WQ0003351_2023 Residual Annual Report_20240229 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0003351
Applicant/Permittee Town of Mocksville
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Brent Collins
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3363993646
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0003351
Has Current Existing permit number
Applicant/Permittee Address*
171 Clement Street, Mocksville, NC 27028
Facility Name*
Town of Mocksville Class B Residuals Program
Please provide comments/notes on your current submittal below.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 Mocksville Annual Report - WQ0003351.pdf 8.22MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/29/2024

M
i— Resources, Inc.
Town of Mocksville
2023 Annual Report
Residuals Land Application
Permit No. WQ0003351
Prepared By:
EMA Resources, Inc.
Phone 336*751.1441 — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028

February 27, 2024
DENR/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report — Town of Mocksville
Treatment and Land Application of Residuals
Permit No. WQ0003351
Dear Sir or Madam:
Enclosed is the 2023 Annual Report for the above referenced land application permit.
During 2023 EMA Resources, Inc. land applied 115.88 dry tons of wastewater residuals
to 60.77 acres of private farmland. Please contact Brent Collins - Director of Technical
Services if you have any further questions regarding this report.
Sincerely,
z� 4: �'
Brent Collins
Director of Technical Services
brent. collinsnemaresourcesinc. com
Phone 336*751.1441 — Fax 336*751.1442
755 Yadkinville Rd — Mocksville, NC 27028

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit#: WQ0003351 County: Davie Year:
2023
Facility Name (as shown on permit):
Land Application Operator:
EMA Resources Inc.
Town of Mocksville
Phone: [phone]
Land application of residuals as allowed by the permit occurred during the past calendar year?
R1 Yes © No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
Total number of application fields in the ermit:
16
Total number of fields utilized for land application during the year:
5
Total amount of dry tons applied during the year for all application sites:
115.88
Total number of acres utilizes for land application during the year-F
60.77
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. R1 Yes ® No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
taken.
) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .1 1 11 were complied with (applicable to 40 CFR Part
503 regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
I I ) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the pert -nit were maintained during each application of residuals.
Part C - Certification:
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations." ,,
Ken Gamble -Town Manager keel GawKe 02/02/2024
KejiGamble (Feb 2, 202405:31 EST)
Permittee Name and Title (type or print) Signature of Permittee Date
�,� 1/26/24 1 /22/2024
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (1212006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number:
Facility Name:
Residual Source WQ # or
NPDES #:
NN'WTP Name:
Residual Analysis Data
WQ0003351
Town of Mocksville
NCO021491
Dutchman's Creek W WTP
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kb)
Cone.
Limit
(mg/k)a
Sam le or Composite Date
1/12/23
4/5/23
7/18/23
16/25/23
Percent Solids (%)
NA
2.07
1.87
1.24
0.986
Arsenic
75
11.4
26.3
20.8
25
Cadmium
85
0.952
5.26
4.17
5
Copper
4,316
162
157
133
128
Chromium
NA
20.2
16.9
20.8
25
Lea4l
840
20.5
15.8
16.7
20
Mercury
57
0.29
1.13
1.75
2.22
Molybdenum
75
6.43
7.11
12.5
15
Nickel
420
13.9
13.9
14.8
15
Selenium
100
15.2
26.3
29.2
35
Zinc
7,510
548
435
269
369
Total Phosphorus
NA
26404
33500
27000
33140
TKN
NA
108000
106000
71400
72500
Ammonia -Nitro en
NA
3120
7320
8830
14400
Nitrate and Nitrite
NA
336
158
83.3
177
'For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties
for submitting false information, including the possibility of fines and imprisonment for knowing violations."
1/26/24
Signature of Preparer * Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26)
DENR FORM RSSF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar ,year. Use additional forms as needed.
WQ Permit Number: WQ0003351
Facility Name: Town of Mocksville
Residual Source NCO021491
NPDES # or WQ#:
WWTP Name: Dutchman's Creek WWTP
Residual Analvcis Data
Laboratory: 1) Waypoint Analytical
2)
3)
4)
5)
Parameter
(mg/kg)
Sample or Composite Date
1/12/23
4/5/23
7/18/23
10/25/23
Aluminum
15100
14900
10700
8910
Calcium
12000
10500
10200
14100
Potassium
8520
11800
9670
13300
pH
6.6
6.9
6.5
7.2
Magnesium
5240
7160
5920
7520
Sodium
7480
9110
10400
19600
PAN
33360
33422
23269.3
24807
SAR
2.06
2.29
2.25
3.28
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Preparer
*.Preparer is dlef ned in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
1/26/24
Date
DENR FORM RSSF - B (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
Total Dry Tons Applied (Annual):
WQ0003351 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
22.92 Acres Permitted: 22.92 Site #: NC-DV08 Field #:
59.48
CeB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample or
Come
Date
1 1
4/5/23
2
7/18/23
3
1WTP
6/23
41
1 51
6
L7 1
81
L 9
—1ol
Li 11
12
% Solids
1.87
1.24
3.27
Arsenic
26.3
20.8
8.27
Cadmium
5.26
4.17
1.52
Copper
157
133
32.4
Chromium
16.9
20.8
80.3
Lead
15.8
16.7
33
Mercury
1.13
1.75
0.655
Molyb-
denum
7.11
12.5
4.55
Nickel
13.9
14.8
33.6
Selenium
26.3
29.2
10.6
Zinc
435
269
105
Total
Phos-
horus
33500
27000
1680
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
••
Event
1
1•
1 1
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1�
1 �.
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1.
1 1�
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1��
1 1
1 1��
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 1•
1 11
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1 1 1
1 1 �
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
•�
1 1 :
1 1
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
1 1
1 1
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
®®
1 •
1 �1
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
•
Total
' •
• •
` •
�:
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
••
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
zeyz 4; 5 /0�_
1 /22/2024
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 1 Acres Utilized: 22.92
Land Owner: Roger Spillman Annual Dry Tons Applied: 59.48 Site #: NC-DV08 Acres Permitted: 22.92
Operator: Roger Spillman Predominant Soil Series: CeB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 156 Crop 2 Name: Crop 2 Max. PAN:
�
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
SoilPrecip.
Cond.
(Dry,
e '
Moist)
Past 24
Hrs.
inches
y
'�
"
•*
0 m
F.
c
Fy :
?: ~
*
o'
Z
N "
* N
0
TKN
mg/kg
Z
1
o
as o
CD Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/3/23
19500
1.87
0.066
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
4.435
NA
Fescue
4/4/23
39000
1.87
0.133
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
8.869
NA
Fescue
6/l/23
36000
1.87
0.122
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
8.187
NA
Fescue
6/2/23
76500
1.87
0.260
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
17.398
NA
Fescue
6/6/23
1
40500
1.87
1 0.138
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
9.210
1 NA
Fescue
6/7/23
22500
1.87
0.077
Dutchman's Creek
Dry
<.5"
S
0.5
1 0.3
106000
7320
158
5.117
NA
Fescue
6/8/23
22500
1.87
0.077
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
5.117
NA
Fescue
6/9/23
13500
1.87
0.046
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
3.070
NA
Fescue
6/26/23
9000
1.87
0.031
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
1 106000
7320
158
2.047
NA
Fescue
6/28/23
1
40500
1.87
1 0.138
Dutchman's Creek
Dry
<.5"
S
1 0.5
0.3
106000
7320
158
9.210
NA
Fescue
6/29/23
45000
1.87
0.153
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
10.234
NA
Fescue
6/30/23
40500
1.87
0.138
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
9.210
NA
Fescue
0
355500
1.218
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
27.577
0.000
TOTALS:
01
760500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
119.6821
0.000
Lime Applied
Annuallbs/acre
0.1063
0.0211
0.6218
0.1768
0.1060
0.0059
0.0394
0.0995
0.1187
1.6342 124.166
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.1843
0.0273
1.2506
0.4192
0.2207
0.0029
0.0839
0.2107
0.1902
3.6966
Current Cumulative lbs/ac
0.2906
0.0484
1.8724
0.5960
0.3267
0.0088
0.1233
1 0.3102
1 0.3089
5.3308
Permitted C. P. L. R.****
36
34
1338
267
1 15
1
374
1 89
2498
Permit PAN Limit 1 st/2nd Crop
1 156
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
e *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/22/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
Supplemental Information
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: W00003351 Field #: 1 Acres Utilized: 22.92
Land Owner: Roger Spillman Annual Dry Tons Applied: 59.48 Site #: NC-DV08 Acres Permitted: 22.92
Operator: Roger Spillman Predominant Soil Series: Ce132 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 156 Crop 2 Name: Crop 2 Max PAN:
o y
o
Q
Volume applied (enter
one)(Dry,--
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
Moist)
preci p•
Past 24
Hrs.
inches
>
''
Q
* °�
C
o
N'
o'
Z
7 a
o
TKN
mg/kg
Z Y
�
o 5
ao o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of CropType
Yp
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/3
4500
1.24
0.010
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
0.472
NA
Fescue
8/22
31500
1.24
0.071
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
3.307
NA
Fescue
8/23
31500
1.24
0.071
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
3.307
NA
Fescue
8/24
36000
1.24
0.081
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
3.780
NA
Fescue
8/25
31500
1.24
0.071
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
3.307
NA
Fescue
8/31
36000
1.24
0.081
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
3.780
NA
Fescue
9/1
36000
1.24
0.081
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
3.780
NA
Fescue
9/5
36000
1.24
0.081
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
3.780
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
6/1
36000
3.27
0.214
Mocksville WTP
Dry
<.5"
S
0.5
0
19300
2700
192
0.661
NA
Fescue
6/2
76500
3.27
0.455
Mocksville WTP
Dry
<.5"
S
0.5
0
19300
2700
192
1.404
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
TOTALS:
01
3555001
1 1.2181
1
1
1
27.577
0.000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/22/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date ***C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (SUPP) (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
Total Dry Tons Applied (Annual):
WQ0003351 Cation Exchange Capacity (non 503 only):
Roger Spillman Owner: Roger Spillman Predominant Soil Series:
17.09 Acres Permitted: 17.09 Site #: NC-DV08 Field #:
27.29
MrB2
8
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
.-•
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
••
Event
1`
1•:
1 1
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11:
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1�
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1 :
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
•'
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1� :
1 1
1 1�:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
®
1�
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •••
Total
' •
• 1
�:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•�
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z� zz 4; 5 1 /�,_
176.T176I1T1Z!
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 8 Acres Utilized: 17.09
Land Owner: Roger Spillman Annual Dry Tons Applied: 27.29 Site #: NC-DV08 Acres Permitted: 17.09
Operator: Roger Spillman Predominant Soil Series: MrB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 141 Crop 2 Name: Crop 2 Max. PAN:
�
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
SoilPrecip.
Cond.
(Dry,
e '
Moist)
Past 24
Hrs.
inches
y
'�
"
•*
0 m
F.
o
Fy :
?: ~
*
o'
Z
N "
* N
0
TKN
mg/kg
Z
1
o
as o
CD Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
7/3/23
36000
1.24
0.109
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
5.069
NA
Fescue
7/5/23
40500
1.24
0.123
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
5.703
NA
Fescue
7/7/23
18000
1.24
0.054
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
2.535
NA
Fescue
9/25/23
117000
1.24
0.354
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
16.475
NA
Fescue
9/26/23
1
91000
1.24
1 0.275
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
71400
8830
83.3
12.814
NA
Fescue
12/15/23
45000
0.986
0.108
Dutchman's Creek
Dry
<.5"
S
0.5
1 0.3
72500
14400
177
5.371
NA
Fescue
12/16/23
31500
0.986
0.076
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
72500
14400
177
3.760
NA
Fescue
12/21/23
45000
0.986
0.108
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
72500
14400
177
5.371
NA
Fescue
12/22/23
76500
0.986
0.184
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
1 72500
14400
177
9.131
NA
Fescue
12/23/24
85500
0.986
1 0.206
Dutchman's Creek
Dry
<.5"
S
1 0.5
0.3
72500
14400
177
10.206
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
0.000
TOTALS:
0
586000
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn P
76.434
0.000
Lime A lied
Annuallbs/acre
0.0722
0.0145
0.4180
0.0722
0.0578
0.0062
0.0433
0.0475
0.1012
0.9956 94.558
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.5977
0.1889
19.2828
6.0148
4.6286
0.0956
0.7403
2.7727
0.5982
74.9583
Current Cumulative lbs/ac
0.6699
1 0.2034
19.7008
6.0870
4.6864
0.1018
0.7836
2.8202
0.6994
75.9539
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1
1 141
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
e *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/22/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
Total Dry Tons Applied (Annual):
WQ0003351 Cation Exchange Capacity (non 503 only):
Arthur Rupard Owner: C.B. Rupard & Sons Predominant Soil Series:
12.04 Acres Permitted: 12.04 Site #: NC-MK01 Field #:
19.93
MsB
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
.-•
Com-
posite
Date
©
©
m
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total©
•
D
-
••
Event
�•
1 1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1 �
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1••
1 1
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 11
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
M
1 1 •
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 1
•'
1 1 :
1 1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 1
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•:
®
1:
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Total
' •
• • 1
•••
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
1 ••
•
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z� zz 4; 5 1 /�,_
?,00,071
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 2 Acres Utilized: 12.04
Land Owner: C.B. Rupard & Sons Annual Dry Tons Applied: 19.93 Site #: NC-MKO1 Acres Permitted: 12.04
Operator: Arthur Rupard Predominant Soil Series: MsB Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Pasture Crop 1 Max. PAN: 167 Crop 2 Name: Crop 2 Max. PAN:
�
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
SoilPrecip.
Cond.
(Dry,
e '
Moist)
Past 24
Hrs.
inches
y
'�
co
•*
a m
c
:
?: ~
* N
o'
Z
Z
* N•
TKN
mg/kg
Z
t
o
as o
Z.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
ReceivingResidual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/5/23
110500
1.87
0.716
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
47.838
NA
Fescue
4/6/23
45500
1.87
0.295
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
19.698
NA
Fescue
11/7/23
108000
0.986
0.369
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
72500
14400
177
18.298
NA
Fescue
11/8/23
49500
0.986
0.169
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
72500
14400
177
8.387
NA
Fescue
11/9/23
1
31500
0.986
1 0.108
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
72500
14400
177
5.337
NA
Fescue
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
0
345000
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn P
99.559
0.000
Lime A lied
Annuallbs/acre
0.0854
0.0171
0.4823
0.0664
0.0577
0.0051
0.0337
0.0474
0.0983
1.3547 110.369
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.3836
0.1778
12.7996
1.0917
2.3844
0.0562
0.7505
1.2102
0.4702
45.9546
Current Cumulative lbs/ac
0.4690
0.1949
13.2819
1.1581
2.4421
0.0613
0.7842
1.2576
0.5685
47.3093
Permitted C. P. L. R.****
36
34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 167
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
e *Application Method: S - Surface, IN - Injection, INC - Incorporation
1/22/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
WQ0003351
Jeff Smith Owner:
4.12 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Town of Mocksville Predominant Soil Series:
4.12 Site #: NC-MK05 Field #:
11.81
CeB2
1
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
Event
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 •11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
�
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
�
1 1:1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:1
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
®
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
. •.
Total
'
` 1:•
1 111
1 111
1111
1 111
1111
1 111
1111
1 111
1 111
1111
1 111
` 1:•
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
I WKbib71Ti71
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 1 Acres Utilized: 4.12
Land Owner: Town of Mocksville Annual Dry Tons Applied: 11.81 Site #: NC-MK05 Acres Permitted: 4.12
Operator: Jeff Smith Predominant Soil Series: CeB2 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
We '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
a F
c
* N
o'
Z
0
W
* N•
TKN
mg/kg
Z a
g
o
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/4/23
97500
1.87
1.845
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
123.352
NA
Fescue
6/9/23
4500
1.87
0.085
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
5.693
NA
Fescue
6/13/23
22500
1.87
0.426
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
28.466
NA
Fescue
6/14/23
27000
1.87
0.511
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
34.159
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0
0
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
0.000
1 0.000
TOTALS:
01
151500
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
191.671
r 0.000
Lime Applied
Annuallbs/acre
0.151
0.030
0.900
0.097
0.091
0.006
0.041
0.080
0.151
2.494 192.089
41.14
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.716
0.147
13.001
2.193
1.753
0.058
0.516
1.544
0.809
Current Cumulative lbs/ac
0.867
0.177
13.901
2.290
1.844
0.064
0.557
1.624
0.960
43.634
Permitted C. P. L. R.****
36
1 34
1 1338
1
1 267
1 15
1
1 374
1 89
1 2498
Permit PAN Limit 1 st/2nd Crop
1 209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/22/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Mocksville
WQ0003351
Jeff Smith Owner:
4.6 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
Town of Mocksville Predominant Soil Series:
4.6 Site #: NC-MK05 Field #:
12.71
CfB2
2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Com-
posite
Date
Total
Phos-
phorus
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total
D
-
••
Event
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 :.:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :.:
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•
1 1:
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1:
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
••
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
®
' 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
� 1�
Total
' •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
•
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
I WKbib71Ti71
Signature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: Town of Mocksville WQ Permit #: WQ0003351 Field #: 2 Acres Utilized: 4.6
Land Owner: Town of Mocksville Annual Dry Tons Applied: 12.71 Site #: NC-MK05 Acres Permitted: 4.6
Operator: Jeff Smith Predominant Soil Series: CfI32 Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue -Hay Crop 1 Max. PAN: 209 Crop 2 Name: Crop 2 Max. PAN:
p
M
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
We '
Moist)
Precip.
Past 24
Hrs.
inches
y
co
a F
c
* N
o'
Z
0
W
* N•
TKN
mg/kg
Z a
g
o
aq o
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4/12/23
91000
1.87
1.543
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
103.115
NA
Fescue
6/14/23
9000
1.87
0.153
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
10.198
NA
Fescue
6/15/23
36000
1.87
0.610
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
40.793
NA
Fescue
6/16/23
27000
1.87
0.458
Dutchman's Creek
Dry
<.5"
S
0.5
0.3
106000
7320
158
30.595
NA
Fescue
0.000
1
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
163000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn P
184.701
0.000
Lime Applied
Annuallbs/acre
0.145
0.029
0.868
0.093
0.087
0.006
0.039
0.077
0.145
2.404 185.121
15.76
18.164
1 2498
Date
lbs/ac
Prior Years Cumulative lbs/ac
2.064
0.263
4.945
12.521
12.233
0.413
0.263
3.908
1.758
Current Cumulative lbs/ac
2.209
1 0.292
5.813
12.614
12.320
0.419
0.302
3.985
1.903
Permitted C. P. L. R.****
1 36
34
1 1338
1
1 267
1 15
1
1 374
1 89
Permit PAN Limit 1 st/2nd Crop
209
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/22/2024 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

Waypointo
ANALYTICAL
1 /24/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-013-0024
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 1/13/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/28/2023
Arkansas
State Program
88-0650
02/07/2023
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
02/18/2023
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
02/11/2023
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2023
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-013-0024
Page 2 of 8

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-013-0024
Client Project Description: Mocksville, NC
Lab No Client Sample ID
92877 Mocksville
Matrix Date Collected
Solids 01/12/2023 09:50
Date Received
01/13/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 23-013-0024
Date: 1 /24/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 93333
Analyte: Aluminum
QC Batch No: 1-659498/1-658994
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93333
Analyte: Calcium
QC Batch No: 1-659498/1-658994
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93333
Analyte: Iron
QC Batch No: 1-659404/1-658994
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93333
Analyte: Potassium
QC Batch No: 1-659404/1-658994
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93333
Analyte: Potassium
QC Batch No: 1-659498/1-658994
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93333
Analyte: Potassium
QC Batch No: 1-659498/1-658994
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 93333
Analyte: Phosphorus
QC Batch No: 1-659498/1-658994
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 4 of 8

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Mocksville, NC
Mr. Brent Collins Report Date : 01/24/2023
755 Yadkinville Rd Information : Received : 01/13/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-013-0024
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 92877
Matrix:
Solids
Sample ID: Mocksville
Sampled:
1/12/2023
9:50
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
97.9
%
1
01/19/23 16:07
FMM
SW-DRYWT
Ammonia Nitrogen
3120 J
mg/Kg - dry
762
4760
1
01/24/23 11:00
CLP
4500NH3C-2011
Nitrate+Nitrite-N
336
mg/Kg - dry
223
223
1
01/18/23 15:20
CLP
4500NO3F-2016
Organic N
105000 J
mg/Kg - dry
761.9
4762
1
01/23/23 08:30
CALCULATION
pH
6.6
S.U.
1
01/20/2314:00
SAR
9045D
Total Solids
2.07
%
0.010
0.010
1
01/19/23 16:07
FMM
2540G-2011
Total Volatile Solids
75.2
%
0.010
0.010
1
01/19/23 16:07
FMM
2540G-2011
Total Kjeldahl Nitrogen
108000
mg/Kg - dry
476
11900
1
01/23/23 08:30
JPJ ')M-4500-NH3C-TKP
Phosphorus
26400
mg/Kg - dry
131
238
1
01/18/23 22:28
TJS
6010D
Aluminum
15100
mg/Kg - dry
220
238
1
01/18/23 22:28
TJS
6010D
Arsenic
<11.4
mg/Kg - dry
11.4
23.8
1
01/18/23 22:28
TJS
6010D
Cadmium
<0.952
mg/Kg - dry
0.952
4.76
1
01/18/23 22:28
TJS
6010D
Calcium
12000
mg/Kg - dry
1840
2380
1
01/18/23 22:28
TJS
6010D
Chromium
20.2
mg/Kg - dry
11.2
11.9
1
01/18/23 22:28
TJS
6010D
Copper
162
mg/Kg - dry
14.8
23.8
1
01/18/23 22:28
TJS
6010D
Iron
15900
mg/Kg - dry
406
476
1
01/18/23 22:28
TJS
6010D
Lead
20.5
mg/Kg - dry
8.57
14.3
1
01/18/23 22:28
TJS
6010D
Magnesium
5240
mg/Kg - dry
123
238
1
01/18/23 22:28
TJS
6010D
Manganese
733
mg/Kg - dry
15.5
23.8
1
01/18/23 22:28
TJS
6010D
Mercury
<0.290
mg/Kg - dry
0.290
6.67
1
01/19/23 15:34
JTR
7471A
Molybdenum
<6.43
mg/Kg - dry
6.43
11.9
1
01/18/23 22:28
TJS
6010D
Nickel
13.9
mg/Kg - dry
5.71
11.9
1
01/18/23 22:28
TJS
6010D
Potassium
8520
mg/Kg - dry
294
476
1
01/18/23 22:28
TJS
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 01/24/2023
755 Yadkinville Rd
Information :
Received : 01/13/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-013-0024
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 92877
Matrix: Solids
Sample ID: Mocksville
Sampled: 1/12/2023 9:50
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<15.2
mg/Kg - dry
15.2
23.8 1 01/18/23 22:28 TJS 6010D
Sodium
7480
mg/Kg - dry
619
1190 1 01/18/23 22:28 TJS 6010D
Zinc
548
mg/Kg - dry
38.6
59.5 1 01/18/23 22:28 TJS 6010D
Sulfur
10300
mg/Kg - dry
247
476 1 01/18/23 22:28 TJS 6010D
Sodium Absorption Ratio
2.07
Ratio
0.01
0.01 1 01/18/23 22:28 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-013-0024
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: 102
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Makayla Weaver Date & Time: 01/13/2023 11:12:03
Page 7 of 8

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Page 8 of 8

Sodium
Calcium
Magnesium
Percent Solids
SAR
SAR =
1 /12/2023
mg/kg mg/L Equiv Weight Milli Equiv
7480 154.836 23 6.732
12000 248.4 20 12.42
5240 108.468
2.07
2.06
Na+
z (Ci a2+ + Mg2+ )
12 9.039
6.73200
0.5( 12.42 2 + 9.03900 2 )

Waypointo
ANALYTICAL
4/13/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-096-0013
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 4/6/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 8

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2023
Florida
State Program
- NELAP
E871157
06/30/2023
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2023
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2023
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2023
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2023
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2023
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-096-0013
Page 2 of 8

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-096-0013
Client Project Description: Mocksville, NC
Lab No Client Sample ID
93337 Mocksville
Matrix Date Collected
Solids 04/05/2023 06:40
Date Received
04/06/2023
Page 3 of 8

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 23-096-0013
Date: 4/13/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 93829 (#2)
Analyte: Aluminum
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Calcium
QC Batch No: 1-675666/1-674801
The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance
ranges. Matrix interference is suspected.
Sample 93829 (#2)
Analyte: Iron
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Potassium
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Magnesium
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 93829 (#2)
Analyte: Sulfur
QC Batch No: 1-675666/1-674801
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 93833 (San Elijo)
Analyte: Mercury
QC Batch No: 1-675254/1-674948
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 8

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Mocksville, NC
Mr. Brent Collins Report Date : 04/13/2023
755 Yadkinville Rd Information : Received : 04/06/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-096-0013
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 93337
Matrix:
Solids
Sample ID: Mocksville
Sampled:
4/5/2023 6:40
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.1
%
1
04/11/2313:02
JLS
SW-DRYWT
Ammonia Nitrogen
7320
mg/Kg - dry
842
5260
1
04/13/23 13:30
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
1583
mg/Kg - dry
52.6
263
1
04/11/23 12:53
ZBD
4500NO3F-2016
Organic N
98470
mg/Kg - dry
842.1
5263
1
04/13/23 08:00
CALCULATION
pH
6.9
S.U.
1
04/11/2311:25
HBT
9045D
Total Solids
1.87
%
0.010
0.010
1
04/10/23 14:09
JLS
2540G-2011
Total Volatile Solids
73.9
%
0.010
0.010
1
04/10/23 14:09
JLS
2540G-2011
Total Kjeldahl Nitrogen
106000
mg/Kg - dry
526
13200
1
04/13/23 08:00
JPJ ')M-4500-NH3C-TKP
Phosphorus
33500
mg/Kg - dry
145
263
1
04/11/23 04:25
JTR
6010D
Aluminum
14900
mg/Kg - dry
243
263
1
04/11/23 04:25
JTR
6010D
Arsenic
<26.3
mg/Kg - dry
12.6
26.3
1
04/11/23 04:25
JTR
6010D
Cadmium
<5.26
mg/Kg - dry
1.05
5.26
1
04/11/23 04:25
JTR
6010D
Calcium
10500
mg/Kg - dry
2040
2630
1
04/11/23 04:25
JTR
6010D
Chromium
16.9
mg/Kg - dry
12.4
13.2
1
04/11/23 22:50
JTR
6010D
Copper
157
mg/Kg - dry
16.3
26.3
1
04/11/23 04:25
JTR
6010D
Iron
15400
mg/Kg - dry
448
526
1
04/11/23 04:25
JTR
6010D
Lead
<15.8
mg/Kg - dry
9.47
15.8
1
04/11/23 04:25
JTR
6010D
Magnesium
7160
mg/Kg - dry
136
263
1
04/11/23 04:25
JTR
6010D
Manganese
461
mg/Kg - dry
17.1
26.3
1
04/11/23 04:25
JTR
6010D
Mercury
<1.13
mg/Kg - dry
1.13
9.32
1
04/10/23 14:11
FDS
7471A
Molybdenum
<7.11
mg/Kg - dry
7.11
13.2
1
04/11/23 04:25
JTR
6010D
Nickel
13.9
mg/Kg - dry
6.32
13.2
1
04/11/23 04:25
JTR
6010D
Potassium
11800
mg/Kg - dry
325
526
1
04/11/23 04:25
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 5 of 8

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 04/13/2023
755 Yadkinville Rd
Information :
Received : 04/06/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-096-0013
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 93337
Matrix: Solids
Sample ID: Mocksville
Sampled: 4/5/2023 6:40
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<26.3
mg/Kg - dry
16.8
26.3 1 04/11/23 04:25 JTR 6010D
Sodium
9110
mg/Kg - dry
684
1320 1 04/11/23 04:25 JTR 6010D
Zinc
435
mg/Kg - dry
42.6
65.8 1 04/11/23 04:25 JTR 6010D
Sulfur
11300
mg/Kg - dry
273
526 1 04/11/23 04:25 JTR 6010D
Sodium Absorption Ratio
2.31
Ratio
0.01
0.01 1 04/11/23 04:25 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 6 of 8

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-096-0013
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T135
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Emily M. Peterson Date & Time: 04/06/2023 09:26:18
Page 7 of 8

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Page 8 of 8

4/5/2023
mg/kg mg/L Equiv Weight Milli Equiv
Sodium 9110 170.357 23 7.406826
Calcium 10500 196.35 20 9.8175
Magnesium 7160 133.892 12 11.15767
Percent Solids 1.87
SAR 2.29
SAR =
Na+
z (Ci a2+ + Mg2+ )
7.40683
0.5( 9.8175 2 + 11.15767 2 )

Waypointo
ANALYTICAL
8/7/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-200-0016
Client Project Description: Mocksville, NC
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 7/19/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/10/2023
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2023
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2023
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2023
Page 1 of 1 00001/23-200-0016
Page 2 of 9

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-200-0016
Client Project Description: Mocksville, NC
Lab No Client Sample ID
82402 Mocksville
Matrix Date Collected
Solids 07/18/2023 06:00
Date Received
07/19/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville, NC
Lab Report Number: 23-200-0016
Date: 8/3/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 82652
QC Batch No: L694427/L694031
One or more Internal Standards are outside method acceptance criteria. Re -analysis and/or sample dilutions are
required.
Sample 82652
Analyte: Aluminum
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82652
Analyte: Arsenic
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 82652
Analyte: Iron
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82652
Analyte: Potassium
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 82652
Analyte: Magnesium
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 82652
Analyte: Manganese
QC Batch No: L694693/L694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Sample 82652
Analyte: Phosphorus
QC Batch No: 1-694693/1-694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 82652
Analyte: Lead
QC Batch No: 1-694693/1-694031
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 82869
Analyte: Mercury
QC Batch No: 1-694489/1-694272
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Page 5 of 9

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Mocksville, NC
Mr. Brent Collins Report Date : 08/07/2023
755 Yadkinville Rd Information : Received : 07/19/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-200-0016
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 82402
Matrix:
Solids
Sample ID: Mocksville
Sampled:
7/18/2023
6:00
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.8
%
1
07/24/23 17:31
KDO
SW-DRYWT
Ammonia Nitrogen
8830
mg/Kg - dry
1330
8330
1
08/02/23 13:00
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
<83.3
mg/Kg - dry
83.3
417
1
07/24/23 14:37
CLP
4500NO3F-2016
Organic N
62580
mg/Kg - dry
1333
8333
1
08/02/23 09:00
CALCULATION
pH
6.5
s.u.
1
08/04/2315:30
CNB
9045D
Total Solids
1.24
%
0.010
0.010
1
07/24/23 17:31
KDO
2540G-2011
Total Volatile Solids
70.5
%
0.010
0.010
1
07/24/23 17:31
KDO
2540G-2011
Total Kjeldahl Nitrogen
71400
mg/Kg - dry
833
20800
1
08/02/23 09:00
JPJ ')M-4500-NH3C-TKP
Phosphorus
27000
mg/Kg - dry
233
417
1
07/22/23 06:51
JTR
6010D
Aluminum
10700
mg/Kg - dry
388
417
1
07/24/23 22:18
JTR
6010D
Arsenic
<20.8
mg/Kg - dry
20.8
41.7
1
07/22/23 06:51
JTR
6010D
Cadmium
<4.17
mg/Kg - dry
4.17
8.33
1
07/22/23 06:51
JTR
6010D
Calcium
10200
mg/Kg - dry
3230
4170
1
07/22/23 06:51
JTR
6010D
Chromium
<20.8
mg/Kg - dry
20.8
20.8
1
07/22/23 06:51
JTR
6010D
Copper
133
mg/Kg - dry
25.0
41.7
1
07/22/23 06:51
JTR
6010D
Iron
13900
mg/Kg - dry
713
833
1
07/22/23 06:51
JTR
6010D
Lead
<16.7
mg/Kg - dry
16.7
25.0
1
07/22/23 06:51
JTR
6010D
Magnesium
5920
mg/Kg - dry
217
417
1
07/22/23 06:51
JTR
6010D
Manganese
580
mg/Kg - dry
29.2
41.7
1
07/22/23 06:51
JTR
6010D
Mercury
<1.75
mg/Kg - dry
1.75
14.5
1
07/24/23 12:36
FDS
7471A
Molybdenum
<12.5
mg/Kg - dry
12.5
20.8
1
07/22/23 06:51
JTR
6010D
Nickel
14.83
mg/Kg - dry
12.5
20.8
1
07/22/23 06:51
JTR
6010D
Potassium
9670
mg/Kg - dry
517
833
1
07/22/23 06:51
JTR
6010D
Qualifiers/ DF
Dilution Factor
J
Estimated value
Definitions MQL
Method Quantitation Limit
Page 6 of 9

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville, NC
Mr. Brent Collins
Report Date : 08/07/2023
755 Yadkinville Rd
Information :
Received : 07/19/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-200-0016
REPOR T OF A
NA L YSIS
Project Manager
Lab No : 82402
Matrix: Solids
Sample ID: Mocksville
Sampled: 7/18/2023 6:00
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<29.2
mg/Kg - dry
29.2
41.7 1 07/22/23 06:51 JTR 6010D
Sodium
10400
mg/Kg - dry
1080
2080 1 07/22/23 06:51 JTR 6010D
Zinc
269
mg/Kg - dry
70.8
104 1 07/22/23 06:51 JTR 6010D
Sulfur
9420
mg/Kg - dry
433
833 1 07/22/23 06:51 JTR 6010D
Sodium Absorption Ratio
2.22
Ratio
0.01
0.01 1 07/22/23 06:51 CALCULATION
Qualifiers/ DF Dilution Factor
Definitions
J Estimated value
Page 7 of 9

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-200-0016
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: T135
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: Makayla Weaver Date & Time: 07/19/2023 10:41:50
Page 8 of 9

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Page 9 of 9

7/18/2023
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
10400
128.96
23 5.606957
Calcium
10200
126.48
20 6.324
Magnesium
5920
73.408
12 6.117333
Percent Solids
1.24
SAR
2.25
SAR =
Na+
z (Ci a2+ + Mg2+ )
5.60696
0.5( 6.324 2 + 6.11733 2 )

Waypointo
ANALYTICAL
11 /7/2023
EMA Resources Inc
Mr. Brent Collins
755 Yadkinville Rd
Mocksville, NC, 27028
Ref: Analytical Testing
Lab Report Number: 23-299-0006
Client Project Description: Mocksville
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
Dear Mr. Brent Collins:
Waypoint Analytical, LLC. received sample(s) on 10/26/2023 for the analyses presented in the following report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling
stage (refer to the chain of custody) results apply to the sample as received.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter
for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in
the scope because NELAP accreditation is either not available or has not been applied for. Additional
certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable.
A full list of certifications is available upon request.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time.
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information.
Sincerely,
Connie Cook
Project Manager
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.corn
Certification Summary
Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN
State
Program
Lab ID
Expiration Date
Alabama
State Program
40750
02/29/2024
Arkansas
State Program
88-0650
02/07/2024
California
State Program
2904
06/30/2024
Florida
State Program
- NELAP
E871157
06/30/2024
Georgia
State Program
C044
11/14/2025
Georgia
State Program
04015
06/30/2024
Illinois
State Program
- NELAP
200078
10/31/2024
Kentucky
State Program
80215
06/30/2024
Kentucky
State Program
KY90047
12/31/2023
Louisiana
State Program
- NELAP
LA037
12/31/2023
Louisiana
State Program
- NELAP
04015
06/30/2024
Mississippi
State Program
MS
11/14/2025
North Carolina
State Program
47701
07/31/2024
North Carolina
State Program
415
12/31/2023
Pennsylvania
State Program
- NELAP
68-03195
05/31/2024
South Carolina
State Program
84002
06/30/2024
Tennessee
State Program
02027
11/14/2025
Texas
State Program
- NELAP
T104704180
09/30/2024
Virginia
State Program
00106
06/30/2024
Virginia
State Program
- NELAP
460181
09/14/2024
Page 1 of 1 00001/23-299-0006
Page 2 of 9

waypoint 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-299-0006
Client Project Description: Mocksville
Lab No Client Sample ID Matrix Date Collected Date Received
92925 Mocksville Solids 10/25/2023 05:30 10/26/2023
Page 3 of 9

Waypointo
ANALYTICAL
Client: EMA Resources Inc
Project: Mocksville
Lab Report Number: 23-299-0006
Date: 11 /2/2023
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 6010D
Sample 63789 (WWTP Cake)
Analyte: Aluminum
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Calcium
QC Batch No: 1-714093/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Iron
QC Batch No: L713991/L713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Potassium
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Magnesium
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Manganese
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Phosphorus
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Lead
Page 4 of 9

Waypointo
ANALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 1 Fax [phone]
www.waypointanalytical.com
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63789 (WWTP Cake)
Analyte: Sulfur
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63789 (WWTP Cake)
Analyte: Zinc
QC Batch No: 1-713991/1-713475
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Solids Total Mercury Analysis - CVAA Method 7471A
Sample 63814 (23102407.01A)
Analyte: Mercury
QC Batch No: 1-713736/1-713529
The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control
acceptance ranges. Matrix interference is suspected.
Page 5 of 9

0
Waypoint, 2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
46245
EMA Resources Inc Project Mocksville
Mr. Brent Collins Report Date : 11/07/2023
755 Yadkinville Rd Information : Received : 10/26/2023
Mocksville , NC 27028 n �
Connie Cook
Report Number : 23-299-0006
REPOR T OF A NA L YSIS
Project
Manager
Lab No : 92925
Matrix:
Solids
Sample ID: Mocksville
Sampled:
10/25/2023
5:30
Test
Results
Units
MDL
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
99.0
%
1
10/26/23 16:12
CAH
SW-DRYWT
Ammonia Nitrogen
14400
mg/Kg - dry
1600
10000
1
10/30/23 10:21
JPJ
4500NH3C-2011
Nitrate+Nitrite-N
177 )B
mg/Kg - dry
100
500
1
11/02/23 15:46
CLP
4500NO3F-2016
Organic N
58100
mg/Kg - dry
31500
1
10/30/23 10:21
DH
CALCULATION
pH
7.2
S.U.
1
10/26/2314:18
ANV
9045D
Total Solids
0.986
%
0.010
0.010
1
10/26/23 16:12
CAH
2540G-2011
Total Volatile Solids
73.7
%
0.010
0.010
1
10/26/23 16:12
CAH
2540G-2011
Total Kjeldahl Nitrogen
72500
mg/Kg - dry
31500
1
11/01/23 09:27
ANH 4500NORGD-2011
Phosphorus
33100
mg/Kg - dry
280
500
1
10/28/23 02:05
JTR
6010D
Aluminum
8910
mg/Kg - dry
465
500
1
10/28/23 02:05
JTR
6010D
Arsenic
<25.0
mg/Kg - dry
25.0
50.0
1
10/28/23 02:05
JTR
6010D
Cadmium
<5.00
mg/Kg - dry
5.00
10.0
1
10/28/23 02:05
JTR
6010D
Calcium
14100
mg/Kg - dry
3870
5000
1
10/30/23 14:45
TJS
6010D
Chromium
<25.0
mg/Kg - dry
25.0
25.0
1
10/28/23 02:05
JTR
6010D
Copper
128
mg/Kg - dry
30.0
50.0
1
10/28/23 02:05
JTR
6010D
Iron
11800
mg/Kg - dry
855
1000
1
10/28/23 02:05
JTR
6010D
Lead
<20.0
mg/Kg - dry
20.0
30.0
1
10/28/23 02:05
JTR
6010D
Magnesium
7520
mg/Kg - dry
260
500
1
10/28/23 02:05
JTR
6010D
Manganese
287
mg/Kg - dry
35.0
50.0
1
10/28/23 02:05
JTR
6010D
Mercury
<2.22
mg/Kg - dry
2.22
18.4
1
10/27/23 11:39
FDS
7471A
Molybdenum
<15.0
mg/Kg - dry
15.0
25.0
1
10/28/23 02:05
JTR
6010D
Nickel
<15.0
mg/Kg - dry
15.0
25.0
1
10/28/23 02:05
JTR
6010D
Potassium
13300
mg/Kg - dry
620
1000
1
10/28/23 02:05
JTR
6010D
Qualifiers/ B
Analyte detected in blank
DF
Dilution Factor
Definitions J
Estimated value
MQL
Method Quantitation
Limit
Page 6 of 9

0
Waypoint,
2790 Whitten
Road, Memphis, TN 38133
Main 901.213.2400 0 Fax [phone]
ANALYTICAL
www.waypointanalytical.com
46245
EMA Resources Inc
Project
Mocksville
Mr. Brent Collins
Report Date : 11/07/2023
755 Yadkinville Rd
Information :
Received : 10/26/2023
Mocksville , NC 27028
Connie Cook
Report Number : 23-299-0006
REPOR T OF A NA L YSIS
Project Manager
Lab No : 92925
Matrix: Solids
Sample ID: Mocksville
Sampled: 10/25/2023 5:30
Test
Results
Units
MDL
MQL DF Date / Time By Analytical
Analyzed Method
Selenium
<35.0
mg/Kg - dry
35.0
50.0 1 10/28/23 02:05 JTR 6010D
Sodium
19600
mg/Kg - dry
1300
2500 1 10/28/23 02:05 JTR 6010D
Zinc
369
mg/Kg - dry
85.0
125 1 10/28/23 02:05 JTR 6010D
Sulfur
13700
mg/Kg - dry
520
1000 1 10/28/23 02:05 JTR 6010D
Sodium Absorption Ratio
3.31
Ratio
0.01
0.01 1 10/28/23 02:05 CALCULATION
Qualifiers/ B Analyte detected in blank
Definitions
DF Dilution Factor
Page 7 of 9

(2)
WayPAoint..
NALYTICAL
2790 Whitten Road, Memphis, TN 38133
Main 901.213.2400 ° Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46245
Customer Name: EMA Resources Inc
Report Number: 23-299-0006
Shipping Method
Fed Ex 0 US Postal 0 Lab 0 Other:
0 UPS 0 Client 0 Courier Thermometer ID: t100
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
F
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
Yes
0 No
COC agrees with sample label(s)?
U Yes
0 No
COC properly completed
U Yes
0 No
Samples in proper containers?
U Yes
0 No
Sample containers intact?
Yes
0 No
Sufficient sample volume for indicated test(s)?
Yes
0 No
All samples received within holding time?
Yes
0 No
Cooler temperature in compliance?
Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
0 N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
0 N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr) F Low concentration EnCore samplers (48 hr)
F_ High concentration pre -weighed (methanol -14 d) Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included?
0 Yes
0 No
Comments:
Signature: mber Smith Date & Time: I10/26/2023 08:50:21
Page 8 of 9

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Page 9 of 9

10/25/2023
mg/kg
mg/L
Equiv Weight Milli Equiv
Sodium
19600
193.256
23 8.402435
Calcium
14100
139.026
20 6.9513
Magnesium
7520
74.1472
12 6.178933
Percent Solids
0.986
SAR
3.28
SAR =
Na+
z (Ci a2+ + Mg2+ )
8.40243
0.5( 6.9513 2 + 6.17893 2 )

PaceAnalytical
ANALYTICAL REPORT
January 24, 2023
EMA Resources
Sample Delivery Group: L1576104
Samples Received: 01/13/2023
Project Number:
Description: Sludge
Report To: Mr. Brent Collins
755 Yadkinville Road
Mocksville, NC 27028
Entire Report Reviewed By
�L W, /� I �-
T. Alan Harvill
Project Manager
Results relate only to the items tested or calibrated and are reported as rounded values. This test report shall not be
reproduced, except in full, without written approval of the laboratory. Where applicable, sampling conducted by Pace
Analytical National is performed per guidance provided in laboratory standard operating procedures ENV-SOP-MTJL-0067 and ,
ENV-SOP-MTJL-0068. Where sampling conducted by the customer, results relate to the accuracy of the information provided,
and as the samples are received.
I
M
FSS
Rn
Rr
FQc
E7GI
rAl
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 1 of 23

TABLE OF CONTENTS
Cp: Cover Page
1
FP1
Tc: Table of Contents
2
Ss: Sample Summary
3
Cn: Case Narrative
4
Sr: Sample Results
5
FSS
MOCKSVILLE L1576104-01
5
rqn
Qc: Quality Control Summary
7
Wet Chemistry by Method 9012 B
7
Fr]
Wet Chemistry by Method 9034-9030B
8
Wet Chemistry by Method 9045D
9
FQ Cl
Wet Chemistry by Method D93/1010A
10
GI
Mercury by Method 7470A
11
Metals (ICP) by Method 6010D
12
rAl
Volatile Organic Compounds (GC/MS) by Method 8260D
14
Chlorinated Acid Herbicides (GC) by Method 8151A
16
FC
Pesticides (GC) by Method 80818
17
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
18
GI: Glossary of Terms
20
Al: Accreditations & Locations
21
Sc: Sample Chain of Custody
22
ACCOUNT: PROJECT: SDG:
DATE/TIME:
PAGE:
EMA Resources L1576104
01/24/23 09:03
2 of 23

SAMPLE SUMMARY
MOCKSVILLE L1576104-01 Waste
Collected by
Brent Collins
Collected date/time
01/12/23 09:50
Received date/time
01/13/23 09:15
C p
Method
Batch
Dilution Preparation
Analysis
Analyst
Location
date/time
date/time
FTC
Preparation by Method 1311
WG1989076
1 01/16/2313:40
01/16/2313:40
JWS
Mt. Juliet, TN
Preparation by Method 1311
WG1989548
1 01/16/2314:46
01/16/2314:46
JTM
Mt. Juliet, TN
Wet Chemistry by Method 9012 B
WG1989902
1 01/18/2310:39
01/18/2317:27
LDT
Mt. Juliet, TN
Wet Chemistry by Method 9034-9030B
WG1988617
1 01/17/23 22:57
01/20/2313:30
AW
Mt. Juliet, TN
Wet Chemistry by Method 9045D
WG1988760
1 01/17/2310:50
01/17/2312:10
NTG
Mt. Juliet, TN
rq
Wet Chemistry by Method D93/1010A
WG1990944
1 01/19/23 01:33
01/19/23 01:33
TOP
Mt. Juliet, TN
Mercury by Method 7470A
WG1989877
1 01/17/2311:05
01/17/2318:23
AKB
Mt. Juliet, TN
Metals (ICP) by Method 6010D
WG1990582
1 01/18/2312:38
01/18/23 22:08
ABL
Mt. Juliet, TN
Fr]
Volatile Organic Compounds (GC/MS) by Method 8260D
WG1989909
1 01/17/2313:21
01/17/2313:21
ADM
Mt. Juliet, TN
Chlorinated Acid Herbicides (GC) by Method 8151A
WG1990310
1 01/18/2318:27
01/20/2315:51
DLH
Mt. Juliet, TN
C
FQ
Pesticides (GC) by Method 8081B
WG1989721
1 01/18/23 22:40
01/19/2318:40
HMH
Mt. Juliet, TN
Semi Volatile Organic Compounds (GC/MS) by Method 8270E
WG1989725
1 01/19/23 05:07
01/20/23 03:37
JNJ
Mt. Juliet, TN
GI
FAI
FSC
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA Resources
L1576104
01/24/23 09:03
3 of 23

CASE NARRATIVE
All sample aliquots were received at the correct temperature, in the proper containers, with the FP1
appropriate preservatives, and within method specified holding times, unless qualified or notated within
the report. Where applicable, all MDL (LOD) and RDL (LOQ) values reported for environmental samples FTChave been corrected for the dilution factor used in the analysis. All Method and Batch Quality Control
are within established criteria except where addressed in this case narrative, a non-conformance form
or properly qualified within the sample results. By my digital signature below, I affirm to the best of my FSS
knowledge, all problems/anomalies observed by the laboratory as having the potential to affect the
quality of the data have been identified by the laboratory, and no information or data have been
knowingly withheld that would affect the quality of the data.
Fr]
4W3'4___ 1,07�a
Qc
GI
T. Alan Harvill rAl
Project Manager
LE
Project Narrative
All Reactive Cyanide results reported in the attached report were determined as totals using method 9012 B.
All Reactive Sulfide results reported in the attached report were determined as totals using method 9034-9030B.
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 4 of 23

R
SAMPLE RESULTS - 01
L1576104
MOCKSVILLE
Collected date/time: 01/12/23 09:50
Preparation by Method 1311
Result
Analyte
TCLP Extraction
TCLP ZHE Extraction -
Fluid 1
Initial pH 8.11
Final pH 4.93
Wet Chemistry by Method 9012 B
Qualifier Prep
Batch
date / time
1/16/20231:40:25 PM
WG1989076
1/16/2023 2:46:10 PM
WG1989548
1/16/20231:40:25 PM
WG1989076
1/16/20231:40:25 PM
WG1989076
1/16/20231:40:25 PM
WG1989076
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Cyanide ND
0.250
Wet Chemistry by Method 9034-9030B
Result Qualifier
RDL
Analyte mg/kg
mg/kg
Reactive Sulfide ND
75.0
Wet Chemistry by Method 9045D
Dilution Analysis Batch
date / time
1 01/18/202317:27 WG1989902
Dilution Analysis Batch
date / time
1 01/20/202313:30 WG1988617
Result Qualifier
Dilution Analysis
Analyte su
date / time
Corrosivity by pH 6.71 T8
1 01/17/202312:10
Sample Narrative:
L1576104-01 WG1988760: 6.71 at 19.6C
Wet Chemistry by Method D93/1010A
Result Qualifier
Dilution Analysis
Analyte Deg. F
date / time
Batch
WG1988760
Batch
Ignitability DNI at 170 1 01/19/2023 01:33 WG1990944
Mercury by Method 7470A
Result
Analyte mg/I
Mercury ND
Metals (ICP) by Method 6010D
Qualifier RDL Limit
mg/I mg/I
0.0100 0.20
Result
Qualifier RDL
Limit
Analyte
mg/I
mg/I
mg/I
Arsenic
ND
0.100
5
Barium
ND
0.100
100
Cadmium
ND
0.100
1
Chromium
ND
0.100
5
Lead
ND
0.100
5
Selenium
ND
0.100
1
Silver
ND
0.100
5
Volatile Organic Compounds (GC/MS) by Method 8260D
Analyte
Benzene
Carbon tetrachloride
Chlorobenzene
Result
Qualifier RDL
Limit
mg/I
mg/I
mg/I
ND
0.0500
0.50
ND
0.0500
0.50
ND
0.0500
100
ND
0.250
6
ACCOUNT: PROJECT
EMA Resources
Dilution Analysis Batch
date / time
1 01/17/202318:23 WG1989877
Dilution Analysis
Batch
date / time
1 01/18/2023 22:08
WG1990582
1 01/18/2023 22:08
WG1990582
1 01/18/2023 22:08
WG1990582
1 01/18/2023 22:08
WG1990582
1 01/18/2023 22:08
WG1990582
1 01/18/2023 22:08
WG1990582
1 01/18/2023 22:08
WG1990582
FP1
FTc
FSS
rqn
FC]
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FAI
FSC
Dilution Analysis
Batch
date / time
1 01/17/202313:21
WG1989909
1 01/17/202313:21
WG1989909
1 01/17/202313:21
WG1989909
1 01/17/202313:21
WG1989909
SDG:
DATE/TIME: PAGE:
L1576104
01/24/23 09:03 5 of 23

MOCKSVILLE SAMPLE RESULTS - 01
Collected date/time: 01/12/23 09:50 L1576104
Volatile Organic Compounds (GC/MS) by Method 8260D
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date/time
1,2-Dichloroethane
ND
0.0500
0.50
1 01/17/202313:21
WG1989909
1,1-Dichloroethene
ND
0.0500
0.70
1 01/17/202313:21
WG1989909
2-Butanone (MEK)
ND
C3 J3
0.500
200
1 01/17/202313:21
WG1989909
Tetrachloroethene
ND
0.0500
0.70
1 01/17/202313:21
WG1989909
Trichloroethene
ND
0.0500
0.50
1 01/17/202313:21
WG1989909
Vinyl chloride
ND
J3
0.0500
0.20
1 01/17/202313:21
WG1989909
(S) Toluene-d8
100
80.0-120
011171202313:21
WG1989909
(S) 4-Bromof/uorobenzene
91.4
77.0-126
011171202313:21
WG1989909
(S)1,2-Dichloroethane-d4
105
70.0-130
011171202313:21
WG1989909
Chlorinated Acid Herbicides (GC) by Method
8151A
Result
Qualifier
RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
2,4,5-TP (Silvex)
ND
0.00200
1
1 01/20/202315:51
WG1990310
2,4-D
ND
0.00200
10
1 01/20/202315:51
WG1990310
(S)2,4-Dichloropheny/Acetic Acid
93.6
14.0-158
01/20/202315:51
WG1990310
Pesticides (GC) by Method
8081B
Result
Qualifier RDL
Limit
Dilution Analysis
Batch
Analyte
mg/I
mg/I
mg/I
date / time
Chlordane
ND
0.00500
0.03
1 01/19/202318:40
WG1989721
Endrin
ND
0.00500
0.02
1 01/19/202318:40
WG1989721
Heptachlor
ND
0.00500
0.0080
1 01/19/202318:40
WG1989721
Heptachlor epoxide
ND
0.00500
0.0080
1 01/19/202318:40
WG1989721
Lindane
ND
0.00500
0.40
1 01/19/202318:40
WG1989721
Methoxychlor
ND
0.00500
10
1 01/19/202318:40
WG1989721
Toxaphene
ND
0.0100
0.50
1 01/19/202318:40
WG1989721
(S) Decachlorobipheny/
91.3
10.0-128
011191202318.40
WG1989721
(S) Tetrach/oro-m-xylene
81.8
10.0-127
011191202318.40
WG1989721
Semi Volatile Organic Compounds
(GC/MS) by Method 8270E
Result
Analyte mg/I
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachlorobenzene
Hexachloro-1,3-butadiene
Hexachloroethane
Nitrobenzene
Pyridine
3&4-Methyl Phenol
2-Methylphenol
Pentachlorophenol
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
(S) 2-Fluorophenol
(S) Phenol-d5
(S) Nitrobenzene-d5
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-d14
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND
31.4
17.8
59.3
61.0
67.5
69.3
Qualifier RDL
mg/I
0.100
0.100
0.100
0.100
0.100
0.100
J4 0.100
0.100
0.100
0.100
0.100
0.100
10.0-120
10.0-120
10.0-127
10.0-130
10.0-155
10.0-128
Limit
mg/I
7.50
0.13
0.13
0.50
3
2
5
400
200
100
400
2
Dilution Analysis Batch
date / time
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
01/20/2023 03:37
0112012023 03.37
0112012023 0337
0112012023 0337
0112012023 0337
0112012023 03.37
0112012023 0337
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
WG1989725
FP1
FTc
FSS
Fqn
FC]
I ql
FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 6 of 23

WG1989902
QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9012 B
L1576104-01
Method Blank (MB)
(MB) R3882279-1 01/18/2317:00
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Cyanide U 0.0390 0.250
L1575716-01 Original Sample (OS) • Duplicate (DUP)
(OS) L1575716-01 01/18/2317:13 • (DUP) R3882279-3 01/18/2317:14
Original Result DUP Result Dilution DUP RPD
DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg %
%
Reactive Cyanide ND ND 1 0.000
20
L1575716-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1575716-02 01/18/2317:15 • (DUP) R3882279-4 01/18/2317:16
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte mg/kg mg/kg % %
Reactive Cyanide ND ND 1 0.000 20
Laboratory Control Sample (LCS)
(LCS) R3882279-2 01/18/2317:01
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/kg mg/kg % %
Reactive Cyanide 2.50 2.52 101 85.0-115
L1576226-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576226-02 01/18/2317:28 • (MS) R3882279-5 01/18/2317:29 • (MSD) R3882279-6 01/18/2317:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Reactive Cyanide 1.67 ND 1.33 1.27 73.6 69.9 1 75.0-125 4.69
Sample Narrative:
MS: Matrix spike failure due to matrix.
MSD: Matrix spike failure due to matrix.
RPD Limits
20
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FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 7 of 23

WG1988617 QUALITY CONTROL SUMMARY
Wet Chemistry by Method 9034-9030B L1576104-01
Method Blank (MB)
(MB) R3883014-1 01/20/2313:30
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/kg mg/kg mg/kg
Reactive Sulfide U 30.0 75.0
Laboratory Control Sample (LCS)
(LCS) R3883014-2 01/20/2313:30
Spike Amount LCS Result LCS Rec.
Analyte mg/kg mg/kg %
Reactive Sulfide 100 72.1 72.1
Rec. Limits LCS Qualifier
53.8-124
L1575687-03 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1575687-03 01/20/2313:30 • (MS) R3883014-3 01/20/2313:30 • (MSD) R3883014-4 01/20/2313:30
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec. Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
Analyte mg/kg mg/kg mg/kg mg/kg % % % %
Reactive Sulfide 100 ND ND ND 40.2 67.5 1 10.0-136 0.000
RPD Limits
20
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FSS
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FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 8 of 23

WG1988760
Wet Chemistry by Method 9045D
L1576104-01 Original Sample (OS) • Duplicate (DUP)
QUALITY CONTROL SUMMARY
L1576104-01
(OS) L1576104-01 01/17/2312:10 • (DUP) R3881706-3 01/17/2312:10
Original Result DUP Result Dilution DUP RPD DUP Qualifier DUP RPD
Limits
Analyte su su % %
Corrosivity by pH 6.71 6.72 1 0.149 1
Sample Narrative:
OS: 6.71 at 19.6C
DUP: 6.72 at 19.6C
Laboratory Control Sample (LCS)
(LCS) R3881706-1 01/17/2312:10
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte su su % %
Corrosivity by pH 10.0 9.90 99.0 99.0-101
Sample Narrative:
LCS: 9.9 at 20.8C
FP1
FTc
FSS
LEI
FSr
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FAI
FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 9 of 23

WG1990944 QUALITY CONTROL SUMMARY
Wet Chemistry by Method D93/1010A L1576104-01
L1576226-02 Original Sample (OS) • Duplicate (DUP)
(OS) L1576226-02 01/19/23 01:33 • (DUP) R3882342-3 01/19/23 01:33
Original Result DUP Result Dilution DUP RPD
Analyte Deg. F Deg. F %
Ignitability DNIat170 DNIat170 1 0.000
DUP Qualifier DUP RPD
Limits
10
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3882342-1 01/19/23 01:33 • (LCSD) R3882342-2 01/19/23 01:33
Spike Amount LCS Result LCSD Result LCS Rec. LCSD Rec. Rec. Limits LCS Qualifier LCSD Qualifier RPD RPD Limits
Analyte Deg. F Deg. F Deg. F % % % %
Ignitability 126 131 127 104 101 95.6-104 3.10 10
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FSS
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ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 10 of 23

WG1989877 QUALITY CONTROL SUMMARY
Mercury by Method 7470A L1576104-01
Method Blank (MB)
(MB) R3881900-1 01/17/23 17:58
MB Result MB Qualifier MB MDL MB RDL
Analyte mg/1 mg/I mg/1
Mercury U 0.00330 0.0100
Laboratory Control Sample (LCS)
(LCS) R3881900-6 01/17/2318:49
Spike Amount LCS Result LCS Rec.
Analyte mg/1 mg/1 %
Mercury 0.0300 0.0276 92.0
Rec. Limits LCS Qualifier
80.0-120
L1576039-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576039-01 01/17/2318:06 • (MS) R3881900-2 01/17/2318:08 • (MSD) R3881900-3 01/17/23 18:11
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/1 mg/1 mg/I mg/1 % %
Mercury 0.0300 ND 0.0262 0.0241 87.4 80.4
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 75.0-125 8.30
L1576217-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576217-02 01/17/2318:13 • (MS) R3881900-4 01/17/2318:17 • (MSD) R3881900-5 01/17/2318:19
Spike Amount Original Result MS Result MSD Result MS Rec. MSD Rec.
Analyte mg/1 mg/1 mg/I mg/1 % %
Mercury 0.0300 ND 0.0252 0.0235 84.1 78.4
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 75.0-125 7.06
RPD Limits
20
RPD Limits
20
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FSS
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FSr
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FSC
ACCOUNT: PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources L1576104 01/24/23 09:03 11 of 23

WG1990582
Metals (ICP) by Method 6010D
Method Blank (MB)
(MB) R3882356-1 01/18/23 20:46
MB Result
MB Qualifier MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
Arsenic U
0.0333
0.100
Barium U
0.0333
0.100
Cadmium U
0.0333
0.100
Chromium U
0.0333
0.100
Lead U
0.0333
0.100
Selenium 0.0363
J_ 0.0333
0.100
Silver U
0.0333
0.100
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1576104-01
(LCS) R3882356-2 01/18/23 20:49
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
Arsenic 10.0
9.96
99.6
80.0-120
Barium 10.0
10.2
102
80.0-120
Cadmium 10.0
9.98
99.8
80.0-120
Chromium 10.0
9.97
99.7
80.0-120
Lead 10.0
9.85
98.5
80.0-120
Selenium 10.0
10.3
103
80.0-120
Silver 2.00
1.98
98.9
80.0-120
L1574874-14 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1574874-14 01/18/23 20:52 • (MS) R3882356-4 01/18/23 20:58 • (MSD) R3882356-5 01/18/23 21:00
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
9.93
10.0
99.3
100
Barium
10.0
0.475
10.5
10.5
100
99.9
Cadmium
10.0
ND
9.96
9.96
99.6
99.6
Chromium
10.0
ND
9.91
9.94
99.1
99.4
Lead
10.0
0.239
10.0
10.0
98.1
97.7
Selenium
10.0
ND
10.3
10.3
103
103
Silver
2.00
ND
1.97
1.97
98.4
98.7
Dilution Rec. Limits
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MS Qualifier
MSD Qualifier RPD
0.721
0.277
0.0204
0.327
0.405
0.148
0.271
RPD Limits
20
20
20
20
20
20
20
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WG1990582 QUALITY CONTROL SUMMARY
Metals (ICP) by Method 6010D L1576104-01
L1576217-04 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576217-04 01/18/23 21:03 • (MS) R3882356-6 01/18/23 21:06 • (MSD) R3882356-7 01/18/23 21:09
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
Arsenic
10.0
ND
10.9
10.8
109
108
Barium
10.0
ND
10.0
9.97
99.1
98.8
Cadmium
10.0
ND
10.5
10.4
105
104
Chromium
10.0
0.609
10.5
10.4
98.6
97.6
Lead
10.0
1.07
11.0
10.9
99.1
98.5
Selenium
10.0
ND
11.4
11.3
114
113
Silver
2.00
ND
2.16
2.13
108
107
Dilution Rec. Limits MS Qualifier
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
1 75.0-125
MSD Qualifier RPD
0.864
0.329
0.542
0.990
0.562
0.706
1.14
RPD Limits
o�
20
20
20
20
20
20
20
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WG1989909
Volatile Organic Compounds (GC/MS) by Method 8260D
Method Blank (MB)
(MB) R3882090-3 01/17/23 12:21
MB Result
Analyte mg/I
Benzene
0.0674
Carbon tetrachloride
U
Chlorobenzene
U
Chloroform
U
1,2-Dichloroethane
U
1,1-Dichloroethene
U
2-Butanone (MEK)
U
Tetrachloroethene
0.0174
Trichloroethene
U
Vinyl chloride
U
(S) Toluene-d8
101
(S) 4-Bromof/uorobenzene
92.2
(S)1,2-Dichloroethane-d4
101
MB Qualifier MB MDL
mg/I
0.0167
0.0167
0.0167
0.0833
0.0167
0.0167
0.167
J 0.0167
0.0167
0.0167
QUALITY CONTROL SUMMARY
L1576104-01
MB RDL
mg/I
0.0500
0.0500
0.0500
0.250
0.0500
0.0500
0.500
0.0500
0.0500
0.0500
80.0-120
77.0-126
70.0-130
Laboratory Control Sample (LCS) • Laboratory Control Sample Duplicate (LCSD)
(LCS) R3882090-1 01/17/23 08:31 • (LCSD) R3882090-2 01/17/2311:21
Spike Amount
LCS Result
LCSD Result
LCS Rec.
LCSD Rec.
Rec. Limits
LCS Qualifier LCSD Qualifier RPD
RPD Limits
Analyte mg/I
mg/I
mg/I
%
%
%
%
%
Benzene 0.250
0.256
0.241
102
96.4
70.0-123
6.04
20
Carbon tetrachloride 0.250
0.287
0.263
115
105
68.0-126
8.73
20
Chlorobenzene 0.250
0.257
0.239
103
95.6
80.0-121
7.26
20
Chloroform 0.250
0.265
0.247
106
98.8
73.0-120
7.03
20
1,2-Dichloroethane 0.250
0.248
0.217
99.2
86.8
70.0-128
13.3
20
1,1-Dichloroethene 0.250
0.300
0.307
120
123
71.0-124
2.31
20
2-Butanone (MEK) 1.25
0.922
0.726
73.8
58.1
44.0-160
J3 23.8
20
Tetrachloroethene 0.250
0.237
0.229
94.8
91.6
72.0-132
3.43
20
Trichloroethene 0.250
0.263
0.239
105
95.6
78.0-124
9.56
20
Vinyl chloride 0.250
0.296
0.229
118
91.6
67.0-131
J3 25.5
20
(S) Toluene-d8
101
99.2
80.0-120
(S) 4-Bromofluorobenzene
97.1
94.9
77.0-126
(S)1,2-Dichloroethane-d4
98.4
102
70.0-130
ACCOUNT:
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SDG:
DATE/TIME: PAGE:
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WG1989909
Volatile Organic Compounds (GC/MS) by Method 8260D
QUALITY CONTROL SUMMARY
L1576104-01
L1576085-01 Original Sample (OS) • Matrix Spike (MS)
(OS) L1576085-01 01/17/2313:01 • (MS) R3882090-5 01/17/2315:20
Spike Amount
Original Result
MS Result
Analyte
mg/I
mg/I
mg/I
Benzene
0.250
ND
0.305
Carbon tetrachloride
0.250
ND
0.331
Chlorobenzene
0.250
ND
0.268
Chloroform
0.250
ND
0.303
1,2-Dichloroethane
0.250
ND
0.258
1,1-Dichloroethene
0.250
ND
0.406
2-Butanone (MEK)
1.25
ND
0.868
Tetrachloroethene
0.250
ND
0.252
Trichloroethene
0.250
ND
0.279
Vinyl chloride
0.250
ND
0.272
(S) Toluene-d8
(S) 4-Bromof/uorobenzene
(S)1,2-Dichloroethane-d4
MS Rec.
o/
ILL
132
107
121
103
162
69.4
101
112
109
97.0
96.1
107
Dilution Rec. Limits MS Qualifier
o/-
v.v-ioo
23.0-159
33.0-152
29.0-154
29.0-151
11.0-160
10.0-160
10.0-160
10.0-160
10.0-160
80.0-120
77.0-126
70.0-130
J5
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EMA Resources L1576104 01/24/23 09:03 15 of 23

WG1990310
Chlorinated Acid Herbicides (GC) by Method 8151A
Method Blank (MB)
(MB) R3883323-1 01/20/2312:44
MB Result
Analyte mg/I
2,4,5-TP (Silvex) U
2,4-D U
(S)2,4-Dichloropheny/Acetic 75.0
Acid
MB Qualifier MB MDL
mg/I
0.000667
0.000667
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1576104-01
MB RDL
Mg/1
0.00200
0.00200
14.0-158
(LCS) R3883323-2 01/20/2312:55
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/1
mg/1
%
%
2,4,5-TP (Silvex) 0.0500
0.0437
87.4
50.0-125
2,4-D 0.0500
0.0464
92.8
50.0-120
(S) 2,4-Dich/oropheny/Acetic
83.0
14.0-158
Acid
L1576038-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1576038-01 01/20/2316:57 • (MS) R3883323-3 01/20/2317:08 • (MSD) R3883323-4 01/20/2317:19
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/I
mg/1
mg/I
mg/I
%
%
2,4,5-TP (Silvex)
0.0500
ND
0.0309
0.0395
61.8
79.0
2,4-D
0.0500
ND
0.0350
0.0480
70.0
96.0
(S)2,4-Dichloropheny/Acetic
67.0
91.0
Acid
Dilution Rec. Limits MS Qualifier MSD Qualifier RPD
1 50.0-125 J3 24.4
1 50.0-120 J3 31.3
14.0-158
RPD Limits
o�
20
20
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EMA Resources L1576104 01/24/23 09:03 16 of 23

WG1989721
Pesticides (GC) by Method 8081B
Method Blank (MB)
(MB) R3882828-1 01/19/2317:12
MB Result
Analyte
mg/1
Chlordane
U
Endrin
U
Heptachlor
U
Heptachlor epoxide
U
Gamma BHC
U
Methoxychlor
U
Toxaphene
U
(S) Decachlorobipheny/
89.7
(S) Tetrach/oro-m-xylene
73.6
MB Qualifier MB MDL MB RDL
mg/I mg/1
Laboratory Control Sample (LCS)
QUALITY CONTROL SUMMARY
L1576104-01
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00167
0.00500
0.00333
0.0100
10.0-128
10.0-127
(LCS) R3882828-2 01/19/2317:21
Spike Amount LCS Result LCS Rec. Rec. Limits LCS Qualifier
Analyte mg/1 mg/1 % %
Endrin
0.0100
0.00885
88.5
57.0-134
Heptachlor
0.0100
0.00979
97.9
27.0-132
Heptachlor epoxide
0.0100
0.00987
98.7
57.0-130
Gamma BHC
0.0100
0.00920
92.0
55.0-129
Methoxychlor
0.0100
0.00976
97.6
54.0-155
(S) Decachlorobipheny/
82.7
10.0-128
(S) Tetrach/oro-m-xylene
72.8
10.0-127
L1575523-01 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1575523-01 01/19/2317:39 • (MS) R3882828-3 01/19/2317:48 • (MSD) R3882828-4 01/19/2317:56
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Analyte
mg/1
mg/1
mg/I
mg/1
%
%
Endrin
0.0100
ND
0.00981
0.00904
98.1
90.4
Heptachlor
0.0100
ND
0.0105
0.00970
105
97.0
Heptachlor epoxide
0.0100
ND
0.0108
0.00997
108
99.7
Gamma BHC
0.0100
ND
0.0100
0.00924
100
92.4
Methoxychlor
0.0100
ND
0.0104
0.00987
104
98.7
(S) Decachlorobipheny/
85.3
84.2
(S) Tetrach/oro-m-xylene
73.5
72.0
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
1 10.0-160
8.17
1 16.0-136
7.92
1 10.0-160
7.99
1 14.0-141
7.90
1 10.0-160
5.23
10.0-128
10.0-127
RPD Limits
39
40
36
40
34
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WG1989725
QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds
(GC/MS) by
Method 8270E
L1576104-01
Method Blank (MB)
(MB) R3882842-2 01/19/2316:14
MB Result
MB Qualifier
MB MDL
MB RDL
Analyte mg/I
mg/I
mg/I
1,4-Dichlorobenzene U
0.0333
0.100
2,4-Dinitrotoluene U
0.0333
0.100
Hexachlorobenzene U
0.0333
0.100
Hexachloro-1,3-butadiene U
0.0333
0.100
Hexachloroethane U
0.0333
0.100
Nitrobenzene U
0.0333
0.100
Pyridine U
0.0333
0.100
3&4-Methyl Phenol U
0.0333
0.100
2-Methylphenol U
0.0333
0.100
Pentachlorophenol U
0.0333
0.100
2,4,5-Trichlorophenol U
0.0333
0.100
2,4,6-Trichlorophenol U
0.0333
0.100
(S) 2-Fluorophenol 32.7
10.0-120
(S) Phenol-d5 19.7
10.0-120
(S) Nitrobenzene-d5 64.2
10.0-127
(S) 2-F/uorobipheny/ 65.7
10.0-130
(S) 2,4,6-Tribromophenol 61.0
10.0-155
(S) p-Terphenyl-d14 71.0
10.0-128
Laboratory Control Sample (LCS)
(LCS) R3882842-1 01/19/2315:51
Spike Amount
LCS Result
LCS Rec.
Rec. Limits LCS Qualifier
Analyte mg/I
mg/I
%
%
1,4-Dichlorobenzene 0.500
0.274
54.8
18.0-120
2,4-Dinitrotoluene 0.500
0.330
66.0
49.0-124
Hexachlorobenzene 0.500
0.272
54.4
44.0-120
Hexachloro-1,3-butadiene 0.500
0.262
52.4
19.0-120
Hexachloroethane 0.500
0.290
58.0
15.0-120
Nitrobenzene 0.500
0.310
62.0
27.0-120
Pyridine 0.500
0.0232
4.64
10.0-120 J4
3&4-Methyl Phenol 0.500
0.188
37.6
31.0-120
2-Methylphenol 0.500
0.198
39.6
28.0-120
Pentachlorophenol 0.500
0.305
61.0
23.0-120
2,4,5-Trichlorophenol 0.500
0.303
60.6
44.0-120
2,4,6-Trichlorophenol 0.500
0.279
55.8
42.0-120
(S) 2-F/uorophenol
29.3
10.0-120
(S) Phenol-d5
20.3
10.0-120
(S) Nitrobenzene-d5
57.3
10.0-127
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
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WG1989725 QUALITY CONTROL SUMMARY
Semi Volatile Organic Compounds (GC/MS) by Method 8270E L1576104-01
Laboratory Control Sample (LCS)
(LCS) R3882842-1 01/19/2315:51
Spike Amount LCS Result
Analyte mg/I mg/I
(S) 2-F/uorobiphenyl
(S) 2,4,6-Tribromophenol
(S) p-Terphenyl-dM
LCS Rec. Rec. Limits LCS Qualifier
59.5 10.0-130
57.0 10.0-155
62.0 10.0-128
L1575756-02 Original Sample (OS) • Matrix Spike (MS) • Matrix Spike Duplicate (MSD)
(OS) L1575756-02 01/19/2317:39 • (MS) R3882842-3 01/19/2318:00 • (MSD) R3882842-4 01/19/2318:21
Spike Amount
Original Result
MS Result
MSD Result
MS Rec.
MSD Rec.
Dilution Rec. Limits
MS Qualifier MSD Qualifier RPD
RPD Limits
Analyte
mg/I
mg/I
mg/I
mg/I
%
%
%
%
%
1,4-Dichlorobenzene
0.500
ND
0.246
0.286
49.2
57.2
1 17.0-120
15.0
40
2,4-Dinitrotoluene
0.500
ND
0.316
0.363
63.2
72.6
1 39.0-125
13.8
25
Hexachlorobenzene
0.500
ND
0.257
0.287
51.4
57.4
1 35.0-122
11.0
24
Hexachloro-1,3-butadiene
0.500
ND
0.220
0.255
44.0
51.0
1 12.0-120
14.7
34
Hexachloroethane
0.500
ND
0.255
0.298
51.0
59.6
1 10.0-120
15.6
40
Nitrobenzene
0.500
ND
0.281
0.333
56.2
66.6
1 12.0-120
16.9
30
Pyridine
0.500
ND
ND
0.105
18.5
21.0
1 10.0-120
12.7
37
3&4-Methyl Phenol
0.500
ND
0.164
0.176
32.8
35.2
1 10.0-120
7.06
36
2-Methylphenol
0.500
ND
0.173
0.187
34.6
37.4
1 10.0-120
7.78
30
Pentachlorophenol
0.500
ND
0.281
0.306
56.2
61.2
1 10.0-128
8.52
37
2,4,5-Trichlorophenol
0.500
ND
0.280
0.304
56.0
60.8
1 33.0-120
8.22
31
2,4,6-Trichlorophenol
0.500
ND
0.269
0.291
53.8
58.2
1 26.0-120
7.86
31
(S) 2-F/uorophenol
26.1
28.9
10.0-120
(S) Phenol-d5
16.6
19.7
10.0-120
(S) Nitrobenzene-d5
50.8
60.8
10.0-127
(S) 2-F/uorobipheny/
56.2
65.3
10.0-130
(S)2,4,6-Tribromophenol
54.5
58.0
10.0-155
(S) p-Terphenyl-d14
63.0
68.7
10.0-128
ACCOUNT:
PROJECT:
SDG:
DATE/TIME:
PAGE:
EMA
Resources
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GLOSSARY OF TERMS
Guide to Reading and Understanding Your Laboratory Report
The information below is
designed to better explain the various terms used in your report of analytical results from the Laboratory. This is not
u
intended as a comprehensive explanation, and if you have additional questions please contact your project representative.
Results Disclaimer - Information
that may be provided by the customer, and contained within this report, include Permit Limits, Project Name,
FTC
Sample ID, Sample Matrix,
Sample Preservation, Field Blanks, Field Spikes, Field Duplicates, On -Site Data, Sampling Collection Dates/Times, and
Sampling Location. Results relate to the accuracy of this information provided, and as the samples are received.
Abbreviations and Definitions
FSS
MDL
Method Detection Limit.
ND
Not detected at the Reporting Limit (or MDL where applicable).
rqn
RDL
Reported Detection Limit.
Rec.
Recovery.
Fr]
RPD
Relative Percent Difference.
SDG
Sample Delivery Group.
Surrogate (Surrogate Standard) - Analytes added to every blank, sample, Laboratory Control Sample/Duplicate and
e
QC
(S)
Matrix Spike/Duplicate; used to evaluate analytical efficiency by measuring recovery. Surrogates are not expected to be
detected in all environmental media.
U
Not detected at the Reporting Limit (or MDL where applicable).
Analyte
The name of the particular compound or analysis performed. Some Analyses and Methods will have multiple analytes
reported.
If the sample matrix contains an interfering material, the sample preparation volume or weight values differ from the
a
Dilution
standard, or if concentrations of analytes in the sample are higher than the highest limit of concentration that the
laboratory can accurately report, the sample may be diluted for analysis. If a value different than 1 is used in this field, the
result reported has already been corrected for this factor.
FSC
These are the target % recovery ranges or % difference value that the laboratory has historically determined as normal
Limits
for the method and analyte being reported. Successful QC Sample analysis will target all analytes recovered or
duplicated within these ranges.
Original Sample
The non -spiked sample in the prep batch used to determine the Relative Percent Difference (RPD) from a quality control
sample. The Original Sample may not be included within the reported SDG.
This column provides a letter and/or number designation that corresponds to additional information concerning the result
Qualifier
reported. If a Qualifier is present, a definition per Qualifier is provided within the Glossary and Definitions page and
potentially a discussion of possible implications of the Qualifier in the Case Narrative if applicable.
The actual analytical final result (corrected for any sample specific characteristics) reported for your sample. If there was
no measurable result returned for a specific analyte, the result in this column may state "ND" (Not Detected) or "BDL"
Result
(Below Detectable Levels). The information in the results column should always be accompanied by either an MDL
(Method Detection Limit) or RDL (Reporting Detection Limit) that defines the lowest value that the laboratory could detect
or report for this analyte.
Uncertainty
(Radiochemistry)
Confidence level of 2 sigma.
A brief discussion about the included sample results, including a discussion of any non -conformances to protocol
Case Narrative (Cn)
observed either at sample receipt by the laboratory from the field or during the analytical process. If present, there will
be a section in the Case Narrative to discuss the meaning of any data qualifiers used in the report.
Quality Control
This section of the report includes the results of the laboratory quality control analyses required by procedure or
Summary (Qc)
analytical methods to assist in evaluating the validity of the results reported for your samples. These analyses are not
being performed on your samples typically, but on laboratory generated material.
This is the document created in the field when your samples were initially collected. This is used to verify the time and
Sample Chain of
date of collection, the person collecting the samples, and the analyses that the laboratory is requested to perform. This
Custody (Sc)
chain of custody also documents all persons (excluding commercial shippers) that have had control or possession of the
samples from the time of collection until delivery to the laboratory for analysis.
This section of your report will provide the results of all testing performed on your samples. These results are provided
Sample Results (Sr)
by sample ID and are separated by the analyses performed on each sample. The header line of each analysis section for
each sample will provide the name and method number for the analysis reported.
Sample Summary (Ss)
This section of the Analytical Report defines the specific analyses performed for each sample ID, including the dates and
times of preparation and/or analysis.
Qualifier
Description
C3
The reported concentration is an estimate. The continuing calibration standard associated with this data responded low.
Method sensitivity check is acceptable.
J
The identification of the analyte is acceptable; the reported value is an estimate.
J3
The associated batch QC was outside the established quality control range for precision.
J4
The associated batch QC was outside the established quality control range for accuracy.
J5
The sample matrix interfered with the ability to make any accurate determination; spike value is high.
J6
The sample matrix interfered with the ability to make any accurate determination; spike value is low.
T8
Sample(s) received past/too close to holding time expiration.
ACCOUNT:
PROJECT: SDG: DATE/TIME: PAGE:
EMA Resources
L1576104 01/24/23 09:03 20 of 23

ACCREDITATIONS & LOCATIONS
Pace Analytical National 12065 Lebanon Rd Mount Juliet, TN 37122
Alabama
40660
Nebraska
NE-OS-15-05
Alaska
17-026
Nevada
TN000032021-1
Arizona
AZ0612
New Hampshire
2975
Arkansas
88-0469
New Jersey—NELAP
TN002
California
2932
New Mexico
TN00003
Colorado
TN00003
New York
11742
Connecticut
PH-0197
North Carolina
Env375
Florida
E87487
North Carolina'
DW21704
Georgia
NELAP
North Carolinas
41
Georgia'
923
North Dakota
R-140
Idaho
TN00003
Ohio—VAP
CL0069
Illinois
200008
Oklahoma
9915
Indiana
C-TN-01
Oregon
TN200002
Iowa
364
Pennsylvania
68-02979
Kansas
E-10277
Rhodelsland
LA000356
Kentucky16
KY90010
South Carolina
84004002
Kentucky 2
16
South Dakota
n/a
Louisiana
A130792
Tennessee' °
2006
Louisiana
LA018
Texas
T104704245-20-18
Maine
TN00003
Texas'
LAB0152
Maryland
324
Utah
TN000032021-11
Massachusetts
M-TN003
Vermont
VT2006
Michigan
9958
Virginia
110033
Minnesota
047-999-395
Washington
C847
Mississippi
TN00003
West Virginia
233
Missouri
340
Wisconsin
998093910
Montana
CERT0086
Wyoming
A21-A
A21-A — ISO 17025
1461.01
AIHA-LAP,LLC EMLAP
100789
A21-A — ISO 17025 s
1461.02
DOD
1461.01
Canada
1461.01
USDA
P330-15-00234
EPA—Crypto
TN00003
Drinking Water 2 Underground Storage Tanks 'Aquatic Toxicity ° Chemical/Microbiological 'Mold 6 Wastewater n/a Accreditation not applicable
Not all certifications held by the laboratory are applicable to the results reported in the attached report.
Accreditation is only applicable to the test methods specified on each scope of accreditation held by Pace Analytical.
FP1
FTc
FSS
rqn
Fr]
R
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FSC
ACCOUNT: PROJECT: SDG: DATE/TIME:
EMA Resources L1576104 01/24/23 09:03
PAGE:
21 of 23

Company Name/Address:
Billing Information:
EMA Resources
Mr. Brent Collins
Pres
75S Yadkinville Road
chk
755 Yadkinville Road
Mocksville, INC 27028
Mocksville, NC 27028
Report to
Email To'.
Mr. Brent Collins
[e-mail];roy.whitak
Project Description:
City/State
Collected: InCCIIIL" LNG
Please Circle
PT MT C1 O
Sludge
Phone: [phone]
Client Project #
Lab Project #
Collected by (print):
Collected by (signature):
Immediately /
Packed on Ice N Y v
Sample ID
..
" Matrix:
SS - Soil AIR - Air F - Filter
GW - Groundwater 8 - Bioassay
WW - WasteWater
DW - Drinking Water
OT - Other F
Relinquished by : (Signature)
Relinquished by : (Signature)
Site/Facility ID #
P.O #
a
a
o
z°
Rush? (Lab MUST Be Notified) Quote #
U
Same Day _ Five Day
Z
J
Next Day _ 5 Day (Rad Only) Date Results Needed
Two Day _ 10 Day (Rad Only) No
V
Three Day of
_J
N
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d
Comp/Grab
Matrix'
Depth
Date
Time
ntrs
U
U
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2
X
x
rks:
Samples returned via:
—UPS _ FedEx —Courier
Date: Time.
i!rIZ3 3,^,Yo
Date: Time
Tracking # 5 q' C j 3
Received by: (Signature) 11
Received by: (Sign
-ha'n ofCu5tody Page _ of
aceAnalytical
17065 Lebanon Rd Mount Whet. TN 37122
Sutxna-g a ampl, na Nis chain of custody
pmtttutes acM—ftnigment and—ptance nl the
pace Tetras and Cond.1— found at.
http,.//,ofo-wcelam com/hubra/pa-Unda.d
teem, par 1 �J
SDG # to Lf
D242
Acctnum: EMARES
Template:T11413
Prelogin: P895402 n
PM: 800 - Justin Carr
A via:fedEX Ground
Remarks Sample # (lab only(
-o�
Sample Rec-irlt Chec4ist
pH Temp
CGC Seal Present/Intact: V
NP
COC Signed/Accurate:
_Y
_
Flow Other
Bottles arrive intact:
/f
_N
N
Correct bottles used:
�Y/_N
Sufficient volume sent:
�7
1. l 0
If Applicable
_N
VGA Zero Headspace:
N
Blank Received: Yes 0
preservation Correct/Checked:
_Y
RAD Screen <0.5 mR/hr:
�ily
N
H MeoH
—N
TBR
Bottles Received:
If preservation required by Login:
Date/Time
7 �
v
Relinquished by : (Signature) Date Time: Received for lab by: (Signature) Date: Time: Hold: Conditio
0415 NCF /
I .

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: Town of Mocksville WQ Permit Number: W00003351
WWTP Name: _
Monitoring Period:
Dutchman's Creek WWTP
From 1 / 1 /2023 To 12/31 /2023
PWS Number: NCO021491
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp)
Alt B (Alk Treatment)[3
Alt. C (Prior Testing)®
A1t.D (No Prior Test) El
I Process to Further Reduce Pathogengs El
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ®
Heat Drying [3
Heat 'Treatment 13
Thermo hilic Q
Beta Ray ®
Gamma. Ray D
t Pasteurization Q
Class B:
Alt. (1) Fecal Density El
I Alt. (2) Process to Significantly Reduce Pathogens [j
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization R1
Air Drying 13
Composting ®
Aerobic Digestion El
Anaerobic Digestion LJ
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
f o
NumberFrequency
Excee-
of Analysis
Sample
Type
Analytical
Tech-nique
Minimun
Geo. Mean
aximu
Unitsences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
M?N
CFU
144928
176714
204082
CFU/g
0
Annually
Grab
SM9222D
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform) I
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.I (VS reduction) Q
Alt. 2 (40-day bench) [I
Alt. 3 (30-day bench) R1
Alt. 4 (Spec. O, uptake) El
All. 5 (14-Day Aerobic) ®
Alt. 6 (Alk. Stabilization ll
Alt 7 (Drying - Stable) C
Alt. 8 (Drying - Unstable)
Alt. 9 (Injection) Ll
Alt. 10 (incorporation) iI
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
21 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if
you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed
to ensure that qualified personnel properly gather and evaluate the information used to determine that the
pathogen and vector attraction reduction requirements have been met. I am aware that there are significant
penalties for false certification including fine and imprisonment."
Dennis Murdoch - ORC
Brent Collins - Director of Technical Services
Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
1/26/24 1 /22/2024
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC: 2T .1112 (26)
DENR FORM PVRF 02T (12/2006)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
or.7� ow!
;0
Contact: Brent Collins Report Date: 1/Page Page 1
Client: EMA Resources, Inc
24/2023
755 Yadkinville Road
Mocksville, NC 27028 Date Sample Rcvd: 1/17/2023
Meritech Work Order # 01172331 Sample: Mocksville 1 Grab 1/17/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.08 % 1/18/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 187,500 CFU/g dry wt 1/17/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 01172332 Sample: Mocksville 2 Grab 1/17/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.06 % 1/18/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 199,029 CFU/g dry wt 1/17/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 01172333 Sample: Mocksville 3 Grab 1/17/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.06 % 1/18/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 179,612 CFU/g dry wt 1/17/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 01172334 Sample: Mocksville 4 Grab 1/17/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.07 % 1/18/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 144,928 CFU/g dry wt 1/17/23 130 CFU/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

low*
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 2
Report Date: 1/24/2023
Date Sample Rcvd: 1/17/2023
Meritech Work Order # 01172335 Sample: Mocksville 5 Grab 1/17/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 1.96 % 1/18/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 204,082 CFU/g dry wt 1/17/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 01172336 Sample: Mocksville 6 Grab 1/17/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids 2.14 % 1/18/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 158,879 CFU/g dry wt 1/17/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 01172337 Sample: Mocksville 7 Grab 1/17/23
Parameters Result Analysis Date Reporting Limit Method
% Total Solids
199 %
1/18/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
170,854 CFU/g dry wt
1/17/23
130 CFU/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. nc Oe
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Brent Collins
Client: EMA Resources, Inc
755 Yadkinville Road
Mocksville, NC 27028
Report Date: 2/22/2023
Date Sample Rcvd: 1/17/2023
Vector Attraction Reduction / Aerobically Digested Sludge (30 Day Test
Meritech Work Order # 01172330 Sample: Mocksville Composite 1/17/23
Total Solids Volatile Solids % Volatile Solids
Week 1 1.04 0.78 0.752
Week 2
1.08
0.80
0.744
Week 3
0.94
0.69
0.733
Week 4
0.78
0.58
0.747
Week 5
0.86
0.63
0.730
Van Kleek Reduction (%): 11.14
I hereby certify that I have reviewed and approve these data. 4ffb Ir H CVaft &-
Laboratory Representative
642 Ta ico Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY23-SL031776
Client: Roger Spillman
Advisor: Brent Collins
Predictive
PO Box 378
EMA Resources Inc
£
Cooleemee, NC 27014
755 Yadkinville Rd
x "
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Davie
Links to Helpful Information
Client ID: 411288
Advisor ID: 405413
Sampled:
Received: 05/04/2023 Completed: 05/15/2023
Farm: DV08
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.5
120-200 0
0 0 0
0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.51 1.01
6.5 78 1.4 5.7 68 177
44 20
59 292 192 192
311
311
95 0.1 2
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL00l 112
Client: Roger Spillman
Advisor: Brent Collins
Predictive
PO Box 378
EMA Resources Inc
£
Cooleemee, NC 27014
755 Yadkinville Rd
x " Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Davie
Links to Helpful Information
Client ID: 411288
Advisor ID: 405413
Sampled: 07/20/2023 Received: 07/24/2023 Completed: 08/04/2023
Farm: DV08
Sample ID: 00008
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1- Fescue/OGrass/Tim, M 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
0 0 0
0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.56 0.98 10.0 85 1.5 6.1 87 203
54 21
32 880 543 543
452
452
265 0.1 1
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler. Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY23-SL031772
Client: Art Rupard
Advisor: Brent Collins
Predictive
134 Rupard TO
EMA Resources Inc
£
Mocksville, NC 27028
755 Yadkinville Rd
x "
Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Sampled County: Davie
Links to Helpful Information
Client ID: 478106
Advisor ID: 405413
Sampled:
Received: 05/04/2023 Completed: 05/15/2023
Farm: MK01
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O Mg S
Mn
Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 120
40 0 0
pH$
0
0 0
Note: 12 Note:
2 - Fescue/OGrass/Tim, M 0.0
120-200 120
40 0 0
pH$
0
0 0
Note: 12 Note:
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V
CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1 Mn-I Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.13 0.98
15.5 95 0.8 6.5 9 50
65 28
27 365 228 228
152
152
192 0.2 1
North Carolina
lobitty lru%t FuivJ Ctwnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY24-SL006079
Client:
Chris Vaughn
Advisor: Brent Collins
Predictive
Town of Mocksville
EMA Resources Inc
£
P. O. Box 532 / 171 South
Clement
755 Yadkinville Rd
Soil Report Mehlich-3 Extraction
Street
Mocksville, NC 27028
Mocksville, NC 27028
Links to Helpful Information
Client IDSamOWunty : Davie
Advisor ID: 405413
Sampled: Received: 10/03/2023 Completed: 10/11/2023
Farm: MK05
Sample ID: 00001
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
100
0 0
pH$ 0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.27 1.11 10.7 100 0.0 7.2 193 19
88 11
34
868
519
618 618
362 0.1 1
Sample ID: 00002
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1 - Fescue/OGrass/Tim, M 0.0
120-200 0
30
0 0
pH$ 0
0 0
Note: 12 Note:
2 - 0.0
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg%
S-1
Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.56 0.99 12.6 100 0.0 7.3 64 57
86 11
47
890
531
295 295
151 0.1 1
North Carolina
A� `� J
lobitt o iru%( Fulxl Umnauukm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

2023 Mocksville Annual Report - WQ0003351
Final Audit Report 2024-02-02
Created: 2024-02-01
By: Brent Collins ([e-mail])
Status: Signed
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