date : 05/10/2023 Northside WWTP Information : Received : 05/02/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-122-0006 REPORT OFANALYSIS Lab No : 61897 Matrix: Solids Sample ID : LTS A -basin 23-1332 Sampled: 5/1/2023 8:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 96.0 % 0.010 1 05/08/2316:55 JLS SM-2540G Sulfur 12400 mg/Kg - dry 250 1 05/03/23 21:35 TJS 6010D Calcium 15900 mg/Kg - dry 1250 1 05/03/23 21:35 TJS 6010D Manganese 983 mg/Kg - dry 12.5 1 05/03/23 21:35 TJS 6010D Zinc 2350 mg/Kg - dry 31.3 1 05/03/23 21:35 TJS 6010D Nickel 56.0 mg/Kg - dry 6.25 1 05/03/23 21:35 TJS 6010D Lead 54.3 mg/Kg - dry 7.50 1 05/03/23 21:35 TJS 6010D Arsenic <12.5 mg/Kg - dry 12.5 1 05/03/23 21:35 TJS 6010D Selenium <12.5 mg/Kg - dry 12.5 1 05/03/23 21:35 TJS 6010D pH 7.6 S.U. 1 05/03/2316:00 CNB 9045D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 52300 mg/Kg - dry 2500 1 05/09/23 09:35 AMS SM-2320 B Organic N 105500 mg/Kg - dry 6250 1 05/08/23 10:30 CALCULATION Total Solids 4.02 % 0.010 1 05/08/23 16:55 JLS SM-2540G Phosphorus 23700 mg/Kg - dry 125 1 05/03/23 21:35 TJS 6010D Copper 450 mg/Kg - dry 12.5 1 05/03/23 21:35 TJS 6010D Magnesium 3650 mg/Kg - dry 125 1 05/03/23 21:35 TJS 6010D Molybdenum 10.9 mg/Kg - dry 6.25 1 05/03/23 21:35 TJS 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 8 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit #: VA0060593 A/P Report Date : 05/10/2023 Northside WWTP Information : Received : 05/02/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-122-0006 REPORT OFANALYSIS Lab No : 61897 Matrix: Solids Sample ID : LTS A -basin 23-1332 Sampled: 5/1/2023 8:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sodium 16700 mg/Kg - dry 625 1 05/03/23 21:35 TJS 6010D Total Kjeldahl Nitrogen 115000 mg/Kg - dry 6250 1 05/08/23 10:30 JPJ ;M-4500-NH3C-TKlN Potassium 4000 mg/Kg - dry 250 1 05/03/23 21:35 TJS 6010D Iron 32300 mg/Kg - dry 250 1 05/03/23 21:35 TJS 6010D Aluminum 31800 mg/Kg - dry 125 1 05/03/23 21:35 TJS 6010D Ammonia Nitrogen 9550 mg/Kg - dry 2500 1 05/09/23 11:00 CLP SM-4500-NH3C Nitrate+Nitrite-N <125 mg/Kg - dry 125 1 05/08/23 15:12 ZBD 4500NO3F-2011 Cadmium <2.50 mg/Kg - dry 2.50 1 05/03/23 21:35 TJS 6010D Chromium 43.0 mg/Kg - dry 6.25 1 05/03/23 21:35 TJS 6010D Mercury <4.48 mg/Kg - dry 4.48 1 05/08/23 12:48 FDS SW-7471B Total Volatile Solids 52.0 % 0.010 1 05/08/23 16:55 JLS SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 8 to Way� PA ► x �... , Main .04.40, Fax 04,,4, www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES Permit #: VA0060593 Lab Report Number: 23-122-0006 Date: 5/9/2023 Metals Analysis Method 601 OD Sample 86092 (ST23MAY01-03-001) Analyte: Aluminum QC Batch No: 1-679930/1-679600 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86092 (ST23MAY01-03-001) Analyte: Iron QC Batch No: 1-679930/1-679600 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86092 (ST23MAY01-03-001) Analyte: Potassium QC Batch No: 1-679930/1-679600 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86092 (ST23MAY01-03-001) Analyte: Sulfur QC Batch No: 1-679930/1-679600 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 8 Way A.4, k L.. Main 804,d "q 44.. •' Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 23-122-0006 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IDavid Lennon Date & Time: 05/02/2023 11:15:01 Page 6 of 8 I < < v > z 0 .0 3 M a M 1 3 0 -!� < > z 0 0 (D CL V Q-1 Cn > -4 CO 3 Cr U) OX 3 O's, q 9 M r) C, r) a Mi Number of Cantallners --4 3 0 -U W Matrix �Refvr to K,-Vl C i C V Cr 0 �G),rab or 1C)ompomite M A EE 0,0 ltwOJ 0, z z 2- V See attached fist a CO, d a Zr < to M > EL X 3 jd CD nFl 7'it > LU < C --43 loom." CL C a -4 55 M U) Cr W p. (D Z 0 5 CL CD Cr M Page 7 of 8 Required Biosollids Tests for Infrarnark Danville, VA WWTP (Waypoint VA Account 79434) Sample: MA64sinD- 113.1 `2 P -. 152575 I" /Z �5 %TS %TVs pH Alkalinity TKN Ammonia-Nitrogeni Nitrate + Nitrite as, Nitrogen Organic Nitrogen (calculation) M W w U PhosphorLJS Potassium Sulfur Calcium! Magnesium Sodium Iron Aluminumrca Manganese Cor Zinc Cadmiuim, Chromium, Nickel Lead Arsenic Mercury Selenium -'Molybdenurn Page 8 of 8 Danville 5/1 /23 mg/kg mg/L Equiv Weight Milli Equiv Sodium 16700 671.34 23 29.1887 Calcium 15900 639.18 20 31.959 Magnesium 3650 146.73 12 12.2275 Percent Solids 4.02 SAR 6.21 SAR Na+ a (Ca2+ + M92+) 29.18870 '',::: 0.5( 31.959 2 + 12.22750 2 ) mil , 5/25/2023 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 23-136-0007 Project Description: VPDES Permit #: VA0060593 Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 5/16/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Brandi Watson Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 (2) Waypoeint7621 Whitepine Load, Richmond, VA 23237 Main 804-743-94010 Fax 8 4-271-6446 ANALYTICAL wo, w,waypointanalyticaLc m Sample Summary Table Report Number: 23-136-0007 Client Project Description: VPDES Permit #: VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 62039 LTS A -Basin 23-1374 Solids 05/15/2023 08:10 05/16/2023 SM-2540G WP MTN SW-7471B WP MTN SM-4500-NH3C-TKN WP MTN 4500NO3F-2011 WP MTN 6010D WP MTN SM-4500-NH3C WP MTN 9045D WP MTN SM-2320 B WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 8 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit #: VA0060593 A/P Report Date : 05/25/2023 Northside WWTP Information : Received : 05/16/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-136-0007 REPORT OFANALYSIS Lab No : 62039 Matrix: Solids Sample ID : LTS A -Basin 23-1374 Sampled: 5/15/2023 8:10 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Moisture 96.1 % 0.010 1 05/22/2317:15 JLS SM-2540G Sulfur 12700 mg/Kg - dry 256 1 05/19/23 01:29 BKN 6010D Calcium 14900 mg/Kg - dry 1280 1 05/19/23 01:29 BKN 6010D Manganese 838 mg/Kg - dry 12.8 1 05/19/23 01:29 BKN 6010D Zinc 2120 mg/Kg - dry 32.1 1 05/19/23 01:29 BKN 6010D Nickel 53.8 mg/Kg - dry 6.41 1 05/19/23 01:29 BKN 6010D Lead 51.0 mg/Kg - dry 7.69 1 05/19/23 01:29 BKN 6010D Arsenic <12.8 mg/Kg - dry 12.8 1 05/19/23 01:29 BKN 6010D Selenium <12.8 mg/Kg - dry 12.8 1 05/19/23 01:29 BKN 6010D pH 7.5 S.U. 1 05/23/2316:00 CNB 9045D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 72100 mg/Kg - dry 2560 1 05/18/23 09:45 BLM SM-2320 B Organic N 40900 mg/Kg - dry 6410 1 05/24/23 10:00 CALCULATION Total Solids 3.91 % 0.010 1 05/22/23 17:15 JLS SM-2540G Phosphorus 22200 mg/Kg - dry 128 1 05/19/23 01:29 BKN 6010D Copper 405 mg/Kg - dry 12.8 1 05/19/23 01:29 BKN 6010D Magnesium 3490 mg/Kg - dry 128 1 05/19/23 01:29 BKN 6010D Molybdenum 9.54 mg/Kg - dry 6.41 1 05/19/23 01:29 BKN 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 8 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit #: VA0060593 A/P Report Date : 05/25/2023 Northside WWTP Information : Received : 05/16/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-136-0007 REPORT OFANALYSIS Lab No : 62039 Matrix: Solids Sample ID : LTS A -Basin 23-1374 Sampled: 5/15/2023 8:10 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sodium 16600 mg/Kg - dry 641 1 05/19/23 01:29 BKN 6010D Total Kjeldahl Nitrogen 52600 mg/Kg - dry 6410 1 05/24/23 10:00 JPJ ;M-4500-NH3C-TKlN Potassium 3970 mg/Kg - dry 256 1 05/19/23 01:29 BKN 6010D Iron 29700 mg/Kg - dry 256 1 05/19/23 01:29 BKN 6010D Aluminum 27700 mg/Kg - dry 128 1 05/19/23 01:29 BKN 6010D Ammonia Nitrogen 11700 mg/Kg - dry 2560 1 05/24/23 14:40 JPJ SM-4500-NH3C Nitrate+Nitrite-N <128 mg/Kg - dry 128 1 05/17/23 14:25 ZBD 4500NO3F-2011 Cadmium <2.56 mg/Kg - dry 2.56 1 05/19/23 01:29 BKN 6010D Chromium 39.0 mg/Kg - dry 6.41 1 05/19/23 01:29 BKN 6010D Mercury <4.31 mg/Kg - dry 4.31 1 05/19/23 13:57 FDS SW-7471B Total Volatile Solids 52.4 % 0.010 1 05/22/23 17:15 JLS SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 8 to Way� PA ► x �... , Main .04.40, Fax 04,,4, www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES Permit #: VA0060593 Lab Report Number: 23-136-0007 Date: 5/24/2023 Metals Analysis Method 6010D Sample 94565 QC Batch No: L682967/L682391 One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are required. Sample 94565 Analyte: Aluminum QC Batch No: L683074/L682391 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94565 Analyte: Calcium QC Batch No: L683074/L682391 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94565 Analyte: Iron QC Batch No: L683074/L682391 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94565 Analyte: Magnesium QC Batch No: L683074/L682391 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 94565 Analyte: Manganese QC Batch No: L683074/L682391 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 5 of 8 Way A.4, k L.. Main 804,d "q 44.. •' Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 23-136-0007 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IDavid Lennon Date & Time: 05/16/2023 11:44:00 Page 6 of 8 oil • Number of Containers MUMMEN MONO i MMEMEMEMOR MWER mill1`11RNI'll Required Slosolid's Tests for Inframark Danville, VA V4WTP (Waypoint VA Account 79434)i Sample: MA,Wn23— J PO. 152575 %TS %TVs PH Alka4nity TKN Ammonia -Nitrogen Nitrate + Nitrite as Nitrogen Organic Nitrogen Qcalcuiatfon) Phosphorus Potassium Sulfur Calcium Magnesium Sodium Iron Aluminum Manganese Copper Zinc Cadmium Chrom:ium Nickel Lead Arsenic Mercury Selenjurn Molybdenum Page 8 of 8 Danville 5/15/23 mg/kg mg/L Equiv Weight Milli Equiv Sodium 16600 649.06 23 28.22 Calcium 14900 582.59 20 29.1295 Magnesium 3490 136.459 12 11.37158 Percent Solids 3.91 SAR 6.27 SAR Na+ a (Ca2+ + M92+) 28.22000 '',::: 0.5( 29.13 2 + 11.37158 2 ) mil , 4/19/2023 Inframark A/P Northside WWTP 229 Northside Drive Danville, VA, 24540 Ref: Analytical Testing Report Number: 23-094-0014 Project Description: VPDES Permit# VA0060593 Dear A/P: Waypoint Analytical Virginia, Inc. received sample(s) on 4/4/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table if applicable. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information Sincerely, Brandi Watson Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 14 (2) Waypoeint7621 Whitepine Load, Richmond, VA 23237 Main 804-743-94010 Fax 8 4-271-6446 ANALYTICAL wo, w,waypointanalyticaLc m Sample Summary Table Report Number: 23-094-0014 Client Project Description: VPDES Permit# VAOO6O593 Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 9045D WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-2320 B WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 6010D WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 4500NO3F-2011 WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SW-7471B WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-4500-NH3C WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-4500-NH3C-TKN WP MTN 61588 LTS A -Basin 23-1245 A Solids 04/03/2023 08:05 04/04/2023 SM-2540G WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 SW-9045C WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 SW-7.3.4 WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 SW-7.3.3 WP MTN 61589 LTS A -Basin 23-1245 B Solids 04/03/2023 08:05 04/04/2023 ASTM D93-80 WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 SW-1311 (ZHE) WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 SW-1311 WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8270C WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8260B WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8151A WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 8081A WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 7470A WP MTN 61590 LTS A -Basin 23-1245 C TCLP 04/03/2023 08:05 04/04/2023 6010D WP MTN WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 2 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www.waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61588 Matrix: Solids Sample ID : LTS A -Basin 23-1245 A Sampled: 4/3/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Potassium 3980 mg/Kg - dry 250 1 04/07/23 06:51 BKN 6010D Magnesium 3550 mg/Kg - dry 125 1 04/07/23 06:51 BKN 6010D Sodium 17700 mg/Kg - dry 625 1 04/07/23 06:51 BKN 6010D Iron 30300 mg/Kg - dry 250 1 04/07/23 06:51 BKN 6010D Zinc 2390 mg/Kg - dry 31.3 1 04/07/23 06:51 BKN 6010D Ammonia Nitrogen 22400 mg/Kg - dry 2500 1 04/06/23 05:50 JPJ SM-4500-NH3C Nitrate +N itrite-N <125 mg/Kg - dry 125 1 04/11/23 12:44 ZBD 4500NO3F-2011 Cadmium <2.50 mg/Kg - dry 2.50 1 04/07/23 06:51 BKN 6010D Chromium 43.3 mg/Kg - dry 6.25 1 04/07/23 06:51 BKN 6010D Mercury <4.70 mg/Kg - dry 4.70 1 04/07/23 11:40 FDS SW-7471B pH 7.3 S.U. 1 04/10/2311:30 HBT 9045D Molybdenum 9.78 mg/Kg - dry 6.25 1 04/07/23 06:51 BKN 6010D Test Results Units MQL DF Date / Time By Analytical Analyzed Method Alkalinity (as CaCO3) 60800 mg/Kg - dry 2500 1 04/11/23 09:45 TKM SM-2320 B Total Solids 3.97 % 0.010 1 04/10/23 14:09 JLS SM-2540G Aluminum 29300 mg/Kg - dry 125 1 04/07/23 06:51 BKN 6010D Selenium <12.5 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Sulfur 12900 mg/Kg - dry 250 1 04/07/23 06:51 BKN 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 3 of 14 ,�f�AL4'�i ICAL Wayp to 79434 Inframark Project A/P Northside WWTP Information 229 Northside Drive Danville , VA 24540 Report Number : 23-094-0014 . Lr PII 0 . 7 �� Tp• Main 43444 www.waypointanalyticaLcom VPDES Permit# VA0060593 REPORT OFANALYSIS Report Date : 04/19/2023 Received : 04/04/2023 Brandi Watson Lab No : 61588 Sample ID : LTS A -Basin 23-1245 A Matrix: Solids Sampled: 4/3/2023 8:05 Moisture 96.0 % 0.010 1 04/10/2314:09 JLS SM-2540G Total Kjeldahl Nitrogen 71000 mg/Kg - dry 6250 1 04/07/23 11:00 CLP ;M-4500-NH3C-TKlN Phosphorus 22500 mg/Kg - dry 125 1 04/07/23 06:51 BKN 6010D Calcium 16500 mg/Kg - dry 1250 1 04/07/23 06:51 BKN 6010D Manganese 900 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Copper 440 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Organic N 48600 mg/Kg - dry 6250 1 04/06/23 05:50 CALCULATION Nickel 55.0 mg/Kg - dry 6.25 1 04/07/23 06:51 BKN 6010D Lead 48.5 mg/Kg - dry 7.50 1 04/07/23 06:51 BKN 6010D Arsenic < 12.5 mg/Kg - dry 12.5 1 04/07/23 06:51 BKN 6010D Total Volatile Solids 52.1 % 0.010 1 04/10/23 14:09 JLS SM-2540G Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 4 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61589 Matrix: Solids Sample ID : LTS A -Basin 23-1245 B Sampled: 4/3/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sulfide (Reactivity) <25.3 mg/Kg 25.3 1 04/13/23 10:30 CNB SW-7.3.4 Cyanide (Reactivity) <0.125 mg/Kg 0.125 1 04/12/23 10:30 CNB SW-7.3.3 Ignitability >96 degrees C 1 04/12/23 04:45 JFM ASTM D93-80 pH Qualifiers/ DF Dilution Factor Definitions 1 04/17/2317:03 CNB SW-9045C MQL Method Quantitation Limit Page 5 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61590 Matrix: TCLP Sample ID : LTS A -Basin 23-1245 C Sampled: 4/3/2023 8:05 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP Metals Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP Pesticide Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP SVOC Extraction Combined 1 04/10/23 13:00 ALM SW-1311 TCLP VOC ZHE Extraction Combined 1 04/10/23 13:00 ALM SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L675452 04/11/23 13:52 Prep Method: 3015A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 04/11/23 19:04 JTR L675662 TCLP Barium <0.250 mg/L 0.250 1 04/11/23 19:04 JTR L675662 TCLP Cadmium <0.0500 mg/L 0.0500 1 04/11/23 19:04 JTR L675662 TCLP Chromium <0.100 mg/L 0.100 1 04/11/23 19:04 JTR L675662 TCLP Lead <0.100 mg/L 0.100 1 04/11/23 19:04 JTR L675662 TCLP Selenium <0.500 mg/L 0.500 1 04/11/23 19:04 TJS L675662 TCLP Silver <0.0500 mg/L 0.0500 1 04/11/23 19:04 JTR L675662 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 6 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61590 Matrix: TCLP Sample ID : LTS A -Basin 23-1245 C Sampled: 4/3/2023 8:05 Analytical Method: 7470A Prep Batch(es): L675539 04/12/23 07:55 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 04/12/23 13:42 FDS L675724 Analytical Method: 8081A Prep Batch(es): L676046 04/13/23 17:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Endrin <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP gamma-BHC <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP Methoxychlor <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP Toxaphene <0.006000 mg/L 0.006000 10 04/14/23 16:58 VIC L676321 TCLP Chlordane <0.004000 mg/L 0.004000 10 04/14/23 16:58 VIC L676321 TCLP Heptachlor Epoxide <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 TCLP Heptachlor <0.000800 mg/L 0.000800 10 04/14/23 16:58 VIC L676321 Surrogate: Decachlorobiphenyl 64.86 Limits: 36-116% 10 04/14/23 16:58 VIC L676321 Surrogate: Tetrachloro-m-xylene 60.58 Limits: 25-123% 10 04/14/23 16:58 VIC L676321 Analytical Method: 8151A Prep Batch(es): L676065 04/14/23 18:00 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 04/17/23 23:29 VIC L676737 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 04/17/23 23:29 VIC L676737 Surrogate: DCAA 65.80 Limits: 20-120% 1 04/17/23 23:29 VIC L676737 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 7 of 14 Waypoeinto ANALYTICAL 79434 Inframark Project A/P Northside WWTP Information 229 Northside Drive Danville , VA 24540 Report Number : 23-094-0014 7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 www,waypointa nalyticaLcom VPDES Permit# VA0060593 REPORT OFANALYSIS Report Date : 04/19/2023 Received : 04/04/2023 Brandi Watson Lab No : 61590 Matrix: TCLP Sample ID : LTS A -Basin 23-1245 C Sampled: 4/3/2023 8:05 Analytical Method: 8260B Prep Batch(es): L676130 04/13/23 08:23 Prep Method: 5030B Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Carbon Tetrachloride <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Chlorobenzene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Chloroform <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP 1,4-Dichlorobenzene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP 1,2-Dichloroethane <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP 1,1-Dichloroethene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Methyl Ethyl Ketone (MEK) <0.200 mg/L 0.200 1 04/13/23 13:07 ASH L676139 TCLP Tetrachloroethene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Trichloroethene <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 TCLP Vinyl Chloride <0.0100 mg/L 0.0100 1 04/13/23 13:07 ASH L676139 Surrogate:4-Bromofluorobenzene 92.2 Limits:71-137% 1 04/13/23 13:07 ASH L676139 Surrogate: Dibromofluoromethane 90.0 Limits: 70-128% 1 04/13/23 13:07 ASH L676139 Surrogate: 1,2-Dichloroethane - d4 116 Limits: 63-136% 1 04/13/23 13:07 ASH L676139 Surrogate: Toluene-d8 93.8 Limits: 70-130% 1 04/13/23 13:07 ASH L676139 Analytical Method: 8270C Prep Batch(es): L675936 04/13/23 11:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP 3&4 Methylphenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP 2,4-Dinitrotoluene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 8 of 14 0 Waypoeint7621 Whitepine Road, Richmond, VA 23237 Main 804-74-9401 0 Fax 804-271-6446 ANALYTICAL www,waypointanalyticaLc m 79434 Inframark Project VPDES Permit# VA0060593 A/P Report Date : 04/19/2023 Northside WWTP Information : Received : 04/04/2023 229 Northside Drive Danville , VA 24540 Brandi Watson Report Number : 23-094-0014 REPORT OFANALYSIS Lab No : 61590 Sample ID : LTS A -Basin 23-1245 C Matrix: TCLP Sampled: 4/3/2023 8:05 Analytical Method: 8270C Prep Batch(es): L675936 04/13/23 11:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobenzene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Hexachlorobutadiene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Hexachloroethane <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Nitrobenzene <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP Pentachlorophenol <0.0500 mg/L 0.0500 1 04/13/23 20:12 VBW L676114 TCLP Pyridine <0.0500 mg/L 0.0500 1 04/13/23 20:12 VBW L676114 TCLP 2,4,5-Trichlorophenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 TCLP 2,4,6-Trichlorophenol <0.0250 mg/L 0.0250 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 2,4,6-Tribromophenol 65.0 Limits: 42-102% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 2-Fluorobiphenyl 57.5 Limits: 24-86% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 2-Fluorophenol 27.3 Limits: 13-37% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP 4-Terphenyl-d14 75.0 Limits: 30-122% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP Nitrobenzene-d5 60.0 Limits: 25-78% 1 04/13/23 20:12 VBW L676114 Surrogate: TCLP Phenol-d6 17.1 Limits: 9-27% 1 04/13/23 20:12 VBW L676114 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 9 of 14 to Way� PA ► x �... , Main .04.40, Fax 04,,4, www.waypointanalytical.com Client: Inframark CASE NARRATIVE Project: VPDES Permit# VA0060593 Lab Report Number: 23-094-0014 Date: 4/18/2023 Separatory Funnel Extraction 8081 Method 3510C Sample 61590 (LTS A -Basin 23-1245 C) QC Batch No: L676046/L676046 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction 8270 Method 3510C Sample 61590 (LTS A -Basin 23-1245 C) QC Batch No: L675936/L675936 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis Method 601 OD Sample 61588 (LTS A -Basin 23-1245 A) Analyte: Aluminum QC Batch No: L674758/L674295 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 61588 (LTS A -Basin 23-1245 A) Analyte: Iron QC Batch No: L674758/L674295 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 61588 (LTS A -Basin 23-1245 A) Analyte: Potassium QC Batch No: L674758/L674295 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 10 of 14 Way A.4, k L.. Main 804,d "q 44.. •' Shipment Receipt Form Customer Number: 79434 Customer Name: Inframark Report Number: 23-094-0014 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier 0 Other Thermometer ID: Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? # Yes 0 No COC properly completed # Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F_ High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_ Low concentration EnCore samplers (48 hr) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes * No Comments: Signature: IDavid Lennon Date & Time: 04/04/2023 13:16:47 Page 11 of 14 N. ..... .... . . ..IM Page 1�1'1'1').f 14 LunuapqAj%N wnivapS Ain ojo..- .)�Uasjv peal P13N ujnit,uo.jqD wniLupeD Duq asaueguevq —'. ujriutwniv — MOM WnIpos on" Lunisauft�Ni jnjjnS wn'SSP10d snjo4dsOI4d (uopejn:)je3) Ua2OJIN:)'UL'SJO1 E? m Ca se IPIN + alOJIN Ua3OJI!N-eRJOWWV - NNII SISZSI Oj v SWI -",EZ u1seq V Srj- :aIdweS (VIEVU juno3:)V VA 4uiodAeM) dIMM VA'alIjAue(I njetuej;ul A01 sisal SpIlosoig pajinba)j Page 13 of 14 f,T 90 fT aSPd Waypohil Amnlytical Laborjtory 23-094-0014 NV NNN�NNNNNN�NN 43 WOW 1311 TCLP Pmp Shm*t 111111111111111110 1111 694 44t= ami 1 o 1 11 It ics: jo'e" h4mm m k ITIOA5 Orgoll u to lunc&hy (Dun VPDES PfjimNt#VAOM)59'J I Y"n)uiaxi vj,i-j/voc 3cljzcn( Z I CIRO Na', JAE,, Report 4: Loochotes Sample Dule; filtra(cs Dale Arrived; Murix: ak �Q) L i AIR, 0 i . ... .. .. ... . Dale Extracted: Balance "T JAI 6dibratiollj Refereticc, 71NI C t'l 1, Charamelization Nw 1EMMw,T`7-L1i(1 �Exuw&ou I Final S ifav S"Imple h6tial Second Eml,wt we�ght nds pH Reduction H) #: Fhdd FALlid V/N --J-Ikl�d 10C C'Tum-�lmerjzaion Cor 1"'mi'acl Fluid ZHE" S"'wnlfle I a l j I r,l [ Second IE",wroc[ \\'eighl 11flS Pressure � �! )JI Fluid vc�i "rams Huid []Llid m"Imullled 5 1 v Iq Y N Y N' I F1 lob ID K Beaker Final Sm"Me F bull filler ,\,:J wilsi,IFT 7N I I( I SIGN, I'1raid 111 Vn I I k ILA, 0", FILlid BIM)k 111) (1�2),: Www" mah H): V hd I One: 21 N1 i R a°tal j v: -------- 1`d[r rte I �ohd 10 T IM& MAKOwul 131 1 0827 18 ANNUAL PA"I"110CFN AND VECRM4 XFOW110NI REDWrio Fo R (OXI" R.muillles) Facwrllmty l ammne:, C;pcy a H),aa.nnvpolat Q l9m�°urmmmuct Number: IC�apD(b �pli'"`96 y10005" apV Name: ayrmmmmh r cma npm,armm ucam @ c a (land 1pd"aramacmm C /'p/'C,(pC, CIl 'p 202 v ................................................................................................. 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I am aware tbaat th ire aam~cm Agmmiiific,aant placmunraallktles fur We certification inrc,CCmmdunug fine and irmmpriiimmmnaaac,tut.''" A" anon 6ou k - 1119ncrpc e fla.an"a(ncar lnrep"arer" 9aunae parch 'ifle (ayl)e or print) .I r,;'a11 r 16,2i7It ISr; Brent C ;ca h ns; 111: ireccor crfF cmc,hnu c° l y(cwu v ac ei Land .ppher Name and T44 (6h"prap plWau.hle)(type or prig) Ygnmaaature cnrPrepaauer* Date Signature caVlll,a nd, Applier (H'aa.r)pHCl]lflC( I.)a.alC m'p"nepamer 1s dc,tlincd nrm 40 Crop R 14150 A(r) aa:md 15ik N CAC C"r .1 102 (26( D1F=:.11 III FURM Py91FRIf- 2..I1. (12/2 p(' 6) I eAnalytical wurmpacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 April 06, 2023 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: INFRAMARK-DANVILLE VA0060593 Pace Project No.: 30574814 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on April 03, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Cl'Yf oi'a, u�tf,C` Cynthia Walker cynthia.walker@pacelabs.com (800)999-0105 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 10 aceAnalytical www.pacallabs.cmim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: INFRAMARK-DANVILLE VA0060593 Pace Project No.: 30574814 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 10 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: INFRAMARK-DANVILLE VA0060593 Pace Project No.: 30574814 Lab ID Sample ID Matrix Date Collected Date Received 30574814001 A BASIN #1 Solid 04/03/23 07:20 04/03/23 12:10 30574814002 A BASIN #2 Solid 04/03/23 07:25 04/03/23 12:10 30574814003 A BASIN #3 Solid 04/03/23 07:30 04/03/23 12:10 30574814004 A BASIN #4 Solid 04/03/23 07:45 04/03/23 12:10 30574814005 A BASIN #5 Solid 04/03/23 07:55 04/03/23 12:10 30574814006 A BASIN #6 Solid 04/03/23 08:00 04/03/23 12:10 30574814007 A BASIN #7 Solid 04/03/23 08:05 04/03/23 12:10 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 10 aceAnalytical www.pacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: INFRAMARK-DANVILLE VA0060593 30574814 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30574814001 A BASIN #1 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30574814002 A BASIN #2 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30574814003 A BASIN #3 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30574814004 A BASIN #4 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30574814005 A BASIN #5 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30574814006 A BASIN #6 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30574814007 A BASIN #7 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 10 aceAnalytical wurmpacallabs.cmim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE VA0060593 Pace Project No.: 30574814 Sample: A BASIN #1 Lab ID: 30574814001 Collected: 04/03/23 07:20 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.4 % 0.10 1 04/04/23 09:16 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 2780 2.778 04/03/23 14:35 04/04/23 12:12 Sample: A BASIN #2 Lab ID: 30574814002 Collected: 04/03/23 07:25 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.8 % 0.10 1 04/04/23 09:18 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 2380 2.381 04/03/23 14:35 04/04/23 12:12 Sample: A BASIN #3 Lab ID: 30574814003 Collected: 04/03/23 07:30 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.3 % 0.10 1 04/04/23 09:21 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 2700 2.703 04/03/23 14:35 04/04/23 12:12 Sample: A BASIN #4 Lab ID: 30574814004 Collected: 04/03/23 07:45 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Percent Moisture Date: 04/06/2023 05:15 PM Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver 96.0 % 0.10 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 04/04/23 09:22 N2 Page 5 of 10 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: INFRAMARK-DANVILLE VA0060593 Pace Project No.: 30574814 Sample: A BASIN #4 Lab ID: 30574814004 Collected: 04/03/23 07:45 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 2500 2.5 04/03/23 14:35 04/04/23 12:12 Sample: A BASIN #5 Lab ID: 30574814005 Collected: 04/03/23 07:55 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.9 % 0.10 1 04/04/23 09:25 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 2440 2.44 04/03/23 14:35 04/04/23 12:12 Sample: A BASIN #6 Lab ID: 30574814006 Collected: 04/03/23 08:00 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.3 % 0.10 1 04/04/23 09:25 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 2700 2.703 04/03/23 14:35 04/04/23 12:12 Sample: A BASIN #7 Lab ID: 30574814007 Collected: 04/03/23 08:05 Received: 04/03/23 12:10 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.3 % 0.10 1 04/04/23 09:27 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 2700 2.703 04/03/23 14:35 04/04/23 12:12 Date: 04/06/2023 05:15 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 10 I eAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: INFRAMARK-DANVILLE VA0060593 Pace Project No.: 30574814 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/06/2023 05:15 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 10 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: INFRAMARK-DANVILLE VA0060593 Pace Project No.: 30574814 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30574814001 A BASIN #1 SM 2540G-15 578212 30574814002 A BASIN #2 SM 2540G-15 578212 30574814003 A BASIN #3 SM 2540G-15 578212 30574814004 A BASIN #4 SM 2540G-15 578212 30574814005 A BASIN #5 SM 2540G-15 578212 30574814006 A BASIN #6 SM 2540G-15 578212 30574814007 A BASIN #7 SM 2540G-15 578212 30574814001 A BASIN #1 SM 9222D-2015 578374 SM 9222D-2015 578376 30574814002 A BASIN #2 SM 9222D-2015 578374 SM 9222D-2015 578376 30574814003 A BASIN #3 SM 9222D-2015 578374 SM 9222D-2015 578376 30574814004 A BASIN #4 SM 9222D-2015 578374 SM 9222D-2015 578376 30574814005 A BASIN #5 SM 9222D-2015 578374 SM 9222D-2015 578376 30574814006 A BASIN #6 SM 9222D-2015 578374 SM 9222D-2015 578376 30574814007 A BASIN #7 SM 9222D-2015 578374 SM 9222D-2015 578376 Date: 04/06/2023 05:15 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 10 O 4 4 {5 .� wx aC rcC � rcC KC 2 FC r.� rx: NS; �, I, �•n. z Z5 ij p' u u E y n o av m a c w ua .r.+ � .c � �, a a-, ra, •w a, rm a cti E nt Q m Z '9: a M w N4 0 2a •*t CSrz x: `+.... " w Pe Z7 W] A7 a .V QW JJ r 2 w p u + eua'�u �N a sa 0 i a av m CP U 4 -.n m a)9 4 ci a •• E r,y ?- z e•� m+> a v a E a a 5 E nw a r m tre m u v n ro e a n a s 0 0 O a � a c a s to s mQ aro m za s- -0uuc r >1 +r 1 41 .vi VJ ea m =M -H U7 V '. w �... H,�. d'rosxar�a cvcawa�xv diu:��': is U7 Cl b qJ Y-d a ri H Y r-I 'Si aJ M it •v-1 00 i.7 .ua a .-{ �a 4 Qu , 57, °H Vr i7, [!7 W 27 oS ua vn .-�. a a•a E a E va E rr re a7 ,.�i. v..CLm a 0 4 a n m vaty uw avi14 a CL aj �. .� .�.r r- 00 CL CS c C mu E u v fl k v a m c o 0 x ._ m o E r a i E w a= z 1 ' .. v as a C) 0 0 0 0 o I' 0 m as _ s p u Q i6,y a o c actr p e cam„ N6'j o.E � e E � I� v v r i , sa. E E E dIn (d LO Z > o ra u(Dr CC) dC) Cy� I-T miA\ C` > ° ll •Il- iceCL - co c C) va t> © CO m a ca ra a r> ra m u E - dcc ® m w- n a c�v cti ev N cu N �. a (9 dfl E Z 47 .. ^- is L"J cs. rn p 'E c+7 r"a m m 4 c N` '' U '> a �x:.i M. "". c..l p . +'a G� t„' r o c� �3 :a ac a i1i ' 't. rii M— y m p e— m a a v p c er ax v r v 0 m E ° E E m cup w 'n y > a ` �• ^ o cs a o w c a s- sx cc - - -• . co o. Q p ^'S Q: y m It 04 ©fi W RCS fwtS c+.S C] ts. m -a C'Y E QD y 0 a a a _ Gar > G "a CL m V IN LO cc 4/1 a E n f cC% r a u Gr1 CP? dlp CJ) {n co U) `c ° a a.. > o vim_. e "m a .p cu "* °- iE = cE as a C c E a o "•, r. i 3 a LIMS73 Lab Sample Condition Upon Receipt (West Virg WO,#:30574814 Client Name: PM: CEW Due Date. 04/13/23 CLIENT;: INFRAMARK Courier: [:] Fed Ex El UPS ❑ USPS XClient 17 Commercial Ll Pace L uiner: Tracking #: Custody Seal on CoolerlBoxXontainers Present: E yes no Seals intact: E yes E-1 no Thermometer Used 2,t Type of Ice: Blue None Cooler Temperature Observed Temp 2, e C Correction Factor: C Final Temp: C 1 Comments: 1 pH paper Loth Lute and Initials of person examining 1 contents; Yes No NIA Chain of Custody Present: 1, Chain of Custody Filled Out: 2. Chain of Custody Relinquished: 3. Sampler Name & Signature on COC: 4. Sample Labels match COC: -5. -Includes date/time/ID Matrix; Samples Arrived within Hold Time: 6. Short Hold Time Analysis (<72hr remaining): Rush Turn Around Time Requested: -7. 8, Sufficient Volume: S. Correct Containers Used: -Pace Containers Used: 10. Containers Intact Orthophosphate field filtered: 12. Hex Cr Aqueous sample field filtered: -pH adjusted within 24 hours? (if yes, indicate acid lot #) 13. Filtered volume received for Dissolved tests: 14. All containers have been checked for preservation: exceptions: VOA, coliform, O&G, LLIMercury, Non -aqueous matrix All containers meet method preservation requirements: 15. Initial when completed pate/time Samples provided to tab C/ Tests not preserved: Headspace in VOA Vials: Trip Blank Present: TripBlank Custody Seals Present: -.,/-16. 17. Initial when completed: IGrate. Client Notfficationi Resolution: Person Contacted: Comments/ Resolution: Dates Dime: Contacted By: Ll A check in this box indicates that additional information has been stored in ereports. *PM review is documented electronically in LIMS, when the Project Manager closes the SRF Review schedule in LIMS. The status may be reviewed in the Status section of the Workorder Edit Screen. A, C) SCUR-WV- rev.082219 M,eritech, Inc. Laboratory Certification No. 165 Report Date: 7/6/2023 Date Sample Rcvci: 5/23/2023 Vector Attraction Reduction / Aerobically Digested Sludge Q0 Day Test) Meritedi Work Order # 05232336 Sample: Danville #1 Composite 5/23/23 lotal S91ids Volatile Solids % Volatile Sqjids Week 1 1,25 O4 M12 Week., 1.17 0.61. 0,520 W—P- 1.06 0.56 O528 Week 4l 1M M4 0,538 Week-5 0,98 M2 M27 Van Kleek Reduction (%)� -6,24 I hereby certify that I have reviewed and approve these data. Laboratory Representative ftW M 1% - I I VMV11" I 6)342-4748 fax.(336)342-1522 x C> a ■ n rb -1 AA 4k Ci 01ul fj III q EK �o 4 1 > Ln Ln F- LU c 0 C CL I.L. UJ w z, CL a-, 7-a c, v 7 5. m LA 0 CP W r— rn 0 VI c cr cu �(Em cz 0 0 X -LV 0 c 0 raiEj 4 lu*li Ln E z 0 141 rq ammm cc QD rr� 10 -0 sk 0 11 M m 0 -0 > SEEN 0 V) ui w 0 u Z COY LZ E fdD 0 LU �Lo CD ce I a IN ANNUAL UAL PA"I"110CFN AND VECRM4 XFOW110 REDWrio Fo R (OXI" R uillles) Facwrlluty l ammne:, C;pcy a H),aa.nnvpppat Q l�m�°urmmmuct Number: IC�apD(b �pli'"`(6 y10005" apV Name: ayrmmmmh r cma npm,armm ucam @gym m niodm� �d"aramacvm I � 72,52, 3 l"'mm / 1 ��� 2.3 ................................................................................................. J'al togeunr Ra^duc tiicmunr (15A NCA " 027' A'(V.06) — l("]Ile ass iilarmdicaale level achieved and aaWn aatWe performed: "Ill «u pa A (d nmc/ac unnpr( 3 . 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I am aware tbaat th ire aam~cm Agmmiiific,aant placmunraallktles fur We certification inrc,CCmmdunug fine and irmmplmriiimmmnaaac,armt.''" A" anon 6ou.uki - lllyncrpce fla.an"uyncar ynrej)"urer" annae pared 'Fill a (ayl)e or print) a %j a��;'�(y11A .I r,;'a11 r 16,2i7It ISr; Brent C;ca h n`; lll: ireccorcrfpcmc,hnu c°l y(cwuvacei Land .pyappevName and T44 (ph"pruy plWau.hle)(type or prig) P210024 Ygnmaaaanure cnrPrepaauer* Date Signature cap"lll,a nd, Applier (H'aa.r)yrHCl]lflC( I.)a.a C m'p"nepamer 1s ayc,tlincd nrm 40 Crop R 14150 A(r) aamd 15ik N CAC C"r .1 102 (C,y( DIF=:.INR' If-C:plfRM PyCIFRF- 2..I1. (12/2 p('6) I eAnalytical wurmpacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 April 26, 2023 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: VA0060593 Pace Project No.: 30579756 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on April 18, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Cl'Yf oi'a, u�tf,C` Cynthia Walker cynthia.walker@pacelabs.com (800)999-0105 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 15 aceAnalytical www.pacallabs.cmim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: VA0060593 Pace Project No.: 30579756 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: VA0060593 Pace Project No.: 30579756 Lab ID Sample ID Matrix Date Collected Date Received 30579756001 A BASIN #1 Solid 04/18/23 08:00 04/18/23 15:30 30579756002 A BASIN #2 Solid 04/18/23 07:30 04/18/23 15:30 30579756003 A BASIN #3 Solid 04/18/23 07:55 04/18/23 15:30 30579756004 A BASIN #4 Solid 04/18/23 07:35 04/18/23 12:00 30579756005 A BASIN #5 Solid 04/18/23 07:50 04/18/23 12:00 30579756006 A BASIN #6 Solid 04/18/23 07:40 04/18/23 12:00 30579756007 A BASIN #7 Solid 04/18/23 08:05 04/18/23 12:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 aceAnalytical www.pacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: VA0060593 30579756 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30579756001 A BASIN #1 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30579756002 A BASIN #2 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30579756003 A BASIN #3 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30579756004 A BASIN #4 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30579756005 A BASIN #5 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30579756006 A BASIN #6 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30579756007 A BASIN #7 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30579756 Sample: A BASIN #1 Lab ID: 30579756001 Collected: 04/18/23 08:00 Received: 04/18/23 15:30 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.1 % 0.10 1 04/21/23 10:33 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 257 0.257 04/19/23 07:30 04/20/23 08:30 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30579756 Sample: A BASIN #2 Lab ID: 30579756002 Collected: 04/18/23 07:30 Received: 04/18/23 15:30 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.8 % 0.10 1 04/21/23 10:35 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 239 0.239 04/19/23 07:30 04/20/23 08:30 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30579756 Sample: A BASIN #3 Lab ID: 30579756003 Collected: 04/18/23 07:55 Received: 04/18/23 15:30 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.3 % 0.10 1 04/21/23 10:45 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 271 0.271 04/19/23 07:30 04/20/23 08:30 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30579756 Sample: A BASIN #4 Lab ID: 30579756004 Collected: 04/18/23 07:35 Received: 04/18/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.9 % 0.10 1 04/21/23 10:09 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 323 0.323 04/19/23 07:30 04/20/23 08:30 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30579756 Sample: A BASIN #5 Lab ID: 30579756005 Collected: 04/18/23 07:50 Received: 04/18/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.8 % 0.10 1 04/21/23 10:12 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 239 0.239 04/19/23 07:30 04/20/23 08:30 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30579756 Sample: A BASIN #6 Lab ID: 30579756006 Collected: 04/18/23 07:40 Received: 04/18/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.4 % 0.10 1 04/21/23 10:23 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 278 0.278 04/19/23 07:30 04/20/23 08:30 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30579756 Sample: A BASIN #7 Lab ID: 30579756007 Collected: 04/18/23 08:05 Received: 04/18/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.4 % 0.10 1 04/21/23 10:24 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform ND CFU/g 278 0.278 04/19/23 07:30 04/20/23 08:30 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 15 I eAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: VA0060593 Pace Project No.: 30579756 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 04/26/2023 12:03 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: VA0060593 Pace Project No.: 30579756 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30579756001 A BASIN #1 SM 2540G-15 582594 30579756002 A BASIN #2 SM 2540G-15 582594 30579756003 A BASIN #3 SM 2540G-15 582594 30579756004 A BASIN #4 SM 2540G-15 582594 30579756005 A BASIN #5 SM 2540G-15 582594 30579756006 A BASIN #6 SM 2540G-15 582594 30579756007 A BASIN #7 SM 2540G-15 582594 30579756001 A BASIN #1 SM 9222D-2015 582309 SM 9222D-2015 582310 30579756002 A BASIN #2 SM 9222D-2015 582309 SM 9222D-2015 582310 30579756003 A BASIN #3 SM 9222D-2015 582309 SM 9222D-2015 582310 30579756004 A BASIN #4 SM 9222D-2015 582309 SM 9222D-2015 582310 30579756005 A BASIN #5 SM 9222D-2015 582309 SM 9222D-2015 582310 30579756006 A BASIN #6 SM 9222D-2015 582309 SM 9222D-2015 582310 30579756007 A BASIN #7 SM 9222D-2015 582309 SM 9222D-2015 582310 Date: 04/26/2023 12:03 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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Environmental Laboratory Laboratory Certification No. 1.65 Report Date: 7/6/2023 Date Sample Rcvd: 5/23/2023 Vector Attraction Reduction Z Aerobically Digested Sludge (30 Day Test) Meritech Work Order # 05232337 Sample: Danville #2 Composite 5/23/23 Total Solids Volatile Solids Y-b Volatile Solids Week 1 1-88 O.97 0,519 Week 2 1.52 0.78 0,51.3, wekk3 1-39 0.72 0,522 Week 4 1.33, 0.70 M29 Week 5 1,43 075 0.521 Van Kleek Reduction (%)- 482 I hereby certify that I have reviewed and approve these data. &L Rair) cko- Laboratoty Representative A z t rD n IT FAFNN CY orl O-IG F cQ Or) R H Ln v ul Uh Vi Ul kill rD 4 4� III cn L'J 7L n ( -0 (D C4 cn 0 0 ;r- 0 LA C> > cn CA . ......... 0 0 E c a j ) rd 0 u ki CL wr ar kn ,6lidm m I 1�11-� 14 - V7 (3) El Ol a' LU ol cr wil Ell 0 C* 0 aj tit > m m-0 Ln W cu 00 . ..... 0 c --k lZ; m U, w 4-wn LU m VI +, ow �u m z tiff0 rn 0 am= Wi E -a < cc 0 CL m U Bu LL T3 Q 0) w cl: 0 ro 0 0 ui 25 0 E u > z 14- Uji 6- Xj < 7 0 I- V _0 E fu E cu > Al UJ 4.1 L.L 0 L0 ro 12 2 ANNUAL UAL PA"I"110CFN AND VECRM4 XFOW110NI REDWrim Fo R (OXI" R.muillles) Facwrllmty l ammne:, C ry dnH),a.nnvfflc Q I�m�°urmmmuct Number: IC�m�D(b �ali'"`(6 y10005" y;V] Name: ayraammh r Moinnolm,amm�unn 11c°,a"(icma :, �Gd"ara acmm 50 n023 ................................................................................................. 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('p��~�a�awy lknv,nad.;laa� ' pn, "p (yCD-�d��ay 1(aarmaa,yn� '�;' .�pp:. 1 �� an.aapaap".d; -5�11y �1da�robp c) A 6 ( ,ppd SL]r:anpnraan.:pdrrm �' Ap F y(�nynirn(( �., Sna Wc) �.L (ICyu vaa (.1�wbn ap"rp�( � (Ilua_pa.,a;daaaan( App, F; (i as danpdam�ad,adnnn( w tau vd da,naac «aad,mana n,adarrn um a9ama,u.na°rma �a�d,a;n naaua�a,wn a,ud paa;irhdadaura; CE "ON°IFICTI)N yuy''TAirC,jl ,NIEKI, (Weme cheek the ➢Iplpur'nmpm i agar; stateiimeiinat( UR "I c:cmr>pailf(r" uucawmdcmur 11penalty caurplawwr" that tpfacm IIpatpfacmgcmaiwm arcmquiilarc,uNnnucm,nts in 15AL NCAC 0:10 106 inn! tpfmcu cckmr aCrac�oum hm 11 A021" A 107 havehccn met." ......... ............................................................................................................................................................................................ y c,carfiify" uiina1lear pc.naaMy or isvv,, thaa1: the IIpaatpimca train ircmqm.afirements hm 15AL NR:?AC 0210L106 aaanaal the vector attractioin areducti any in 1 NCAC O:yT A 107 ]have not ymcmen armm&" QPlllc,ascm note if you check this s aatam mut attach an explanation why you ]have W anniaet one mmur ppadmth or the olmeca.an�ac�cmaaacmanc�:.,( " "pPn�iiv c cn�c„a°unm(ination has ppmc;mi urvmaade under mW a: i cc;.tion and smmpcsur"vpc«aplc:mcia munn accordance with 111cs system a emignc°apl to enmaame that qualified 1pc,:rsoinaaaacmlll lllmarcmp:mcmrlµy gather and c,vWtia e the incmfamarauraaatmaaana used to apllctc,rinmuianac, that the 1poaathugen and vector attraction na arca luc.t:ion rcnquiirc°,auraents lhave been met. I am aware tbaat th ire aam~cm significant pjpeinaaallkdes fur We certification inuc,CCaadung fine and irmmplariiimmmnaaac,armt.''" hArn Q(dma.nydy -1111mgjn.,ct l anaa((�,L ynrej)"arer" aanaC: arndp 'Fillc (ayl)c or print) a %j a��;'�(y11A .I r,;'a11 r "2i7It ISr; Timm (Wins; inns; 110irrd,d°(dar dmp° p dwd°hrJ("ad Servaces Land .pyappevName and T44 (ph"ay plWau.hle)(typa"; or prig) y 30 023 Ygnmaaaaure dnrPrepaaaenw* Date Signature dmp"lll,a nd, Applier (H'1a.r)yrHC1]1flC( I.)a.a C m'I"nepamer 1s dd incdy nrm 40 CroF R 141 :a6y: A(r) aamdy 15ik N CAC C"r .1 102 (C,y( DF=:.INR FURM PyCIFRF- 2..I1. (12/2 (('6) I eAnalytical wurmpacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 May 12, 2023 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: DANVILLE VA0060593 Pace Project No.: 30583218 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on May 01, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Cl'Yf oi'a, u�tf,C` Cynthia Walker cynthia.walker@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 15 aceAnalytical www.pacallabs.cmim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: DANVILLE VA0060593 Pace Project No.: 30583218 Lab ID Sample ID Matrix Date Collected Date Received 30583218001 A BASIN #1 Solid 05/01/23 07:30 05/01/23 12:00 30583218002 A BASIN #2 Solid 05/01/23 07:35 05/01/23 12:00 30583218003 A BASIN #3 Solid 05/01/23 07:40 05/01/23 12:00 30583218004 A BASIN #4 Solid 05/01/23 07:45 05/01/23 12:00 30583218005 A BASIN #5 Solid 05/01/23 07:50 05/01/23 12:00 30583218006 A BASIN #6 Solid 05/01/23 07:55 05/01/23 12:00 30583218007 A BASIN #7 Solid 05/01/23 08:00 05/01/23 12:00 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 aceAnalytical www.pacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: DANVILLE VA0060593 30583218 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30583218001 A BASIN #1 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30583218002 A BASIN #2 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30583218003 A BASIN #3 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30583218004 A BASIN #4 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30583218005 A BASIN #5 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30583218006 A BASIN #6 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30583218007 A BASIN #7 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Sample: A BASIN #1 Lab ID: 30583218001 Collected: 05/01/23 07:30 Received: 05/01/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.9 % 0.10 1 05/05/23 11:53 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Sample: A BASIN #2 Lab ID: 30583218002 Collected: 05/01/23 07:35 Received: 05/01/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.8 % 0.10 1 05/05/23 11:56 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Sample: A BASIN #3 Lab ID: 30583218003 Collected: 05/01/23 07:40 Received: 05/01/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.9 % 0.10 1 05/05/23 12:47 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Sample: A BASIN #4 Lab ID: 30583218004 Collected: 05/01/23 07:45 Received: 05/01/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 98.7 % 0.10 1 05/05/23 12:47 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Sample: A BASIN #5 Lab ID: 30583218005 Collected: 05/01/23 07:50 Received: 05/01/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 97.1 % 0.10 1 05/05/23 12:48 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Sample: A BASIN #6 Lab ID: 30583218006 Collected: 05/01/23 07:55 Received: 05/01/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.5 % 0.10 1 05/05/23 12:49 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: DANVILLE VA0060593 Pace Project No.: 30583218 Sample: A BASIN #7 Lab ID: 30583218007 Collected: 05/01/23 08:00 Received: 05/01/23 12:00 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 97.0 % 0.10 1 05/05/23 12:50 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <10 CFU/g 1.0 1 05/02/23 07:30 05/03/23 08:30 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 15 I eAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: DANVILLE VA0060593 Pace Project No.: 30583218 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/12/2023 03:20 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: DANVILLE VA0060593 Pace Project No.: 30583218 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30583218001 A BASIN #1 SM 2540G-15 586021 30583218002 A BASIN #2 SM 2540G-15 586021 30583218003 A BASIN #3 SM 2540G-15 586021 30583218004 A BASIN #4 SM 2540G-15 586021 30583218005 A BASIN #5 SM 2540G-15 586021 30583218006 A BASIN #6 SM 2540G-15 586021 30583218007 A BASIN #7 SM 2540G-15 586021 30583218001 A BASIN #1 SM 9222D-2015 585394 SM 9222D-2015 585499 30583218002 A BASIN #2 SM 9222D-2015 585394 SM 9222D-2015 585499 30583218003 A BASIN #3 SM 9222D-2015 585394 SM 9222D-2015 585499 30583218004 A BASIN #4 SM 9222D-2015 585394 SM 9222D-2015 585499 30583218005 A BASIN #5 SM 9222D-2015 585394 SM 9222D-2015 585499 30583218006 A BASIN #6 SM 9222D-2015 585394 SM 9222D-2015 585499 30583218007 A BASIN #7 SM 9222D-2015 585394 SM 9222D-2015 585499 Date: 05/12/2023 03:20 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 15 0 U C7 O p z N ✓1 ?i � ."+� ?+. 'N ?w �w }e �.+ }n .'+�. Y� .,�'y,t S7. � � � gyp" m ro u C 0 H is '• i. H... 4A 3.: c .N a % 'CY° Q p1 N Yf1 l " rV E.. m .µ C1 H p, 4 V E 'a C O '.. -p Ca 07 p tl➢ R°' C1 C 01 10 H w m p. +� �. �. U. U "N C .a.J N .mN `�^ U 'o .H H 0) C Cf] ". iW 9 N W 4 E'. 41 N E G m a W . w r m w .dl m Cn 0? .-1. U •H m N D 0 u C7 .. d "' -H .4Y "✓ 4d i� a.T. '.�," .-d ¢Y cn Al Ire +ow E m E W 6 0 d E. n -y 8 y m Q*�Ia y U f)] m. .Q 2". 0.1.4j as 0 Q9 °� I 3 tl p r C C •• �a m w h M^ U t3 tJ t J 'S- Q !a C wWd m G] 41 H m5, C Q� N 0 ? 0 m W«} ^H N 6t. Ud mH a! 'U pl Sy Sl rL C4 aP � s«4 NS H i3 +2 Ud N Cj ...«" O 0 L7 0 = 0 !� r"X 9b ^H H A Q w '-7 m. +- � 4 � C3 9 i, � add O m N -y rt C: ? 01 4 o.0 S:'. iJ U ui3 r.,} Ub V] «"`" � V3 m: C} m7 C4 Vb �-7 4-1 i-1 a� J oz <1 z.. m Q i �? m f1 Q1 .. a z C01 IQ nrll�CLE C m w C s : N a r- Q E E E v UJ. m io m rn 0N. m .` d allpals -@ y p .vim Z c C w a �' 0 G.J r _ ',, chi z E a ( �''� °� {"� ... ,„„„, a °� _ G' C?,. C3 O S� CY C] C3 pm mti mo '} m N 'IG... ...«. P 1.- CL :�. p .... c m c m m 4L- s ✓8 p pj N !. QC7 i '', t.. t A E m a CL Cy N,..., gym) w , r i a t CES, Ca m C] E CD ° tl w m Ln n Qj a w a p' &i a' E E O a, CL v a E s a S m E v i is p n t (i Z U' ..� C Ci a Q L �". CY)n °^ m 0 cj �? � � coo � ° v � 6`- P`- h� t- I° 1. - Cy E C) < .>' �e L] �p m O Cl) Cl) f`7.... S"'i co Cl) M p E CS am E z .y __ m �+-.. .- -E "� ea o f r C3 p C � G Z '7 G u 0t O C�J F`7 O Q tom.}. ii N fiJ Gl w V5oc, U'Y°1 > N P.�.. -{j"`.... O CS 0 at7 00 > co PLO'Q' r CD LoC a. 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Environmental Laboratory Laboratory Certification No. 165 Contact: Brent Collins Report Date: 7/6/2023 Client: EMA Resources, Inc 755 Yadkinville Road Mocksville, NC 27028 Date Sample Rcvd: 6/1/2023 Vector Attraction Reduction Aerobically Digested Sludge (30 Day Test) MeritechWot-kOrdet-# 06012309 Sample: Danville #3 Composite 6/1/23 Total Solids Volatile Solids Volatile Solids Week 1 1.16 0.61 0,522 LVggk 2 0.92 0,50 O�,542 We OAS 0.47 0.534 Week 4 0.86 0,48 0-558 Weigh 5 0.80 0.45 0.567 Van Kleek, Reduction (%)l: -19.99 I hereby certify that I have reviewed and approve these data. 4haana�:L 'Ha 4cs�z Y6, Laboratory Representative tel.(33,6)342-4748 fax.(336)342-1522 •; any III IV m I rA (yq uIt 51 54 rA FA 0 CD ft > 2 0. CL CL CL0. QU Ln o a U EX1. 6F X c y cj 1�3PN :�-' CL 0 wi 07 vi LL 0 kn -p tn LYJ W ci 0 CL w cn W LJ iA < u c 0 —M Ln in Lu r, rn r 0 U c ai 0 �o m 0 z kA to E "0 s U U-1 a, rd 0 Z E ro Qj o Gnaw (A un 0 CL E CL 0 1 0 0 0 0 u to %A D Ul -M 0 LAJ E v Z cq) ui C LY, -F, 4- V) C7 z aj -T CL m > U"l u It z E W I Z c E LD 41 m 1%0 * LU 0 E _0 a) a c 0 V) E, El E—] Fac—TllmCy l a:mmm c:, C ry a 11'D,,a.aavpppat WQ 114°armmmuCm:l iummmmpiaer:, WQ00365M 11"11 ] Name: Norllhsde °I"C'l MIDES Nuamaraber: VA0060593 N Camnnnpm,armrtin Period: Cd"nramnnm . 1p 5/1.023 "`pl"am r/p."(r`CC123 11,111mmm a;unr Wda ctiiamunr (15A I C". C 021T "C 1.06) - C("]Ile"'Isa, iilnradicaale level a aucpklieva;d aannra� amlllCa^arurr�aaC.(rva, p�a.urCamm�n�mmarmC: -- C "Ill «u :� pC A (pnnnicAcrrnpr( 0 77 ( ppa � rm amCrnnu nnC( � it C: (Illannuar @ a ��"Cnawaj,(( � CC i ) (No I)r"nuar T t) p' rear a ss w (uurrfpra it Reduce 1p' dry�numaa� F CC"mappllhiaralllallie �a(;aaiteraaave manrC'arnrmed (CCass.oinly( uumdiaatm"Piraaa aa to FuirillheirRReduce Pmthm�mms"': —-------—— —------............................ ornpr�C aa Drying (3 11at ra�(^ana`nrrnophdic....�: -- ---- - . Beta Kay C ar nrmrna Ray [3 6maas uMauirnraC,na.mra D ~ 717 pp (C( F u cal >n Cu nnsrn "' ` h- (`) Prarmm sr Crr S� gnnnpra anfly llR rflaam m P �r4ll�nrr��ens [ .. .. lI1 'aaCaipmlllmam-1lllml1c to IDCmanrnniaapaive IpamnrC'orinmaa . (Class ass CC amnnc111y( findica�mCma C nramcess to amCCnrmpiCiiicaintlly Reduce C��rtpfmamCCmannt�w"°'':, Ip arena---- ---- „arms-- —0 - ---- � ynr—I)rynrnr�-------------------C,'r t npo „ann g-- [3 CCcruu�una lll�n�nm�strrmn-0---------- Ana11leranl(uau .pC o sdon -- If as m lllicaahlla�Cto aal111cri nnm�llive pei°f'mmnr�amrmam�� � ass or Class 1 co m��o�e(tmr��alhe following�i�u�nmmumou��:mmriinnmq, dal:rm.( C "yaannfU as ppumvaaa�rpa C,amva;p �a n(:1rum;!a n p.Ca rawuC Fir�M°q ue na;y �yarnmrmrC,rpaa f n afynuaraap 11[nuu.r�aunm�aa°p;uar. .�.�.�.�.�.�.�.�.�.�.� .�.�.�.� .�.� .�.� .�.�.�.�.�.�.�.� .�.�.�.� .�.�.�.� lI �a~a aa.. aun� pruapge llIh uI CuCO. CCIA"rMArXir"rnmurn' Urnil,8 da.uaces of'Analn�^',!„ ly I@' rya, Ta;ck-vniquic 2 a 10 to the ° P 61,h proaaaver pet yr,ra�m�n ann "auulaap C'um (amrrna nano a0 aan o au FU 222 42 26") (ppl j l/((; 0 C u:raramC.aafl.) 0 SM9222CC p 000 anpnn pet yPd.aaa anlCaaaaA soh d Wiry vva;u,.;;-nr,ji "yaalln�aaana,lldan yraaa0a;n-a„:a e� l•✓111"'� pnnc;n" l yf;n<arr'rrnq (a t dnut auk f s.aaf tot�d SoNd ( fi°y arn'ndarunnai Weil"h,, -- Vector Attraction C edua,p:(«nnr (15A.1 C C:" 02 �1�" A (V.CCy"( - Please indicate aa]llrernaafive pl:merl' anrinnted: <u,.11 " maaaCaaa°4,pon�n) p4, �. (���� �a�awy lknv,a�aa.; a( Ape, "� (yCD �a��ay 1(naaaaa,Cn� � Apr:. � "� aa;a°,. Cy a�u.maCaap a; ( 1u��� Mt. 5 � p� p�aay �am�a�anpnpc( [ �pu 6 ( .ppm aL'Ar uaparaau.:pmrrn �' Apr F (p�ayartg .� �u�a(r1�( filly, 8 (Dl ypnayn (.lnnwbn ap�rpc( � Ah, 9 (Iluu_pa.,a;nnanan( All 10 (I na amrpon.i�,no n( �w uu vector «nf aaa rnamnm u"r.,chteuroru zdtc nnaadvc,,,n were preirkmane d;Ca; C1°CC,"CC:w "C°1CC:'CI TAlTEM E,1 ,'T (pIlaaasca aCack CCmas appropriate sCa tei meinit) UR "C a:a°;rCaH,, mmnndaaur 11puraamlllC.yar4' platwwr, C.hamC: C:ha°; IIpaC:plammgarain nreqmaiiinra,uNmnnr,nI:s in 1CC 0:11" A 10Cm and the a^a toir attraction nredmmamC:iawnn in 11 NCAC 0211"' "C 10Ilhave bacin mmrmeC:,�s '-'-I a,am,rfill. , muuawadler pcinaalty of laa �,, Chat C:p e IlpaaC;pimma again ireq utfiremen I's pima ISA NCAC 0211"' AL106 and the va,a toir attractictin nredmmcti inn fen 1 NCAC 0211"' "C 107 have not been met." (Please note pill' you check C:phiis statement attach aain a, polllaainnafimmnrm va�1hy you ]hnam c not mmnnet ammme many ppamntb mml° CpNe olmeq m.m irememmcC s.) "This miaaC:c,.,r°unni(iunamC(iamnnr has pNaanenrn made maunaCer only dam a a;.C:iaamni amunnml amml1peir pc«aplori mintn acoirthunc with 111c system da,siginla°d to maunnsum e Chat qualified ipm,:rsoinrnrammlll lllanrmnpl:maar lµy gather aaind evaluate Cllhe finfamirmaaC.mannnr m.ased to ap11a C:a,:rnrannpninic that Cpkaaa 1paaaCbogelin and vectur affiraa,C(iamunr reduction nraaaplaa(imra°,aanarnts 1puraa a been met. C am aware tbaat th ire aam~aa significant plaaaunraa]Ilfies C"a:mnr, CamllIse cerC:iC"pia;amC.ioinr finra,CCmadiiinig Mine aanrmm.0(iurmmplmnNmiiiaammm�ucmaa,nrmC:.''" Aiaa.nn 6ou.uki - 1111r"oje CL Iaunmar(na,rr ------------------------- C rej)"arerm" (arri pinup Titie (pyj)uC or print) (mC 6(0112( 111 Cr"uanma( C ;r fi n` -, 110(m"a ctorr arfp rich npcari Scr amass �Land .Cnpppa r N1.rrwnC aarnuti T4iC (p 'drj)PhCi1u.bpa)(Lyj)a"; or pr�rvt) p / 4 /'y',((24 Sig,nanCuurcrrH1rcf)11trcr* Date n(nn-aua.C.amra:Of] Alnd Applier(H'ua.r)CrHC,']r1r(e( 111Caftc n'PICPp arer is defile-uea( nrrn 40 CroF I�1PArrC 5019(r( aArin ( p 5A " CAC.' 2T . p p ((C, (26( DF=:.II IIFC FURM PyCIf'aClf'- 2..l1. (12/2006) I eAnalytical wurmpacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 May 23, 2023 Kimberly Wickemeyer Inframark 229 Northside Drive Danville, VA 24540 RE: Project: VA0060593 Pace Project No.: 30587678 Dear Kimberly Wickemeyer: Enclosed are the analytical results for sample(s) received by the laboratory on May 15, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Beaver • Pace Analytical Services - Lexington If you have any questions concerning this report, please feel free to contact me. Sincerely, Cl'Yf oi'a, u�tf,C` Cynthia Walker cynthia.walker@pacelabs.com Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 15 aceAnalytical www.pacallabs.cmim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 CERTIFICATIONS Project: VA0060593 Pace Project No.: 30587678 Pace Analytical Services Beaver 225 Industrial Park Road, Beaver, WV 25813 North Carolina DEQ 466 Virginia VELAP 460148 Kentucky Wastewater Certification KY90039 West Virginia DEP 060 Pennsylvania DEP 68-00839 West Virginia DHHR 00412CM Pace Analytical Services Lexington 782 North Lee Highway, Lexington, VA 24450 Virginia VELAP 460150 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE SUMMARY Project: VA0060593 Pace Project No.: 30587678 Lab ID Sample ID Matrix Date Collected Date Received 30587678001 A BASIN #1 Solid 05/15/23 07:35 05/15/23 12:44 30587678002 A BASIN #2 Solid 05/15/23 07:40 05/15/23 12:44 30587678003 A BASIN #3 Solid 05/15/23 07:45 05/15/23 12:44 30587678004 A BASIN #4 Solid 05/15/23 07:55 05/15/23 12:44 30587678005 A BASIN #5 Solid 05/15/23 08:00 05/15/23 12:44 30587678006 A BASIN #6 Solid 05/15/23 08:05 05/15/23 12:44 30587678007 A BASIN #7 Solid 05/15/23 08:10 05/15/23 12:44 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 15 aceAnalytical www.pacallaba.caim Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 SAMPLE ANALYTE COUNT Project: Pace Project No.: VA0060593 30587678 Analytes Lab ID Sample ID Method Analysts Reported Laboratory 30587678001 A BASIN #1 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30587678002 A BASIN #2 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30587678003 A BASIN #3 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30587678004 A BASIN #4 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30587678005 A BASIN #5 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30587678006 A BASIN #6 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE 30587678007 A BASIN #7 SM 2540G-15 AK 1 PASI-BV SM 9222D-2015 TLB1 1 PASI-LE PASI-BV = Pace Analytical Services - Beaver PASI-LE = Pace Analytical Services - Lexington REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30587678 Sample: A BASIN #1 Lab ID: 30587678001 Collected: 05/15/23 07:35 Received: 05/15/23 12:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.1 % 0.10 1 05/17/23 09:24 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <256.41 CFU/g 0.26 0.257 05/16/23 07:30 05/17/23 08:15 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 5 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30587678 Sample: A BASIN #2 Lab ID: 30587678002 Collected: 05/15/23 07:40 Received: 05/15/23 12:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.2 % 0.10 1 05/17/23 09:27 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <263.16 CFU/g 0.26 0.264 05/16/23 07:30 05/17/23 08:15 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30587678 Sample: A BASIN #3 Lab ID: 30587678003 Collected: 05/15/23 07:45 Received: 05/15/23 12:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 96.2 % 0.10 1 05/17/23 09:30 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <263.16 CFU/g 0.26 0.264 05/16/23 07:30 05/17/23 08:15 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30587678 Sample: A BASIN #4 Lab ID: 30587678004 Collected: 05/15/23 07:55 Received: 05/15/23 12:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.5 % 0.10 1 05/17/23 09:33 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <222.22 CFU/g 0.22 0.223 05/16/23 07:30 05/17/23 08:15 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 8 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30587678 Sample: A BASIN #5 Lab ID: 30587678005 Collected: 05/15/23 08:00 Received: 05/15/23 12:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.9 % 0.10 1 05/17/23 09:34 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <243.9 CFU/g 0.24 0.244 05/16/23 07:30 05/17/23 08:15 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 9 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30587678 Sample: A BASIN #6 Lab ID: 30587678006 Collected: 05/15/23 08:05 Received: 05/15/23 12:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.6 % 0.10 1 05/17/23 09:35 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <227.27 CFU/g 0.23 0.228 05/16/23 07:30 05/17/23 08:15 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 10 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 ANALYTICAL RESULTS Project: VA0060593 Pace Project No.: 30587678 Sample: A BASIN #7 Lab ID: 30587678007 Collected: 05/15/23 08:10 Received: 05/15/23 12:44 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual BVR Percent Moisture Analytical Method: SM 254OG-15 Pace Analytical Services - Beaver Percent Moisture 95.5 % 0.10 1 05/17/23 09:38 N2 LBIO Fecal Coliform By MF Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Lexington Fecal Coliform <222.22 CFU/g 0.22 0.223 05/16/23 07:30 05/17/23 08:15 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 11 of 15 I eAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALIFIERS Project: VA0060593 Pace Project No.: 30587678 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A complete list of accreditations/certifications is available upon request. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 05/23/2023 04:46 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 15 aceAnalytical www.pacallabsxom Pace Analytical Services, LLC 1638 Roseytown Road - Suites 2,3,4 Greensburg, PA 15601 (724)850-5600 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: VA0060593 Pace Project No.: 30587678 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 30587678001 A BASIN #1 SM 2540G-15 588627 30587678002 A BASIN #2 SM 2540G-15 588627 30587678003 A BASIN #3 SM 2540G-15 588627 30587678004 A BASIN #4 SM 2540G-15 588627 30587678005 A BASIN #5 SM 2540G-15 588627 30587678006 A BASIN #6 SM 2540G-15 588627 30587678007 A BASIN #7 SM 2540G-15 588627 30587678001 A BASIN #1 SM 9222D-2015 588379 SM 9222D-2015 588381 30587678002 A BASIN #2 SM 9222D-2015 588379 SM 9222D-2015 588381 30587678003 A BASIN #3 SM 9222D-2015 588379 SM 9222D-2015 588381 30587678004 A BASIN #4 SM 9222D-2015 588379 SM 9222D-2015 588381 30587678005 A BASIN #5 SM 9222D-2015 588379 SM 9222D-2015 588381 30587678006 A BASIN #6 SM 9222D-2015 588379 SM 9222D-2015 588381 30587678007 A BASIN #7 SM 9222D-2015 588379 SM 9222D-2015 588381 Date: 05/23/2023 04:46 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 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L() .2 (D (D a. a 00 0 L) 0 00 r-- E E z3 :3 uj Q E E z3 z3 uj UV 0 > 0 0 CL a) a) 0 LL LL oE 0 CL a) a) 0 L� % " I I L) c,4 0 'a -- cn C, C14 cn C, .2 .In Z w a 06 06 U Cl) L) CN L) CN 0 o r W Cl) W L) C6 0 -T �Z, G� cn 0 0 ca CL a E E cy? E E Co. m I cn :i m cn —i 0 CD .c E E m 6 2 CL N ry Final ALIdit If (;lPOII Cirea�ed!! 202A-01-26 By! ElireiM C.',(.-)Illlllins sLaWa! Signed "Firainsadloill ED!! CIB,JCII-ilIBCAAIBAAIN,7c.1111V�.JlpirnIBYa,JIIMu.usIpC)"r�irlr)41ll-ilCgirc.IZ5 I I C, ��, I'ignature Pages"IIHistory "ollkins [Docurneint cireated �by Bireint C. 2024-01-26 - b: 10:130 11PIM (.ill\All'- UP adder ess:: 206 8b 202.26 Docuivneint eirriadk-d k) A4n Gmfld (,�dain ould&infiraimairk coirn) foir slginahue 2024-01-26 - b: 1035 a=IIIM GIVIF Eirnadl vk..,wed Iby Alain (3,ould (alain goiJd&inf'n-.Iimai* curn) 2024-01 -?b - b:34:10 F"INA 1111=" addifo,au 166 nV n 15 22 2024-01-26 Docuivnee nt e4gined Iby Alain GOLAH (4ain goiJkl&infirairnairk coirn) SiI r im-Aime Datu 2024-01-26- h�31):48 PING A MT- IFm Suir Irrocc,�: ,-,cirv(,,ir- IlFladdires&� n66.13( 1 lb.22 ;.air Agireeirneint coirqpleted 2024-01-26- b:35:48 FlIM GIM ]IF s Adobe Acrobat Sign g a t i ...... . ........ (a�, g e s Final Audit Report Created: 2024-01-26 By: Brent Collins (brent.collins@emaresourcesinc.com) Status: Signed Transaction ID: CBJCHBCAABAA8g8mcAQJOUndNnNl7gxaqrl—GoQXXoOi "Signature Pages" History Document created by Brent Collins (brent.collins@emaresourcesinc.com) 2024-01-26 - 7:32:06 PM GMT- IP address: 206.85.202.26 Document emailed to Alan Johnson Oohnsra@danvilleva.gov) for signature 2024-01-26 - 7:32:11 PM GMT Email viewed by Alan Johnson (johnsra@danvilleva.gov) 2024-01-29 - 8:23:50 PM GMT- IP address: 216.146.48.10 Document e-signed by Alan Johnson (johnsra@danvilleva.gov) Signature Date: 2024-01-29 - 8:24:42 PM GMT - Time Source: server- IP address: 216.146.48.10 Agreement completed. 2024-01-29 - 8:24:42 PM GMT