WQ0006594_2023 Residual Annual Report_20240229 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0006594
Applicant/Permittee Unifi Manufacturing, Inc.
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:* Wastewater Irrigation High -Rate Infiltration
Other Wastewater Reclaimed Water
Closed -Loop Recycle Residuals
Single -Family Residence Wastewater Other
Irrigation
Permit Number:* WQ0006594
Has Current Existing permit number
Applicant/Permittee Address* PO Box 1437, Reidsville, NC 27323
Facility Name* Unifi Manufacturing Class A Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Unifi Annual Report - WQ0006594.pdf 12.8MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/29/2024

--Resources, Inc.
Unifi, Incorporated
2023 Annual Report
Residuals Land Application
Permit No. WQ0006594
Prepared By:
EMA Resources, Inc.
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

February 27, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report — Unifi, Incorporated
Treatment and Land Application of Residuals
Permit No. WQ0006594
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 139.19 dry tons of wastewater residuals
to 37.91 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
Brent Collins
Director of Technical Services
brent.collins&emaresourcesinc.com
Phone [phone] — Fax [phone]
755 Yadkinville Rd — Mocksville, NC 27028

CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM
WQ PERMIT #: WQ0006594 FACILITY NAME:
IWOWell X
Unifi, Incorporated
COUNTY: Rockingham OPERATOR: Unifi, Inc.
FACILITY TYPE (please check one): © Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C)
❑ Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes © No ❑ —op- If No skip parts A, B, C and certify form below
Part A*:
Part B*:
Month
Sources(s) (include NPDES # if
applicable)
Volume (dry tons)
Recipient Information
Amendment/
Bulking Agent
Residual In
Product Out
Name(s)
Volume (dry tons)
Intended use(s)
January
February
March
April
May
Unifi Inc. Plant No. 2 Reidsville
55.84
55.84
Lofton Lovelace
55.84
soil amendment
June
July
August
Unifi Inc. Plant No. 2 Reidsville
57.06
57.06
Kevin Knight
57.06
soil amendment
September
October
November
December
Unifi Inc. Plant No. 2 Reidsville
26.29
26.29
Lofton Lovelace
26.29
soil amendment
Total from FORM DMSDF (sup)
0
0
0
1
0
Totals:
Annual (dry tons):
0
139.19
139.19
139.19
Amendment(s) used: I I Bulking Agent(s) used:
* If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1
Part C:
Facility was compliant during the past calendar year with all conditions of the land application permit ® Yes
(including but not limited to items 1-3 below) issued by the Division of Water Quality: ❑ No 1, If No, Explain in Narritive
1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached.
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality.
No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Lira 1fa�iles
Lisa Haynes (Feb i, 202408:36 EST)
Signature of Permittee
01 /02/2024
Date Signature of Preparer**
(if different from Permittee)
**Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
Date
DENR FORM DMSDF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
WQ0006594 Laboratory:
Unifi, Incorporated
M-0104
WWTP Name: Unifi, Inc. Plant No.2 Reidsville
Recidnal AnAvcic Data
1)
2)
3)
4)
5)
Waypoint Analytical
Parameter
(mg/kg)
Conc.
Limit
(mg/kg a
Sample or Composite Date
1/5/23
4/5/23
7/10/23
10/5/23
Percent Solids (%)
NA
2.66
3.03
2.77
1.83
Arsenic
75
9.52
9.42
8.93
27.8
Cadmium
85
0.741
0.645
1.8
5.56
Copper
4,300
137
138
165
164
Chromium
NA
46.3
56.5
62.1
58.3
Lead
840
67.4
73.9
81.1
77.2
Mercury
57
0.249
0.716
0.81
1.24
Molybdenum
75
5
4.35
5.36
13.9
Nickel
420
16.3
19.3
21.80
22.3
Selenium
100
11.9
10.3
12.5
27.8
Zinc
7,500
574
626
707
700
Total Phosphorus
NA
2820
3290
3860
3390
TKN
NA
30700
21400
11100
19800
Ammonia -Nitrogen
NA
2470
3580
2970
7440
Nitrate and Nitrite
NA
178
32.3
6790
425
a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Ll;fa 1fa�as 01 /02/2024
Lisa Haynes (Feb , 202408:36 EST)
Signature of Preparer *
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number:
WQ0006594
Facility Name: Unifi, Incorporated
Residual Source
NPDES # or WQ#:
M-0104
WWTP Name: Unifi, Inc. Plant No.2 Reidsville
Residual Analvsis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
Sample or Composite Date
• 1
1 11
11
11
--------
•11
•
• 11
•111
11
1 11
--------
------------
------------
------------
------------
------------
------------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Li fa 1fa� a, r
Lisa Haynes (Feb , 2024 08:36 EST)
Signature of Preparer *
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
01 /02/2024
Date
DENR FORM RSSF - B (12/2006)

1 /5/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 16500 438.9 23 19.08261
Calcium 21600 574.56 20 28.728
Magnesium 7630 202.958 12 16.91317
Percent Solids 2.66
SAR 3.99
SAR
Na+
z (Ca2+ + M92+ )
19.08261
0.5( 28.728 2 + 16.91317 2 )

4/5/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 16000 484.8 23 21.07826
Calcium 24800 751.44 20 37.572
Magnesium 9740 295.122 12 24.5935
Percent Solids 3.03
SAR 3.78
SAR
Na+
z (Ca2+ + M92+ )
21.07826
0.5( 37.572 2 + 24.59350 2 )

7/10/2023
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
21400
592.78
23 25.77304
Calcium
30200
836.54
20 41.827
Magnesium
18100
501.37
12 41.78083
Percent Solids
2.77
SAR
3.99
SAR
Na+
z (Ca2+ + M92+ )
25.77304
0.5( 41.827 2 + 41.78083 2 )

10/5/2023
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
30700
561.81
23 24.42652
Calcium
25700
470.31
20 23.5155
Magnesium
13300
243.39
12 20.2825
Percent Solids
1.83
SAR
5.22
SAR
Na+
z (Ca2+ + M92+ )
24.42652
0.5( 23.516 2 + 20.28250 2 )

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Unifi, Inc.
WQ0006594
Donald Lovelace Owner:
9.24 Acres Permitted:
Total Dry Tons Applied (Annual): 18.89
Cation Exchange Capacity (non 503 only):
Lofton Lovelace Predominant Soil Series: CgB2
9.24 Site #: RC041 Field #: 5X
Residual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
610AMM
Com-
posite
Date
ME
an
no
no
Bonn
an
Boa
OEM
no
0
Total
Phos-
phorus
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
�
n
NEEMBEEMM
m
oose
EventNEW
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
®
1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2!:f—e 1/27/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Unifi, Inc.
Lofton Lovelace
Operator: Donald Lovelace
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0006594 Field #:
Annual Dry Tons Applied: 18.89 Site #:
Predominant Soil Series: Cg132
Crop 1 Max. PAN:
156.75 Crop 2 Name:
5X Acres Utilized
RC041 Acres Permitted:
Cation Exchange Capacity (non 503)
Crop 2 Max. PAN:
9.24
9.24
0
0
o
Volume applied
enter one Solids/
)
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#.
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
o
0 w
o
o
?:
°�0
��,
=
N
?:
TKN
mg/kg
Z a
o
qQ °
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/10
52000
3.03
0.711
Unifi
Dry
<.5"
S
0.5
1 0.3
21400
3580
1 32.3
10.194
NA
Fescue
5/15
97500
3.03
1.333
Unifi
Dry
<.5"
S
0.5
0.3
21400
3580
32.3
19.114
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
149500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
29.309
0.000
Lime Applied
Annuallbs/acre
0.039
0.003
0.564
0.231
0.302
0.003
0.018
0.079
0.042
2.559
13.450
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.039
0.003
0.564
0.231
0.302
0.003
0.018
0.079
0.042
2.559
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
156.75
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of tines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/27/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Unifi, Inc.
WQ0006594
Donald Lovelace Owner:
15.97 Acres Permitted:
Total Dry Tons Applied (Annual): 63.24
Cation Exchange Capacity (non 503 only):
Lofton Lovelace Predominant Soil Series: CgB2
15.97 Site #: RC041 Field #: 6X
Residual Analvsis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Com-
posite
Date
1 1
4/5/23
2
10/5/23
3
4 j
5
6
7
8 j
9
10 J
11
12
% Solids
3.03
1.83
Arsenic
9.42
27.8
Cadmium
0.645
5.56
Copper
138
164
Chromium
56.5
58.3
Lead
73.9
77.2
Mercury
0.716
1.24
Molyb-
denum
4.35
13.9
Nickel
19.3
22.3
Selenium
10.3
27.8
Zinc
626
700
Total
Phos-
horus
3290
3390
Annual Heavv Metal Field Loadings (Calculated in lbs/acre):
Total
E
•�e
NEW
NEEMBEEMBT/Ac./
os
Event
1 1
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1• •
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 •
1111
1111
1111
1111
1111
1111
1111
1111
1111
1111
®��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 • •
®
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1 1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
®
1 1:•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1•
®
1 1
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
®
: •
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
•
• 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
• : •
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2!:f—e 1/27/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

Facility Name:
Land Owner:
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Unifi, Inc.
Lofton Lovelace
Operator: Donald Lovelace
Crop 1 Name:
Fescue -Pasture
WQ Permit #: WQ0006594 Field #:
Annual Dry Tons Applied: 63.24 Site #:
Predominant Soil Series: Cg132
Crop 1 Max. PAN:
156.75 Crop 2 Name:
6X Acres Utilized
RC041 Acres Permitted:
Cation Exchange Capacity (non 503)
Crop 2 Max. PAN:
15.97
15.97
0
0
o
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#.
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
o
0 w
o
o
?:
°�0
��,
=
N
?:
TKN
mg/kg
Z a
o
qQ °
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
5/8
117000
3.03
0.926
Unifi
Dry
<.5"
S
0.5
1 0.3
21400
3580
1 32.3
13.271
NA
Fescue
5/9
123500
3.03
0.977
Unifi
Dry
<.5"
S
0.5
0.3
21400
3580
32.3
14.008
NA
Fescue
5/10
52000
3.03
0.411
Unifi
Dry
<.5"
S
0.5
0.3
21400
3580
32.3
5.898
NA
Fescue
12/14
169000
1.83
0.808
Unifi
Dry
<.5"
S
0.5
0.3
19800
7440
425
12.683
NA
Fescue
12/15
175500
1.83
0.839
Unifi
Dry
<.5"
S
0.5
0.3
19800
7440
425
13.171
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
637000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
59.032
0.000
Lime Applied
Annuallbs/acre
0.135
0.021
1.179
0.453
0.596
0.007
0.066
0.163
0.139
5.202
26.386
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.135
0.021
1.179
0.453
0.596
0.007
0.066
0.163
0.139
5.202
Permitted C. P. L. R.****
36
1 34
1 1338
267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 156.75
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of tines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/27/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: Unifi, Inc. Total Dry Tons Applied (Annual): 57.06
Permit #: WQ0006594 Cation Exchange Capacity (non 503 only):
Operator: Kevin Knight Owner: Kevin Knight Predominant Soil Series: Cgl32
Acres Used: 12.7 Acres Permitted: 12.7 Site #: RC134 Field #: 1X
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
610AMM
Com-
posite
Date
ME
an
no
no
Bonn
an
Boa
OEM
no
0
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
NEW
NEE
MBEEMM
moose
Event
1 1:1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:1
®
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
®
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
®
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1 ••
1 111
1111
1 111
1111
1111
1 111
1 111
1111
1111
1111
1 111
1 ••
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
Phos-
•:•
1 111
1111
1 111
1111
1111
1 111
1 111
1111
1111
1111
1 111
•:•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
2!: f. e 4;:; � 41-
1/27/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Unifi, Inc.
Land Owner: Kevin Knight
Operator: Kevin Knight
Crop 1 Name: Wheat
WQ Permit #: WQ0006594 Field #:
Annual Dry Tons Applied: 57.06 Site #:
Predominant Soil Series: CgB2
Crop 1 Max. PAN: 114 Crop 2 Name:
1X Acres Utilized
RC134 Acres Permitted:
Cation Exchange Capacity (non 503)
Crop 2 Max. PAN:
12.7
12.7
0
0
o
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
pp p
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#.
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
past 24
Hrs.
inches
a
o
0 w
o
o
?:
°�0
��,
=
N
?:
TKN
mg/kg
Z a
o
qQ °
�
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
8/17
97500
2.77
0.887
Unifi
Dry
<.5"
S
0.5
1 0.3
11100
2970
1 6790
19.002
NA
Fescue
8/18
71500
2.77
0.650
Unifi
Dry
<.5"
S
0.5
0.3
11100
2970
6790
13.935
NA
Fescue
8/21
71500
2.77
0.650
Unifi
Dry
<.5"
S
0.5
0.3
11100
2970
6790
13.935
NA
Fescue
8/22
78000
2.77
0.709
Unifi
Dry
<.5"
S
0.5
0.3
11100
2970
6790
15.202
NA
Fescue
8/23
78000
2.77
0.709
Unifi
Dry
<.5"
S
0.5
0.3
11100
2970
6790
15.202
NA
Fescue
8/24
97500
2.77
0.887
Unifi
Dry
<.5"
S
0.5
1 0.3
11100
2970
1 6790
19.002
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp
to this form):
TOTALS:
01
494000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
96.277
0.000
Lime Applied
Annuallbs/acre
0.080
0.016
1.483
0.558
0.729
0.007
0.048
0.196
0.112
6.353
34.686
Date
lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Current Cumulative lbs/ac
0.080
0.016
1.483
0.558
0.729
0.007
0.048
0.196
0.112
6.353
Permitted C. P. L. R.****
36
34
1 1338
267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 114
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of tines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/27/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
1 /16/2023
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-006-0004
Client Project Description: Reidsville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
www.waypointanalytical.com
Dear Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1 /6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
r
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Pa_
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
02/11/2023
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-006-0004
Page 2 of 8

(2)
2790 Whitten Road, Memphis, TN 38133
Waypoint Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-006-0004
Client Project Description: Reidsville, NC
Lab No Client Sample ID
90143 Unifi
Matrix Date Collected
Solids 01/05/202312:20
Date Received
O1/06/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Reidsville, NC
Lab Report Number: 23-006-0004
Date: 1 /16/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 99364
Analyte: Aluminum
QC Batch No: L657906/L657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Calcium
QC Batch No: L657906/L657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Iron
QC Batch No: L657906/L657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Potassium
QC Batch No: L657906/L657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 99364
Analyte: Manganese
QC Batch No: L657730/L657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 90143 (Unifi)
Analyte: Manganese
QC Batch No: L657906/L657395
Target analyte(s) was identified in the method blank associated with this project, below the Method Quantitation
Limit. Per laboratory protocol any associated affected sample result is flagged "B" to indicate that it was detected
in the method blank.
Sample 99364
Analyte: Lead
QC Batch No: L657730/L657395
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Reidsville, NC
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 01/16/2023
Received 0�1/06/2023
Connie Cook
Report Number :23-006-0004
REPORT OFANAL YSIS
Project
Manager
Lab No : 90143
Matrix:
Solids
Sample ID : Unifi
Sampled:
1/5/2023
12:20
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.3
%
1
01/06/2315:55
FMM
SW-DRYWT
Ammonia Nitrogen
24703
mg/Kg - dry
593
3700
1
01/16/23 14:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<178
mg/Kg - dry
178
178
1
01/09/23 14:25
ZBD
4500NO3F-2016
Organic N
282703
mg/Kg - dry
592.6
3704
1
01/16/23 10:30
CALCULATION
pH
7.7
S.U.
1
01/13/2313:23
SAR
9045D
Total Solids
2.66
%
0.010
0.010
1
01/09/23 15:55
FMM
2540G-2011
Total Volatile Solids
74.3
%
0.010
0.010
1
01/09/23 15:55
FMM
2540G-2011
Total Kjeldahl Nitrogen
30700
mg/Kg - dry
370
9260
1
01/16/23 10:30
JPJ iM-4500-NH3C-TKP
Phosphorus
2820
mg/Kg - dry
102
185
1
01/09/23 20:28
TJS
6010D
Aluminum
9520
mg/Kg - dry
171
185
1
01/09/23 20:28
TJS
6010D
Arsenic
9.52 J
mg/Kg - dry
8.89
18.5
1
01/09/23 20:28
TJS
6010D
Cadmium
<0.741
mg/Kg - dry
0.741
3.70
1
01/09/23 20:28
TJS
6010D
Calcium
21600
mg/Kg - dry
1430
1850
1
01/09/23 20:28
TJS
6010D
Chromium
46.3
mg/Kg - dry
8.74
9.26
1
01/09/23 20:28
TJS
6010D
Copper
137
mg/Kg - dry
11.5
18.5
1
01/09/23 20:28
TJS
6010D
Iron
4700
mg/Kg - dry
316
370
1
01/09/23 20:28
TJS
6010D
Lead
67.4
mg/Kg - dry
6.67
11.1
1
01/09/23 20:28
TJS
6010D
Magnesium
7630
mg/Kg - dry
95.6
185
1
01/09/23 20:28
TJS
6010D
Manganese
160 B
mg/Kg - dry
60.4
92.6
5
01/10/23 20:53
TJS
6010D
Mercury
<0.249
mg/Kg - dry
0.249
5.70
1
01/11/23 13:56
JTR
7471A
Molybdenum
<5.00
mg/Kg - dry
5.00
9.26
1
01/09/23 20:28
TJS
6010D
Nickel
16.3
mg/Kg - dry
4.44
9.26
1
01/09/23 20:28
TJS
6010D
Potassium
1610
mg/Kg - dry
229
370
1
01/09/23 20:28
TJS
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 5 of 8

0
Waypoint
2790 Whitten
Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Reidsville,
NC
Brent Collins
Report Date : 01/16/2023
755 Yadkinville Rd
Information :
Received : 01/06/2023
Mocksville , NC 27028
Connie Cook
Report Number :23-006-0004
REPORT OFANAL
YSIS
Project Manager
Lab No : 90143
Matrix: Solids
Sample ID : Unifi
Sampled: 1/5/2023 12:20
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<11.9
mg/Kg - dry
11.9
18.5 1 01/09/23 20:28 TJS 6010D
Sodium
16500
mg/Kg - dry
481
926 1 01/09/23 20:28 TJS 6010D
Zinc
574
mg/Kg - dry
30.0
46.3 1 01/09/23 20:28 TJS 6010D
Sulfur
6410
mg/Kg - dry
192
370 1 01/09/23 20:28 TJS 6010D
Sodium Absorption Ratio
4.03
Ratio
0.01
0.01 1 01/09/23 20:28 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 6 of 8

(2)
��nt,M 2790 Whitten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-006-0004
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T102
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Imakayla Weaver Date & Time: 01 /06/2023 10:57:08
Page 7 of 8

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Page 8 of 8

Waypointo
ANALYTICAL
4/13/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-096-0015
Client Project Description: Unifi
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
r
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Pa_
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-096-0015
Page 2 of 8

(2)
2790 Whitten Road, Memphis, TN 38133
Waypoint Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-096-0015
Client Project Description: Unifi
Lab No Client Sample ID Matrix Date Collected Date Received
93339 Unifi Solids 04/05/2023 09:17 04/06/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Unifi
Lab Report Number: 23-096-0015
Date: 4/13/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 93829 (#2)
Analyte: Aluminum
QC Batch No: L675666/L674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Calcium
QC Batch No: L675666/L674801
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 93829 (#2)
Analyte: Iron
QC Batch No: L675666/L674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Potassium
QC Batch No: L675666/L674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Magnesium
QC Batch No: L675666/L674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Sulfur
QC Batch No: L675666/L674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 93833 (San Elijo)
Analyte: Mercury
QC Batch No: L675254/L674948
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Unifi
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 04/13/2023
Received 0�4/06/2023
Connie Cook
Report Number :23-096-0015
REPORT OFANAL YSIS
Project
Manager
Lab No : 93339
Matrix:
Solids
Sample ID : Unifi
Sampled:
4/5/2023
9:17
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
96.9
%
1
04/10/2313:07
JLS
SW-DRYWT
Ammonia Nitrogen
3580
mg/Kg - dry
516
3230
1
04/13/23 13:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<32.3
mg/Kg - dry
32.3
161
1
04/11/23 12:54
ZBD
4500NO3F-2016
Organic N
17810
mg/Kg - dry
2848
5742
1
04/10/23 14:44
CALCULATION
pH
7.7
S.U.
1
04/11/2311:25
HBT
9045D
Total Solids
3.03
%
0.010
0.010
1
04/12/23 15:13
JLS
2540G-2011
Total Kjeldahl Nitrogen
21400
mg/Kg - dry
5740
1
04/10/23 14:44
ANH 4500NORGD-2011
Phosphorus
3290
mg/Kg - dry
89.0
161
1
04/11/23 04:46
JTR
6010D
Aluminum
10500
mg/Kg - dry
149
161
1
04/11/23 23:00
JTR
6010D
Arsenic
9.423
mg/Kg - dry
7.74
16.1
1
04/11/23 23:00
JTR
6010D
Cadmium
<0.645
mg/Kg - dry
0.645
3.23
1
04/11/23 23:00
JTR
6010D
Calcium
24800
mg/Kg - dry
1250
1610
1
04/11/23 23:00
JTR
6010D
Chromium
56.5
mg/Kg - dry
7.61
8.06
1
04/11/23 23:00
JTR
6010D
Copper
138
mg/Kg - dry
10.0
16.1
1
04/11/23 04:46
JTR
6010D
Iron
5100
mg/Kg - dry
275
323
1
04/11/23 04:46
JTR
6010D
Lead
73.9
mg/Kg - dry
5.81
9.68
1
04/11/23 23:00
JTR
6010D
Magnesium
9740
mg/Kg - dry
83.2
161
1
04/11/23 04:46
JTR
6010D
Manganese
173
mg/Kg - dry
10.5
16.1
1
04/11/23 23:00
JTR
6010D
Mercury
<0.716
mg/Kg - dry
0.716
5.94
1
04/10/23 14:14
FDS
7471A
Molybdenum
<4.35
mg/Kg - dry
4.35
8.06
1
04/11/23 04:46
JTR
6010D
Nickel
19.3
mg/Kg - dry
3.87
8.06
1
04/11/23 04:46
JTR
6010D
Potassium
1980
mg/Kg - dry
199
323
1
04/11/23 04:46
JTR
6010D
Selenium
<10.3
mg/Kg - dry
10.3
16.1
1
04/11/23 23:00
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoint
2790 Whitten
Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Unifi
Mr. Brent Collins
Report Date : 04/13/2023
755 Yadkinville Rd
Information :
Received : 04/06/2023
Mocksville , NC 27028
Connie Cook
Report Number :23-096-0015
REPORT OFANAL
YSIS
Project Manager
Lab No : 93339
Matrix: Solids
Sample ID : Unifi
Sampled: 4/5/2023 9:17
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
16000
mg/Kg - dry
419
806 1 04/11/23 23:00 JTR 6010D
Zinc
626
mg/Kg - dry
26.1
40.3 1 04/11/23 23:00 ]TR 6010D
Sulfur
6350
mg/Kg - dry
167
323 1 04/11/23 23:00 JTR 6010D
Sodium Absorption Ratio
3,83
Ratio
0.01
0.01 1 04/11/23 04:46 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 6 of 8

(2)
��nt,M 2790 Whitten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-096-0015
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T135
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: jEmily M. Peterson Date & Time: 04/06/2023 09:29:12
Page 7 of 8

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Page 8 of 8

Waypointo
ANALYTICAL
7/28/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-192-0033
Client Project Description: Unifi
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 7/11/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
r
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Pa_
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-192-0033
Page 2 of 9

(2)
2790 Whitten Road, Memphis, TN 38133
Waypoint Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-192-0033
Client Project Description: Unifi
Lab No Client Sample ID Matrix Date Collected Date Received
97971 Unifi Solids 07/10/202312:00 07/11/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Unifi
Lab Report Number: 23-192-0033
Date: 7/28/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 97975 (Shelby WTP)
Analyte: Aluminum
QC Batch No: L693030/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Arsenic
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97975 (Shelby WTP)
Analyte: Calcium
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 97975 (Shelby WTP)
Analyte: Chromium
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Copper
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Iron
QC Batch No: L693030/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Potassium
QC Batch No: L693030/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample 97975 (Shelby WTP)
Analyte: Magnesium
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Manganese
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Lead
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Sulfur
QC Batch No: L692735/L692238
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 97975 (Shelby WTP)
Analyte: Selenium
QC Batch No: L692735/L692238
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 97975 (Shelby WTP)
Analyte: Mercury
QC Batch No: L692588/L692341
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Unifi
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 07/28/2023
Received 0�7/11/2023
Connie Cook
Report Number :23-192-0033
REPORT OFANAL YSIS
Project
Manager
Lab No : 97971
Matrix:
Solids
Sample ID : Unifi
Sampled:
7/10/2023
12:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.2
%
1
07/14/23 18:53
KDO
SW-DRYWT
Ammonia Nitrogen
29703
mg/Kg - dry
571
3570
1
07/28/23 07:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
6790
mg/Kg - dry
35.7
179
1
07/13/23 14:50
CLP
4500NO3F-2016
Organic N
81713
mg/Kg - dry
5214
10500
1
07/17/23 13:42
CALCULATION
pH
5.9
S.U.
1
07/12/2317:00
CNB
9045D
Total Solids
2.77
%
0.010
0.010
1
07/14/23 18:53
KDO
2540G-2011
Total Volatile Solids
69.9
%
0.010
0.010
1
07/14/23 18:53
KDO
2540G-2011
Total Kjeldahl Nitrogen
11100
mg/Kg - dry
10500
1
07/17/23 13:42
ANH 4500NORGD-2011
Phosphorus
3860
mg/Kg - dry
100
179
1
07/13/23 23:39
TJS
6010D
Aluminum
14100
mg/Kg - dry
166
179
1
07/13/23 23:39
BKN
6010D
Arsenic
<8.93
mg/Kg - dry
8.93
17.9
1
07/13/23 23:39
TJS
6010D
Cadmium
1.803
mg/Kg - dry
1.79
3.57
1
07/13/23 23:39
TJS
6010D
Calcium
30200
mg/Kg - dry
1380
1790
1
07/13/23 23:39
TJS
6010D
Chromium
62.1
mg/Kg - dry
8.93
8.93
1
07/13/23 23:39
TJS
6010D
Copper
165
mg/Kg - dry
10.7
17.9
1
07/13/23 23:39
TJS
6010D
Iron
5640
mg/Kg - dry
305
357
1
07/13/23 23:39
TJS
6010D
Lead
81.1
mg/Kg - dry
7.14
10.7
1
07/13/23 23:39
TJS
6010D
Magnesium
18100
mg/Kg - dry
92.9
179
1
07/13/23 23:39
TJS
6010D
Manganese
214
mg/Kg - dry
12.5
17.9
1
07/13/23 23:39
TJS
6010D
Mercury
<0.807
mg/Kg - dry
0.807
6.68
1
07/13/23 11:15
MRE
7471A
Molybdenum
<5.36
mg/Kg - dry
5.36
8.93
1
07/13/23 23:39
TJS
6010D
Nickel
21.8
mg/Kg - dry
5.36
8.93
1
07/13/23 23:39
TJS
6010D
Potassium
2130
mg/Kg - dry
221
357
1
07/13/23 23:39
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

0
Waypoint
2790 Whitten
Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Unifi
Mr. Brent Collins
Report Date : 07/28/2023
755 Yadkinville Rd
Information :
Received : 07/11/2023
Mocksville , NC 27028
Connie Cook
Report Number :23-192-0033
REPORT OFANAL
YSIS
Project Manager
Lab No : 97971
Matrix: Solids
Sample ID : Unifi
Sampled: 7/10/2023 12:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<12.5
mg/Kg - dry
12.5
17.9 1 07/13/23 23:39 TJS 6010D
Sodium
21400
mg/Kg - dry
464
893 1 07/13/23 23:39 TJS 6010D
Zinc
707
mg/Kg - dry
30.4
44.6 1 07/13/23 23:39 TJS 6010D
Sulfur
7390
mg/Kg - dry
186
357 1 07/13/23 23:39 TJS 6010D
Sodium Absorption Ratio
4.01
Ratio
0.01
0.01 1 07/13/23 23:39 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

(2)
��nt,M 2790 Whitten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-192-0033
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T135
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: jEmily M. Peterson Date & Time: 07/11/2023 10:11:10
Page 8 of 9

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Page 9 of 9

Waypointo
ANALYTICAL
10/18/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-279-0051
Client Project Description: Unifi
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a' -'symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
r
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Pa_
Page 1 of 11

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-279-0051
Page 2 of 11

(2)
2790 Whitten Road, Memphis, TN 38133
Waypoint Main 901.213.2400 ° Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-279-0051
Client Project Description: Unifi
Lab No Client Sample ID Matrix Date Collected Date Received
99271 Sludge Solids 10/05/202314:00 10/06/2023
Page 3 of 11

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Unifi
Lab Report Number: 23-279-0051
Date: 10/18/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 81146 (Land Applied Sludge)
Analyte: Aluminum
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Arsenic
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Arsenic
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Calcium
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Cadmium
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Cadmium
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Chromium
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Chromium
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 11

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample 81146 (Land Applied Sludge)
Analyte: Copper
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Copper
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Iron
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Iron
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Potassium
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Potassium
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Magnesium
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Manganese
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Manganese
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Molybdenum
Page 5 of 11

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Molybdenum
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Sodium
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Sodium
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Nickel
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Nickel
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Phosphorus
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Lead
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Lead
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Sulfur
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Page 6 of 11

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
www.waypointanalytical.com
Sample 81146 (Land Applied Sludge)
Analyte: Selenium
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Selenium
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81146 (Land Applied Sludge)
Analyte: Zinc
QC Batch No: L710015/L709635
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81146 (Land Applied Sludge)
Analyte: Zinc
QC Batch No: L710352/L709635
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 7 of 11

Waypointo
ANALYTICAL
46245
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville , NC 27028
Project Unifi
Information :
2790 Whitten Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
www.waypointanalytical.com
Report Date : 10/18/2023
Received 1�0/06/2023
Connie Cook
Report Number :23-279-0051
REPORT OFANAL YSIS
Project
Manager
Lab No : 99271
Matrix:
Solids
Sample ID : Sludge
Sampled:
10/5/2023
14:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.2
%
1
10/06/2316:00
CAH
SW-DRYWT
Ammonia Nitrogen
7440
mg/Kg - dry
889
5560
1
10/18/23 14:37
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
425
mg/Kg - dry
55.6
278
1
10/11/23 15:32
CLP
4500NO3F-2016
Organic N
<19780
0% - dry
9833
19780
1
DH
CALCULATION
pH
7.8
S.U.
1
10/11/2317:00
CNB
9045D
Total Solids
1.83
%
0.010
0.010
1
10/06/23 16:00
CAH
2540G-2011
Total Kjeldahl Nitrogen
<19800
mg/Kg - dry
19800
1
10/10/23 15:15
ANH 4500NORGD-2011
Phosphorus
3390
mg/Kg - dry
156
278
1
10/10/23 17:59
TJS
6010D
Aluminum
12200
mg/Kg - dry
258
278
1
10/10/23 17:59
TJS
6010D
Arsenic
<27.8
mg/Kg - dry
13.9
27.8
1
10/10/23 17:59
TJS
6010D
Cadmium
<5.56
mg/Kg - dry
2.78
5.56
1
10/10/23 17:59
TJS
6010D
Calcium
25700
mg/Kg - dry
2150
2780
1
10/10/23 17:59
TJS
6010D
Chromium
58.3
mg/Kg - dry
13.9
13.9
1
10/10/23 17:59
TJS
6010D
Copper
164
mg/Kg - dry
16.7
27.8
1
10/10/23 17:59
TJS
6010D
Iron
6000
mg/Kg - dry
475
556
1
10/10/23 17:59
TJS
6010D
Lead
77.2
mg/Kg - dry
11.1
16.7
1
10/10/23 17:59
TJS
6010D
Magnesium
13300
mg/Kg - dry
144
278
1
10/10/23 17:59
TJS
6010D
Manganese
206
mg/Kg - dry
19.4
27.8
1
10/10/23 17:59
TJS
6010D
Mercury
<1.24
mg/Kg - dry
1.24
10.3
1
10/10/23 12:00
MRE
7471A
Molybdenum
<13.9
mg/Kg - dry
8.33
13.9
1
10/10/23 17:59
TJS
6010D
Nickel
22.3
mg/Kg - dry
8.33
13.9
1
10/10/23 17:59
TJS
6010D
Potassium
1910
mg/Kg - dry
344
556
1
10/10/23 17:59
TJS
6010D
Selenium
<27.8
mg/Kg - dry
19.4
27.8
1
10/10/23 17:59
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 8 of 11

0
Waypoint
2790 Whitten
Road, Memphis, TN 38133
Main 901,213,2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Unifi
Mr. Brent Collins
Report Date : 10/18/2023
755 Yadkinville Rd
Information :
Received : 10/06/2023
Mocksville , NC 27028
Connie Cook
Report Number :23-279-0051
REPORT OFANAL
YSIS
Project Manager
Lab No : 99271
Matrix: Solids
Sample ID : Sludge
Sampled: 10/5/2023 14:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Sodium
30700
mg/Kg - dry
722
1390 1 10/10/23 17:59 TJS 6010D
Zinc
700
mg/Kg - dry
47.2
69.4 1 10/10/23 17:59 TJS 6010D
Sulfur
8110
mg/Kg - dry
289
556 1 10/10/23 17:59 TJS 6010D
Sodium Absorption Ratio
5.19
Ratio
0.01
0.01 1 10/10/23 17:59 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions MQL Method Quantitation Limit
J Estimated value
Page 9 of 11

(2)
��nt,M 2790 Whitten Road, Memphis, TN 38133
Wayl?
Main 901.213.2400 ° Fax [phone]
N A LYT I C A L www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-279-0051
Shipping Method
Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
T100
Shipping container/cooler uncompromised?
# Yes
0 No
Number of coolers/boxes received
I '
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
Yes
0 No
COC properly completed
Yes
0 No
Samples in proper containers?
Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
0 N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr)
High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes 0 No
Comments:
Signature: Icarleen Qualls Date & Time: 10/06/2023 10:44:47
Page 10 of 11

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Page 11 of 11

(:�;a'ne A nalXical "'ANALYTIREPORT
January 16, 2023
zTc
Ss
EMA Resources 3
Sample Delivery Group: L1573612 [Cn]
Samples Received: 01/06/2023
Project Number: FSr
Description: Sludge 1QC1
E
Report To: Mr. Brent Collins
755 Yadkinville Road CAI
Mocksville, NC 27028
FSCI
Entire Report Reviewed By
zzt'�� V�
Reagan Johnson
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accwacy of the information provided,
and as the samples are received.
mdlh AP
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573612 01/16/2311:53 1 of23

TABLE OF CONTENTS
Cp: Cover Page
1
1-CP1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
ISS]
UNIFI L1573612-01
5
[Cn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Isr
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
1QC1
Wet Chemistry by Method D93/1010A
10
GI
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
CAI
Volatile Organic Compounds (GC/MS) by Method 8260D
14
Chlorinated Acid Herbicides (GC) by Method 8151A
16
ISCI
Pesticides (GC) by Method 8081B
17
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
18
GI: Glossary of Terms
20
Al: Accreditations & Locations
21
Sc: Sample Chain of Custody
22
ACCOUNT: PROJECT: S DG:
DATE /TIME:
PAGE:
EMA Resources L1573612
01/16/2311:53
2 of23

UNIFI L1573612-01 Waste
Collected by
BRENT COLLINS
Collected date/time
01/05/2312:20
Received date/time
01/06/2309:00
Cp
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
RC
Preparation by Method 1311
WG1984764
1 01/07/2313:16
01/07/2313:16
BTP
Mt. Juliet, TN
Preparation by Method 1311
WG1984782
1 01/07/2315:30
01/07/2315:30
BTP
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1983961
1 01/09/2317:11
01/10/2314:42
CAT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1986127
1 01/11/2311:00
01/13/2319:30
AW
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1985927
1 01/10/2310:20
01/10/2312:00
SIDE
Mt. Juliet, TN
Rn
Wet Chemistry by Method D93/1010A
WG1987120
1 01/12/23 02:25
01/12/23 02:25
TOP
Mt. Juliet, TN
Mercury by Method 7470A
WG1985082
1 01/08/2317:27
01/09/2314:29
SRT
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1985249
1 01/09/2314:05
01/09/2318:49
ZSA
Mt. Juliet, TN
FSr
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1985098
1 01/09/2316:53
01/09/2316:53
ACG
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1985228
1 01/12/23 08:21
01/13/2319:29
JMB
Mt. Juliet, TN
1QC1
Pesticides (GC) by Method 8081B
WG1985657
1 01/11/2310:45
01/12/2316:07
RDH
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1985658
1 01/13/23 05:38
01/13/2314:21
JRM
Mt. Juliet, TN
F
CAI
FSCI
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1573612
01/16/23
11:53
3 of 23

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the [—CP]
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOO) values reported for environmental samples 17C
have been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my ISS]
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
I
Sr
5
QC
GI
Reagan Johnson CAI
Project Manager
Project Narrative I _SC
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1573612 01/16/2311:53 4 of23

SAMPLE RESULTS - 01
L1573612
UNIFI
Collected date/time: 01/05/23 12:20
Preparation by Method 1311
Result Qualifier Prep
Batch
Analyte
date / time
TCLP Extraction
1/7/2023 3:30:14 PM
WG1984782
TCLP ZHE Extraction
- 1/7/2023 1:16:01 PM
WG1984764
Fluid
1 1/7/2023 3:30:14 PM
WG1984782
Initial pH
8.08 1/7/2023 3:30:14 PM
WG1984782
Final pH
4.80 1/7/2023 3:30:14 PM
WG1984782
Wet Chemistry by Method 9012 B
Result Qualifier RDL
Analyte mg/kg mg/kg
Reactive Cyanide ND 0.250
Wet Chemistry by Method 9034-9030B
Dilution Analysis Batch
date / time
1 01/10/202314:42 WG1983961
Result Qualifier RDL Dilution Analysis Batch
Analyte mg/kg mg/kg date / time
Reactive Sulfide ND 75.0 1 01/13/202319:30 WG1986127
Wet Chemistry by Method 9045D
Result Qualifier Dilution Analysis
Analyte su date / time
Corrosivity by pH 7.82 T8 1 01/10/202312:00
Sample Narrative:
L1573612-01 WG1985927: 7.82 at 20.3C
Wet Chemistry by Method D93/1010A
Result
Analyte Deg. F
Ignitability DNI at 170
Mercury by Method 7470A
Qualifier Dilution Analysis
date/time
1 01/12/2023 02:25
Result Qualifier RDL Limit
Analyte mg/I mg/I mg/I
Mercury ND 0.0100 0.20
Metals (ICP) by Method 6010D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic
Compounds (GC/MS) by Method
8260D
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Benzene
ND
0.0500
0.50
Carbon tetrachloride
ND
0.0500
0.50
Chlorobenzene
ND
0.0500
100
Chloroform
ND
0.250
6
ACCOUNT:
PROJECT:
LIMA Resources
Batch
WG1985927
Batch
WG1987120
Dilution Analysis
date / time
1 01/09/202314:29
Batch
WG1985082
Dilution Analysis
Batch
date / time
1 01/09/202318:49
WG1985249
1 01/09/202318:49
WG1985249
1 01/09/202318:49
WG1985249
1 01/09/202318:49
WG1985249
1 01/09/202318:49
WG1985249
1 01/09/202318:49
WG1985249
1 01/09/202318:49
WG1985249
Dilution Analysis
Batch
date / time
1 01/09/202316:53
WG1985098
1 01/09/202316:53
WG1985098
1 01/09/202316:53
WG1985098
1 01/09/202316:53
WG1985098
SDG:
DATE/TIME: PAGE:
L1573612
01/16/23 11:53 5 of 23

UNIFI
SAMPLE RESULTS
- 01
Collected date/time: 01/05/23 12:20
L1573612
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
FPAnalyte
mg/l
mg/l
mg/1
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1
01/09/202316:53
WG1985098
ITC
1,1-Dichloroethene
ND
0.0500
0.70
1
01/09/202316:53
WG1985098
2-Butanone (MEK)
ND
0.500
200
1
01/09/202316:53
WG1985098
Tetrachloroethene
ND
0.0500
0.70
1
01/09/202316:53
WG1985098
Rs
Trichloroethene
ND
0.0500
0.50
1
01/09/202316:53
WG1985098
Vinyl chloride
ND
0.0500
0.20
1
01/09/202316:53
WG1985098
Rn
(S) Toluene-d8
108
80.0-120
011091202316:53
WG1985098
(S)4-Bromofluorobenzene
102
77.0-126
011091202316:53
WG1985098
(S)1,2-Dichloroethane-d4
90.1
70.0-130
011091202316:53
WG1985098
Chlorinated Acid Herbicides (GC) by
Method 8151A
PC]
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/l
mg/l
mg/1
date/time
GI
2,4,5-TP (Silvex)
ND
0.00200
1
1
01/13/202319:29
WG1985228
2,4-D
ND
0.00200
10
1
01/13/202319:29
WG1985228
s
(S) 2,4-Dichlorophenyl Acetic Acid
82.5
14.0-158
011131202319:29
WG1985228
AI
Pesticides (GC) by Method 8081B
FSCI
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/l
mg/l
mg/1
date/time
Chlordane
ND
0.00500
0.03
1
01/12/202316:07
WG1985657
Endrin
ND
0.00500
0.02
1
01/12/202316:07
WG1985657
Heptachlor
ND
0.00500
0.0080
1
01/12/202316:07
WG1985657
Heptachlor epoxide
ND
0.00500
0.0080
1
01/12/202316:07
WG1985657
Lindane
ND
0.00500
0.40
1
01/12/202316:07
WG1985657
Methoxychlor
ND
0.00500
10
1
01/12/202316:07
WG1985657
Toxaphene
ND
0.0100
0.50
1
01/12/202316:07
WG1985657
(S) Decochlorobiphenyl
53.8
10.0-128
011121202316:07
WG1985657
(S) Tetrochloro-m-xylene
31.9
10.0-127
011121202316:07
WG1985657
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Qualifier RDL
Limit
Dilution
Analysis
Batch
Analyte
mg/l
mg/l
mg/1
date/time
1,4-Dichlorobenzene
ND
0.100
7.50
1
01/13/202314:21
WG1985658
2,4-Dinitrotoluene
ND
0.100
0.13
1
01/13/202314:21
WG1985658
Hexachlorobenzene
ND
0.100
0.13
1
01/13/202314:21
WG1985658
Hexachloro-1,3-butadiene
ND
0.100
0.50
1
01/13/202314:21
WG1985658
Hexachloroethane
ND
0.100
3
1
01/13/202314:21
WG1985658
Nitrobenzene
ND
0.100
2
1
01/13/202314:21
WG1985658
Pyridine
ND
0.100
5
1
01/13/202314:21
WG1985658
3&4-Methyl Phenol
ND
0.100
400
1
01/13/202314:21
WG1985658
2-Methylphenol
ND
0.100
200
1
01/13/202314:21
WG1985658
Pentachlorophenol
ND
0.100
100
1
01/13/202314:21
WG1985658
2,4,5-Trichlorophenol
ND
0.100
400
1
01/13/202314:21
WG1985658
2,4,6-Trichlorophenol
ND
0.100
2
1
01/13/202314:21
WG1985658
(S) 2-Fluorophenol
32.6
10.0-120
011131202314:21
WG1985658
(S) Phenol-d5
19.7
10.0-120
011131202314:21
WG1985658
(S) Nitrobenzene-d5
57.3
10.0-127
011131202314:21
WG1985658
(S) 2-Fluorobiphenyl
61.5
10.0430
011131202314:21
WG1985658
(S)2,4,6-Tribromophenol
71.0
10.0455
011131202314:21
WG1985658
(S) p-Terphenyl-d14
82.0
10.0-128
011131202314:21
WG1985658
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1573612
01/16/2311:53
6 of23

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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
Intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
Sample ID, Sample Matrix, Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
RDL
Reported Detection Limit.
Rec.
Recovery.
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
u
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
E
The analyte concentration exceeds the upper limit of the calibration range of the instrument established by the initial
calibration (ICAL).
J3
The associated batch QC was outside the established quality control range for precision.
J6
The sample matrix Interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1573612 01/16/2311:53 20 of23

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-05-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TNO02
California
2932�
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolina'
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhode Island
LA000356
Kentucky's
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
AI30792
Tennessee
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TNO03
Vermont
VT2006 _
Michigan
9958
Virginia
110033
Minnesota
047-999-305
Washington _
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A2LA
A2LA — 150 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025'
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks ' Aquatic Toxicity 4 Chemical/Microbiological ' Mold ' Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
ACCOUNT: PROJECT: SDG: DATE/TIME:
LMA Resources L1573612 01/16/2311:53
PAGE:
21 of 23

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2023 Unifi Annual Report - WQ0006594
Final Audit Report 2024-02-01
Created: 2024-02-01
By: Brent Collins ([e-mail])
Status: Signed
Transaction ID: CBJCHBCAABAA4y6OKv3hfQaKkrh4PUIFMXXylhOnMtg7
"2023 Unifi Annual Report - WQ0006594" History
Document created by Brent Collins ([e-mail])
2024-02-01 - 1:30:19 PM GMT- IP address: 206.85.202.26
P-► Document emailed to Lisa Haynes ([e-mail]) for signature
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Document e-signed by Lisa Haynes ([e-mail])
Signature Date: 2024-02-01 - 1:36:33 PM GMT - Time Source: server- IP address: 173.94.201.27
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