HomeMy WebLinkAboutWQ0003034_Permit Application_19950803DIVISION OF ENVIRONMENTAL MANAGEMENT
GROUNDWATE.lR 'SECTION
3) 1 q96
MEMORANDUM TO: J i l A lez
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7 n�e cw{le Regional Office AW 7 1995
FROM: c' e� o f f3-/eS C'V' MANAGEMENT �
PAVE '
SUBJECT: Application for Permit Renewal V RED. CFFICE, N
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(� �P�%in�t-�Amen.m"enter
y- New Permit
Facility Name: )occa.-/eVS
County: i�c•SeSc v
Type of Project: 14
APPLICABLE PERMIT NO.s:
UIC
W0- 000 303 4
DEH
EPA
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The Groundwater Section has received a copy of the referenced permit
application, a copy of which should have been sent to your Regional
Water Quality Supervisor - IF A COPY HAS NOT BEEN RECEIVED IN THE
REGIONAL OFFICE, PLEASE LET ME KNOW.
_Z__�The Groundwater Section has received copy the referenced permit
application. A'*co . A of�the p� plSeat'-�on'-d"ocumen�8�we receive3--is
�tta�ed.
The Groundwater Section has received a subsurface disposal project
from the Div. Env. Health's On -Site Wastewater Section. A copy of
the application has been forwarded to DEH's Regional Soil
Specialist, Please coordinate your review with
that Soil Specialist.
�PZea _e�view the application materials for completeness. If you feel
additional information is necessary, please let me know no later than
41 5yst i s� A755 �}' A copy of any formal request for additional information
*aid;--e_.forwardedjto, you.
If you do not need any addition -Info t on toacomplete your review,
please provide your final comments liy " u.sf Z'f /9f5 . If) }you request and/or
receive additional information, your^ -fins comment`akd due no later than
14 days after you receive the additional information.
\TRANS.SHL
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Division of Environmental Management
$ - 3-`15
Date
MEMORANDUM
To: Bob Cheek, Supervisor
Permits & Compliance Unit
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Groundwater Section
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From:
I�IIcNAEI ALLEry Project Engineer
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Permits & Engineering Unit
Water Quality Section
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Subject: Groundwater Review
Non -Discharge Application No.
Facility Name: Rc,ccc ru�_icE�rs ,qwe iow.
County: 'r_ 'n 'SON '
(GW # 95I75 )
Attached you will find plans, specifications, and supporting information
for the above project
Please let me know whether you will or will not be conducting an
extensive review of the subject project by
If I can provide additional information, please contact me at ext S 4
y n :will
(: -0 The Groundwater Section E]will not* conduct an extensive
`� ✓ _ review of the subject.
Groundwater Section will not review application for the reason
listed below:
e�
(2) A request for additional information will be forwarded to you by the
IV -
reviewer listed below.
GW Reviewer: C, O)/ V/1 s Date: 14L-51& s � '?/ /s I
9/6/90
APPLICATION FOR PERMIT AMENDMENT
LAND APPLICATION OF RESIDUAL SOLIDS
ROCCO TURKEYS, INC.
ST. PAULS, NORTH CAROLINA
Prepared for:
Rocco Turkeys, Inc.
Post Office Box 9
Highway 20 East
St. Pauls, North Carolina 28384
Prepared By:
SWE, Inc.
3718 Old Battleground Road
Greensboro, North Carolina 27410
July 1995
July 30, 1995
N.C. Division of Environmental Management
Water Quality Section
Permits and Engineering Unit
Post Office Box 29535
512 North Salisbury Street
Raleigh, North Carolina 27626-0535
ATTENTION: Mr. Michael Allen
REFERENCE: MODIFICATION OF PERMIT NO. W00003034
Rocco Turkeys, Inc.
S&ME Project No. 1588-95-041
Dear Mr. Allen:
S&ME, Inc. is under contract with Rocco Turkeys, Inc. (Rocco) for the management of
their land application of residual solids program. S&ME wishes to modify the current
Rocco Non -Discharge Permit No. WQ0003034 by adding an additional source, the effluent
lagoon residual solids.
Operating procedures will involve the land application of the effluent lagoon residual solids
onto the currently permitted acreage in Permit No. WQ0003034 (1,944.0 acres). An
estimated volume of 1,500,000 gallons is being requested for addition to the permit at this
time. Land application activities will be done within agronomic rates in accordance with
Permit No. WQ0003034 and monitored closely by Rocco and S&ME. Operations will
continue to involve application of currently permitted wastewater residuals to the permitted
sites. All applications of the effluent lagoon residual solids will be subsurface injected.
No direct contribution of domestic waste is associated with these residual solids.
SWE, Inc. 3718 Old Battleground Road, Greensboro, North Carolina 27410, (910) 288-7180, Fax (910) 288-8980
�m a.
North Carolina Division of Environmental Management
July 30, 1995
Page 2
Your prompt attention in the review of this modification would be greatly appreciated.
Please contact us immediately if you require additional information or have questions in
the review of the permit modification application.
Sincerely,
S&ME, Inc.
ZJA't T. W g-c�,
Robert P. Willcox, Jr., C.P.S.Sc.
Soil Scientist
N.C. Land Application/Residuals Operator #13285
G.F. Rick Baker, P.G.
Branch Manager
N.C. Land Application/Residuals Operator #13169
Enclosure: Permit Package, $400.00 submittal fee
cc: Barry Tyner, Rocco
Billy Daniels, Rocco
TABLE OF CONTENTS
Section No. Title Page No.
MANAGEMENT PLAN
SPILL CONTROL PLAN
APPLICATION RATES
MONITORING
RECORDS
II LAND APPLICATION OF RESIDUAL SOLIDS
APPLICATION FORM
APPENDICES
APPENDIX I: RESIDUAL SOLIDS ANALYSIS REPORTS
Rocco Effluent Lagoon Residual Solids
Nutrient and Metal Analysis
TCLP Analysis
1
4
5
7
8
SECTION I
MANAGEMENT PLAN
SPILL CONTROL PLAN
APPLICATION RATES
MONITORING
RECORDS
MANAGEMENT PLAN
The residual solids management plan describes the process by which the residual solids
from the Rocco Turkeys, Inc. (Rocco) Poultry Processing Facility's Wastewater Treatment
Plant (WWTP) will be land applied to the currently permitted fields as an agricultural
resource at agronomic rates. The residual solids will be applied to row crops and hay or
pasture land at agronomic rates for total or partial replacement of conventional nitrogen
(N) and phosphorus (P) fertilizers. The actual amount of residual solids applied will be
dependent upon the nutrient requirement of the specific crop and the nutrient content of
the residual solids.
Residual solids application scheduling will be dependent upon residual solids production,
storage at the respective treatment plant, and the crop management program. On farms
utilized for hay and pasture production, residual solids will be applied in split applications
as is normally done when conventional fertilizers are applied to hay and pasture land.
These applications will correspond prior to grass growth in the spring, after each cutting
in the growing season, or whenever most appropriate. On farms utilized for row crops,
residual solids will be land applied between crop rotations.
The fields will receive residual solids in an agronomic manner based on requirements
listed in Permit Number WO0003034. Residual solids will be applied at agronomic rates
which are limited by nitrogen loading rates. An acceptable pH will be maintained in the
soil, residual and lime mixture greater than 6.0 on all land application sites to insure
optimum yield for the crop being grown.
Prior to an application event, an application rate will be determined based on a current
residual solids nutrient analysis. Representative residual solids samples will be collected
prior to the haul period and composited for analysis. This composite sample will then be
delivered to a qualified laboratory familiar with residual solids analysis and analyzed for
1
ammonia nitrogen, nitrate/nitrite nitrogen, percent total solids, total Kjeldahl nitrogen,
phosphorus, potassium, calcium, magnesium, sodium, copper, zinc, cadmium, chromium,
nickel, lead, aluminum, chlorides, sulfate, mercury, arsenic, selenium, molybdenum and
pH. Plant available nitrogen (PAN) will then be calculated from this residual solids
analysis. This information will be used to calculate the loading rate for the field and crop.
Once the appropriate application rate has been calculated, the residual solids will be
removed from the respective treatment plant and transported to the site in tankers
adapted for liquid residual solids. Liquid residual solids will be loaded into tankers which
will then travel major traffic routes to the fields whenever possible. Once at the field, the
tanker will proceed to a designated staging area. The liquid residual solids will then be
transferred to a residual solids applicator designed and operated to obtain an even
application consistent with agricultural requirements. An AG Chem Terragator 2505 or
equivalent will be utilized to land apply the liquid residual solids.
All residual solids will be removed from the staging area by the end of the working day,
unless equipment breakdown or weather prohibits the residual solids application. At the
start of each day, all fields will be inspected by the field superintendent. Equipment will
only enter a field when conditions are appropriate for the application. Residual solids will
only be applied when the field is capable of supporting equipment. When field conditions
are not appropriate for an application, such as during wet periods, the residual solids will
remain at the WWTP until field conditions are suitable for land application. Prior to the
residual solids operations, the field superintendent and appropriate Rocco personnel will
inspect the site. During the field inspection, the field superintendent will note the standard
North Carolina Division of Environmental Management (DEM) buffer zones, including:
homes, drainage ditches, roads, wells, surface water, and property boundaries (listed in
Table 1 below). On the basis of these standard DEM buffers for land application
programs, buffers will be established in the field. These buffers will be identified in the
field by the placement of pin flags.
2
TABLE 1
DEM Buffers for Current Permit WO0003034
Application Method
Subsurface
Surface
Area Description
Injection
Spreading
------------------------
feet ----------------------------------
Property boundary
100
100
Public right of ways
50
50
Residences
200
400
Places of public assembly
200
400
Water supply sources
private
100
100
public
100
100
Stream, lake or impoundment
50
100
Upslope drains or
water diversions
10
10
Downslope drains or
water diversions
25
25
Groundwater drainage systems
and surface drainage ditches 25 25
9
SPILL CONTROL PLAN
ROCCO TURKEYS, INC.
ST. PAULS, NORTH CAROLINA
In the case of a spill, the following action shall be taken immediately:
1. Halt the source of the spill: Ruptured line or valve, or damaged tank unit.
2. Contain spill: Use straw bales to form a barrier. Straw or hay bales can be
obtained from several sources for this purpose. Soil near the site can also be
used to form a barrier for containment.
3. Clean up: Use residual solids application equipment to recover as much of the
material as possible. After the application equipment has recovered as much
material as possible, it will be land applied as per the management plan. A
temporary sump pit may be dug in the containment area and spilled material
washed into it to enhance recovery.
4. Final Clean up: Any unrecoverable material will be washed from the road
surface and incorporated into an adjacent tillable area.
5. Notification: As soon as possible after a spill occurs notify:
A. Rocco Turkeys, Inc. (910) 865-3800
B. Department of Environment, Health and Natural Resources
Division of Environmental Management
Fayetteville Regional Office (910) 486-1541
C. Robeson County Sherrif's Department (910) 671-3100
D. Fire Department if assistance is required for washdown
E. S&ME, Inc. Greensboro Branch (910) 288-7180
6. Management of clean up efforts: The field superintendent shall take
immediate charge of the clean up activities. Additional labor will be requested
from the treatment plant and other departments as needed.
7. Reporting: Within 24 hours of a spill the field superintendent shall present a
written report detailing the cause of the spill and all action taken in response to
the spill.
APPLICATION RATES
The residual solids application rate will be based on the plant available nitrogen (PAN)
requirement for the crop and the PAN content in the residual solids. The PAN requirement
for the specific crop will be derived from limits in current Permit No. WQ0003034 (Table 2).
Crops typically grown in the area counties are coastal bermuda, small grains, soybeans,
corn, cotton and fescue.
TABLE 2
Plant Available Nitrogen (PAN) Limits for Crops
based on Permit No. WO0003034
Crop Pan Recommendations
pounds/acre/year
Alfalfa
200
Bermuda Grass (Hay, Pasture)
220
Bermuda Grass (Coastal)
350
Blue Grass
120
Corn (Grain)
160
Corn (Silage)
200
Cotton
70
Fescue
250
Forest (Hardwood & Softwood)
75
Milo
100
Small Grain (wheat, barley, oats)
100
Sorghum, Sudex (Pasture)
180
Sorghum, Sudex (Silage)
220
Soybeans
200
Timothy, Orchard & Rye Grass
200
The PAN content of the residual solids will be based on total Kjeldahl nitrogen (fKN),
ammonium -nitrogen (NH; N), nitrate -nitrogen (N0; N), nitrite nitrogen (NO2 N) content, and
the mineralization of organic N into inorganic N. Most of the nitrogen in the residual solids
is in an organic form. As the residual solids are incorporated into the soil, the soil
microorganisms utilize the residual solids as an energy and njitrient source. In the
process, a portion of the organic N is mineralized or biologically converted into inorganic
N.
5
Various environmental factors such as temperature, moisture, and carbon to nitrogen ratio
will affect the mineralization rate. Mineralization rates can also be established in relation
to the treatment process which occurs at each plant. Typical mineralization factors range
from 0.20 to 0.40. A mineralization rate of 0.40 has been selected for the Rocco
dissolved air flotation (DAF) solids because of the treatment process. A mineralization
rate of 0.30 has been selected for the Rocco sequencing batch reactor (SBR) residual
solids because of the aerobic digestion process, and a mineralization rate of 0.30 has
been selected for the Rocco Effluent Lagoon residual solids due to open lagoon storage
and aeration of the solids. The PAN application rate will be calculated based on the
mineralization rate, ,TKN, NHa N, NO; N, NO2 N content, and method of application.
Residual solids which are injected into the soil typically retain a large portion of the NH3
gas which is found in the residual solids or is converted from the NHq N form. However,
when the residual solids are surface applied to hay or fallow row crop fields, a large
portion of the NH,-N is volatilized and lost as a nutrient for crop uptake. The actual plant
available nitrogen content for equal residual solids is less when the residual solids are
surface applied compared to when the residual solids are injected into the soil and the
NH; N gas is trapped by the soil. To reflect the lower PAN content for surface applied
residual solids due to the volatilization of NH,-N gas, the portion of NHa N in the residual
solids contributing to the PAN is reduced by 50 percent.
The PAN content of the residual solids is then calculated for injected and surface
applications as follows:
A. PAN injected = 0.30 (TKN - NH; N) + NH; N + N0; N + NO2 N
B. PAN surface applied = 0.30 (TKN - NH; N) + 0.5 (NH4 N) + NO; N +NOz N
WHERE:
0.30 =
mineralization factor (effluent lagoon residual solids)
TKN =
Total Kjeldahl Nitrogen
NHa N =
Ammonium nitrogen
NO; N =
Nitrate nitrogen
NO2 N =
Nitrite nitrogen
0.5 =
Volatilization factor
PAN Applied = (gal/ac)(8.34 Ib/gal)(% Solids)(% PAN) = Ibs PAN/ac
MONITORING
The residual solids and soil will be sampled at specific intervals to insure the beneficial
utilization for agricultural production. Residual solids samples are to be obtained annually
by permit. However, samples will be collected for each land application event. The
residual solids samples will be collected and delivered to a laboratory qualified to analyze
residual solids and is familiar with routine environmental sample preparation and
standards.
A residual solids analysis will be conducted for, but not limited to, the following
parameters: percent total solids, chlorides, phosphorus, lead, copper, cadmium, sodium,
total Kjeldahl nitrogen, nitrate nitrogen, nitrite nitrogen, magnesium, sulfate, potassium,
zinc, nickel, chromium, calcium, ammonia nitrogen, arsenic, mercury, selenium,
molybdenum and pH. Annual Toxicity Characteristics Leaching Procedure (fCLP)
analysis for regulatory compliance will also be conducted.
Once each year, the fields will be sampled for routine soil fertility and lime requirements.
Although the soil samples will likely be collected in the fall or winter seasons, they may
also be collected between croppings. Once the soil samples are collected, they will be
delivered to either the North Carolina Department of Agriculture -Agronomic Division or
A & L Eastern Agricultural Laboratories, Inc. for routine soil analysis.
7
RECORDS
Records pertinent to the successful management of the land application program will be
maintained for the benefit of DEM, Rocco, S&ME and the landowner. Each year an
annual summary of the activities of the program will be prepared and delivered to the
appropriate agencies and participants on or before the 1st of March. The annual
summary will include:
1. A) Source of residual solids
B) Date of residual solids application
C) Location of residual solids application (field number)
D) Method of application
E) Weather conditions
F) Soil conditions
G) Type of crop or crop to be grown on field
H) Volume of residual solids applied in gallons/acre and dry tons/acre
1) Annual and cumulative totals of dry tons/acre of residual solids, annual
and cumulative pounds/acre of each heavy metal (which shall include,
but not be limited to lead, nickel, cadmium, copper, zinc, arsenic,
chromium, mercury, selenium and molybdenum), annual pounds/acre
of plant available nitrogen (PAN), and annual pounds/acre of
phosphorus applied to each field
2. A representative annual soil analysis which will include the following
parameters: standard soil fertility test, percent base saturation, phosphorus,
potassium, lead', zinc, magnesium, pH, manganese, cation exchange
capacity, sodium, nickel', cadmium', copper, and calcium.
3. A minimum of quarterly residual solids analyses which will include the following
parameters: percent total solids, chlorides, phosphorus, lead, copper,
cadmium, sodium, total nitrogen, nitrate nitrogen, nitrite nitrogen, magnesium,
sulfate, potassium, zinc, nickel, chromium, calcium, ammonia nitrogen,
arsenic, mercury, selenium, molybdenum and pH.
4. An annual TCLP analysis of residual solids.
R
Soil Analysis for these parameters shall be conducted once prior to permit renewal on each site
which has recieved residual solids during the permit cycle.
SECTION If
LAND APPLICATION OF RESIDUAL SOLIDS
APPLICATION FORM
I.
II.
State of North Carolina L3
Department of Environment, Health and Natural Resources �0
Division of Environmental Management
Non -Discharge Permit Application Form
(THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
w E3 n
LAND APPLICATION OF OTHER RESIDUAL SOLIDS
This application is intended for facilities which are EXEMPT from 40 CFR Part 503 r,
N UJ
GENERAL INFORMATION: co
c:
1. Applicant's name (please specify the name of the municipality, corporation, individual, etc.):
Rocco Turkeys, Inc.
2. Print Owners or Signing Official's name and title (the person who is legally responsible for the facility and its compliance):
Nash Lindsey, General Manager
3. Mailing address: Post Office Bog 9
City: St. Pauls State; N. C. Zip: 28384
Telephone Number: ( 910 ) 865-3800
4. Application Date: July 30, 1995
5. Fee Submitted: S 400.00 17he permit processing fee should be as specified in 15A NCAC 2H .0205(c)(5).j
6. Specify whether these residuals will be land applied to: % agricultural lands, _ forest, _ public contact sites,
reclamation sites; (Please be advised, if these residuals will be distributed for lawn or home garden use, the
application for the "DISTRIBUTION OF RESIDUAL SOLIDS" should be completed rather than this application.)
7. If the alternative for residual disposal consists of "surface disposal" as defined under 40 CFR Part 503, please complete the
application titled "SURFACE DISPOSAL OF RESIDUAL SOLIDS. Please identify if there is any storage of residuals in
a surface impoundment or disposal thru landfilling. Explain:
N/A
8. Please specify the number of acres on which residual solids are to be land applied under the authority of this permit:
proposed in this application: N/A acres; total (current and proposed): 1,944.0 acres
9. County(ies) where residuals will be land applied: Robeson
PERMIT INFORMATION:
I. Application No. (will be completed by DEM):
2. Specify whether project is: _ new; _ renewal'; % modification
For renewals, complete all sections included in the application, in addition, please submit updated cumulative loadings
for the heavy metals and updated owner's agreement for O&h site.
3. If this application is being submitted as a result of a renewal or modification to an existing permit, list the existing permit
number WQ0003034 and its issue date January 31, 1995
FORM: LAORS 06/94 Page 1 of 18
* Rocco Turkeys Effluent Lagoon Residual Solids
III. FACILITY INFORMATION (attach additional pages for additional sources of residuals):
1. Name of facility where residuals are generated or prepared: Rocco Turkeys, Inc.
2. Facility permit number: W00001173 ; facility permit holder. Rocco Turkeys, Inc.
3. Specify whether facility in Section III.1 is owned by:_ federal; % private; _ state; _ local government.
4. Specify facility design flow:
Type of residual storage: _
mgd; facility average daily flow:
— * Not Used for Storage *
Volume of residual storage: Cleaning Accumulated Solids From Effluent Lagoon
mgd;
Length of residuals storage at facility: N/A days (the Division requires a minimum 30 days storage in units that
are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.);
Maximum storage time of residuals between application events: N/A days.
Estimated volume of residuals: 375 (dry tonslyr.);
5. Are there any other storage facilities, other than the above, currently on site: % Yes, No.
If Yes, please identify: 2 — Digesters
6. Facility contact (person familiar with residuals preparation): Barry Tyner, Billy Daniels
7. Facility contact's telephone number: ( 910 ) 865-3800
8. Location of treatment facility: North Carolina
9. Mailing address:
Post Office Box 9
State;
Robeson
St. Pauls, N. C. 28384
10. Latitude: 34' 48' 10" Longitude: 780 54' 55"
County
11. Specify the source of the residuals: _ treatment of water (alum sludges); _ treatment of industrial wastewater
(100% industrial residuals); _ treatment of industrial wastewater mixed with domestic wastewater (please specify
appropriate percentages of % industrial wastewater, % domestic wastewater);
% othar(explain): Treatment Of Process Waters Used In The Killing And Dressing out
Of Turkeys
Attach an explanation of either the treatment process, manufacturing process, or how the waste is generated. Provide full
and complete details of the entire process. * See Page Following 2 Of 18
12. Does the facility which generates the residuals have an approved pretreatment program? _ yes; % No. N/A
This includes facilities which are classified as a "Class I" facility (any publicly owned treatment works required, under 40
CFR 403.8, to have an approved pretreatment program or any facility treating domestic sewage that is classified as "Class
I" by the appropriate federal or State authority)
IV. RESIDUALS INFORMATION (attach additional pages for additional sources of residuals):
1. Information for Hazardous Waste (RCRA) Determination. The information requested on the limitations specified below
pertain only to those residuals that are generated from a municipal wastewater treatment facility with industrial contribution
or active pretreatment program and from any other treatment facility with wastewater sources that include industrial sources.
a. Are any of the residuals covered by this application listed in 40 CFR 261.31-261.33? _ Yes; % No. if Yes,
list the number(s):
FORM: LAORS 06/94 Page 2 of 18
MANUFACTURING PROCESS OF HOW WASTE IS GENERATED
The combined wastewater flow Is generated primarily from the process of waters used in the killing
and dressing out of turkeys; which Includes both process water and chiller water (0.652 mgd), plus a small'
contribution of san" waste (0.013 mgd), which Is discharged directly to the biological treatment system
The process water flows to two rotating drum screens, which separate feathers and meat and bone pieces
prior to the pretreatment system. The pretreatment system Is a physkal/chemical system with a dissolved
air flotation tank (DAF) which separates fats, oils, greases, suspended solids, and adjusts pH. The under
flow then goes to a biological treatment system (SBR) where the activated sludge generated during the
process cycles Is pumped to aerated digestors for stabilization.
b. Do the residuals exhibit any of the four characteristics defined by 40 CFR 261.21-261.24? _ Yes; % No.
Attach laboratory results for the Toxicity Characteristic Leaching Procedure Analyses, Reactivity, Ignitability, and
Corrosivity for each residual.
Note: If the following constituent levels (as determined by the Toxicity Characteristic Leaching Procedure Analyses) are
exceeded in the residuals or if the pH of the residual is not within the range listed below, the residual is by
definition a Hazardous waste. Chemical analyses must be made to Minimum Detection Levels.
Arsenic
Benzene
Carbon tetrachloride
Chlorobenzene
Chromium
m-Cresol
Cresol
1,4-Dichlorobenzene
1,1-Dichloroethylene
Endrin
Hexachlorobenzene
Hexachlorcethane
Lindane
Metboxychlor
Nitrobenzene
Pyridine
Silver
Toxaphene
2,4,5-Trichlorophenol
2,4,5-TP (Silvex)
pH (2:1 volJwt):
EEM
EEM
5.0
Barium
100.0
0.5
Cadmium
1.0
0.5
Chlordane
0.03
100.0
Chloroform
6.0
5.0
o-Cresol
200.0
200.0
p-Cresol
200.0
200.0
2,4-D
10.0
7.5
1,2-Dichloroethane
0.5
0.7
2,4-Dinitrotoluene
0.13
0.02
Heptachlor (and its hydroxide)
0.008
0.13
Hexacbloro-1,3-butadiene
0.5
3.0
Lead
5.0
0.4
Mercury
0.2
10.0
Methyl ethyl ketone
200.0
2.0
Pentachlorophenol
100.0
5.0
Selenium
1.0
5.0
Tetrachloroethylene
0.7
0.5
Trichlorcetbylene
0.5
400.0
2,4,6-Trichlorophenol
2.0
1.0
Vinyl chloride
0.2
>2.0 s.u. - <12.5 s.u.
NOTE: IF ANY OF THE RESIDUALS MEET THE DEFINITIONS OF A HAZARDOUS WASTE,
AS NOTED IN EITHER "A" OR "B" ABOVE, A PERMIT CANNOT BE ISSUED FOR
THAT RESIDUAL AND IT SHOULD NOT BE INCLUDED AS PART OF THIS
APPLICATION.
2. For each residual, please attach a complete chemical analysis of the material. This analysis must be comprehensive enough
to completely characterize the residual and must be based upon a review of the process that generates the material. If the
facility that will generate the residual is not yet in operation, the characterization must be based on simila existing
facilities and projection based on the type of facility. The analysis must include a minimum of the following parameters
and any other (mown and suspected contaminants that are tributary to the system.
Cadmium
Aluminum
pH
Copper
Ammonia -Nitrogen
Phosphorus
Lead
Calcium
Potassium
Nickel
Magnesium
Sodium
Zinc
Nitrate -Nitrite Nitrogen
TKN
% Total Solids
Pliant Available Nitrogen (by calculation)
3. Wastewater residuals shall not be applied to the land if the concentration of any pollutant in the residuals exceeds the ceiling
concentrations specified in the table below. Specify the pollutant concentration of these residuals (attach lab analysis):
Pollutant
Pollutant Ceiling Concentration (mg/kg)
Dry Weight Basis
Pollutant Concentration (mg/kg)
Dry Weight Basis
Cadmium
85
1.0
Copper
4300
595.0
Lead
840
22.0
Nickel
420
116.0
Zinc
7500
2,350.0
FORM: LAORS 06/94 Page 3 of 18
V . PATHOGEN REDUCTION ViFORMATION (attach add. pages for additional sources of residuals):
In accordance with 15A NCAC 2H .0200, pathogen reduction can be achieved using either 40 CFR Part 257 or 40 CFR Pan
503. Since the pathogen reduction requirements found in 40 CFR Pan 257 (note, "Processes to Significantly Reduce
Pathogens" or PSRP) are incorporated into 40 CFR Part 503, only Part 503 is listed below. Please check which of the
following applies to the subject residual:
100% Industrial Residuals with no domestic contribution (Skip this section, proceed to Section VI)
Residuals from the treatment of water (Alum Sludges) with no domestic contribution (Skip this section, proceed to Section
VI)
% Residuals from animal processing plants (if the residuals are being injected into the soil, please explain the process and the
equipment used, skip this section and proceed to Section VI
Industrial residuals with domestic contribution
1. In accordance with 40 CFR Part 503, a residual cannot be land applied if it does not meet one of the following alternatives
for Class B pathogen reduction.
Please specify a, bl, b2, b3, b4, b5 or c from below (submit all lab analysis, test results and calculations):
a. at least seven residuals samples should be collected at the time of use and analyzed for Fecal coliforms during each
monitoring period. The geometric mean of the densities of these samples will be calculated and should be less than
2,000,000 most probable number per gram of total dry solids, or less than 2,000,000 Colony Forming Units per gram
of total dry solids.
b. the residuals must be treated by one of the following "Process to Significantly Reduce Pathogens" (PSRP).
1. Aerobic Digestion - residuals are agitated with air or oxygen to maintain aerobic conditions for a mean cell
residence time and temperature between 40 days at 20o C and 60 days at 150 C.
2. Air l2tdn¢ - residuals are dried on sand beds or on paved or basins for a minimum of three months. During two of
the three months, the ambient average daily temperature is above Oo C.
3. Anaerobic Digestion - residuals are treated in the absence of air for a mean cell residence time and temperature
between 15 days at 350 C to 550 C and 60 days at 200 C.
4. Compgsting - using either the within -vessel, static aerated pile, or windrow composting methods, the temperance
of the residuals are raised to 400 C or higher for five days. For. four hours during the five days, the temperature in
the compost pile exceeds 550 C.
5. Lime Stabilization - sufficient lime is added to the residuals to raise the pH of the residuals to 12 after two hours
of contact
c. The residuals shall be treated by a process that is equivalent to a "Process to Significantly Reduce Pathogens" (PSRP),
as determined by the permitting authority, based on an evaluation of the recommendations provided by the Pathogen
Equivalency Committee.
VI. RESIDUALS TRANSPORT AND APPLICATION:
1. How will the residuals be delivered to the application sites (leak proof trucks, etc.)?
Reference Section I — "Management Plan"
2. What type of equipment will be utilized for land application?
Reference Section I — "Management Plan"
3. How will the application of the residual be controlled to ensure that there is proper distribution over the site?
Reference Section I — "Management Plan"
FORM: LAORS 06/94 Page 4 of 18
4. Will the land application operation utilize a contractor who specializes in Residuals Management or will the perminee
management the program? %Y Contractor; _ Permittee. If a contractor is utilized, provide the name of the fum, a
contact, address, and telephone number:
S&ME, Inc.
G. F. Rick Baker 3718 Old Battleground Road
(910) 288-7180 Greensboro, North Carolina 27410
VII. SITE EVALUATION AND RECOMMENDED LOADING RATES:
1. The following sites are to be used for land application under this permit application [please attach map(s),see La.]:
Application Area [acres] Maximum slope
Site No County Owner/Lessee (excluding buffers) (in percent)
* No New Sites Being Applied For *
Note: If more than ten (10) sites are to be covered by this application, please attach a form listing all of the sites along
with the information listed below:
a. A vicinity map must be attached. This map must show the location of each site in relation to at least two
geographical references and major intersection (numbered roads, named strearrshivers, etc.).
b. For all new or modified sites, a detailed site location map must be attached delineating both total and buffered acres.
This map must be drawn to scale with topographical contour intervals not exceeding ten feet or 25% of total site relief
(whichever is more descriptive) and showing the property limes; all existing wells, all surface waters and drainage ways
and all dwellings within 500 feet of the land application areas; and all buffers.
Note: The following buffers must be maintained. If residuals are sprayed on the sites, larger buffers may be required:
1. 400 feet from any habitable residence or place of public assembly under separate ownership or which is to be sold
for surface residual application,
200 feet from any habitable residence or place of public assembly under separate ownership or which is to be sold
for subsurface residual injection.
2. 100 feet between the disposal area and any public or private water supply source, all streams classified as WS or B,
waters classified as SA or SB and any Class I or Class II impounded reservoir used as a source of drinking water.t
3. 100 feet between any surface residual application area and any stream, lake, river, or natural drainage way,
50 feet between any subsurface residual injection area and any stream, lake, river, or natural drainage way.t
4. 50 feet between the residual application area and property lines for both surface and subsurface application (if the
original permit was issued with the buffer distance to property line as 100 feet, updated maps must be submitted
and new acreage delineated for the buffer to be reduced).
5. 10 feet between the disposal area and any interceptor drains or surface water diversions (upslope).
6. 25 feet between the disposal area and any interceptor drains or surface water diversions (downslope).
7. 25 feet between the disposal area and any groundwater lowering and surface drainage ditches.
t SPECIFY THE NAME OF AND CLASSIFICATION OF THE CLOSEST DOWNSLOPE SURFACE WATERS
(as established by the Environmental Management Commission) TO THE LAND APPLICATION SITE(S). USE
THE ATTACHED INFORMATION SHEET (PAGE 9 OF 18) TO OBTAIN THIS INFORMATION.
FORM: LAORS 06/94 Page 5 of 18
Note: The maximum slope for land application of residuals is 10% for surface application and 18% for subsurface
application.
For each land application site, attach a soil evaluation by a soils scientist (the evaluation must be signed by the soil
scientist) which addresses soil color; the depth, thickness and type of restrictive horizons; the presence or absence of a
seasonal high watertable or bedrock within three vertical feet of the deepest point of residual application; pH and cation
exchange capacity. If the depth to either groundwater or bedrock is less than three feet, please also attach a demonstration,
using predictive calculations or modeling methods acceptable to the Director of the Division of Environmental
Management, that the use of this site will not result in the contravention of classified groundwater standards as contained in
NCAC 2L .0200. In no case shall the separation be less than one foot. This report must be signed by the soil
scientist and submitted with application.
3. For each site, please attach a project evaluation conducted by an agronomist including recommendations concerning cover
crops and their ability to accept the proposed loading of liquids, solids, nitrogen, phosphorus, heavy metals, salts and any
other contaminant know to be in the residual. A part of the agronomists recommendations must be a crop management
plan. This plan must determine the crops to be grown on the site(s), when they should be grown and how they should be
harvested and marketed. This report must be signed by the agronomist and submitted with application.
4. Attach a representative soils analysis of each site. The soils analysis shall include the following parameters, along with
any other significant parameter that has been shown to be contained in the residual:
Standard Soil Fertility Test (which includes):
And the following Pollutants:
pH
Phosphorus
Acidity
Calcium
Magnesium
Zinc
% Humic Matter
Sodium
Base Saturation (by
calculation)
Cadmium Lad
Potassium
Manganese
Copper
Cation Exchange Capacity
Nickel
5. In order to assist DEM in the review of the proposed loading rates, please complete the calculations contained in the
attachment titled "Calculations Work Sheet" (beginning on Page 11 of 18). If more than one residual is to be covered by
this permit, additional worksheets must be attached.
VI. GENERAL INFORMATION:
1. Five (5) complete copies of the permit application and five (5) copies of all required supporting information, including
cover letters must be submitted or the application package will be returned as incomplete.
2. Please explain how access to the land application sites, by both people and animals, will be controlled following the
application of residuals:
Reference Section I — " Management Plan
a. Animals shall not be grazed on the land application sites within 30 days after the application of residuals.
b. Appropriate measures must be taken to control public access to the land application sites during the active site use and
for 12 months following the last application event. Such controls may include the posting of signs indicating the
activities being conducted at the site.
3. Please explain the procedures that will be used to establish and maintain the buffers during the application process (i.e. will
the sites be flagged): Reference Section I — " Management Plan "
4. Please attach an executed "Agreement For the Land Application of Residuals to Private Lands" for each land application site
that is not owned by the applicant. A copy of the DEM approved form is attached. If the applicant wishes to use a
different form or a modified form, prior approval must be received from DEM.
5. Each application site must be assigned a site identification number.
6. Attachments may be utilized to provide the information that is requested in this application form; however, if attachments
are utilized, their location should be so indicated on the application form. All attachments must be numbered to correspond
FORM: LAORS 06194 Page 6 of 18
to the individual parts of the application that require the attachmtint. If the attachments are part of a larger docum:__ a
table must be provided that lisps the locations of the required information.
Applicant's Certification:
I, Nash Lindsey attest that this application for
Permit No. WQ 0003034
Modification Of
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that if all required parts of this
application are not completed d that if all inquired supporting information and attachments are not included, this application package
will be returned as " corqple
Signature �tG� C. �r
Date �/ zi �
THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND
MATERIALS, SHOULD BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DIVISION OF ENVIRONMENTAL MANAGEMENT
WATER QUALITY SECTION
PERMITS AND ENGINEERING UNIT
POST OFFICE BOX 29535
RALEIGH, NORTH CAROLINA 27626-0535
TELEPHONE NUMBER: (919) 733.5083
FAX NUMBER: (919) 733-9919
FORM: LAORS 06194 Page 7 of 18
* No New Sites Being Applied For
Instructions:
Processing of this application will not be initiated until five (5) copies of all of the following
items have been submitted in addition to five(5) copies of the completed application form. If
any of the below items have been excluded from the package, please explain.
1. Is a general location map included?
YES or NO x N/A
2. Is a site map (drawn to scale) included which delineates total and buffered acres and
shows all property lines, buffers, existing wells within 500 feet, topography, drainage
features, and any surface waters?
YES or NO x N/A
3. Is a vicinity map enclosed which clearly indicates the projects location with respect to
State roads and named Surface waters?
YES or NO x N/A
4. Is a signed soil scientist report included which defines the following:
a) field descriptions of texture, color, and structure,
b) depth and thickness of soil horizons,
c) presence of any restrictive soil horizons or layers,
d) depth to seasonal high water table,
e) the hydraulic conductivity,
f) recommended loading rate for the site,
YES or NO x N/A
5. Is a signed agronomist's report included which identifies the crop and loading
recommendations for N-P-K?
YES or NO x N/A
6. Is the Crop Management Plan included in the application package?
YES or NO x N/A
7. Has the Land Owner's agreement been completed and signed?
YES or NO x N/A
8. Appropriate fee in accordance with 15A NCAC 2H .0205(c)(5)-(eff. February 1, 1993):
New Applications, Modifications or Late Renewals $400.00
Timely Renewals without Modifications $250.00
YES x or NO N/A
9. Five (5) copies of all reports, evaluations, agreements, supporting calculations, etc. must
be included as a part of the application package.
FORM: LAORS 06/94 Page 8 of 18
* No New Sites Being Applied For
This form must be completed by the appropriate Regional Office and included with the
submission of the application package.
INSTRUCTIONS TO APPLICANT
In order to determine the classification of the watershed in which these land application activities will be
located, you are required to submit this forth, with items 1 through 8 completed, to the appropriate Division of
Environmental Management Regional Water Quality Supervisor (see attached listing). At a minimum, you must
include an 8.5" by 11" copy of the portion of a 7.5 minute USGS Topographic Map which shows the subject
surface waters. You must identify the location of the facility and the closest downslope surface waters (waters for
which you are requesting the classification) on the submitted map copy. The application may not be
submitted until this form is completed and included with the submittal.
1. Applicant (please specify the name of the municipality, corporation, individual, or other ):
2. Name and Complete Address of Applicant:
Citv:
Telephone Number: ( )
State:
3. Project Name:
4. Volume of residuals to be land applied:
5. Name of closest surface waters:
6. County(s) where land application site is located:
7. Map name and date:
8. Applicant Signature:
a
dry tons per year
TO: REGIONAL WATER QUALITY SUPERVISOR
Please provide me with the classification of the watershed where these land application activities will occur,
as identified on the attached map segment:
Name of surface waters:
Classification (as established by the Environmental Management Commission):
Proposed Classification, if applicable:
Signature of regional office personnel:
Date:
FORM: LAORS 06/94 Page 9 of 18
DIVISION OF ENVIRONMENTAL MANAGEMENT REGIONAL OFFICES (11/93)
Asheville Regional WQ Supervisor
59 Woodfin Place
Asheville, NC 28801
(704)251-6208
Fax (704) 251-6452
Avery Macon
Buncombe Madison
Burke
McDowell
Caldwell
Mitchell
Cherokee
Polk
Clay
Rutherford
Graham
Swain
Haywood
Transylvania
Henderson
Yancy
Jackson
Fayetteville Regional WQ Supervisor
Wachovia Building, Suite 714
Fayetteville, NC 28301
(910)486-1541
Fax (910) 486-0707
Washington Regional WQ Supervisor
Post Office Box 1507
Washington, NC 27889
(919) 946-6481
Fax (919) 975-3716
Beaufort
Jones
Berrie
Lenoir
Camden
Martin
Chowan
Pamlico
Craven
Pasquotank
Currimck
Perquimans
Date
Pitt
Gates
Tyrell
Greene
Washington
Hertford
Wayne
Hyde
Mooresville Regional WQ Supervisor
919 North Main Street
Mooresville, NC 28115
(704)663-1699
Fax (704) 663-6040
Raleigh Regional WQ Supervisor
Post Office Box 27687
Raleigh, NC 27611
(919) 5714700 .
Fax (919) 5714718
Chatham
Nash
Durham
Northampton
Edgecombe
Orange
Franklin
Person
Granville
Vance
Halifax
Wake
Johnston
Warren
Lee
Wilson
Wilmington Region. WQ Supervisor
127 Cardinal Drive Extension
Wilmington, NC 28405-3845
(910) 395-3900
Fax (910) 350-2004
Anson
Moore
Alexander
Mecklenburg
Brunswick New Hanover
Bladen
Robeson
Cabamts
Rowan
Carteret Onslow
Cumberland
Richmond
Catawba
Stanly
Columbus Pender
Harnett
Sampson
Gaston
Union
Duplin
Hoke
Scotland
hedell
Cleveland
Montgomery
Lincoln
Winston-Salem Regional WQ Supervisor
8025 North Point Boulevard, Suite 100
Winston-Salem, NC 27106
(910)896.7007
Fax (910) 896-7005
Alamance
Rockingham
Alleghany
Randolph
Asbe
Stokes
Caswell
Surry
Davidson
Watauga
Davie
Wilkes
Forsyth
Yadkin
Guilford
FORM: LAORS 06/94 Page 10 of 18
CALCULATIONS WORK SHEET
This work sheet is designed to assist the Division of Environmental Management in reviewing this application as expeditiously as
possible. Its preparation in a complete and accurate manner is critical to this review. For permits that cover multiple sources of
residuals or different residuals from the same source, use additional work sheets.
A. List the specific residual that is covered by these calculations (place or process of origin)
Rocco Turkeys, Inc. (Effluent Lagoon Residual Solids)
What are the total dry tons of this residual to be land applied each year?
Total Dry Tons = Gallons of Residuals • % Solids • 8.34 lbsJgallon
produced annually 100
2,000 lbs./ton
ToWDryTons= 1,500,000 • 6.0 •8.34lbsJgallon
100
2,000 lbs.hon
= 375
Dry Tons per year
If the quantity of residual will vary significantly or if there will be a larger initial application, please attach a detailed
explanation and provide calculations for each variation.
B . Complete the following calculations to establish the portion of the residual that is made
up of the various parameters:
% Total Solids = 1.72
(PLEASE NOTE THAT ALL CONSTITUENTS ARE TO BE IN TOTAL CONCENTRATIONS)
PARAMETER
m /L
+ % Solids Decimal
- (drywt.
x 0.002
= IbsJdr ton
Cadmium
= 1.0
x 0.002
= 0.002
Co er
= 595.0
x 0.002
= 1.190
Lead
= 22.0
x 0.002
= 0.044
Nickel
= 116.0
x 0.002
= 0.232
Zinc
= 2,350.0
x 0.002
= 4.700
Ammonia-N
= 13,400.0
x 0.002
= 26.800
Calcium
= 7,500.0
x 0.002
= 15.000
Magnesium
= 2,800.0
x 0.002
= 5.600
NO3-NO2-N
= 221.8
x 0.002
= 0.444
Phosphorus
= 4i 100.0
x 0.002
= 94,200
Potassium
= 2,300.0
x 0.002
= 4.600
Sodium
= 9,700.0
x 0.002
= 19.400
TKN
- 69.200.0
x 0.002
= 138.400
OTHER:
=
x 0.002
=
=
x 0.002
=
=
x 0.002
=
=
x 0.002
=
=
x 0.002 1
=
FORM: LAORS 06/94 Page 11 of 18
C. Plant Available Nitrogen (PAN) calculations and land application area requirements:
1. Mineralization Rate (MR) 30% %
(These values can be established for the specific residual or default values can be used for domestic wastewater treatment
residuals. If actual values are established, attach the documentation. The default values are as follows):
Unstabilized Primary and Secondary Residuals 40%
Aerobically Digested Residuals 30%
Anae obically Digested Residuals 20%
Composted Residuals 10%
(If the default values are used, attach an explanation as to why the specific chosen default value is appropriate.)
2. Complete the following calculations for the application method proposed (Please note, the Mineralization
Rate [MR] should be utilized in the following calculations as a decimal):
PAN for Surface Application
PAN = [(MR) x JXN - NH3)] + .5 x (NH3) + (NO3-NO2-N)
PAN=[ 0.3 x( 69,200
PAN = 23,662
- 13,400 )]+.5 x ( 13,400
PPM Dry Weight
PAN for Subsurface Application
PAN = [(MR)x(TKN - NH3)] + (NH3) + (NO3-NO2-N)
PAN=[ 0.3 x( 69,200 13,400 )l+( 13,400
PAN =
30,362
PPM Dry Weight
3. Total PAN to be land applied per year
Totalof residual to be land applied per year: 375
Total PAN in pounds (PAN in mqIkg Ehy Weight) x 2000 Pnundlz / Ton
per dry ton 111 111
_ (PAN in PPM Dry Weight) x 0.002
)+ 221.8
221.8
60.72 Pounds/Dry Ton/Year
Total PAN in pounds = (PAN in Pounds / Dry Ton) x Total tons of residual to be land applied
60.72 x 375
22770 Pounds/Year
Due to the fact that organic nitrogen is mineralized slowly over time, the amount of nitrogen that comes available in years
following the initial application must be taken into consideration when calculating application rates for the subsequent
years. This being the case, please attach an evaluation of this factor and its impact on loading rates. Show the adjusted pan
for at least five years. * See Next Page For Table
The maximum adjusted annual PAN is 8,182.5 Pounds/Year. (Thru Five Years —
4. Crop information on nitrogen uptake per year Residual PAN Remaining)
(Division Recommendations) (Provide for the Crops Specified)
Crop(s) PAN (lbs./acre/year) PAN (lbsJacre/year)
Alfalfa 200 200
Bermuda Grass (Hay, Pasture) 220 220
FORM: LAORS 06/94 Page 12 of 18
July 7, 1995 ROCCO TURKEYS EFFLUENT LAGOON RESIDUALS ANALYSIS
TKN = 69,200 mg/kg
NH3 = 13,400 mg/kg
N0; NO,-N = 221.8 mg/kg
P N = [min. rate (TKN - NH3) + 0.5 (NH3) + NO3 - NOZ] 0.002
_ [0.30 (69,200 mg/kg - 13,400 mg/kg) + 0.5 (13,400 mg/kg) + 221.8 mg/kg] 0.002
_ [0.30 (55,800 mg/kg) + 6,700 mg/kg + 221.8 mg/kg] 0.002
[16,740 mg/kg + 6,700 mg/kg + 221.8 mg/kg] 0.002
_ [23,661.8 mg/kg] 0.002
P N = 47.32 Ibs/DT
Calculate residual nitrogen for years 2,3,4 and 5 following the initial application to determine
the amount of P N/DT remaining.
2ND YEAR RESIDUAL PAN
P N = [min. rate (1st year org. - N-2nd year min. - N] 0.002
[0.15 (55,800 mg/kg - 16,740 mg/kg)] 0.002
_ [0.15 (39,060 mg/kg)] 0.002
[5,859 mg/kg] 0.002
P N = 11.72 Ibs/DT remaining from 1st year application
3RD YEAR RESIDUAL PAN
P N = [min. rate (2nd year org. - N-3rd year min. - N] 0.002
_ [0.08 (39,060 mg/kg - 5,859 mg/kg)] 0.002
_ [0.08 (33,201 mg/kg)] 0.002
_ [2,656 mg/kg] 0.002
P N = 5.31 Ibs/DT remaining from 1st year application
4TH YEAR RESIDUAL PAN
P N = [min. rate (3rd year org. - N-4th year min. - N] 0.002
_ [0.05 (33,201 mg/kg - 2,656 mg/kg)] 0.002
[0.05 (30,545 mg/kg)] 0.002
[1,527 mg/kg] 0.002
P N = 3.05 Ibs/DT remaining from 1st year application
5TH YEAR RESIDUAL PAN
P N = [min. rate (4th year org. - N-5th year min. - N] 0.002
_ [0.03 (30,545 mg/kg - 1,527 mg/kg)] 0.002
_ [0.03 (29,018 mg/kg)] 0.002
_ [870.5 mg/kg] 0.002
P N = 1.74 Ibs/DT remaining from 1st year application
Residual P N from years 2 thru 5 after the initial application = 21.82 Ibs/P N/DT
c:%WP51%1599%Farwwwa\aa95039c.1 (aJn)
Bermuda Grass (Coastal)
350
350
Blue Grass
120
120
Com (Grain)
160
160
Com (Silage)
200
200
Cotton
70
70
Fescue
250
250
Forest (Hardwood & Softwood)
75
75
Milo
100
100
Small Grain (Wheat, barley, oats)
100
100
Sorghum, Sudex (Pasture)
180
180
Sorghum, Sudex (Silage)
220
220
Soybeans
200
200
Timothy, Orchard, & Rye Grass
200
200
Please provide the basis for the uptake rates used if
different than Division Recommendations:
5. Total acres needed to land apply the pounds
of available nitrogen calculated above
Total acres needed: = Mazimum total mundc off ant available nitrogen (PAN)
Pounds of nitrogen needed for crop*
22,770
* Most Restrictive
PAN
70*
For Cotton
Minimum acres needed based on most restrictive PAN = 325.3
acres
* This value must be the value for the crop to be grown that has the lowest nitrogen uptake rate per acre.
If there are various crops that will only be utilized for certain sites, please attach the calculations for each site and determine
the total needed acres using the format outlined above.
D. Calculate the Sodium Adsorption Ratio (SAR)
(**This section must be completed in mg/l, to convert: mg/kg x % solids [as a decimal] = mg/1**)
SAR = Na Milli Equivalent + 10.5 (Ca Milli Equivalent + Mg Milli Equivalent)] 0.5
CONCENTRATION (mg/1) + Equivalent Weight = Milli Equivalents of Ion
SODIUM (Na) 166.84 (mgn) + 23 = 7.25
CALCIUM (Ca) 129.00 (mg/1) + 20 = 6.45
MAGNESIUM (Mg) 48.16 (mg/1) + 12 = 4.01
SAR = 3.17
If calculation sheets are being completed for more than one residual or site, please attach a
summary sheet that bring the results of all the calculation sheets to one point.
FORM: LAORS 06/94 Page 13 of 18
E. Determine the Site Life for this land application site:
The lifetime pollutant loadings'shall not be exceeded. The site fife is determined by calculating the number of years that the site
can receive the residual without exceeding the lifetime pollutant loadings. The site life calculations will be based on the most
restrictive crop plant available nitrogen (PAN) requirement specified and the maximum dry tons of residuals to be land applied
annually. Therefore, in the table below the Tons of Residuals to be Applied/AcrefYear will be calculated as:
1. Most restrictive crop based on the plant available nitrogen (PAN) requirement
Associated plant available nitrogen (PAN) requirement
70
Cotton
(lbsJacre/year)
2. Minimum acres needed based on most restrictive PAN (as found in C.5 above): 325.3
3. Dry Tons of Residuals to be land applied per year. 375 dry tons per year
4. Tons of Residuals to be Applied/AcreJYear= icy Tons/Year of Residuals to be land aWfied
Minimum number of acres required for land application
Tons of Residuals to be Applied/Acre/Year =
acres
If any of the application sites are to be loaded at greater than the rate specified above, please specify the loading rate and explain:
Tons of Residuals to be Applied/AcreNear (different from above) = 3.29
Explanation: .200 lbs PAN/AC/YR For soybean : 60.72 lbs/PAN/DT = 3.29 DT/AC/YR
For the purpose of site life determination, the lifetime pollutant loadings shall not exceed the following for the corresponding
Cation Exchange Capacities (CEC). Site life for the site covered by this application sball be determined by using the lowest
CEC. The appropriate column should be chosen and applied in the "Allowable Lifetime Pollutant Loadings based on CEC" in
the table below.
Pollutant
CEC < 5
(lbs /acre)
CEC 5-15
(lbs /acr)
CEC > 15
(lbs /arm
Lead
500
1,000
2,000
Zinc
250
Soo
1,000
Copper
125
250
500
Nickel
125
250
500
Cadmium
4.5
9
18
In the table below, the highest annual loading (Tons of Residuals to be Applied/Acre/Year) specified above, will be multiplied
by the lbsJdry ton of each pollutant as found in B above. The Site Life can tben be determined by:
Site Life (Years) = Allowable Lifetime Loadings (Ibc /acre)
Projected Pounds to be Applied/Acre/Year
Pollutant
Tons of
lbs./dry ton of each
Projected
Allowable Lifetime
Residuals to be
pollutant
Pounds to be
Pollutant Loadings
Site Life
Applied per
(as found in Part B
Applied/Acre
based on CEC.
(Years)
Acre per Year
above)
/Year
From Chart above
lbs./acre
Lead
3.29 *
0.044 =
0.145
500
= 3,448.3
Zinc
3.29 *
4.700 =
15.463
250
= 16.2
Copper
3.29 *
1.190 =
3.915
125
— 31.9
Nickel
3.29 *
0.232 =
0.763
125
= 163.8
Cadmium
3.29 *
0.002 =
0.007
4.5
— 642.8
Compare the five (5) pollutants above and determine which pollutant that will result in the shortest life for this site.
The Limiting Pollutant Is zinc
The Site Life is
years.
FORM: LAORS 06/94 Page 14 of 18
Bo Bev bites tieing Applied for
North Carolina Division of Environmental Management
AGREEMENT FOR THE LAND APPLICATION OF WASTEWATER RESIDUALS
TO PRIVATE LANDS
Permittee:
Contact Person:
Address of Permittee:
List of wastewater residuals to be applied to these lands:
Site ID Number:
Field Number:
Location of Land to be used for residual application (include map for each site):
Owner of Property used for residual application:
Lessee of Property (if appropriate):
Land use or cropping patterns: _
Intended use or disposition of crops:
The undersigned land owner or his representative hereby permits
hereinafter referred to as the Permittee, to apply the above listed residuals onto the land at the location
shown as described herein in accordance with the restrictions and stipulations as given below. The
landowner or his representative receives, in consideration, full use of the nutrient value of the applied
residuals while the Permittee receives, in consideration, the use of the land described above for the
disposal of wastewater residuals. This agreement shall remain in effect for the length of the Division of
Environmental Management land application permit and shall be renewed each time the land application
permit is renewed. The undersigned land owner or his representative and the Permittee agree to abide with
the following restrictions and stipulations until such time as written notification, given thirty (30) days in
advance, modifies or cancels this Land owner's Agreement.
Notification of cancellation of this agreement shall be immediately forwarded to:
Division of Environmental Management
Permits and Engineering Unit
Post Office Box 29535
Raleigh, North Carolina 27626-0535
FORM: LAORS 06194 Page 15 of 18
STIPULATIONS:
The landowner or his representative hereby authorizes the Permittee, County and State Officials or
their representatives to inspect each parcel of property prior to, during, and after residual application
and to established monitoring facilities on or near the application site as required by the residual land
application permit.
The landowner or his representative authorizes the Permittee, County and State Officials or their
representatives to take necessary soil, surface and ground water samples during the term of, and
twelve (12) months after termination of, this Agreement.
3. The Permittee will provide each landowner or his representative with a copy of the land application
permit as issued by the N.C. Department of Environment, Health and Natural Resources
(NCDEHNR) Division of Environmental Management (DEM) for the land described above prior to
commencement of residual application. The NCDEHNR-DEM permit will specify maximum
application rates, limitations and other restrictions prescribed by the laws and regulations.
4. The Permittee has provided the landowner or his representative with information and data concerning
the program for land application of residuals to privately owned lands which includes an analysis of
constituents of the residual, residual application methods and schedules for typical cropping patterns
and a description of the equipment used by the Permittee for residual application.
5. The Permittee will furnish each landowner or his representative with a copy of the results of each soil
analysis.
6. The site shall be adequately limed to a soil pH of at least 6.0 prior to residual application. Residuals
may be applied to sites with a pH of less than 6.0 provided a sufficient amount of litre is also applied
to achieve a final pH of the lime, residual and soil mixture of at least 6.0.
The landowner of his representative will inform the Permittee of any revisions or modifications to the
intended use and cropping patterns shown above prior to each planting season to enable the Permittee
to amend this Agreement and schedule applications at appropriate periods. Within the limits of the
NCDEHNR-DEM permit, the owner or his representative and the Permittee will determine residual
application rates and schedules based on crop patterns and the results of soil samples.
Crops for direct human consumption shall be harvested in accordance with the conditions of the
permit
9. The landowner or his representatives or successors shall adhere to the provisions of this Agreement
for a period of eighteen (18) months from the date of the most recent residual application.
10. Appropriate measures must be taken by the Permittee or Land Owner (Lessee) to control public
access to the land application sites during active site use and for the twelve (12) month period
following residual application. Such controls may include the posting of signs indicating the
activities being conducted at each site.
11. Spec residual application area boundaries shall be clearly marked on each site by the Permittee or
Land Owner (Lessee) prior to and during application.
I2. Should the landowner or his representative lease or otherwise permit the use of the land by a third
party, the landowner shall be responsible to insure the third party agrees and complies with the terms
and conditions of this Agreement.
13. The existing lessee, if any, of the site agrees, by execution of this Agreement, to comply with all
provisions of this Agreement.
FORM: LAORS 06/94 Page 16 of 18
14. This Agreement shall be binding on the grantees, the successors and assigns of the parties hereto
with reference to the subject matter of this Agreement.
15. Animals should not be grazed on residual applied lands within a thirty (30) day period following the
residual application. Application sites that are to be used for grazing shall have fencing that will be
used to prevent access during these periods after each application.
16. Prior to a transfer of this land to a new owner, a permit modification must be requested and obtained
from the Division of Environmental Management. The request shall contain appropriate fees and
agreements. In addition, a notice shall be given by the current landowner to the new landowner that
gives full details of the materials applied or incorporated at each site.
17. Any duly authorized officer, employee, or representative of the Division of Environmental
Management may, upon presentation of credentials, enter and inspect any property, premises or
place on or related to the application site and facility at any reasonable time for the purpose of
determining compliance with this permit; may inspect or copy any records that must be kept under
the terms and conditions of this permit; or may obtain samples of groundwater, surface water, or
leachate.
18. The landowner shall not enter into any additional waste disposal contracts or agreements with
another municipality, contractor, or other permitted entity for the land specified by this Agreement.
The land application of any additional wastewater residual sources, other than the residuals specified
by this permit, is prohibited.
RESTRICTIONS:
FORM: LAORS 06194 Page 17 of 18
• f f t f f i f t/ f f 1} i f f• f f f 1 f f t f t f f•} 1 f f f f i f i f f 1 f f f} t f f f f f t M t f
1, have read this land owner's agreement and do hereby grant permission
to the Perminee to apply sludge/residual to my lands as specified herein.
NORTH CAROLINA,
I, the undersigned Notary Public, do hereby certify that
Land Owner
Date
COUNTY,
personally appeared before me this day and acknowledged the due execution of the forgoing instrument.
WITNESS my hand and official seal this day of 19
ARY PUBLIC
My commission Expires
SEAL:
L
the stipulations and restrictions as specified herein.
1
the stipulations and restrictions as specified herein.
have read this land owner's agreement and do hereby agree to abide by
Lessee
Date
have read this land owner's agreement and do hereby agree to abide by
Permittee
Date
FORM: LAORS 06/94 Page 18 of 18
APPENDIX I
RESIDUAL SOLIDS ANALYSIS REPORTS
ROCCO TURKEYS, INC. EFFLUENT LAGOON RESIDUAL SOLIDS
NUTRIENT AND METAL ANALYSIS
ROCCO TURKEYS, INC. EFFLUENT LAGOON RESIDUAL SOLIDS
ROCCO TURKEY'S
LAND APPLICATION PROGRAM
RESIDUALS ANALYSIS
Residual Type: Wastewater Treatment Plant
Date: July 7, 1995
pH: 7.2
LAGOON SLUDGE 1.72 % Solids
Parameter
%
PPM Dry Weight
x 10,000)
Pounds/Dry Ton
PPM x 0.002
Nitrogen (TKN)
6.920
69,200.000
138.400
Phosphorus
4.710
47,100.000
94.200
Potassium
0.230
2,300.000
4.600
PAN (injected)*
3.036
30,360.180
60.720
PAN (surface)*
2.366
23,661.800
47.324
Ammonia Nitrogen
1.340
13 400.000
26.800
Calcium
0.750
7,500.000
15.000
Calcium Carbonate Eq.
0.000
0.000
0.000
Magnesium
0.280
2,800.000
5.600
Sodium
0.970
9,700.000
19.400
Sulfate
0.299
2,990.000
5.980
Nitrate N
---
220.000
0.440
Nitrite N
- - -
1.800
0.004
Manganese
- - -
1,590.000
3.180
Chloride
---
810.000
1.620
Iron
- - -
114,000.000
228.000
Aluminum
- - -
9,250.000
18.500
Arsenic
- - -
2.140
0.004
Cadmium
---
1.000
0.002
Chromium
- - -
116.000
0.232
Copper
- - -
595.000
1.190
Lead
- - -
22.000
0.044
Mercury
- - -
0.240
0.000
Mol bdenum
- - -
7.000
0.014
Nickel
- - -
116.000
0.232
Selenium
- - -
1.3201
0.003
Zinc
---
2,350.000
4.700
A&L Hepon No. H182-136
Determination of Plant Available Nitrogen (PAN):
Injected Application:
(Mineralization Rate) (TKN -Ammonia N) + Ammonia N + Nitrate N + Nitrite N = % PAN
(0.3) (6.92-1.34) + 1.34 + 0.022 + 0.000 = 3.036 % PAN
Surface Application:
(Mineralization Rate) (TKN-Ammonia N) + (0.5)(Ammonia N) + Nitrate N + Nitrite N = % PAN
(0.3) (6.92-1.34) + (0.5) (1.34) + 0.022 + 0.000 = 2.366 % PAN
p Cl�a� A & L: EASTERN AGRICUVWRAL. LABORATORIES, INC.
0-- 7621 WtAtapins P.oad : 'Richmond, Virginia23237 • (804) 743-9401
Fax No. (a04) 271-64-46
pla:;-136 ACCOUNT 45J99 PAGE 1
a
REPORT NUMBER
a
9
r
9
9
ROCCO TURKEY PO 011105 i B
ATTN: BILLY DANIELS
Pus 9
ST PAULS NC 2Ei384
SLUDGE ANALYSIS REPORT
LAR NUMBER = 42 936 0. 3 ( (o.92 - /. 34) f 1. 34 4 0 •D 2 _' lS
SAMPLE ID = LAGOON SLUDGE - 1. (074- t ), 34- -4 0. D22 IS'
DE rFCl-ION
RESULT RESULT LIMIT
PARAMETER ( 'x ) (MG/KG) (MG/KG) ANALYST
P!'LLY DANi::LS
4
C
r
i
Y
DATE SAMPLED 06/29/95 N
RATE RECEIVED 06/30/9:i
DArE REPORTED 07/07/95 U
ANALYSIS
DATE METHOi1 REFERENCE
SOLIDS I.72 17=:100 5C•:� JCh: uA/30/i`5 fi14 254)G
.n .�ITc OSI.N (T".N? 6. c_ t.0_L00 1t}0 ,-, •ntS �', ,- .'•F, .-. -' =i
P!'.OSrHfl}US 1.?1 474,00 P.0 i+isi.
z :,DTASSWil 0.23 2300 ;00 E..C14 07/i3/95 Sw ':41.-6Gi
./ C-At-crum 0.iS 7500 1dQ DCN 6'7/011,1:75 sic 23-:6-60ii+
1ACNESI!1M 0.20 2800 100 i!CN 07/pz/95 SW 646-601!i
SODIUM 0.97 9700 100 r1cc 07/03/95 sw 846-•6010
y IRON 114000 ? DcN r7/0=%/95 Sig 541)-30:i 0
ALUMINUM 9250 10 r.ICN 07/03/95 sw +G46-6010
MO:NGANESE 1590 13C& 07/03,195 Sid 046-6010
COPPER 595 1 DcN 07/C3195 -ow 046-6010
D ZINC 2550 4.Io�dt I DCN 0//03/9b JW 846-6010
n n AMMONIA !NITROGEN 1,34 13400 100 LDR 07/03/95 EPA 350.2
NITRATE NITROGEN 220 10 LCiii 07/03/95 EPA -3N2.1
:AIIMIL'M i.0 I DCN 07/03/9't SW 846-6010
T CHROM,UM 116 5 rlcN O//03/95 SW 846-6010
0 NICKEL 116 5 LCN 07/03,195 Su 046-6010
LE AG 22 S DCN 07/0;;/95 Si.l E46--6010 of
ALL VALUES EXCEr`T. SOLIDS AND TSS ARE ON A DRY WC r .H7 BASIS , - „( a lye
W repOft OW bOrt me br ft mdovwand mMdoOW u Wout 050Al,aM May ..nt 60 le L H. tt ��ym / N INMAN
wO.k. Wereadla a'Ihn rnmurnrN awMwnki.n ...w:mmw t r Wwin pet r.or may.mytelmaou lw .natlelO U+e !\ .
y rSNoduratt� O
• 4
A:uc LEAeSTERN` A ORiCiLTURA , LAE307AT-RATc
7621 Wh Wpioe Road' ►; Richmond,Yfglrna 23237 (804) 743-8401 _
Fax No. tW 4j 271 6446
c'~v RIU2-136 ACCOUNT 45799 PACE 2'
REPORT NUMBER �
N
ROCCO TURKEY FYI tI30518 BILLY DANIELS
ATTN: BILLY DANIELS
POP 9
ST PAULS NC 283R4
b SLUDGE ANALYSIS REPORT
PATE SAMPLED :, N
06/29/9
LAIC NUMBER = 42936 LATE kLt.EiVEl) 06/30/?.`,
m
SAMPLE iP = LAGOON SLUDGE LATE RePORTED 07/07/95 tq
Ul
7
' DETECTION
RESULT C:tPiULT: LIMIT AiM}LYSI S
PARAMETER C X > (M6/K6) (MG/KG) ANALYST DATE METHOD REFERfHCE
NRsE N iC 2.14 0.4 VLN 07/05/95 sw 846-7061
c:%JRY , .24 n, 04 8%lt -. 5 Sly 84E.-7 t71
SELENIUM 1.32 0.1 DCN 07/Or!`>5 5ii 046-7741
YI1 (STANDARD UNITS) iN V— V-4 9:, EF'A 1S0. 1
'J :;RGANIC NITROGEN 3.58 11,100 iJO t.� ;�%/�.;/?:� i'li.� ij; I.TF LI
z n01_YB£�Eh1UM - `; DrN 07l03l?• sw 646-6010
CHLORIDE- a10 1 LDR 07/DA/94 3N 4500-Cl_
NITRITE NITROGEN 1.80 0.0; ":CS 0710=/95 F-A, 3-�4.1
SULFATE 2990 10 JCM 071J3/95 sw 846-9039
D
n
D
O
7
T
ALL VALUES EXCEPT SOLIDS AND TSS ARE ON A.DRY_WEIGHT BASIS. }/ /JLXti1X � � 0
F�AUi_ C. q. CHl} FHA WES N
CLrropwteandfNart enfordb anitiue antlo�nfidanYat�eof ouftlienlS. anOynsy tql bnreoaxHCEa da nrmpart. mr mrq any rdererw tromWero uw �/
wv0.um rnw3. or the co pry in any wig. wars wge ,or othmP We anpaudce„bvm wnta l0l>Wf kV our pia. w%m Wdhwkmbo . CopyrgOtlwl
TCLP ANALYSIS
ROCCO TURKEYS, INC. EFFLUENT LAGOON RESIDUAL SOLIDS
=R211;K5NIC9 =HX
TO. Si0285858u - .IjL 2!• 1985 =.d2
00\01%k�k
CEntrE Analytical
Laboratori
ES. Inc.InC
9W8 RNNYoh OrlYe4 BLfte Co7h7ge FA 10001 014-2.91.M2 FAX 074-231.1233
ROCCO TURKEYS Dete Received: 05-JUN-95
PO BOX 9 DALe RemTtcd: 16-JUN-9T.
SAINT PAMIS , NC 28384
ACCOUnt NBnber: 1248 Invoice NumLerl 7673
Contact: BILLY DAHIEL$ DACE C013CCFCd: 02-J1.:-95
rllCnt ID: LAIYJON 5LUW5
14b TD: L9163-1
?ADWMER UNTTS I RESULT I QUAhTIF1 CATION TES7 METHOD TEST DATE ANALYST
Nd11DIC,ip;1Se Y�itLP J:��>^.}.;;,.;•,;.,,': y t;
2,4-1)
ug/T,
c .5
I .5
SPA 6:50
09-JUN-95
C9
SILVEE
ug/L
< .167
I .167
EPA 61.50
D9-.nm-94
Os
707RCURY-TLMP LEACH41E
tD9/L
.00J7
.0002
EPA 7470
14-JUN-95
jR
!b^:AL5.t+^ICiiP;':+T,97;'.w;.•:', :�: „:::.`;.
SII.VRR-TCLI' MACHATE
mg/L
< .05
.05
EA 200.7
06-JUN-95
JH
ADRRNTC-TY'Ln TRAC71IITk
RiJ!L
< .OS
r
V6•JUN-95
EARITP4-TCLP LEACHATE
I:g/L
.754
.31
EPA 2CD.7
in
CAMIUN-1'CLP LEACNATE
ng/L
< .01
.02
EPA 200.7
06-JUN-95
CHROMIUM!-TCLP LEACITATF
eg/L
c .01
.vi
EPA 200.7
06-JUN-95
JH
1,RAD-TCLP LEACHATE
UO/L
c .03
.03
EPA 200.7
H
9P.LENTUM-PON' I•LACRATE
mg/L
c . Ga
EPA 200.7
06 JUN-95
JH
.05
OS•JUN-0s
v
- -
3A.WA-ORC
HEMCI1LOR
U0/L
ug!L
•. .132
173
EPA 0080
06-GVN•5b
C6
HEPIACWDR EPDXIDE
11q/L
c .133
.133
SPA 996D
OB-JUN-96
CS
RNI
ug/L
c .333
.133
EPA 008D
08--95
CiETn S
NETAOIY(ODAR
u9/L
< .233
c .507
.133
EPA 8000
08-4tmJC01
-95
CS
TO%APHKNH
ug/L
< 6.67
.66•1
6.67
EPA 8080
EPA Soeb
08 JUN•D5
CS
uy/L
< 0.87
6.67
EPA 8000
00-JUN•9S
CSSYILORDM'n
08-JUN-95
CS
E 4m'ru3LPNe ul,
u8/L
c 20
20
EPA 9270
1-M�rl'HYLPlItli01
ug/I,
< 20
20
EPA 6270
DO-JUN-95
CS
4-MMIYLFMOT,
uR/L
c 20
7.n
EPA $270
DO-JUN-95
CS
PNN UILDRODDENOC,
ug/L
< 20
20
00.011H-95
Cs
2,4. 5-TR7C:RIDR0l'IIENOL
EPA 8270
08-J�-95
(S
2,4.6.07<1CHLUHOP1iENOI.
u�/T.
< 20
xR
SPA 8270
08-JCT4-95
CS
IR:%AC31TOR0R771ANE
ug/L
c 20
20
EPA 8270
us-itim-95
CS
HNXACIMMODUTAWM.
ug/L
< 20
20
EPA 8270
08-JUN-95
CS
N77RnRRNPRRa
ug/L
< 10
•u
SPA 8270
EPA 6270
08-J'JN-95
C8
yNXACifLDAODENP.RNY.
uE/L
a 20
20
EPA 8270
09-JUN-96
CS
09-JUN-95
CS
® P7eeee refer to the re Worse owe for our elenderd lerme and Oond440ne.
=RDN;K7NIC�i =Fix
TO: �-10zasa5aJ 7JL 21, 1565 c: 02pI [_
I 1�1 r I • • I
Gk\eNk CCntrE Analytical
Laboratories, Inc..
3048 Raaearoh Drive, State College PA 18801 814-014032 FAX 814-01-12m
ROCCO TMKFYS
PO Box 9
SAINT PAUL'S , NC 283e4
Account Number: 124E
Contact: BILLY DANIELS
Cli.coy ID: La[KI 17 9LVDUC
'Lab ID; 1,8185-I
PARAMETER
UNITE
2,4-OINITROT'OLUENE
v5/L
PYR7Lin1:
ug/L
9DffiTSLES TCLP:: �LTBT .,......
vlayL cMLUE1De
ug/L
1,1-DICHLOROETIIENE
ug/L
2-NU1'ANONS
V9/L
C=ROPDRM
ug/L
CARBON TsIRACALOR1DE
ug/L
RRNRRNR
uQ/L
1,2-DI0=..OETNANE
ug/L
TRICNIAROETNRVF:
Vg/r.
T117T,MM114noM:1@nC
ug/L
CHLORODINZENE.
ug/L
3,4 UICflWkOH±NVWXN
u9/T,
PERCENT SOLIDS %
c 2C
20
2.12
Date Received: O6-.TON-95
Dato Rcported: 16-JUN-95
Invoice Number: 7673
Date Collected: 02-JUN-95
LIMIT
—
or
QUANT1EICA'1'ION
TEST
METHOD
TEST DATE
ANALYS`J'
20
EPA
8270
08•JUN-95
CS
20
➢PA
02U
00-JUN-90
c9
le
EPA
"40
74-JVN-9b
E5
5
EPA
8240
14-JUN-9L
aF
70
EPA
8240
14-JUN-95
FS
5
EPA
B240,
14-JUN-95
AS
5
EPA
6246
34-JUN-95
FS
S
EPA
A24n
Id-.nm-9c
R8
5
EPA
5246
244UN-95
RE
5
EPA
8246
14, XN• 9i.
AS
0
DPA
0240
14-JVN-95
A9
5
EPA
82dO
14-JUN-95
R-S
b
EPA
824D
14•JON-95
IS
.01 SM 2LdDA 06 ,-UN-95 R➢SH
SubmiLL6d by
Contra Analytical Labe, Inc.
Reviewed end AAnmvnd My,
Kevin J. Lloyd
Laboratory Svpervieor
® Plasm refer to the reverse a/da for our 8184dard forma and condUidns.