WQ0003824_2023 Residual Annual Report_20240213 (2)

Initial Review
Reviewer
nathaniel.thorn burg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2023
Permit Number (IR) * WQ0003824
Applicant/Permittee City of Graham
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer Wanda Gerald

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Cris Routh
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
3365706721
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0003824
Has Current Existing permit number
Applicant/Permittee Address*
P. O. Drawer 357, Graham, NC 27253
Facility Name*
City of Graham Class B Residuals Program
Please provide comments/notes on your current submittal below.
Attached is the Land Application 2023 Annual Report for the City of Graham.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
2023 City of Graham LA Annual Report.pdf 42.07MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
Submission Date 2/13/2024

LAND APPLICATION
m<% �
> .ra
G
2,023 ANNUAL REPORT

"I'l Y OF (I"RAHANI
LAND APPI JCA HON REPORl­
FOR 2023 REP 01'R flNG YEAf'�Z
ORDER OF'CON FENTS
GOVER LETTER
1. ANNUAL LAND APPI-ICATION CERTIFICA'"riON IFORM
(RESULTS FOR GITY OF GRAHAM WINTP ONLY)
2. ANNUAL RESIDUAL SAMPLING SUMMARY FORMS
(RE'SUL ?"S FOR Cl TY OF GRAHAM WWTP ONLY)
3. ANNUAl.... METALS FIELD LOADING SUMMARY FORMS BY FIELD (1, 2,3,4,55, 6,7,8, 10)
(RFSUL TS FOR Cl TY OF GRAHA M WWTP ONLY)
4. ANN' UAL LAND APPLICATION FIELD SUMMARY FORMS BY FIELD (1, 2,3,4,5,6,7,8,l0)
(RESULTS FOR CITY OF GRALLAM WW7-P ONLY)
5. EXPANDED MERCURY CALC ULATIONS FOR FIELDS 3,4,5,6 & 7
6. VVVVTP SLUDGE FLOW SCHEMA"I'IC
7. QUARTERLY SLUDGE SAMPLING REPORTS
8. SODIUM ABSORPTION RATIO CALCULATIONS SUMMARY
9. TCLP FOR VVWTP RESIDUALS REPORT
10. FECAL COLIFORM REPORTS
11. SO, U,R REPORTS
12. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORMS
11 SOIL TEST REPORTS
14. CROP YIELD RECORDS FOR 2023

vd� tit
P.O. Dravvew 3617
20 1 South Main Street
(i ra k tarn, hk)i th C,,arobf ia 2 /P53
Ted: [phone] / Fax: (336) !-3 70- 6 703
DEN' R/f.,)VVQ/VVATE F? QUA.Lrry si!- ' c noiq
Non -Discharge Compliance Unit
'1617 Mail Service Center
Raleigh, N.C. 27699-1617
February 9, 2024
Dear Sirs:
The following data and report are for the City of Grah,arn's land application
program:
Permit NUrnber
Period Covered
Sources of Sludge
Method of Application
VVQ0003824
JanA, 2023 thru Dec.31, 2023
City of Graham wwria,
Surface Applied
Bio-solids, frorn the City of Graham Wastewater Treatment Plant were land
applied in all -twelve months during 2023. Applied metal calculations for 2023 reflect
Wastewater Treatment Plant sludge only. Effective January 1, 2021, Ferric sludge
from the City of Graham Water Treatment Plant is applied on land provided by
Synagro Southeast, Inc. of Clemmons, NC and those results are no longer included
in this report. The metal loadings, (ending 12/31/2022) were added to the 2023
WWTP bio-solids to arrive at the ending 2023 accumulated metal totals.
Items of note from 2023:
1. Information on all forms is for the Wastewater Treatment only. Synagro
results are no longer included in this report.

2. Mercury resultsfor Fields 3, 4, 5, 6 & 7 are all reported as "0.000". A
separate, pagu foHows tsar Sumnixy Fornis" that exparrds arid vl( rifies
these reSUIN.
3, Quarterly Sludge Analysis was r.)erformed during March, May, August, and
October of 20,23.
4,, The TCLP Analysis san,iifle was (.ollecN.)d on 0(',tober 19, 2023,
5. Soil sarnples were collected in August 28, 2()2'13.
6, Grop Yield restAlts for 2023 are included at the end of ffiis report.
1 he City meA the 40 CI-R 5013(B) ruiles for Pathogen Reduction (Class B, Alternal.ive
I for Fecal ofifoirn artd Vector Afl-JaGtion Rate by Specific Oxygen Uptake Rate.
The City of Graham uses H-ie North Carolina DepartrT-Went of Erivir-or-imenlall and
Natural Resources rnethod developed by them" for the US Ef"I/V
If any additional information or explanatiori is noodled, please, contact rne at
[phone].
Sincerely,
Crispian T. Routh
Plant Superintendent
City of Grahan,i

ANNUAL 1,ANDAPP1,1CATION CERTIFICATION FORM
Pcrffdt-/h WQ0003824 Coillity: ALAMANCE Year: 2023
. .........
U,acifity Nanic (as shown on perndt)- CITY OF GRAHAM
............
Land Application Operator- Crispian T. Routh plloue 336.570,6721
Land application of residual solids as allowed by the permit occurred during flac past calendar year?
N Yes 0 No If No, sidle, Part A, and Part B and procced to the certification. Also, if residiials were
gencrate'd but rent: land applied, please retiree h an explanation on how the residuals were handled,
Pa, r t A:
. ............... . . ...... . - j711 "�)cr#njt. — - — --- --------------- -- -- — - - - ----------
Total number of application fields V r 9111 9
...............
Total naunber offields land application occuirred during tile ye 6
. .......... . ....... -
...Total number of acres land application occurred during the 51.6
............... ....................... . ......
Part ter
Facility was compliant during calendar year 2023 with all conditions of 1he land application permit
--.1-- . ..........
(including bul not hinited to Hems 1,42 below) issued by the Division of Water Qaalio,Yes 0 No
1frio, please, provide as written description why the facility wars not coin plian t, the dates, and explain
corrective action takeu
1. Only residuals approved for this perunit were applied to the perinitted sites,
2. Soil pH 'was k1djUsted as specified in the permit and linie was applied (if needed) to achieve a soil pH of al.
least 6.0 or the limit specified in the permit,
3. annual soils analysis were perf6rined on each site receiving residuals dUring the past calendar year and three
(3) copies of laboratory results are attached.
1. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies ofeertified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table I of 40 CFR Part 503.13 or flic
POIlUtarit Loading Ratcs in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities),
7All general req u iretne tits in 40 CFR Part 503,12 and management practices in 40 CFR Part 03,14 were
complied with (applicable to 40 CFR Part 503 ['CgUlated facilities).
8�. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received frorn the Division of Water Quality.
9. No contravention Of Ground Water Quality Standards occurred at a rrioniloring welt or explanations of
violations are attached to include appropriate actions and rernediations.
l 0, Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan,
11. No runoff of residuals from the application sites onto adJacent property or nearby surface waters has occurred.
12, All buffer requirements as specified on the permit were rnaintained during each application of residuals,
"I certi(y, tinder penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Tonyx A. Mann / Utilities Director Y ,� d< ,r" � :`.a^ � ,,,�., �.. �w m � ���
Perrilittee Name and Title (type or print) Sig'nafti e of Permittee Date
Signature of Preparer* Date Signature of Land Applier Date
(if different from Permittee) (if different from Pert-nittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r)

61-

1q)
�X
I U
�4 m
U
0
4n
cl
03
(d
w
wow
rimm
NT
00
C)
U
U)
(J)
CA
em
. . ........
4. 0 6 , xn
awe of)
Z
. ......... . ....
�45
U�
r.-
-4
. . . .... . ... ........ . . ... . .. . .............. ... . . ..... . . .................... . . ..... . . ..... . .. . . . ........... . .......... . . . . . .. . . .................. . .. . .... . .. . ... . ..... . . . ............ . ... .... . ................. . . ..
tl
4.0
CvNIU) Wco: C("i —c")ILO -U'Ni- co
v
N(CD)- C<ND
(mv14 co
m U, LO — 06 (NI 4v
TI
C.T) M
CQ Lf) CCD C:) C)
C) - Cy� co
CD 110 F) (X)
(,o co C'D WO
C-0 L,r)
00 v CN LO 4�
( (Z)
Z) CD CD CN
cli 00 co l-, M, r�. CD Lo Lo (f)
cyj LO C%4 co C-) M Lo 4o
C'4 C) Lo m CNI CO L6 v
v v
CIIj C14 C,41 -J- <D CD C.D
cl") CO co 00 CD CD CY) r,- 0) mCq qdNO
-
v 00 rq f �-z'ry v
CI)
V) W) CJ (Z) W CCJ al
0 --a 'i� -LI.
�L4
�j
aau
Ln
0
0
X� a4
cj 7�
0
o
71
nn 50

A
B
Z
v
Qq
.....
_
..........
__,a
rdT1 W�"�"tl
n
1
�W
t
0
m�
...................
... _..
..........
...p..�,
.a............m.....m.m
.....__..
a...._...._
.m_.
��,.
�
..
�'?
YuWw
*raga
Qrd
xr
r„
(n
D
T
(`WI
Cl)C.-D
CD
CD
CD
00
c t
CD
C,
y
I
r1..
L6
^c—
r
"nmm
4 "7
{gym
CV
I,—Lco
a
",
o
, r
Ln
c aCDC
I
C
C
�
"
L
=
u7
I`-,-
.
c�)
c.�
C�
C)
CD
(Y')
m
C7
�D
C_'wy
C\qLO
�
t'D
C;57
"mro
LO
ti �i
IC,5
C1
Oo
c5
C`4
3
c
w
�"�'
wumxiwm�w
w
S
6
d
U)
-2
=
"
0
cra
CJ�
s
CO
G
d,
Ca
CL,
C 7
c
rA
l
)
w

B a► 10

P,
9
ti IN
I'd
c
<5
rs
rL
rL
4)
0..)
Q
V
V
Q
A)
00
0
U
IJ
7311.11.1 6
4n 0
P
u
U
Q
U,
t�
U
'o
Ij
oo
U
U
U
0
U
'o
m NO
6
rK"
v
v
q.)
�o
ro)
%d
ol,
.
.........
. . .......
.. .
......
In
0�
fn
p
cp
m
Iq
"')
�-
If)
C�
15
C)
C5
0
C.5
cz,
6
4a CJ
'..
Q.
vi
.r3
c-i
6
6
c�'
z; tf
`2
CD
.
..... . .
do
cl)
an bl)
v Tj 0
CF
CIA
CA
(11 W)
r") V, r'l
Niti-ogel E'
ol
1�1
In
In
1r)
�C) C:) CD
0 tII-
(',d C-14
a.
. ....... . ........
I,
.
...................
...
................... .
...................
................. . .
. . ......... . . .
--j—
J,
o
M i 11 c I -a z -a o 11
cd
It)
cs
il,
I-,--
m
V o la(I I i z at i 011
In
In
In
In
In
In
In
CL
CJ V� cl�
n
c5
c-5
6
6
C5
6
CL
'7
"Is
Application
(n
cn
c")
(n
bf,
q.) a "3-
method"
en
V3
V)
Q,
V)
'7�
lz i
CD
CD
6, -
4)
On
(U
cd
cli
r4
41
rA
z
z
z
z
z
7-
.
. .
. ...
. ....... .
. ...... .
.
.....
CL
u
00
........... .
"o
<�
-
ON
00
cn
;,, M
10 LO
o
Lo
Z
,:a
z:1
'M
Tj
'I
I'D
O�
CA
r
e-A.
CsS
VA
qj
=a U CS
CD
I:*
Cl
I'D
C�
In
-t
"IR
�o
cl)
"o
r�
IN
CD
C3
CI
CI
C
C�
C>
C�
C�
CI
CD
C�
�l
C�
lb
C4
m
In
cz�
llr
o
clr
0
c>
eaC--
�
o
6
CD
Cl)
6,
7�
o
Cad
N
Cal
N
rl'
CIO
rt
00
llJ
Cl
CY
C�
Cl
C�
CP
73
ul
C'4
Id
(14
—
—
—
—
—
--
an
�D
11
CD
o
CD
00
<D
CD
C=
"St
14)
o
C-1
clq
lc
It
o
ou 1= ol
6.a-,
0 0
u
>
ln'
t-. El
ql UON

-s
u
Pm
U
u
OZ
5)
U
C)
i-q
c
0
CY
u
141
&I
FNMA
cl
c.
z
1.4
�n
I
Ld
1AJ
LL-
LL-
0
LQ
qd
U
c)
CA
ly
co.
.....
.
Al11
73
u
to)
C)
zu
Pe
1A
V1
V)
1�
11,
V,
V�
V�
V,
v
V)
U
1)
c�
bO
C,7�
. ............
. . . ... . ...
f-Mmmmma
rtlh 01",
rn.
if7
1171
1711
r-1
ID
lz�
c"',
C),
(D
C1
ID
c)
C>
CD
0 W
CD
181
bf)
X.,
0" c7l
Od qd Tl
Ammonia
Nitrogen
c> '.0 'j�)
bij
�s
I.. c;
0�
I.M
00
13
E
. . .............. .
11 cra zat i oil
0
c� VO 00
4 bij "4
Rate*
chi
W .1,1
Volatilinkon
Rate*',
Application
C,.:. 0" O�,
method"
1,
0
Chi 14) "0C�
In
14
0
00 CIO
V)
�
c44y
6 F�, F�
71
4)
u
c�
54'
C, C% c�
4
lz�
Cy
lz�
=�
<:7)
�=
lz�
C)
C�
C:�
8,
C:C
00 m
X!
6
6
6
6
6
6
6
6
6
6
6
CD
73
0
.......... ................ ................ ...
.
. . . .
. .. ......
.. .. ........
0
4)
Q)
'R
Tj
U
0 rd 7:�
'7Z$
ctl
qjuON
.10 01P
;Z
U

i L' if
cd
03
0 m
0
0
ce
0
ri
7— 00 6
r,:
4
r
Ot
ft4
U L�
C)
Ljj
Z)
u
vi
Li
I
1,4
xg
Ic,
qo 4)
0 P,
U
lu
U
U
U
U
u
v
li
W
lu
vi 4z
n�
0
.j
1l
:13
1,
1.13
1J
VY
1i
11
11
11
Z
'
13
11
v
0
u
qJ
1)
aj
a)
v
Oj
OL)
Z,
7-
7�
7,
Z
Z
Z
Z
1 <8
NO
ul
TJ U
In
Cr
C�
CD
C>
C�
C)
CD
C�
C)
0
C.)
CD
C'�
C>
rj
0
"0
C.5
6,
25
c;
c)
25
CL:)
c"
6
c>,
6
c7,
CS
6
rm,
i
aZ,
U CA
ul Od
......... . . . . .. ....
7j �4
In
..........
Iv
1-0
Qj
S
�N,l
en 7,
Nill-Ogell E
't
...............
. .
.....
cp
-
g
- m
vD
-
�jl
01
fA d)
I"
r)
t--
Z� r-! "0
f.-, z:j Q
.... .. ..........
. .—
--
- ---
-----
ZI--—
=
O-
N
bu3
wf
Rate""
Volatilization
�n
In
�n
Rate"
6
6
6
Application
�
bf,
C:>
cn
m
I
Method*
C�
1-1
C)
N.
C-�
Qj
CY
rn
-d'
00
aj
r
uc
—,,i V7
In
c
<71
In
'c
C,7
C)
C:)
C7
C>
CD
C?
C)
4D
Ch
C?
b'O
Cd
CD
CD
CD
4Y
s9J
bl)
cd
I
r cr
aj
U
qjUOw
11
30 111,G,
CL

ON ON
ILI,
�d
PA
u
09)
ci
M
4
0
'A,
w
M,
1—D
u
(Y
'o
cq
ON
ON
4 41
M1
CY
0
0
u
u
u
rx.
Os
0
1 ,
-
-- - —
------
-------
. .....
(4
m Cd
l
CD
qE!
u
f tin.
U
['uEA,
�Qu
�u
.
,l
QS
.
. . . . . .
...............
.......
. ............. .
.....
CA
CD
bb
0t.A
rL
zl
Cd
0
m
I—
I"
lei
Od bg
—'4
r)
fn
�o
\o
lei
C'
r�l
rA
,
E
1 "'
'I.
",
.",
V.)
r)
W)
14"s
Ammonia
c�
✓"o
c>
cl
�'T
'79
ri FF ar)
Nitrogen 0
0�
C�
-J.
00
bh 0
U
U)
C-1)
C"
CD
�D
rD
C)
cl-�
(D
cl"-�
C5
CD
<D
cr, xn
'v car
rq
m
"n
n
m
'i
r1i
r-
lcY
C11
C11
N
N
W�
C7>
C) 03
'-1
N41non,flization
�x-
"
x'
0
LI)
t 0
0
.
�a4
�.7
rn
rn
cn
rq
cn
m
1)
r1i
j
41
Volatilization
lr�
W�
M
0
cli
fo
o. S e'..' z u
Rate"
<D
C5
(D
C>
C) C11 (11
0 *
"; r-� >
r.1l .
E
-------
----
Application
44
cz� C)
Lrj
mehod"
CD C
c r4tom..
t0 0 03
10
V) 0
L)
94
. . . .. . .........
. . ....
11J!
u
-7
H
I-
7;
>1
u
C7
<D
(N
C14
0\
a,
G�
oc
CD
Z)
C7
c—
Z
Q
oo
00
-!
1.0
C9
C')
-�
C�
C3
C)
C7
C�
C7
00
C:�
<D
CD
CD
0
Ca
C>
1=
C,
rj
N
rl
DO
00
oO
C>
CD
0
CI
-
C)
C)
C�
CD
C-�
C�
tD
12)
10
1�41
r-4
co
C;>
C�
(11
"o
00
C�4
11)
lt
kri
C14
�k
cq
73
>
Jo OJUG
Z
t4 Z

Lli
u
Ln
lij
Ll-
bB
44
dmm
u i
�j
ro 0
..0
lz U
X 03
0 m
0
ON
P'm cg Ewa
u u
A4
0
3
U-
LL
0
u
u
;; � L:
. .. ... . ....
JI,
b2
. . .......
..........
> E
5
'A
q
V,
C5
V,
EI
1�
5
1�
V,
qd
(.5
11
11
5
V�
4)
D"
"l
6)
6
W
dlp
u
4)
1i
11 p
..............
.
............ . . . . .
n
m
0
m
4
0,
ON
m
0
"
m
rn
M
�o
I,1�4
�o
r)
G^
In
01
In
0,
'D
r,l
"D
I'l
'D
(,I
'rI
V)
I")
V)
C-4
Ammonia
cp
o
0
cD
q
c,j
q
rl
j
ID
coo oc
-5 C,� rl�
rn, a� r'!
N iti-Ort'Al E'
ON
ON
rl) cyj rn �d-
CA
CD
<D
m
I'D
f,`
C-1)
CD
(D
CD
�0
Z�
r,,.
10
m
CD
(n,
00 In q
10 ON
<71
E
,I
t-
It
rj
;n
11
m
r4
m
N
r)
rl
cl
—
(,I
—
(,I
—
�
Mineralization
I;' ,
;R
0
Rate""
CC
cl cl
m
In
m
C�.)
In
C��
In
CD
rn,
CID
On
C;7a
11)
��n
In
c5
rn
In
Volaklization
In
In
v-1
In
In
In
In
f)
In
v)
In
w
Rate*
C>
C>
C.)
<D
C�)
KD
CD
C:
lkpplicafion
In
Method I *
C10
tLn
V]
V)
111)
V)
V)
U0
Cr
vi
V)
7,
17-
7
Z
7,
Z
Z
cd�
<
. .
.
..... . ... . .
. ............. . .
. ...
. .......... .
.
ON
c
. ...
.. ...........
.............
. . ........
cm
rq r4
oc
In
0
V)
Idd
`a7:1 00
U
es
��D
00
0�
c7N
I'D
O�
-V
c:I
CN
"T
m
c
2
C4
"1
'q-
In
C:)
'q
c�
09
In
C,W
<=�
—
rn
r')
—
'o
1�11
V-�
CD
c.,
—
c�
r-
01
ON
(71
0 1
>
c')
c>
cd
c-D
C-D
6
6
16
6
6
6
6
rq
clq
w
cc
w
=1
m
ff�
ON
I�
C-4
(q
c')
Kev (Z
CD
c:,
C;C
Cz
lz�
c�
c7
ID
I'o
0
cz�
IS
CD
00
) c
It
lz�
fN
C)
lz�
- E
8
I-
0
CL .myrn
oc
r-
10
cy,
rnr1l
In
rq
00
fV
IrI
N
-I-
00
w
10
>
M.
>
qjuow
u
a.I
F-
u
>
0
E
E
E
.10, QJL�-G
e
I
c
,
4-1
Mb
cq
-,n)
r-p
U
ad
In
cl w
IS
c,
cr,
C,d
Rai
10)
ILI
1.4
........... .
.1
",
pp
I
KA E�
bb
(d
0 �
re,
oGf
Lj)
In
OL: a•CSC
jDB
Im
Cd tv
B,
0
ho.
wd
tdl
CIS
cn
o > U CIA
cl 44
ej
41
7;
cri

ik -It,:
o
0
(14
w
0
1
ol
r
cu
411
uw
r-1
04
cm
rITO
u
Ln
La J
LL-
u
�61
bfi -2
.
..... .
.. .
.......
o'
11)
o
o
u
u
u
0
u
J
cl
cm
1. CP
�5
o.C)
U
0
0
"0
4'0
..........
.11L
F1
Z
'z
'z
�
�z.
'4
z
z
Z
7,
Z
Z
M
JI
wry
u
fa,mm
aptI
<
CA , W)
06
. . ....... .
r-
0�
eNj
I—
"'.I'
cn
It)
�O
k-
Csm
Cy�
C-)
C)
C>
C�
CIcy
C)
assz
af
0
Cu
Ch
t—
I—
—
0,
C)
m
CD
I—
C>
CD
-6
Ca
v) bl
U,
QD
ln
110
(1)
ro
Ir.,
r'i
M3
nr C,4
In
a,
I(,)
to
ti
�o
C-�
0
Ammonialry
rg
g
CD
a-,
0
Nitrogen E
o'
01
<t
lt
w
C.
C>
cu
_2
m
m
do
'D
C'.
C14 '�T 0,
. ... .
. . ......
(11
... ...... .
(11
. . .
r'4
......
........
'q
21'
CD
....... .
.
17')
cpsIn
rD
1-1
n
e
rD
C�
�D
lc�
Ratc***
I)
r)
m
IN
------- -- . ............. . .
........... .
CKi
Cam0
volmilizatiol I
'r,
C;�
In
C�
'rI
I"
I,
In
In
In
f:1 > -g
Rate"
C -i
44
Application
m
C/1
E")
V�
V)
CA,
V}
{'n
V)
V)
� Cq rq
Method"
<D cD 01
ell
",d
vo N)
rq m
t
zz4zz4z���
L)
(A
>-f
;te
t
C�
[--
rt
di rjr
Tj
m
m
c D
0
C)
C,
C�
C�
CR
C)
CR
1z'
w
CD
4�
4'o
C>
lu
Or,
V)
0
C)
lz�
C3
C)
CD
C�
C�
0
C.
W)
C14
�
(1)
In
�z
00
r4
rq
0S
OW
M
Cl)
In
CA
t-
m
r
zi
—d
T�
> p
U U
V)
'o
q1uow
z
m
<
0
-15
—LL�L
I,,

il-!
Tj Q)
Z
I
0
(Y
ri
z
.0
rL M
o
Cd
:9
0
I
,rj
,
a r,�, aj
of) 2
CU
ai
aj
-5
a.)
5
n.)
n
v
5
w
:3
u
5
u
5
0
-j
o
�5
In
�A
V�
0
'A
0
,I
u I
Q
Q
V,
(d
'A
U
V)
u
U
u
rP
0
Q
L,
V
U
—
- - ---------
-- -
r—
Cj
z rL
.......8
"2
In
C�
r-1
Or,
w
r 2
C�
c)
4D
Cu0
p
cI
CD
p
C�
0) W o 4
(,I
C,
Ci
<D
Ca
CD
C7,
vj Qj W
M
cl
co
N
Im 4
Z
r
ins 1
A111111011i a
co
CD
CN
I
a,
Id
x.
a rasa CU
4..
>
<D
CD
C>
C:>
C)
C')
CD
CI C>
vl
rn
m
In
�,D
I"")
m
( 'I
V)
r FM
(A
C� ,
TJ 'D
.
.......
. .....
cl
w
Mineralization
C>
CD
Ca
C>
C)
0
44
I,)
ell
M
c)
111
11)
cz
Volatilization
In
In
r)
In
In
In
—
0
IN
— —1 m
W z U
Rate"
CL >
44
Application
FA
U11
C/a
V)
V)
cep
01".
C)
0 0
methop
C) C)
tw
..
........
fA4
-a 0
Ir)
CD m
z
z
,
U
... . ........
CL
U- DO 0�
8 —C,3
C 0�
Ei
u
7�
CID
cg
0
CD rn
-
—
—
—
—
- - - - - - - - - -
dJ—
ri
00
rn
CD
C�
rA
X
C:I
C�
IN
IN
cc
'oc
"0
C)
C�
C,
C�
CL
.... .............. .. .
. ......
C)
0
t'j U
= ,
o
C)
n-
C>
0
C�
1�0Ci
Do
DO
00
C>
00
t-
al
00
C,)
0
73 P.
7j
u L) r
t1juON
>
0
.10 ajpc[
z
71
PU.

CD
12
W
It I)
E
Q�
r4
D.
On
u
u
I
I
I
Ljj
D
u
vi
LU
LL—
I
c", -c�
CI
. . .. . ..... ......
ca
11
7l
0
3
II.J
J
0
7J
11)
-1
0
0
U
0
u
�J
�
r:�
—
•ca
0
u
Q
u
u
,
0
q
o
60
. . . .
...... .......
cj
<
<
CD
0
41
O
O_•CD
—
-7
C�
Et#TMd Z P ,ICE
>
>
>
>
>
>
>
co lu
Cj
n
(L)
o
n
q
is
q
rp
p,
p
CD
V, oj
ci
4L
-�L
Z�L
44,
4t-
-14k
-U,
4t
4�
......... .
C-
�2
Z
F4
Kai
Ammonia
N'
jaiCI a'
bi)
iti
N -ogen F-
Ci
W rn cd u W PL,
6, �u
. . . . . . .. . . ...........
. .
.... . . .. ....... . ...... . ...
<-� —
�>
Z,
VI
C> ell (11
E
r
. . . .......
0' W
Mineralization
u
7 bb
rn
R"Ito",
-4
w
x.
cm
Volntilixmion
cd
6! �V, z u
Rate*
E'.
C�
0
-XI
-l< 0 Ih
.
.... . .......
Pk
Application
C l(— a—
C,
Method*
TI
0
NJ
r
CD
..
. . ........
. . ...... . ...
. .
-
—
—
—
—
—
lz
C/S
CL
C�,
C�
ou
Oo
Ln
7-d
C)
En
V'1
U
C>
CD
C�
Cd
ID
U f7�
CD
E;
E:;
FZ5
C-5
c—;,-
C—D,
>
>
��
>
a
>
a
>
E
>
a
>
>
6
E
Q)
E
o
Q
0
r—)
CD
CD
C-�
fn�
. . ........ W
U
i '�,.
0
0
M L.
CLI
p.
E
>
Ln
(�
c
p2
+,
tpuON
UO
v
0
.10 3113cl
0
u
4,

CD
Q)
0
u i�
uj
7D
u
LA
LLJ
LL
u
2 C?.
c-
x)
blj
...
...... .
Cal
Cva
U
tU
Irl
1�
r�
14
ll�
In
7,
21
2.�
M��
rj"
�.lr�
J�z,,
rl
Q
lJ
<
<
2
�1:
4
;7E',
rZ
Z
rj
C—D"
Fco,
'D
c,
c,
C,
c."
..................... .
441
-#
Z41
Z"-
-it-
4�
qB-
-14-.
4= :
41
4z
L', rm
z
M M
10
Nitrogen Em
06
Cl
. .. . .. . ... . ... . ..... . . . . ....... .
r-
i:� F�
E
I I C 1'il I i 7, a t 0 1l
0
UOl
CD l
�
Watilization
C14
0
6
Rale"
Application
Method"
CD C> CD
n..
ea
...... . ....... . . .. . ........ .
S
:
kc�
ri
..........
rg,
co
-------------
I'D
U, Cc
0
>
a,
>
a'a
>
>
a
>
a
>
>
a
>
>
>
-Q
>
F�
>
F)
r-
>
c-:)
ra
a
C�
C)
CL
.............
. ............ .
In*
>
L)
u
tn'
tiluo IN
co
JO OWG
0
0
(4
j
bb
ca
0
cG bl)
>
0
CL
w�
73
V
0
I

-l" Y F I E L D: 1 3 2, 3, 4, 5, 6, 7, 8 & 1--#,,,

ANNUAL METALS FIELD LOADING SUMMARY FORIW*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Faciffly ISTarne: C11YU1 6KAHA VVVVIV total Dry Tom APPIM.1 (A1111t1M): 30.10
Permit lh, NCO021211 Cation Exchange Capacity (non 503 only): 32,5
. ....... . .
Openalor- CRISPIANT, ROIJ-1-11-. 1 Owner: CITY OF GRAFIAM Predominant Sofl Series: IaB
-------- . ..... . . ..... . .............. .
Acres Used: '7 Acres Pea-mitte(P. 7 Site li: 1 Field fl..
Residual Analysis Data (Heavy Mtals auldTotal Phosphorus usc ing/l(g, % Solids use Raw Percent fl).
.... . ..
.... . .... . 6
0 1 qt2_3
Carts 1 1/23 5/18/23 1 O/23 8/10/23 10/19/23 10/1W23
3/2 1/231 )/)7 1'
posite
Date
% Solids 2.32
-.- . . . . . . . .. .. .. .. ............... . -,
Arsenic 182
Cadftlifflii 334
Leaid
g-ofy-[
Nickel
Selenium
Zinc
otal
Plios-
246
38.6
30.6
0.04-3
5.93
IT]
wW
2.16
871
2 32
2.32
1,79
1.68
1.68
1.90
1,90
1.90
2.82
2.82
2.81
2.98
2.98
163
163
2.63
3,34
3.34
2.08
3.39
3.39
2.56
mm
2,56 _..........._.�.._
156
. ..... .
2416
246
239
264
264
216
216
216
38.6
38.6
40.7
36,1
36.1
34.8
3/1.8
34.8
30.6..-
30.6
23"7
2(a,.9
26.9
21.9
--.3-1.,9
21.9
0.043
0.043
01.056
0,01,59
0.059
0.053
0,053
0.053
5,93
5.93
5,25
7.02
7.02
6.42
6.42
6.42
17.1
17.1
34.4
20,5
20.5
18�8
. ........ . .
18�8
18,8
2.16
2.16
2.81
. ... .. .. . . .....
2.9,8
1 2.98
2-63
2.63
2,63
871
871
685
738
1 '738
73.7
717
717
32,900 1 32,900 q 32,900 1 28, 700 139,900 139,900 1 30,400 � 30,400 130,400
Annual
Heavy
Metal Field
Loadings
(Calculated
in lbs/acre).
T-­
7-
-9
'6 ..... . .. . .....
'76"
.
. ... . . . . . . . .
DT/Ac)
0
App.
.
Event
0,310
0348
1,161
1.069
0,645
0.336
0.,317
0,761
0.222
AjdSejjjC
0.002
0.002
0.007
O�006
0,004
0.002
O�002
0.004
O�001
...... . .
0,000
0.000
0�0010
0.029
.
CadmiUm
. ............................... -.- -,
0,002
-- . ............ . .....
0.002
.
O008
0.004-
0.004.
0,0102
0.002
0.004
. . .
0.001
0.000
0.000
0.000
0.030
Copper
0,153
0171
0.571
0.511
0341
0J77
0,137
0,329
0,096
0.000
0,.000
0,000
2.485
Cliroinitmi
0.024
0.027
0,090
0.087
0.047
0.024
0.022
0,0�53
0.015
0.000
0,000
0"000
0,389
--Lead
0,019
0.021
0.071
0,051
0.035
0,018
0.014
0,033
0,010
0.000
0.000
0.000
0272
mercul'y
0,000
0.000
0.000
0.000
0,000
0.0010
0,000
0.000
0.000
0.000
0.000
0.000
0.001
Molyb-
0,004
� 0,004
0,014
0.011
0.009
0,005
0.004
0.010
0,003
0.000
0.000
0.000
0.063
dentim
Nickel
0,011
0,012
0,040
O�074-
0,026
0,014
0,012
0.029
0.008
0.000
0.000
0.000
0.225
SeleniUm
0.001
0,002
0,0,05
0,006
0.004
0.002-
--0.002-
0M4
0,001
0,000
0.000
0.000
0.027
Zinc
0,540
0.606
2.022
1,465
0.952
0.496
0,047
0�1 12
33 0,0
0.000
0.000
0,000
6.273
-70-tal
P110s.. 20398 21898 76.394 61,361 51.471 26,813 19,274 46.269 � 13.498 0.000 0.000 0.000 338,375
"I certify, under penalty of law, that this doeumentwas prepared under any direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z., 7 - 2c,2'I
Signature of Land Applier Date
�DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Aftacli this Form to tire, corresponding Field Loading Summary Form to be submitted in Annual Report
Fqcifity Name. CITY OF'GRAFIAM Wrl" Total DryTons Applied (Annual); 0,00
Permit 8: Cation Exchange Capacity, (non 503 only): l 6A
Operator- (""R,ISPIAN T, ROUTH Owner: CITY OF'GRAHAM Preftininant Soil series: 'TaB
. ... . ...... .
Acres Used: 3,6 Acres Perflfte& 5m9 Site 9. Field -11:
. .... . ..... .....
Residual.Analysis Data (11cavy Metals �mrd]'otal Phosphorus use ing/kg"!/0 SolidNyasa Raw Per 11):
. . .. . ..... 0 2 ......... . ... - - - - - ---------------
S"wilple or --2
I)OS ite
,Date
............. . .
1Y. Solids
Au-senic
Cadniiuin
Chroinftfln
l,ead
Nickel
Seluiiuni
zilic
Total
Plios-
Annual Heavy
lot,7
DT/Ac./
App,
-Event
Ai-suic
0,000
Cadmiuni
0.000
Coppei,
OM00
Efi-ro;;i-w,,-C
.0-00
T-e-ad
0,000
Mercury
0.000
Molyb-
0.000
denurfl
Nickel
0.000
Seleiiiwil
0,000
Zinc
0,000
Total
Pllos-
0,000
Metal Field Loadings (Calculated in lbs/acre):
--j
2,
E
14
0,000
0.000
0.000
0,000
0.000
0�000
0�000
0,000
0.000
-- -
0.000
-
0.000
.- - . - - --
0-000
. ..........mmmm
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.000
0.,000
0,000
0.000
0.000
0.000
0.000
0.000
0,000
0,000
0.000
-0,000
0.000
0.000
0 „000
0.000
0-,000
-6-00-0
-0,000
-0,000
-0,000-
-0,000
-0066-
0.000
0,000
0.000
0.000
0.006
500
---o-.-000
-a-o 0-6-
-0.000
-O 70R
0.000
0.600
0M00
0.000
0.000
0,1000
0,000
0.000
-6,00-0
-0.000
0.000
0.000,--
0,000
0.0010
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0,000
0,000
0.000
0"000
0.000
0.000
0,000
0,000
0.000
0,000
0.000
0.000
0.000
0,000
0.000
0M00
0.000
01,0010
01000
1 0.000
1 0.000
0.000
1 0,000
1 0.000
0.000
0.000
0.000
0.000
0.0010
0.000
omo
F 0,000
1 0,000
0.0-0-0-
T 0.000
1 0.000
I 0.000
i 0.000�
0.000
omoo 10.000 II 0.000 1 0,000 1 0.000 1 0.000 1 u00 1 0.000 11 0.000 1 0.000 1 omoo 1 0.000
"I certify, under penalty of law, that this docurnent was prepared under my direction or supervision an accordance
with as system designed to assure that qualified personnel properly gathered anti evaluated the information submitted.
I as aware that there are significant penalties for submitting false information, including the passibility of fines and
imprisonment for knowing violations".
Signature of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL IVIE"AL S HELD LOADING SUMMARY FORW
Attach this
form
to the corresponding Field Loading Summary Form to be submiUed in Annual Iteport
Facility Marne:
CITY Ol"GRAHAM ww"rP Total Dry Tons Applied (Annonl):
-Cation
4.78
Permit th
W �. J0­0" 0" 3 8 2-4 Ex"c_1i_ange Capacity (awi 503 only):
1 6 5
Operakor'.
C _111 Ownei. Cn"Y U," GRAH" sciies:
Dl,,)B
Acres Used
4.6 Acres Permitted: 4.6 Site H.. Fick! -ft.
............ . . ........ .
3
Residual Analysis Data
(Heavy Melals and Total Phosphorus use Png/kg, % Solids
use Raw Percent
H.):
....... . .....
smilpicol-
1]
21
3�
7 1 ..... . ... . . . ......
7781 ................................
Com,
X/
Date
Solids
S.
2,32
1.78
1.68
. . ..........
Arsenic
2.82
2.81
2.98
. ...........
Cadndmn
3,34
2.08
3. 3 9
Coppei-__
_-2.46
239
264,
(2111-0111iUni
38.6
403
36,1
-
- - - - - - ---------
Lead
30,6
23,7
26�9
Merctvy
0.043
0.056
U59
. . . .
. ........ . .
MoCI lyLI b­
5.93
5.25
7,02
. . . . ....... .
. .. . .............
Nickel
ITI
34.4
20.5
Seleniuni
116
181
198
Zinc
871
685
'738
...........
..... . ....
ToW
Nos-
32,900
128,700
39,900
..................... . . ...........
L ........ . ....... . .
. . ...... . .
Tinual Heavy Metal Field Loadings (Calculated in lbs/acre):
3
4
. . . . .........
. ...... . .... . ... . . . .
App.
Event
0.059
0.768
0,213
..... ... .......
Arsenic
U00
0.004
0.001
0,000
0,000
0.000
-0-000
0,000
0.000
0.000
"00
0.()00
006
01
11 Cadminm
0,000
. . .
0.003
. . .... . .... . . ... ...............
0,001
0,000
0.000
0,000
0,000
0,000
0.000
0.000
0.000
0.000
7��005
Copper
0,029
0,367
0,112
O�000
O�,000
0.000
0,000
U00
0M00
0,000
0,000
0.000
ChromiUM
0.005
0.063
0.015
0,000
0,000
0,000
0,000
0.000
0,000
0,000
0.000
0.000
0,082
Lead
0.004
0.036
0,011
0,000
0D00
0,000
0,000
0,000
0.000
0.000
0.000
0.00-0-0,0517
Mel-GLHY
0.000
0,000
0,000
0.000
0.0'00
0,000
0,000
0,000
0.000
0.000
0.000
0,000
0.000
Molyb-
0.001
0.008
0,003
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.012
denum
Nickel
0,002
0.053
0.009
0.000
0.000
uoo
0,000
0.000
0.000
0,000
0.000
O.000
0.064
SeleniUM
0.000
0,004
0.001
0, (LO-6-
0.000
R
uoo
moo
0,000
0.000--
0.000
0,000
U00
0.006
Biala
0.103
1.052
0,314
.00-
0 0
)oo
�0
0,000
0,000
0.000
0.000
U00
0.000
0,000
. 0,000
1.469
........... ...
Him-
3,882
44.083
16,997
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
64,963
Llo, us..
4 certify, under
penalty of law, that this document was prepared under my direction or supervision in accordance with
a system designed to assure
that qualified personnel properly gathered and evaluated the information
submitted. I ain
aware that there
are significant penalties for submitting false information, including the possibility of fines and
imprisonment foi- knowing
violations".
Signaftll-C of Land
Appliet,
Date
BEER FORM MFI-SF (12/2006)

ANN UAL METALS FIELD LOADING SUMMARY FORIVI"'
Alftich this form to the corresponding fleld Loading Summary Form to be submitted in Anntud Report
F'acifity Name. i,.l FY OF UKAMAJA VVYV; r [otal M-y TORS AI)PHCU kA111111M)' IV. -IV
Permit 4: W--00212111 Cation Exchange Capacity (ijwi 503 only): 45.0
operntor-, CRISPIAN 'f, ROU"I'l-I Owner,-, (ATY OF GRAHAM 111-001-ninant Soil seo-iesFaB
Acres Used. 5,9 Acres Pei,inifted: 5.9 Site H: Field th 4
14,esidual Analysis Data (11eavy Meilals and Total Phosphorus use inn/kg, % Solids use Raw Pereent -8,)-
m�mmP, 0 ............... 0'1
C0111- 5/1,",/23 1 9/10/23 10/19/23 W/19/231"'
4.5
3/21/23 3
posile
Date
Solids 2.32 2.32
Arsenic 2.82 2.82
C,adniii,un 3.34 334
Uad
Nickel
selenit,1111
Zinc
'I'Otal
Plios-
2,46
3&6
30.6
0,943
5.93
17,1
216
871
246
38.6
30,6
O.043
5,93
17.1
2,16
871
2.32
1.7
1,78
1.68
......... .. . ....
1.90
1.90
2,82
2.81
.
181
.
2,98
2.63
2.63
3,34
2.08
108
3.39
2.56
2.56
............
246
239
239
26zl
.... . ......
216
216
38.6
40.7
40.7
36.1
34,8
348
30.6
23.7
23,7
26.9
21.9
21.9
0,04")
0.056
0.056
0,059
0.053
0.0153
5.93
5.25
5.25
7.02
6.42
6,42
---- -
17A
- ----
34.4
34A
20.5
18,8
18.8
2.16
2.81
2.81
2.98
26,3
2.63
871
1 (Ii T"
685
l3,
73.7
717
32,900 132,900 1 32,900 128,700 1 28,700 139,900 130,400 11 30,400
Annu,all
eavy
Metal Field
Loadings
(Calculated
in lbs/acre):
�Otal
71-
-k�
-7
7-7
TT"""'
DT/Ac./
App.
Event
0,367
0.505
0.689
0.669
0,282
0.066
0.639
0.038
Ai-senic
0.002
0,003
0.004
0.004
01,002
O�000
0.0103
O�000
0.000
0.000
0.000
0,000
0.018
Cadmkiin
0,002
O�O�03
.. .. . .......................................... ......... .
0,,005
O�O�03
0,001
0.000
0,0103
0.000
0.000
0.000
0,000
0.000
0.0,18
Copper
0A81
0.248
0.339
0,320
0A35
0.035
0276
0,016
0.000
0.0010
0.000
0.000
1.550
Chi-oniiuni
0.028
0,0139
0.053
0.054
0.023
0,005
0,044
0.003
0.000
0.000
0,000,
0.000
0.250
--Fe-ad
0,022
-0.-031
42
0.0-
0.032
0,013
0.00 " 4
0.028
0.002
0.000
0.000
-
0,000
-
0.000
-
OA74
memul-y
--�-00-0-
O�000
0�000
-
0.000
0.000
0�000
omo
-
omo
-T-
000
0.000
0,000
0.000
0.000
1vlolyb-
0.004
0.006
0.008
0,007
0,003
0,00 l
0.008
0.000
0.000
0.000
0,000
0.000
0.038
d e2t, iln i-
.-
-,-
-
Nickel
0.013
0017
0,024
0.046
0,019
0,003
0,024
0.001
0.000
0.000
0,000 1
0.000
0,147
Seleniurn
0,002
0,002
0.003
01,004
0.002
0,000
0,003
0,000
0.000
0.000
0-000
0.000
0.016
Zinc
0.639
0,880
1,200
0.917
0,386
0.09'7
0.094
0'0 16
0,000
0.000
0.000
0,000
4219
F23
Phos-
24J49
31229
45.336
38.401
16.187
5,267
38,851
10
0.000
0,000
0.000
0.000
203.730
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel property gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of flues and
imprisonment for knowing violations".
111-1 - z
7 -
Signatui°e of Land Applier Date
DENR FORI\A MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUDAMARY F0JZfW*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
FacflWy Name. CH Y OF GRAI]AM VVVY I V total Dry TonS APP&O tA001HIM)' .)
. . . .. .........
Permit 9; N(-'O(.)2'1 2 11 Calion Exchange Ca pacily (non 503 only), 48.9
opelator., CRISPIAN T� F=1 1-1 Omier: CVTY OF IW-IAM I'll•edbminmw i soil scrks; DbB
Acres Used: 14A Acres Permitted: 14.4 Site lk I Field fl:
Residual Analysisf)ata (Heavy MetaN and Total Phosphorus use mg/kg,
"/6 Solids use 1aw Percent'4)w
7
1
F�
:
7�
T .......................
7om,
�3/21/23
2 3,
3 1r2 10
5/18/23
5/18/23
S�/10 /23
8/10/23
0 il
10/ 1 W23
10/ 9/2 _�J`
()
posde
Date
IX., Solids 1,32 232
. . . .......
Ai-senic 2.82 2.82
ac m i Li m it �3 4
Lead
Mef-CLI
Nickel
Selenium
Zinc
Total
Plies-
246
38.6
30,6
0.043
17,
2.16
871
. . ........ ...
246
38.6
30.6
O.043
5,93
17.1
2. l 6
871
232
1 .')' 8
1. /8
1.68
1,68
1.68
L90
1.90
1.90
192
181
191
2,98
2.98
198
2.63)
163
2.63
3.34
2.08
2.08
3.39
339
3.39
2.56
156
2.56
246
239
239
264
264
264
216
216
216
38.6
40.7
40.7
36,1
36.1
36,1
34.8
34.8
34.8
30,6
23.7
23:7
'26.9
26,9
26.9
2k9
21.9
2 1.9
0.043
0,056
0.056
0 O�59
0.059
.. . .
0.059
.............
0.053
0,053
. . ........ -
0.053
593
5,25
5.2.5
7M2
7.0 2
T02
6.42
6.42
6.42
1711
. ...... ...
34.4
34A
20.5
20.5
20.5
18.8
l '8
18.8
2.16
2,81
2.81
198
2.98
2.98
163
2.63
2,63
-.-- .
871
. ....... . . . ..... .
685.
685
738
738
738
13.7
73.7
717
32,900 132,900 1 32,900 128,700 128,700 139,900 139,900 139,900 130,400 130,1100 130,4400
Annual Heavy
7,7, f - 7�
App,
Event 0.226
Arsenic 0,001
Cadm'imu 0.002
Copper 0,111
Cliromium 0,017
Lead 0.014.
mercury7 -00 0
Molyb- O003
denL1111 Nickel 0.008
Selenium 0.001
Zinc 0.394
Metal Field Loadings (Calculated in lbs/acre):
.... ... .. .
0.546
0.508
0.808
0.101
0.259
0. 109
0.136
0J39
0,462
0.15
0.003
0.003
0.005
O.001
0,002
0.001
0.001
0.001
0,002
0,001
0.000
0.019
E-004
0.003
0.003
0.000
0.0'02
0.001
0.0'O 1
0,001
0.002
0.001
(TOOO
0,020
O.269
0,250
0.386
OM48
0. 137
0,058
0,072
0.060
0.200
0.067
0.000
1,657
0,042
0.039
0,066,
0,0,08
0,019
0.008
0.010
0,010
0.032
0,011
0,000
0.262
0,033
. .. ........ ....
0,031
0,038
0,005
0.014
0,006,
0.007
0.006
0,020
0,007
0,000
0.182
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
0.000
0.006
0.006
0,008
0.001
0.004
0.002
0,002
0,002
0.006
0.002
0.000
0.041
0.019
0,017
0.056
0.007
0,011
0.004
0.006
0,005
0.017
0.006
0.000
0.155
0,002
0,002
0.005
0.001
-2
0.00
.001
0,001
0.001
0.002
0.001
0.000
0,018
0,951
7885
1,107
0.138
0.382
0.161
0,201
0,020
0.068
0.023
0.000
4.330
Total
PlIos- 14.871 35.927 33,426 46.379 5.797 20,668 8.698 10.853 8,451 28.090 9363 0.000 222.524
9 certify, under penalty of law, that this document was prepared under my direction or supervision ill accordance with
a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am
mare that there are significant penalties for submitting false information, including the possibility of filles and
imprisonment for knowing violations".
Signature of Land Applies
7 , "I - 7 n q,,l
uate
DENR FORM MFLSF (12/2006,)

ANNUAL UA.L METALS FIELD LOADING SUMMARY ` RW
Alt«aa:,h this form tea the a~orresponding Field .,Lading Suminary Foran to be subinitted in Annual Report
aaaalit &auataew T"I C � Or �"R�I-1
_... .__._a.... _......__ _..._�.., AM 1yvvV 1 Dry Total Dlcaa1s I)PLICU (�4nnu m):
"
a uaait 11C O02.1 11 t-,jalaoaa Exchange Capacity non 503 only),�.
Operator: CRISPIA 1, ltC3Wl"H owner: CITY OF GRAHAM Predominant Sail ScHes I a13
.
Acres Used; l.8. -_ Acres Penni'tlecl �._. ...m.m �1Y. .._......w_.. Site t7Po.... ( la+"ielalth
Residual Analysis Data (Ileavy Metals sand 1 W44 Phosphorus
Rise Ru/kg, % Solids use: Raw1eree t ff).
Co
31'
31
llS
l2:;
lYil?a
SlI01`
f101'3
1(flJ
( :iroa
111?
Jmsite::
Date
% Solids
2,:3.2 ..
.....
AM.seni
2,82
Cadmium
3,34_
�C,0l)pe1
246
Lead
M ea'e tit
Nickel.
`~selenium
Zinc
.Total ..
Pilos-
3(DY6_
30,6
0.043
5,9.3
17.1
2,16
871
2,32
2,32
1.78
1.78
1.68
1.68
1.90
1.90
2,81
2.81
2.98
2.98
2.63
2.63
3.3 l._._
...��..
-3.34
.mom....
2.08
,,,,..
2.08....
3,39....
3.39...
w,
2 ,56
2.56
246
246 _
239
�.. 239 -W
......264
264
21..6
216....
38.6
3&6
40.7
40,7
--...
36.1
... ......�....
36.1
.,... .......,..�..
34.8
_.........
34.8
..�...,�,�� �.
.. ..
30.6
....... ....._.,.
_30.6
.,,:.,. .. ....
�13.7
�. .....
23.7
26.9
26.9
21.9
it 1.9
0.043
0,043
0.056
0,056
0,059
0,0.59
0.053
0 053
5.93
5.93
5,25
5.2.5
7.02
7.0'2
6.42
6A2
IT 1
17.1 ..m,
3 -l. L � .
�.... . 34A ........
r�..1a 0.5......
_ 2.,05
.....�,.1...
.,63
..�. 18.8
_.
2.16._.._
2,16
2
.� ,81
�....._�.
2. 81
2,98
2.98..
2.63
2.63
871
871
685
685
739
738
73 7
'717
32,900 132„900 1 32,900 128,700 128,700 139,900 139,900 1 30,4001 30,400
nnuaal Heaavv Metal Field Loaadin s (Calculated in lbs/aacre)m
Total
..._w
DT1Ac,i
A pp.
Event
0.055
11 0.387
0.332
0,339
0.382
0.180
0,401
0,59
0.32
Arsenic
0,000
0.002
0.002
0,002
0.002
0.001
0,002
0.003
0.00
0.000
0,000
0.000
0,017
Cadmium
0,006
.......6...O�CM� -j-
0.002
0,001,
0,002
0,001
0.003
0M03
0.002
0.000
0.0010
0,000
0,017
Copl)er
0,027
0,190
0.163
0.162
0.183
0.095
0,212
0.25d
0.137
0.000
0.000
0.000
I A24
Chrornitun
0,004
0.030
0.026
0,028
0.031
0,01.3
0,029
0.041
0,022
0,000
0,000
0,000
_...
0,223
Lead
O.003
0.024
0.020
0,016
j 0.018
0.01.0
0.0122
0,026
0.014
0.000
0,000
0.000
0.152
Mercury
0,,000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0M00
Molyla-
0.001
0,005
0,004
0.004
0,004
0.003
0.006
0.008
0.004
0,000
0.000
0.000
0.037
denum
Nickel
0,002
0M 13
OM I 1
O.023
0.026
0.007
0.016
0.022
0.012
0.0'00
0.000
0.000
0,134
`selenium
0.000
0.002
0.001
0.002
0.002
0,001
0,002
1 0.003
0.002
0.000
0.000
0.000
0.016
Zinc
TO96
0,674
0,578
0,464
�1.523
0.266
0.592
.......................
0.087
_ .............__._.
0.047 .�_
0,000
._...
0.000
0.000
3,327
Total
_
......
Phos-
3,619
25,465
2.L846
19.459
21,927
14.364
32.000
35.81.1
19.274
0.000
0.000
0.000
193.763
)''orals
..I certaty, "naaer penalty oa imv, that taaas aaoeaaanent was prepaareaa unner any taaa°eetaon or supervision in aaccorataance
with as system designed to assure that qualified personnel properly gathered and evaluated the infaaranaatiaan saalaataitted.
<aaaa aware that there are significant penalties for snbanitting false information, including the possibility of fines and
imprisonment for knowing violations".
040
ignature of Land Applies
IMIQ
DEER FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY.I.TOWW'
Attach this Corin lo the corresponding Field Loading Summary Form to be submitted in Annual Report
'11) QQ
.1'acility Name- I I Y U r kil KA, 11 AM vy W�P 101,10 Dry Ions Applied kAnnua y:
N(1002(non 503 oidy). 29.9
1 11afion E
2, Cxchange C,
............ ......... .
Operator: CRISPIA11 T. RO(JITI-1 Owiie#­ C 1, FY 0 F G RA [-I AJIA Predondnant Soil Series CoaB2
Acres Used: 9,9 Acres Pergy10tted: 9.9 SiIe ft. H. 7
........... . . . . . ...... . . . . ........
Residual AnAysis Data (Haway Metalsand 'J'otal Phosphorususe jug/kg,`1/0 SoIlids use Raw Pereent). .. ...
Cone.
3/2 1/23 30, J /23 8/10/23 9/23 10/19/23
posite
Date
% Solids 2.32 232
. . . ................ . ........ . .
At'senic 2,82 2.82
Cadnliunr 3.34 334
Lead
MCRAWY
Molyb-
Nickel
Zinc
otal
Phos-
246
38.6
30.6
0,043
5.93
2,16
871
2d6
38.6,
30.6
0,043
5.93
IT 1
2.16
871
1.78
1.68
1,90
1,90
2.81
198
2.63
2.63
2,08
3.39
2.56
2,56,
239
2611
216
216
40.7
36,1
34.8
3 4, 8,
217
26.9
21.9
_21,9
0.056
0.059
0,053
0.053
5.25
T02
6.42
6,42
34.4
20.5
18.8
18.8
181
2.98,
2.63
1 2.63
685
738
73.17
'73.7
32,900 132,900 128,700 139,900 1 30,400 � 30,400
Annual
Heavy
...........
Total
DT/Ac./
App.
Event
0.164
Aisenic
0.001 ...
­­­ .
Cadi-niuni
. .... . ..... . .......
0.001
Copper
0,081
Cliromiuni,
0.0 13
Lead
0.010I
Mercury
0.000
Molyb-
O.002
denL1111
Nicked
0,006
Selenhun
0,001
Zinc
_0_2_86
otal
8=1
Calculated in
0,164
OJ26
0.198
OA03
0.246
0.001
0,001
0.001
O�002
................
0,001
0.001
0.001,
0,001
0.002
0.001
O.081
0.060
0,105
0,17474
0.106
0,013
O.010
0.014
0.028
0.017
0,010
6-
.00(
011
0.018
0.011
-
6 .666
_
,666
T
0�000
6--o-oo
0,000
-0-,003
0.002
0071
0-003
0.005
0I.006
0.009
0,008
0M15
0.009
0.001
0,001
0.001
0.662
0.001.
-6.036
0,286
0,173
--6.292
O.059
Phos- 10.791 1, 10.791 1I T232
15,800 1 24,502 1 14n957
0.000
0.000
0.000
0,000
0,0010
0.000
LL 0.007
0,000
0.000
0.000
0.000
0.000
0.000
01.01017
0.000
0.000
0.000
O.000
0,000
O.000
0,607
0,000
0,000
0.000
0M00
0.000
0.000
0,095
0.000
.......... . .. .
01,000
0,000
OMOO­
0.000
0.000
0,065
0.000
0,000
0M00
0.000
0.000
0.000
0,000
0,000
0,000
0.000
0,000
0.000
0M00
0.016
0.000
0.000
0,000
0.001
0,000
0.0(0)0
0.052
,
0560
0,000
-0.000
0.000
0.000
-
0.000
0 .007
0,000
1 0.000
0.000
0.000In
0,
()o000
0.000
IJ32
0.000 N 0.000 10,000 10.000 1 0.000 1 0.000 1 84.074
Tif -certify, u nde r -penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for, Icnowing violations,".
7 Z 2-V
Signature of Land Applier Date
DEER FORM MFLSF (12/2006)

ANN UAL, METALS FIELD WADING SUIVEMIARY FORIW*
Attach this form to the corresponding Field 1,oading Summary Form to be subrnitted in Annual Report
Facility Name: CITY OF GRAFIAM WWTP ToW Dry Tons Applied (Annual): 0.00
Ile I-FRI it M., NC0021 211 Cation Exchange Capacity (non 503 only), i o, 6,
..................................... . ...................... ...................
operator. CRiSPIAll T, (tOUTH Owner: Cl fY OF GRAHAM Predominant SCP:1
Acres Used: 0 Acres Pernflited- 15 Site 4: 1 Field 9: 8
Residual Analysis thita (Ileavy Metals and Total Phosphorus use ixig/kg, % Solids use Raw Percent /1).
7 ......................... . . . . .
F7
J)osite
Date
...........
% Solids
Arscris
C-adnifijin
Col)],)er
MUCLUN
Annual
Heavy
Metal Field
Loadings
(Calculated
hi lbs/acre):
m
'Total
[7T­-'_7­­­­`]
2]
1 �4
5
- -
- ------------- -
� �3_j
DT/Ac./
0
App,
0
V
Eveiit
. .... . ...... . ---
------- - - - ---
-- ---------------- ......
. .... . .... ................
Arse,j)ic
000
�000
0.0,00
0,000
1 0�000
0.000
0,000
0.000
0M00
0.000
0,000
0,000
0M00
0M00
............. . ....... ­4__
Cadil7iLL111
0M00
0,000
0,000
0,000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
0.000
0.000,
Copper
0.000
0,000
0,000
0000
110­0
0,000
0.000
0.000
0,000
0�000
0M00
0.000
0MOO
0,000
'ChrODIWIT)
0.000
0.000
0,000t
0
0.000
01.000
0.000
0.000
0,000
0.000
0.000
0.000
01.000
Lead
U00
U00
0.000
0.000
0,000
0,000
0.000
0,000
0.000
U00
0.000
0.000
0A0
Mercury 0.000
0,0100
0,000 0,000
0,000
0,000
0.000
0.000
0.000
O.00O
0.000
0,000
0,000
Molyb-
0.000
0.000
0.000 0.0100
0.000
0.000
0,000
0.000
0,000
0,000
0,000
0,000
0.000
d,eriuni_
Nickel
0.000
0.000 0,0100
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
.0.0100
SeleniU111 0,000
0.000
0.000 0.000
0.000
0.000
0.000
0.000
0,000
0.000
0,000
01,000
0,000
zinc 0.000
0.000
0,000 0.000
0.000
0,000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
Total
Pl7os- U00
0.000
0,000 0.000
0.000
0.000
0.000
0.000
2000
0.000
0,000
0M00
0.000
liorus
I certify, under penalt-y of law, that this clocument
was prepared under iny direction or supervision in accordance
with a system designed
to
assure fliat qualified personnel properly gathered and evaluated the
inforination submitted.
I am aware that there
are
significant penalties for submitting false information, including the
possibility
of fines and
imprisonment for knowing violations".
..... ........ .. . ............... ... .... .. ................... . .................... . ........
Signature: of Land Applier Date
DENR FORM MFLSF (12/2006)

ANNUAL IVIETALS FTELD LOADING SUMMARY FOI?M44
Attach this fore to the corresponding Field Loading Summary Form to be submitted in Animal Ieport
Fa c i I i ty Na n i e: CII Y OF* GRAMM WIT Total Dry Toiis Applied (Atmual):
000
Permit fi: 11C0021211 Cation Exchange Capac"ity (11011 503 offly):
7.8
............. . .................
Operator: CRIiSPIAN T. ROW-H Owner- CITY OF" (,i[W-iAM
Cg--C[iA
........... .
Axres Use& 0 Aexes Pe#-niMetL M Site ft- 1 Field
10
ResidualAnalysis Data (Heavy Metals and'] 'ot,,fl Phosphorus use rng/kg, 'Yo Solids use
Raw Percent
4):
E7
Date
..
. ...... . ......
% Solids
...........................
CadMiLIM
. . .........
COPI)eI.
---
-------------
Lead
---, ...............
.
.....
mel-cu1.y
. .... ........
. . . ........
................. . . .
.... . .
.....
. . . ........
Mo lyb-
... . ...... . .
deiiuiii
Nickel
. ..... .
.........................
. ...... . ..
. .........
selellitini
.
.
..........
. ....... ...........................
. ... ........... .
................... . ......... .
. . . .
. ........... . .
Zilic
........ ..
offal
iaI
.. . ....... ...
. .........
....... .
Pflos",
10111S
Annual Heavy Metal Field Loadings
(Calculated in lbs/acre):
Tiztal
7
77-"'
--7'-
77--
9
1-171
2
.7
......... .
D'r/Ac./
.App
Event
Ai-seiiic
0,000
OMO
0000
0.000
0.000:
0.000
0.000
0,000
0.000
0.000
0,000
0.000
0,000
Cadniituii
0.000
OMO
0.000
0.000
0.000
OMO
0.0100
OMOI
0.000
0.000
0.000
0.0100
0.000
Copper
0,000
0,000
70,00-0
0.000
0.000,
0,000
0�000
0�000
. ...........
0,000
0.000
0.000
0.000
0,000
Chroafluill
0,000
0.000
OMO
0,000
0,000
0,000
OMO
0,000
0,000
0,000
OMO
0.000
0,000
Lead
0.000
0.000
0.000
0.000
0,000
0.000
0.000
0.000
0.000
moo
omo
0.000
0,000
Mel-Cury
0,0010
0.000
0,000
0.000
0.000
0.000
. . ..
OMO
..........
0.000,
0.000
0.000
0.000
0.000
0,000
Molyb-
0.000
0,000
0,000
0,000
0,000
0.000
0,000
0.000
0.000
0.000
OMO
0,000
0.000
dentin
Nickel
0.000
0.000
0,000
0,000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0,000
selelliuni
0.000
0.000
0,000
0,000
0,000
0.000
1 0,000
0,000
0,000
0.000
0.000
MWW MOO
0.000
zinc
0,000
0,000
0.000
0,000
0,0010
0,000
0,000
0.000
0.000
0.000,
0.000
0.000
0.000
Total
Phos-
0,000
0.0100
01,000
0,000
0,000
0,000
0.000
0,000
0,000
0,000
0.000
0.000
0,000
)1101- S
"I certify, under penalty of law, that this document was prepared under my direction
or supervision in
accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information
submitted.
I am aware that there are significant penalties for submitting false information, including the possibility
of fines
an(I
imprisonment for hnowing violations".
U4 -7 2
I. IV 2,
Signatui-e of Land Applier Date
DENR FORM MFLSF (12/2006)

FIELDS, 5, 6,

Expanded Mercury calculations for Fields 3, 4, 5, 6 & 7
. . . . .......... - . . . . . .........
Morcury results as
reported on MFLsr
Mercury resuft as reported by
duet "<" providing errors when
Meritech, Inc. (mg/kg)
calculating
(mg1l(g)
........................ . . .
3/21/202�3
. . .............. . . . ....... . ................ ......
<0,043
3/21/2023 0.043
......... . .
15/18/2023
0,056
5/18/2023
. ................. . . . .
O�.056
. . . .......
8110/2023
0,059
8/10/2023
0,059
10/ 19/2023
0.053
-10/19/2023
. . . .............
0.053
FIEI 03
Using formu]a
Recorded Hg value
I otfl DT/Ac/App.
SLIppfied in cell
As shown to three
Month applied
(m/kg)
Everit
N32 to determirm
decknal placf,,ns
annuM lbs./acre
JANIJARY
.......... 0.043
0.059
0.000005014,
. . ....... . . .
w. 0,000
...........
APRIL
.
0.056
0.768 .............
0,0000860,16
. ......
0,000
. . ......... . . .....
J L) Ly
0.059
C13
0.000025134
0.000
IJ
O,000116224
0,000
Flftr 0 4
Using formula
Recorded Hg value
Total DI'lAc/App.
supplied in. cell
As shown to three
Month applied
(rnqIkg)
Event
N32 to detervyflne
decirnal places
annual lbs./acre
JANUARY
0.043 ..... .
0,367 . . . .....
0.000031562
0.000
FEW JARY
0043
0.505
0.000043430
0,000
MARCH
0.043
OM9
0.000059254
0.000
MAY
0,056
0.6�69
. ........ .
0.000074928
0.000
JUNE
.............
O�056
0.282 .................. . ......
0. 000031584
.....
0,000
AUGus r
0.059
0.066
0.,000007788
0.000
OCTOBER
0.053
0.639
OM0067734
....... . . ..........
0.000 --n—nnnn—
NOVEMBER
.......... . . . . . .. .. .. .. .. ........
0.053
0.038
0.000004028
OMO
-b-0-07-0,308
�-0.00I�

r-'IELD ;
mm,...m ..........
....... .._........... __...... ............._.,
Using formula
Recorded H0 v lui
'Total l l"/Ac/Apj,,),,
supplied in c0
As shown to thiree
Montle applied
(inglkg)
Event
14 32 'to determine
dechn l places
annual lb �.l c'�r
.............�.....�......... ....._.......
,.JANUARY
_
0.043
.._._._ _
0.22.6
.....
0.000019436
0.000
FEBRUARY
0.043
Ol546
�...._..............._...:.w...............m..
0.t�0004ka�56
_ ........ _
0.000_
...
MARCH
0.043
_........ ......................�.mm
0.508
_........._.....
(:) 0004�3688
_ _..__._
(1 C�00
__.._w...........
..__�...
Al`�1-�11_
0.056 ......w.._ .
� & 08 _.
0.00009c. ._..._
_ .. - ._
...lOt _... .
,JUNE
0,053
0.1101
0.000011312
0.000
....._-- 0,259 __..._.0.0000..3.0n
m5..6_..2rv_._.._.._
_._0..000
�.......mm.......
_..... _JC_Y
AICJST
_........_0.059 _
0,059
0.1109
0.000012862
0.000
SEP EMBER
0.059
01,36
.....
.�
OCTOBER
0.05 3 � .
_.. 0 139
0.0000'14 734
0.000
NOVFI BER
0.0� ,
0A62
0.000048972
0.000
v��������
� 01
�. _ ...
__...w_..._
� l���Jl �����
. 03513
.
FIELD
I,Jsinq fcarm.ul
Recorded d Fig value
Total DTIAOApp.
supplied in cell
As shown to three
Month applied
��aaa plc
vet
N32 to deterrvilne
decimal places
annual ltaa� ./acre
,JANUARY _-
_.........0.043 .....,.M,...._...
.,w...,..,0.055 __............_
0,000004730
____ ....._-..
0.000
.�............m._
FEBRUARY
0.043 _a._.
0.,387
0,000033282..
0,000
MARCH
0.043
0.332
0,000028552
0.000
MAY
.. 0.056
0.339
0.00003 /968
-
0.000
_......_...xw.. _.............._
_
J U N E
0.056
0.382
0.000042784
0.000
JI..1l.Y
0.059
.,,,............
0.180
_ _..N ._.. _...
0.000021240
0.000
_a....._p_ _.
.
AUGUST
�......._
0,059
0.401
0.000047318
0.000
OCrTOBER
0.053
0.589
0.000062434
0,000
NC3V�CMl3L=....
.....�....�._.�
0.053
0.317
0.000033602�0.000
ONiVI', =
0.000311010
0.000
Using formula
Recorded Hg value
Total DT/Ac/App.
supplied in cell
As shown to three I
Month applied
(rngi )
Event
N32 to determine
decimal places
annual lbs./acre
FEBRUARY
0.Old 3
0.164
0.000014104 _
0.000
MARCH
0.043
0.164
0.000014104
_ 0.000
MAY
0.056
0.126
0.000014112
0,000
AUGUST
0.059
.,w,w,,.....,.
0.198
'.,..._ _ ......,..,,, ,.,,,.... ..,.,,,,,,,......
0,000023364
.,.. ............ ..,.u..... .......-
0.000
---�
OCTOBER
0.053
0.403
0.000042718
0.000
NOVEMBER 0,053
� 0.246
0,000026076
0,000
qM' =
0.000"134 "7
0A000

c
S2
m
I
00
(D
-0
Co
-0
0 -�a
CD
10 (D
U)
LO
-0
:3
FJ)7
H

ECTION 7
QUAR"I"ERI...'Y SLUDGE SAMPI,,,,,,,ING REPOR I""'S

Meritech,
hic.
Environmental Laboratory
Labmmumy Ceoddudon Nm 165
,'j
Uq)ovt Date:
217120,"?1,
Contan Chris Routh
1l/:-,3/2023
Me= (Wharn, CRY of
NPI)ES0
INQ00H8211.
PAI Drawer 357
PAIN:
CredWrcl
GrAnnq NC 27253
Date SamIde Rcvd:
.....................
3/21/2U23
Meriu-,,ch Work 0ider M 032 12352 WIDE
SkAge Holding Tank
Grah
3/2 1/23
11"'mingim
IsmadIN
MASS 'mt
Mthod,
`34oT4"Aal
232 9a
3/23/23
0-100 1%
SM 254013
Ut-al SmpmWed Soliels
211,BOO ny/L
3/23/23
15 mUL
SM 2540 D
Ammonk, Mogen
<431 mg/kg
3/23/23
431 mg/Kg
EPA 350A
TKN
Z1300 ny/kg
3/29/23
20 nidkg
EPA 3512
Wratc/DJUM, Nivagan
<431 mg/kg
3IZ4/23
W
Aluminum, total
36500 mg/kg
3/31/23
2.S0 rng/kg
EPA 2003
Arsenic, totul
2M mg/l(gr
3/20/23
130 rnUkg
EPA 2017
Calcium, total
1,2200 mg/kg
3/31/Z3
0200 mg/lq!,
E ["A 2003
Cacinhun, toufl
2134 mg/kg
3/213/23
0,200 nig/kg
EPA 200.7
Chromium total
313A mdkg
3/28/23
11M05 nqakg
EPA 200.7
Copper, tow]
246 mg/kg
3/20/23
0.250 mg/l(g
1,PA ZOO./
total
3M6 tail; kg
3/20/23
2,00 indlig
EPA ZOM7
MAgnebunL teat
3540 mg/kg
3/20/23
IaO mWkg
EPA 2017
Mermy, total
M043 mg/kg
3/20/23
0043 mg/kg
EPA 245.1
MulybdenunL total
193 mgAg
3120/23
().S00 Ing/kg
EPA 200,7
Nickel, total
FT 1 mg/kg
3/20123
1 MO tail, kg
EPA 20M7
Phosphmus, total
32900 mg/kg
3/31 JZ3
TOO nIg/kg
EPA 2003
Potassium, toUal
3630 mg/kg
3/20/23
20.0 indlig
EPA 20M7
Selenium total
42,16 mg/kg
3/213/23
2A6 rnWkg
EPA 200,7
Silver; total
1.64 mg/kg
3/2B/2a
1-20 mg/kg
EPA 200.7
Sodium, total
9480 mg/kg
3/31/23
20.0 irNg/kg
EPA 2003
Zinc, total
871 mg/kg
3131/23
0.500 Ing1kg
EPA 200.7
I he eby certibi that I have r-eviewed mid uppime thew data.
mm Lab oratmy Repimmi tative
642 "Parcae Road, Ileidsville, North Carolina 27320
te1,[phone] fin(336)342-1522

ryryry EYR �" x" II µmy" "
ry�
r. arWID
E
y C"
qqk
b-= h
On
;-
.... , V7....
� t
Lu
rr H
1.1.. I..t.V'
_. � �C ,�,.. 0 "� erY rnYa
..,..�..... c ��..�'21
"� .may � �` •e-
CY
rw
M.
ILI
a u
(,
c C" CL w CLQ
CA, ya
" � .�
na
,
CL
eN
........, . »,�.."... .,....�._ .� ' ...,..,,,,. w.. '�,�
{il "'tiiy
bhp lip
.........."
LLJ
uumicr.' d` ""f uti ltA
Nil
� nr c.a i"t ra
+ rr5 ru .. _
EJ
ca_ to
C *}x v qu
an ,
c
c�
.. nr a as a Yyw
2 tlCr
kr u
EE Sy
IM

D
0 0
0 0
0 C)
+
3.,
LH
L'O
tP
wui
Lt
sa
0 Ci-I z
L— C,� UJ
0 W
C4
F-
fy
Y.
LU
LIJ
<
<
Z<
Lij
:E
LU
o
<
Lij
z
C5-
Csoy
t'5

contact: Cris pouch
Rp.porl Date:
6/2/2023
Oierw Graham, City nl
NPOFS4:
WQ0003824,
P.O. Drawer 357
P.R If:
cre(lit card
Graham, NC M.53
Date Sample kcvd:
5/1.8/2023
Merltech WLTrl, Order if 051G23711 Stamplc: Slucloe SLorage Grab
5/18/23
Parameters
Results
Analysis I"D ij
Re.po)rting 1. inijt
Method
IKI Total Solicls
1.713 °/a
5/19/23
0-100 cy
SM 2540B
Fecal Cohlorm
511 C F1j/ g dry
5/18/23
130 CFU thy
SM 9222 D
Mta yilech kVork Orciei' P 05182378A Sample:
5luclge Storaage Crab
5/18/23
paritmeters
R es. uI t
Analysis D_ite
Reporting 17 Limit
Method
%%oral Solids
1.78 1%7
5/19/23
0-100 (%,
SM 25,10B
Total Suspce lded Solitis
14,500 mg/L
5/19/23
2.5 mg/L
SM 2S4O D
Ammonia, Nitrogen
4,900 mg/kg
5/22/23
680 3r)g/kg
IPA 350.1
TKN
25, i00 nag/kg
5/24/23
20 mg/kg
IPA 353.2
Nitrale/Nitrite, Niiropi
<562 mg/kg
5/19/23
562 ang/lcg
L:PA 353.2
Aluminum, total
•11,100 mg/kg
5/26/23
2.50 mg/kg
EPA 200.7
Arscaic, l[ataal
<2.81 mg/kg
5/26/23
2.81 nit;/kg
EPA P-00.7
Calcium, total
1.3,700 mg/kg
5/26/23
0.200 mg/Icg
EPA 200.7
Cadmium, total
2.O8 mg/kg
5/26/23
0.200 mg/kg
EPA 200.7
Chromium, total
40.7 mg/kg
5/26/23
0.005 mg/Icg
EiPA 200.7
Copper, total
239 mg/kg
5/26/23
0,250 mg/kg
EPA 200.7
Lea(], tonal
23.7 mg/kg
5/26/23
2.00 mg/Icg
FPA 200.7
Magnesium, total
4,800 mg/Icg
5/26/23
10.0 mg/kg
F'PA 200.7
Mercury, total
0.056 mg/kg
5/19/23
0.02 mg/kg
E'PA 245.1
Mc}lybdel�um, ic�4.al
5.25 mg/kg
5/26/23
0.501E mg/Icg
FPA 200.7
Nickel, total
3dA. mg/kg
5/26/23
1,00 nlg/Icg
F'PA 2003
Phospllor[ls, total
28,700 nag/kg
5/26/23
2.00 Ing/Icg
LTA 200.7
Potassium, total
5,170 mg/kg
5/26/23
20.0 Ing/Icg
HPA 200.7
Selenium, total
<2.81 mg/l<g
5/26/23
2.81 Ing/kg
FPA 200.7
Silver, total
<1..10 mg/I<g
5/26/23
1.40 mg/kg
EPA 200.7
Soclium, total
13,600 mg/l<g
5/26/23
20.0 ing/Icg
IPA 200.7
Zinc, total
685 mg/kg
5/26/23
0.500 Ingftg
EPA 200.7
I hereby cei-tify that I have reviewed and approve these data. 'AlKh(-Ho_ un "'2a ,
Laboratory Representative
642 'i anico Road, Reidsville, North Carolina 27320
tel.[phone] bx.(336)34Z-1SZZ

27
> 0 0
0
q)
Z.1
ul�
C,
Te-2--
In
CL-
ul ru
LL
7V
"Z U,
( A r 75
( IL�
CV
ro 71
'If
Ca
O
di
lb
I'D
!LJ r w
rg,
Z
cc o ru cuin ro
amwm
.6 1 Ln
ry)
m m m
(Y) ca-
u
0
I -Jo
u u U bf
D
tw
0 uj CD ej
v
u E SO)
0� F- uj (7)
amm
ru
0 cc z
4-1 0
LU 5
E LD (0
44-
(v 0 Gj
>
0 LAJ E
Q)
M
-C _0
ru C,
93-
0 0

w
5
C,4
CD
UJ C-)
LJ
UJ u
< <aC
Lij 0-
I—
W
UJ
M
UJI
�j
0
LX
w
SO
U)
LL
Lu
<
Yll
<
LLJ
Co!
GAF
LAJ
........ .. .
ry
0
LLI
LD
y aW
F-
L) 'o u
<
�,A
0 (D
.-J -C =
0
0 CL
0
C)
7- C—
E
=0 E
: 2
<
,
R
ro T
Of a)
ui
CU m
0 U) U i=
z

h
Meritech, Inc.
Aal Laboratory
jtip r
L,,abovatory ("eafficabon No, 165
C'onlmct: CrO.; Routh Repoi,L Date: 8/2 1 /2023
Clielit: Graham,City of Nl1DJ.,,:Sti: WQ0003824
P,O. Drawer 3,57 Ro� iL Credit Cud
Graham, NC 27253 Datc Sarnlc Rcv& 8/10/2023
fAcritech Work Order il 081023156 Runplc�: Sludge SLorage Grab 8/1.0/23
Llanun Qu,-us, —RQ 1 d4 k-a1,vqjLw ( _p �,py,[JDZLk� I i L IM-!Ih Kid
130 'yo B/"H/23 0-100 1% !S M 151l01,
Fec".11 Coliforin 2,674 CTU/ g +Iry 8/10/23 130 CFU/ g dry SN 9222, D
Merituch Work Order 11 081.0231 56A, Saaiple: SludgeStori.,qg 8/10/23 .,e Grab
IMOTotai Solids 1 ,68 % 8/1 1/23 100 'yo S 10 2S4 0 B
Total Sustmicicd Solids 16,700 9/15/23 2.5 rng/ L SM 25'40 D
Arnmorda, Mtmg,(,,n 4,420 mg/kg 8/1.4/23 (a80 nig/kg E, 1) A 350.1
TKN 23,600 mg/kg 8/15/23 20 mg/1% EPA 3S3,2
Nitrate/Nitrite, Nitrogei 595 mg/kg 8/16/23 562 nig/l(g EPA 353.2
AILMIiII11M, tOti'll 51200 n-ig/kg 8/i/1/n 2.50 Ing/ki-, EPA 2003
Arsenic, total 2.9 8 inn/kg 8/14/23 2."-)8 Ing/kg EPA 2003
CalcJum, total 1-6800 1a11/11 8/14/23 0,200 mg/l(g EPA 200.7
Cadillk,1111, total 3.39 8/1.4/23 0,200 ing/l(g EPA 200,7
Chl'0111iU111, WWI 3 6,1, mg/kg 8/14/23 O.00S rang/kg LTA 2003
Copper, total 264 mg/kg 8/14/23 0.25O mg/kg EPA 200.7
Lead, LuLal 26,9 nig/kg 8/14/23 2M mg/kg I-,, 41 A 200.7
maj."llesium, total 54,60 mg/kg 8/1,4/23 10,0 mg/kg EPA 200,7
Mercury, total 0. 0 "'S 9 11,11;/1% 8/15/23 0.02 mg/kg EPA 245A
Mo�ybdenuni, total 7.02 mg/kg 8/14/23 0.500 mg/kg EPA 20U
Nickel, total 20.5 rtig/kg 8/14/23 1.00 mg/l(g EPA 200,7
Plata rphorus, total 39900 lllk'/I(g 8/14/23 2,00 mg/kg EPA 200,7
POLW641111, total 5770 mg/kg 8/14/23 20.0 mg/kg EPA 200.7
Selenium, total <2"98 mg/kg 8/111/23 198 mg/kg EPA 200,7
Silver, tool 2A-4 mg/kg 8/1/23 1,40 1aag/1% EPA 200.7
SOChU111, total 1,8400 mv/kp, 8/14/23 20.0 mg/kg FT A 200.7
Zinc, total 738 mg/kg 8/14/23 0.500 log/kg F' , 1) A 2 0 0.7
I hereby certify that I have revievve(I and cipprove these dtita . ..... . ..... . . IMI_ 'UT jla
Labor atoty Representative
642 Taincu Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]S22

_..,.:..
N
�i I
wi
..Q.
�"�a�" w v,�..:�.. ". "a ..N
LI
C. N .... . _.,,,,.... ... _ .. I .. C ...
f,
I GO M �N9
4
ry f "f f fM
_
f 1 .&1
✓"' ti �. I l 4 C'M1u � c
,. A
la
�J
CIL
G�� cup
i , 0 NN
La. a
Tj
+l.r T7 NM
uLn
J...,
rz
12
e�
c N r k P � 'cc
.J t' aN c I
<NJ
o cv,1 a . "
Cap
fN.Y r afi L7 Q R..3 Y
C 1 u twi
U.1 CD
C.:J it"Y f" C r
t U cj ua r ca
CMOM
0 a:r. U`pia 1 y e
min >
"a:,U.J �u
mkC tt1
uj
to
woml,4-10 CJ r~
M „.

Pr
o
/J
z
LU
M
< u
w 'Y
z
LL LU .
0 w u I-
tJ
ICU,
w M
uj
cr
i uj
LI)
C) in
Li
<
P z
<
CL
uj
flF
LD
CU
t5
LLJ GlY
0 (1)
0 q) 0
-a t
w
0 rL
E
Q�LU
m 0 E
0
0 w 0 F--
z

Merited, Inc.
Environniental Laboratory
t.,abovatory certificatiork No, 1 (56
Chris Routh
Rupw Mw
10/27/111-1
Cliun: Gr�llmnl' City (,)I'
tj P [) t"S fl, �
" C
Vv 0 � d 2 tiJ'
PHO:
Credbt COrd
G
S�HKPI(x Rcvd:
10/1 9/202�,
Meritech Woj-k Mer R
101 WWI Somple:
Sludge Stor�:ige
10/19/23
Piu�m-'I—ecs
&NUILS
Malmia-rh'U!�
IYIj Tolill c7Nadla.l
1.90
10/20/23
0.- 100 NX)
S N/I 2 ,� 4 0 0
TOU11 SLISJ)(Alded SOlidS
15,900
1(112412.
2's mg1t,
sm 2,5410 D
AmmonQ Nitrogm
<526 rig/kg
10/23/23
526 ny/kg
EPA 3ST1
Fecal CoMmi
3 9 2 niglkp
10 / 19/ 2 :'°,
20 1Nad / k. g
F-', I'A 35 1,1
TKN
k 2,300 nig/1'af
10/24/23'
20 kj?
Nitrogeii
<526 mg/kg
10/24/23
526 mg/kg
EPA 353,2
Aluminum, Lotal
41100 aT/ kg
10/23/23
250 mg/kg
[,'[)A 20U
Ar!,,.cnic, lot;.fl
<163 mg/kg
IO/Z3/23
2,63 m�
DIA 200,7
CWdunL mud
1d,}300 mg/lq.
I O/Z3/23
0.200 mg/kg
l,JIA 200.7
CadndunqtMural
2.56 mg/kg
10/2A/23
(1200 mg/kg
IIIA 2017
Chrowhim, total
34.8 mg/kg
IO/Z3/23
0,005 mg/kj-',
[l,'PA 2003
Coppen too
216 rng/kg
10/23/23
0150 ny/kg
EPA 2OR'7
Lund, total
21,9 111 g/kg
10/23/23
2,00
HTA 2 0 0. 7
MapneMunn total
4,980 n1g,/kg
10/23/23
IRO mdkg
EPA 20(17
Mermy, total
- 0 5,3 mg/kg
10/23/23
0.043 m'g/kg
d l"A 24 5. 1
Molybdenum, toW
6A2 mdkg
IO/13/23
(1500 ny/kg
EPA 200.7
Nickel, total
18.8 nig/kg
10/23/23
1AU inWkg
EPA20M7
I'll losphorus, WU-ad
:3 0, 1 t) 0 mg�/kg
10/23/23
2.00 mg/l(g
I �A`A �2001 � 7
PoLassiL.1111, tOtal
SA40 nW/kM
10/23/23
M ;ndkg
EPA 2017
Selenium, total
<2A3
tO/23/23
2,63 mg/kg
EPA l00.7
shw4toml
3,58 mg/kg
10/23/23
1.20 mg/lo",
VP A 2003
SO(HUM, total
11400 mg/kg
10/23/23
ZOM ludkg
EPA 2017
ZNq total
73,7 mg/kg
1.0/23/23
M500 mg/kg
EPA2OM7
hmvby cmlqp fdhot I 1mve reviewe(I aml approve these elaut,
Lciboratoty Representative
642 Tamco Road, Reidsville, d' og,tjj Carolina 27320
tel.[phone] f'ax.(336)342-IS22

21
0 C)
CL I
C)
L- LL
Q—e
4L
<
im
Ln
w
Cf)
Fc
-
Z
C)
W)
ru
comma
LD
rel
-0
—
r
X:
0
u
13
CD
u
co
'S
tD
rr
44
cz
17
E
'17
IA
QO
ro
V,
oo
CD
CL

if
uj
T, z
<
. . ..... . .
(L
CL
LU
I w
-6
<
-6 .2
a)
15
z
<
LLJ M
Lu
a) ca
0
Ci
F
T
cl� ui
�--
w aD
z
q'i

is-

c) c') 0 (D
0
Cj
cq
M
ce)
0)
0) C.) 0 a)
W
(N
Q)
fl-
0
Ill-
Nt, En M
Li)
CA
0)
03
CD
04
to
M
If
'n W"s
S,n
cm w (j)
m
ol
(.Y)
(,u
0)
OR z u
CIL
......
..........
co
..................
LLJ
w C") 0 C
C"�N
-
Cr)
LO
'-Nt'C)
00
Ur)
(0 0(-)(()
C`J
r--.
ul
a or 00 V
0)
CA
V-
CAS
cq
W Q0 00
C)
(YD
(3)
Q-)
10
13
V- T-
01
CA
LIJ
11
cs
U
1
L----------- A
0.
Lu
ce
m
0
40�()
d
U)
al
M
M
(Ti
0)
z 0
z
u
12L
0
LLJ
ST
— - —
— — — — — — —
-------------
---
...........
co
7-0 37 COD 7-07 73
a.)
(r)
—i-
m
I-
0 0 C)
(D r,- 00
0 .
(X)
.
74, .
V) .
= .
0 .
cq
(Y)
U)
0
N
I-
E
0
CA
't
(mm
Ck)
cq
CY
C6
-UO)
D-
cr
cr
0) CD o)
E
E
E
C
z u
w
co
iz
0
w
.......
........
........
--
......
XC3
cy Q CD CD
Q
cy
wt
CP
M
4-
"I
CA
Co
It-
05
q 65 cD Or
(N CD CN 0)
0)
co
v
CA
C)
W-
Ni
Q6
04
00
00
C4
rm
4.
w
m
a CD
-6)
-
0-
CT
11
I —,
0) 0)
E
E
E
E
E
E
fp
U)
Cu
(5
CD
m
cu
0)
z C) >--
z
()
2
z

91 a* �C

meritech, ftix.
Environmental LaNwatory
'qn
Laboratory CeitiRcutlon Na, ITS
;bra'
SO W
COHMCQ CHS Row 11
ChCiW
NPDF""� (L
W Q 0 0 0 l ('? 1)
11, O. Dr�-twer 357
Gndwm, NC 27253
Dwe Smnme OWL
I U/ twm:-�
Meritech k Or N 10 192310)
SanqAW Sodge SuUmme Qab
19/20z:1
"I"CIT, Metals
. . . . ........... ... . ...... . .. .. . . ....... . .... . .... . .....
Wawa Amaxla Vaig VaLLAR L ulhi Mediml
Arsenic
<OA 00 ny/L
10/26/23
(), I () (:)
"i.()
F'PA 20W7
Rmourl
0.107 n ig, / L
10/26/23
0050
1 () (). 0
ill" 200.7
Cadmkm
< 0,020 nig/l,
10/26/23
0.020
Lo
L, 1) A 2003
Chromil'Im
<0.050 I I'l g, / 1"
10/26/23
().(6S0
FJ-1A 2003
Imad
<OA00 nig/t,
10/26/23
11.()()
50
1,1'7120 0.7
Mermury
< 0' 0 2 0 n1g,/1'
10/31/23
().lip:()
0.2
EPA 24-5.1
Selenium
<OA00 nig/k
IO/Z6/23
(1100
1 J)
HIM 2001
Sover
MOS ny/L
10/261Z3
OM05
SA
EPA 200,7
............
. . . .......
TCLFI Orgarfics
.... . . ... . ..... . .
Result;
Xnalylks Rate
un A
blud
VokOks H260
MUa(,,'Iwd
10/27/23
8260
S(-, rn i V ) 1, R 27 0
AtMched
11/2/23
U270
MACAW
.... . .... . . .... ..... .... . . . .......
Parameter R Ls iflu>, A-Aal �l —Si s. L) att IVI e hli-d
(ja&dq Wal
M500 mg/kg
10/24/23
V300 IvIg/lig
LA I A 3 3 5, 4
Sumde
<110 mg/kg
10/21/23
110 mWkg
SW M 9038'
Ignitabilhy
>140 T
10/26/23
EPA 1030
("ol-rnsitivity (J)H)
6.4 SAI,
10/20/23
11) - 14M & U,
SM 4500 1113
6421'awiwo Rimd, Reidsville, N()rth Ca t,oliina 27320
tW133q3424148 bwj33qa4Ol5Z2

Meritech
a
Environmental Laboratory
Laboi-atory Certification No. 1€ 5
Page 2
i�epoil Date: 11/6/2023
NPDES #: WQ0003829
Graham, NC- 27253 Date Sample Rcvd: 1.0/19/2023
Mci-jLech Work Orclej- ff 10192329 Saml)le: Sludl;c Storage Grab 10/19/2023
Pesticides Herbicides
Pesticide - SW-846 8081A
Parameter
Restaits Analysis Date let. Urnit -1 nnjt. WIL1601) Factor
Amic.hecl
Chloixiane
Attache cl
Toxal)hene
Ataac°hed -
Methoxyc..hlor-
Attachecl
l-lej}tachlu]"
Atladied -
Lindane
Attached
Herbicides - SW-846 8151A
Parameter Results analysis Hate Let. Limit Ree. Limit Dilution Factor
2,4-D Attached - -
2,4,5-TP (Silvex) Attached
! hereby certify that f have reviewed and approve these data, CZ)
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

(lie1w
[ToJecL
M E., RITE CH, INC.
Environt'riental Laboratories
1'.rAbw'Mory certilicate', 8165
C it ol'Gulham WWI 11
fl 0/ 19/23
10 192 �129
volntHes� M%/-'44(� s?('O
Anol ' v!'Js. 10/2 7/'2,
1 ' ml rIciow
10/23/23
Arollyst� v W \1
Kcporl Daw:
Parameter
Resuh
tjIlits
DO, Limit
Ref", !JH6l N111flon Unclor
Bell/k"ne
< 0.0 100
11 ng/1'
OM 100
0,30
("'m-hall Teiradihm-idc
OM 100
nl�/I
0. 0 1()()
0 () 10
('Worobc+ lxene
OM 00
nwd
100
100 10
"Ifloi ol'orm
0 0 00
lilp/1'
WO 100
6'0 1
< (U) 100
Mg/l'
0.l)100
0, 50 111
(W 100
Ing/L
100
1) J () I
Mcillyl D11.0 Kelmic
(). 100
111VA,
O.V00
200 1
OM WO
mufl,
0.0100
0,70 1
< 11,0I00
n 110
(M) 100
0,50 1
vinyl (,°hkwi&
0.0200
111g/1'
W)20
0,20 Ill
Send- Vola I ilvs. S'W-846 8270
Amdysi,s: 11/02/213
"'W"acllon:
10/231:73
Anulys,l: I I M
13C1101-1 DUIC:
I
Panillicler
Residl
Units
DO,, Limit
13, c i I ql i Dillifilill Vactor
IA-Dividon)[minne
00
I'lig/1'
100
7.5 1
0,100
lvg/l
100
(). 13 10
I lumlelfloro- I '14xilticlielle
<1). a 00
mg/�
C),I () 0
0.5
I leuk"111or(wth"11W
-Ol 100
Ing/L
O.10O
3.00 Ill
O-CIVS01
O. 100
111gd.
100
200 1
1116,11-cresol
-.0,204)
1) 1 V/1 .
0.200
200 1
TOU'd CWSOIS
11,300
nigil,
0,300
200 10
Nkrobenzene
'� (), 100
ing/1'
(), 100
2,00 k 0
I ImInclOoropl wool
<0.500
11qfl,
0.500
100 it)
Pyridille
A. 100
100
5,0 10
2,4,5 -Til ch Iurw yl ienol
-10, 100
mg/Ts
t1,100
400 f0
2,4,6-Trich loroplicnol
<0. 100
mg1l
0100
2.00 10
2"1 DinitnmAUCtIC
ti.100
nl�/[
100
13 1Nl
I hereby cedijj� lhuil ho iv re
viewed and eippro ve
Mese loll).
Laborwoiy RepresciHafive
64,2 "I'anico Road " Reidsville, NC 27320
(336) 3424748 " [e-mail]

w0ft2 l, 102 08
3.41G1 Plain St.
CuY,dwgxj PWA,
Ohie), 44,223
[)Mv Ropoikkt;
10/277DQ3
253,1"JI ; VJX,
(33Q), 253-44,0
C'm npail,v: IIvlcrilvcdl
RcwckvIlIo Nt
120
ece, i vet
'Heit Dfl
L;d) IDN
CoHITted Awflylv
Rep Imit
Pxsulf T.Jults
,hull -is
jNJ CG I I G) (1
1)17
Rmi
A n i lys
10 1323,3 1
µArt 002
10/ 12/2023 Chlordamd, tolal
5,00
N 0 pg/L
Sludge GVUV
I..-.'I'A 808 1 B
2
30,0
M27/2023
PGP
10 132 3-3 1
002
1 Oil 2)2023 1 cxaj:)henu
'10.0
ND pg/L
Sludge
EPA 808 1 B
2
500
IW2712023
F)GP
I U 1323-3 1
002
10112/2023 [:Indi in
I R)
ND lig/L
ISI udg e,
E PA 806 1 B
2
20,0
10127/2023
FIG
10 1323-31
002
10/12/2023 quwma-1311C
1,00
NO jiglL
SILW�JUI
EPA 8081 B
2
400
10127/2023,
11 G F�
10 1323-31
0021
1,00
ND Ij(-IIL
Skidge,
CPA 808 1 B
2
800
10121/2023
P(",I"
101323-31
002
l0/12J2023jIopIachloi elmxklk.
1.00
ND puft.
13,kidge
EPA 8081 B
2
UO
1007/2023
PGP
10 13,23- 31
002
10/ 12)2023 (001 mxYcHoi
'I "00
HD ligh-,
slivk)e
F,"ID A 608 1 B
10000
1012'0202:3
PGP
I'(' L V
11 c rb i c ki cs
liem I DP
LAb MIJ
(:0II4AA(41 /XWdVIU
Rvp L.Int
Rusuli UIIHS
Matrix
M ethud
DF
Reg -I'd
Rim Ana(vsj
10I311".13-JI
002
10/12/20232,4-D
(Wiou
ND myll-
Sludue
EFIA 332 1 B
1
U.) 0
10/2612023
MIG,
I U l323-3 t
002
W/ 1 2M231 2,4,5-1 P
0.0100
NO niqlL
;Iudqe
IPA 1132 1 I
1
1,00
10/26/2023
MIG
(livill ID#
Imb IDH
("4111cded AlWyle
Rup LaA
Result Lluik
)VIntrix
Alldhod
DF
Rim
Awl dysj
101923-29
003
1
NO L
lig/
SlijPA
81 ID
2
30 0
1 0/27)202,9
F'(,r F'
101923-29
003
10/19/2023 Toxaphene
1:0,0
ND Jigh
Sludge
EPA 808111
2
500
1012,7/2023
PGP
—1(1j923-29
003
10/1912023 EndrIn
1.00
ND 1,#L
Sludge
EPA 808 1 B,
2
200
10)27i2O23
PGP
10 9'Y3-29
003
1011912023 garnimn-13HC
-smO
N1 I pg/L
Sludqc.I
EPA 808 11)
2
400
10/2712023
FIGP
10192329
003
10119/2023 Fleptaitior
1,00
ND lig/L
Sludge
EPA 8081 U
2
8,00
10/27/2023
PGP
101923-29
003
10/1912023 Hoplachlor epoxido
1,11tD
NEI li g/ L
Slu(We
EPA 8081 B
2
8M
'I 0/27f2023
PPP'
101923.29
003
10/ 191202 3 MelhoxyO dur
1.00
ND jig/L
0a
SIu(R
EPA 808 1B
2
10000
1 W2712023
PGP
TC1,11
I I c rbie id es
("HeIII, ID11
Lab IDY
Colleded AmMytt,
Rep I"nif
ReaM Uldis
Mi h ix
Nit,thod
OF
RcgLv�
Run
Analyst
10 11923-29
003
10/19/2023 2,44)
0,0100
ND mg/L
Skidge
EPA 83216
1
10�0
IW261202'3
M"rG
101923-29
003
1 D/ 19/2023 2,4,5- TP
00100
ND ing/L
Sludge
EFTA 83218
1
1,00
10126/2023
MTG
Page 4 of 14,

E
f]
fV
_
O
7
a, uV
�._
-
�
m
UA
Cl-
ct
i
r
x
L
`
..
a
CL,
CU
-�
<.
QJ
O �•- _
S.7
r
®,1
h--
+
v
cz-
aj
F
m
rn
u
G7
m
M
n
(�
ca
a?
u
cv
Z3
O
aj
F
Eto
u
Q
�
.2
r
a
r;
n
V
�n
91
is
,
Q
Ul
ni
)
4
c
ty
ti
b
n
y
v
r9
lu
w
.
a
c
�
ar
ci
r
ci
�-
of
n
„�
a
c
�
o
_
�
D
m
doat
0
n
cl
n
Q
�
C�J
y
a,
x
u
v
r-
cn
��
to
ai

22. X114 KOM" x I

C� T-Y OF GRAHAM
WASTEWATER TREA]"MENT"PLAN"I
GEOME rRIC MEAN CALCULATIONS FOR Sl
1503 B
FIRST QLJARTER - 2023
DAIT
RESU LTSJ��9�19.!.N)�
. . . ................
UMTS
% DRY SOILIDS
March '14, 2023
6060
CF'-[,.J/g dry
2,40
March '15, 2023
5237
C',I'"'U/g dry
2.4.3
March 16, 2023
1 735 5
(",FL)/g dry
24.2
March 21, 2023
5161
CFLJ/g dry
2,29
March 22, 2023
6577
CFLJ/g dry
2,313
March 23, 2023
13462
C.FU/g dry
1. 56
M a r c h 2T 2023
13242
.. . ........
CFU/g dry
�2191
GEOMETRIC MEAN
3547
CAFE /g dry
2.23

Mentech, Inc.
Envirolu-nental, [aboratory,
Laboratoty Certificanon No, 165
Ow
Cmdact' Ci-is Routh
Client: Gi-ahati), City of
P.O. Drawer 3,5­7
Gi'ahwii, NC 27253
Mei-itech Wor'k OnJei- ff 032/1-23164 Saniple: Sludge Storage Gs,-ab
ljal:g AmtUe-u'; Re *WLs Aitaly�ds.-Ua —LQ
" Yo Total Solids 2A. "/0 3/16/23
Fecal Cofifot'm 6,060 CFU/ g dry 3/14'/n
r�cj--rw-L Date: '3/23/2023
NPDFS-ff; VVQ0003821
P. 0. 11- - Ccedit Caj'd
Date Samlfle� Pcvd: 3/14/2023
Bggg!IJ [j][TIA
Method
0 100 % SM 254-08
130 CFU/gdiy SM 9222 D
lherebycertify that fhave reviewedand approve theseduta. U,r z"'
Lahorafoiy Rep resen ta live
642 Tanico Road, Reidsville, North Carolina 27320
tel,[phone] fax.[phone]

y
"T"
f
e
LO
cz
Vi
y
a,
�
.:=_ �^-�
✓ � pp �
�
...mod " i
u....
i.,
O
Y5 n.
Y
_ rcl
m
4E
0
?
>
-TT
mz
I
w
Oj
Ai
U Q
Q
c
V L7
m Q
0
O
Q m
10
c
U
m El
0 rf) m t C)n
o
Q
°,
©
< w r
`
o
'—' Lf
C
Q
a
rro
-
to
0
ai
taa o
m ra
o
W
O
®
uj
Eea ui
Q
+�
~
u
ro
x
us
p
IL
fl
v,
v
1
Q
u_
Cj
a
Ml,
c,✓

Meritech, Inc.
W, 04
Laboratory
Lzboratory Certification mpS
Conracl! Cris Routh
Report Date:
3/28/2021-i
Oicmt: Grahani, City of
N P 1) E S Iff :
WQ0003)824
RO. ffiawer,3L—
P, 0. 9:
Credit Card
Grahaij'i, NC 2725""3
Date Sample Rckd:
............ . . ...... ...... . . . . ...
3/15/2023
Merited) Wurk Ordet k, 0 15231.12
Sample: Sludge, Storage Grab
A ,1 sisfa'c
Re pr..Q C t 1 n _- FTM�ilpnft Method
%Total Soicfs
243 %
3/16/23
0 - 10 0 0%
SM 2540B
Fec,al Coliform
5,237 CF1J/ g (Iry
3/15/23
130 CFU1 - chy
SM 9222 D
I hereby certify that I have reviewed and approve these data.
W.cu
Laboratory RepresentatNe
642 Tamco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

\;
V
—
n
fro
� ram'
'-1
u
�
O
r •
' -
P -
�
--
.�
f-
.ri
w IV
L
N
fG
r
u_
u
c—I91
_
'-
a
91
aj
Ea.
cL
Ln
�......� ...
❑.,
7 17
'A
..Q
.Q
N
N
C
C
. L✓
C
-F+
U
Y
U
C`
ui
na
ri
c
a
Qj
'C
m
pa
m,
1
ts. rrl m u1
0
I
�2
u
ab. ® m rn �
Q
o
cc ej
O
,.14
V
f Y L C J
•
Q
cL U- aj
.
Lujp?�
ai
LU Q
Ln
r
j1
rev -
1
�
a �
_
>. aru
II
61
pJ
W
C
u
�-
a
O
�
o
w
cu
a
t:
L
D
ri

IVIeritech, Inc.
M
mill
Eiriv wommental, Laborator 1
LaboratoT,17 Cero Fic.atifmi, No, 1,65
(­m-atoct, CHs Routh Repoa D,--ae� 3/29/2023
Chent: Gi-Liham, City of NJPDFS-lf: W(,�003824
11.1 C -7
vlO' D 1�Awk� F ja P'O' M � &edj I: Cal-C]
Gi-ahatn, NC 27253 Date Sample t-,mid: 3/16/?0?3
Me�ltcchWork(.')a-cier it 031(,23215 Saniple" Sludge Stouage Grab 3/16/23
L 2 —r a ri, Li t L,,-; Result
Analy�Ls Dgg R ort Mell-iod
IN Total, Solids 142 'Y6 3/17/23 0-100 % SM 2540B
Fec,-A Coliron-ri '17,355 CFU/g&y 3/16/23 130 CFU dry SM 9222 D
I herebY certify that I have reviewed and approve these data,
Lahoratoyy Representative
642 Tanico Road, Reidsville, North Carolina 27320
tc1.(336)342-474.8 fax,[phone]

P
y p
Qu
d` r4r '1 n 01
��
�M
r 4 f 4
_ y\
731
C rn I
r�
,w
V r R I 0 Ul
rr
. Q..k" 3
w P
CU
7.3
Im
vi
C
f p M)q
c ry L
o .. 4' F ri
" C.S.. lJ
as 0,
Q,7 ai { r�
LL
rN c ,
r' 8 = CU r r
r
� , -0 C
,� u✓uo-,� tel rra _.. _._.... .�.....,. .�... ,�. n C
CLL
UJ6�
LLJ
wmmm
C r.
�p v u „lamQj
ra V.)
� "~�... m
"' CJ T{ .
y� i,J r p S CL8 uCl
qJ
LoL7 D k—I ���.
J ,..

C ,
wInc.
Environmental Laboratory
atory
Laboratory Certification No. 165
r ram:
Contact: Cris Louth Report Date: 3/30/2023
Client: Graham, City of NPDES#: WQ0003824
P.O. Drawer 357 P.O. #: Credit Card
Graham, NC 27253 Date Sample Rcvd: 3/21/2023
Meritech Work Order # 03212351 Sample: Sludge Storage Grab
i?araMeters
Results Analvsis Date
3/21/23
>'epgr-tig,� Urnit Method
% Total Solids
2.29 %
3/23/23
0-100 %
SM 254013
Fecal Cohform
5,161 CFU/ g clay
3/21/23
130 CFU/ g dry
SM 9222 D
I hereby certify thatl have reviewed and approve these data. g:�
LaboratoiyRepre ntative
642 'Tamco load, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

ol
CL U
<
uj
L, LE
ct
4-j
Gi
Ln
Y�l
(A
LU
ri
u
mJ
0
uaj
E
Qj
rN
UJ
L)
>
u
E
-=
—
ru
O
M
u
0
I
O
O
za�
CL
2
o
CL
in
ci
PIN
am
co
<) "T
Cl-
ci
u
0
E
CL
Lr]
Qj
O
ci
7D CI
O E
ci
>
-FD LW
Q)
pj

Meritech, Inc.
Laboraf.ory C"ertification No, 165
Contact: Cri's, Routh, Re.porl Dzite: 3/'J'J /20213
C I i e 1-1 G, L: ra h �"] rn, C i ty 0 NPDF,�#: VVQ000382/1-
P. 0. L) nzi w (-,, r 357 1-1 . 0, It: Credit Card
Graham, d\IC 27253 DaLe SamjAe. Rcvd: 3/22/2023
Meritech Work Ordur it 03222345 ;ampe� Sludge Storage Grab 3/22/23
Anaivsis Date L invit Medlod
%Total Solids
2.35 'Yo
3/23/23
0.100 %
S M 2 54 0 B
F"ecal Coliffirm
6,577 CF(J/ t; dry
3/22/23
130 CFU/ g dry
SM 9222 13
I hereby certijj, that I have reviewed and approve these dala. &-'L"gc'), —
Laboratwy Representative
642 'ramco Road, Reidsville, North Carolina 27320
tel.[phone] fax.[phone]

n-
�
c
m
:Z
Lon
'
Qk
ro
ifs
u
L
r _
_
o
d..
u-.
LAJ-
r
vy
,3
✓
f
o
73ci
_
ro
7
U
U
r
o r
v
_ p
c
CJ
OL.
U
a
N
O
a
N
�
aj
i
...... IIII .........
uI
Ln.......................... - __ .. a ........
..
... ....
re
m
uu
&,,
0
n
n
EMMM
m
E
p
m
'rn
L-
o
j
bt}
o
LL
a)
O
U
QJ ' C�
6
Q
C.?
_
:
C..?
r'•.
a
].
m
c
m4-1
'm1
CAS..
r
o
1
''.'
v7
_
Lu
O
S
•_�
V> E LU
vet
ILl
D
F
Q
J
rz
r
4-
O
}
L
u
0J
\�
CD
r
Lu a�
L
O
Q
a
cu
- J!
i

Meritech, Inc,,
['xMroumetwtal Laboratc)r,y
F,M)OP��,9)tor'y C(THficatima No, 165
Conact: Cris ROUth
Crllc�ntt, Graham, City of
P.O. Drawer 357
G�'aham, NC 27253
Meritech Work Oi,dei- it 03232135 SaMI)IC: SIUdgC' Storage Grab
LI aural _rn OLLILS Results Ara a - R, Date
%Total Solids 1, 5 6 "/o 3/23/23
Fecafl Colifol-11-1 "13,462 CFIJ/gdry 3/2"3/23
ICepo[-L DaLe:
4/"3/2023
NPI)ESP:
WQ0003824
P-O� #:
C rc d i L Ca rcl
Date Sarnpe I�cvd:
3/?3/2023
3/23/23'
B.L�p hx1g, inift
0 .11 () 0 IYU SM 2S40B
1 '3 0 C F U dry SIVI 9222 1)
f hereby certibi that1have rev iewedandapprove these data.
Laboratory Representative
642 J'anrico Roid, Reidsville, NorLh Carolhia 27320
teI.[phone] fax.[phone]S22

CL
77
Cy
J d
u`
ca
E
w
CL LL• Lu Ll 0 R 2
y,
w
21
0
LD
OJ
ni
C
41
\
4l4
C
I
�--i
1
4-1
Ia
) m m
¢
cz
\1
0
}
i�
0) �J
F
O
ro a-r
O-
a as
LM
i
n
L.J O
rn L�3{
cn C
o
ry./ fj
N 1
V
U
>
�?
O
LU n
C,
V
C
/
vi�•,
�n
3-1
Syf
N
L
v
O
0
c7
v
ra J^
C�1
J
o:i

Meritech, hic,.
['nvironniental. Laborat 'ory
Laboratory Certification No,, 165
(11'ollt�ct Crhs P'Outh
CHerit: GFafi;mi, City of
P.O. Drawei- 357
Graham , NCI 27253
-implc� Shidge Storage Grab
Nicritech Work Order If 032721309 0
E—algLne�Lej-'a Results Anal, Date
V �Si IS ----
IA Total Solids 2A9 IYO 3/28/23
Fecal Coliform 13,2,12 CPU/ g dry 3/27/23
TZeport Ditc
4/S/2023
NPDF"'Sl-f:
11VQ0003824
P 0. it:
Credit Urd
Datc, Sairtpe Rcvd:
3/27/2023
3/27/23
R ort.n Lbrift Method
-g-
0-100 % SM 2540B
130 UU/p.-Iry SM 9222 1)
I herebj, certij� that I have reviewed and approve these data—
Labor(itoiy,Representative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone] fm(336)342-IS22

CL
Ln
Lli
IT
wi
c—,
O
Ln
>a
12
D
ru
Lo
OD
zm
13-
Oj
LU N LLJ
c
qj
Gj
�7-
ici
0
L-U
LL
u
E
Ln
LLJ
0
C)
m
a)
EMM=
rf)
C:
Q)
ra
0�
0
EMIM
0
-6
rlj =
sirLu
Lr-
u
>
14—
LLJ
LO
L-
LO
Ll
CL
Err
to
Ln
:3
V)
0
CL
Ucu
o
cu
O
Z3
ti
O
cu
>
ui
T3
4-1
Q)
c
to
Fj

DATE
May 9, 2023
May 10, 2023
May 11, 2023
May 16, 2023
May 17, 2023
May 18, 2023
May 22, 2023
xkblrflv��
WASTEWATER TREATMENT PLANT
'GEOMETRIC MEAN CALCULATIONS FOR SLUDGF
503
SECOND QUART ® 2023
RESULTS (c)Ilg dry)
UNITS
% DRY SOLIDS
2418
CFU/g.dry
1.80
2054
CFU/g.dry
1.77
1944
CFU/g.dry
1.87
2902
CFU/g.dry
1.88
1004
CFU/g.dry
1.81
511
CFU/g.dry
1.78
4041
CFU/g.dry
1.80
GEOMETRIC MEAN - � .
r, i' i; ' ': w �

Meritech, Inc.
Environmental Laboratory
Laboratory Certifical tion Nui,165
Coritact: Cris R,00ffi
C' I j e rat (s r,a 1w a i, w i, C i ty, 0 f
PAI), Drawer 357
(jralmm, NC, 27253
Meritecli Work Order,# 0509231(55 Sample: Sludge Storage Grab
Fla a iEt QE'
% Total Solids 1.88 0/o 5/11/23
Fecal Coliforni 2,418 CFU/gdry 5/9/23
Report Dace; S/18/2023
NPDESN� WQ0003824
PV. tfCredit Card
Date Sample Rcv& 5/9/2023
flg,ps�rih 19,1-WA i mohcw
0 - 10 0 I/Io SM 2540B
130 CFU/ g dry SM 9222 D
1hereby certft that I have reviewed and approve these data. 'WAI
Laboratory Representative
642 Tamco Road, Reidsville, North Carolina 27320
teL[phone] fm(336)342-1S22

0 C)
0 C)
cl�
a
C:
CL
(Y) "J
Ln
ru
qz� w
CL
m
LL 2
LO)
Qj tlJ
4—J
aj 0
LU
to
CP
CL W..
E
CL
E ftiC
pr ro
z
U0 LV
E
ai
...........
ra
00 CJ E c
L) Gi
E 4�
ro
Z (A
EL
CL
m
0
'o cl
CL m
ru
LU
4�
u @) E C: 0
ammo
4-0
0 W. 0 -C
4�
CC o z E u
(h LU
u co LU
u >
z uj E Im
w � .0 V "
41
elf SL
4- >
x
Ln UJ ju
LA Ln

Mentech., hic.
Envirm'unental Laboratory
iNo, 16S
Cris Routh
Cfiem:° Grahmn, City of
11 . 0 D ra we r 3 57
G r,i h a m, N CI' 27,21
Meritech Work Order. # 05 102356 SampleSludge Swrage Grab
a r Mtim RgN!AI:U' Analysi,5 );qj!�
%Toud Solids 1,77 % 1 2 3
Fecal C.,oliforri'l 2,0 5 4 C FU / g d ry 5 / 1, 2 3
N-�,,escar. Dam eS/19/2023
N11MSM-: W'00003824
11,0. 4 Cr(,Ait Card
Date Samp�e Rc-v& 5/10/2023
5/10/23,
B-i-mim'Ohig Lim Mgjw.�?d
Otoo ly) SM 25410B
130 CFU/ g dry SM 9222 C.
C-0
I hereby certify that I have reviewed and approve these data.
I Representative
642, 'ramco Road, Reidsville, Norda Carolina 27320
tel,(336)342-4,748 fax,(336)342.-1527,

M1w
j1r �
0,CA 21
j fin
C a )
rrr I� fi�
bl.��.,
Yr M..
w'.: .. u' ¢ „4
°.., mm.. .. ..... ,... moms,„..
C
..dmm
�u M .�4 k
�VOvj
4x tl c
CZ
LLI
4'a o„o p w
Pa'd°. ._
cr41
W:°�„.
ai
�� r ��I�III�IIk wa
W q "aRa k�,4m�w
u 45 I
Cry P P �. �, tf v
.�'a',
..,,5 21
t� ICI re,M rro wM
to
a�
a M4 CL
ro
°.,
�„& Y
i
u w."
W
E.1CJ ti:.
A F m 4C"°b r.
Q a d ° w7
WI �
CL
CZ I —
CO
^' " .. . .
C
Ln cui° ur
6��.+ dw1 C:Y
Iya rw
MEN=s°��:w E
"
_° mm.........u. _ __ .. ... ...mm .. a
.: C5 cta
LLJ°°ww~
ILA calrcv
Now='.wra S� .3
41
U 4"N r
w
„AE �..
`'LU
a (,.w .Y °
red
.. s
1
CAS
h ,r tld
aLLa
p � j Wg I py f py��
ru I��I'
..,. .,.

Metitech, Inc.
Envirommental Laborah.,ory
Laboratory (:erbficabon Nco, J 65
()1,,; RoLldl
clic,rat, G r::a 1) "1 I'll, of
RO, Drawer 357
NC 27253
Swi-iple� Sludge Stor�ige Grab
MoritecIll Wol-k 01'dctIt � 05112' 11-9
AM 51NA
%Total SO& 1,87 'A S/ 12/231
Fmil Coliform 1,944 C FU / g d ry 5/11/23
Repcw( Oate: 5 [,, 1 / 2 0 23
rODE'Sit: VVQ0003824
P,O' #Creclit (_,aird
[)at.e Sample Rcml: 5/ 1.1/2023
5/11/23
d
10 0 O/b Sm 251,011
1.30 C F'U / g I. I ry !:i M 9222 D
lair -ebb certifiv that 1have reviewed and approve these data,
_ / I het
Laboratory Representative
642 Tanico Road, Reidsville, North Carolina 27320
tel.[phone],8 fax.[phone]

.. .... ... ......
U
F.
C
a, C,
U)
to
p
I-2
�Lc
u
din
<)
x
'o
C6
C-1
Ul W
u
JZ
fCs
C
0
0
o-
Q-
LEI
a-,
EL
FU
cr
LO L.
S;
(3)
cl;
0
C
ii CL
0
ID
— J(V�l
31
O
O
u
-0
ID
ai
0
u
<
CL L
LD
u
Qj
E
E
a-
cn
Ln
ro
(U
L6
U'l
=0
06
z 0
L)
V)
E
0
CL
FAMM
LO �D
rl) m _0 E
m
<
---
LJ
rn m
M
0
u
u u
0 X
tLo
E
aro
_0
ll�
0
to
E
@)
E
ru
LU CD 0
fu
a(-4
4-
E
ro
_0
0
0 4-j
:3
0
cu
4�
V)
cl, u
cc 0 E
ui
a;
u
u
>
Z
E
a)
w i
2i No
+1
,*, v
LO of
0
C:
_0
E
H
E
0
C:
u
im
4-
(10
4--
0
4-
aj
>
E
Ln
x
LU
w
CU
aj
4.1
Lj-
o
m
C
L)
-1) L
0.(n
IJM

Meritech, Inn
Environmental laboratory
1,;ibor,itom,y'(,ey�kii�icatioNi No16-5
I lontack CAI,; Routh
(,jieut: Grahw'n, CAY Of
P,O. Drower 357
Graliam, NC 27253
Meraech VVodk Order 0 05162399
skjr:-� R�!.
Toud SoHds 1. 8 8 yu 5117/23
Fecal CuHform 2102 CP(J/gchT 5/16/23
Relm Do to
5/25/20K'
j4puESh:
VVQ0003824,
P'(.'), H
C' re d j t C ;� r d
Me SanQ RM
5/16/2023
5/16/23
0-100 SO SM 254013
130 CMJ/ 9 c4w y SM 9222 ED
I hemLy, certifly jilat I have reviewed and approve these data.
Lab oratoyy Representative
642 Tamco, Road, Reidsville, North Carolina 27320
tel,[phone] fax.[phone]

(A
N
0
ID
m
Q id (), �
CY �7 11) —0 V/ I/ I I
V)
Ll. U.J sl-
CC
4-J
OJ
cuLd
M
Lv
,J
00
I
C
Ro
g
E
z
t
",
rl
qf
(D
u
=too
'D
E
ry,
cy.�
19
0
X
C".
U
bi)
0
c
0)
UJ
kJ
Of
mmm
(Tj
C)
">�
a
z
'6
r�
"U
U ll
+J
0
0
o
z E
Q-)
E
q—
C)
w
)-.
,,,
a. 4
a.
TD
�j
V)
(1)
17,
tl
rat
ri
ur
D .0
Xtiv
Co
al
E
E
E
E
<
Ca
rrs
u
cu
aj
.,r7,
cr nj
4-1

meritcych, 111cc.
Environnierital Laboratory
p,,sjl)ov-atow-y Ceaffication. No. 165
A.v
Contaw Cris Roudi
Client (Awharr; Cil cm '
PD. Dramr 357
GrkranL NC 272S3
Mc ritech Work Or 0 051723110 SanWle: Sludge S(or,.ige Grab
L5 �kay.ILH
lyo'rotal Solids I Al "/o S/17/23
Fecal Colifonli L004 CRJ/ g dry 5/17/23
Report Data 5/26/2023
NPIJESH: VVQ0003824
PAI A MR Uird
Da��c Samplc Rcvd: 5/17/'2023
S/1 7/2.-3
&mig,Lduu. UPA mUh9d
0-100 1% SM MOB
130 CFU/ g chy SM 9222 ED
I heteby certijY Mhave at I ha)-eviewed A-
I appywe these daM.
LabomtotjvRepre entadve
642 Tamco Foad, Reidsville, North Camlina 27320
W11336)342-4748 fan(336)342-1522

O
tb
Q
C)
CL
a
PS3
w
n
E
E
�
h
vi
W C
•�
QJ
C?
l
LL
.4
(D
[s-
mpUl
Y
9
6
�s 8
C
aJ
V
�'
LL/
C L'
L•L'
'
!
-o
n
CJ
fu
u
73
0
w
m�
{
m
a
Ln
Q
m
to
vi
C
n
a C
au
�
C
N
`,.
IL
E
p
U
Q
A
u
o
ti
E
M
E
E
W
&n
E
a
6J
a`ni
E
C r,
c!
a
f�
p
Ll
® N
MCL
b
;
Lb � f
tlt4m rn t�
o
CL
w .
n7
©
o
to
C- of 0 v
ro
o
v
!
n
V
z
a
i
mury'
�
c
LM
O
0 w U m
f
w
av
LU
q
.0
*
�
a�
a
a' j
�
a
E
n
M
U
C
�
E
O
Q
a-
U
awc
O
+1
ro U
0 '9`�
j
aJ
cn
w
4-
0-
a
�,

Meritech, Inc.
Environmental Laboratory
Laboratory Certification No. 165
ConuAct: Cris Routh
Client: Graham, City of
11.0. Drawer 357
Graham, NC 27253
Meritech Work Ordcr U 05182378 Sample: Sludge Storage Grab
Parameters Results Analysis Date
r%Total Solids 1.78 °/, 5/19/23
Fecal colifornl 511 CTU/ g dry 5/18/23
Meritech Work Order #f OS I H2378A Sample: Sludge Storage Grub
12eporl Date:
6/7%7023
NPD1'Sli:
WQ0003t324
P.O, 4:
Credit Card
Hate Srample Rcvd:
5/18/2023
5/18/23
Reuor•tin2 Limit
Method
0-1.00 %
SM 25406
1.30 C1711/ g dry SM 9222 D
5/18/23
€farResults Analysis oato 12etanrting Limit lvlethod
%, Total Solids
1.78 0/0
5/19/23
0-100 %,
Slid 2511013
Total Suspended Solids
14,500 nag/l.
5/19/23
2.5 mg/L
SM 2540 D
Ammonia, Nitrogen
4,900 mg/I<g
5/22/23
680 mg/ko
EPA 350.1
TKN
25,300 mg/kg
5/24/23
20 mg/kn
EPA 353.2
Nitrate/Nitrite, Nitrogen
<562 mg/kg
5/19/23
562 n1g/kg
EPA 353.2
Aiunlinulal, total
41,400 mg/kg
5/26/23
2,50 nag/Icg
EPA 200.7
Arsenic, total
<2.01 mg/kg
5/26/23
2.81 mg/lc-
EPA 200,7
CaldUITI, total
13,700 mg/kg
5/26/23
0.200 mg/kg
EPA 200.7
Cadmium, total
2.013 Ing/kg
5/26/23
0.200 mg/kg
EPA 200.7
Chromium!, total
40.7 mg/lig
5/26/23
0,005 mg/kg
EPA 200.7
Copper, total
239 mg/kg
5/26/23
0.250 mg/I<g
EPA 200.7
Lead, total
23.7 mg/kg
5/26/23
2.00 mg/kg
EPA 200.7
Magnesium, total
4,800 mg/kg
5/26/23
10.0 mg/kg
EPA 200.7
Mercury, total
0.056 mg/kg
5/19/23
0.02 mg/kg
EPA 245.1
Molybdenum, total
5.25 mg/lcg
5/26/23
0.500 mg/kg
EPA 200.7
Nickel, total
34.4 mg/kg
5/26/23
1.00 Ing/kg
E11A 200.7
Phosphorus, total
28,700 mg/kg
5/26/23
2,00 mg/kg
EPA 200.7
Potassium, total
5,170 mg/kg
5/26/23
20.0 mg/kg
EPA 200.7
Selenium, tonal
<2.81 mg/kg
5/26/23
2.81 mg/kg
EPA 200,7
Silver, tonal
<1,40 mg/kg
5/2b/23
1.40 nag/kg
EPA 200.7
Sodium, total
13,600 sang/kg
5/26/23
20.() mg/kg
EPA 200.7
Zinc, total
68S amg/Icg
5/26/23
0.500 mg/kg
EPA 200.7
I hereby certify that I have reviewed and approve these data, ' CdL)'- Ua f
Laboratory Repr-esentative
642 Tamco !toad, Reidsville, North Carolina 27320
tel.[phone] fax.(336)342-IS22

O a bJ
1 = 1 Y
TO
Qj
uj
— - ° �? �r s
ra a u, Cl-ci a,
cr
cu X py 4 yyty� - a1
� `Q ,. ` BUJ C
V)
Ln
J
7CL �
mro
�.
0 Q
N 73
0
c E E E
WY
h o v)
a
g N
m O � o o r�on a
m _@ y l
u ro
C1 x +' a ro
-a a. a C Z
M � d
w
ten_
o
4 ro >
Q0 cc:
VD cr
U C
ro 4—
� U cx rc cc
p 1
x
w 4y
n l/7

Meritech, Inc.
-onmen'tal Laboratory
Envit
Laboratory Certification Nu. 1.65
C0I0:iIC[: ('IJI-WU6 ct �)a L u "10/2023 Ckent: Graham, City of N P D k S I-f: W00003824
1W, Drawer 35) N: Ccedil Card
Cwaham, NC 27253 Date Sampte I�cv& �/22/2023
MerHvch Work Order. A 0522232?, S,,impfeSludge Storage Grab
p a a L R eni L i I ts Ai gy�ls.Datg
'YoTotal Solids L 8 0 (Vo 5/23/23
Fecal Cloliform 4, 0 41 C F U / g d ry 5/22/23
S/22/23
Rmm,uiina-W.wR Method
0-100 O/o SM 2,540B
13 0 C FU / g d ry Sm 9222 D
thereb certij, that Ihave reviewedand approve these data.
-4.K Aa- -kuf--
Laboratmy Representative
642 Tainco Road, Reidsville, North Carolina 27320
tel.[phone],748 fax.[phone]

an
>
CL
CL
m EL <
vi D
L) m
ID
Ea
C)
m
ui Z-
0 Fo
fl-
cam
. ... . ..... ... . ....... oj
Ln m LL
0 ➢—
OL -0
c ai
iz
CL tor_
ry
o
Lq M,
bn
r-
Ln
u m at0
U u -25
-C
E
4- o -
O
(A i- P
ci
FJJ
U'l
E
41 c
ru
Z o (A 0 0
L) 0
smom rn CL
E
M ct: rn
0 E
ft. 0 re)
u 0 Q
Qj
Utx4 E r-6
+1 CL
Z V) w Cal CL
LL 0) L'i to �3
E cz,
u E 4- v
V)
LU 0 0 0
ro c u ro rJ
z N
r,
w U
LLJ 5 0 z -u C
aj
Vu 0
-2 LU cu
14— E >
> o 2
N
� (3)
a)C:
-C
u E
ru E C,
0
= J-7
c u
.2
az
4—
LU
)
m LE

DATE
August 8, 2023
August 9, 2023
August 10, 2023
August 15, 2023
August 16, 2023
August 17, 2023
August 21, 2023
GEOMETRICx: N . ,
RESULTS (col/g dryi
UNITS
% DRY SOLIDS
4729
CFU/g.dry
1.73
5166
CFU/g.dry
1.76
2674
CFU/g.dry
1.70
1045
CFU/g.dry
1.74
< 532
CFU/g.dry
1.71
2642
CFU/g.dry
1.72
_ 2078
CFU/g.dry
1.75

M 1, -1,, 1 erited
Environmental Lcalmratory
-tificatimi No, 165
Laboratory Cei
Con:Ulct� cri's Routh Repmr ' DuAe� 8 /16 / 2 0 2':.)
C it N7,t; G r�) I rn, Cl i ty of NPDFS#, WQ000382/1-
P.O. Drawer,,357 P. 0. ll � Credit c"'Ird
Gr)Iir m, NC 272S3 DIte snniple kf,,'Vd8/8/2023
.... . . ...... ........... - — ---- . .....
Mctftech Ww k Order It 08082394 SMHJ)1(2; S&idgc Stocage Gcab 8/8/23
Parameters Results Anal sis Date
L8C�1 ELr-t —fi I g Ll I & Method
lyo 'Fot�fl Solids 133 'Yo 8/10/23 10 () I% S I'vi 254,013
Fcczll C'Offurol d,721) CFU/ g dry 8 3 13 0 C F'U / g dry S M 9 2 2,2 D
I hereby certi& that I have reviewed and opprove these data. All, L - —f- t Z! . . .......
Laboratoiy Representative
642 Tamco ftoad, Reidsville, North Carolina 27320
tel,(336)34,2-474,8 fax.(336)34,2-1522

a: C'„
41,4 f V �' rx
n1
..., .,, (14
_,_,.._.. _....., ......»,.».«.,.» .....�,.: ......»..» .4 iwy ..... pµ
1
� a
f
oLi
I,I r I
fa b m ' n.
era
J
TJ I22 q»I
_�e.
�.xa r lo.0
T, r
d pry
ni r„
19
F:1
n p rxcl
ai
c.v
r3 c
i
i s 7 ! ll5 M1 C.
MQ9r
to
Cu
a A r`. ..,.,.... Iql
i r r
ai
wgi bA"d L:w In f"a """ r"S rta
MOM
I G'
v'
A
r �
DID c N
rat ro f:k " .."...,�,.. _,,.. .�_. -.
umri�ll at C� 9 �" ___..w __ .m,m
�w rri raro ru � ".b �
" 4-1
41)
s✓"' p rya w
,� 4a
. _ _. _ .."....
fkJ (p 42 ay.
. rLf C C)
. a'm�
LLJ
( aT E a
IN ti "
v"Dc cc
ma raa rt!
cr u
t47 r. r r.
C: �)em
i}; tfh >r
i mma (1) r LA as 4� "ri
Ira
{tea L El `S" ��

Mei-itech, Inc.
1,aboratory
Imbumuny CendRadon Nm 165
Colamn (his Routh
Cliel)c: Graham, CRY of
RO. Drawer 357
NC 27253
MII Work Order H 08092360 Sample: Sludg(-; Storage Grab
P a r Lu. 1 -1 L, 13 AnaWsi5MtUi
Wrl TTrawl Solid S 1 .7 6 (X) 13/10/n
Fecal Ckd&rai 5,165) CJ',U/gdry 8/9/23
kepm t Da h,r� 8/1 7/2,U23
WDES I VVQ0003B24
P'0ft: Credit Card,
Date S'amplc 1'3cvd: 8/9/2023
Ru), Qwn-L" I � i I V, i t Miffl,19A
0-100 % SM 254013
1. 3 0 C R J I ry Sm 9222 1)
I hereL91 ceplj that I hove reviewed and upprove these data. - Ax
Laboratog Repwent afive
642 Tamco Road, Reidsville, North Carohna 27320
U013303424748 W433034T1522

N
� 0 nx IT i
a
p
�r n
i.L.A m \
r l
d
qj
c_ u� 4r1
,I..
cw J „.
.�, " C�
Tj
co
vi
f17 , Ci {r5 J
1 . „ CL
is
Ln nP r nP
E co(' i rer car
0, x^tiP rl$ eke
0 .
J„ �0
a C.
d.
qi c ni GJY I °UO
O
" 0i
,� ca as
n c� 4j C �_
u ON
CCIN ap
y
s dJ
4 ..) E -
n z u >1
(7LLA4-1
31
� Am
m
I
qJ Cl„ CY
c1.1 r- C1
„
.ry. ..MNm,

mer-itecil, lrw.
E 1 win" nmental, Laboi"atory .0
-y Certification Nu,
165 Laboratoi
MAPS
JAWTV"M
ma
Contoct': Cris Routh Report D�ite: �i/21/2023
cjjent: C;ralnon, City of NPI)EStt: WQ0003824
P, 0. 1) rawe r 35 1) �-
11.0, #: Credit Czird
Graham, NC 27253 Date Sample Rcvci: 8/10/2023
Meritech Work. Orcler 11 W3 10231So Sample� Slticlge Silorage Grab 8/10/23
Eilraincip"u, a�I".. ind
'YoToUfl solicts
1. 3 0, M)
8/14/2.3,
0 - 1. 0 0 M)
SM 25,1,O1:1
Fecal CoMorm
2,,674 ("I'M J/ g chy
8p 0/23
13 0 C FU / g, (I y
"3M 9222 D
081023156A
San-)ple:
Sluclge Storage Grah
8/10/23
PavanjeterLs
Rem-ubtfk
A-us-flyaiv-Dii
Rp� Ung-Li-i i CU
1AS(WI-1(hil
,K)'Foral :oljcls
1,68 'Yo
8/11/23
0-100 '1/
SM 254013
Total Suspenciect Solids
16,700 mg/l.,
8/15/23
2'5 mg/l,
SM 2540 D
Ammonia, Nitrogen
4,420 mg/1(g
8/14/23
680 nag/kg
EPA 350.1
TKN
23,600 mg/l(g
8/15/23
20 mg/1%
EPA 353,2
Nitrate/Nitrite, Nitrogei
595 trig/1%
8/16/23
562 mg/kg
IPA 3512
Aluminum, total
51200 nig/kg
8/11/23
2,50 mg/kg
EPA 2003
Arsenic, total
< 2.9 8 mg/kg
8 / 14/ 23
2.98 rat g/kg
EPA 2003
Calcium, total
16800 mg/kg
8/14/23
O200 mg/kg
EPA 2,00.7
CM.IffliLlol, 1:0(Lil
3.39 mg/kg
8/14/23
0200 mg/kf.,
EPA 20 03
C111,0111juni, total
36A mg/kg
8/14/23
0.005 mg/1%
EPA 200.7
Copper, total
264. mg/kg
8/14/23
0.25O n-ig/kg
F, 1) A 2 0 03
Lead, total
26.9 mg/1%
8/14/23
2MO nig/l(g
EPA 200.7
MaglIeSiL1111, t0tal
.5460 rnVr,/kg
8/14/23
10,0 mg/kg
EPA 200.7
MerCLIFY, total
0,059 Ing/1%
8/1S/23
0,02 mg/l(g
EPA 24-S.1
Molybc1eilL.1111, tOtJl
7.02 mg/kg
8/14/23
0,500 11)g/l(g
EPA 2003
Nickel, total
20.5 nig/1%
8/14/23
1.00 n113/l(g
EPA 200.7
Phosphorus, total
39900 mg/l(g
8/14/23
2,00 i�Tig/kg
EPA 20M
Potassium, total
5770 mg/l(g
8/14/23
MO mg/kg
EPA 2003
SeefliUfla, t0t."11
<198 in1 /1%
8/14/23
2,918 mg/leg
EPA 200.7
Silver, total
2.44 ing/kg
8/14/23
1-40 ing/kg
EPA 2003
Soclium, toLzil
184.00 m g/kg
8/14/23
2 (), 0 mg/k.g,
LTA 200,7
Zinc, total
738 mg/l(g
8/14/23
MOO mg/l(g
rPA 200.7
y thatihave i-eviewed and appk-ove these data, T),r -------
Laboi-atmy Repi,esentative
642 Tainco Road, Rei(Isville, North Carolina Z73ZO
tel,[phone] 1'ax.(336)342-15ZZ

um
Meribech, Inc.
Environniental Lalboi-alory
J.,rIJ;oracory' Certification No, [65
1410
Antum bis ffoutl� RvpnO than H/23/2M
("'ity (fl' PUDESO: VVQ0003024
PD. - �7 il.O' U, (; I m'� d i t- c":1 n 1
GO= NC 27ZS,'-1 1we Sanqde Rcvd: 8/15/2023
............
N/leritech Work Order # 08152374 Sampla Nudge Stmage Choi)
fl�ninR'N Ajo �"Jwil'sJ').W'±
1.7d % 11/17/Z3
Uccal (Thform 1,045 CFU/ X My Opsjn
U/ I sp"3
jltakor� i np.-Uiukt WOt�)d
5 100 'yo SM 254013
130 CFU/ g MY SM 9222 D
I hereby certift that I have rMwed and approve these data �, � .. �..� _..��_'.��1::�"�
,Llahoratoi� y Representative
642 Tamco RomL RekAvWejAmTh CmvHna Z7320
0433M3424140 Mx433Q34TIS22

aG
a
n
_
r
(V
a
f
o
w
�µ
Gl
p
0
x
a <
f6
o
O
E
n
u.a
cL
CL
rt,
C.
`aLn
lzn
v
�
i
c
p
tx!
C
CC
0
p
ro
a
I,._;
r
OJ
41
C
�ai..
C
i
r-. r•
0 rG„a
rcv
l.)
U Q)
O
ni ui ai
th
cu
p_
.9
Qj
VY
RAJ
6�J
•M'
p
vi Ci c�� "�
•gyp
p
tEry
n
v�
m
u
�a
Q J
0
r"
"�
C3
0
0
CL
LX
• x-.
LA
�
t�A7
-
O
d
LL a
CCS
E
p
a
LU
o pCC-
LO
e)
N
CU
o
v
k
LO
n
ro
cr
u
ai
D
Q1 w aj
_L
10 o 1r .:
Ln
_

IVAN&, hicc.
Environmental Laboratory
Laboratory Certification No, 16S
AntaW MIS Routh
(;lit nt� of
P, (), D ra w c 1 357
CnAam, NC 27253
or C)rdur. 0 08162356 Sampin Tudp SUump (Amb
Kcanum AwdviL' b,.Ag
U, Atal Solids 1,71 �/o 0/17/23
Coliforn') <532 CFU/ g My 8/16/23
P,cporl- 8/24/2,023
10DEST WQ0003021
11,0. v�: crcclit Card
Me WIN Rcvd: IV I 6/ZOZ3
n/ I h/ 2:3
e 12-9 i� tigxg-L i w i M qS b �Ld
Ch 100 'Yo SM 254013
532 CFU/ g thy SMA222 ED
Q/2 . .. . .......
,41
I firer certi& that f luive revieweel and approve these datm QT -...—AYJ - I '-- — -
Laboratoiy Representative
64Z Tamco Road, Reidsville, Nortit Carolina 27320
tel.[phone] fax.(336)342,4S2Z

N
O
°
a
o
no °
N
IC]
L
= C
V
..
v
ca yg E
E
y„
Nr
E.
LJ 01
ur
a�
CL
a
Li-
Lu
ra
n_
n,
°
a
..d.
p
cs
=
G
16
( j
CL
C 1.
f}
F
v
O
V
p
ro
c
C J
_
O
E
i
i-J
d
V
°
fd
air Y ai
l0'1 lo N Fj
rN
T
V
iv
..
N
rti
N
0
m d O
U
0 m
Co
©
c a
0
� o
a
LU
lammw a o
n cD ra
.9
o
Qj
'co
:Eof
D
® U
L
p E �'
0
,tU W
a
N
O
Y
L
ru
Q
•
- �-'
4—
f0
0
>
�:
L
ICL

7 ,
Of
" Is Rol, lflM
("tmta(:L (" �
t'ii
o W ! ( ; N'n I M" I m , ( " i 1y of
PXI Dmwor 357
GrOam, NC 27253
Meritecli., Inc.
f7mvirmirrienLal L,abopratory
No, I 6S
NIMA Work Orhur 4 081723 151. Smnj)lc: Sh'l�'Ige Stovag'c GI -A)
Rg,�iuk- uplysis Dats
%Total Solids 132 "Vo 8/17/23
Fecal Colibmi Z642 CFU/ g Q 0/17/23
I(epoM Datc
8/25/202113'
NPUESH:
VVQ00038211
PJ)' II:
C'I'c(fit
Me SaMe AM
H/ 17/2023,
0/ 17/13
KnowdlyWIN! hiethQ
I LOO % SM 25401-3
130 CFO/ g di-y SM 9222 1)
-eviewed and approve these dutu,
I hueb '6. 1 . ! -
,y ceiliIJI that I have i
I al-b-oratory Repn'.�seatutive
642 Tanmu Road, Reidsville, North Carolina Z73Z()
teL[phone] faa(336)342-1522

a
S. lJ12
a<
r4
�
�
� r,.
O
i2
u •�
m a
� �
�
�_
C
(
r
67
_E
i
rd�
(y
cc
4`
p fl
fl' -
rO
ca
C
d
—
m
xmw.
rt
0-
U-
LLI
Ll.
0-
N. C
4r_
O
of
o'
^
L
, 0
1
)
Q d
`
A
4.
- Q
`
::s
cc
CL
C
T
c
ro
J
I`.
i�
a
is75
ai
rd1
Qi
73
j
F
C
CU
N\
A
N
p
a
p M m
Lid m
m
a
©
x to
h
_0
n. I-L
0.
0
V
LLJ
U1
p
O
ul O 0
CY
ri ry
'A
Q7
�:
0
U scf
rxLJJ
u
cu
> E � w qj
n
na
a
rt�
uI r-
a
;
C
C7
C
�a
rs
O
.n
O
LL1
v
a)
N
E
Ln
Q
v
Cs
f
a
Qj
�
In
=
J
�
A

Meritech, In(,.-.
Environmental Laboratory
1.,� ,11)oratory certification No. i ("vS
(41"C"IN101
ChcW: Grahmn' CH'y of
PR DmwcN357
Mahm NC 2710
tlC�Jeritcch'Work Order H 08212332 Sample: Mudge Skwoge (AW
1yo Total S'olj(k 1.75 % 8/21/23
FOCL'11 Colif , orm l,078 (11 J / g dry 0/21/Z3
kcpml Oah�� Hf�B/2U3
WDESn: VVQ00030ZII,
im 0: CmdR Card
Date Sample RCVT U/21/2023
8/2 1/23
R v-�mtiw; U!'Ui! W�dlod
0 - 100 'Yo SM 2540H
13 0 C I " L) / g d ry AM 9222 D
I 1,1,ej•ejy (�ertjfy that I hove iwowmi and appivVe these daW
Laboratoty Repi�esejitative
642 Tamco Road, Reidsville, North Carolina 27320
tel.(:336)342-4.748 fax.[phone]

7f
U-1
q
pro
b
u7�
a
j_
u)
n:,
o,_
�..
r
LL
--
p
�n
Ul
`)
71
r
ETD
`r
L'
m
"
72
1
Ln
QJ
I—
ni
•
fi
V
�
C
�
r
['�
00
U
cz
Q Y
p
ff9
O
R
m
[
>U
rn
�
ro
-Q
-17
0- €i
0
i
0
LLJ
E
c
Q!
ILi
O O
vl
GY'
(...�
i-�
iu
C7
4J of U CO
Q
V)
O S_...
uj
> O
"
LU
n
in
�}
.aM r
sz
0
Qj
v
f
C
{
LLI
-ro_�
K
Vl
i

CITY OF GRAHAM
WASTEWATER TREATMENT PLANT
GE014ETRIC MEAN CALCULATIONS FOR SLUDGE
503 B
FOURTH QUARTER - 2023
DATE
RESULTS (col/g dry)
UNITS
% DRY SOLIDS
October 10, 2023
11,979
CFU/g.dry
1.92
October 11, 2023
8,392
CFU/g.dry
1.95
October 12, 2023
5,652
CFU/g.dry
1.93
October 17, 2023
12,176
CFU/g.dry
1.93
October 18, 2023
12,169
CFU/g.dry
1.89
October 19, 2023
2,392
CFU/g.dry
1.90
October 23, 2023
4,196
CFU/g.dry
1.95
GEOMETRIC MEAN
7,026
CFUlg dry
1.92

Meritech, Inc.
Erivironnienbil Laboratory
L,aboratory Cerrificadon No, ME;
COHL)CU C111S IlOUJII
C 1 1: G r", t I �rl n 1, C i ty o' f
Pn, UMWONG/
N(,,27253
blurkechWork(KW4 10IM319il
11 g,� u R
'Skidge Storap-, Gn'.Ib
'yo "Total Solicls ['92 %1 10/11/23
Fecal Cohform 11,979 CfV1gdrj,, 10/10123
R r"'� V i S ('�! d I) a t : I / 1 it?l? 0 ? 4
Repoll OM(-1Cl/ I � / ',() 2 '
NPDESH; vvQ=3821
11.0, t Credit Card
DaW SamMe RM JW10n023
10/10/23
R-(--u2r-tinu-Uka D(' 1 Dald
0-100 1A SM 2540B
1.s10 C FJ J / p, d vy Sly 9222 1)
I herelo, cembj that I have revkwed and upwme these dum
y Repj�esenwbve
642 14mco Road, fleidsvilkle) North Carolina 27320
teL[phone] fam(336)342-1522

�
m
�
PA
ro
vi
a LL
li
C�Oj
�I..LJ
W
C
cl
t
L
i
E
cm
C7
A�
A
ai
� �
+
u
<
0
U ¢(
<
a
u
QCJ�
EiJ
Is
G
00
of
w
Ln
r
aj
m
Ci
M
m
L°
cc(
0
0
©
u
u
db
s
ui
uj
QUl
v
r
>]
m
C
u
_0
N
..
D
U
ro
Ln
LLJ
`�,
>
{7J
LLI
.
d
2i
m
>
p
6A.iu
r
L_
M
to
i
c.
Q
r.
�
n
c
a
ri
�
IIf
W
v
Cam. i
D
a{�i�l
L
3 a
C6
0
l
C
o
q
qj
C
N
�
P
f
N
4-1
a
LW
�
a4
�
p
�
c
J�n:
C
-
�
at
ti
u
m
"EJ
0
iv
ni
ai
r..
ni
c
in
y-
`w
t_1
„
C
n
47
m
0 ..
-m
a -J
La
n
O
ct
—
n
o
CL
a
°
�
Ln
�
v
C
n
�
4
til
cu
cu
L
y.
..
ai
61
m
ai
cv
a
E
N
ti
E
�
cr
u'
O
c
U
Qz
4-
0
7
)
C

Merg ted"i, Inc.
Environmental Labor"atoi y
Laboratory Certfflu.wbon No, 165
CoOm CxRouffl
ClientGrd-loilll' Cit v of,
P.ODrawer 357
Grnlmm, NC 272S'i
Meritech Work Order. 0 10 1 12390 Sample. Sludge Storage Grah
Reskilts Analy5js Dal-.e
Total Solids "I A 5 'Yct o I
F'ccr lj (](diform 3 1-) 2 C I ' U / g d I 'Y W/I 1/23
Rlemrt Date:
B 0/ 18,120,23
NITI)FMI:
WQ000382d,
1"0. P:
Credit ( ' 'a and
to/1,1/2023
I o / t I / n", : �'
0- too 'Xil S M 2 54 0 13
I I M (IFUhIdly s 1\4 I-) 1� ), 2 D
lbereb cei•tiltlintlliaver-eiietiled(iiidapi,)i,ovetliesedat(.-i.
Laboraimy Representative
64.2 Tamco Road, Reidsville, North Carolina 273210
CeL(336)342-4748 fax,(336)342-11;22

Ln
aj
00
E
�
J
IC
of
I
_
=
G
r
O
_ y
x.
�'....
_ w
cc
ti<
CSL L�
Ll
-tT)
41
41
F--
jZL
cc 0
r�
QjZ
ro
u
�
m
o'
S
N
0 r•]
� ry. ©
vt
�
�
�
za
_ci
Imam
(cc m
fiY
o
Q
in
<CL
17 x
_
i...
_
C;
�1
O
pm
own
�
c
Ln
~
4
V)
LU o
w
LU
--
-
u
is
"'-'
N
O
us
a3
as
LL
-C
CL
3
uL
4-1
Q1
m

Merit,ech, In(,,,.
F�nvironynental Laboratory
LaborM,,.rry Certific-ation No, 165
Cfml"-wlCris
ClierW Grallam'Cily of
Grllll�im' W? I'253
Merillecli Work Order 11 1011 2379 SLAn')p1e: S41clge stw".lf."(" (rzlb
Resuhs
A ma 1 Y,"wis-- P—a t el
(yo Tot'd soli(k I 'l)"3 "% 10/12/23
Fe cz.)l CoMorni F), (-) S 2 C I -M / 12) d ry 1, o / 12. /'.� .3
9 /2 0 2i
N 1-1 D I S ft: W(,'!0003Uf
Ditc �411jlplc lkv(.k 10/ 1 2/202:1'
TO/ 12/23
0_11"� I I t�j Medmil
0'. 100 lyo S m 2,5 4 0 H
1 '3 0 C' I " U / g d ry S M 9 222 2 0
I hereky certify that I have reviewed and approve these (Iota, . ......
Laborotwy Representative
6421'anwo Road, Reidsville, North Carolina 27320
tei.(336)34.2-4748 1ax.(336)34`/"-1SZ2

fll
rx
�lz
0i
E
0
A-
L"
EL
>
LL Ld a
cr-
4-j
Ln
L9
C
n
fA-
Q�
rc
D cm
ra
1,
0
u
-
iL)
27
Ir
ej
70
CK) rq
cIy
LU
Qj
4-1
Gi
E
GeV" rf)
rn
0 rn
cu
CO
UD
UJrD
CJ
V:7
'A
LU C) 0
4-
cr
4�
VI
c
--W-
>
z
kD Lk'
�IIT
W
oj
Ln
1-0
75
LL
J7-1
N
iN,

mentech, Inc.
Environinerital Laboratory
Labot atory Certification No. 165;
contna: (vis now
Chent: ("waliarn, City dal
PJ)� 1)1"awer 3F)7
61 a I i a ji o, NC 2 7 253
MeHtech Work Order N 10172350 Sample Mudge WmgeGrab
P. i1nimtJ �".x -.! f � (nadts Analys�i Qatg'
it ToNd SoHds 1.93 'Vo 10/18/23
Fecal Cold'orm 14 176 CVU/ g cKy 10/"/23
Report Dat:(,-:
1 0/25/2023
fqPDHS#!
VVQ0003824
11'0�fl
crcd�t Card
Date Samplu kcvd:
10/ 17/2023
to/ 17/23
Lk.w,tr t 111 unit, M-CLUwA
130 CFU/ g IT SNI 9222 D
I herepy ceitif}l that I have twiewed and appywve these data. �Z.
Loboowuny Rept-,esentadve
642 Tamco Road, Reidsville, North Carolima 27320
teI.[phone] fax,[phone]

, F.
V�
tp>
CL
I�
LU
0-
0
c
u
0 0
Tj—
tn
r
Ca
An�
a,
cm,
O
cr
07
.47
4-j
ca
caw
V)
U)
C)
U
Ln
W,
(,j
LU
z
Ln
m
E
M
0
'3�
u
u
bf)
LU
LU
�m
D
E
E
�w
Q
c
(D
CL
ra
O
AU
In
4'
k
J7-
4-
E
Q)
>
-0
V)
CL
Lu
-0
m

Meritech, Inc.
Enviromnental Laboratory
Laboracory Cerdficabo#i lqo� 165
Conmra Ws Routh
chullt� Grallaw, GLY of'
11.0 Di awt,-�r 357
Graham, NC 27253
Nleritech Work Order h 10 182392 &"npkn TudRu ShHuRe (Hal)
P-anm� 1[3,tnoAU�', Anallysis. Ra!�.,
'YoToNI Sohd�; 1, �3 9 lyr, 10 / 2 3/ 23
Fecal Colifulm 12J69 CFU/gdq I np SID
RepmT Ito u: I 0/25/2U23,
IN 11 D [,'S 11 WQ00():�1,82d
PJ14:
Jbie Smnjfle Rrv& 10/ 18/2023
I n/ I S/n
-10 0 'yo Ski 254CIR
130 CFU/ g dry SM 9"M D
I hemby cei,tify that I have mvMwed and uppime these data,
. . ......... I- . . . . ............. . . ..... ..
Labotwtmy Relwesentutive
642 Tanwo Road, Reidsville, North Camfina 27320
tel.[phone] fax.[phone]

71
-6 U
z
-0
Qj
0
-1
V)
VI
LAJ
u
U-
LU
(-L
n-'
4—J
--5 ro
>
u
LL
QD
dl
-0
ra
Lu
4�aj
ro
c2
LA-
M
0
LU
0
0
jA
cc
2
m
Co
ro
'0
z
0
w
as
4-
LU
>
z
>
0
LU
V)
m
-C
I
LI
oz
s
of
uJ
ul
E:
0

Meuritech, fric.
Environniental L.aboratory
Laboratory Certification lvo,
Conta.W Chris N, �'()uth
Client: Grall"'1111, City or
P.O. 1:rawer'357
G r;,-i I m III, N C 2 7 2 5-3
M e r I Ve c l-I W (-) I, I -I-) 10192,328 Sal"Ple: Sludge Storage (",rab
P, I's
Results
Awal si Da
'yo Total Solids
TOUd SLISPeDd(ld SO(JS
Ammonia, Nitrogen
Fecal Cohfonn
T K N
Nitrate/Nitvil-,e, Nitrogen
AILIMilILIM, (OU11
Arsenic, total
CalciI.1111, total
(-'a d III i U 111, 111 tI I
Chroinhim, total
(,opper, total
Lead, total
MaglIOSiLIM, t0t-,Il
M erc u ry, to ta l
MolybclenLIM, WWI
Nickel, total
Phosphorus, total
Potassiutn, total
Soleninni, total
Silver, tot"d
S o d i u n), to ta I
Zinc, u)tal
1.90"op
t 0/2 ' 0/23
15,900 g,
10/24/2;3
<526 g/ k p,
l 012 '13 /2 -3
),392 nqy/kg
'I ()/ 19 / 23,
12,:300 11,1g/kg
10 / 24/ 2 13
<526 mg/kg
10/24/23
zl 3,100 n1g/kg
10/ 2 3 / 2:`,3
< 2,6 '3 mg/kg
10/23/23
14,800 mg/l(g
1-(1/2-3/23
2,56 as
0/23/23
34"8 mg/kg
10/23/23
216 mg/kg
10/23/23
21") I'-fIg/kg
10/23/23
4, 9 8 mg/kg
10/23/23
53 mg/kg
10/23/23
6A,2 III g/ kg)
10/23/23
18,8 rjIg/l(g
10/23/23
30,400 mg/kg
1 D/23/23
S,040 rng/kg
10/23/23
<2.63 mg/kg
-10/23/23
1,58 mg/kg
10/23/23
1 S'd DO mg/l(g
10/23/23
7 33 mg/kg
10/23/23
Nlepoo� ["),Ite: 10/27/20231
NITI:',(',4V WQ( ' 1003824
PDAt: Crcdit(]�Ird
L1,atarwirat I PIC R(Td: 10/19/20213
,10/19/23
R-M)LaLthl' -Urnit
Method
0-100 Iyu
SM 2540f]
2.S rng/L
SM 2S40 D
526 mg/kg
F,'PA 350,1
20 mg/lig
RJ1 A 3 N'") 1, 1
20 mg/kg
IISIA 353.2
526 njg/kg
1`11 A 3 5,'.3, 2
2.!,-,10 mg/kg
L-WA 200.7
2.63 nIg/kg
EFTA 200,7
0.200 mg/k,g
EPA 200,7
0,200 mg/kg
EPA 2003
OMOS n1g/kg
ETA 200.7
0,250 ing/kg
11,'PA 2003
2.00 mg/kg
F"* P A 200.7
MO Ing ,,/kg
f-TA 2003
0-0/13 mg/kg
l'�"PA 245.1
0,500 Ing/kg
EPA 2 0 0,7
f MO In/kg
CPA 200,7
2,010 mg/kg
MO mg/kg
2,63 rng/l(g
1.20 111 g/kg
20,0 ing/kg
0500 jIIg/kg
EPA 2,003
ETA 200.7
HPA 200.7
11" P A 2 0 0.7
EPA 2003
fherebY CeITY,' thilt I luive reviewed antf ripprove these dwa,
I Uiboratoty Representative
642 'ramco Road, Reidsville, North Carolina 27320
tel.[phone] fax[phone]

m
a
C �
ru
M1rM
ra
fl tl�ry
IZ 1ry
....�.
_
y
i
aH
t] a I
7C
I d
Y'4
t
t)
dq
i (y W
"�,.,
7.3
p
6
.,
Cr
,
x
utlY T
10
1
I
73
�w.
f
Icl
✓
C".a "'.
wfa l?
I
}
f Y
qlf
✓Y
(110
Ga.
tl,.A
R.,f
fLY it
'. kL 4{,„
,,..,
rrid
all
rz
ui
4w'
Y""I
E
C�
I t'1J �,Q)
`1
rwl
a)M
LNi
l J
1Or
wY
w f
a
m.
_..
.
.„...
.I
minlm
f�
�p
WIWW
—0
ILY.k
ui
CL
.Lb°W�pq
RNMEN
Ud
0
(Ty
—b
CC
CV
°
P,.A.J
47D
' ,
LU
Q
J
w
t}
LO
ctf
0
a�
t
v,t�
0.
u
`vr
.°'w
polll
tlb
la
�,
rva
9vi>
r3l
m
0
V
rxv
d+',S
air
rdk
t7�
r
awi q"
_ ........,_
.. . ......
.....„_
it
fe'
p
tlC'9
t W,
G ff
W
x"}
4 L,
Id9
Gi
�
cu
Q`
f,�
2
IwT
k,
Y
ai
t1J
�
r
�
-�,
as
�4
c
}
ll=..,
¢r 47
73
Y�
yr
..i,,..
f L!

M(,.witech, Inc.
I riviromriental Laboratory
Labmawry Certification Nu. 165'
Wimp (As Houth
Gri"111mil, City of
PJ1 Diawer 357
(`.rah�im, N(, 27211'
Muritech Work Order 0 1 OZ323 15 Sumphy Mudpc Sunage Choh
jlaraumkEl RQLSL1.j_tS AawygirCd)iklg
0/(� Tok-11 ; or ick, AS % 10123/23
[" C, c �1 I C." 0 1 i fo 1, 1 m m 1, 11ii) (" 1 �' t I rainy 10/2 3/23
Rejmr� O;Aet (),/ '3 o / �' (C ,� :,
NPHSO: VVQ000382,1
PAI ll C1 udit ("ard
1.11tc S":111119ic Rcvd: 1 01L,�120,L3
10/23/13
fML4_)rU_ug_LJ un it INV Ile, t hu x I
0-100, `VU SM 2540F�
130 ("'FU/ g, dry SM 9222 1)
< , 2i
4/1
I here4y certafv that I have ItmWed and approve these AM
taboratmy Representotive
642 Tamco Road, Reidsville, Nofth Carolina 27320
OL(336)342-4748 fav(336)342-1522

a
nrnn
�
r->
�
t
�
t
Jj
73
oj
�
XD
i
Ln
4J
Q
4
aT
e
SA
i
o
V'
bo
a
f`
c
oj
013
C
a
v
a
Gj
E
n
CL
E
E
E
Q m q
E
°
M
(C1
a
Pa
Mh
ai v
o
o
U
abb
L
0
LUloon
of
Lu © o
mmom
7S
`0
cc
N
C
n
O
=
a
a
4->
c u o
UJo
cu
E
x
(,I
lD cG
L
cll
�
�
_cc_'
�
c
a
P
w;
Tu
v
N
lJ
h
`a«-
Ln
J
_

f
0 m � �

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Bate:
Digester Temperature:
Sampling Date/Time'.
Sampled By:
Analysis Date/Time'.
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature,
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
3/27/23
15.5
3127/23 0937
3/27/23
CS
2.0
16.2
16.8
0.13
7.1
0.98
Dry Solids
egrees Celsius
earees Celsius
8.02 mg Oxygenlhr
0.40 mg Oxygenlhrlg
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

M
0o I� tD 0 N3- M N — O
([/Btu) U013AXO pan[aSS[®
co
LO
�r
co
N
r
a--
r
Q
r
N
c
r-
co
C'7
N

Vector Attraction Reduction
Option 4 SOUR DATL
GRAHAM wwm"r,p SOUR TEST
DIGESTER-
. .................... . . .
-rEMPERATURE ATCOLLECTION:
SAMPLED BY:
....... . .. . . ....................... . ... ....... . ........
ANALYSIS BEGAN DXTEITIME.1,1
ANALYZED BY: 5,
4 114 ANAYLSIS ENDED C)ATE/11ME.
BEGINNING SOURTESTJTMPERATURE:� 4—)
- — -- . ................
ENDING SOUIRT'Es-r TEMPERA"FURE:
Tinw in Minute
omwwwwwwwwww ..... . . . . . . . . ......
. . . .. . . .........
2
3
I LI-1
12
2
13
14
15
I- � b? �, � ,
DO METER CAIABRATED: AT
% - mg/L

�01
31,
DO
r'
LU
>
C)
U)
"
"=
0
0
w
CD
8
n
al
u
U] ro
CIO
DO
bf)
bl)
ArY
Cjn
c c
0
sl .r
bi)
M
a) o
V2
p
u
z

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosofids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
o Dry Solids
egrees Celsius
egrees Celsius
0.10
6.2
0.80
5.76 mg Oxygen/hr
0.29 mg Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

W,
[O f— CQ Ln I;r CY) CV r O
(1113W) UOBAXO POAIOSsI(]
LD
(Y)
N
c--
O
m
E
w
E
CS7
Ln
C7
N

Vector Attraction F?,edUCfi0I'l
Optior� 4 -- SOUR DAT E c­:11"I'l� 8
GRAHAM W'WTP SOtf-RTEST
UGES.JER-1
TEMPERArURE A-r COLLECIIOR
DATE/11ME COLLECTED-
SAMPI
ANALYSIS BEGAN DA'T'E/TH "I
ANALYZED BY
ANAYL.SIS ENDED DATO WE: 3y" e"")
", " P/""
ENUNG SOUR rEST p-l"EMPERATURE:
ire in Minutes
D.0. mg/L
ir
'4
ry
12
cl'�
13
1 (1 -1Z
14,
Q
Is
DO, METER CALIBRATED: AT _212 _'8Anaiyst (15

rri
71
E
bf)
Wvl
"ri
uj
w
C4
73
r/5
C.D
bf
urD
of
CD
Z�l
ID I
CNN
T.1
h—S
0
E
w
E,d5.5
Z
Z
> �M
F-
j
,
bij
coo
LLJ
Cl)
Cfj
cr
cn
66
L/D
co
E3

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
0.13
8.6
0.98
7,52 mg Oxygenlhr
0.40 mg Oxygenlhrlg
15 degrees Celsius
1.40
Temperature Corrected Specific Oxygen Uptake Rate: 0.56®mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

I—
cj
x
Nr
r�s
0
FT
9
O CD 00 f— co LO IT co N r C?
r
(IIBW) UOBAXp POAJOSSI©
LD
T
cY3
N
T
CD
E
w
co E
Lo
co
CN
T

Vector A,ttrac,don Reduction
Option 4. - SOUR
GRAHAM WWTP
I E S ]' I.__ E :
TEMPERATURE AT
DATE/,r'IN E COLN_.L:p(m; ..LN � N E °......_..
ANA[ YSIS BEGAN DATE/TILE ,'N^' , � f er
ANALYZED BY: cl,
AN" Ar" L IS ENDED D..t..L/1 NNVNN:.,
BEGINNING SOUR TIESTTEMPERATURE:
ENDING SOUR
"FEST E PE
,...SOUR TEST
I
g
^r
_a.
ryry
�a,�
- � C�n�M.
10
1
13
0 o 0
1
ls
DO METER CALIBRATED:
_�� C,`� "` ) AT e) �' Analyst
N /a
.�rngfL
'

10
C"S
11
U
UJ
u)
a, (Lu D
cu
bi
of Q
—
big
cn
r'y
'(4
w
Yam,
pp
Irr
E',
I
RAI/
VI
bf

I irne
(minutes)
0
1
2
3
4
5
7
8
9
10
11
12
13
14
15
I`aciflty Name,
Biosolids Permit Number:
Date:
Digester feniperature'.
Sarripling Date/ finie:
Sampled By,
Analysis Dateffirne:
Analyzed By,
J otal Solids:
13c.,ginning Ten­lperaWre:
End Ternperatiire:
Dissolved Oxygen Level
Slope-.
I ntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAVIAM WWTID
VVQ0003824
o 11 o I I o I I I I I I I I I I I I I I I I I I I I o I o I I I I I I I A A A � IN � I N M A o o � o I o I o I I I I I I I 11 A5
141
3/29123 1430
mlwmlomwmormmwuuuumwuwwwwwwwowwwwwwl
CS
3/29123 1437
'(910 N W 9 A 1r�NO (M I offed- a , wNi M 10
CS
­NNMNNI1.9
14.4
­.—NINIMMIRAIII�
15.0
0,10
8A
0.96
I o Diy Solids
egrees Celsius
egrees CelSiLIS
5,79 mg Oxygen/hr
0.30 mg Oxygen/hr/g
15 degrees Celsius
1.40
Temperature Corrected Specific Oxygen Uptake Rate] *.*.� ". mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes, "I"he Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

r10
c) co CO LO �t r] N r O
(ll13ui) U06AXO PGAJOssiCI
c�
Y._
C7
T'
N
r
r
C?
r
E
co C
PZ
LO
IT
co
N
r

Vector Attraction Reduction
Optiori 4 - SOUR DATE.
2RAFIAM WWI P SOUR TEST
DIGESTER
"rEMPERATURE A-1- COLLECTION-
........ ................................... .
I
DATUTIME C0LLE(,TEE),... " [
aT - " ­­. ,, ........ . . .....
SAMPL,ED BY-
. . . . . . . . . . . . . ...................... .
AN1\1 YSIS BEGAN DATEITIR14 AE-1�1`,,
........ -------- ----------------------
.... ....-
ANALYZ[.,,.D BY:
ANAYLSIS ENDED DA-m/TIME:
B1 GINNING SOURTESI" TEMPF'RA-TI)RE:
ENDING SOURI-11,.-,ST
.... .. .. . ........
.. .........
TirTeln Minute-
... . ......
. ...... . .....
0 .... . ............... . .... .....
. ...... . .......
2
............
17 61 611
. . ........ . . . ..... .
. .......... . .............
... . . ..... - ......... . -
12
. ....... .............. .... . . .......
13
14
15
DO METER CALIBRATED: AT

H
oil
S,
bf)
b
rn
owk
b'
+
cq
uj
uW
Lt.]
Oj
E
(L
I
rJO
M
tv
%
of
C-D
bil
+
n
rn
Am D
as
0
ui
._
0
co
Cn
Cn
F-
>

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility dame:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis DatelTime:
Analyzed By, -
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate. -
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor
% Dry Solids
degrees Celsius
.......................
degrees Celsius
OM
8.5
0.94
4.33 mg Oxygenlhr
0.23 mg Oxygenlhrlg
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

R-
LO co L La
C6 r-�
(I/6 ) UO6AXp POAIOSsia
c�
T
N
T
r
r
O
T
E
a/
a)
cG E
r
co
N
T

Vector Attraction Reduction
Option 4 .- SOUR D A I'E �- .-" - � "' �,) I >
GRAHAM ww rp SOUF1 TESI
DIGES"FER:
EMPERAl""URE AT COLLECTION:
[)AT E/T I M E C 0 L L E CT E D:3
.. . ...... ............ - - ----- - ---------------
SAIVIPLEE) BY�
...........
I .... . .. .... .. ruq
ANALYSIS BEGAN DA'FE/TIME:
. . . . ............... . .... .
ANIAYLSIS ENDED DATE/l IME
-rEs-r"T'EMPERA-FU RE
BEGINNING SOUR
ENDING SOUF1, -FES'T"TEKAPERATURE:
5 r —n e.Tn V In uies rng/L
. . ......... - ........ ............
........................
10
Ll
P7
12
13
14
?l
5
15
DO METER CALIBRATED: AT I I (,­p I
. .................. ......

Ay,
"Al
(n
Off
i
7'l-Y'
ara
do
CD
rL
1p
QN
Indus
+
05
LLI
D
LIJ
0
0
21
p
V)
v
o
III
b
b
(f)
coo
0
'.VJ
ry)
1-1
11
va
Ld
CD
C
0 0
0
as
Is --as
,S:l
u a'
(S
0
>
9r
r.
all
V3
ul

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate. -
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
CS
.9 % Dry Solids
11 degrees Celsius
13.4 degrees Celsius
0.12
7.8
0.89
7.42 mg Oxygen/hr
0.39 mg Oxygenlhrlg
13 degrees Celsius
1.61
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

iTo
L
L _J
p co f-- CO LO NT m N r G]
r
(I/BL r) UOBAXp POAIOSsl®
N
r
CD
fl9
Q? �
E
00 E
lL..
Lo
N
r

Vector Attraction RedUcti n
RAHAIW WWTP SOUR TEST
DIGESTER J
.........
DAtER"IIVIE COLLECTI' C 30 J I�Wc
SAMPLED BY:
ANALYZED BY..
,NAYL. 11S ENDED E t E..l M IMF : 3, ' w
BEGINNING SOUR 1 E :.~~w T I"EMP m-R r(J E:
ENDING SOURTEST"T'EMPERATURE:
.' " — — -------- : -
lirnein Minutes
mg/L..�...
dk
4
3
7
10
10
11
1
....
«y
13
........ .._.....��f�...,.....W................... _
6.
14
_.............. 1k'
w
"
DO METER CALHBRATED7 b AT ..m(Y"; C p ._.....Analyst ( mm
......0 ...___..... _......., ...............................................

>
ED
Cab
$re
75
0
bl
�Z
rj\
cq
U)
7j
0
0
u)um
LU
t)
bf)
bf)
W)
o
F,
>
E"),
u
zip
ol.
n
o
(Y)
U
(
�J
CD
o-
(1)
6 �
Aj
>
LJJ
I
'JI
E
0 0
0
LU
�2
bb aft
bf)
0
bj)
b
V)
CFI
i
Ul
C/I
bf)
0-4
Ell,
T
ui
0
bf.)
0
bf)
aL4
ZE
<
(n
�
n
ty.
,,
pi
U)
�-4
UJ
00
V)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By. -
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate.
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ000382
3/31 /2
3/31 /23 124
3/31 /23 125
C
1.9 % Dry Solids
13.4 degrees Celsius
13.9 degrees Celsius
0.09
8.4
0.99
5.16 mg Oxygen/hr
0.27 mg Oxygen/hr/g
14 degrees Celsius
1.50
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

LJ
C7 O O Q d O O
O L d Lf} O L O
of oo 711OW) UO6AX® pOAIOSSII cfl csi
cry
N
r
e-
r
ti3
0
N
LO
V-
co
N
r

Vector, Pvttraction Reduction
Option 4 -- SOUR DATF� 3
. . .. . ............ ----- - . ......
(3RAHAM WWTP SOUR TEs-'r
D II G E S T1 f
nom
�'3,AMPLED BY,
......................... .
AN" AL. BEGAN DATE/ HME:
ANALYZED
AN/M.-SIS EN IDE-D DATE/TIIME:,,
7
BEGINMNG'SOUR 'T'Es-r TENAPEFUUTME.-
ENDING SOURTEs-r TEMPERATURE:
Time in� Minutes
............ . . . . . ......... . .
D rrhg/L
12
13
14
is
DO METER CALIBRATED: 1"4
-2LJA-mg/L

rq
0
j
CD
(X
Tj
LU
biD
�"5
CD
CL
Z
rN
pp"
C-1
Sj)
0 0
LUdd
H Q)
01) hf)
bf)
IJ
0
E
tl
+
LJ-4 C�
0 o
to
a
CIO
bll
F—I
1-1
W4
6-
L)
bf)
Cf-)

P,
D
W
ClJ
U)
w
z
E-L
Q
U)
U)
z
Q
U)
��y
V
C_J C"
(D Q N N
T
LO
m
N
n
CL
,t
n
o0
t
,'
cO
T
C�
C)
T
r
Ln
M
o
M
[L
t,--
CL
M
,t
�-
N
N
®
C)
LO
N
N
N
LO
M L" N Q T Q C) f� CS)
00 c 00 T
(� N CA (n Co fJy CS) L1� Cp
T_
(10 CO " 0 C) (/} M 00 T
N W� U {� r 00 C3)
co ['""' C) C) T T
LO
(5S E
E
E
�_
ou
aV_
® h
h
®!
h
Q3
®
_
CL
s
L3f
V1
N
N
4
per-
C
U)CD
®
tj
W
Ca
(1)
ci
-
CO
W
­r
CD
C)
(D
N
l:L
CO
T
Ob
C)7
C,
N
M
L)
M
00
r�
I-
";r
ll�r
CO
0
O
M
00
CO
O)
r--
r`
r--
co
Co
Co
(a
m
C()
CC)
c�
M
M
Ct
IT
I�r
O)
M
M
M
LO
N
"T
dr
0
T
LI)
m
m
N
9
00
CO
m
U-1
d'
m
N
®®
W
CO
m
CO
CO
L()
LO
m
Lo
Lo
Lo
m
LS7
Ld)
tS)
I
00
"T
M
W
r-
M�
CO
N
CO
M
O)
M
T
r-
00
(D
CO
LO
d"
M
N
N
T
T
CD
o
M
O)
Gf
00
00
Lo
Lo
U7
6
LC)
U')
LC)
L!)
Ui
L6
L6
et
4
4
4
c�
N
�
CO
07
07
T
�
t~
T
et
CrT
N
(O
o0
N
M
0
Nr
CO
N
T
T
CD
M
M
CO
tl-
fti
CO
LO
LO
00
Lf)
N
W
CO
CO
W
It
O
r-
d'
T
I'-
LO
N
CO
00
a
O)
O
CO
N
T
T
T
O
0
®
M
O)
O)
M
CO
00
w
r--
0
0
m
0
0
0
CD
(D
Lei
LO
m
m
LO
LO
0
00
Co
U)
O)
C-)
I--
I,-
CO
T
r--
U)
U)
00
�
�
O)
00
LO
T
00
CO
r,-
CO
d
N
N
T
0
O�
r-
w
w
r--
r`
CO
0
m
(D
CD
(D
0
cs)
CO
(D
Lo
Lo
M
CA
T
M
M
LC)
CO
C)
M
T
M
N
T
(Q
LQ
O)
C7
N
CD
0)
Cl)
CC)
M
N
N
-
T
CD
M
00
r`
�
t--
(D
(D
CO
(D
QD
CO
QD
CO
CO
(0
(.0
LO
r--

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient. -
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
o Dry Solids
egrees Celsius
egrees Celsius
0.14
7.8
0.88
8.25 mg Oxygenlhr
0.43 mg Oxygenlhrlg
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

Eo
O m CO CO Lh IT m
r
(I/BW) UGBAxp PGAIOSsi(]
cn
r
I
c�
N
r
0
r
C
0
U
N
T

VectorAttraction Reduction
Option 4 .- SOUR DATE
GRAHAM WWTOP SOURTEST
MES-FEIRc
DAIT',J-1-WE C(DIA.EC"I'M
> ...'J,
.................
SAMPl-ED B'Y':
/\N/U.Y'W Bl-�:(,,,]Alll DATE/TWE-
. .. . ....... . .. ......... .. ....... . . . 7�
ANAI-YZE[) BY':
..........................
ANAYI-SIS ENDED DATE/TWE: I"
BEGINNING SOL )R"FEST"I'EMPERATURE-1
ENDING SOURTEST 1-EMPEFZATURE: @ (I I, "
wwmmmmmwowwm
Time in Minutes
. ........ . . .. . ............ .
uwuwuu
D.O. mgl
. ...........
. .........
r,z
............
10
1
. .. . ........... .. . .......... 12 . . . ............................... . . . .
13 . .
. .. ...............
'14
15
DO METER CALJBRATED. 5"" b "',Z, AT H _rPAnalyst—
Oa,

"Of
f"P\
,
CA
is lyof
" Q I
"JC,
Lr�tio�-,F,
uj
0
0
u)
Ly
off}
"",I
bO
un
F- >
I
sra
I-J
bi
vJ
YLw
LU
U)
JJJ
0
-6
Q bf) bO
b@
MtL I I I � I >'.

Time
(minutes)
0
'i
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosoftls Peirnit Number:
1.')ate:
Dgester TomperatUrC 3'.
Sarripling l'.)ate/'Tirne:
Sarnpged By'.
Analysis Datc/Tirne:
/\nalyzed By,
J'otal Solids:
j TeroperaWre:
End Temperature:
Dissolved Oxygen LevO
Slope-,
Intercept:
Correlation Coefficient!
Oxygen Uptake Rate'.
Ambient Specific Oxygen Uptake Rate:
Average'Verriperature'.
Temperature Correction Factor:
GRAHAM WWTP
WWWW
19.3
wiflffiff��
5/0/23 0920
CS
NIHIMIM IMIM_ww�
5/9/23 0928
CS
1.9
19.6
I
) Dry Solids,
egrees Codsius
agrees Celsius
10.42 mg Oxygen/hr
0,55 rrig Oxygen/hr/g
20 degrees Celsius
1,00
Temperature Corrected Specific Oxygen Uptake Rate-, C."."=.,5_]5mg Oxygen/hr/g
instructions: Enter Data in the Blue Boxes, 'Flee CaICLdation and the Spreadsheet execute autonnafically.
Updated 10/23/2013,

A
O 0) CO ti CD LO �t M N r O
r
(JIBLU) UOBAXp POAIOSsip

Vector Attraction Reduction
GRAHAM WWTP oc"OUR 'TEST
(AG S' R:
D LT[TI E C,0I-L.EC_I_ ���
SAMFILED BY,
a. .. .. ,.. „�. .
ANAYI
II EN D I. ': L) DATE/1-WE:
BEGINMG S'OUI 1 ES I..... — IEIVNP..RA 9 lwJ E-.
Gµ r
" (.) I ICI I I-E ��_.I _rE I P E RATU F E:
,g;
.. ..iq X Ae II19 Mmuux m II41 41 t&,ro j,
tl
I'i w wq d '.� wwoowvv
F
_mm_
a�
�:.....: ..w_., i
�" dC�
i t b^
lot
12
13
rV
114
/Y
DO DETER CALIBRATED: �s - � .. �p,.�� AT �.�;Poa��i k I Analyst
5

H
HY {
r
nbn
Ell
Y
y
I
O
bl)
�B
L
(U
6!)
,may
bB
..f
bB
CD
LLJ
=
Q
by
/..,
t
bq
>
bB
is
i
F(`
`''�
�
F
�
1�•}
i
„
- IK,
w
}�
Q
; �.
art
�
�
�
-_)
E
'
OD
1 bB
LO
1
v}
va
a�
°J
N
U
1LLJ
ALu
—A
0
14,
It
pw�
cq
�}�p
m®
n o
o
Ui
b-0
b-0
hp
U
....�°'
N
bA bB
b.6
>
{
Lo
Eu1
k�l
C""�
✓'
4/
o
'
n
CIO
C/I
61)
H
O
f
CL`J�
31
If--1.
[i%-�)1CO
C,5
W x
Q
F7 L�

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
5/10/23
5/ 10123
I WWTP
0003824
5/10/23
19.2
1309
CS
1316
Dry Solids
egrees Celsius
egrees Celsius
0.12
7.2
0.71
6.96 mg Oxygenlhr
0.37 mg Oxygenlhr/g
20 degrees Celsius
1.00
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

R
M ,
p 67 00 i-- C9 Lh I1r CO N <- O
(IlBw) UOGAXp panlossl®
M
�r
N
n
Es
to
0
co
N
w

Option
rGRAHAM WWTP SOUR TEST
DATE/TIME COLLECTED: �_...h.'...' "I..............
SAMPLED Y-
ANALYZED BY-.
ENDING SOUR BEGINNING SOUR TEST TEMPERATURE: I
'TEST _.....
_.. {
me
...
....,...� . . �...m..,,....---.........�,�.......,�.
4ua�
q I pry
�lfrA�' -5
yy.
p�
10
u'E�
P
<;k
1
DO METER CALIBRATED:
AT � Analyst �

hl�.,uu
v �
C ��
F iw �,
��
I
bl
61,
14
ry
cl
0
0
uj
EWM
0
>
a
(A b
bf)
big
r ji)
Ctjai
bf,
i
z

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility ]Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWTP
WQ0003824
18.5
KP
5/11 /23 1201
1.9 % Dry Solids
18.7 degrees Celsius
19.0 degrees Celsius
0.13
7.1
0.75
7.50 mg Oxygen/hr
0.39 mg Oxygen/hr/g
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

H
LO
m
N
r
E
0
00
Ln
O O] co N (D to It (`) N r O
(616M) U8BAXp PGAJOSsia

Vector Attraction Reduction
Option 4 - SOUR ()ATE
GRAHAM W'WTP SOUR TEST
"'I'EIVIPERATURE ATCOLLECTION:
DATE/TIME COLLECTED� 5 ;r c",
SAIMP1,P) BY�
.... . ..... . ....... ..........
ANALYSIS BEGAN DA-FE/TIME.
ANALYZED BY:
ANAYI-W ENDED DA] E/-f'IME-. "A
BEGINNING SOURTEST TEMPERATURE: � �); t , "
ENDING SOUR -I -EST TEMPERATURE: , 1 , o'' ",
......... . ...... .
kne in Minutes
......
D.O�. rng/L
. . . . . .. . . . . . ....................... ... .... ...... .....
. ....... . .
4,
tw
5, q
'10
12
5, A
13
. . ........ . . . .
14
15
DO METER CAUBRATED; '� 4 4 ' .. AT ..,,2,_Ana lyst t,J'

b f
bJ'
W.
aa
bil
Of
F.Q.
a.
Of
CY
U,J
b
l�
LL
. ..
bf,
ct
rI
1p
to
0
W
Gw
cz
a
0
0
qj
to
bf),
bf)
CN
u)
w
>
ra
W-4
I
sm
IN
N
—bf)
bb
—bf)
bb

"I"irne
(rniinutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
"15
Facility Narne',
[3iosolids Permit Nurnber:
Date:
Digeseer "I'einpemtLlre'.
Sampling Date/ I"' I i n e:
Sarnpled By:
Analy�.Js Dateffin'ie:
Analyzed By!
"I'atai Solids.
Bcginning TOMperaftlre:
End Terriperaft,ire:
Dissolved Oxygen Levell
Slope:
I ntercept:
CorreIation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate!
Average Temperature:
Temperature Correction Factor:
GRAHAM VVWT
wrvwwwwwwowwuwwwww
VVQ000382
H�Mmmw ww-
5/15/2
M
5/15/23 '112
K
5/15/23 113
K
HIMEM
ummmmmmmiwmuuuummiwwwwwwwwwwwwwwuwwwuwwwwwwwwwwwww
20,
0.13
6A,
0,.65
s Dry Solids
egrees Celshis
egrees Celsius
7.75 rng Oxygen/hr
0.41 mg Oxygen/hr/g
20 degrees Celsius
1,00
Temperature Corrected Specific Oxygen Uptake Rate:[ . .... —"'.E41 ]mg Oxygen/hr/g
Instructions: Enter Data in the Eue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

RIO
IM
T
(1ISLU) ual3AXO panlossl®
c0

Vector Attraction Reduction
Option 4 - SOUR DA-i 'E:
GRAHAM WWTNP SOLA"IEST
"FEMPERATURE ATCOLLECTION:
DATEMME C0LLE(,TED:l-`
SAMPLED BY-
. . ............................................................... .
ANALYM BEGAN DATEMME:
ANALYZED BY:
ANAYLSIS ENDE'.'D DATE/ NVIE-_
BEGINNING SOUI--�"T`EST TEMPERATURE
ENDING SOURTES-F TEMPERATURE
.......... --------
�kq
10
12,
ell
13
14
15
CO METER CALIBRATED: .5 t'j-r,43AT fl 6 Lc_Analyst KP
raw

0
0
z
w
bf�
W,
bl
Of
lbf,
CA
CA
CA
V)
C/)
�pdd73emu.
r�l
Iri
C3
"
CD
c
Lu/
0
C
u5
LLCCL I
2-Z6
EvOf)
b)
tl)—r�
Ap
C
> Q
0
>
a
UJ
U)
cr
I
Z
I 1w
� --4 b J
Ell

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit [Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
1.8 % Dry Solids
I
9A degrees Celsius
9A degrees Celsius
0.14
6.8
0.94
8.55 mg Oxygenlhr
0.47 mg Oxygenlhrlg
19 degrees Celsius
1.07
Temperature Corrected Specific Oxygen Uptake Rate: =mq Oxygenlhrlg
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/2312013

FIR
WJ
u
m T 0
(116w) uaf3AXO panlossr©
cc�
T
uO
�lr
T
N
a
0
a�
r`
0
uO
0
co
N
T
H

Vector Attraction Red Llcfiori
Option 4 .- SOUR DATE
GRAI-1AM WWTP SOU'
DIGESTER: It
TEMPERAT'UTZE XT- COLLEC'I"IM
DATEITIME COLLECTED-
. ...... ..................... . . . ...................... . ..
SAMPI FD BY: k, P
A
.1 NALYSIS BEGAN DATErrwlE.-,
ANALYZED BY.
A NAY L,S I S E N D E D DATE.E/1" I'NA E
BEGINNING SOUR TEST TEMPERATURE I Il-,
ENDINGSOUR TESTI-ENAPEF-MFURE:
Time in M MOM,
... . .....
7
10
eD .......... . .
12
13
14
ls
DO METER CALIBRATED: S P G AT yst (2 11_L _.Anal
V

rra
2
qo
0
Fl,
robdMI
z
v
H
"If
bi
LLI
_5
10
v
cq
c
cn
Tj
V)
T
H
41.
CIS0)
�,,;
H
U
w
LLI
w
0
CD
0
0
0
'-
U)
F
Cm
bf)
90
Lu
7
0)
bf)
bf)
Of)
F—)
03
xry
c
rA
Do
4
b
b
b a
is
�4
IEZI
LOD
bf)
are
rL
914
cn
Lo�
CS
y
o�
W
U)
w
QC
in.
rZ)
C/5
cn
cn
bb
c bf)
bf)
E'4
Cq
m

Time
(rninutes)
0
2
3
4
5
6
7
8
91
110
11
12
13
'14
15
Facility Name:
Hiasolids Permit Nurnber:
Date:
r)igeAter -romperatun-e:
Sampling Date/Tin-ie:
Sampled By:
Anaiysis F)ate/_Firne:
Analyzed By:
Total ScAds:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept"
Correlation Coefficient. -
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correcflon Factor:
VVQ0003824
5/17/23
20.3
M�.
5/17123 1003
5/17123 10111
i 'X, Di y Soficls
2
()- degrees CelSiLJS
20 1 degrees Celsius
I.
8.97 mg Oxygen/hr
0.47 mg Oxygen/hr/g
20 degrees Celsius
1.00
Temperature Corrected Specific Oxygen Uptake Rate: Qm47 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

5M
CO I` (D LO tt co N r O
(116W) ua6Axp POAIOSsE❑
LD
d
N
r
r
r
a
r
Uf
E
0
co E
CO
LO
coo
N
r

Vector Attraction Reduction
w
it FIAM �....._...........� ESIW"
�m
"Y�GL S)..t..t R" :
..N_LM0'ER ..'raN E AT COLLECTION: l
DATE/TIME COLLECTED:
AAYSIS BEGAN DA t E/ I NMI. f
ANALYZED BY:
ANAYLSNS ENDED DATE/TIME:
BEGINNING SOURTEST TEMPERATURE- _SURE- ;'� , t "'
ENDNNGSOUR TEST TEMPERATURE: : A m; r.„
Time in Min-q
r4
u, 3���,
�Nt9
12
13
14
DO METER CALIBRATED: �5 P n A p AT L'��"< fim�r��l '�sk 1 r
...._ � ............._. Y �� '.�m�..,..,...._.........----
tl7 , w % - mg/L

r-1
mfK1
Cif
UJ
U
uj
rD
CNx
1
n
CN
CA
CO
LLA
n-j
0
w
Rda
0
0
0
0)
lJJ
ui
"T)
z
.
.
... .. .
Uc

0)
00 0
. ..
CO
........
P-
.
CD
V-
U)
00
(0
01
CN
us
r-
(-A
0) �T
C\l
0)
CA
0
so
CD
Of
.
CN
u)
r'
Noy to
-q
'q'
(
A'
T's
(Oxj
(Ej
(6
UK
uj
as
as
ED
aj
ai
UK
U6
aj
(6
C6
(y)
N ca
0,
co
C,
a
U)
a
r-
CA
Nr
03
n--
CA
cf;
—
00
N
K
CA
0
CA
NT
CA
coo
CA
06 if)
�e
IS)
� e
(A
6
L6
01
no!
Q
W
013
Nf
ul
V)
01
cq
-
C3
0)
04
ul
1.
cy OD
0
OD
ccP
CA
CA
a)
r-
r-
E;D
0
s)
CC) "
(6
(,6
E6
(6
a3
E6
(6
� 6
00
OD Li)
0,
Ot
Q,
CD
00
CO
CA
C-j
M
Cr)
0
C3
n-
(y)
Lr)
IS)
<Y)
(f)
(Y't
L()
CIA
W A
Ic"
ej
vi
vi
4
LQ
'q:
Lf�
'1y
q
o)
OR
J�-
(D
Lr)
'gip-(1)
CIA
'I-
4
Z:
12
N
CA
co
Y
Yam.
F,
r-
to
(0
(,b
('6
(6
(s)"
(f),
c)
00
V)
cq at
0)UD
00
to
Cq
CD
P-
QD
ul
CD
c-
CA
0
0-
CD
0.)
1-
cq
c:)
�z
CA
CA
CA
(OX)
I? -
(LO
ED
(.0
(f)
ED
(D
QD
CD
to
(D
ED
00
OD
OD
M
00
CO CD Ul
UD
0
OD
Nt
00
Q
CO
LO
Q
Q
00
00
CO
CD
Cq
�T
OD
00
ED
CA
le
CA
vi
V
a; aq
up
ul
U?
q
C?
C5
LI)
I-
I' --
CD
N
CA
CA
00
1-
rl-
r--
Y r
fl-
1-
I--
rl_
1
(0
ED
(0
(1)
00
(Y)
I,- W
0"
l-
0-
0
l-
0
CNI
Q)
ED
0
-4-
VA
())
1•-
00
(Y)
1'--
00
se
ag
No
N,
V,
N!r,Y
(0
(q
u;
u;
or
q.
V)
CA
CA
CA
0)
T
"7
cpq
T2
CD
25
00
W
ED
ED
(0
00
(D
03
00
OD
UD
(Q0
(6
6
L6
Lo
Go
(Y)
0)
CL
I--
CL
0
ED
00
V� C)
CA
-41
cr)
(0
CO
M
00
ED
LO
m
(N
m
CIA
N
(N
f
CAICA
(N
>
(X)
(f)
UJ
(0
(.0
(.0
(o
(6
(1)
E6
(6
(0,
E6
(,c)
to
(c)
c;
00
. .. .
. ..... . . ................
0
0- (D
>,
0
U)
C3
V-
04
ps
W
W
F.
00
CD
C)
r-
(14
0
114
AP
't-
E E
E
:2
6
w --
-
F-
0
oo
C)
L
as
M
W
N
fl
E
0.
E
D
a)
CL
w
(D
CD
CL
E
w
W
0
E
Ix
CO
CO
0 E
CL
E

Time
(rninutes)
0
1
2
3
d.
5
6
7
8
9
10
11
12
13
14
15
Facility Narne:
Biosolids Permit Nurnber:
Date.
Sampling Date/Tirrie:
Sarnple,d By:
Analysis DaIeMnie�
Analyzed By-
'I-otal Solids:
Beginning Temperature:
End Ternper�ibwe:
Dissolved Oxygen Level
sbpe"
I ntercept.-
Correlation Coefficient:
Oxygen Uptake Rate:
AmUent Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
i wwTP
0003824
�11111111111111111111M
8/"7/23
8/7/2',3 1109
KP
8/7/23 1117
K P
Y solk- S 2,0 r
�M�
24,6 degreps Gelsh.jc;
uuuuuuumm�
iv� NhINIIIIII 123,8 degrees Celsius
0.09
7.3
0,74
5.61 mg Oxygen/hr
0.28 mg Oxygen/hr/g
24 degrees Celsius
0.82
Temperature Corrected Specific Oxygen Uptake Rate: = mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute autornatically.
Updated 10/23/2013

R.
O CA 00 fl- CD LO IT C") N r C7
(110M) UDOAXp POAIOSS!®
r
Cl)
r^
N
e-u
r
C]
r
CT,
C
fp
00
Ln
C'1
N
r

GRAHAM PSOUR
TEST
F E I1f V R' q.`.�. � ,v'"W .II . RJ 6 V IE Al" �4 r .� N�_�. II �.��d�,..11 � N . r �
ANALYSIS BEGAN DATE/11MEJ) 1,
ANALYZED °. k.�J°
u
�M-�. 9��ING Ol-ESA .T'E']V�PEFV\-F(JlR�� a ..
�e
_t..,.
m
1
1
i
ml.m
DO METER CALIBRATED: �� ��� � AT

�4ar
PIL
A
III
Q
Q
LU
-� 4
L)
U)
W
a
1,
0
bl)
OJD
d)Ind
4�—Cy10
o
CD
r)
X I ,
ll"
r1
Of
`"
52
n-
7),
73
.
n
C4
w
, tw to
Ojo
ci
ay
-
A
y�Y
—,
!
a
bO
uj
P-1
�4
Fjl
L)
0.
UD cf)
CA'] �

Tirne
(rrflr1L1teS)
0
'I
2
3
4
5
6
12
13
14
15
Facility Name] Gl`tAHAM W
Binsolids P(,,,rrnit Nun�ibei­.
WQOOO
ouuuu uuuuuuuu000uw00000i000moi000000ioiouuwmimumoioioioimuuuuuuuuuuuuuuuu
Digoster Ternperatiureuumuuummwiwwwmmwuuwmmmmw
Sampling DateffiiT)e
818123
Sampled Fayi
Arialysis Date/Time.
Arialyzed By:
r8�/8/23
Fotal Soli(Js:
Beginning 1'ernperah,ire,,
End
Dissolived Oxygen k evO
Slope:
Intercept'.
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
El
KP
OVuNmlmIIIIIIIIIIIIIIIIoU
2,0 % Dry Soli(Js
24.4 degrees Celsii..�s
OwwwwwUlwill
24,0 de(irees Celsius
0,10
7.2
0,74
6.16 mg Oxygen/hr
0.31 rng Oxygen/hr/g
24 degrees Celsius
0.82
Temperature Corrected Specific Oxygen Uptake Ratef­no, tt.25 mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute autornatically.
Updated 10/23/2013

F*
LWJ
O 67 00 i— CO LO co O
(116LU) ua6AXO POAIOSsp❑
z.
LO
r
c7
r
N
r
O
E
0
00 E
r-
Lo
Nr
co
N
r

Vector Attraction Reduction "I
Option 4 SOUR DATE. '12
GRAHAM WWTP SOUR TEST
I.,)IGESTER:
[EMPERA"I'l JRE A F("�OLLECT]Cft 14 ,'1 `C
(11
DA'VE/1"IME ("'01-LEC"l 1-11"ID" '!S 8
------ . . ....... . .......... . . . .
SAMPLED B
. ........................................................
ANAt YSIS BEGAN DATE/TWE: 8-,1341 t I)
ANALYZED BY: kP
ANAYL.S�S ENDEI) DATE/1"IME:.
BEGINNING TE"IMPERATURE: 4 � A.j
............... -.1-1 . .....
ENDM,'; SOUR TEST""I"EMPERA 1-URE-1
. . . . . . . . . ..... . ..... . ........................
11 rr� e i ii PA i
.
50. rng/L
. ....... -------------
. ..........
Ryp I'l
.. . . . ..................
......... ..
7-
31
90.
ei..�,,,,pqpp��'"���l
10
11
12
u
13
14
--F--
Tl�
DO METER CALIBRATED: Y'P,',23 AT 011�3 A5

PC
ni
g ,
c��
CO
ASS
I
tiY
j
I
O
'a
Q}
I•
�
r,n ?
bn
t
_
n
o
73
cn � rn
0
Lu
ca hA
bA
bA
`� Q
r<!J
r
LU
Q
v�
Q
o
O
�
ll
©
CO
�✓
G
�
Y
�
~
I
(
{C}
c
C3
H
(7
r
o
I I
�
I°:7
�n
• �
w�
a
e
rCd
bA
'
lf'>
Lo
U1 _bD bA bf7 b0 P-4 b]]
14 CJ]
W
c 1:4 cu

I ryl e
(rnhlutes)
0
,l
2
3
4
5
6
7
12
13
1 /1
15
Facility Name:
Biosolids Permit Number:
Date:
Sampling
Sampled By.
Analysis Date/'Firnei
Analyzed By::
Total Solids:
Beginning Ternperature'.
End ­rernpematuie�'.
Dissohfed Oxygen Level
Slope:
Intercept:
Correlation Coefficient'.
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WWT
8/9/23
8/9/23 1015
IMP
KP
oar
2.O % Dry Solids
M` 23,8 degrees Gelsitis
23.4 Celsius
I
5.61 mg Oxygen/hr
0.28 mg Oxygen/hr/g
24 degrees Celsius
0.82
Temperature Corrected Specific Oxygen Uptake Rate: rng Oxygen/hr/g
Instructions: Enter- Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated '10/23/2013

LO
N
T
c(i
4-
x
LD
Cl)
Q
i!o
rM
O m 00 r (D LD IT c7 N T O
T
(Ij6 ) UGrl,&XO POAIOSSiQ
(D
LD
co
N
r
G7
r
T
6) �
i
R•
(`
Rr
m
()
N

Veclor Altradbn RedUCJCAl 11 C� ll�
Option 4 , S(-.)lJP\ OAI-E-
.. . ... ---- --
F 1-rIAM WW'---P) C!,
, Ar 11 l!"ir; U R T E S T
'rEIVIPERA-FURE ATCll0L-LEC-fl0N:--
)A-1 hA E (" 0`
. ............
SNOF"LED BY:
ANAL.YSIS BEGANI DAl-E/1-HME:
ANN..."(ZED L�
_, J�j,-
ANAY! SIS ENDED nA-f F-11"]IOP
BEGINNING SOUR "FEST -rEMPERATURE:
Q
ENDING) S)OUR1 T-- C. .....
F TEIMPERATI)RE-1
A 3,,
x.fol,
ime �n Wfinutes
0
. ...... . ........ .
9 q,
2
.. . .
. .. . ......... . . .. .......
7
IL 3�
o ae"
pp
13
14
15
cej J---j
DO METER CALIBRATED.- �b' I' AT J-

I
R
CL
kIN
Cd,
5
ra
m
"a"
In
Lu
Gj
V
Lu
6b
I-V
+1 �41
0
tto bl)
S2
y
Ira toob
I'D
t)D
Ell
Lu
—1
V7)
m-
cn
En
bf)
W
UD
crj

Tirr'le
(tTdnutes)
0
.l
2
3
41
5
6
7
8
9
10
12
'13
'14
15
Facility Name:
Biosolid,,', 4Ierm4 Wirnber:
Date:
Digester -Vernperature:
Sarripling Date/
Sarnpled By:
Analysis Date[firrie:
Analyzed By:
'I"'Otal Solids:
Beginrflng Ternperature:
End Temperature:
Dissolved Oxygen Level
Slope:
I ntercept'.
Correlation Coefficient:
Oxygen Uptake Rate:
ArnNent Specific Oxygen Uptake Rate:
Average Teroperature:
Temperature Correction Factor:
VV00003824
8/10123
23.3
8/10123 1004,
CS
8/10/23 '1009
2.0
MI M.
22.9
O.07
7A
0.66
Dry SoWs
egrees
egrees CelSiUS
4.27 mg Oxygen/hi
0.21 rng Oxygen/hr/g
23 degrees Celsius
0.86
Temperature Corrected Specific Oxygen Uptake Rate: =FjjBrng Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

00
x
0
6
m
Q)
CL
D
co
x
Nol
►J
CD m 00 r- (O In V co N r (D
(116ua) uoBAxC) POAJOSsoCI
c2
uO
�s
r
C�
rw
N
r
r
0
r
N
CD
E
0
00 E
Lo
C'7
N

Vecto� Atback,n Reduction
C' 2
A
)UR TEST
"j, ' M WW
i X
E) N G E-7 f"T" R, 40''a",
fl-00DERATURE A ]- G() LEC"flONL
EA a 0
S,/V\AFl_.E[D BY -
ANALYSIS BE(3AJN� DATE[ f � N� E.'
ANALYZED BY:
Ai',JAYLSBS ENDED DATE/TH0E
[D
B E G I N N I N G S I F?, I E S" f f"E IM E TURE:
ENDING SOUR TEST TEIMPEFZATURE: 'z "a,
n s D.O. mg I
-- — -------- -
10.
12
13Ea
14_
1 S
DO METER CALIBRATED: '� - W AT 01�51 _

w
. . .... . .. .. .. .
L
b1i
"(VI
Aq
AZ
AGay3
jz,
vj
l-tC7
71,
w
bO
JfJ
ll 4-
LU
CriFol
'All
............. mW
-
p
bYy
Lu
0)
p--1
Y._l
"D
17 bf)
fu
bf)
Iq
fT I
Ulf)
p"
b,D bf)
to

I i In e
(minutes)
0
'I
2
3
4
5
6 . 7
8
11
12
13
14
15
Facility Name:
Bosc)Hds Permit Nurnber:
[)ate.
Digester "femperatUre:
Szunpling Date/1-ime:
Sampled By:
Analysis E)ate/Tirne:
Analyzc,)d By:
-Ilr otal 1,3olids�
Bcqjinning Tcn"iperature�
End Ternperatffe�
Dissolved Oxygen 11, evel
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average -temperature:
Temperature Correction Factor:
VV00003824
8/14/23
25.8
8/14/23 1315
8/14/23 1324
Kt
2, % Dry Solids
CelSiUS
? 8 degre(
N16 decArees Celsius
013
7.9
0.93
7.63 mg Oxygen/hr
0.38 mg Oxygen/hr/g
25 degrees Celsius
O78
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

R
M
u
LO
x
N
0
u
a
(D O) 00 f- {p LO IT C) N O
(916w) uoBAxp POAIOSsI®
N
(D
u�
E
a)
00 E
p
Sri

Vector,Attraction Rc.,dt-dJU-1
Optiori,l - SOUR DATE:
TEMIFIERATLJFE A-f C','0LLEC­FK)N: 1:��
R,',)ATE/ k4 ,,,CA EC"] E D, �W -j
S 1.
ANALYSIS BEGAN DATEITVV
ANIAL-"(ZED BY� k, p
... . ........ .
ANAYIS 1,"-3 E f\ E D D A A h /I F 3
A5,,e &C,
BEGINNINCI G SOUR ­FEST'-FEMPERATURE; S?
ENDING SOUR TES TTDOP E RAI UR
rn e i n
... . . .......... . ... . ... ...
13t)
. ... . .......... . . . . . ...... . -.- . .....
53
. ... . ...... . .....
7
�40
. . . ...... .
12
(#1 4f 3
--..-,13 —.- ------ --
fe, lf,
14
J14-
15
4p
DO METER CAUSRATED: q�,jiLj-Q'5Al` I B 0 f?

ci
'"S I
bf.)
to
F- ELI
xr
bf)
bD
bD
60
Ob
ui
p
Cd
sl
cn,
ILI
CD
LU
P-o
da
aj
00
P4
14
ryI
Clio
VD
PL
bb 01) 1-
tz
UO
F-11
<
P,
P,

Thi'm
(rninutes)
0
'I
2
3
4
5
6
7
8
9
12
13
14
15
Facility Marne:
Biosolids Permit Number:
Date:
Digester TernperaturE
Sampling Dateffirrie:
Sarnp[ed By:
Analysis Dateffirne:
Analyzed By:
Total Solids-.
Beginn4ig Temperature:
End T'ernpeiatwe:
Dissolved Oxygen LevO
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate-.
Average Temperature:
Temperature Correction Factor:
MILTHIMI'MRINT011
8/15/2
2�6,
25
0.12
7.6
0.85
D Dry Solk.js
egreps Celsius
egrees Celsius
7.20 rng Oxygen/hr
0.36 mg Oxygen/hr/g
25 degrees CeISiLJS
0.78
Temperature Corrected Specific Oxygen Uptake Rate: = mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. 'I"he Calculation and the Spreadsheet execute automatically.
Updated 10123/2013

LJ
O 6� co f-- (O Uo IT ro N r O
(1/6uj) ua6fX0 PeAloSR1®
rF
N
r
O
r
c
Kel
Lo
IT
co
N

VeGtCl- Attracflon Red�,�ct�on
OpHorl 4 SOLM, DATE:
.......... ..
WWII IF`
. . . . . ......... . . .. ...... .
"ADOPERA"I'LIRE A"'1- COLLE-C1,10N..-
DATE-FfNNdLE" CIC)L L,L i
................ .. . .... . . . . . . . . . . ......... )
A N A L Y S � S Fil E G A 1\1 EV),"T Eff] 1\4 E g
ANALYZED B'(,.
BE -GINNING S('-)LJR 'TEST TEMPERATLIRE: 5
ENDING SOUR -n,7-,.s-F TEMPERA T' IJ R E:
'T �,me in Minu
DO g
............
...........
. ..............
10
12
13
'14
DO METER CALIBRATED: c R!j''j
c
�v
v
v

ll"
I
I
bf,
+
J
O
;Z,
7-D
Cj
0
bp
w
"V
J
Iv
II
4�
(7)
7-j
bl)
�71
VIC
chn
0
3
IN,
C/)
no

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling DatelTime:
Sampled By:
Analysis Date/Time:
Analyzed By:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
2
24
0.08
7.5
0,71
Dry Solids
egrees Celsius
egrees Celsius
5.01 mg Oxygen/hr
0.25 mg Oxygen/hr/g
25 degrees Celsius
0.78
Temperature Corrected Specific Oxygen Uptake Rate: =mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically,
Updated 10/23/2013

rn
m
x
u7
cn
CD
C�
0
F-M
O 0) 00 ti CD In It CV) N r^ G7
r
(I/BW) U013AXO panlossla
�r
m
r
N
r
0
m
0
i�
r-
co
Ln
M
N
r

Voc;b:,�r Adrac,,Jon ReducfJ( m
Option 4 - SU-IF? DATE, re,
M �Vllf S 0 U R T E S T
MR F
TDAFIEfRATI-RE A (" C, (1) LLE"(' Il (I'D b�,,l : "')
'15
VV L arr
IL
SAk/H­"LED E'3"Y,
ANALYSIS BECAN D/)Jl,,_/­fhME-.. I
AU` ALYZEDBYE
ANAYLSIS ENDED - ------- - - -- ----------- ­...........- /_
BE(.';H\fl\HNG' SOURTES"'r "FEk/lFlER/\_FURE:
E 1\1 I'- I )ING SOUR TESTT"ENeil PERATURE.- ), + 11 ele,P('
. . . . . . . ........... .................... f ..... ...... .
vTng/l
.. . ...............
0
. . . . .. . .............. ------
- am
2
. ....... . ........ 3
Le 1-1 Pl�
.... . . . ....
IRS
. ... . . . ....... . . . .................
. .........
51
tl
12
(e
14
t �tl
DO METER CALIBRATED: Al- At
. . . . ........... p

on
IX
kp.
Fz
rr,
dz
ILI
_i
Q
.
.
—
/I
14
f,7
21
lie
/(o
Lu
CA
00 bfl
U)
�121
cri
bl)
I
z
bf) t)b
r,� Fl, u
C)
cr)
" >
f—I
0
Qj
a bf)
�A]
11 0
I
UD
DID

C)
(D
1"-
C)
(Y)
1�--
IT
c
(L (N
0-
0
IF)
(X)
(C)
I-
(\I
(N�
1,0
It
N-
(X)
v-
G)
CO)
LC)
LO
'IT
(NI
C-)
C)).
(Z)
(3)
0
(),
(Y)
0)
C14
w
CD
c
0
M
0)
W
CO
Q)
W
ED
00
QD
I'-.
(K.)
P-
(X)
r-A
r.-
i-
C-D
CO
(D
NY
(V)
00
0)
(1)
1--
in
Ix)
V)
-q ,q-
-q-
00
f11-
('14
6
C-)
(6
(N
Nr
(X)
(D
(D
(0
(D
(-)
oi
aj
(xi
aj
c6
oc;
o6
(xi 6
(d
6
o6
c.6
c6
aJ
1.0
)
0
CD
M
G)
(Y)
0)
0)
0')
0)
LI)
(Y)
04
(5)
U)
o)
oo
GO Co
(X)
co
(y,
C)
0
o)
(J) c-
C�
(
0)
00
GO
00
I--
W
P--
V-,
(0
-j-
N
n-
U)
(14
(3)
0
0
06
00
r--
00
P-
I--
P-
P,�
-�
f--
I`--
(0
(0
(,0,
(.0
02
(Y)
()0
()0
t-
C)
00
00
m 7*
0
m
.... . .
. .....
"
N
m
m
.
"
... . .......
m
n
r-
Nt
1-1
w
("-4
-'r
L()
C,)
-j
(.0
(X)
9
CY)
(Y)
V.-
C)
0)
00
00
00
CX)
CO
1'-
11-
CD
(0
0
co
0
cy.)
0
0)
Ou
00
OD
00
co
r-:
f-,
1-,
1,-'
C)
0
(0
IX)
Ct7
0
0
N
0
)
in
C14
V-
y-
0
cry)
to
CIO
r-
00
M
0
1,-.
eq
(14
r-
�T
C-)
m
m
m
m
N
w
r-
r--
w
w
0
LO
0)
C)
>
w
w
w
w
w
w
00
CO,
fl-,
t--'
],--
r-,
1,-,
P-,
0
I
. .....
. .....
L.J
0
W
00
M
0
T-
CM
cll�
-r
W
W-
-(yj
E
E
E
oo
00
—
CD
(1)
CL
CL
(n
CD
w
N
(D
0
E
U,
E
(n
E
0 E
0
CL
(D
E

Tirne
(rr,iinutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
'15
Facility Names
Nosofids PeFrnit Number:
Date:
Digester' "TernperatUre:
Sa
mpling Date/Tirnw
Sampled By�:
Analysis Date/Time.
Armlyzed By'.
I otal Solids,
Scgnning Tempenature'
End Temperature,
DisscAved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate-,
Average Temperature,
Temperature Correction Factor-,
WQ0003824
mHauumMENmmmmmmuwmmuumMNIN PON"i-
10/9/23
15.6
M�m
10/9/23 1055
CS
..�nm
1019/23 1101
CS
IYo Dry Solids
I" degrees (,Ile�s slu
16.2 deorees CeISLIS
4.95 rng Oxygen/hr
0.25 mg Oxygen/hr/g
16 degrees Celsius
1,31
Temperature Corrected Specific Oxygen Uptake Ratef._,I.M mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes, The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

R
07 00 (D It N 00 00 Co N [n 00
(116LU) UOFJAX® POAIOSSl®
t--
�r
cm
N
C]
m a�
E
CD
co E
LO
r

Vector Attraction Reduction
Option 4 - SOUR DAT E: j
GRAHAM WWTP S�OUR ImEST
DIGESTER-. . . ... . .....
TEMPERA"I"IJIRE A-r, COLLE("A
DA"FE/T]ME COLl EC FED:. , 1,
SAMPI ED BY:
ANAL.Y= BEGAN DA"FE/TlME,,,,,� ,l i. .................. . .
ANALYZED BY: (7
. ........... . ........... ....... . . . . ....
ANAYL.SIS IEN D DATERIME:I,(,-j 4:", I /, f C �
.. .......... 1 --
BEGINNING1 S0l,.JR TEST TEMPERAT�JRE,,,
ENDING SO�JF�'l"ESI"-�EIV�PERA'T(JRE-..
Time in Min'��
`-4
12
............. . .........
13
14
0
DO METER CALIBRATEDj AT u —.--fi,alyst_
rnglL
J,

I
rn
Ca
fx�
11P
CD
bf)
Go
ia�
04
(5
ri
'21
2
F1
57
c9)
uo
P,Sl
0 1 1 , lr--
z
i 4��j
bf)
bb
1 $
cn UD
CII

"I"i m e
(minutes)
0
1
2
3
4
5
6
9
10
11
12
13
14
15
Facility dame:
BiosoHds [�Ierrnit NUrnber:
Date:
Digester Tewiperature:
Sampling Date/1-irne:
Sarnpled By:
Analysis Date/Tin,)e:
Amaly7ed By:
[otal S,olids:
Bcginning Temperature:
End "'I'emperature:
Dissolved Oxygen Level
Slope:
intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
AmNent Specific Oxygen Uptake Rate:
Average Ternperature:
Temperature Correction Factor:
vv()000�
1011
'10/10/23 08
10/10/23 09C
K
16
MR
'18
0,07
8,6
0,86
D�y Solids
egrees Celsius
egrees Celsius
4.50 mg Oxygen/hr
0.22 mg Oxygen/hr/g
18 degrees Celsius
1,14
Temperature Corrected Specific Oxygen Uptake Rate! mg Oxygen/hr/g
1....2.
Instructiorm Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

N
d-
C6
x
d
WJ
O CD o0 CD LO m N �- d
r
(i16W) ua6AXO PGAIOSsia
cc�
m
r
N
d
r
c
I-
(D
Fai
co
N
i

'Vector Attraction Redudion
DIGESTER- t
GRAHAM WWTP SOUk . .... TES ------- T ----- - -- - .. ......
'A N E t II I COI__t. ECT to
f
BEGINNING S01..JR IEST TEMPERATURE: lj
ENDING '-' )OUR I'EST'I"EMPERATURE:
P in 1r1ut.
_..mmmm.....
D /
....._.....
1
1
s�
b
14
p
15,
DO METER CALIBRATED AT Analyst

0)
E
Pb
rtD I.
UD
(,0,
4Z
Ll
cn
M�F7,7.C/D
,J
CD
CD
bl)
ta)
�nnl
LD
cz
C/D
ca
era OE
�
5
�71
pil
R4
Z,
un

Time
(miiNei utes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Facility Narne:
Biosolids Number:
Date:
Digester' Ternperaftire:
Sarntflirig Date/Time:
Sarnpled By:
Amalysis Date/ I ime:
Analyzed By:
Tol-al Sobris:
Beginning Temperature -
End Ternperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
'Terri Peratu re Correction Factor:
VVQ0003824
.m.-MMOM woumonn
'10/12/23
2/23 0901
1 OPI 2/23 0909
KP
2.0 % Dry Solids
15,6 degrees Celsius
17,41degmes Celsius
0,15
8.7
0.92
9A7 rng Oxygen/hr
0,46 mg Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake fate: = mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

L
co
c6
x
w
N
L
0
n
a
E1
X
......... ........... .
0 0 0 0 0 0 0 0 0 o a
p O O O 0 O o O O O o
o m 00 r- (I/BWI UOBAXLp paAj s51(] ri cv r o
I
m
N
r-
0
r
I~
EW
LO
0
N

Vector Attraction Reduction
Option 4 - SO� UR DA f"E . ........... . . ....... . . ............................................
GRAHAM WWTP SOUR TEST
D N G E X`3 )"T f-" R -, I
TEMPERAT(JRE Al"'COLLECTION:
DATE/1-WE BOA AL-EC"TER,
SAMPLED BY-
ANALYSI'll') BEGAN DATEMME
ANALYZED B'Y-,
ANAYLSIS ENDED DATE[THME-
BEUNNING SOUR TEST TEMPERATL)RE:
ENDING SOUR TEIS)l
vyzln Minutes—F
D. mg/L.
. . . ........... . .. . ..............
. . . .......... . ......
....... . ...............
........ .....
10
At,
11
12
'13
is
DO METER CALIBRATED: st d, . . . . . . . ... .............. . .

c
Z�
!'Q
. . . . . . .. .
LU
"1-)
-45
err
0
b bn
En
Ll
T-1
(n
w
0 14 oo DO
0
al
rQ
u
4
iwnx1�
4-4
U)
LLJ
u
.60
sad
Cv
Cl
N \X
cn cn
bFJ W)
bl)
bd)
uo
bo

Tiiate
(minutes)
0
1
2
3
4
5
6 .7
8
9
10
11
12
13
14
15
FacHity Name: 1G7,,RAHAN/I VV 0"o
Biosolids Permit Number: VVQOOO
irate I UP
Digester Ternperatt.rre:
Sampling Dateffirne: 1 ON 6/23
Sairnpled By:
Ariafysis Dateffirne: 10/ 16/2 3
Analyzed By:
Total Solids:
B(,;,ginninq Ten­lperature:
End
Dissolved Oxygen Level)
Slope,:
Intercept:
CorreWtion Coefficient..
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate,
Average Temperature"
TemperatUre Correction Factor:
11
15
OM
8.6
0.81
'D Dry "'.3olids
agrees tealsines
egrees, Celsius
3.35 mg Oxygen/hr
0.17 nig Oxygen/hr/g
17 degrees Celsius
1.23
Temperature Corrected Specific Oxygen Uptake Rate-, mg Oxygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

is
Lq O') LO 00 Lo f�
C
(JIBLU) UO6AXO POAIOSS814
zt
LO
r
r
m
r
N
r
r
O
N
m
c

Vector Attraction Reduction
GRAHAM WWTP SOURTEST
NGE ATE : J
D F. II !L.m..A - Y tl W Y CL L II..._. C TE M..,,✓ 1
ANALYSE BEGAN DATErrw-,)�.,�
Tirr ire
.ute
�......
�W .._ _ .....�
ff f.r-
4m....�.:.®_.w.m.
pig
12
q'
13
is
v„1 - �f
DO METER CALIBRATED: w AT Anal st i
% " l rm7 IL

Ql
Ell
141
i El,
ea
i
U-j
03
tb
a1
[-LA
.51)
-8b �bb bp bD
HI, 5 0 oi
I P; 1 �,5 � , ,
V)
�-j
,—i
DO
bb
bf)

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
'15
Facility Narne:
BiOSONJS Perry"flt Nurnb(:
Date:
01gester Temperature:
Sampling Dateffi�rne-
Sampled By:
Analysis Datei"Mrie:
Analyzed By,
Tot�.,fl SoNds,
far ,,ginrdng Temperah,.rr("'!
End Ternperature:
Wss6ved Oxygen I -eve]
Slope:
I ntercept:
Correlation Coefficient:
Oxygen Uptake Date:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
GRAHAM WV
WQ!0003
13.1
W�
)901
10/17/23 0911
KP
7
2.0 % airy SoNds
�MMM��-
14:14 degrees Celsitifs
16,3 degrees CelSiLIS
0.06
91
0.85
3.60 mg Oxygen/hr
0.18 mg Oxygen/hr/g
15 degrees Celsius
1.40
Temperature Corrected Specific Oxygen Uptake date: =0.25 mg O,xygen/hr/g
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 10/23/2013

r10
LO co Lo
m C
(I/6w) uaSAxp POAJOSSrCI
r-
�r
c�
0
E
0
co E
m

Vec,tor Attraction Reduction
Optiori 4 - SOUR DA FE
GRAHAM wworp SOUR TEST"'
NGEs-rER-
TEMPERATUF�E AT COLLECIION) % I I
DA-[Efl-IME COLLEGTED:..-� i W11�14,1
—! — --------- . ..... —
SAMPI ED 1-3Y--
ANALYSIS BEGMN DATE/TIME-,
AN`NAI YZED BY,
ANAYLSIS ENDED DATE/ HME,_
BEC'MNING SOUR TEST TEMPERATURP f "'I - L—
ENDING SOI.JR"I-ES'l''FENMPEIRA"f'LJRE: i AIY -"",
ThTle in Mint,ites
D.O. mg/L
. . . ........
. . . .......
. ....
10
ILI 11"
'12
13
14
15
DO METER CALIBRATED: - ----- -- AT Analyst..
" i�r,J
4k
% - mg/L

C.)
u
rn
S i4
C)
ern
rj
0
57
C4
Ul
x
x
C/)
bJJ
bf)
ofj
to
cn
on
P-4
6—j
V�
t�
I
bf)
'--
DO
C.
bLO
tj
cr) or, cr)
41
Xl
1p�,

naie
M i ni U Ites
2
3
4
7
8
9
10
ill
12
13
14
`15
Fadkty Name:
Biosolids Flerrnit Number:
Date:
Digester Temperature:
Saryipling Date/Time:
Sarnpled By:
Anaiysis Date/"Firrie:
Analyzed By!
Jotal
Beginning Temperature:
End "remperature:
Dissolved Oxygen Level
Slope-,
lntercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature."
Temperature Correction Factor:
GRAHAM W
W()000
'13.
lXy Solids
T4 "i degrees Celsius
16 ijbegre(,,s CelSiIAS
O.07
8.8
0,82
4.32 mg Oxygen/hr
0,22 trig Oxygen/hr/g
16 degrees Celsius
1,31
Temperature Corrected Specific Oxygen Uptake Rate: = mg Oxygen/hr/g
Instructions.- Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.
Updated 101/23/2013

C]
r
ME
LJ
C] 0] 00 r- CD LO Nr m N r C7
([16w) ua6Ax® POAJOSsi®

Vector AflTaction lRe(JuCCN n
N IG H' S"FER:
DATUTIME COLLECTED: ILL
SAMPLEF) BY:
ANALYSIS E G N [) T E/ I I N �:� �,.:.�....... ........ . �'
ANALYZED BY:
BEGINNM � OUR .TI EST 1m", M ER TURF: r,�,
ENDING S C: L1 N T m [.. ,T. Nth : N A_]-N,.J
Time in Mi -P I
N O img/L ..._
_,.......M..
1
'?r
1
'
1
1
DO METER CALIBRATEDD fsi �!°���-�.:"..A� _"_.�:�.�' ��..__.__._...Analyst _... r
J
,,, % - __ "b mg/L. � ,

rE
Lu
0
17)
bf
�Ti
NO
C/D,
bl) tf) tw tDO
r—1 5, ol
-TI
ay bf)
bb
bf)
1
f7
("") (/) (f)
on
z
1
tom'

"I"ime
(rninutes)
0
1
2
3
6
7
8
9
10
,11
12
13
14
15
Facility Naffie: GRAFIAIVI WWTI-)
[3io,solids Perrnit Number: WQ0003824
Date
Dgestei Ternperature:
Samplim g iDeiteffirne- 10/1
Sampled By:
Analysis Dateffime� 10/1
A nzilyzed By:
Total Solids:
Beginning Ternperature�
Enid Temperature:[
Dissolved Oxygen Level
Slope:
I ntercept:
Correlation Coefficient:
12.
9
3 091 11
20 11/a Diy Solids
�wu
`, _/ degrees COsk,is
16.0 degrees Celsius
1;
Oxygen Uptake Rate: 3,93 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.20 rng Oxygen/hr/g
Avei age Temperature: 15 degrees Celsius
Temperature Correction Factor: 1 A0
Temperature Corrected Specific Oxygen Uptake Rate: mg Oxygen/hr/g
Instructions! Enter Data in the Blue Boxes. -rhe Calculation and the Spreadsheet execute autornafically.
Updated 10/23/2013,

LWJ
LO q7 LO 06 Ln f— Lo
O] 00 CO
(I/BLU) UOBAX® POAJOSSla
LO
r-
r
c+)
r
N
r
0
N
E
CD
co E
ti
d-
c�
N
r

Vector Attraction RedUction
Op[Jon 4 - SOUJ��� DATE:
GF 1AHAM WWI P S 0""' UR TESoT
DIGESTER:
TEMPERATURE A"TCOLLECTK)NI:
.....................
DATEMME COLLECTED: � �,, �,,, 1j / r1i lo,'
SAMPLE'l) BY- " I
ANALYSIS BEGAN DA]"PIAME:
ANALYZED BY.
ANAYLSIS ENDED DAFUTHVII-�!:`.
BEGINNING SOUR-m-s-t-TEMPERATI IRE: rlf� (,
ENDING SOUR TEST TEMPERA LJRE-. f /," t "
DO METER CALIBRATED: AT C, Analyst
. .......... .. . . . ... . ....... . .......
C

El
ho
76
'43
F (D
bl)
ryry
0 1 1 _r-
Lill
r1b
CD
t7f)
Ul
U')
va
0
09
CD
1)
-6b
I.
bf)
bf)
r4
bJJ
bb
bQ
tc
yR
I

ANNUAL PATHOGEN AND VECTOR ATT RACTION REDUCTION FORM
Facility Name. CH"Y OF G.RAHAMPertnff Number. WQ0003824
WWT P Name- CITY OF GRAHAM N111DES Number; NC0021211
Monitoring PeriodFrom I/l/202'3' 0 3/31/2023
...........
Pathogen Reduction (40 CFR 503.32) Please indicate level achieved and alternative perforkned:
C lass T: r . . .... A I to rna.1i'vel Alternative 2 Alternative 3'
❑
a ti Ve 5 Alternative 6
Alk,,rna i 4. ern Alt
11'applicable to afternative per -formed (Class A only) indicate "Process to Further Red"ce Pathogens"
....... . -
. .. . ............... . .. ... . ..... - - --- ------- ...
1jearl,reatirlent -1 Therillophi lie
i leat J.Jry�ng M E
.....❑ . . .... . ...... . ..........
Beta fkav Garnt-na flay Pasteurization
........... . Alternative 2 Alte7n7ive 3
'Ve.... . . . ............ . . ........ . . .... Titer,na c
if applicable to alternative performed (Chiss B only) indicate "Process to Significantly Reduce Pathogens"-
----------
Urne Stabilization Air Drying ic Digestion
Anaerobic Digestion El
.If a p I t altermma9ive Performed (Class A or Class B) complete the following moniforing data- -A —6 5Tychi —1 —caT
Allowable Level Pathogen Density Nomfie� 6f'Trecl�Fncy Sarnple
Pararnetcr Excve- of Te-
irl SlUdge MinitriurGeo, MenMaximua Units d_n�es_Alra ems_
Tpr a_--.__-- ­­­_ e MCh
2 x 10to dre Lq_
61h
po%ver MPN per 0,005 0.009 0.017 WIN 0 QTRLY GRAB 9221 B/L
granr of total
o lids or-) x 10, k)
f,'ecaj (,ojiforrn the 6th power
. . ... .......
1000 n1pil Per
gram of total solid
(dry ,,Height)
Salmonella bacteria 3MPNper 4
(ill lieu Of fecal grarris total solid
I coliforni)
Vector Attraction Reduction (40 CFR 503.33) ­ Please indicate option performed:
CERTIFICATION STATEMENT (please check We appropriate statement)
* "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.3�2 and the vector
attraction reduction 1 0 CFR 503.33 have been met."
,Le�quirernent in 44 ............ ........... ......... . .
* "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an expllanation why you have not met one or both of the requirements.)
"This determination has been Ruade under my direction and supervision in accordance with the
system designed to enstore that qiialified personnel properly gather aril evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been rnet. I
an aware that there are significant penalties for fialse certification including fine and im prison inen L"
Crispian T. ROLIth / I'lant Superintendent
Preparer Narne and Title (type or print)
Signature of Preparer Date
Crispian T. ROUth / Plant SUPeFintendent
L,and Applier Narne and Title (if applicable)(type or print)
Signature of Land Applier (if applicable) Date

ANNUAL PATHOGEN AND VECTOR ATTRAcriON REDUCTION FORM
Facility Name: CITY OF GRAHAM Vermit Nuinbei,. WQ0003824
WWTP Name: CITY OF GRAHAM NPDES Number: 1" C0021211
Monitoring Period. From 4/l/2023 0 6/30/2023
---- -------
Pathogen Reduction (40 CFR 503.32) - Please hidicate level achievedand alkerjoifive performed.
............. `Xlt�7,;'ative I Alternative 2 xli�;-iza-tmve- El
- - - - ---------
Alternative, Alternative 5 Alternative 6
If applicable toalternative perforpried (Class A only indicate "Process to Further Reduce Pathogens` .
T—
�S heat -Freal.aient 1"herrnophilic
Coll eat DIX, 2,
..........
Garnma, Ray ion El Beta, Ray
Iris l3: Alt lllative I
Alternative 3 El
If applicable to afterliative performed (Class B only) indicate "Process to Significantly Reduce Pathogens"
.... . ...... . ---- -:. - --------- ----- . .. . ............ M—
Liole Stabilization Air Drying composi Aerobic Digestion
Anaerobic Digestion El
If applicable to anpternative performed (Class A or Class B) complete the following moolito -ing data.,
N'-Liiii-Ber—oT-'T,re—ciCie-,jic—y -- n , C-1 I —y 57
AllmvaWe Level Pathogen Density S"I'luple Teell-
ParalTICACt' E'Xcee- C) Typ(�,
ill Sludge MillilllUai Geo,, Mean Maxin-meni Ui-lits den A IIWJ�j
. ......... .... -- . . . . . . ............... --- —Al 111=5
2 x 10 to the 6th
power Ml-`N per ().()o 1 0.,002 0.00/1 MplllJ 0 QTRI,,Y GRAB 9221 13/13
gram of total
solids or 2 x 10 to
Fecal Colifoni,n the 6th power
L,rlll of
I 000 mpn per
gram of total solid
(dry weight) . . ......
Salmonella bacterial 3MPNpei-4
(hi lieu of fecal grains total solid
coliforna)
. . . ........ . ...
Vector Attraction Reduction (40 CFR 503.33) -- Please indicate option performed-
CERTIFICATION s,rATEMENT (please check the appropriate statement)
9 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 an(] the vector
attraction reduction reqnirentent in 40 CFR 503.33 have been inet."
- — - - ....., - - - - - .................. . . . ...........
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been inct." (Please note if you chech
this statement attach an explanation why you have not niet one or both of the requirements.)
"This determination has been inade under Ruy direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather, and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been mnet® I
ann. aware that there are significant penalties for false certification including fineand imprisontnent."
Crispian T, Routh / Plant Superintendent
Preparers, Name and Title (type or print)
ld4g
Ct'ispian'f. Routh / Plant Superintendent
Land Applier -Name and Title (if applicable)(type or Ian-int)
Signature of Preparer
Date Signature of Land Applicr (if applicable) Date

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name- CITY OF GRAHAM Permit Number- WQ000382d-
WWTP Name: CITY OF GRAFIAM NPDES Number: 14C0021211
...... .... . . ........
iWonitoring Period- From 7/1/2023 To 9/30/2023
Patitogen#Ze(itiel-ioii(40CFR50�3,.32) Please indicate level achievedrind aherilafive perforl.�I'ked:
ci; S X]" Afternalive I El I AlternativcAltemative 3
2..
.... . . . ...
Alteniative 5 Alternative 6
e 4 Alternat
If applicable toalter native pertnped (Chiss A only) indicate "Process to Further Reduce Pathogens".
I leal. Trea
Heat Dryin Thertnoph, h
Compost, El
. ........ — — - --------- . . .......
Beta R,ay
—17—EGan-irria 1tayLL E
iaS;T.
........ . ..... ...........
If applicable to alternative performed (Choss B only) indicMe "Process to Significalffly Reduce Pathogens".
. . . . .................
Lime Stabilization Air Drying -01TIposting robic Digestion
Anaerobic Digestion
[Aicable to I f ap alterna I e performed (Class A or Class B) complege the followia g Allonitoring data.
--T Nq-61-11F)e-F—OT -reqtIoncy ytica
Allo%vable Level PathovIn Density Tech -
Parameter Excee- of' Type
in SILICIgC Mi ni MUni G co. Mean Maxim uni Units dences -1\.naly-
. ............
2 x 10 to the 6th
powei, WIN Per 01.001 UO2 0.0105 MPN 0 QTRLY GRAB 9221 B/E -
gram of total
solids or 2 x 10 to
Fec,al Cohtbrm the 6f h power
of
1000 n1Pfl PCr
zollmil of total solid
(&y weight)
T, I -, i bacteria 3 M TIN per 4
(ill lieLl Of fecal grams total solid
colifonli) (dry weight) .. . . ...... . . . . . .........
Vector Attraction Reduction (40 CFI 503.33) - Piearse indicate option perfornied.
CERTIFICATION STATEMENT (please check the appropriate statement)
"I ceo-tify, under penalty of law, that the pathogen requirements i,n 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 50,3.33 have been me.t.'l .................
.... ............... . . . . . . . . . . . .. . . . . .
9 certify, under penalty of law, that the pathogen requirements in 40, CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been meet." (Please Panty if you check
this statement attach an explanation why yota have not met one or both of the requiremeillts.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the padiogen and vector attraction reduction requ I irements have been niet. I
am aware that khere are significant penalties for false ccrtification including fine and imprisonment."
crispian T. ROUth / Plant Superintendent
Preparer Name and Title (type or print)
Crispian T. Routh / Plant Superintendent
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer
Z el
Date Signatt,111-C of Land Applier (if appticable) Date

ANNUAL PAT110GEN AND VEC'rOR ATTRAC710N REDUCTION FORM
Facility Naine-, crry OF GRAHAM Permit Number- WQ0003,824
WWTI'Name: CITY 0['GRAHAM NPDES Nwimber: NCO021211
. . . . ..... ....... . ........................................... . ... ....... . . .
Moplitoring Period. Fron-1 10/ 1/2023 f , 0 12/31/2023
. . ....... . . ...... ................. . ........
Pathogen Reduction (40 CFR 503.32) Please indicate level achieved andalternative perfortned:
hass A. Afternali ... Alteitmtive ' 2 Alternative
.. ......
-na
Altetnaiive 4. 5 Altei"native Altet tive6
.............
Rapplicable to alternative perforined (Class A. �orgly) indicate "Process to P'Rirther Reduce Pathogens`
Thel"t-nophilic 17:T777.
.C101,11post Heal Treati-nent
Beta Fa; 0 Ganit-na Ray Paste til, i zati On
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
F1
U-i i I —iz a-tl El AitDi,ying Cornposting Aei,obie Digestioti ❑
. . . . ...........
... . . .............. Anaerobic Digestion
It' a pp fica ble to a I terna five perfo rah ed (Chass A o r Clas
s B) coin plete ti followilgitiollito-ingti.itai,,
Numbe, r
AHowable Level Pathogen ensity Fof Satnple
Parameter l"Acee.- of'
Uni(s
ill Sludge Minimum Geo. Mean Maximut Type
dences Alm le
............ . . .
2 x 10 to the 6[h
powclr MPN per 01,010 11 0.007 0,012 MPN 0 QTRI,,Y GRAB 9221 B/E
gl.,9111 of total
solids or 2 N 10 to
Fecal Colif'orm the 6th powei-
-2F�U p—uma—nlof
1000 mpn per
gram of total solid
(dry weight)
Salllloliclla—Nqcteria 3 MPN per 4
(hi heat of fecal granis total solid
0 1, ii 1116 1 . 1,11) (d, wejgl�
Vector Attraction Reductiopi (40 CFR, 50333) - Please indicate option performed:
CERTIFICATION STATEMENT (please check the appropriate statement)
9 certify, under penalty of haw, that the pathogen requirements in 40 CFI 503.32 and the vector
attraction reduction requirenrent in 40 CFR 503.33 have been niet."
.. ...........
4 certify, under penalty of law, that the pathogen requirements, in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFLU 503.33 have not been met." (Please note if you check
this statement attach an explanation why yoii have not imet one or both of the requirements.)
"This determination has been made under ory direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to, determine that the pathogen and vector attraction reduction requirements have been imet. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Crispian T. Routh / Plant SUperintendent
Prepa.n'er Name and Title (type oi- print)
x,
k"
1�
Signature of Pireparer Date
—Crispian 1'. Routh / Plant Supet'intendent
Land Applier Name and Title (if appl icable)(type oi, print)
Signature of Land Applier (if applicable) Date

CD
O
cn�
-1
N
�
Np
Gu
© = Z
C Q) �
LL fq (j) N
Z C i(7
O to
07 N
® Z Z
•m+ {V N
O y{4�
C
O O
G Z Z
ry
Z
P!j
U)
W
N N
© Z Z
` N N
®
N N
C Z Z
"
Z
UJ
i.
U)
W
C] N O
m C1 0
© O
U 0 C
g
©
Z C7
T
L30 0
�a 0
Q
LO
LO
T
V
h]0 0
Q�
No O
Q O
C O)
f�l
G
tV
f9
(6
tll
C C)
N
C_
m M
Q d
11 0-
d x E
a�
U
y
m
U
m
j �
Uy O O
.... C
`� Ui 0 C)
c r-
•O
O N 3
to �•-�
C
O
4f7
C
U n LO
ro� C) LO
N
.7
m
E vco
m -a
Z x» o o
c
Z moo
C o
V
p
m
®
o
n U m
Lcf2
U r!S
ro
O
c c
0a 0
u�
co
C)
OD
co
tm
v u
w
00
co
U) IT
O 0 0
0
CL
o
a..
o
w
o
U
�E . �,
"
�,
"E
o 0
o 0
E
z o o
e
0 o
E rn
LLf LL
N N
F
r N
� V
C?
Z
U NC)
Z — LO
d
m
N
[n
tli U p CD
N
V O C)
i r
C
E N o o
-E
E
y o
E
-� G
U
-� G
0
r
C)O
a
O
o
w
az
ate
-,
a rn
a
t
m
• U
N ` `
�-
N
c
N
m (7 C7
C
m C7 C7
r
[1
w O
V 00
,y
$ 00
m
wr _
N a)U
E V V
0 V
w Q O
Q N N
E U U
V v N
Q O
E Ul N
V
N U7
V
p p
0 0.O Lv LW
u G0 LL 1i
o
v v
C)r04UrN
�
i
E m
c m
O
C)
W
UJ m
O
b
Qs`fc`�
N
C O
O
Cl) =
a
o
_
o
o
m
--
h
fA J
I-

0
Lo
0 0
0
0 0
TO
0 0
awl
C14
c
z
1=
0 Z Z
CD
0
0
m
(10
0
z z
Z 2f,
0
z z
U.
CL
LU
ri) o o
z
T kn
V)
I.
C) o
N
:2,
CD CD
0
(D
C
P,4 (0
12
IT
(D
kn
uy
cl 0-
P4
rm C-C),
T
Z,
m L4
re
(ki
(a 04
to
r
as
uJ U) o 0
r ('�I'
0
co
V) cD CD
0
d)
0
D
0
n
CN
E
Z71
00
co
. (N
z 9,
0
EN
f7l
0
6,
ED
>
0 o CD
0 0 0
a
0 C)
CT)
LO
m
00-
(D CD
0 Cl.)
0
0
"T
Lo
000
ko
0 0 0
N
U5
000
cq
CL
CL
LL
;",:,
F
0 r,
CD 0
0
a, 0
0 0
E
E
Q 0
CV C�9
(a w
0 CD
N (N
M CO
N
M
ry'0)
0 co
00
co
0 0
.11
0
a) m o o
C3 0
—
0) 0 00
2 c-,
r
yw.C),
0Gay
CD
CD C'A
CIA
EL
n n
NI,
E r-
F E
Ef F
65
r
V) 0
z
U) ul
(n 0 w
U) 9)
0 (n V)
CL
z
0
(D o
.0
.1 6
co U"
is CJ
'a 00
00
00
E
UJ
a
E
C) 00
w 0
Lu <t b
E U) W
E 0 U)
E (n 0
W
0 L� U-
q-
10 ClCD CO
.
LL U-
0 Ll (D 0)
LL, LL
-E
U)
o
fn C)
1
co
�2
LU
w
C)
til L6
0
0
Lo 0 -r
0
lc
7r
0
m
-4:
0
0
C�
U)
7S
6 0
0
0
M
0)
(n
0
06
<
i
rz
�E
a,
a
(D
0
E E
F E
E E
ly,�
0 X 0
z
U)
0 _J:
g

......... - —
z
- --------
Cl)
0 0
Il
I
'1
0
C)
z
i , z z
z
Z 7
0 0
z
"PI CIA N
"J
E,
U)
Iq
6 6
U)
0
rL
CM Z Zi
Z Z
Is-
00 c) o
c
(p
u
(D 0
Pli
LO
0
I.-
(D
X
(.o
G)
0-
ITI
v) c-) C)
M
1:9
0) CD 0
35
=
Q)
Z CD
0 CID
Z Ln
00
Cw
m
a)
m
c per.
0 ci o
a 0
a cr)
ewa
CO
a r---
ko
0 0
0"
000
N (7.) CD
a.
a.
4
CL
0 (D
0 C)
C) C>
Q (D
QJ
,,grow0
z
0
c"I N
(D
6
ens
ro
0 0 0
0 C:)
z
w 0 0 CD
Z
C) 0
z
E
w
0
co
0
CD W
17
U) U)
(n V>
cn U)
0 0
CP91
0 0
0 0
— —
— —
d) a) a)
-- —
(D (D
0
0) a)
n :3
L) 0 (D
:D -
L) 0
:D
0
lw
E 0 0
w
Q) U)
0 CL (D Q)
U3 0)
0 0. Q) (D
(n co
0 (D a)
0 0 LL
LL LL
"E
0 0
M ,
fy o N
Gs
C7 ra
C.)
U' Get
(D
co
m
(Y)
E
w C6
LU
w
0
0
C)
CD
C5
C)
LO
C)
0
E
w
C:)
(0,
12

...... . . . . . .......... . . .
.. . ............ . .. . .....
(D
LO
0
z
z
C)
z Z
6 ate,
ul
LU
rl) o CD
on )
0
z
t) 0 0
W
Z co
o 0
N
00
W
C:)
a s-
00
co 10
tl,—o
CD LD
if) 0 ("1 (N
0
E
o o
0
0
CP
>aS
C) C)
0 Cll� 0
xu
LO
7 0
N
U)
0
000
0 0
-1
0
ce)
C-) 0
0 0
(NI C\j
6
q
W
z
A
0
F
Z co
ay ca 0 0
0
C.5
CD
tO
Lf)
F: E
(D
E
V?
C�
0 (15 M
m (o
z
V) fn
T 2
(0
0
6
ol )
'a
rm-
m 0 (D
CL
0 0
V 0 0
m
C�
E Do Do
w
E U) cn
o a 0 W
I'L LL
C
9
U)
:se
In S77m
'o
E
w
ILIJ
Q
0
r-
0
0
(n
0'nY
Gets
ca
(n

c')
c) Liz
Q
E
C.")
W
.7,
L
(D
cl Q
0
N
i7i q
ol
tz
-Fj
03
vo
x
T �2 �5)
0)
r.:
(U
V)
c 'vi 73
z
n, 0- E-
Q)
x
.. f-,
cl.
13>
L) 0
E
u
Cr
63 F,
r s:
>
fa
2 IFt!
Lu
Ili Cda
C.)
c
c)
's
c.
2
CL
6. s, E
�i
r, 0 0 D cl
fO Y) V-1
0
z
cL
-1
o
0
0--
n-
W
0), ag Ui
M W 0 �O ()
0)
u.1
� ZEE
n
:r
:z z z 0 m. CL CL
Co U) r'l N
lCka..p
(Z",
_0
a.
>
0
0
cl c:
c3
U}
C cD
0
5,
vu
")
c (b -, ,
:3 Zi (1)
0) 0 -.0 04
N U)
W
0
(V
4
2-
..u)
0
0
sz
-c' ,
E
0
C--) c
C')
0) :3 (-;)
w o
Q- 0
tD 0
fy �:, Cr'
(1) r.
>
-
I
ry)
0
> 0 q)
V (D
CL T)
,.- — . -
(b
(1) (f)
cn Cl Iz
as C-)
w
S
> >
c (1) 0 'T
-
N
Z 6 ---
a
m (V (0
C..) - M
cn
KC
a)
(n
C'
0
u) (o
12 E
2 r- I -
-Cz U)
1-
(D
(1)
T ,
-0
U) u)
0
ua
>
--
- 0
u E
E E
Qjfla
.0
0
U
ca 0 'F
CL E U
'c:
L: co
E
c.
(1) c')
u) U)
�2 0
(Z
cl, :�T-
d
CL -a E
0 a) W
v
0
10
N
r-
c) --
cu fX 0
M
's 2
(o Q) NI
Z2
E
r_
E
> C =
16
m
b)
-
0
Cu
F,
0 (1)
(TI
iv -
(7,
4)
v) rVi
U)
CX Q 0
to-
E c)- Ili i"5
1, 0
Q)
Cu
0
(1)
— c _0
'z�
C�L CO u)
0 E
0
co
> (1)
Co
0
LLI -c
CL -c
0 co
C u) , , r-
rmCl
U)
LL
—
0 0
0
0
C)
E
a.
E
0
0 0
0 co
(n M
12
W (D w
(D E
(D
D
fu
0-
-0 C
fA7
C a)
u) 0)
EL
m
0
CD I-
0
0 (D 0
k- 0 C, "
(D
—
WS (1) E
- co
:E
CL
E 20
0 o
0 N
D
'3
m
b E
,Ln
19 E
IL C,-L 0
E
— (n o
0
u) 0 E
Lz.
0
u
0
ct�iNa
gCxN to
c:
Q)
11
vi
W
&,
. 0 M
0 U rZ C)
40, 2
a)
-0
0 -3
-
CCJ
E
(n
co U)
CL
L ID
c) a)
C' a
rZ --
0) 0
0
0
c
0
- 0
QS
1=
CIO
.0
0
(13 o C)
0
(1) L:
>
CL u
as
p
cn (D
-0
U) CI) V)
-0 V) M
W
-tf
o (v C c
_0 0 0
"
(D
_0
-N
-
-0
(D
r
-
0
0
o
EL a
w
0
4T >,
>
0
E
0 a)
WE 0
'2
a)
(n mca
Co
E
a) > (1)
=
D b
E (1)
u) 0
E
Y
as
0
Ca w
cu iz OL
a
(15"
'-E
0) 0 ><
(1),
0
E Oa
0 E
0 Lj- 4-- .(n
w
U.
(1)
cr- — Cu M
0
(13 0 a)
LL c c cz
a)
0�
=— 1
0)
I-
-EZ >
Cu

iz
57,
LVJ
w
C
,ww
ww
�
CN„I
w�co
COED
i
"O
�w
.w.. . ......... _
� � w-�J
........._
__._
........
.....
.� �....
i
__.................._..
RmW.)QD
'bmnm
®y
LO
co
�'
�rwwwne
aD
ILLpsp �•�
LO
wII
6�Auwmei
COY)''
....�,....,'.I ,..
' ''
..«.....
i� .........
....
.....�.,..,,
�
...,.,..., „
.....,....
.,
.....
iiii
.:r.. nnn�i��
uw... ..
..,,rm......
..
..
.
OD
'WY)
on
00
Po6e
ru V
N
N
( V$111
a�q'
�i✓
Y(NJ
CNJ
CNN
Q
nz,
1--