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HomeMy WebLinkAboutNC0006033_Wasteload Allocation_19890605NPDES WASTE LOAD ALLOCATION PERMIT NO.: NCOO 0(,0033 FACILITY NAME: _jf5 r6 Facility Status: � EXISTM@) PROPOSED -- (circle one) Permit Status: ER 4141�ON UNPERN ED (circle one) MaJor wtnor Pipe No: 00/ Design Capacity (MGD): D +► Mod!.JZ Date Rec. s i J Drainage Area (mid) (/.3`5- Avg. Streamflow (cfs): m 7Q10 (cfs) Winter 7Q10 (cfs) 'aL 30Q2 (cfs) raw Toxicity Limits: IWC X (circle ono) Acute /Chronic Instream Monitoring: Domestic (X of Flow): Industrial (X of Flow): C/�,W oe Comments: Laments: s- Jh LIS�y/i. o iMA.e w owAdaf22w Le�Ir, RECEIVING STREAM: /[ni �4. &It6 Class: W 5 — 777 Sub -Basin: 03 040-34 Referents U /SGS Quad: G /4 (please attach) County: Regional Office: As Fa �9 Ra Wa Wf WS (circle one) . Requested By: Date: Prepared R- Date: Reviewed By: �&60 JIZRL'l Date: Parameters L042 lure PCOI !1>llrurm 70 erxviu li Upstream Location Shr m orou &// Downstream Location f}rmcS}YGnG �/1GiC� Effluent Characteristics zJbLji it lay SODS Ubb 6-62, IL 6P7A- CC!)Obld 347� -/399 (a, aPT TSS Obld) Zq All? r,ek r F. Col. (/100ml) /goo pH (SU) 0-g B%-)I ) ;o{rAl db U,5 8,9 a lPhenol5 f lbl d o,7 = Zl u .P l FOR APPROPRIATE DISCHARGERS. LIST COMPLETE GUIDELINE LIMITATIONS BELOW ///a/,,� 64IJ/66-0 Effluent Characteristics Monthly DailyAverage Maximum Comments D5 oS.12.6 11 39 5 U. T33 8. 9/ j Type of Product Produced Lbs/Day Produced gbCce Effluent Guideline Reference 4�� 4/D 417")- 3% 501) 43 6 40 - 4 10. `l0cr �SP7-) (aPT� (BPS Request Ho^: 5150 —... .... .... ------- WASTELOAD ALLOCATION FORM -~--------------- »�C. FaciIiiy Name: JPS �utomotive Products Cnr�UN ^�n� NPDES No,: NC0006033 -,�^��xvv-^w^N� -° ox, Type c.�f Waste: 79% Industrial (Textile} �zwpUxmr Status: Existing1,,dificatic'n "'AA ^ � H �nn Receiving Stream: S.F. Catawba River , '"v� Classificatior: WIII OF Subbasin: 030836 �ranage i County: Gason Summer 7Q I0��� Regiola Office: 1, 1RUl Win+efr 7O!0: ��0 Reques'ur: Lula Uarris A;erage flow: 81O cfs Date of Request: 2/2Ic 3/2 cfs Quad: G14NE ---~---------------- RECOMMENDED EF FiUENT LI mIT� -----------'---`--------- R�comsend Recommend Mu.Avg. Dly Max Wasteat low (mgU4.0 BOD5 <lb/d>: 304 53� EL,8PT 249 COD lb/d): 3747 7399 EL,BPT WWI Sul1�ide (lb/d): G.7 17.R EL. OPT �7 EL,JFT 77o Total Chromum (lb/l}: 4.5 8.9 EL'GPT Phenols (lb/d ug/l 0.7 21 ug/l WQ pH Fecal Colifsrm (#/100 ml>: 10Sr.) WO mpn Toxicity Testing See Attarhed --------------------------- MOM1TORI1N',G Upstream Y (y/N): Y Loc�tion: Dridlge just opstream of outfall Downstream (Y/N): '( Location: Upper Armstrong Bridge -------------~~-------------- COMMENTS 171F E instream monitoring 1,or temperature, fecal c&liform, DO� [�ODD � and conductivity � ^ ����U���) MAR 21 198 ---- _-------- -. Recommended by: _.... ..... .... __�____� Reviewed by Tech Support Supervisor: _ _ _____ Date: _31 cl� Regional Supervisor: _ Date: Permits & Engineering: ____ Date: RETUR� TO TECHNICAL SER;ICES BY: Facility Name - )9,5 Aufhaxshye- Qndurt% r ro_ Permit # &Qb0i foa3 CHRONIC TOXICITY TESTING REQUIREMENT (QRTRLY) The effluent discharge shall at no time exhibit chronic toxicity in any two consecutive toxicity tests, using test procedures outlined in: 1.) The North Carolina Ceriodaphnia chronic effluent bioassay procedure (North Carolina Chronic Bioassay Procedure - Revised *February 1987) or subsequent versions. The effluent concentration at which there may be no observable inhibition of reproduction or significant mortality is % (defined as treatment two in the North Carolina procedure document). The permit holder shall perform quarterly monitoring using this procedure to establish compliance with the permit condition. The first test will be performed after thirty days from issuance of this permit during the months of MaC S . Effluent sampling for this testing shall be performed at the RPDES permitted final effluent discharge below all treatment processes. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR-1) for the month in which it was performed, using the parameter code TGP3B. Additionally, DEM Form AT-1 (original) is to be sent to the following address: Attention: Technical Services Branch North Carolina Division of Environmental Management P.O. Box 27687 Raleigh, N.C. 27611 Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should any sin ale quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will revert to quarterly in the months specified above. Should any test data from this monitoring requirement or tests performed by the North Carolina Division of Environmental Management indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test and will require immediate retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute noncompliance with monitoring requirements. 7Q10 125 cfs Permited Flow 14.0 MGD IWC% 4.? Basin & Sub -basin 5IA31. Receiving Stream -5.r. l River County &*A Recommended by: �?ulk C - Oad- Date ? **Chronic Toxicity (Ceriodaphnia) P/F at kJ,? %„ nta(3un ozo DeL, See Part 3_, Condition iS . �' P5 A A-fomo h vc- �J�b Copp � C t'o(k Ca4c 'River 11gq `i; U3�31.e cam_ bC'`Ck - c-- _ �rrm- . --�_ _��I�h�h ohiCh -. chi - - _ -� �c,�11.__S?"eCa m -�C h�i?' L _ ✓1� f tC�CC�..�Y�_ - !�� - if . r�_- - U mar D i - { - �o. k: :� - ArMo rnx Ll ter q, I0 3ZO ,_1,3 - - 1i� . IR r �" _Gr�(1►J �, o Aj 12-5 0% i h L" Cd - L4cwdaLty (Drn C-trrb 4 0 zj - 2- c6 Y;5b %t7 bw� 1 JCb /�uFomohv� Rt)d(-Lr-b Corp, 5, cork C 4C i i R'Ver- 03083Ca �r tome, u(. kecwa cuy c 0 (%3l.z c(�')1:_WJ P) CA)21. z _ a uJcl2 &OD- �7 Irlct �O*c 31alsq Ur (_ �hu fir,/) CfiOMjLtM f--&me - L*9ream cOnC 621 A j i e (f25c(sX-32.1 -uclk) = lt.z c�SXC,��= �r3r.zc�3)_(�0��1�� CIO _ When. keud a rrz ctct run Tay 1col a6to earn (_-�fecyldcr<y _i m, _ feefecl �Iru onl jrr„ on b _ lick y- _ CcX1� Form d1frt .erf _.SFco�cuc_ c_Zid_ob11- Opcfecf_- -_OIL 4w.(t c, 5luc Irmd_oh ' _%Ct % " (vrrn) -- Fr lrn<fd ) C42 /NJ C'nr�.enud _d�sJ�r'i Glow �l = � hml6_ L_Jb1d -- - - - ChrL6 will J be J,,-. `� Cd 14L - corr. _ Unit)-f(o-L5,ock_ _-o_L a)o o j ©i'.i3�e -- - , I iv Sf f =ram 1 P Poo) - ---- 1 Vof le, uO- - - - -- - -- --- — ---_ 1., Mup� - - - - - - - - - - ----}--e--�-«- -- - ----- -- -- t �y /O)hu - - ---1 /IaNg --- - !� _ - - - - -- - --- -- - - --- - z— -- - -- -- -- I� - t >nc 3l-7189 l b, S�al� oa w5nz Lti I3/a m; up.�tclA, South Fork Catawba River at McAdenville of dixho y- ) The South Fork of the Catawba River flows into Lake Wylie near Belmont, in Gaston County. The river at the McAdenville site (upstream of the lake) is a wide (40 meters) and fairly deep (maximum depth of 1.5 meters) piedmont river with a substrate composed mostly of sand and grave;. The river at this point receives effluent from several textile plants and WWTP's. Average conductivities for 1985 were much higher at this location (143 umhos/cm) than they were at an upstream BMAN site at Startown (72 umhos/cm) for the same time period. Taxe richness of benthic macroinvertebrates were very low (55/16), suggest- ing a Fair bioclassification using criteria for piedmont rivers. Very few taxa (3) were abundant: a tolerant mayfly (Tricorvthodes) and two very tolerant chironomids (Cricotoous bicinctus and Polvoedilum illinoense). This community indicates some instream toxicity. �m iG 3rrl�nl Daa AeweAJ Aq-eO(renf rCwrel?r 5-ve L)Orearn 1ahyoical khan vah.16 o` exce/�enf d rz� ca�c 13,95'(O i iahl) uv�'eczm 13 lsfe�[ Co parr -31- %%,091 Y.11:a Mop Station No. Mo. Station Location Table A-3 Cheadcal Biological Strestn Rating Classification Classification Miles 1986 87 1986 1987 C-1 Catawba River at SR-1273, McDowell Co. C 7.5 - Cond Cr2 02137513 Catawba River near Old Fort, I 40 C 0.1 NS Cood{air CC3 Catawba River at 9t-1234. McDowell Co. C 2.6 - Cord -Fair C-4 02137727 Catawbe River near Pleasant (hrders, SR-1221 C 7.3 hS Gmd-Fair C-5 Claris Creek at M-1227. MDwe11 Co. %-III Tr 1.7 - Coos C-6 oati Creek below Old Fort WWT kS-III N 3.2 - Poor C-7 Mackey Credo froi source to Catawba River C 1.5 - - C-8 0213M Linville River near Nebo. NC Hwy 126 B 6.9 PS - C-9 02139036 Catawba River near Glen Alpine, SR-1147 VS-111 17.7 PS - 0-10 North Mddy Creek at SR-1750, MLbwell Co. C 16.9 - Grad -Fair C-11 Ccpemitg Creek at SR-1819, WDcwell Co. C 4.7 - Fair C112. Copemvg Credo at SR-1794, MDowell Co. C 1.0 - Fair C-13 0213975ESO High Shmols Credo at Dysartsville C 2.6 PS - 0-14 Little Fork near W Ray 181. Burke Co. C Tr 3.1 - Fsellmt C-15 Beck Greek, from aamce to Irish Creek IS-111 2.9 _ _ 0-16 Lick Branch from aerate to Johns River B 0.6 - - C-17 02140304 Wilson Creek near Gregg. lS Hwy 221 B Tr 14.3 S Coal C-18 Wilson Creek near B%mmt, SR-1358 B Tr 8.8 - 15kcellent G19 Harper Creek, from source to Wilson Credo C Tr 9.0 - - 0-20 021ZC4272D Math Harper Creek near Kawera. USFS 058 C Tr 6.1 S Rkcellent G-21 02141245 Lair Creek near Morplmton. SR-1501 C 21.9 S - F-' C-22 Hoyle Creek from sauce to Catawba River C 3.3 - - wC-23 Ur Catawba River from sauce to Cstambe River C 2.0 - - C-24 02142938 Catawba F-ver near Scoth Belmont 6S-111 3.8 S - C-25 02142000 Lower little R. or All Healing Springs, SR-1313 C 24.0 PS - C-26 02.14253830 Norwood Creek near Peet limbo, SR-1328 C 5.4 S - C-27 Big Branch from satiate to Hicks Creek C 2.5 - - ' C-28 02142648 Catawba River near Ricks Crossroad, W Hy 73 WS-17TT. 6.5 S - C-29 MDag11 Creek, sauce to Mountain Island Lake C 6.3 - - C-30 Car Creek, from sauce to Mountain Islad lake WS-111 4,1 - - C-31 02142808 Catawba River near Thrift, NC Pray 27 WS-m 5.9 S - C-32 02142722D4 Dutclmens Creek at Mammin Island, SR-1918 C 8.4 PS - C-33 02142900 lag Creek near Paw Creek. SR-2342 C 15.3 PS Cood-Fair C-34 Uf Fites Creek, 4 ate abaue/blw Jedco4kghes C 0.4 - Poor C-35 S Fork Catawba River near Staxtown. IC Ray 30 VS-72I 0.3 PS Fair 1 �;:ni JP•jt 0-36 02145112 S Fork Catawba River at MAdenville. SR-20D3 NS-III 17.8 S - allym; .W C'37 02145442 S Fork Catawba River nr South Belaont, SR-2524 Wi-1.11 4.1 S - C-38 02143000 Harry Fork near Henry River, SR-1124 C 45.6 PS Cocd-Fair C-39 02143040 Jaccb Fork at Ptameey, SR-1904 WS-112 Tr 7.8 PS - 040 Uf Wdte Oak Creek from sauce to U.O k Creek WS3II Tr 1.5 - - C-4l 02143250 Clark Creek at Lincolntor. SR-1008 C 5.1 PS - C-42 02143500 Indian Creek near laboratory, SR-1252 C 7.2. PS Cad-Fnir C-43 Ur Mnney Creek from sauce to K�smey Creek C 0.8 - - C A 0211ADW lmg Greek near Bessemer City, SR-1456 WS-ITI 13.3 NS - C,+d lag Creek at Castaris C 5.9 - - Cr46 02145524 Catawba Creek at W,-SC State Line.SR-2302 C 1.8 S - 0-47 02145640 Ctewders Creek near Bawling Ckeen, SC C 16.5 NS - C-48 Ur Ctcwd-m Creek from sauce to CroWers Ck. C 1.5 - - G-49 AbemetFy .reek, above Lithimm Corp discharge C 2.2 - - Fbm jq%-i98-? k3Q56 FIeprE Cood-Fair Other Date Rating basis Reference - PS _ PS Pscellent Sr _ PS Ceo1 - _ PS - PS _ PS Coed -Fair - _ PS _ PS _ IS - S - S - S _ PS Cad -Fair PS Coed -Fair - C"Od rml-Fair - _ PS Cmd-Fair - - PS _ pg - PS Fair - t15,j)0.btl0y sup7am 0 n 5 E AJO WCS.88 M Aq Tm, 87 E ARC) WCS, 88 P. FIiT WGS.88 M Mack Ch.88 M Aq Tom, 87 M VRC.88 M TEM Comp. M Aq Tm. 87 M Aq Too, 87 M Mae Ca.88 M Mek Ch,88 H USCS.88 M WW'88 M KU Aq Tmk, 97 M Aq Tmk, 87 M Aq Tok, 87 M rm, F6-87 M Aq Tax, 97 E ARD WCS, BB M Aq Tuc. 87 Overall Assessae:t Cayes Seerees Dating Feral, Ip Fecal TSS, Fecal W. 75n. Tak. Ni Std, Ni Ni Sad As Sad, Fecal Tm Sad, Pesticides Seri Feral. BT, Sad Too. N, 7n Fecal Tm As Feral, T1ab F9 7lub M.b T1nrb, P, Tm Taub, P Ch Zn. Ph. Tap. T b Tart a Tarb, P Tak Feral, Thrh Or. Ni P. Tm Fecal, DO, MO Tau P I P Pjp P F P P N? p Pe,nl Wyiar`t 38 _ 344 26 27 If 1 t It 1 ' t1111iJIN 11 f • � I/I11N 11 It f tl { �. I f t t 11 It i11 f{r e r M It ! i11 tf of to LA PNMI i111 r f u Is Maw- _29 j rpr-7rj� k 62 AOL- too WIVE ��!` ter ��,► 69 52 • i •• • Figure 1 b. River Basin. (Lower Catawba Drainage . t PlICif:I�� DATA: 89041495-+ #1 SCAFIS 00 TO 650 V 5,"C, 7 J9 16 : 41 : 01,) C AL I : l'0041499 #? SAMPLE: '.• :1 ABN l'9041499 C iNDS-i.: 1 ! 1L. i i,*1 DB RANGE: G 1 ! 2' 00 LNE.EL: 14 C1, 4.0 QUA! H 01. F J ►D BASE: U '20 L, 3 4:? 6150 tit :: `:•_t_; 5s41 Ss.:.' 1 A 7 100 t'i I OR I C' DATA 04' 1499 41 SANS 650 TO 1000 05 ,' i r / 89 1 F : 4 7 : 00 CAL I : 89041499 #+ SAMPLE: 1:1 AERN 89041499 RANGE: G 1, 27 00 Lr��E.E:L: 14 �:� : 4. f=i C,!' I�;t : A Q.-1. �i LI 0 BASE:LI '��, I�i 414f i1 -i 14 - 1'�:04 1 4 , 1•;: 14:12 TIC 1.11 OR I DATA: 89041499 # 1 S:)CA 1S 1000 TO 1400- rr5/07/29 16: 4 : 00 CALI : Er 041439 #i �. -.AMPLE: 1:1 ABN 8904149q CONDS.: 1! 1L 01-1 DB-5 WA E: G 1: 7100 LHEEL: 14 0 : 4. 0 QUAN: A Ei : 1. 0 J 0 E.HaE: U 2'0 100.0�/ / 4183 • 1 E� 1� � 14 I 1 �t ! 11 s C .i i I-1 •� 1 •'1 r • 1 i. �' ! L i.1 � � . � T,� i 1 . �' 1- 1 'r r. � i `.r ti•_ ' �w�r.�w�, .� 1 _ . ... . 70.`1�2i Af 24 11 :ly; 1 : . l'�= 1Lr• a..= ., •� M I GP I C CGHTH : 890 ;1 �'1 # 1 SCANS 1350 T1 i 1'� �O r'F-i7, 8,y 16:64 C11_i 1'0LI• 8904142_2 9 ' SAMPLE: 1: i ABN RJ=_141499 i,;OHEI .: i UL 01.1 DW Rtijqr,E: i; . 14=-�1, 270C! LABEL: 14 0. 4.0 1=lk.jAN: A Cl, 1, 0 _I 0 BASE: U 20., ti C• V1 U/Isr I I. �- �; 1=:._ ' t J cL ram, ' : i � � 1 r'i� 'i i _� i -� � � .1 1 _._, r=i. i' _ �..::; 't .•. 11I DR I C DATA: 89;'-'414•r c-' # 1 SCARS 1900 TO SAMPLE: 1:1 Hc','l-I rl904142 t i IL i ii•1 IS-5 I . i I i F. . i i ' ''� '.. • � j _,,, i 1 � � «I.�� _ � i _ ' t' - 1� « rim... •;i 1~ � 1 . • � tel: --�: 1• ;. 1 S E4i 100. SAMPLE: 1:1 Hr,l•# ,:,_=04149' ,_ CII D'= .: 1 UL Cif•# DB--5 1 , F;NI IGE : G 1112700 Li '.;- L-L . 11 0., 4.0 Q AN : H 0.. 1.0 . i 0 BASE: I I 2-0j IJ f1 I 1 1 -Y 1 1 _ �I..i •� �.�'� �r r• �r �.r;� 1 r� �r I w.. { LI I / l i �: 1f -• 1 i tir �' j 1 i �I ai ly� �'I , -, E. 23 _i 1 ', :: i.L i L� ` ► l .i �,' 1 1� �,�,1 IL 1 / y i. ' t i 11. 1" r�� I1f I ` r l , _ 2 �; 'fir '111 1 � 1 ' I i �: jjJJ t �// 1i Ir•I •1 1 � r I 1 Y (' 1 �.� r•. 1 1 ' "-1... 1�� � t 1 ter, t, i�) ill 1 t � • � � t 1 `1 tl, .+ `.- i �� ti f t •.. t � ..r . r :1 �' ' I l �"• �Ir I 1 � 1' ti L'- -`t ..� �� 4• .:• '� � f : I r^ 1 �, rtil If l i l .1 i� � � ; J� ,r I 1 i � 1 1��1• t 1 � tl �I 1� � � � �JI, � ..� � 1 I / I I J 1 I 1 ( 108. i �•'� .L.L�:.' .f..+..��?'\w' IYi �.tt•�:�Li jy''j. I,rJ �,..\.ti: * ..tl •}� '1sr tC� 1 st :'� tt•' r� 4:rI'7 °ni:Ti 3�): �'Ii0 T�Ir ;L 1T S•tiI �... L loci. RIC M I DR I r DATA: 89041499 # 1 SCANS '2500 TO '2 7 00 ti 5. 0 7 %09 1 F : 47: 00 CAL I : 89041499 # SAMPLE: 1:1 ABN 904145+3 Cnf IL�' i l�L ��f.1 DF-5 RAFTGE : G 1, t r 00 LABEL: hl 0) 4.0 Q AH : H 0 ) 1.0 J 0 EH"E I I 0 3 5: 30 ^5r5'0 3 `' : 12 � Ia 013 3:.55 .c.'G)50 36 7 • 2'. �:EF 1 17 UU : 20 MID MASS SPECTRUM 05/07/89 1E:47:00 + 5:17 SAMPLE: 1:1 ABN 89041499 C0NDS.: 1 UL Gil DB-5 GC TEMP: EB DEG. C EHHHt•!CED : B 15B M OT 59 50.0 M/2 DATA: $9041499 # 3 7 2 BASE 1-1 ? : 53 CAL I : 89041499 #2 R I C : 76C'0. 319'. 100 SAMPLE E C I I. H20.02 1.1 WT B PK 101 RANK 1 FIT Cl-Cf. H40. 0'_' E: PK 1 Cl I k 0 35` FIT 74 H-iri. UL 1► �i�t►� 11 WIT =:I B PK 101' F'Ni•iK =� # ..3 FIT 7Gi I M MID LIBRARY SEARCH 05/07: 89 1 E: 47: B© + 5:17 'AMPLE: 1:1 ABN 89041499 i_ OND 1 UL ON GB-5 ENHANCED 156 214 OT> 1, CA—DfOj OLAN'E. 2—Ul L'LrHE<<,`;'L-4.5—GI1-1ETHYL.-- 1: —GIs i <'—PENTADEC r r � i:-i r r t r- � r�.ri r•r.� � 1 , ..i•-L1 I t►.�,i.n. titaE: 4: =u i i 1r.TH �'L— r Lr•aTHC�t 1- l L-- 1 CiCt 150 DATA: 69041455 # 372 CAL I : 89041499 # 2 n ?cl0 BASE ll, -: 59 RIC: 7 t.47. Lcz 00 100. D 50. 0 1-1; 2 MID MASS SPECTRUM 05i 07/89 16: 47: 00 + 10: 5 5 SAMPLE: 1:1 ABN 83041439 CONDS.: 1UL ON DF-5 GC TEh1P: 125 DEG. C E14HAI-ICED S 158 11•1 OT 73 L• DATA: 69041499 #7E9 CAL I : 89041499 # 2 BASE tel: �: 72 FIC: ?q64. E.E1 ►i 1► cl 1 =i 141� 1E��� 10.0 =�t� 112- 11 j-. MID LIBRARY SEARCH 05/07/89 16:47:00 + 10:55 SAMPLE: 1:1 AB14 89041499 :S.: 1 UL ON D6--5 COHD ENHANCED (S 158 2H OT 1000, SAMPLE C 10. H30. 05 . S 15 M WTI C PK 73 RANK 1 # 34650 r FIT 8?8 C23. H 17.03 JI M NT ;ass r PK 3`'C RANK y 3 '-?0 7 FIT 343 C21.H2:E.02.H.r-5.SI2 1 twirl 14 I -IT 47"s B PK 73 RANK -' 3 92$'37 r i T ?'-:S .4..,r..�._.�.- I DATA: 89041499 # 7E9 EASE 11 2: 73- 1 CALI: 89041499 # 2 RIC: 2963. CYCLOPEHTA'SILOXANE, DECAMETHYL- 2, 41H::'H`t—Q SINOLIh1EDIshii.: 3—E'Ehi?%.t`L— :PHEt�;'LrIETH'�`L�— • -' '- �-i-�-r-�T�--T-i--f-�-T•--r-•-T'-T-y-^l-•-T•-T-�-�".--Z-.--T-� i-•T-•�--�-.-•f-r-�-•-r �. �..�.— . r . . .. �. . ter. ram. r . � ♦ t . � r s ♦ • L t.T�il rEH-ltf�IEtTHAN1411NIE, N-L(PEHTti"FLUi�-'-O HEN►L%01MEtH11214tI BETA.:4-Gil'_. ! — 100 150 LsiO 2`Sk3 3 00 ^5 ',� ., 0 40 � 450 i MID MA $B -SHURL 1f1 06f07/89 16:47:00 + 15:07 SAMPLE: 1:1 i iBN 89041499 COND9.: i UL ON DB—S GC TEMP: 167 DEGO C ENHANCED (S 1 %cjE, eta 0T ) 100.0 50.0 M/ 2 i rio DATA: 89041499 # 106D BAI;E M/Z: 103 CALI: 89041499 #L RIC: 11376. �0 1-1 I D LIBRARY SEARCH 05/07i35 16:47:00 + 15:07 SAMPLE: 1:1 AN 89041499 Cf_NDS.: I UL ON DF-5 ENHANCED ('S 158 2N OT) 1083 SA14PLE Cam.. H12. 0.142 1 �. �1 11 WT r* I E, P1�; 57 ' F'A1Ik; I -- FIT 9)0 ,I C: i Ci. H 1 G. F.J �1 •'1 ell M WT L' F F'1, 1►�'� ��H1•i�'� :: r =� FIT c, 6 C10. H16. 04. S, ' 11b;Tf 6 F'K 1 C S; R.CiNK rIT L.:i L M Z 4,0 1 1H—MIDAKLE. 1-0—i�iXOPENTYL?— DATA: 89041499 CAL I : 89041453 # 2 !- T I t 1' i j r _ t A �D T t 1 • �' J '� •�r' 1 J {-i •>' J -• j Y! )- 1' l r.'!: i�_�i S. ! _.'. ! `i-CJ �.1 i- 1 H ! -1 CL �I� - -Z 1 1 - r I BASE 11/Z : 109 RIC: 10975. h0 E10 1 12>:1 1. 0 160 180 200 100. 0 50.0 50.0 WE MID MASS SPECTRUM 65/07/65 16: 47: r 0 + 27: 27 SAMPLE: 1:1 ABN 89041499 COND6.: 1 UL GH DD-5 GC T81-IP: 3y1 DEG. C ENHANCED : S 158 211 OT a 31 c.ri DATA: 89041499 #19:33 BASE K.,?: '300 CAL I : 89041455 #2 R I C : 11 U24. , 1 m20 i ��:� i Fri 11- o ►�.�_, l t i LLLl t( firr• 3 - .-- 13. 13 i is 1000 SAMPLE C12. H15 1 hill M WT 1E5 E PK 119 -- FIT 859 C 1 %5s. H2-3. ►_ 1 M !JT�� B PK 119 RANK # FIT 4 C11. 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