WQ0001863_2023 Residual Annual Report_20240220 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0001863
Applicant/Permittee City of Mount Holly
Email Notifications
Does this need review by the hydrogeologist? * Yes No
Regional Office Mooresville
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Lysa Finnerty
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
4105376150
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0001863
Has Current Existing permit number
Applicant/Permittee Address*
435 Williams Court, Ste 100, Baltimore, MD 21220
Facility Name*
City of Mount Holly Class B Residuals Program
Please provide comments/notes on your current submittal below.
Submission of the 2023 Annual Report for City of Mount Holly, NC
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
Mt Holly NC 2023 Annual Report FINAL.pdf 30.37MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Alva �Cit'wt%tl�
Submission Date 2/20/2024

435 Williams Court, Suite 100
Baltimore, MD 21220
www.synagro.com
FEBRUARY 20, 2024
NCDEQ
Division of Water Resources
Information Processing Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: 2023 Annual Report for Permit No. WQ0001863
Dear NCDEQ:
SYNAGRO
Synagro is submitting one electronic copy of the above referenced report on behalf of the City
of Mount Holly, NC.
If you have any questions or need additional information, please do not hesitate to contact
Danny Jackson at [phone] or Alex Fox at [phone].
Sincerely,
P '�ELY--
Derrick Shivar
Environmental Compliance Manager
Enclosures
cc: Danny Jackson, City of Mount Holly
Alex FoxM, Synagro
YOUR PARTNER FORA CLEANER, GREENERWORLD

City of Mount Holly, NC
RESIDUALS LAND APPLICATION PROGRAM
Permit No. WQ0001863
2023 ANNUAL REPORT

City of Mount Holly, NC
Residuals Land Application Program
2023 Annual Report
TABLE OF CONTENTS
1. Certification Form and Annual Operations Summary
2. Annual Residual Sampling Summary Forms and Residuals
Analyses
3. Annual Land Application Field Summary Forms
4. TCLP Analysis
5. Pathogen ReductionNector Attraction Reduction
6. Soil pH & Lime Application Records
7. Soil Analyses

SECTION 1

ANNUAL LAND APPLICATION CERTIFICATION FORM
WQ Permit #: W00001863 County Gaston Year 2023
Facility Name (as shown on permit) Mount Holly WWTP & WTP NPDES No. NC0021156 & 01-36-020
Land Application Operator Synagro Phone# [phone]
Land application of residuals as allowed by the above permit occurred during the past calendar year?
X YES NO. If NO, skip Part A, and Part B and proceed to Part C. Also, if residuals were generated but not land applied,
please attach an explanation on how the residuals were handled.
Part A — Residuals Application Summa
Total number of application fields in the permit: 16
Total number of fields utilized for land application during the year: 6
Total amount of dry tons applied during the year for all application sites: 108.83
Total number of acres utilized for land application during the year: 92.90
Part B — Annual Compliance Statement:
Facility was compliant during calendar year 2023 with all conditions of the land application permit (including but not limited to items
1-13 below) issued by the Division of Water QualityX YES NO.
If no, please provide a written description why the facility was not compliant, the dates, and explain corrective action taken.
I . Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit,
3. Annual soils analysis was performed on each site receiving residuals during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading
Rates in 15A NCAC 02T .1105(b) (Applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503
regulated facilities).
8. All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503
regulated facilities).
9. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
11. Vegetative cover was maintained and proper crop management was performed on each site receiving residuals, as specified
in the permit.
12. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13. All buffer requirements as specified on the permit were maintained during each application of residuals.
Part C — Certification.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete.
am aware that there are significant penalties for submitting faas(gauture
, including the possibility of fines and imprisonment for
knowing violations." //j�
Jonathan Blanton Cit Manager U;"
Permittame and itle ( e or print) Pqrmittee ate
l!/ « 2/01/2024
gnature of Prcp rer* bate i a re of Jd Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006)

OPERATIONS SUMMARY - LAND APPLICATION - NORTH CAROLINA
ALL COUNTIES - ALL SITES
PERMIT # WQ0001863
DATE RANGE: 1/1/2023 - 12/31/2023
MOUNT HOLLY, NC
MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
MONTH/YEAR
August 2023
October 2023
November 2023
IEel /_1I
Units Key: D - Dry Tons; G — Gallons; W — Wet Tons; Y — Cubic Yards
Report Date: 2/1/2024 5:03:02 PM
AMOUNT
UNIT
DRY TONS
UNIT
DRY METRIC TONS
415,400.00
G
33.26
D
30.17
477,400.00
G
31.45
D
28.53
669,600.00
G
44.12
D
40.01
1,562,400.00
G
108.83
D
98.71

SECTION 2

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00001863
Facility Name: MOUNT HOLLY, NC
Residual Source WO # or
NPDES#: NCO021156
WWTP Name: MOUNT HOLLY WWTP
Residual Analysis Data
Laboratory:
PACE ANALYTICAL; Waypoi nt Analytical Virginia
Inc.
Product Type
Sample or Composite Date
AEDLIQ
01/12/23
AEDLIQ
04/04/23
AEDLIQ
07/05/23
AEDLIQ
10/03/23
Parameter (mglkg dry weight)
Ceiling Conc.
Limit
Percent Solids (%)
NA
1.45
2.01
1.92
1.58
Arsenic
75
8
4.7
<22
<31.3
Cadmium
65
2
1.1
<5.4
<6.25
Copper
4300
490
330
560
441
Chromium
NA
250
140
260
255
Lead
840
11
9
21
<18.8
Mercury
57
<1.2
<0.92
<0.99
<11.4
Molybdenum
75
<11
<7.3
<43
<15.6
Nickel
420
17
9.3
<45
17.3
Selenium
100
<8.6
<6
<35
<31.3
Zinc
7500
800
480
690
663
Total Phosphorus
NA
21000
13000
13000
13900
TKN
NA
85000
65000
72000
93800
Ammonia -Nitrogen
NA
7900
7700
15000
11800
Nitrate and Nitrite
NA
720
430
187.5
<313
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
Z-e, i& /' 41
Signature of Preparer* Date
*Preparer is defined in 40 CPR Part 503.9(r) and 15 A NCAC 2T.1102(26) DENR FORM RSSF (12/2006)
Printed: 2I3/2024 6:54:46 PM For: 170101

ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B
Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past
calendar year. Use additional forms as needed.
WQ Permit Number: WQ0001863 Laboratory;
Facility Name: MOUNT HOLLY, NC PACE ANALYTICAL; Waypoint Analytical Virginia
Residual Source Inc.
NPDES # or WQ#: N00021156
WWTP Name: MOUNT HOLLY WWTP
Residual Analysis Data
Product Type
AEDLIQ
AEDLIQ
AEDLIQ
AEDLIQ
Sample or Composite Date
01/12/23
04/04/23
07/05/23
10/03/23
Parameters (mglkg dry weight)
Aluminium
17000
10000
14000
11800
Calcium
13000
6900
10000
10300
Magnesium
3900
3400
3500
3170
pH (sx.)
7.50
7.10
7.40
7.40
Potassium
4200
4700
<2700
3080
Sodium
7800
6100
5300
7810
PAN
27800
21470
24788
30795
SAR (Ratio)
1.8495
2.1214
1.6049
2.1625
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordiance with a system designed to assure that qualified
personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the
possibility of fines and imprisonment for knowing violations."
1,r-, �4 Z' LwZ-
Signature of Preparer " rDate
'Preparer is defined in 40 CFR Part 503.9(r) and 15 A NCAC 2T.1102(26)
Printed: 2/3/2024 6:56:13 PM For: 170101 DENR FORM RSSF-B (12(2006)

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Mt. Holly
Lot Number:YA12094
Date Completed:01/30/2023
NIM�� Mr�
01/30/2023 3:05 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: YA12094
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Sample -001 has been analyzed using approximately three grams of sample due to the low percent solid
level. The LOQs have been adjusted accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:YA12094-001
Description: MT HOLLY Matrix: Solid
Date Sampled:01/12/2023 0845 % Solids: 1.45 01/16/2023 1842
Date Received:01/12/2023
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 01/16/2023 1842 TAD
65010
1 350.1
(Ammonia - N ) 350.1
5 01/25/2023 1321 DMA
65582
1
(Nitrate - N ) 353.2
1 01/26/2023 1128 CMM
66119
1
(Nitrite - N ) 353.2
1 01/26/2023 1128 CMM
66116
1
(Phosphorus) 365.1
10 01/16/2023 1849 DMA
01/16/2023 0859
64846
1
(Soil pH meas) 9045D
1 01/13/2023 1435 BMG2
64417
2 351.4
(TKN) 351.2
1 01/19/2023 1753 DMA
01/17/2023 1258
64991
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 254OG
1.45
%
1
Ammonia - N (gas diffusion)
350.1
7900 S
340
180
mg/kg
1
Nitrate - N (soluble)
353.2
590
14
1.8
mg/kg
1
Nitrite - N (soluble)
353.2
130
14
1.8
mg/kg
1
Phosphorus
7723-14-0 365.1
21000
3400
690
mg/kg
1
Soil pH measured in water @
19.2 ° C
9045D
7.5
su
1
TKN
351.2
85000
3400
1700
mg/kg
2
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471B
7471B
1 01/14/2023 1401 MRW2
01/14/2023 1025
64810
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
4.9
1.2
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
1 01/18/2023 0007 JMH
01/17/2023 0843
64804
2 3050B
601OD
1 01/19/2023 0101 JMH
01/17/2023 0843
64804
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
17000
430
160
mg/kg
1
Arsenic
7440-38-2 6010D
8.0 J
16
5.3
mg/kg
1
Cadmium
7440-43-9 6010D
2.0 J
5.3
1.3
mg/kg
1
Calcium
7440-70-2 6010D
13000
5300
660
mg/kg
1
Chromium
7440-47-3 6010D
250
11
2.7
mg/kg
1
Copper
7440-50-8 6010D
490
11
4.8
mg/kg
1
Iron
7439-89-6 6010D
9900
110
48
mg/kg
1
Lead
7439-92-1 6010D
11
11
4.8
mg/kg
1
Magnesium
7439-95-4 6010D
3900 J
5300
660
mg/kg
1
Manganese
7439-96-5 6010D
220
16
6.3
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
43
11
mg/kg
1
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:YA12094-001
Description: MT HOLLY Matrix: Solid
Date Sampled:01/12/2023 0845 % Solids: 1.45 01/16/2023 1842
Date Received:01/12/2023
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date Batch
1 3050B
6010D 1 01/18/2023 0007 JMH
01/17/2023 0843 64804
2 3050B
6010D 1 01/19/2023 0101 JMH
01/17/2023 0843 64804
CAS Analytical
Parameter
Number Method
Result Q LOQ
DL
Units
Run
Nickel
7440-02-0 6010D
17 J 43
11
mg/kg
2
Potassium
7440-09-7 6010D
4200 J 5300
660
mg/kg
1
Selenium
7782-49-2 601OD
ND 21
8.6
mg/kg
1
Sodium
7440-23-5 6010D
7800 5300
660
mg/kg
1
Zinc
7440-66-6 6010D
800 53
13
mg/kg
2
LOQ = Limit of Quantitation B = Detected in the method blank E = Quantitation of compound exceeded the calibration range DL = Detection Limit Q = Surrogate failure
ND = Not detected at or above the DL N = Recovery is out of criteria P = The RPD between two GC columns exceeds 40 % J = Estimated result < LOQ and > DL L = LCS/LCSD failure
H = Out of holding time W = Reported on wet weight basis S = MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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Yes N 12. V4'crc all satuplrs Ioeive€f Wililiti ; the holding tint off,18 hours, Aiichever c0331c.31
es tea 13. Were rill sa,nplt s coidabicrs accowl[od rao (,%io nvsszn excess]
'Yes L]Nu W]NA ld_ Ware O,, S(115C mdRSK-175 samples f= of�ubblea >-pca-sire° (ia, r 61r3m io
I&I"Iftf) iA filly offic VOA vials?
- RYes Tin V A 15, Were All DRCk taisfimtrlcrq matt ley rCCet9led St a 1� ?
Yes Igo 'A 16, Werc all aide 1� reeeivtA ak a I > 12 and sulQde 4ao 1cs received n a
[:]YcK []NO 0N,� 17 6. Were ill aMllkab . r 8.3 < 0.5v> f.) s.-dcples fjzV o
idtlaI rhlorirrc?
nYcs No �ldA i _ 4rfas file q wte ffili �ncM
C listed on � contahier labol` if yes. ote.o
JLuplr PH3( %-M99 (Mtls: be complzotd iar arty samples) ii icarrectl pk' s rveff or l',ril$ l�cadsp ice_}
jnpS) NA WT.' feccivcd iucoin� dlylircwrved wid v?m adjastrtl acmrd11lt4,ly
sauJplc feoeking 1011 i'aA _mL of circke : H $04. HNOS, H(`i. NaOH using SR V
rID Of prestry ore NA. If mmr than one piesavalive i3 needed, please Ilan ila the cOQItr1 nm lie )w_
` VMW 11XL1W-d with Nibbles >6 nini iu dianwter.
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t'%tm IccciWd VOh '[ RC i I1.5 ingfl_ ,If #19 is pm}Jii14 Wevu
ed accor&loy ilk &vf',plerff&%'[lOVXA SOIR011 t]tiosulfarc (Nvi,SzOj' with Uiliflur ID: NA
�lJEitlIJS3Ik�:
QualtroxiD,56215D PaceOAnaryticaf Servloes, ULC
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (7800 x 1.4500) = 100 = 113.1
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (13000 x 1.4500) = 100 = 188.5
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3900 x 1.4500) = 100 = 56.55
Na meq = Na mg/I = Molec.Wgt.Na = 113.1 = 23 = 4.91739
Ca meq = Ca mg/I = Molec.Wgt.Ca = 188.5 = 20 = 9.425
Mg meq = Mg mg/I = Molec.Wgt.Mg = 56.55 = 12 = 4.7125
Sample Date Report Range Ratio
1 /12/2023 1 /1 /2023 - 3/31 /2023 1.8495
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.91739 = SgrRoot[0.5(9.425+4.7125)] = 1.84954

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Mt. Holly
Lot Number:YD05129
Date Completed:04/27/2023
NIM�� Mr�
04/27/2023 3:24 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: YD05129
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
The following samples were classified as biosolids therefore in order to ensure proper digestion, the
samples were weighed out around 3.00-3.50 grams: YD05129-001. The LOQ has been adjusted
accordingly.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] vvvvvv.pacelabs.com
Page 2 of 7

Client:Synagro Laboratory ID:YD05129-001
Description: Mt Holly Matrix: Solid
Date Sampled: 04/04/2023 1000 % Solids: 2.01 04/10/2023 1756
Date Received:04/05/2023
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 04/10/2023 1756 TAD
72264
1 350.1
(Ammonia - N ) 350.1
5 04/14/2023 1532 CMM
72694
1
(Nitrate - N ) 353.2
1 04/19/2023 1433 CLL2
73337
1
(Nitrite - N ) 353.2
1 04/19/2023 1433 CLL2
73569
1
(Phosphorus) 365.1
10 04/11/2023 1739 DMA
04/07/2023 1132
71968
2
(Soil pH meas) 9045D
1 04/10/2023 1530 BMG2
72224
1 351.4
(TKN) 351.2
2 04/10/2023 1314 BMG2
04/07/2023 1040
71967
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 2540G
2.01
%
1
Ammonia - N (gas diffusion)
350.1
7700 S
250
130
mg/kg
1
Nitrate - N (soluble)
353.2
230 S
9.9
1.3
mg/kg
1
Nitrite - N (soluble)
353.2
200 S
9.9
1.3
mg/kg
1
Phosphorus
7723-14-0 365.1
13000
2500
500
mg/kg
1
Soil pH measured in water C
16 ° C
9045D
7.1
su
2
TKN
351.2
65000
5000
2500
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 04/18/2023 1817 KAJ
04/13/2023 1410
72168
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
3.8
0.92
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D
1 04/13/2023 1135 JMH
04/08/2023 1347
71943
2 3050B
6010D
2 04/20/2023 0819 JMH
04/08/2023 1347
71943
3 3050B
6010D
1 04/26/2023 0116 JMH
04/22/2023 0250
73363
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 6010D
10000
290
110
mg/kg
1
Arsenic
7440-38-2 6010D
4.7 J
11
3.7
mg/kg
1
Cadmium
7440-43-9 6010D
1.1 J
3.7
0.92
mg/kg
1
Calcium
7440-70-2 6010D
6900
3700
460
mg/kg
1
Chromium
7440-47-3 6010D
140
7.3
1.8
mg/kg
1
Copper
7440-50-8 6010D
330
7.3
3.3
mg/kg
1
Iron
7439-89-6 601OD
6200
77
35
mg/kg
3
Lead
7439-92-1 601OD
9.0
7.3
3.3
mg/kg
1
Magnesium
7439-95-4 601OD
3400 J
7300
920
mg/kg
2
Manganese
7439-96-5 6010D
100
11
4.3
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client:Synagro Laboratory ID:YD05129-001
Description: Mt Holly Matrix: Solid
Date Sampled: 04/04/2023 1000 % Solids: 2.01 04/10/2023 1756
Date Received:04/05/2023
ICP-AES
Run
Prep Method
Analytical Method
Dilution
Analysis Date Analyst
Prep Date Batch
1
3050B
6010D
1
04/13/2023 1135 JMH
04/08/2023 1347 71943
2
3050B
6010D
2
04/20/2023 0819 JMH
04/08/2023 1347 71943
3
3050B
6010D
1
04/26/2023 0116 JMH
04/22/2023 0250 73363
CAS Analytical
Parameter Number Method Result Q LOQ DL Units Run
Molybdenum
7439-98-7
Nickel
7440-02-0
Potassium
7440-09-7
Selenium
7782-49-2
Sodium
7440-23-5
Zinc
7440-66-6
601OD
ND
29
7.3
mg/kg 1
601OD
9.3 J
29
7.7
mg/kg 1
601OD
4700
3800
480
mg/kg 3
601OD
ND
15
6.0
mg/kg 1
601OD
6100 J
7300
920
mg/kg 2
601OD
480
37
9.2
mg/kg 1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
DCK Tatlo- EIdV-FRM-�NCOL- 85 Vb _S�Impl�s Rec i Q�e�l�list;5li j
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Page I of I
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (6100 x 2.0100) = 100 = 122.61
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (6900 x 2.0100) = 100 = 138.69
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3400 x 2.0100) = 100 = 68.34
Na meq = Na mg/I = Molec.Wgt.Na = 122.61 = 23 = 5.33087
Ca meq = Ca mg/I = Molec.Wgt.Ca = 138.69 = 20 = 6.9345
Mg meq = Mg mg/I = Molec.Wgt.Mg = 68.34 = 12 = 5.695
Sample Date Report Range Ratio
4/4/2023 4/1 /2023 - 6/30/2023 2.1214
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.33087 = SgrRoot[0.5(6.9345+5.695)] = 2.12139

0p
0
PaceAnalyfical
Report of Analysis
Synagro
12701 Lancaster Hwy
Pineville, NC 28134
Attention: Alex Fox
Project Name: Mt. Holly
Lot Number:YG07060
Date Completed:07/25/2023
07/25/2023 7:11 PM
Approved and released by:
Project Manager II: Lucas Odom
Q PCCRBp��
AAW
'ye I
ANSI NdmlAccre00- Board
eORft
Al
A C C R E D I T E D
TESTING LABORATORY
The electronic signature above is the equivalent of a handwritten signature.
This report shall not be reproduced, except in its entirety, without the written approval of Pace Analytical Services, LLC.
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172
Tel:[phone] Fax:[phone] www.pacelabs.com
Page 1 of 7

PACE ANALYTICAL SERVICES, LLC
SC DHEC No: 32010001 NELAC No: E87653 NC DENR No: 329 NC Field Parameters No: 5639
Case Narrative
Synagro
Lot Number: YG07060
This Report of Analysis contains the analytical result(s) for the sample(s) listed on the Sample Summary
following this Case Narrative. The sample receiving date is documented in the header information
associated with each sample.
All results listed in this report relate only to the samples that are contained within this report. Where
sampling is conducted by the client, results relate to the accuracy of the information provided, and as the
samples are received.
Sample receipt, sample analysis, and data review have been performed in accordance with the most
current approved The NELAC Institute (TNI) standards, the Pace Analytical Services, LLC ("Pace")
Laboratory Quality Manual, standard operating procedures (SOPs), and Pace policies. Any exceptions to
the TNI standards, the Laboratory Quality Manual, SOPs or policies are qualified on the results page or
discussed below.
Pace is a TNI accredited laboratory; however, the following analyses are currently not listed on our TNI
scope of accreditation: Drinking Water: VOC (excluding BTEX, MTBE, Naphthalene, & 1,2-
dichloroethane) EPA 524.2, E. coli and Total coliforms SM 9223 B-2004, Solid Chemical Material: TOC
Walkley-Black, Biological Tissue: All, Non -Potable Water: SGT-HEM EPA 1664B, Silica EPA 200.7,
Boron, Calcium, Silicon, Strontium EPA 200.8, Bicarbonate, Carbonate, and Hydroxide Alkalinity SM 2320
B-2011, SM 9221 C E-2006 & SM 9222D-2006, Strontium SW-846 6010D, VOC SM 6200 B-2011, Fecal
Coliform Colilert-18, PFAS by Isotope Dilution SOP.
Pace is a DoD/DoE and TNI accredited laboratory; however, Pace is not accredited for PFAS Direct
Aqueous Injection or Method D8421.
Where applicable, all soil sample results (including LOQ and DL if requested) are corrected for dry weight
unless flagged with a "W" qualifier.
If you have any questions regarding this report, please contact the Pace Project Manager listed on the
cover page.
The pH analysis associated with the sample(s) in this report was/were performed after the method
recommended 15 minute holding time.
Inorganic Metals
Sample -001 was classified as biosolids therefore in order to ensure proper digestion, the sample was
weighed out to between 3.0 - 3.5 grams. The LOQ has been adjusted accordingly.
The method blank for analytical batch 80621 contained Copper greater than the acceptance criteria. The
associated samples contained detections for this analyte at concentrations greater than 1 OX the value
found in the method blank; therefore sample results are not impacted. The data has been reported.
Inorganic Non -Metals
The method blank for prep batch 79588 contained total phosphate greater than the method acceptance
criteria. The associated samples contained detections for this analyte at concentrations greater than 1 OX
the value found in the method blank; therefore sample results are not impacted. The data has been
reported.
Pace Analytical Services, LLC (formerly Shealy Environmetal Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 2 of 7

Client: Synagro Laboratory ID: YG07060-001
Description: Mt Holly Matrix: Solid
Date Sampled: 07/05/2023 0930 % Solids: 1.92 07/11/2023 1543
Date Received:07/07/2023
Inorganic non-metals
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1
(% Solids) SM 2540G
1 07/11/2023 1543 CVR
79671
1 350.1
(Ammonia - N ) 350.1
10 07/10/2023 1229 CMM
79501
2
(Nitrate - N ) 353.2
1 07/22/2023 1358 CLL2
80779
2
(Nitrite - N ) 353.2
1 07/22/2023 1358 CLL2
80778
1
(Phosphorus) 365.1
10 07/14/2023 1531 DMA
07/10/2023 2319 79588
1
(Soil pH meas) 9045D
1 07/11/2023 1304 LMM2
79636
1 351.4
(TKN) 351.2
2 07/10/2023 1454 BMG2
07/09/2023 1855 79567
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
% Solids
SM 2540G
1.92
%
1
Ammonia - N (gas diffusion)
350.1
15000
520
270
mg/kg
1
Nitrate - N (soluble)
353.2
180
10
1.4
mg/kg
2
Nitrite - N (soluble)
353.2
7.5 J
10
1.4
mg/kg
2
Phosphorus
7723-14-0 365.1
13000
2600
520
mg/kg
1
Soil pH measured in water C)
10.2 ° C
9045D
7.4
su
1
TKN
351.2
72000
5200
2600
mg/kg
1
CVAA
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 7471 B
7471 B
1 07/14/2023 0313 KJEW
07/13/2023 2210 79760
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Mercury
7439-97-6 7471B
ND
4.1
0.99
mg/kg
1
ICP-AES
Run Prep Method
Analytical Method
Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
601OD
5 07/19/2023 1819 LAB
07/12/2023 1123 79687
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Aluminum
7429-90-5 601OD
14000
1700
650
mg/kg
1
Arsenic
7440-38-2 601OD
ND
65
22
mg/kg
1
Cadmium
7440-43-9 601OD
ND
22
5.4
mg/kg
1
Calcium
7440-70-2 601OD
10000 J
22000
2700
mg/kg
1
Chromium
7440-47-3 601OD
260
43
11
mg/kg
1
Copper
7440-50-8 601OD
560
43
19
mg/kg
1
Iron
7439-89-6 601OD
11000
430
200
mg/kg
1
Lead
7439-92-1 601OD
21 J
43
19
mg/kg
1
Magnesium
7439-95-4 601OD
3500 J
22000
2700
mg/kg
1
Manganese
7439-96-5 6010D
260
65
26
mg/kg
1
Molybdenum
7439-98-7 6010D
ND
170
43
mg/kg
1
Nickel
7440-02-0 6010D
ND
170
45
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 3 of 7

Client: Synagro Laboratory ID: YG07060-001
Description: Mt Holly Matrix: Solid
Date Sampled: 07/05/2023 0930 % Solids: 1.92 07/11/2023 1543
Date Received:07/07/2023
ICP-AES
Run Prep Method
Analytical Method Dilution Analysis Date Analyst
Prep Date
Batch
1 3050B
6010D 5 07/19/2023 1819 LAB
07/12/2023 1123 79687
CAS Analytical
Parameter
Number Method
Result Q
LOQ
DL
Units
Run
Potassium
7440-09-7 601OD
ND
22000
2700
mg/kg
1
Selenium
7782-49-2 601OD
ND
86
35
mg/kg
1
Sodium
7440-23-5 601OD
5300 J
22000
2700
mg/kg
1
Zinc
7440-66-6 601OD
690
220
54
mg/kg
1
LOQ - Limit of Quantitation B - Detected in the method blank E - Quantitation of compound exceeded the calibration range DL - Detection Limit Q - Surrogate failure
ND - Not detected at or above the DL N - Recovery is out of criteria P - The RPD between two GC columns exceeds 40% J - Estimated result < LOQ and > DL L - LCS/LCSD failure
H - Out of holding time W - Reported on wet weight basis S - MS/MSD failure
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 4 of 7

Chain of Custody
and
Miscellaneous Documents
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 5 of 7

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106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 6 of 7

PACE ANALYTICAL SERVICES, LLC
DC# Tide, ENV-FRM-WCOL-0286 v02_Samples Receipt Ciec6€rst ISRC)
Effective Date: OJ2022
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Q�Itraac R�636t} Pat c' Fin slytical Services, LLC Page 1 of 1
Pace Analytical Services, LLC (formerly Shealy Environmental Services, Inc.)
106 Vantage Point Drive West Columbia, SC 29172 [phone] Fax [phone] www.pacelabs.com
Page 7 of 7

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (5300 x 1.9200) = 100 = 101.76
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10000 x 1.9200) = 100 = 192
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3500 x 1.9200) = 100 = 67.2
Na meq = Na mg/I = Molec.Wgt.Na = 101.76 = 23 = 4.42435
Ca meq = Ca mg/I = Molec.Wgt.Ca = 192 = 20 = 9.6
Mg meq = Mg mg/I = Molec.Wgt.Mg = 67.2 = 12 = 5.6
Sample Date Report Range Ratio
7/5/2023 7/1 /2023 - 9/30/2023 1.6049
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 4.42435 = SgrRoot[0.5(9.6+5.6)] = 1.60488

Waypointo
ANALYTICAL
10/18/2023
Synagro Central LLC/ Technical
Mary Brewer
284 Boger Road
Mocksville, NC, 27028
Ref: Analytical Testing
Report Number: 23-277-0012
Project Description: Mt Holly
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Dear Mary Brewer:
Waypoint Analytical Virginia, Inc. received sample(s) on 10/4/2023 for the analyses presented in the following
report.
The above referenced project has been analyzed per your instructions. The analyses were performed in
accordance with the applicable analytical method. Sub -contracted testing is noted on the Sample Summary Table
if applicable.
The analytical data has been validated using standard quality control measures performed as required by the
analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all
parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA
(including 40 CFR 136 Method Update Rule May 2012) and NELAC unless otherwise indicated.
Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of
sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time
Refer to sample analysis time for confirmation of holding time compliance.
The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as -
received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to
the samples included in this report.
Please do not hesitate to contact me or client services if you have any questions or need additional information
Sincerely,
&;'-� ­AldA�
Brandi Watson
Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the
analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis.
Page 1 of 9

•
7621 Whitepine Road, Richmond, VA 23237
Waypoint
Main 804-743-9401 0 Fax [phone]
ANALYTICAL www.waypointanalytical.com
Sample Summary Table
Report Number: 23-277-0012
Client Project Description: Mt Holly
Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
63613
Mt Holly
Solids
10/03/2023
09:30
10/04/2023
SM-4500-NH3C
WP MTN
9045D
WP MTN
4500NO3F-2016
WP MTN
6010D
WP MTN
SW-7471B
WP MTN
SM-4500-NH3C-TKN
WP MTN
SM-2540G
WP MTN
WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN
Page 2 of 9

WayPANALYTICAL
46622
Synagro Central LLC/ Technical Project Mt Holly
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Number : 23-277-0012 REPORT OFANALYSIS
Report Date : 10/18/2023
Received : 10/04/2023
Brandi Watson
Lab No : 63613
Sample ID : Mt Holly
Matrix: Solids
Sampled: 10/3/2023 9:30
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Moisture
98.4
%
0.010
1
10/06/2316:00
CAH
SM-2540G
Phosphorus
13900
mg/Kg -
dry
313
1
10/07/23 02:22
BKN
6010D
Sulfur
12400
mg/Kg -
dry
625
1
10/07/23 02:22
BKN
6010D
Calcium
10300
mg/Kg -
dry
3130
1
10/07/23 02:22
BKN
6010D
Aluminum
11800
mg/Kg -
dry
313
1
10/07/23 02:22
TJS
6010D
Manganese
313
mg/Kg -
dry
31.3
1
10/07/23 02:22
BKN
6010D
Copper
441
mg/Kg -
dry
31.3
1
10/07/23 02:22
BKN
6010D
Zinc
663
mg/Kg -
dry
78.1
1
10/07/23 02:22
BKN
6010D
Organic N
81940
mg/Kg -
dry
15630
1
10/16/23 14:30
CALCULATION
Nickel
17.3
mg/Kg -
dry
15.6
1
10/11/23 14:17
TJS
6010D
Lead
<18.8
mg/Kg -
dry
18.8
1
10/07/23 02:22
BKN
6010D
Arsenic
<31.3
mg/Kg -
dry
31.3
1
10/07/23 02:22
BKN
6010D
Selenium
<31.3
mg/Kg -
dry
31.3
1
10/07/23 02:22
BKN
6010D
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Solids 1.58 % 0.010 1 10/06/23 16:00 CAH SM-2540G
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 3 of 9

WayPANALYTICAL
46622
Synagro Central LLC/ Technical Project Mt Holly
Mary Brewer
284 Boger Road Information
Mocksville , NC 27028
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Report Number : 23-277-0012 REPORT OFANALYSIS
Report Date : 10/18/2023
Received : 10/04/2023
Brandi Watson
Lab No : 63613
Sample ID : Mt Holly
Matrix: Solids
Sampled: 10/3/2023 9:30
Test
Results
Units
MQL
DF
Date / Time
By
Analytical
Analyzed
Method
Total Kjeldahl Nitrogen
93800
mg/Kg -
dry
15600
1
10/18/23 10:30
JPJ ;M-4500-NH3C-TKI`
Potassium
3080
mg/Kg -
dry
625
1
10/07/23 02:22
BKN
6010D
Magnesium
3170
mg/Kg -
dry
313
1
10/07/23 02:22
BKN
6010D
Sodium
7810
mg/Kg -
dry
1560
1
10/07/23 02:22
BKN
6010D
Iron
10800
mg/Kg -
dry
625
1
10/07/23 02:22
BKN
6010D
Ammonia Nitrogen
11800
mg/Kg -
dry
6250
1
10/16/23 14:30
JPJ
SM-4500-NH3C
Nitrate+Nitrite-N
<313
mg/Kg -
dry
313
1
10/11/23 15:37
CLP
4500NO3F-2016
Cadmium
<6.25
mg/Kg -
dry
6.25
1
10/07/23 02:22
BKN
6010D
Chromium
255
mg/Kg -
dry
15.6
1
10/07/23 02:22
BKN
6010D
Mercury
<11.4
mg/Kg -
dry
11.4
1
10/10/23 11:41
MRE
SW-7471B
pH
7.4
S.U.
1
10/09/2316:05
CNB
9045D
Total Volatile Solids
76.5
%
0.010
1
10/06/23 16:00
CAH
SM-2540G
Molybdenum
<15.6
mg/Kg -
dry
15.6
1
10/07/23 02:22
BKN
6010D
Qualifiers/ DF Dilution Factor
Definitions
MQL Method Quantitation Limit
Page 4 of 9

Waypointo
ANALYTICAL
Client: Synagro Central LLC/ Technical
Project: Mt Holly
Lab Report Number: 23-277-0012
Date: 10/18/2023
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
CASE NARRATIVE
Metals Analysis Method 601 OD
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Aluminum
QC Batch No: 1-709731/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Calcium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Cadmium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Copper
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Iron
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Potassium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Magnesium
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Page 5 of 9

Waypointo
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Analyte: Manganese
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Phosphorus
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Lead
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 63602 (61A-0146-Syncon-Replace Cooling Tower)
Analyte: Zinc
QC Batch No: 1-709473/1-709057
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Arsenic
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Calcium
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Cadmium
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Iron
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Potassium
QC Batch No: 1-710659/1-709902
Page 6 of 9

Waypoint".0
ANALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Magnesium
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Manganese
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Nickel
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Lead
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Sulfur
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Selenium
QC Batch No: 1-710201/1-709902
This analyte was analyzed at a dilution due to IEC interference/matrix interference.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Selenium
QC Batch No: 1-710659/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post
digestion spike was performed and passed quality control acceptance ranges. No matrix interference is
suspected.
Sample 81582 (WRC Topsoil (Oct))
Analyte: Zinc
QC Batch No: 1-710201/1-709902
The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test
was performed and passed quality control acceptance ranges. No matrix interference is suspected.
Page 7 of 9

WayPAoInt..
NALYTICAL
7621 Whitepine Road, Richmond, VA 23237
Main 804-743-9401 0 Fax [phone]
www.waypointanalytical.com
Shipment Receipt Form
Customer Number: 46622
Customer Name: Synagro Central LLC/ Technical
Report Number: 23-277-0012
Shipping Method
0 Fed Ex 0 US Postal 0 Lab
0 UPS 0 Client 0 Courier
0 Other:
Thermometer ID:
Shipping container/cooler uncompromised?
* Yes
0 No
Number of coolers/boxes received
Custody seals intact on shipping container/cooler?
0 Yes
0 No
Not Present
Custody seals intact on sample bottles?
0 Yes
0 No
Not Present
Chain of Custody (COC) present?
# Yes
0 No
COC agrees with sample label(s)?
# Yes
0 No
COC properly completed
# Yes
0 No
Samples in proper containers?
# Yes
0 No
Sample containers intact?
# Yes
0 No
Sufficient sample volume for indicated test(s)?
# Yes
0 No
All samples received within holding time?
# Yes
0 No
Cooler temperature in compliance?
# Yes
0 No
Cooler/Samples arrived at the laboratory on ice.
Samples were considered acceptable as cooling
process had begun.
# Yes
0 No
Water - Sample containers properly preserved
0 Yes
0 No
N/A
Water - VOA vials free of headspace
0 Yes
0 No
N/A
Trip Blanks received with VOAs
0 Yes
0 No
N/A
Soil VOA method 5035 — compliance criteria met
0 Yes
0 No
0 N/A
F_ High concentration container (48 hr)
F_ High concentration pre -weighed (methanol -14 d)
F_ Low concentration EnCore samplers (48 hr)
F_ Low conc pre -weighed vials (Sod Bis -14 d)
Special precautions or instructions included? 0 Yes * No
Comments:
Signature: IDavid Lennon Date & Time: 10/04/2023 12:55:27
Page 8 of 9

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Page 9 of 9

Sodium Absorption Ratio Calculation (SAR)
Product Code Product Name
1701-01-AEDLIQ-NC MOUNT HOLLY, NC WWTP AEROBICALLY
DIGESTED LIQUID
Na mg/I = (Na mg/kg x % Solids) = 100 = (7810 x 1.5800) = 100 = 123.398
Ca mg/I = (Ca mg/kg x % Solids) = 100 = (10300 x 1.5800) = 100 = 162.74
Mg mg/I = (mg mg/kg x % Solids) = 100 = (3170 x 1.5800) = 100 = 50.086
Na meq = Na mg/I = Molec.Wgt.Na = 123.398 = 23 = 5.36513
Ca meq = Ca mg/I = Molec.Wgt.Ca = 162.74 = 20 = 8.137
Mg meq = Mg mg/I = Molec.Wgt.Mg = 50.086 = 12 = 4.17383
Sample Date Report Range Ratio
10/3/2023 10/1 /2023 - 2.1625
12/31 /2023
SAR = Na meq = SgrRoot[0.5 x (Ca meq + Mg meq)] = 5.36513 = SgrRoot[0.5(8.137+4.17383)] = 2.16248

SECTION 3

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: MOUNT HOLLY, NC WO PERMIT #: W00001863 FIELD#: NC-LT-00046-0-0001- ACRES UTILIZED: 11.8
LANDOWNER: TONY JONES ANNUAL DRY TONS APPLIED: 9.43 SITE #: NC LT 00046 ACRES PERMITTED: 11.8
OPERATOR: TONY JONES PREDOMINANT SOIL SERIES: CECIL CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 209 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Date or
Month
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
Amount UOM
%
Solids Dry Tons/Ac
Residual
Source
Site
Cond.
Dry, Wet,
Moist
Precip
Past 24 Hrs.
Inches
Application
Method*
Volati-
lization
Rate**
Mineral-
ization
Rate***
TKN
mg/kg
Ammonia
Nitrogen
mg/kg
Nitrate
and Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1 Crop 2
8/9/2023
Aug-23
117,800.00 (G)
117,800.00 (G)
1.920 0.799
MHAEDL
MOIST
0-<1/2""
SUR
0.5
0.30
72,000.00
15,000.00
187.50
39.624
FSH
Total 0.799
Total
39.624 0.000
AS CD
CU
CR
PB
HG I
MO
NI
SE
ZN I
P
Lime Applied
Annual Ibs/acre Applied
0.035 0.009
0.895
0.416
0.034
0.002
0.069
0.072
0.056
1.103 1
20.781
Date Lbs/Ac
Cumulative Ibs/acre Applied 0.205 0.062 i 13.807 E 6.698 I 0.749 I 0.031 0.265 { 0.631 0.237 I 21.519
Permit PAN Limit (Ibs/acre) 1st Crop ( ( I I I [ 209
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
MHAEDL = MOUNT HOLLY, NC W WTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant pe 1 es for submi ' g false information, including the possibility of fines and imprisonment for knowing violations."
L' _ Q
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM"
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: MOUNT HOLLY, NC
Permit #: WQ0001863 Cation Exchange Capacity (non 503 only):
Operator: TONY JONES TONY JOKES Predominant Soil Series:
Owner:
Acres Used: 11.80 Acres Permitted: 11.80 Site #: Field #:
NC LT 00046
9.43
CECIL
NC LT 00046 0001
Source
MHAEDL
Sample or
Composite
Date
1
7/05/23
2
3
4
5
6
7
8
9
10
11
12
Solids
1.92
Arsenic
22.000
Cadmium
1 5.400
Copper
560
Chromium
260.00
Lead
21.00
Mercury
0.990
Molybdenum
43.00
Nickel
45.00
Selenium
35.00
Zinc
690
Total Phosphorus
13000
Source
MHAEDL
-
Total DT/Ac.
I App.Event
1
0.80
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.035
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.035
Cadmium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Copper
0.895
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.895
Chromium
0.416
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.416
Lead
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
Mercury
0.002
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.002
Molybdenum
0.069
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.069
Nickel
0.072
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.072
Selenium
0.056
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.056
Zinc
1.103
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.103
Total Phosphorus
20.781
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
20.781
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are si i ant penalties for ,foor'submitting false information, including the possibility of fines and impris
o
nment
for knowing violations".
Signature of Land App� Date DENR FORM MFLSF (12/2006)

FACILITY NAME: MOUNT HOLLY, NC
LANDOWNER: TONY JONES
OPERATOR: TONY JONES
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WO PERMIT #: W00001863 FIELD#: NC-LT-00046-0-0002-
ANNUAL DRY TONS APPLIED: 47.38 SITE #: NC LT 00046
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 209 CROP 2 NAME:
ACRES UTILIZED: 45.2
ACRES PERMITTED: 45.2
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
10/27/2023
142,600.00
(G)
1.580
0.208
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
12.802
FSH
10/29/2023
6,200.00
(G)
1.580
0.009
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
0.557
FSH
10/30/2023
179,800.00
(G)
1.580
0.262
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
16.142
FSH
10/31/2023
148,800.00
(G)
1.580
0.217
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
13.359
FSH
Oct-23
477,400.00
(G)
11/1/2023
93,000.00
(G)
1.580
0.136
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
8.349
FSH
11/2/2023
80,600.00
(G)
1.580
0.117
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
7.236
FSH
11/3/2023
68,200.00
(G)
1.580
0.099
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
6.123
FSH
Nov-23
241,800.00
(G)
Total
1.048
Total 64.568 0.000
AS
CD
C I
CR
PB
HG
MO NI
SE
ZN P Lime Applied
Annual Ibs/acre Applied
0.066
0.013
0.925
0.535
0.039
0.024
0.033 0.036
0.066
1.390 29.144 Date Lbs/Ac
Cumulative Ibs/acre Applied
0.245
0.048
12.063 5.326
0.560
0.048
0.197 0.526
0.215
19.723
Permit PAN Limit (Ibs/acre)
1st Crop
209
Federal C.P.L.R. (Ibs/acre)'*'*
36.6
34.8
1,339.0
267.9
15.0
375.0
89.0
2,500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significa nalties for submitting false information, including the possibility of fines and imprisonment for ]mowing violations."
SIGNATURE OF LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

Facility Name:
Permit #:
Operator:
Acres Used:
ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
MOUNT HOLLY, NC
W00001863 Cation Exchange Capacity (non 503 only):
TONY JONES TONY JONES Predominant Soil Series:
Owner:
45.20 Acres Permitted:
45.20 Site #:
NC LT 00046
Field #:
47.39
CECIL
NC LT 00046 0002
Source
MHAEDL
Sample or
Composite
Dale
1
10/03/23
2
3
4
5
6
7
8
9
10
11
12
Solids
1.58
Arsenic
31.300
Cadmium
6.250
Copper
441
Chromium
255.00
Lead
18.80
Mercury
11.400
Molybdenum
15.60
Nickel
17.30
Selenium
31.30
Zinc
663
Total Phosphorus
13900
e. -i w.- m-i Finid i -di- tr:eiodetud in the/acrnt.
Source
MHAEDL
Total DT/Ac.
/ App.Event
1
1.05
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
0.925
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.925
Chromium
0.535
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.535
Lead
0.039
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.039
Mercury
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Molybdenum
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Nickel
0.036
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.036
Selenium
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.066
Zinc
1.390
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.390
Total Phosphorus
29.144
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
29.144
" I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are sign ca penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations".
Signature f and Applier Date DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: MOUNT HOLLY, NC WO PERMIT #: W00001863 FIELD#: NC-LT-00046-0-0003- ACRES UTILIZED: 9.9
LAND OWNER: TONY JONES ANNUAL DRY TONS APPLIED: 13.90 SITE #: NC LT 00046 ACRES PERMITTED: 9.9
OPERATOR: TONY JONES PREDOMINANT SOIL SERIES: CECIL CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 209 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount I UOM
Solids Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mg/kg
mg/kg
Crop 1 Crop 2
Crop 1 Crop 2
8/2/2023
18,600.00 (G)
1.920 0.150
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
72,000.00
15,000.00
187.50
7.457
FSH
8/14/2023
155,000.00 (G)
1.920 1.254
MHAEDL
DRY
0-<112""
SUR
0.5
0.30
72,000.00
15,000.00
187.50
62.144
FSH
Aug-23
173,600.00 (G)
Total 1.404
Total
69.601 0.000
AS CD
CU
CR
PB
HG I
MO
NI
SE
ZN
P
Lime Applied
Annual lb./acre Applied
0.062 0.015
1.572
0.730
0.059
0.003
0.121
0.126
0.098
1.937
36.503
Date Lbs/Ac
Cumulative Ibs/acre Applied 0.252 0.074 15.742 7.601 0.839 0.036 0.341 0.751 0.301 24.213
Permit PAN Limit (Ibs/acre) 1st Crop 209
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0 267.9 15.0 375.0 89.0 2,500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant penalti L
bing false information, including the possibility of fines and imprisonment for knowing violations."
�
SIGNATURE F LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

Facility Name:
Permit #:
Operator:
Acres Used: 9.90
ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
MOUNT HOLLY, NC
W00001863 Cation Exchange Capacity (non 503 only):
TONY JONES TONY JONES Predominant Soil Series:
Owner:
Acres Permitted: 9.90 Site #: Field #:
NC LT 00046
13.90
CECIL
NC LT 00046 0003
Source
MHAEDL
Sample or
Composite
Date
1
7/05/23
2
3
4
5
6
7
8
9
10
11
12
Solids
1.92
Arsenic
22.000
Cadmium
1 5.400
Copper
560
Chromium
260.00
Lead
21.00
Mercury
0.990
Molybdenum
43.00
Nickel
45.00
Selenium
35.00
Zinc
690
Total Phosphorus
13000
Source
MHAEDL
Total DT/Ac.
/ App. Event
1
1.40
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.062
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.062
Cadmium
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Copper
1.572
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.572
Chromium
0.730
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.730
Lead
0.059
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.059
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molybdenum
0.121
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.121
Nickel
0.126
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.126
Selenium
0.098
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.098
Zinc
1.937
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.937
Total Phosphorus
36.503
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
36.503
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significan a hies for submitting false information, including the possibility of fines and imprisonment for knowing violations".
Signature of
d ApI5lier Date s�
DENR FORM MFLSF 12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: MOUNT HOLLY, NC WQ PERMIT #: WQ0001863 FIELD#: NC-LT-00046-0-0004- ACRES UTILIZED: 19.4
LAND OWNER: TONY JONES ANNUAL DRY TONS APPLIED: 8.58 SITE #: NC LT 00046 ACRES PERMITTED: 19.4
OPERATOR: TONY JONES PREDOMINANT SOIL SERIES: CECIL CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 209 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Gallons (G) Site
Name of Crop Type
or Cubic Yards (Y) Cond.
Precip
Volati- Mineral- Ammonia
Nitrate
PAN Applied Receiving Residual
Date or or Wet Tons (W) % Residual Dry, Wet,
Past 24 Hrs.
Application lization ization TKN Nitrogen
and Nitrite
(Ibs/acre) Application
Month Amount UOM Solids Dry Tons/Ac Source Moist
Inches
Method* Rate** Rate*** mg/kg mg/kg
mg/kg
Crop 1 Crop 2 Crop 1 Crop 2
11/1/2023 55,800.00 (G) 1.580 0.190 MHAEDL DRY
0-<1/2""
SUR 0.5 0.30 93,800.00 11,800.00
313.00
11.672
FSH
11/2/2023 74,400.00 (G) 1.580 0.253 MHAEDL DRY
0-<1/2""
SUR 0.5 0.30 93,800.00 11,800.00
313.00
15.562
FSH
Nov-23 1 130,200.00 (G)
Total 0.443
Total
27.234 0.000
AS CD CU CR
PB
HG MO NI SE ZN
P
Lime Applied
Annual Ibs/acre Applied 0.028 0.006 0.390 0.226
0.017
0.010 0.014 0.015 0.028 0.586
12.293
Date Lbs/Ac
Cumulative Ibs/acre Applied 0.189 0.035 9.831 4.352
0.455
0.030 0.159 0.442 0.148 16.471
Permit PAN Limit (Ibs/acre) 1st Crop
209
Federal C.P.L.R. (Ibs/acre)**** 36.6 34.8 1,339.0
267.9
1 15.0 375.0 89.0 2,500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant pe 1 es for submitting false information, including the possibility of fines and imprisonment for ]mowing violations."
SIGNATURE OF LAND APPLIER
DATE
NR = Not Reported or Not Required
***
Mineralization Rates: Compost-0.1, Anaerobically digested-0.2,
Aerobically
digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
****
C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
*****
See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024
DENR FORM FSF (1212006)

ANNUAL METALS FIELD LOADING SUMMARY FORM`
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: MOUNT HOLLY, NC
Permit #: W00001863 Cation Exchange Capacity (non 503 only):
Operator: TONY JONES TONY JONES Predominant Soil Series:
Owner:
Acres Used: 19.40 Acres Permitted: 19.40 Site #: Field #:
NC LT 00046
8,58
CECIL
NC LT 00046 0004
Source
MHAEDL
Sample or
Composite
Date
1
10/03/23
2
3
4
5
6
7
8
9
10
11
12
Solids
1.58
Arsenic
31.300
Cadmium
6.250
Copper
441
Chromium
255.00
Lead
18.80
Mercury
11.400
Molybdenum
15.60
Nickel
17.30
Selenium
31.30
Zinc
663
Total Phosphorus
13900
YP Source
`. MHAEDL V
Total DT/Ac.
/App.Event
1
0.44
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
0.390
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.390
Chromium
0.226
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.226
Lead
0.017
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.017
Mercury
0.010
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.010
Molybdenum
0.014
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.014
Nickel
0.015
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.015
Selenium
0.028
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.028
Zinc
0.586
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.586
Total Phosphorus
12.293
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
12.293
"I terrify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are significan jlfies for subnuuin�,false information, including the possibility of fines and imprisonment for knowing violations".
-���
PP
Signature of Land A lief Date ` DENR FORM MFLSF (12/2006)
9

ANNUAL LAND APPLICATION FIELD SUMMARY FORM Page: 1
FACILITY NAME: MOUNT HOLLY, INC WQ PERMIT #: W00001863 FIELD#: NC-LT-00046-0-0008- ACRES UTILIZED: 6.6
LAND OWNER: TONY JONES ANNUAL DRY TONS APPLIED: 9.93 SITE #: NC LT 00046 ACRES PERMITTED: 6.6
OPERATOR: TONY JONES PREDOMINANT SOIL SERIES: CECIL CATION EXCHANGE CAPACITY (NON-503):
CROP 1 NAME: FESCUE HAY (FSH) CROP 1 MAX. PAN: 209 CROP 2 NAME: CROP 2 MAX. PAN:
RESIDUAL SOURCE(S): * See list at bottom of report
Date or
Month
Gallons (G)
or Cubic Yards (Y)
or Wet Tons (W)
Amount UOM
%
Solids
Dry Tons/Ac
Residual
Source
Site
Cond.
Dry, Wet,
Moist
Precip
Past 24 Hrs.
Inches
Application
Method*
Volati-
lization
Rate**
Mineral-
ization
Rate***
TKN
mg/kg
Ammonia
Nitrogen
mg/kg
Nitrate
and Nitrite
mg/kg
PAN Applied
(Ibs/acre)
Crop 1 Crop 2
Name of Crop Type
Receiving Residual
Application
Crop 1 Crop 2
8/2/2023
80,600.00 (G)
1.920
0.978
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
72,000.00
15,000.00
187.50
48.472
FSH
8/3/2023
6,200.00 (G)
1.920
0.075
MHAEDL
DRY
0-<1/2""
SUR ?
0.5 1
0.30
72,000.00
15,000.00
187.50
3.729
FSH
8/9/2023
37,200.00 (G)
1.920
0.451
MHAEDL
MOIST
0-<1/2""
SUR
0.5
0.30
72,000.00
15,000.00
187.50
22.372
FSH
Aug-23 1
124,000.00 (G)
i
Total 1.504
Total
74.573 0.000
AS
P110
Lime AppliedLbs
Annual Ibs/acre Applied
pp
0 066 0 OD16
1 685
0.782
0 063
0 003
0.1029
O.N35
0 105
2.076
39
Date /Ac
Cumulative Ibs/acre ADDlled
0.249 0.073
15.324
7.404
0.819
0.036
0.344
0.744
0.302 1
23.450
Permit PAN Limit (Ibs/acre) 1st Crop 209
Federal C.P.L.R. (Ibs/acre)**** 36.6 1 34.8 1 1,339.0 267.9 15.0 1 375.0 1 89.0 1 2,500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
aware that there are significant p ties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
SIGNA3 URE Or LAND APPLIER DATE
NR = Not Reported or Not Required *** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation **** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0 ***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024 DENR FORM FSF (12/2006)

Facility Name
Permit #:
Operator:
Acres Used:
ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
MOUNT HOLLY, NC
W00001863 Cation Exchange Capacity (non 503 only):
TONY JONES TONY JONES Predominant Soil Series:
Owner:
6.60 Acres Permitted:
6.60
Site #:
NC LT 00046
9.93
CECIL
Field #: NC LT 00046 0008
------------�-- --
Source
•---- ------
MHAEDL
--- - ---- - - -..
..
_.
Sample or
Composite
Date
1
7/05123
2
3
4
5
6
7
8
9
10
11
12
Solids
1.92
Arsenic
22.000
Cadmium
5.400
Copper
560
Chromium
260.00
Lead
21.00
Mercury
0.990
Molybdenum
43.00
Nickel
45.00
Selenium
35.00
Zinc
690
Total Phosphorus
13000
Source
MHAEDL
Total DT/Ac.
/ App.Event
1
1.50
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.066
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.066
Cadmium
0.016
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.016
Copper
1.685
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.685
Chromium
0.782
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.782
Lead
0.063
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.063
Mercury
0.003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.003
Molybdenum
0.129
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.129
Nickel
0.135
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.135
Selenium
0.105
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.105
Zinc
2.076
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.076
Total Phosphorus
39.110
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
39.110
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are signif�n�ties forfor submitting information, including the possibility of fines and
diimprisonment for knowing violations".
Signature of Land Applier Date DENR FORM MFLSF (12/2006)

FACILITY NAME: MOUNT HOLLY, NC
LAND OWNER: DEAN & DALE CONNELL
OPERATOR: DEAN & DALE CONNELL
CROP 1 NAME: FESCUE HAY (FSH)
RESIDUAL SOURCE(S): * See list at bottom of report
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
WQ PERMIT #: W00001863 FIELD#: NC-MG-00037-0-0001-
ANNUAL DRY TONS APPLIED: 19.61 SITE #: NC MG 00037
PREDOMINANT SOIL SERIES: CECIL
CROP 1 MAX. PAN: 209 CROP 2 NAME:
ACRES UTILIZED: 18.3
ACRES PERMITTED: 18.3
CATION EXCHANGE CAPACITY (NON-503):
CROP 2 MAX. PAN:
Page: 1
Gallons (G)
Site
Name of Crop Type
or Cubic Yards (Y)
Cond.
Precip
Volati-
Mineral-
Ammonia
Nitrate
PAN Applied
Receiving Residual
Date or
or Wet Tons (W)
%
Residual
Dry, Wet,
Past 24 Hrs.
Application
lization
ization
TKN
Nitrogen
and Nitrite
(Ibs/acre)
Application
Month
Amount UOM
i
Solids
Dry Tons/Ac
Source
Moist
Inches
Method*
Rate**
Rate***
mg/kg
mglkg
mg/kg
Crop 1
Crop 2
Crop 1 Crop 2
11/3/2023
99,200.00(G)
1.580
0.357
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
21.997
FSH
11/6/2023
198,400.00 (G)
1.580
0.714
MHAEDL
DRY
0-<1/2""
SUR
0.5
0.30
93,800.00
11,800.00
313.00
43.994
FSH
Nov-23
297,600.00 (G)
Total 1.071
Total 65.991 0.000
AS CD C I CR
PB
HG MO NI
SE ZN P Lime Applied
Annual Ibslacre Applied 0.067 0.013 0.945 0.546
0.040
0.024 0.033 0.037
0.067 1.421 29.787 Date Lbs/Ac
Cumulative Ibs/acre Applied 0.375 0.072 14.760 6.948
0.745 0.054 0.266 0.681
0.317
23.249
Permit PAN itTs/acre) 1st Crop
209
Federal C P L.R. (Ibs/acre)**' 36.6 34.8 1,339.0
267.9 15.0 375.0 89.0 2,500.0
MHAEDL = MOUNT HOLLY, NC WWTP AEROBICALLY DIGESTED LIQUID
"I certify, under penalty of law, that this document was prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel property gathered and evaluated the information submitted. I am
aware that there are significant penaltie�fbmittin�information, including the possibility
of fines and imprisonment for knowing violations."
SIGNATURE OF LAND APPLIER
DATE
NR = Not Reported or Not Required
*** Mineralization Rates: Compost-0.1, Anaerobically digested-0.2, Aerobically digested-0.3, Raw Sludge-0.4
* Application Method: SUR - Surface, INJ - Injection, SURIN - Incorporation
**** C.P.L.R.: Cumulative Pollutant Loading Rate
** Volatilization Rate: Surface 0.5, Injection/Incorporation 1.0
***** See Site pH & Lime Application Records Section of Report
Printed: 1/24/2024
DENR FORM FSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Total Dry Tons Applied (Annual):
Facility Name: MOUNT HOLLY, NC
Permit #: W00001863 Cation Exchange Capacity (non 503 only):
Operator: DEAN & DALE CONNELL DEAN & DALE CONNELL Predominant Soil Series:
Owner:
Acres Used: 18.30 Acres Permitted: 18.30 Site #: Field #:
NC MG 00037
19.61
CECIL
NC MG 00037 0001
Source
MHAEDL
Sample or
Composite
Date
1
10/03/23
2
3
4
5
6
7
8
9
10
11
12
Solids
1.58
Arsenic
31.300
Cadmium
1 6.250
Copper
441
Chromium
255.00
Lead
18.80
Mercury
11.400
Molybdenum
15.60
Nickel
17.30
Selenium
31.30
Zinc
663
Total Phosphorus
13900
Source
MHAEDL
Total DT/Ac.
/App. Event
1
107
2
3
4
5
6
7
8
9
10
11
12
Totals
Arsenic
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Cadmium
0.013
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.013
Copper
0.945
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.945
Chromium
0.546
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.546
Lead
0.040
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.040
Mercury
0.024
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.024
Molybdenum
0.033
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.033
Nickel
0.037
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.037
Selenium
0.067
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.067
Zinc
1.421
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.421
Total Phosphorus
29.787
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
29.787
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that
there are signific s for submitting false information, including the possibility of fines and imprisonment for knowing violations".
07; -z-,;-
Signature of Land Applier Date DENR FORM MFLSF (12/2006)

SECTION 4

SUMM111
ENVIRONMENTAL TECHN❑LOMZ3. INC
Arraly0ca1 Laboralorfas
January 24, 2023
Alex Fox
Synagro
284 Boger Rd.
Mocksville, NC 27028
TEL:
FAX:
RE: Mt Holly
Dear Alex Fox:
Summit Environmental Technologies, Inc.
3310 Win St.
Cuyahoga Falls, Ohio 44223
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
Order No.: 23010831
Summit Environmental Technologies, Inc. received 1 sample(s) on 1/13/2023 for the
analyses presented in the following report.
There were no problems with the analytical events associated with this report unless noted
in the Case Narrative.
Quality control data is within laboratory defined or method specified acceptance limits
except where noted.
If you have any questions regarding these tests results, please feel free to call the
laboratory.
Sincerely,
Jennifer Woolf
Project Manager
3310 Win St.
Cuyahoga Falls, Ohio 44223
Arkansas 88-0735, California 2943, Colorado, Connecticut PH-0108, Florida NELAC E87688, Idaho 01100923, Illinois 200061, Indiana C-OH-13,
ISO/IEC 17025:2017 119125 L22-544, Kansas E-10347, Kentucky (Underground Storage Tank) 3, Kentucky 90146, Maryland 339, Michigan 9988,
Minnesota 1780279, Nevada 011009232020-1, New Hampshire 2996, New Jersey 011006, New York 11777, North Carolina 39705 and 631, North Dakota
R-201, Ohio DW, Ohio VAP CL0052, Oklahoma 2019-155, Oregon OH2O0001, Pennsylvania 68-01335, Rhode Island LA000317, South Carolina
92016001, Texas T104704466-19-16, Utah 011009232020-12, Virginia VELAP 10381, West Virginia 9957C
Page 1 of 39

MM' Y Summit Environmental Technologies, Inc. Case Narrative
SU3310 Win St.
ENVIRONMENTAL TEC„NQLOG4r;S,INC. Cuyahoga Falls, Ohio44223 wo#: 23010831
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com Date: 1/24/2023
CLIENT: Synagro
Project: Mt Holly
WorkOrder Narrative:
23010831: This report in its entirety consists of the following documents: Cover Letter, Case Narrative,
Analytical Results, QC Summary Report, Applicable Accreditation Information, Chain -of -Custody,
Cooler Receipt Form, and other applicable forms as necessary. All documents contain the Summit
Environmental Technologies, Inc., Work Order Number assigned to this report.
Summit Environmental Technologies, Inc., holds the accreditations/certifications listed at the bottom of
the cover letter that may or may not pertain to this report. Please refer to the "Accreditation Program
Analytes Report" for accredited analytes list.
The information contained in this analytical report is the sole property of Summit Environmental
Technologies, Inc. and that of the customer. It cannot be reproduced in any form without the consent of
Summit Environmental Technologies, Inc. or the customer for which this report was issued. The results
contained in this report are only representative of the samples received. Conditions can vary at different
times and at different sampling conditions. Summit Environmental Technologies, Inc. is not responsible
for use or interpretation of the data included herein.
All results for Solid Samples are reported on an "as received" or "wet weight" basis unless indicated as
"dry weight" using the "-dry" designation on the reporting units.
This report is believed to meet all of the requirements of the accrediting agency, where applicable. Any
comments or problems with the analytical events associated with this report are noted below.
Analytical Sequence Sample Notes:
23010831-001A TCLP-VOC-MSTR 8260D: CCV ane LCS-R156775 exhibited high recoveries for
Vinyl chloride, Carbon tetrachloride, and Trichloroethene. Sample is ND for these analytes. Possible
low bias for 1, 1 -Dichloroethene due to low recovery in CCV. Compound demostrates adequate
instrument sensitivity in RLC. Sample is ND for 1,1-Dichloroethene.
23010831-001A TCLP-SVOC_8270E: Possible low bias for Pyridine due to low recovery in the CCV.
Compound demonstrates adequate instrument sensitivity in RLC.
Analytical Sequence QC Notes:
MBLK VOC-MSTR_NPW(8260): Possible low bias for 1,1-Dichloroethene due to low recovery in
CCV. Compound demostrates adequate instrument sensitivity in RLC.
Original
Page 2 of 39

SUMMIY Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TEC„NQLOG4r;S,INC. Cuyahoga Falls, Ohio44223
Arralyi9cal Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Mt Holly
Case Narrative
wo#: 23010831
Date: 1/24/2023
LCS VOC-MSTR_NPW(8260): LCS-R156775 exhibited high recoveries for for Vinyl chloride, Carbon
tetrachloride, and Trichloroethene. Associated samples are ND for these analytes. Possible high bias for
Vinyl chloride due to high recovery in CCV. Possible low bias for 1, 1 -Dichloroethene due to low
recovery in CCV. Compound demostrates adequate instrument sensitivity in RLC.
MB/LCS-62313 SVOC-BNA_TCLP(8270): Possible low bias for Pyridine due to low recovery in the
CCV. RLC demonstrates control for this analyte.
Original
Page 3 of 39

MM' Summit Environmental Technologies, In Qualifiers and Acronyms
SU3310 Win S
EkiwllOMM@NTALTECHN❑LOG{r,23.INC Cuyahoga Falls, Ohio442� WO#: 23010831
Arraly0cal Laboralorlas TEL: [phone] FAX.- (330) 253-44E
Wehsite: httn:11www.settek.co Date: 1/24/2023
These commonly used Qualifiers and Acronyms may or may not be present in this report.
Qualifiers
U The compound was analyzed for but was not detected.
J The reported value is greater than the Method Detection Limit but less than the Reporting Limit.
H The hold time for sample preparation and/or analysis was exceeded.
D The result is reported from a dilution.
E The result exceeded the linear range of the calibration or is estimated due to interference.
MC The result is below the Minimum Compound Limit.
The result exceeds the Regulatory Limit or Maximum Contamination Limit.
in Manual integration was used to determine the area response.
d Manual integration in which peak was deleted
N The result is presumptive based on a Mass Spectral library search assuming a 1:1 response.
P The second column confirmation exceeded 25% difference.
C The result has been confirmed by GC/MS.
X The result was not confirmed when GUMS Analysis was performed.
B/MB+ The analyte was detected in the associated blank.
G The ICB or CCB contained reportable amounts of analyte.
QC-/+ The CCV recovery failed low (-) or high (+).
R/QDR The RPD was outside of accepted recovery limits.
QL-/+ The LCS or LCSD recovery failed low (-) or high (+).
QLR The LCS/LCSD RPD was outside of accepted recovery limits.
QM-/+ The MS or MSD recovery failed low (-) or high (+).
QMR The MS/MSD RPD was outside of accepted recovery limits.
QV-/+ The ICV recovery failed low (-) or high (+).
S The spike result was outside of accepted recovery limits.
Z Deviation; A deviation from the method was performed; Please refer to the Case Narrative for
additional information
Acronyms
ND
Not Detected
RL
Reporting Limit
QC
Quality Control
MDL
Method Detection Limit
MB
Method Blank
LOD
Level of Detection
LCS
Laboratory Control Sample
LOQ
Level of Quantitation
LCSD
Laboratory Control Sample Duplicate
PQL
Practical Quantitation Limit
QCS
Quality Control Sample
CRQL
Contract Required Quantitation Limit
DUP
Duplicate
PL
Permit Limit
MS
Matrix Spike
RegLvl
Regulatory Limit
MSD
Matrix Spike Duplicate
MCL
Maximum Contamination Limit
RPD
Relative Percent Different
MinCL
Minimum Compound Limit
ICV
Initial Calibration Verification
RA
Reanalysis
ICB
Initial Calibration Blank
RE
Reextraction
CCV
Continuing Calibration Verification
TIC
Tentatively Identified Compound
CCB
Continuing Calibration Blank
RT
Retention Time
PLC
Reporting Limit Check
CF
Calibration Factor
DF
Dilution Factor
RF
Response Factor
This list of Qualifiers and Acronyms reflects the most commonly utilized Qualifiers and Acronyms for reporting.
Please refer to the Analytical Notes in the Case Narrative for any Qualifiers or Acronyms that do not appear in this
list or for additional information regarding the use of these Qualifiers on reported data.
Original
Page 4 of 39

�� 1 � Summit Environmental Technologies, Inc.
SU3310 Win St.
ENVIROMMEWAL YECHNO ijULES. JNG, Cuyahoga Falls, Ohio 44223
Analytical Laboralorlas TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
CLIENT: Synagro
Project: Mt Holly
Lab SampleID Client Sample ID
23010831-001 Mt Holly
Tag No Date Collected
1/12/2023 3:00:00 AM
Workorder
Sample Summary
WO#: 23010831
24 Jan-23
Date Received Matrix
1/13/2023 10:20:00 AM Solid
Page 5 of 39

SUMMIT
Summit Environmental Technologies, Inc.
3310 Win St.
DATES R PORT
ENVIRONMENTALTECHN❑L0G1ES,11+1C
Cuyahoga Falls, Ohio44223
WO#: 23010831
ArWyft cal Laboraloriag
TEL: [phone] FAX.- [phone]
Wehsite: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Mt Holly
Sample ID
Client Sample ID Collection Date Matrix Test Name Leachate Date
Prep Date Analysis Date
23010831-OOIA Mt Holly 1/12/2023 3:00:00 AM Solid Ignitability of Solids (SW-846: 1030)
1/18/2023 7:17:11 PM
pH (SW9045D)
1/20/2023 4:11:32 PM
Reactive Cyanide (9014/7.3.3.2)-Solid
1/18/2023 2:21:00 PM
Reactive Sulfide (9034)/7.3.4.2
1/18/2023 2:21:00 PM
TCLP Herbicides by EPA 8321B
1/18/2023 5:29:00 PM
TCLP Mercury Analysis (SW1311/7471/17/2023 4:15:00 PM
1/18/2023 2:30:00 PM 1/19/2023 10:47:00 AM
TCLP Metals Analysis (SW1311/6010:1/17/2023 4:15:00 PM
1/18/2023 2:00:00 PM 1/19/2023 1:47:00 PM
TCLP Pesticides Analysis (SW1311/8(1/17/2023 4:15:00 PM
1/18/2023 10:31:44 AM 1/19/2023 1:30:00 AM
TCLP Pesticides Analysis (SW1311/8(1/17/2023 4:15:00 PM
1/18/2023 10:31:44 AM 1/19/2023 1:30:00 AM
TCLP Semi-Volatiles Analysis 1/17/2023 4:15:00 PM
1/19/2023 10:40:00 AM 1/20/2023 7:21:00 PM
(SW1311/8270)
TCLP Volatiles Analysis
1/19/2023 2:44:00 PM
Original
Page 6 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNQLOGIE$,IRC Cuyahoga Falls, Ohio44223
Arralyt9cal Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 23010831
Date Reported: 1/24/2023
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/12/2023 3:00:00 AM
Lab ID: 23010831-OOIA
Project: Mt Holly
Client Sample ID Mt Holly
Analyses Result RL Qual Units DF Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
TCLP MERCURY ANALYSIS (SW1311/7470)
TCLP Mercury
ND 0.00200 mg/L
SW7470A SW7470A Analyst: ICA
1 1/19/2023 10:47:00 AM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW6010
SW301OA Analyst: RJE
TCLP METALS ANALYSIS (SW1311/6010)
TCLP Arsenic(As)
ND
0.500
mg/L
1
1/19/2023 1:47:00 PM
TCLP Barium(Ba)
ND
5.00
mg/L
1
1/19/2023 1:47:00 PM
TCLP Cadmium(Cd)
ND
0.100
mg/L
1
1/19/2023 1:47:00 PM
TCLP Chromium(Cr)
ND
0.200
mg/L
1
1/19/2023 1:47:00 PM
TCLP Lead(Pb)
ND
0.500
mg/L
1
1/19/2023 1:47:00 PM
TCLP Selenium(Se)
ND
0.0500
mg/L
1
1/19/2023 1:47:00 PM
TCLP Silver(Ag)
ND
0.500
mg/L
1
1/19/2023 1:47:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8270
SW351OC Analyst: JAP
TCLP SEMI-VOLATILES ANALYSIS (SW1311/8270)
1,4-Dichlorobenzene
ND
0.100
mg/L
1
1/20/2023 7:21:00 PM
2,4,5-Trichlorophenol
ND
0.250
mg/L
1
1/20/2023 7:21:00 PM
2,4,6-Trichlorophenol
ND
0.250
mg/L
1
1/20/2023 7:21:00 PM
2,4-Dinitrotoluene
ND
0.0500
mg/L
1
1/20/2023 7:21:00 PM
Cresols, Total
ND
5.00
mg/L
1
1/20/2023 7:21:00 PM
Hexachloro-1,3-butadiene
ND
0.0200
mg/L
1
1/20/2023 7:21:00 PM
Hexachlorobenzene
ND
0.0500
mg/L
1
1/20/2023 7:21:00 PM
Hexachloroethane
ND
0.100
mg/L
1
1/20/2023 7:21:00 PM
Nitrobenzene
ND
0.100
mg/L
1
1/20/2023 7:21:00 PM
Pentachlorophenol
ND
0.250
mg/L
1
1/20/2023 7:21:00 PM
Pyridine
ND
0.250
QC- mg/L
1
1/20/2023 7:21:00 PM
Surr: 2-Fluorophenol
61.3
10 - 157
%Rec
1
1/20/2023 7:21:00 PM
Surr: Phenol-d6
71.5
10 - 169
%Rec
1
1/20/2023 7:21:00 PM
Surr: Nitrobenzene-d5
61.6
32.1 - 130
%Rec
1
1/20/2023 7:21:00 PM
Surr: 2,4,6-Tribromophenol
93.0
45.4 - 166
%Rec
1
1/20/2023 7:21:00 PM
Surr: 2-Fluorobiphenyl
67.0
35.7 - 130
%Rec
1
1/20/2023 7:21:00 PM
Surr: p-Terphenyl-d14
85.8
70 - 145
%Rec
1
1/20/2023 7:21:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or
analysis exceeded
M Manual Integration
used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
OG1
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection
Limit
Page 7 of 39

SUMMIT Summit Environmental Technologies, Inc.
3310 Win St.
ENVIRONMENTAL TECHNQLOGIE$,IRC Cuyahoga Falls, Ohio44223
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone]
Website: http://�i,-"-m,.settek.coin
Analytical Report
(base report)
WO#: 23010831
Date Reported: 1/24/2023
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/12/2023 3:00:00 AM
Lab ID: 23010831-OOIA
Project: Mt Holly
Client Sample ID Mt Holly
Analyses
Result
RL
Qual Units
DF
Date Analyzed
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8081
SW351OC Analyst: PGP
TCLP PESTICIDES ANALYSIS
(SW1311/8081)
Chlordane, total
ND
0.00250
mg/L
1
1/19/2023 1:30:00 AM
Toxaphene
ND
0.00500
mg/L
1
1/19/2023 1:30:00 AM
Endrin
ND
0.000500
mg/L
1
1/19/2023 1:30:00 AM
gamma-BHC
ND
0.000500
mg/L
1
1/19/2023 1:30:00 AM
Heptachlor
ND
0.000500
mg/L
1
1/19/2023 1:30:00 AM
Heptachlor epoxide
ND
0.000500
mg/L
1
1/19/2023 1:30:00 AM
Methoxychlor
ND
0.000500
mg/L
1
1/19/2023 1:30:00 AM
Surr: TCMX
69.3
10 - 119
%Rec
1
1/19/2023 1:30:00 AM
Surr: DCB
69.5
10 - 119
%Rec
1
1/19/2023 1:30:00 AM
TCLP HERBICIDES BY EPA 8321B
SW8321
Analyst: SRA
2,4-D ND
0.500
mg/L
50
1/18/2023 5:29:00 PM
2,4,5-TP ND
0.500
mg/L
50
1/18/2023 5:29:00 PM
Surr: 2,4-Dichlorophenylacetic aci 82.4
70 - 130
%Rec
50
1/18/2023 5:29:00 PM
TCLP METALS, VOC, BNA, PEST, HERB -SOLID
SW8260
Analyst: EMB
TCLP VOLATILES ANALYSIS
1,1-Dichloroethene ND
0.100
QC- mg/L
20
1/19/2023 2:44:00 PM
1,2-Dichloroethane ND
0.100
mg/L
20
1/19/2023 2:44:00 PM
MEK ND
2.00
mg/L
20
1/19/2023 2:44:00 PM
Benzene ND
0.100
mg/L
20
1/19/2023 2:44:00 PM
Carbon tetrachloride ND
0.100
QL+ mg/L
20
1/19/2023 2:44:00 PM
Chlorobenzene ND
1.00
mg/L
20
1/19/2023 2:44:00 PM
Chloroform ND
0.100
mg/L
20
1/19/2023 2:44:00 PM
Tetrachloroethene ND
0.100
mg/L
20
1/19/2023 2:44:00 PM
Trichloroethene ND
0.100
QL+ mg/L
20
1/19/2023 2:44:00 PM
Vinyl chloride ND
0.0400QC+QL+mg/L
20
1/19/2023 2:44:00 PM
Surr: 4-Bromofluorobenzene 98.9
70 - 130
%Rec
20
1/19/2023 2:44:00 PM
Surr: Di brom ofl uorom ethane 95.8
70 - 130
%Rec
20
1/19/2023 2:44:00 PM
Surr: Toluene-d8 105
70 - 130
%Rec
20
1/19/2023 2:44:00 PM
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H Holding times for preparation or analysis exceeded
M Manual Integration used to determine area response
MC Value is below Minimum Compound Limit.
N Tentatively identified
compounds
ND Not Detected
OG1
P Second column confirmation exceeds
PL Permit Limit
Original
R RPD outside accepted recovery limits
RL Reporting Detection Limit
Page 8 of 39

MMIT
Summit Environmental Technologies, Inc. Analytical Report
SU3310 Win St.
ENVIRONMENTAL TECHNOLOGIE_3, IRC Cuyahoga Falls, Ohio 44223 (base report)
Arrafyt9caf Laboralorfas TEL: [phone] FAX. [phone] WO#: 23010831
Website: http://www.settek.com Date Reported: 1/24/2023
CLIENT: Synagro Tag Number:
Matrix: SOLID Collection Date: 1/12/2023 3:00:00 AM
Lab ID: 23010831-OOIA
Project: Mt Holly
Client Sample ID Mt Holly
Analyses Result
RL Qual Units
DF
Date Analyzed
RCI
SW9014
Analyst: MS
REACTIVE CYANIDE (9014/7.3.3.2)-SOLID
Cyanide, Reactive ND
0.481 mg/Kg
1
1/18/2023 2:21:00 PM
IGNITABILITY OF SOLIDS (SW-846: 1030)
SW1030
Analyst: SMZ
Ignitability Non-flammable
mm/sec
1
1/18/2023 7:17:11 PM
RCI
SW9045D
Analyst: SMZ
PH (SW9045D)
pH 6.9
s.u.@20.8C
1
1/20/20234:11:32 PM
RCI
SW9034
Analyst: MS
REACTIVE SULFIDE (9034)/7.3.4.2
Sulfide, Reactive ND
25.0 mg/Kg
1
1/18/2023 2:21:00 PM
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or analysis exceeded
M
Manual Integration used to determine area response
MC
Value is below Minimum Compound Limit.
N
Tentatively identified compounds
ND
Not Detected
OG1
P
Second column confirmation exceeds
PL
Permit Limit Original
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 9 of 39

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
ENwIROMMEWALYECHNOL.OG{r,S,INC
Cuyahoga Falls, Ohio44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
23010831
Wehsite: http://www.settek.com
24 Jan-23
Client: Synagro
State: NW
Project: Mt Holly
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
23010831-OOIA Solid
Ignitability of Solids (SW-846: 1030)
Ignitability
A
Solid
pH (SW9045D)
Hydrogen Ion (pH)
A
Solid
Reactive Cyanide (9014/7.3.3.2)-Solid
Cyanide, Reactive
U
Solid
Reactive Sulfide (9034)/7.3.4.2
Sulfide, Reactive
U
Solid
TCLP Herbicides by EPA 8321B
2,4,5-TP
A
Solid
TCLP Herbicides by EPA 8321B
2,4-D
A
Solid
TCLP Mercury Analysis (SW1311/7470)
Mercury
A
Solid
TCLP Metals Analysis (SW1311/6010)
Arsenic
A
Solid
TCLP Metals Analysis (SW1311/6010)
Barium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Cadmium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Chromium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Lead
A
Solid
TCLP Metals Analysis (SW1311/6010)
Selenium
A
Solid
TCLP Metals Analysis (SW1311/6010)
Silver
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Chlordane, total
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Endrin
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
gamma-BHC
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Heptachlor epoxide
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Methoxychlor
A
Solid
TCLP Pesticides Analysis (SW1311/8081)
Toxaphene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
1,4-Dichlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,5-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4,6-Trichlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
2,4-Dinitrotoluene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Cresols, Total
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachlorobutadiene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Hexachloroethane
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Nitrobenzene
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pentachlorophenol
A
Solid
TCLP Semi-Volatiles Analysis (SW1311/8270)
Pyridine
A
Version #2
Page 10 of 39

Summit Environmental Technologies, Inc.
Accreditation
Program
SUMMIEF
fr3310 Win St.
Analv n tes Report
EMOROMMEWAL YECHNOL.OG{r,S,
INC Cuyahoga Falls, Ohio 44223
J
Y
Arraly0cal Laboralorlas
TEL: [phone] FAX.- [phone]
Wo#:
23010831
Wehsite: http://www.settek.com
24 Jan-23
Client: Synagro
State: NW
Project: Mt Holly
Program Name: NC_WW_SCM
Sample ID Matrix
Test Name
Analyte
Status
23010831-OOIA Solid
TCLP Volatiles Analysis
1,1-Dichloroethene
A
Solid
TCLP Volatiles Analysis
1,2-Dichloroethane
A
Solid
TCLP Volatiles Analysis
2-Butanone
A
Solid
TCLP Volatiles Analysis
Benzene
A
Solid
TCLP Volatiles Analysis
Carbon tetrachloride
A
Solid
TCLP Volatiles Analysis
Chlorobenzene
A
Solid
TCLP Volatiles Analysis
Chloroform
A
Solid
TCLP Volatiles Analysis
Tetrachloroethene
A
Solid
TCLP Volatiles Analysis
Trichloroethene
A
Solid
TCLP Volatiles Analysis
Vinyl chloride
A
Version #2
Page 11 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://nnn.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: 62279
Sample ID: MB-62279
SampType: MBLK
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/18/2023
RunNo: 156731
Client ID: PBS
Batch ID: 62279
TestNo: SW8081 SW3510C
Analysis Date: 1/18/2023
SegNo: 4172749
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, total
ND
0.00250
Toxaphene
ND
0.00500
Endrin
ND
0.000500
gamma-BHC
ND
0.000500
Heptachlor
ND
0.000500
Heptachlor epoxide
ND
0.000500
Methoxychlor
ND
0.000500
Surr: TCMX
11.7
Surr: DCB
11.6
20.00 58.4 10 119
20.00 57.8 10 119
Sample ID: LCS-62279
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/18/2023
RunNo: 156731
Client ID: LCSS
Batch ID: 62279
TestNo: SW8081 SW3510C
Analysis Date: 1/18/2023
SegNo: 4172750
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Chlordane, tot
Toxaphene
Endrin
gamma-BHC
Heptachlor
Heptachlor epo
Methoxychlor
Surr: TCMX
Qualifiers:
al 0.0183 0.0
ND 0.0
0.0108 0.00
0.00848 0.00
0.0103 0.00
xide 0.00917 0.00
0.0114 0.00
12.0
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0250 0 0 70
0500 0 0 70
0500 0.0100 0 108 10
0500 0.0100 0 84.8 10
0500 0.0100 0 103 10
0500 0.0100 0 91.7 10
0500 0.0100 0 114 10
20.00 60.1 10
E Value above quantitation range
M Manual Integration used to determine area response
OG 1
R RPD outside accepted recovery limits
130
130
130
130
130
130
178
130
H Holding times for preparation or anal
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 12 of 39
B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
0250 0 0 70
0500 0 0 70
0500 0.0100 0 108 10
0500 0.0100 0 84.8 10
0500 0.0100 0 103 10
0500 0.0100 0 91.7 10
0500 0.0100 0 114 10
20.00 60.1 10
E Value above quantitation range
M Manual Integration used to determine area response
OG 1
R RPD outside accepted recovery limits
130
130
130
130
130
130
178
130
H Holding times for preparation or anal
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 12 of 39
130
130
130
130
130
130
178
130
H Holding times for preparation or anal
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original
Page 12 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: 62279
Sample ID: LCS-62279
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date: 1/18/2023
RunNo: 156731
Client ID: LCSS
Batch ID: 62279
TestNo: SW8081 SW3510C
Analysis Date: 1/18/2023
SegNo: 4172750
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Surr: DCB
8.64
20.00
43.2 10 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 13 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: 62288
Sample ID: MB-62288
SampType: MBLK
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 1/18/2023
RunNo: 156724
Client ID: PBS
Batch ID: 62288
TestNo: SW6010 SW3010A
Analysis Date: 1/19/2023
SegNo: 4173032
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
ND
0.100
TCLP Barium(Ba)
ND
5.00
TCLP Cadmium(Cd)
ND
0.100
TCLP Chromium(Cr)
ND
0.200
TCLP Lead(Pb)
ND
0.100
TCLP Selenium(Se)
ND
0.100
TCLP Silver(Ag)
ND
0.100
Sample ID: LCS-62288
SampType: LCS
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 1/18/2023
RunNo: 156724
Client ID: LCSS
Batch ID: 62288
TestNo: SW6010 SW3010A
Analysis Date: 1/19/2023
SegNo: 4173033
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.14
0.100
2.000
0
107
80
120
TCLP Barium(Ba)
ND
5.00
2.000
0
103
80
120
TCLP Cadmium(Cd)
2.01
0.100
2.000
0
100
80
120
TCLP Chromium(Cr)
2.03
0.200
2.000
0
101
80
120
TCLP Lead(Pb)
2.04
0.100
2.000
0
102
80
120
TCLP Selenium(Se)
1.97
0.100
2.000
0
98.6
80
120
TCLP Silver(Ag)
2.11
0.100
2.000
0
106
80
120
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 14 of 39

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 23010831
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: 62288
Sample ID: 23010844-001AMS
SampType: MS
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 1/18/2023
RunNo: 156724
Client ID: Batch=
Batch ID: 62288
TestNo: SW6010 SW3010A
Analysis Date: 1/19/2023
SegNo: 4174124
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
2.06
0.500
2.000
0
103
70
130
TCLP Barium(Ba)
ND
5.00
2.000
0.1455
100
70
130
TCLP Cadmium(Cd)
1.78
0.100
2.000
0
89.2
70
130
TCLP Chromium(Cr)
1.81
0.200
2.000
0.002100
90.3
70
130
TCLP Lead(Pb)
1.81
0.500
2.000
0
90.4
70
130
TCLP Selenium(Se)
1.98
0.0500
2.000
0
99.1
70
130
TCLP Silver(Ag)
2.06
0.500
2.000
0
103
70
130
Sample ID: 23010844-001AMSD
SampType: MSD
TestCode: MTL-TCLP-7( Units: mg/L
Prep Date: 1/18/2023
RunNo: 156724
Client ID: Batch=
Batch ID: 62288
TestNo: SW6010 SW3010A
Analysis Date: 1/19/2023
SegNo: 4174125
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
TCLP Arsenic(As)
1.96
0.500
2.000
0
98.2
70
130
2.058
4.72
20
TCLP Barium(Ba)
ND
5.00
2.000
0.1455
95.0
70
130
0
0
20
TCLP Cadmium(Cd)
1.71
0.100
2.000
0
85.5
70
130
1.784
4.22
20
TCLP Chromium(Cr)
1.72
0.200
2.000
0.002100
85.8
70
130
1.807
5.08
20
TCLP Lead(Pb)
1.73
0.500
2.000
0
86.6
70
130
1.809
4.34
20
TCLP Selenium(Se)
1.90
0.0500
2.000
0
94.9
70
130
1.982
4.35
20
TCLP Silver(Ag)
1.96
0.500
2.000
0
98.2
70
130
2.056
4.63
20
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 15 of 39

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 23010831
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Mt Holly
BatchID: 62305
TCLP Mercury ND 0.00200
TCLP Mercury 0.00407 0.00200 0.00400 0 102 80 120
TCLP Mercury 0.00413 0.00200 0.00400 0.0000230 103 75 125
Sample ID: 23010844-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/18/2023
RunNo: 156722
Client ID: Batch=
Batch ID: 62305
TestNo: SW7470A SW7470A
Analysis Date: 1/19/2023
SegNo: 4172607
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
TCLP Mercury
0.00419 0.00200
0.00400 0.0000230 104 75
125
0.00413 1.44 20
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OG1
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 16 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Mt Holly BatchID: 62305
WO#: 23010831
24-Jan-23
Sample ID: 23010844-001AMSD
SampType: MSD
TestCode: HG_TCLP(74 Units: PPM
Prep Date: 1/18/2023
RunNo: 156722
Dient ID: Batch=
Batch ID: 62305
TestNo: SW7470A SW7470A
Analysis Date: 1/19/2023
SegNo: 4172607
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 17 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Mt Holly BatchID: 62313
WO#: 23010831
24-Jan-23
Sample ID: MB-62313
SampType: MBLK
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/19/2023
RunNo: 156871
client ID: PBS
Batch ID: 62313
TestNo: SW8270 SW3510C
Analysis Date: 1/20/2023
SegNo: 4175949
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
ND
0.0250
2,4,5-Trichlorophenol
ND
0.0250
2,4,6-Trichlorophenol
ND
0.0250
2,4-Dinitrotoluene
ND
0.0250
o-Cresol
ND
0.250
Cresols, Total
ND
0.0500
Hexachloro-1,3-butadiene
ND
0.0250
Hexachlorobenzene
ND
0.0250
Hexachloroethane
ND
0.0250
Nitrobenzene
ND
0.0250
Pentachlorophenol
ND
0.0250
Pyridine
ND
0.0250
Surr: 2-Fluorophenol
0.735
Surr: Phenol-d6
0.858
Surr: Nitrobenzene-d5
0.727
Surr: 2,4,6-Tribromophenol
1.03
Surr: 2-Fluorobiphenyl
0.800
Surr: p-Terphenyl-d14
1.02
1.000
73.5
10
135
1.000
85.8
10
161
1.000
72.7
16.8
150
1.000
103
32.5
179
1.000
80.0
34
133
1.000
102
60.8
163
QC -
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 18 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Mt Holly BatchID: 62313
WO#: 23010831
24-Jan-23
Sample ID: LCS-62313
SampType: LCS
TestCode: SVOC-BNA_T Units: mg/L
Prep Date: 1/19/2023
RunNo: 156871
client ID: LCSS
Batch ID: 62313
TestNo: SW8270 SW3510C
Analysis Date: 1/20/2023
SegNo: 4175950
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.463
0.0250
0.8000
0
57.8
35
130
2,4,5-Trichlorophenol
0.858
0.0250
0.8000
0
107
44
144
2,4,6-Trichlorophenol
0.873
0.0250
0.8000
0
109
45
141
2,4-Dinitrotoluene
0.845
0.0250
0.8000
0
106
56
136
o-Cresol
0.729
0.250
0.8000
0
91.1
36
134
Cresols, Total
1.48
0.0500
1.600
0
92.5
36
135
Hexachloro-1,3-butadiene
0.547
0.0250
0.8000
0
68.4
30
130
Hexachlorobenzene
0.825
0.0250
0.8000
0
103
58
130
Hexachloroethane
0.448
0.0250
0.8000
0
56.0
28
130
Nitrobenzene
0.698
0.0250
0.8000
0
87.3
39
133
Pentachlorophenol
0.849
0.0250
0.8000
0
106
33
151
Pyridine
0.191
0.0250
0.8000
0
23.9
10
130
Surr: 2-Fluorophenol
0.742
1.000
74.2
10
135
Surr: Phenol-d6
0.844
1.000
84.4
10
161
Surr: Nitrobenzene-d5
0.739
1.000
73.9
16.8
150
Surr:2,4,6-Tribromophenol
1.20
1.000
120
32.5
179
Surr:2-Fluorobiphenyl
0.834
1.000
83.4
34
133
Surr: p-Terphenyl-d14
0.963
1.000
96.3
60.8
163
QC -
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 19 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Mt Holly BatchID: 62313
WO#: 23010831
24-Jan-23
Sample ID: 23010844-001AMS
SampType: MS
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/19/2023
RunNo: 156871
client ID: BatchQC
Batch ID: 62313
TestNo: SW8270 SW3510C
Analysis Date: 1/20/2023
SegNo: 4175972
analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.475
0.100
0.8000
0
59.4
15.2
124
2,4,5-Trichlorophenol
0.802
0.250
0.8000
0
100
30.6
152
2,4,6-Trichlorophenol
0.815
0.250
0.8000
0
102
27.6
150
2,4-Dinitrotoluene
0.760
0.0500
0.8000
0
95.0
58
141
o-Cresol
0.654
0.250
0.8000
0
81.8
26.9
132
Cresols, Total
ND
5.00
1.600
0
83.4
27.6
132
Hexachloro-1,3-butadiene
0.533
0.0200
0.8000
0
66.6
10
156
Hexachlorobenzene
0.742
0.0500
0.8000
0
92.8
54.3
142
Hexachloroethane
0.465
0.100
0.8000
0
58.1
1.92
131
Nitrobenzene
0.653
0.100
0.8000
0
81.6
21
135
Pentachlorophenol
0.762
0.250
0.8000
0
95.2
47.4
134
Pyridine
0.422
0.250
0.8000
0
52.7
10
130
Surr:2-Fluorophenol
0.726
1.000
72.6
9.77
146
Surr: Phenol-d6
0.758
1.000
75.8
20.7
130
Surr: Nitrobenzene-d5
0.646
1.000
64.6
13.9
156
Surr:2,4,6-Tribromophenol
1.08
1.000
108
27.3
183
Surr:2-Fluorobiphenyl
0.709
1.000
70.9
21.4
153
Surr: p-Terphenyl-d14
0.883
1.000
88.3
54.8
154
QC -
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 20 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
Client: Synagro
Project: Mt Holly BatchID: 62313
WO#: 23010831
24-Jan-23
Sample ID: 23010844-001AMSD
SampType: MSD
TestCode: TCLP-SVOC_ Units: mg/L
Prep Date: 1/19/2023
RunNo: 156871
Dient ID: Batch=
Batch ID: 62313
TestNo: SW8270 SW3510C
Analysis Date: 1/20/2023
SegNo: 4175973
4nalyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1,4-Dichlorobenzene
0.470
0.100
0.8000
0
58.8
15.2
124
0.4750
1.06
30
2,4,5-Trichlorophenol
0.857
0.250
0.8000
0
107
30.6
152
0.8018
6.70
30
2,4,6-Trichlorophenol
0.872
0.250
0.8000
0
109
27.6
150
0.8152
6.71
30
2,4-Dinitrotoluene
0.827
0.0500
0.8000
0
103
58
141
0.7602
8.39
30
o-Cresol
0.686
0.250
0.8000
0
85.8
26.9
132
0.6544
4.74
30
Cresols, Total
ND
5.00
1.600
0
88.5
27.6
132
0
0
30
Hexachloro-1,3-butadiene
0.540
0.0200
0.8000
0
67.5
10
156
0.5330
1.27
30
Hexachlorobenzene
0.832
0.0500
0.8000
0
104
54.3
142
0.7424
11.4
30
Hexachloroethane
0.460
0.100
0.8000
0
57.5
1.92
131
0.4650
1.08
30
Nitrobenzene
0.668
0.100
0.8000
0
83.5
21
135
0.6528
2.27
30
Pentachlorophenol
0.846
0.250
0.8000
0
106
47.4
134
0.7618
10.5
30
Pyridine
0.416
0.250
0.8000
0
52.0
10
130
0.4218
1.43
30
Surr:2-Fluorophenol
0.705
1.000
70.5
9.77
146
0
Surr: Phenol-d6
0.806
1.000
80.6
20.7
130
0
Surr: Nitrobenzene-d5
0.693
1.000
69.3
13.9
156
0
Surr:2,4,6-Tribromophenol
1.16
1.000
116
27.3
183
0
Surr:2-Fluorobiphenyl
0.794
1.000
79.4
21.4
153
0
Surr: p-Terphenyl-d14
0.950
1.000
95.0
54.8
154
0
QC -
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 21 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156695
Sample ID: LCS-R156695
SampType: LCS
TestCode: Ignitability_S Units: mm/sec
Prep Date:
RunNo: 156695
Client ID: LCSS
Batch ID: R156695
TestNo: SW1030
Analysis Date: 1/18/2023
SegNo: 4171894
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Ignitability
7.69
7.240 0 106 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 22 of 39

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 23010831
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Mt Holly
BatchID: R156754
Cyanide, Reactive ND 0.495
Cyanide, Reactive 11.9 0.495 12.50 0 95.4 85 115
Cyanide, Reactive 0.646 0.495 0.5000 0 129 50 150
Sample ID: 23010716-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 156754
Client ID: Batch=
Batch ID: R156754
TestNo: SW9014
Analysis Date: 1/18/2023
SegNo: 4173205
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
8.58 0.490
10.00 0 85.8 75
125
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OG1
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 23 of 39

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 23010831
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156754
Sample ID: 23010716-001AMS
SampType: MS
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 156754
Client ID: Batch=
Batch ID: R156754
TestNo: SW9014
Analysis Date: 1/18/2023
SegNo: 4173205
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sample ID: 23010716-011AMSD
SampType: MSD
TestCode: Cyanide,Rea Units: mg/Kg
Prep Date:
RunNo: 156754
Client ID: Batch=
Batch ID: R156754
TestNo: SW9014
Analysis Date: 1/18/2023
SegNo: 4173206
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Cyanide, Reactive
8.94 0.490 10.00 0 89.4 75 125
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
OG 1
R RPD outside accepted recovery limits
Page 24 of 39
H Holding times for preparation or anal
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 23010831
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156756
Sample ID: 23010716-011AMS
SampType: MS
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 156756
Client ID: Batch=
Batch ID: R156756
TestNo: SW9034
Analysis Date: 1/18/2023
SegNo: 4173277
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 1600 25.0 1780 0 89.9 80 120
Sample ID: 23010716-011AMSD
SampType: MSD
TestCode: Sulfide,React Units: mg/Kg
Prep Date:
RunNo: 156756
Client ID: Batch=
Batch ID: R156756
TestNo: SW9034
Analysis Date: 1/18/2023
SegNo: 4173278
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive 1640 25.0 1780 0 92.1 80 120 1600 2.47 30
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
OG1 P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 25 of 39

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223 WO#: 23010831
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156756
Sample ID: MB-R156756
SampType: MBLK
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 156756
Client ID: PBW
Batch ID: R156756
TestNo: SW9034
Analysis Date: 1/18/2023
SegNo: 4173265
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive ND 25.0
Sample ID: LCS-R156756
SampType: LCS
TestCode: Sulfide,React Units: mg/L
Prep Date:
RunNo: 156756
Client ID: LCSW
Batch ID: R156756
TestNo: SW9034
Analysis Date: 1/18/2023
SegNo: 4173266
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
Sulfide, Reactive
1660 25.0 1780 0 93.3 85 115
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range H Holding times for preparation or anal
M Manual Integration used to determine area response MC Value is below Minimum Compound
OG1 P Second column confirmation exceeds
R RPD outside accepted recovery limits RL Reporting Detection Limit
Original
Page 26 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156775
Sample ID: 23010834-001AMS
SampType: MS
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: Batch=
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173523
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1, 1 -Dichloroethene
0.599
0.100
0.400
0
150
13.6
202
1,2-Dichloroethane
0.495
0.100
0.400
0
124
55.7
138
MEK
2.08
2.00
2.00
0
104
65.3
118
Benzene
0.559
0.100
0.400
0
140
49.2
145
Carbon tetrachloride
0.486
0.100
0.400
0
121
26.7
156
Chlorobenzene
ND
1.00
0.400
0
126
33.7
159
Chloroform
0.499
0.100
0.400
0
125
48.5
145
Tetrachloroethene
0.469
0.100
0.400
0
117
19.2
191
Trichloroethene
0.471
0.100
0.400
0
118
38.4
167
Vinyl chloride
0.620
0.0400
0.400
0
155
27.3
161
Surr:4-Bromofluorobenzene
986
1000
98.6
91.7
109
Surr: Dibromofluoromethane
957
1000
95.7
75.5
118
Surr: Toluene-d8
1050
1000
105
94.1
105
QC-
Q L+
Q L+
QL+QC+
S
Sample ID: 23010834-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: Batch=
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173524
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
M-Dichloroethene
0.537 0.100
0.400 0 134
13.6
202
0.599 10.9
25 QC-
1,2-Dichloroethane
0.469 0.100
0.400 0 117
55.7
138
0.495 5.48
25
MEK
2.21 2.00
2.00 0 110
65.3
118
2.08 5.84
25
Benzene
0.499 0.100
0.400 0 125
49.2
145
0.559 11.4
25
Qualifiers: B
Analyte detected in the associated Method Blank
E
Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M
Manual Integration used to determine area
response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OG1
P
Second column confirmation exceeds
PL
Permit Limit
R
RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 27 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156775
Sample ID: 23010834-001AMSD
SampType: MSD
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: Batch=
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173524
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.434
0.100
0.400
0
109
26.7
156
0.486
11.2
25 QL+
Chlorobenzene
ND
1.00
0.400
0
109
33.7
159
0
0
25
Chloroform
0.454
0.100
0.400
0
114
48.5
145
0.499
9.36
25
Tetrachloroethene
0.405
0.100
0.400
0
101
19.2
191
0.469
14.7
25
Trichloroethene
0.423
0.100
0.400
0
106
38.4
167
0.471
10.6
25 QL+
Vinyl chloride
0.583
0.0400
0.400
0
146
27.3
161
0.620
6.28
25 QL+QC+
Surr:4-Bromofluorobenzene
981
1000
98.1
91.7
109
0
25
Surr: Dibromofluoromethane
990
1000
99.0
75.5
118
0
25
Surr: Toluene-d8
1030
1000
103
94.1
105
0
25
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 28 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156775
Sample ID: MBLK
SampType: MBLK
TestCode: TCLP-VOC-M Units: mg/L
Prep Date:
RunNo: 156775
Client ID: PBS
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173517
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
1, 1 -Dichloroethene
ND
0.100 QC-
1,2-Dichloroethane
ND
0.100
MEK
ND
2.00
Benzene
ND
0.100
Carbon tetrachloride
ND
0.100
Chlorobenzene
ND
1.00
Chloroform
ND
0.100
Tetrachloroethene
ND
0.100
Trichloroethene
ND
0.100
Vinyl chloride
ND
0.0400 QC+
Surr:4-Bromofluorobenzene
1000
1000 100 70 130
Surr: Dibromofluoromethane
980
1000 98.0 70 130
Surr: Toluene-d8
1020
1000 102 70 130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 29 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156775
Sample ID: MBLK
SampType: MBLK
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 156775
Client ID: PBW
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4173516
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
1, 1 -Dichloroethene
ND
0.00500 QC-
1,2-Dichloroethane
ND
0.00500
MEK
ND
0.0250
Benzene
ND
0.00500
Carbon tetrachloride
ND
0.00500
Chlorobenzene
ND
0.00500
Chloroform
ND
0.00500
Tetrachloroethene
ND
0.00500
Trichloroethene
ND
0.00500
Vinyl chloride
ND
0.00200 QC+
Surr:4-Bromofluorobenzene
49.6
50.00 99.3 70 130
Surr: Dibromofluoromethane
49.6
50.00 99.2 70 130
Surr: Toluene-d8
50.2
50.00 100 70 130
Sample ID: LCS
SampType: LCS
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 156775
Client ID: LCSW
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4174204
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit HighLimit RPD Ref Val
%RPD RPDLimit Qual
M-Dichloroethene
0.0286
0.00500
0.0200 0 143
49
161
QC-
1,2-Dichloroethane
0.0271
0.00500
0.0200 0 135
48
151
MEK
0.0970
0.0250
0.100 0 97.0
10
190
Benzene
0.0275
0.00500
0.0200 0 138
34
169
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OG1
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 30 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156775
Sample ID: LCS
SampType: LCS
TestCode: VOC-MSTR_ Units: mg/L
Prep Date:
RunNo: 156775
Client ID: LCSW
Batch ID: R156775
TestNo: SW8260
Analysis Date: 1/19/2023
SegNo: 4174204
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Carbon tetrachloride
0.0290
0.00500
0.0200
0
145
76
134 S
Chlorobenzene
0.0264
0.00500
0.0200
0
132
54
144
Chloroform
0.0258
0.00500
0.0200
0
129
70
130
Tetrachloroethene
0.0259
0.00500
0.0200
0
130
66
134
Trichloroethene
0.0285
0.00500
0.0200
0
142
70
136 S
Vinyl chloride
0.0339
0.00200
0.0200
0
170
49
136 SQC+
Surr:4-Bromofluorobenzene
49.7
50.00
99.4
70
130
Surr: Dibromofluoromethane
51.0
50.00
102
70
130
Surr: Toluene-d8
48.2
50.00
96.5
70
130
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 31 of 39

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMEWAL I ECHNO LQgir,-3, INC
Cuyahoga Falls, Ohio 44223
WO#: 23010831
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Mt Holly
BatchID: R156776
2,4-D ND 0.0100
2,4,5-TP ND 0.0100
Surr: 2,4-Dichlorophenylacetic acid 0.732 1.000 73.2 70 130
2,4-D
0.0120
0.0100 0.01000
0 120
50
150
2,4,5-TP
ND
0.0100 0.01000
0 0
50
150 S
Surr: 2,4-Dichlorophenylacetic acid
0.00870
0.01000
87.0
70
130
Sample ID: LCS TCLP 0.3 ppm
SampType: LCS
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 156776
Client ID: LCSS
Batch ID: R156776
TestNo: SW8321
Analysis Date: 1/18/2023
SegNo: 4173531
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D
0.274 0.0100
0.3000 0 91.3 60.5
141
2,4,5-TP
0.267 0.0100
0.3000 0 88.9 68.3
144
Surr: 2,4-Dichlorophenylacetic acid 0.267
0.3000 89.1 70
130
Qualifiers: B
Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J
Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND
Not Detected
OG1
P
Second column confirmation exceeds
PL
Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 32 of 39

MM' T Summit Environmental Technologies, Inc. QC SUMMARY REPORT
SU3310 Win St.
ENVIRONMEWAL I ECHNO LQgir,-3, INC Cuyahoga Falls, Ohio 44223 WO#: 23010831
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://www.settek.com 24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156776
Sample ID:
LCSD TCLP 0.3 ppm SampType: LCSD
TestCode: TCLP-SVOC- Units: mg/L
Prep Date:
RunNo: 156776
Client ID:
LCSS02 Batch ID: R156776
TestNo: SW8321
Analysis Date: 1/18/2023
SegNo: 4173533
Analyte
Result
PQL SPK value SPK Ref Val
%REC Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
2,4-D 0.292 0.0100 0.3000 0 97.5 60.5 141 0.2740 6.53 30
2,4,5-TP 0.292 0.0100 0.3000 0 97.5 68.3 144 0.2666 9.23 30
Surr: 2,4-Dichlorophenylacetic acid 0.293 0.3000 97.7 70 130 0 0
Qualifiers: B Analyte detected in the associated Method Blank
J Analyte detected below quantitation limits
ND Not Detected
PL Permit Limit
E Value above quantitation range
M Manual Integration used to determine area response
OG 1
R RPD outside accepted recovery limits
Page 33 of 39
H Holding times for preparation or anal
MC Value is below Minimum Compound
P Second column confirmation exceeds
RL Reporting Detection Limit
Original

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 23010831
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Mt Holly
BatchID: R156838
pH 7.0 7.0 0 100 90 110
pH 12.5 0 0 0 0 12.5 0.2 10
pH 7.0 7.0 0 100 90 110
Sample ID: 23011173-001ADUP
SampType: DUP
TestCode: pH_S(9045D) Units: s.u.@20.5C
Prep Date:
RunNo: 156838
Client ID: Batch=
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175312
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 6.5 0 0 0 0 6.4 0.6 10
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 34 of 39

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 23010831
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Mt Holly
BatchID: R156838
pH 7.0 7.0 0 100 90 110
pH 7.6 0 0 0 0 7.6 0 10
Sample ID: LCS-R156838
SampType: LCS
TestCode: pH_S(9045D) Units: s.u.@20.5C
Prep Date:
RunNo: 156838
Client ID: LCSS
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175326
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 7.0
7.0 0 101 90
110
Qualifiers: B Analyte detected in the associated Method Blank
E Value above quantitation range
H
Holding times for preparation or anal
J Analyte detected below quantitation limits
M Manual Integration used to determine area response
MC
Value is below Minimum Compound
Original
ND Not Detected
OG1
P
Second column confirmation exceeds
PL Permit Limit
R RPD outside accepted recovery limits
RL
Reporting Detection Limit
Page 35 of 39

SUMM' T
Summit Environmental Technologies, Inc.
3310 Win St.
QC SUMMARY REPORT
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,.
Cuyahoga Falls, Ohio 44223
WO#: 23010831
Arrafyt�cal iaboralorfas
TEL: [phone] FAX.- [phone]
Website: http://www.settek.com
24-Jan-23
Client:
Synagro
Project:
Mt Holly
BatchID: R156838
pH 7.0 7.0 0 100 98.6 101.4
pH 6.9 6.9 0.4 5 H
pH 7.0 7.0 0 100 98.6 101.4
Sample ID: 23010912-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@19.7C
Prep Date:
RunNo: 156838
Client ID: Batch=
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175285
Analyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
pH 6.3 6.3 0.5 5 H
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 36 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMf_WAL I ECHNG LQgir,-3, INC,. Cuyahoga Falls, Ohio 44223
Arrafyt�cal iaboralorfas TEL: [phone] FAX.- [phone]
Website: http://mmm.settek.com
QC SUMMARY REPORT
WO#: 23010831
24-Jan-23
Client: Synagro
Project: Mt Holly BatchID: R156838
Sample ID: 23010912-001ADUP
SampType: DUP
TestCode: pH_NPW(450 Units: s.u.@19.7C
Prep Date:
RunNo: 156838
Dient ID: Batch=
Batch ID: R156838
TestNo: SW9045D
Analysis Date: 1/20/2023
SegNo: 4175285
4nalyte
Result
PQL SPK value SPK Ref Val %REC
Lowl-imit Highl-imit RPD Ref Val
%RPD RPDLimit Qual
Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or anal
J Analyte detected below quantitation limits M Manual Integration used to determine area response MC Value is below Minimum Compound
ND Not Detected OG1 P Second column confirmation exceeds Original
PL Permit Limit R RPD outside accepted recovery limits RL Reporting Detection Limit
Page 37 of 39

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Page 38 of 39

Summit Environmental Technologies, Inc.
SUMMIT 3310 Win St.
ENVIRONMENTAL TECHN❑L4Ga1�S.IfiC Cuyahoga Falls, Ohio44223 Sample Log -In Check List
Arrafocaf Laboralorias TEL: [phone] FAX.- [phone]
Website: http://`h,,",m,.settek.coin
Client Name: SYN-NC-27028 Work Order Number: 23010831 RcptNo: 1
Logged by: Anthony W. Britton 1/13/2023 10:20:00 AM'
Completed By: Anthony W. Britton 1/13/2023 5:27:54 PM
Reviewed By: Jennifer Woolf 1/16/2023 2:58:03 PM
Chain of Custody
1. Is Chain of Custody complete? Yes ❑d No ❑ Not Present ❑
2. How was the sample delivered? UPS
Lop In
3. Coolers are present? Yes ❑d No ❑ NA ❑
4. Shipping container/cooler in good condition?
Yes
d❑
No
❑
Custody seals intact on shipping container/cooler?
Yes
❑
No
❑
Not Present V
No. Seal Date:
Signed By:
5. Was an attempt made to cool the samples?
Yes
❑d
No
❑
NA ❑
6. Were all samples received at a temperature of >0° C to 6.0°C
Yes
❑d
No
❑
NA ❑
7. Sample(s) in proper container(s)?
Yes
❑d
No
❑
8. Sufficient sample volume for indicated test(s)?
Yes
❑d
No
❑
9. Are samples (except VOA and ONG) properly preserved?
Yes
❑d
No
❑
10. Was preservative added to bottles?
Yes
❑
No
❑d
NA ❑
11. Is the headspace in the VOA vials less than 1/4 inch or 6 mm?
Yes
❑
No
❑ No VOA Vials ❑�
12. Were any sample containers received broken?
Yes
❑
No
❑d
13. Does paperwork match bottle labels?
Yes
No
❑
(Note discrepancies on chain of custody)
14. Are matrices correctly identified on Chain of Custody?
Yes
❑
No
❑d
15. Is it clear what analyses were requested?
Yes
❑d
No
❑
16. Were all holding times able to be met?
Yes
No
❑
(If no, notify customer for authorization.)
Special Handling (if applicable)
17. Was client notified of all discrepancies with this order?
Yes
❑
No
❑ NA V
Person Notified: Date:
By Whom: Via: ❑ eMail ❑ Phone ❑ Fax ❑ In Person
Regarding:
Client Instructions:
18. Additional remarks:
Cooler Information
Cooler No
Temp °C
Condition
I Seal Intact
Seal No
Seal Date
Signed By
1
15.0
Goodl
Not Present
Page 39 of 39

SECTION 5

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: W 0001863
WWTP Name: Mt Holly WWTP NPDES Number: NC0021156
Monitoring Period: From O1/01/2023 To 03/31/2023
Pathogen Reduction (40 CFR 503.32115A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I IA (tinicltemp) Alt. 2B (Alk Treatment) Alt, 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Therinophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
If nnnlir9hip to attPrnufiva nnrfnrmnti rr loce A nr !lace R1 nn.n..lnty fi. f Il ..,:. ... :a A -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Minimum Geo. Mean Maximum Units
Excee-
dences
of
Analysis
Type
Technique
Fecal
2x10 to the 611'
MPN
Coliform
power per gram
MPN/g
of total solids
CFU
218,182
257,263
303,030
CFU/g
0
Quarterly
Grab
SM9222D
1000 MAN per gram of
Col/G/
total solids (dry weight)
Salmonella
3 MPN per grams total
bacteria (in
solids (dry weight)
lieu of fecal
cohform
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt. 2
(40-day bench)
Option/Alt. 3 Option/Alt. 4
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
( l4-Day Aerobic)
Option/Alt. 6
(Alk Stabilization)
Option/Alt, 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement in40 CFR 503.33/15A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been inade under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Keith Lynch Division Manager Wastewater
Preparer N e a Titl {typ or prime Land Applier Name and Title (if applicable) (type or print)
Sign tune of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Alex Fox
Client: Synagro
284 Boger Road
k
Page 1
Report Date: 1/19/2023
Mac sville, NC 27028 Date Sample Rcvd: 1/12/2023
Meritech Work Order # 011223105 Sample: Mt Holly 1 Grab
Parameters
Results Analysis Date
1/12/23
Reporting Limit Method
% Total Solids
1.71 %
1/13/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
239,766 CFU/g dry wt
1/12/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 011223106 Sample: Mt Holly 2 Grab 1/12/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.59 % 1/13/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 270,440 CFU/g dry wt 1/12/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 011223107 Sample: Mt Holly 3 Grab
1/12/23
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.65 %
1/13/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
218,182 CFU/g drywt
1/12/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 011223108 Sample: Mt Holly 4 Grab 1/12/23
Parameters Results Analysis_Date Reporting Limit Method
% Total Solids 1.76 % 1/13/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 267,045 CFU/g dry wt 1/12/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 011223109 Sample: Mt Holly 5 Grab 1/12/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.65 % 1/13/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 303,030 CFU/g dry wt 1/12/23 130 CFU/g dry wt SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Page 2
Report Date: 1/19/2023
MOCkSVllle, NC 2702$ Date Sample Rcvd: 1/12/2023
Meritech Work Order # 011223110 Sample: Mt Holly 6 Grab
Parameters
Results Analysis Date
1/12/23
Resorting Limit Method
% Total Solids
1.66 %
1/13/23
0-100 %
SM 2540B
Fecal Coliform (Sludge)
253,012 CFU/g dry wt
1/12/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 011223111 Sample: Mt Holly 7 Grab 1/12/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.67 % 1/13/23 0-100 % SM 2540B
Fecal Coliform (Sludge) 257,485 CFU/g drywt 1/12/23 130 CFU/g dry wt SM 9222D
I hereby certify that I have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 01/12/2023
Reported: 02/20/2023
For: Mt Holly
Comments:
4 STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230112-31-01 30 Day Benchscale Mt Holly
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
i• •
EPA625-R-92/0 01/12/2023 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Condition of Receipt
Sample Number 230112-31-01 Temp on Arrival: 3.0
Parameter Schedule:
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

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STATESVILLE
ANALYTICAL
Analytical Results
Synagro For: Mt Holly
284 Boger Rd
Mocksville, NC 27028
Entered: 1/12/23
Reported: 2/20/23
Sample ID: 220112-31-01
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids Volatile Solids % Volatile Solids
1 0.42 0.35 0.8333
2 0.38 0.30 0.7895
Week 3 0.42 0.32 0.7619
.41 0.31 0.7561
Week 5 0.44 0.34 0.7727
Week 6 0.40 0.30 0.7500
Volatile Solids Reduction: 0.8333 - 0.7500 X 100 = 39.9 %
0.8333 - (0.8333 X 0.7500)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.i# 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID # 220112-31-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.42
0.34
2
0.43
0.36
3
0.40
0.35
Average:
0.42
0.35
0.8333
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.40
0.32
2
0.41
0.32
3
0.32
0.26
Average:
0.38
0.30
0.7895
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.42
0.31
2
0.42
0.32
3
0.42
0.32
Average:
0.42
0.32
0.7619
Ciai Dl chi 14M
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.41
0.31
2
0.41
0.31
3
0.41
0.31
Average:
0.41
0.31
0.7561
WF.F.K 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.40
0.30
2
0.49
0.39
3
0.42
0.32
Average:
0.44
0.34
0.7727
WFF.K 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.40
0.30
2
0.40
0.30
3
0.41
0.31
Average:
0.40
0.30
0.7500
Van Kleeck Reduction: 0.8333 - 0.7500 X 100 = 39.9 %
0.8333 - (0.8333 X 0.7500)
Final Result: 39.9%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

%VS R
(older, more conservative method)
%VS in 1 0.8333 - Enter in
%VS out 1 0.75001 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 39.99
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in
%VSR= 10.00
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: _WQ_OOO 1863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 04/01/2023 To 06/30/2023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt, PA (time/temp) Alt. 2/13 (Alk Treatment) Alt, 3/C (Prior Testing)
Alt. 4/1) (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
if annlirahle fn alfarnnfivn nnrrnrn.o.l fi-l— A — U1 ..IoFo Etie v rr ..,o _ a .
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
deuces
Analysis
Fecal
2x 10 to the 61h
MPN
Coliform
power per gram
MPN/g
of total solids
CFU
92,262
133,504
159,091
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
Coliform}
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. 1
(VS reduction)
Option/Alt, 2
(40-day bench)
Option/Alt. 3 Option/Alt, 4
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
(14-Day Aerobic)
Option/Alt, 6
(Alk Stabilization)
Option/Alt. 7 Option/Alt. 8
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503,32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
reduction requirement m 40 CFR 503.33/I 5A NCAC 02T.1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Keith Lynch Division Manager Wastewater
Pre2ef
me an Title (ty !e or pri t)
1iv c�
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville NC 2702$
Page 1
Report Date: 4/13/2023
' Date Sample Rcvd: 4/4/2023
Meritech Work Order # 040423205 Sample: MH1 1 Grab
Parameters
Results Analysis Date
4/4/23
Reporting Limit Method
% Total Solids
1.74 %
4/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
126,437 CFU/g dry wt
4/4/23
216 CFU/g dry wt
SM 9222D
Meritech Work Order #
040423206 Sample:
MH12 Grab
4/4/23
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.74 %
4/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
149,425 CFU/g dry wt
4/4/23
221 CFU/g dry wt
SM 9222D
Meritech Work Order #
040423207 Sample:
MH13 Grab
4/4/23
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.70 %
4/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
147,059 CFU/g dry wt
4/4/23
215 CFU/g dry wt
SM 9222D
Meritech Work Order #
040423208 Sample: MH14 Grab
4/4/23
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.72 %
4/6/23
0-100 %
SM 2540E
Fecal Coliform (CIass B Sludge)
157,163 CFU/g dry wt
4/4/23
222 CFU/g dry wt
SM 9222D
Meritech Work Order #
040423209 Sample: MH1 5 Grab
4/4/23
Parameters
Results
Analysis Date
Reporting Limit
Method
% Total Solids
1.70 %
4/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
117,647 CFU/g dry wt
4/4/23
225 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Contact: Ryan Copeland
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 2
Report Date: 4/13/2023
Date Sample Rcvd: 4/4/2023
Meritech Work Order # 040423210 Sample: MH1 6 Grab 4/4/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 1.32 % 4/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 159,091 CFU/g dry wt 4/4/23 214 CFU/g dry wt SM 9222D
Meritech Work Order # 040423211 Sample: MH1 7 Grab . 4/4/23
Parameters Results Analysis Date Reporting Limit Method
11/6 Total Solids 1.68 % 4/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 92,262 CFU/g dry wt 4/4/23 198 CFU/g dry wt SM 9222D
f hereby certify thatl have reviewed and approve these data. zz�t'c
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 04/04/2023
Reported: 05/10/2023
For: Mt Holly
Comments:
4 STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230404-42-01 30 Day Benchscale Mt Holly
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
23.4
EPA525-R-92i0 04/04/2023 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Condition of Receipt
Sample Number 230404-42-01 Temp on Arrival: 3.0
Parameter Schedule:
Received on Ice
Chemicals in containers, lab
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

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STATESVI LLE
R ANALYTICAL
Synagro
284 Boger Rd
Mocksville, NC 27028
Entered: 4-4-23
Reported: 5-10-23
Sample ID: 230404-42-01
Analytical Results
For: Mt Holly
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids Volatile Solids % Volatile Solids
k 1 0.66
0.7879
Week 2 0.60 0.47 0.7833
Week 3 0.55 0.43 0.7818
Week 4 0.51 0.39 0.7647
Week 5 0.49 0.37 0.7551
Week 6 0.46 0.34 0.7391
Volatile Solids Reduction: 0.7879 - 0.7391 X 100 = 23.4
0.7879 - (0.7879 X 0.7391)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample 1D # 230404-42-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.70
0.53
2
0.63
0.51
3
0.64
0.51
Average:
0.66
0.52
0.7879
WEEK 2
-Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.61
0.46
2
0.59
0.46
3
0.61
0.48
Average:
0.60
0.47
0.7833
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.54
0.43
2
0.57
0.43
3
0.55
0.43
Average:
0.55
0.43
0.7818
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.52
0.39
2
0.51
0.38
3
0.51
0.39
Average:
0.51
0.39
0.7647
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.52
0.39
2
0.48
0.36
3
0.47
0.35
Average:
0.49
0.37
0.7551
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.47
0.34
2
0.46
0.33
3
0.46
0.34
Average:
0.46
1 0.34
0.7391
Van Kleeck Reduction: 0.7879 - 0.7391 X 100 = 23.4 %
0.7879 - (0.7879 X 0.7391)
Final Result: 23.4%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

%VS R
(older, more conservative method)
%VS in 0.7879 - Enter in
%VS out 0.7391 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 23.74
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in
%VSR= 6.19
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount [lolly WQ Permit Number: WQ0001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 07/01/2023 To 09/30/2023
Pathogen Reduction (40 CFR 503.32115A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. UA (time/temp) Alt, 2/13(Alk Treatment) Alt. 3/C (Prior Testing)
Alt. 41D (No Prior Test) Alt. 5/Process to Further Reduce Pathogens Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost [seat Drying Heat Treatment Thermophilic
Beta Ray Galnnta Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Ait. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
rf annlirahln to alfPrna41VP n—ffl .A fd l— A — dri.cc Rl nnm..ln4n +h. Fnnn...:n...,,.,„:k...-i— A.t -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10to the 611
MPN
Coliform
power per gram
MPN/g
of total solids
CFU
14,778
24,639
39,409
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
Salmonella
3 MPN per 4 grams total
bacteria (in
solids (dry weight)
lieu of fecal
coliforin)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed-
Option/Alt. 1
Option/Alt, 2
Option/Alt. 3 Option/Alt. 4
(VS redaction)
(40-day bench)
(30-day bench) X (Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7 Option/Alt, 8
04-Day Aerobic)
(Alk Stabilization)
(Drying — Stable) (Drying — Unstable)
Option/Alt. 9
Option/Alt. t0
(Injection)
(Incorporation)
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1106 and the vector attraction
X reduction requirement in 40 CFR 503.33115A NCAC 02T.1107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32115A NCAC 02T.1106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T_1107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnet properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met. I am aware that there are significant penalties for false certification including fine and imprisonment."
Keith Lynch Division Manager Wastewater
Preparer ame a tid Tit e ( pe or p ' t)
1
Signature of Preparer* Date
Land Applier Name and Title (if applicable) (type or print)
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Page 1
Contact: Alex Fox Report Date: 7/12/2023
Client: Synagro
284 Boger Road Project: Mount Holly
Mocksville, NC 27028 Date Sample Rcvd: 7/5/2023
Meritech Work Order # 07052334 Sample: MH 1 Grab 7/5/23
Parameters Rea1� Analysis Die Reporting Limit Method
%Total Solids
2.01 %
7/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
34,826 CFU/g dry wt
7/5/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order # 070S233S Sample: MH 2 Grab 7/5/23
Parameters Results Analysis Date ReportingLimit ethod
% Total Solids 2.03 % 7/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 24,631 CFU/g dry wt 7/5/23 484 CFU/g dry wt SM 9222D
Meritech Work Order # 07052336 Sample: MH 3 Grab 7/5/23
Parameters
Results
Analysis
Reporting Limit
Method
%Total Solids
2.06 %
7/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
29,126 CFU/g dry wt
7/5/23
484 CFU/g dry wt
SM 9222D
Meritech Work Order # 070S2337 Sample: MH 4 Grab 7/5/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids 2.03 % 7/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 14,778 CFU/g dry wt 7/5/23 130 CFU/g dry wt SM 9222D
Meritech Work Order # 0705233E Sample: MH 5 Grab 7/5/23
Parameters Results Analysis Date Reporting, Limi Method
%Total Solids
2.03 %
7/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
39,409 CFU/g dry wt
7/S/23
491 CFU/g dry wt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Alex Fox
Client: Synagro
2B4 Boger Road
Mocksville, NC 27028
Page 2
Report Date: 7/12/2023
Project: Mount Holly
Date Sample Rcvd: 7/5/23
Meritech Work Order # 07052339 Sample: MH 6 Grab 7/5/23
Parameters Results Analysi5 J)ate Reporting Limit Method
% Total Solids 1.98 % 7/6/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 20,202 CFU/g dry wt 7/5/23 489 CFU/g dry wt SM 9222D
Meritech Work Order # 07052340 Sample: MH 7 Grab 7/5/23
Parameters Results Analysis Date Reporting Limit Method
% Total Solids
2.15 %
7/6/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
18,605 CFU/g dry wt
7/5/23
130 CFU/g dry wt
SM 9222D
I hereby certify that I have reviewed and approve these data. 4 fY]�"ypc OCjL-
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 07/05/2023
Reported: 08/15/2023
For: Mt Holly
Comments:
4 1TATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
230705-27-01 30 Day Benchscale Mt Holly
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
26.4
EPA625-R-92i0 07/05/2023 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 4

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A234

STATESVILLE
ANALYTICAL
Synagro
284 Boger Rd
Mocksville, NC 27028
Entered: 7/5/23
Reported: 8/15/23
Sample ID: 230705-27-01
Analytical Results
For: Mt Holly
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge (30day)
Total Solids
Volatile Solids
% Volatile Solids
Week
1
0.71
0.55
0.7747
Week
2
0.71
0.54
0.7606
Week
3
0.65
0.49
0.7539
Week
4
0.65
0.49
0.7539
Week
5
0.61
0.44
0.7213
Week
6
0.60
0.43
0.7167
Volatile Solids Reduction: 0.7747 - 0.7167 X 100 = 26.4
0.7747 - (0.7747 X 0.7167)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.## 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 4

30 Day Bench Worksheet
Sample ID 0 230705-27-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.72
0.56
2
0.71
0.54
3
0.70
0.54
Average:
0.71
0.55
0.7747
WEEK 2
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.69
0.53
2
0.74
0.56
3
0.70
0.53
Average:
0.71
0.54
0.7606
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.66
0.49
2
0.65
0.48
3
0.65
0.49
Average:
0.65
0.49
0.7539
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.65
0.48
2
0.67
0.50
3
0.64
0.48
Average:
0.65
0.49
0.7539
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.60
0.43
2
0.61
0.45
3
0.62
0.44
Average:
0.61
0.44
0.7213
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.60
0.43
2
0.60
0.43
3
0.59
0.43
Average-
0.60
0.43
0.7167
Van Kleeck Reduction: 0.7747 - 0.7167 X 100 = 26.4 %
0.7747 - (0.7747 X 0.7167)
Final Result: 26.4%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 4

%VS R
(older, more conservative method)
%VS in 1 0.7747 - Enter in
%VS out 1 0.71671 decimal form
%VSR= (%VS in - %VS out)
((%VS in - (%VS in x %VS out))
%VSR= 26.43
(method from p.132 of WH manual)
%VSR= (%VS in - %VS out)
%VS in
%VSR= 7.49
Results must be either greater than 38%; less than 17% for a 40-day bench -
scale test; or less than 15% for a 30-day bench -scale test.

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Mount Holly WQ Permit Number: W00001863
WWTP Name: Mt Holly WWTP NPDES Number: NCO021156
Monitoring Period: From 10/01/2023 To 12/31/2.023
Pathogen Reduction (40 CFR 503.32/15A NCAC 02T.1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. I/A (time/temp)
Alt. 4/1) (No Prior Test)
Alt. 2/B (Alk Treatment)
Alt. 5/Process to Further Reduce Pathogens
Alt. 3/C (Prior Testing)
Alt. 6 (Equivalent to PFRP)
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost Heat Drying Heat Treatment Thermophilic
Beta Ray Gamma Ray Pasteurization
Class B:
Alt. (1) Fecal Density X Alt. (2) Process to Significantly Reduce Pathogens
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestion
Ifanntieahip M nlfPrnativP nPrinrmPd Wincc A nr (`Iacc R1 emmniptP the fnllawinu mnnitarim data -
Parameter
Allowable Level in Sludge
Pathogen Density
No. of
Frequency
Sample
Analytical
Excee-
of
Type
Technique
Minimum Geo. Mean Maximum Units
dences
Analysis
Fecal
2x10 to the 611
MPN
Coliform
power per gram
MPN/g
Quarterly
Grab
SM9221C
of total solids
CFU
189,349
309,853
447,059
�
CFU/g
0
Quarterly
Grab
SM9222D
1000 MPN per gram of
total solids (dry weight)
onella
3 MPN per4 grams total
ria (in
L
solids (dry weight)
f fecalorm)
Vector Attraction Reduction (40 CFR 503.33/15A NCAC 02T.1107) - Please indicate option/alternative performed:
Option/Alt. I
Option/Alt. 2
Option/Alt. 3
Option/Alt. 4
(VS reduction)
(40-day bench)
(30-day bench) X
(Spec. 02 uptake)
Option/Alt. 5
Option/Alt. 6
Option/Alt. 7
Option/Alt. 8
(14-Day Aerobic)
(Alk Stabilization)
(Drying — Stable)
(Drying — Unstable)
Option/Alt. 9
Option/Alt. 10
(Injection)
(Incorporation)
No vector attraction reduction alternatives
were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
X reduction requirement in 40 CFR 503.33/15A NCAC 02T.1 107 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32/15A NCAC 02T.1 106 and the vector attraction
reduction requirement in 40 CFR 503.33/15A NCAC 02T.1 107 have not been met." (Please note if you check this statement attach an
explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified
personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have
been met I am aware that there are significant penalties for false certification including fine and imprisonment."
Keith Lynch Division Manager Wastewater _
Preparer N >.e anj Tit[ (ty or pr t) Land Applier Name and Title (if applicable) (type or print)
al�w,.�
Sign ture of Preparer* Date' Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T.1102 (26)

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No.165
Page 1
Contact: Alex Fox
Report Date:
10/10/2023
Client: Synagro
284 Boger Road
Project:
Mount Holly
Mocksville, NC 27028
Date Sample Rcvd:
10/3/2023
Meritech Work Order #
100323165 Sample: MH 1 Grab
10/3/23
Parameter
Results Analysis Date
Reporting Limit
Methad
Total Solids
1.70 % 10/5/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
270,588 CFU/g dry wt 10/3/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
100323166 Sample: MH 2 Grab
10/3/23
Parameters
Results Analysis Date
Reporting Limit
Method
%Total Solids
1.69 % 10/5/23
0-100 %
SM 2540B
Fecal Coliform CClass B Sludge)
366,864 CFU/g dry wt 10/3/23
484 CFU/g dry wt
SM 9222D
Meritech Work Order #
100323167 Sample: MH 3 Grab
10/3/23
Paralneters
ResultsAnalysis Date
Reporting Limit
Method
%Total Solids
1.70 % 10/5/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
447,059 CFU/g drywt 10/3/23
484 CFU/g dry wt
SM 9222D
Meritech Work Order #
100323168 Sample: MH 4 Grab
10/3/23
Parameter
Results Analysis Date
Reporting LimitLimit
Method
Total Solids
1.70 % 10/5/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
376,471 CFU/g dry wt 10/3/23
130 CFU/g dry wt
SM 9222D
Meritech Work Order #
100323169 Sample: MH 5 Grab
10/3/23
ParamCter
Results Analy-lis Date
Reporting Limi
Method
% Total Solids
1.68 % 10/5/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
273,810 CFU/g dry wt 10/3/23
491 CFU/g drywt
SM 9222D
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
Contact: Alex Fox
Client: Synagro
284 Boger Road
Mocksville, NC 27028
Page 2
Report Date: 10/10/2023
Project: Mount Holly
Date Sample Rcvd: 10/3/23
Meritech Work Order # 100323170 Sample: MH 6 Grab 10/3/23
Param Resu Analysia Date Reporting Lim! Method
% Total Solids 1.69 % 10/5/23 0-100 % SM 2540B
Fecal Coliform (Class B Sludge) 316,568 CFU/g dry wt 10/3/23 489 CFU/g dry wt SM 9222D
Meritech Work Order # 100323171 Sample: MH 7 Grab 10/3/23
Parameters Results Analysis Date Reporting Limit Method
%Total Solids
1.69 %
10/5/23
0-100 %
SM 2540B
Fecal Coliform (Class B Sludge)
189,349 CFU/g dry wt
10/3/23
130 CFU/g dry wt
SM 9222D
1
l hereby certify that) have reviewed and approve these data.
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

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Analytical Results
Synagro
284 Boger Rd.
Mocksville, NC 27028
Receive Date: 10/03/2023
Reported: 11/15/2023
For: Mt Holly
Comments:
STATESVILLE
ANALYTICAL
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
231003-47-01 30 Day Benchscale Mt Holly
Respectfully submitted,
Melissa Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
11.4
EPA625-R-92/0 10/03/2023 MD
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 1 of 5

Condition of Receipt
Sample Number 231003-47-01 Temp on Arrival: 3.0
Parameter Schedule:
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 of 5

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PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 3 of 5

STATESVILLE
ANALYTICAL
Synagro
284 Boger Rd
MocksVille, NC 27028
Entered: 10/3/23
Reported: 11/6/23
Sample ID: 231003-47-01
Analytical Results
For: Mt Holly
PARAMETER: Vector Attraction Reduction/Aerobically Digested Sludge 30da
Total Solids
Volatile Solids
% Volatile Solids
Week
1
0.59
0.44
0.7458
Week
2
0.58
0.42
0.7241
Week
3
0.58
0.43
0.7414
Week
4
0.55
0.39
0.7091
Week
5
0.51
0.36
0.7059
Week
6
0.54
0.39
0.7222
Volatile Solids Reduction: 0.7458 - 0.7222 X 100 = 11.4 %
0.7458 - (0.7458 X 0.7222)
Respectfully submitted,
Melissa Myers
Statesville Analytical, Inc.
NC WW Cert.# 440NC
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 4 of 5

30 Day Bench Worksheet
Sample ID # 231003-47-01
WEEK 1
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.60
0.44
2
0.58
0.42
3
0.60
0.45
Average:
0.59
0.44
0.7458
WEEK 2
Samples
I Total Solids
Volatile Solids
% Volatile Fraction
1
0.58
0.42
2
0.59
0.43
3
0.58
0.42
Average:
0.58
0.42
0.7241
WEEK 3
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.59
0.44
2
0.57
0.43
3
0.57
0.42
Average:
0.58
0.43
0.7414
WEEK 4
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.55
0.39
2
0.55
0.40
3
0.54
0.39
Average:
0.55
0.39
0.7091
WEEK 5
Samples
Total Solids
Volatile Solids
% Volatile Fraction
1
0.52
0.37
2
0.51
0.35
3
0.51
0.36
Average:
0.51
0.36
0.7059
WEEK 6
Samples
Total Solids
Volatile Solids
% Volatile Fraction
I
0.58
0.41
2
0.54
039
3
0.51
0.37
Average:
0.54
0.39
0.7222
Van Kieeck Reduction: 0.7458 - 0.7222 X 100 = 1 l.4 %
0.7458 - (0.7458 X 0.7222)
Final Result: 11.4%
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 5 of 5

SECTION 6

Agricultural Lime Application Log
Year: 2023
Project: MT Holly
Field
(state -county -site -field)
Soil
pH
Lime Requirement
(from soil analysis)
Tons/Acre
Applied(CCE Eq.)
Date Applied
LT-46-1
5.2
1.3/AC
LT-46-2
6.6
O.OT/AC
LT-46-3
4.9
1.9T/AC
LT-46-4
6.6
O.OT/AC
LT-46-8
6.0
O.OT/AC
MG-37-1
6.9
O.OT/AC
* Lime is ordered and will be spread soon

SECTION 7

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY24-SL003609
k5i I"14'4+;4,
Client:
Alex Fox
Advisor:
Predictive
Synagro
284 Boger Rd
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Links to Helpful Information
Sampled: Received: 09/08/2023 Completed: 09/18/2023 Farm: Lt-46
Client ID:
Sampled County : Lincoln
501947
Advisor ID:
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.3 120-200 0
60
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 0
60
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I
Zn-AI
Cu-I Na
ESP
SS-1 NO3-N
0.46 0.83 7.8 72 2.2 5.2 212 41 56 13
64 546
345 345
449
449
1102 0.2
3
Sample ID: 3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn
Zn
Cu
B
Information
Lime History:
1-Fescue/OGrass/Tim, M 1.9 120-200 0
80
0 0
0
0
0
0
Note: 12
2- Fescue/OGrass/Tim, M 0.0 120-200 0
80
0 0
0
0
0
0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-AI2
Zn-I
Zn-AI
Cu-I Na
ESP
SS-1 NO3-N
0.86 0.76 8.4 65 2.9 4.9 203 28 48 16
75 171
120 120
496
496
650 0.2
2
North Carolina
Tai wLm Truk f and Ctwinlsskm
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY24-SL003609
Alex Fox
Page 2 of 3
Sample ID: 8
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg
S
Mn
Zn
Cu B
Information
Lime History:
1-Fescue/OGrass/Tim, M 0.0
120-200 0
90
0
0
0
0
0 0
Note: 12
2- Fescue/OGrass/Tim, M 0.0
120-200 0
90
0
0
0
0
0 0
Note: 12
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All
Mn-Al2
Zn-I
Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.51 0.86 10.4 86 1.4 6.0 161 25
62 23 72
162
114
114
641
641
508 0.4
4

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY24-SL003609
Alex Fox
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NOs-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm

Page 1 of 2
Report Number: 24-002-0527
Account Number: 07778
Send To: Synagro/Alex Fox
Alex Fox
284 Boger Rd
Mocksville NC 27028
•
Waypoint
ANALYTICAL
"Every acre... Every year. "rM
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Grower: MT HOLLY
Farm: LT-46
SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Lime Index Humic Matter Loss On Ignition
Water pH
Date Received: 01/02/2024 Date Of Analysis: 01/03/2024 Date Of Report: 01/03/2024
OM
W/V
ENR
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
Field ID
Number
%
Soil
Ibs/A
M3
K
Mg
Ca
Na
Soil
Buffer
H
Class
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
pH
Index
meq/100g
meq/100g
2
24244
1.4
67
249 VH
73 L
132 M
1053 M
24 VL
6.6
0.8
7.6
NC = 207
NC = 37
4
24246
1.4
67
211 VH
63 L
130 M
1061 M
28 VL
6.6
0.8
7.6
NC=176
NC=32
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salts
Sample ID
Field ID
K
Mg
Ca
Na
H
NO3 N
S
Zn
Mn
Fe
Cu
B
SS
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
2
2.5
14.5
69.3
1.4
11.8
12 L
20.9 VH
22 H
7.9 VH
0.6 M
NC=25
NC=522.5
NC=138
NC=395.0
4
2.1
14.3
69.8
1.6
11.8
12 L
19.8 VH
19 M
6.8 VH
0.6 M
NC=25
NC=495.0
NC
NC=340.0
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a
soil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing.
H (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble by.
C.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared by: waypoint Analytical Carolina, Inc.

Page 2 of 2
Report Number: 24-002-0527
Account Number: 07778
Send To: Synagro/Alex Fox
Alex Fox
284 Boger Rd
Mocksville NC 27028
Date Received: 01/02/2024
Date Of Report: 01 /03/2024
Waypoi nt(D
-
ANALYTICAL
"Every acre... Every year. "rM
Farm: LT-46
SOIL FERTILITY RECOMMENDATIONS
2850 Daisy Lane, Wilson, NC 27896
Main 252-206-1721 ° Fax [phone]
www.waypointanalytical.com
Grower: MT HOLLY
Nitrogen
Phosphate
Potash
Magnesium
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Sample ID
Intended Crop
Yield Goal
Lime
N
P205
K20
Mg
S
Zn
Mn
Fe
Cu
B
Field ID
Tons
Tons/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
Ib/A
2
Fescue Hay
4
0.0
200
0
250
0
10
0
3
0
0
4
Fescue Hay
4
0.0
200
0
250
0
10
0
3
0
0
Comments:
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied, concerning crop performance is made."
Our reports and letters are for the exclusive and confidential use of our clients„ and may not be reproduced in whole or part, nor may any reference be made to the
work,the results, or the company in any advertising, news release, or other public anouncements without obtaining our prior written authorization. Copy right 1977.

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/ Report No. FY24-SL003604
k5i I"14'4+;4,
Client:
Alex Fox
Advisor:
Predictive
Synagro
284 Boger Rd
�- Soil Report Mehlich-3 Extraction
Mocksville, NC 27028
Links to Helpful Information
Sampled: Received: 09/08/2023 Completed: 09/18/2023 Farm: MG-37
Client ID:
Sampled County : Mecklenburg
501947
Advisor ID:
Sample ID: 1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre) N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1 -Fescue/OGrass/Tim, M 0.0 120-200 10
70
0 0
pH$ 0
0 0
Note: 12 Note: $
2 - Fescue/OGrass/Tim, M 0.0 120-200 10
70
0 0
pH$ 0
0 0
Note: 12 Note: $
Test Results [units - W/V in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]:
Soil Class:
Mineral
HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg%
S-1 Mn-I
Mn-All Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP
SS-1 NO3-N
0.18 0.99 10.3 93 0.7 6.9 58 34 59 32
38 452
274 274
344 344
481 0.1
1
North Carolina
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Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY24-SL003604
Alex Fox
Page 2 of 2
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at onE
Ca%
% CEC occupied by calcium
time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate
CEC
cation exchange capacity
is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-I
copper index
ESP
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
manganese
only on reports for greenhouse soil or problem samples.
Mn-All
Mn-availability index for crop 1
Mn-Al2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
Mn-
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients_ In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomi/pubs.htm.
NOs-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagr.pov/apronomi/obpart4.htrntfsfind information that
P-1
phosphorus index
may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
Test Results
SS-1
soluble salt index
W/V
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The
Zn-AI
zinc availability index
Zn-1
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinel
available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.pov/agronomi/uyrst.htm