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WQ0036723_2023 Residual Annual Report_20240124 (2)
Initial Review Reviewer nathaniel.thornburg Is this submittal an application? (Excluding additional information.) * Yes No If not an application what is the submittal type?* Annual Report Residual Annual Report Additional Information Other Annual Report Year* 2023 Permit Number (IR) * WQ0036723 Applicant/Permittee Town of Mooresville Email Notifications Does this need review by the hydrogeologist? * Yes No Regional Office Mooresville CO Reviewer Admin Reviewer wanda.gerald@deq.nc.gov Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. Name* Matthew R Herman Email Address* mherman@mooresvillenc.gov Project Information ......................... Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 7046632460 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Permit Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number:* WQ0036723 Has Current Existing permit number Applicant/Permittee Address* 369 Johnson Dairy Rd, Mooresville, NC 28115 Facility Name* Town of Mooresville Class A Residuals Program Please provide comments/notes on your current submittal below. Subject: 2023 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone:704-663-2840 2) Responsible official and facility contact— Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone:704-799-4063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit # W00036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2023 were transported to Randy Boyd in Mt. Ulla NC, Doug Carrigan in Mooresville NC, Scott Atwell in Mooresville, NC, Mike Bowers in Troutman, NC, and Rob Bailey in Mooresville NC. Total = 926.4 dry metric tons (See Attached Hauling Summary Sheets). Our Class A distribution permit was modified in December 2021 which increased our total dry tons to 1600 Dry Tons per Year. All laboratory data from quarterly TCLP analyses have been included in this report. I have attached our daily dryer logs. At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) Class A Annual Report Scan Complete 2023.pdf 3AMB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signature Submission Date 1/24/2024 Town of Mooresville NORTH CAROLINA 2023 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 Annual Class A Report, WQ0036723 Rocky River Wastewater Treatment Facility Mooresville, N.C. 28115 Town of Mooresville NORTH CAROLINA NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699 ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 FAX (704) 662-8473 POST OFFICE BOX 878 MOORESVILLE, NC 28115 1/10/24 Subject: 2023 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone: 704-663-2840 2) Responsible official and facility contact — Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone: 704-799-4063 3) Class "A" dried biosoiids were distributed under Town of Mooresville permit # WQ0036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2023 were transported to Randy Boyd in Mt. Ulla NC, Doug Carrigan in Mooresville NC, Scott Atwell in Mooresville, NC, Mike Bowers in Troutman, NC, and Rob Bailey in Mooresville NC. Total = 926.4 dry metric tons (See Attached Hauling Summary Sheets). Our Class A distribution permit was modified in December 2021 which increased our total dry tons to 1.600 Dry Tons per Year. All laboratory data from quarterly TCLP analyses have been included in this report. I have attached our daily dryer logs. 5) (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: L Hendren Biosolids Coordinator Reviewed by: Jamie Levis, WWTP Plant Manager Signature I -zo - ZA Date - Signature, Date ROCKY RIVER W.W.T.P TELEPHONE (704) 662-8470 Town of Mooresville FAX (704) 662-8473 NORTH CAROL.INA POST OFFICE BOX 878 MOORESVILLE, NC 28115 ' 1/10/24 U.S. EPA Region 7 ATTN: BIOSOLIDS CENTER W WPD/WEN>" 11201 Renner Boulevard Lenexa, Kansas 66219 Subject: 2023 Annual Sludge Report, WQ0036723 Distribution of Class A Residuals Following is the information requested to accompany our Class "A" Annual report. 1) Facility - Rocky River Wastewater Treatment Facility 369 Johnson Dairy RD. Mooresville, N.C. 28115 Phone: 704-663-2840 2) Responsible official and facility contact — Larry Hendren, Bio-solids Coordinator P.O. Box 878 Mooresville, NC 28115 Phone: 704-799-4063 3) Class "A" dried biosolids were distributed under Town of Mooresville permit # WQ0036723 4) (Part A) and (Part B) Distribution of Class "A" Residuals for 2023 were transported to Randy Boyd in Mt. Ulla NC, Doug Carrigan in Mooresville NC, Scott Atwell in Mooresville, NC, Mike Bowers in Troutman, NC, and Rob Bailey in Mooresville NC. Total = 926.4 dry metric tons (See Attached Hauling Summary Sheets). Our Class A distribution permit was modified in December 2021 which increased our total dry tons to 1600 Dry Tons per Year. All laboratory data from quarterly TCLP analyses have been included in this report. I have attached our daily dryer logs. 5) (Part C) I certify, under penalty of law that the above information is, to the best of my knowledge and belief, true and accurate and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations. Prepared by: LM Hendren Biosolids Coordinator Reviewed by: Jamie Levis, WWTP PIant Manager ✓' Signature: ' ��— �--Y ��� Z Date Signature. Y Date Town of Mooresville 2023 Class A Hauling Summary Sheet DATE TONSg „ TRANSPO*RTER DESTINATION `COMMENTS; 1/10/2023 7.1 Town of Mooresville Atwell farm 1 Load 1/12/2023 20.9 Town of Mooresville Atwell farm 3 Loads 1/18/2023 14.0 Mike Bowers Mike Bowers 2 Loads Troutman 1/19/2023 14.4 Mike Bowers Mike Bowers 2 Loads Troutman 1/30/2023 14.4 Town of Mooresville Atwell farm 2 Loads 2/6/2023 13.8 Town of Mooresville Atwell farm 2 Loads 2/7/2023 20.5 Mike Bowers Mike Bowers 3 Loads Troutman 2/14/2023 21.6 Town of Mooresville Atwell farm 3 Loads 2/21/2023 26.8 Town of Mooresville Doug Carrigan 4 Loads 2/21/2023 12.6 Town of Mooresville AFH Sod farm 2 Loads 3/7/2023 33.4 Town of Mooresville AFH Sod farm 5 Loads 3/7/2023 6.9 Town of Mooresville Doug Carrigan 1 load 3/15/2023 26.4 Town of Mooresville Doug Carrigan 4 Loads 3/21/2023 14.0 Town of Mooresville Doug Carrigan 2 Loads 3/21/2023 6.8 Town of Mooresville Randy Boyd 1 Load 3/21/2023 14.3 Town of Mooresville AFH Sod farm 2 Loads 3/24/2023 7.0 Town of Mooresville Randy Boyd 1 Load 3/29/2023 14.3 Mike Bowers Mike Bowers 2 Loads Troutman 4/4/2023 20.7 Town of Mooresville Doug Carrigan 3 Loads 4/4/2023 13.4 Town of Mooresville Randy Boyd 2 Loads 4/4/2023 13.0 Town of Mooresville AFH Sod farm 2 Loads 4/13/2023 28.4 Town of Mooresville Doug Carrigan 4 Loads 4/18/2023 7.3 Town of Mooresville Randy Boyd 1 Load 4/18/2023 13.6 Town of Mooresville Doug Carrigan 2 Loads 4/20/2023 13.4 Town of Mooresville AFH Sod farm 2 Loads 5/2/2023 13.9 Town of Mooresville Doug Carrigan 2 Loads 5/4/2023 20.6 Mike Bowers Mike Bowers Troutman 3 loads 5/8/2023 6.8 Mike Bowers Mike Bowers Troutman 1 Load 5/9/2023 6.9 Mike Bowers Mike Bowers Troutman 1 Load 5/9/2023 6.8 i Town of Mooresville Randy Boyd 1 Load 5/11/2023 6.7 Mike Bowers Mike Bowers Troutman 1 Load 5/17/2023 14.0 Mike Bowers Mike Bowers Troutman 2 Loads 5/18/2023 6.9 Mike Bower's Mike Bowers Troutman 1 Load 5/31/2023 6.8 Town of Mooresville Doug Carrigan 1 load 6/29/2023 20.8 Mike Bowers Mike Bowers Troutman 3 Loads 7/5/2023 13.5 Town of Mooresville Doug Carrigan 2 Loads 7/6/2023 13.4 Town of Mooresville Doug Carrigan 2 Loads 7/7/2023 13.6 Town of Mooresville Doug Carrigan 2 loads 7/11/2023 28.0 Town of Mooresville Doug Carrigan 4 Loads 7/12/2023 21.4 Town of Mooresville Doug Carrigan 3 Loads 7/18/2023 22.1 Town of Mooresville Atwell farm 3 Loads 7/25/2023 22.4 Town of Mooresville Randy Boyd 3 Loads 8/1/2023 21.1 Town of Mooresville handy Boyd 3 Loads 8/9/2023 8/15/2023 14.2 28.7 Town of Mooresville Mike Bowers Doug Carrigan Mike Bowers Troutman 2 Loads 4 Loads 8/18/2023 17.4 Town of Mooresville Doug Carrigan 2 Loads 8/23/2023 21.3 Town of Mooresville Doug Carrigan 3 Loads 9/5/2023 9/19/2023 29.7 14.9 Town of Mooresville Town of Mooresville Doug Carrigan Doug Carrigan 4 Loads 2 Loads 9/19/2023 22.1 Town of Mooresville Randy Boyd 3 Loads 9/20/2023 14.7 Town of Mooresville Randy Boyd 2 Loads 10/3/2023 21.1 Town of Mooresville Doug Carrigan 3 Loads 10/10/2023 29.1 Town of Mooresville Doug Carrigan 4 Loads 10/17/2023 28.8 Town of Mooresville Randy Boyd 4 Loads 10/23/2023 21.2 Town of Mooresville AN Sod farm 3 Loads 10/25/2023 10/27/2023 14.0 7.1 Town of Mooresville Town of Mooresville Doug Carrigan Doug Carrigan 2 Loads 1 Load 10/31/2023 14.4 Town of Mooresville Doug Carrigan 2 Loads 11/2/2023 7.1 Town of Mooresville Doug Carrigan 1 Load 11/3/2023 7.0 Town of Mooresville Doug Carrigan 1 Load 11/7/2023 14.2 Town of Mooresville Doug Carrigan 2 Loads 11/14/2023 7.3 Town of Mooresville AN Sod farm 1 Load 11/15/2023 14.4 Town of Mooresville Doug Carrigan 2 Loads 12/5/2023 14.4 Town of Mooresville Doug Carrigan 2 Loads 12/5/2023 7.2 Town of Mooresville Atwell Farms 1 Load 12/5/2023 14.5 Town of Mooresville Mike Sowers Troutman 2 Loads 12/6/2023 7.2 Town of Mooresville Atwell Farms 1 Load 12/14/2023 7.2 Town of Mooresville Atwell Farms 1 Load Total tons 1063.90 Avg. % solids 0.96 Dry tons 1021.13 Conversion factor 0.907184 Metric tons 965.2 Dry metric tons 926.4 Calculation: Dry metric tons= total tons * avg.% solids* conversion factor Waypdint(D ANALYTICAL 1/24/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref; Analytical Testing Lab Report Number: 23-009-0005 Client Project Description: Class A TCLP Dear Whitney Munroe: 449 Springbrook Rd, Charlotte, NC Z8217 Main 704.S29.6354 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/9/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Anslysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, (DJVL�) Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypointo ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanaiyti cal.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2023 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016/23-009-0005 Page 2 of 8 (D Waypoint, 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalocal.com Sample Summary Table Report Number: 23-009-0005 Client Project Description: Class A TCLP Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 97027 Class A Sludge 01/09/2023 08:47 01/09/2023 11:31 SW-1311 WP MTN 97027 Class A Sludge 01/09/2023 08:47 01/09/2023 11:31 8270C WP MTN 97028 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 97028 Cass A Solids 01/09/2023 08:47 01/09/2023 11:31 SW-7.3.3 WP MTN 97028 Class Solids 01/09/2023 08.47 01/09/2023 11:31 2540G-2011 WP MTN 97028 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 SW-7.3.4 WP MTN 97028 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 9045D WP MTN 97028 Class Solids 01/09/2023 08:47 01/09/2023 11:31 ASTM D93-80 WP MTN WP MTN - Memphis, TN: WaypointAnalytical - TN, Memphis, TN Page 3 of 8 Waypoint(D ANALYTICAL_ Client: Town of Mooresville/RR WWTP Project: Class A TCLP Lab Report Number: 23-009-0005 Date: 1123/2023 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE Flashpoint Method ASTM D93-80 QC Batch No: L659394 The sample analysis was performed using a modified version of the reference method. Due to the sample matrix, the continual stirring required by the method had to be omitted. Separatory Funnel Extraction 8270 Method 3510C Sample 97027 (Class A) QC Batch No: L6597281L659728 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Sernivolatile Organic Compounds - GUMS (TCLP) Method 8270D Sample 97027 (Class A) QC Batch No: L6598951L659728 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Page 4 of 8 • • Waypoint 449 Springbraak Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A TCLP Whitney Munroe Report Date : 01/Z4/2023 369 Johnson Dairy Rd. Information : Received : 01/09/2023 Mooreseville , NC 28115 60104 Report Number : 23-009-0005 REPORT OFANALYSZ5 Terri W Cole Laboratory Project Manager Lab No: 97027 Matrix: Sludge Sample ID : Class A Sampled: 1/9/2023 8:47 Test Results Units MQL DF Date 1 Time By Analytical Analyzed Method TCLP SVOC Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 Analytical Method: 8270C Prep Batch(es): L659728 01/20/23 14:30 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP 3&4 Methylphenol <0.200 mg/L 0.200 2 01/21/23 01:03 VBW L659895 TCLP 2,4-Dinitrotoluene <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP Hexachlorobenzene <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP Hexachlorobutadiene <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP Hexachloroethane <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP Nitrobenzene <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP Pentachlorophenol <0.200 mg/L 0.200 2 01/21/23 01:03 VBW L659895 TCLP Pyridine <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP 2,4,5-Trichlorophenol <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 TCLP 2,4,6-TOchlorophenol <0.100 mg/L 0.100 2 01/21/23 01:03 VBW L659895 Surrogate: TCLP 2,4,6-Tribromophenol 44.2 Limits: 42-102% 2 01/21/23 01:03 VBW L659895 Surrogate: TCLP 2-Fluorobiphenyl 46.3 Limits: 24-86% 2 01/21/23 01:03 VBW L659895 Surrogate: TCLP 2-Fluorophenol 15.2 Limits: 13-37% 2 01/21/23 01:03 VBW L659895 Surrogate: TCLP 4-Terphenyl-d14 47.2 Limits: 30-122% 2 01/21/23 01:03 VBW L659895 Surrogate: TCLP Nitrobenzene-d5 47.8 Limits: 25-78% 2 01/21/23 01:03 VBW L659895 Surrogate: TCLP Phenol-6 9.60 Limits: 9-27% 2 01/21/23 01.03 VBW L659895 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 5 of 8 0 Waypoint, 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL. www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A TCLP Whitney Munroe Report Date : 01/24/2023 369 Johnson Dairy Rd. Information : Received : 01/09/2023 Mooreseville, NC 28115 V Report Number : 23-009-0005 REPORT OFANALYSIS Terri W Cole Laboratory Project Manager Lab No : 97028 Matrix: Solids Sample ID : Class Sampled: 1/9/2023 8:47 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sulfide (Reactivity) <25.0 mg/Kg 25.0 1 01/23/23 10:30 FMM SW-7.3.4 Moisture 3.68 1 01/12/2315:43 AMB SW-DRYW7' Cyanide, Reactive <0.125 mg/Kg 0.125 1 01/23/23 10:30 FMM SW-7.3.3 Ignitability >96 degrees C 1 01/18/23 08:40 OR ASTM D93-80 pH 6.4 H s.u. 1 01/23/23 14:00 SAR 9045D Total Solids 45.9 H % 0.010 1 01/17/23 16:06 FMM 2540G-2011 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 6 of 8 Waypoint.0 ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704:529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: O1205 Customer Name: Town of Mooresville/RR WWTP Report Number: 23-009-0005 Shipping Method 0 Fed Ex 0 US Postal Lab 0 Other: 0 UPS 0 Client 0 Courier Thermometer ID: IIRT15 1.2C Shipping container/cooler uncompromised? * Yes 0 No Number of coolers/boxes received F 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? Yes 0 No COO agrees with sample label(s)? Yes 0 No COC properly completed Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? # Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Yes 0 No Samples were considered acceptable as cooling process had begun. Water - Sample containers properly preserved # Yes 0 No 0 NIA Water - VOA vials free of heads pace 0 Yes 0 No # N/A Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No NIA F- High concentration container (48 hr) F Low concentration EnCore samplers (48 hr) (— High concentration pre -weighed (methanol -14 d) F- Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes (0) No Comments: Signature: Angela Norvell Date & Time: 0110912D23 12:25:15 Page 7 of 8 z ri mCA m L L v, z mn 01 L D N .cmn L LL c� u Li L z n n f!! ' L: L ♦: 0 w a V m h mm ym n� O z C Mb O { = o oeFM c1mn3 "' a m v m o vm c o>ro m m = m W �0In D m 3 aIr 0 r'o m m p X. m a = � o 0 any. CL o m CL Z. � wit 0, Z 3'C H y N m ro as D w�Z �13 r0 .orr� All CA- z 0 6" � N O m � V V1 C y fC C ? -0 m� a m N d m 7 mm O N 3 mmc N � m Zam C W m W S y n G p a. o c m p m T rr z m n m w' O om�m 'on CLf�7 7 !? z m m z am, O o �a m 23Q z� M Lf° RI �.�+ W 'xzn�pa y'p N .. D W aW i 0 a p w n W fb Z n O no4; v .}. �ry�- m . w 6 -d m i7t ryL1aro O m S►. -0 m 0 p C bl m � zm�OA�p �.9 a d t E)� z ci °. CIO vneaiID own �'o 7 c En 3 b �n w +ez iw� = BMW v 4Q� • j} � � � 01 mAdC� A..rAo m m In Cq�y' 3 -0 m O m CD ` r - z 0 0 co A z 3 EF . s C w m o z a cn p a �zma� a_Q<. a m z m m rp^ 5 �. co is a dwco N CON m O Z •9 Z js (R N D ro �7 n.7 C • A Cp J7� r] G x m i �IS lm Ip Gro n�E I n # c> Page 8 of 8 (D WayP0.1. nt.V ANALYTICAL 2/14/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Revised Lab Report Number: 23-009-0011 Client Project Description: Class A Dear Whitney Munroe: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/9/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 20 Waypoint(D ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2023 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lair ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016123-009-0011 Page 2 of 20 • • 449 Springbtooic Rd, Charlotte, NC 2$217 WaypointMain 704.529.6364 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 23-009-0011 Client Project Description: Class A Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 97038 Class Sludge 01/09/2023 08:27 01/09/2023 11:31 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 7470A WP MTN 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 8270C WP MTN 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 SW-1311 WP MTN 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 6010D WP MTN 97038 Class Sludge 01/09/2023 08:27 01/09/2023 11:31 8151A WP MTN 97038 Class A Sludge 01/09/2023 08:27 01/09/2023 11:31 8081E WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 350.1 AES 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 9045D WP MTN 97039 Class Solids 01/09/2023 08:47 01/09/2023 11:31 7471A WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 6010D WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 4500NORGD-2011 WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 SW-DRYWT WP MTN 97039 Class A Solids 01/09/2023 08:47 01/09/2023 11:31 254OG-2011 WP MTN 97079 Class A SAR Solids 01/09/2023 08:47 01/09/2023 11:31 SW-DRYWT WP MTN 97079 Class A SAR Solids 01/09/2023 08:47 01/09/2023 11:31 Saturate Paste WP MTN AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 20 Waypointo ANALYTICAL anent: [Own of Mooresville/RR W►NTP Project: Class A Lab Report Number: 23-009-0011 Date: 2114/2023 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE This is a revised report and supersedes the original laboratory report dated 2/3123. Calcium, magnesium, and sodium have been added to the metals list (mg/Kg). Report Comments Ammonia was subcontracted to Analytical Environmental Services. Block Digestion and 1=IA Method 4500MORGD-2011 QC Batch No: L658309 Matrix spike recovery is outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Separatory Funnel Extraction 8081 Method 3510C Sample 97038 (Class A) QC Batch No: 1-659760/1-659760 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction 8270 Method 3510C Sample 97038 (Class A) QC Batch No: 1-659728/1-659728 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis Method 60100 Sample 97039 (Class A) Analyte: Aluminum QC Batch No: 1-658928/1-658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Calcium QC Batch No: L6589281L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Copper QC Batch No: L658650/L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Potassium QC Batch No: 1-658928/1-658311 Page 4 of 20 Waypoint.(D ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Potassium QC Batch No: L659032/L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Magnesium QC Batch No: L658650/L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97039 (Class A) Analyte: Phosphorus QC Batch No: L658928/L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. ,No matrix interference is suspected. Sample 97039 (Class A) Analyte: Zinc QC Batch No: L658650/L658311 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D Sample 97038 (Class A) QC Batch No: L659895/L659728 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. SAR = [ Na ] / SQRT { ([Ca] + [Mg] )/2} SAR=[7.59]/SQRT{([14.4]+[11.0])12} SAR=[7.59]/SQRT{([25.4])12} SAR=[7.59] /SQRT{ 12.7} SAR = 2.13 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (53100-3120) + 0.5 * (3120) + (10) PAN = 16559 Page 5 of 20 Waypoint,(D ANALYTICAL 01205 Town of Mooresville/RR WVV7P Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalyti ca I.coin Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 Report Number :23-009-0011 REPORT OFANAL Y$ZS Lab No : 97038 Matrix: Sludge Sample ID : ClassA Sampled: 1/9/2023 8:27 Test Results Units MQL DF Date / Time By Analytical Analyzed Method TCLP Herbicide Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP Metals Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP Pesticide Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP SVOC Extraction Leachate 1 01/12/23 14:00 PHE SW-1311 TCLP VOC ZHE Extraction Leachate 1 01/12/23 12:00 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Satch(es): L658666 01/16/23 11:20 Prep Method: 3015A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 01/16/23 17:41 TJS L658925 TCLP Barium <0.250 mg/L 0.250 1 01/16/23 17:41 TJS L658925 TCLP Cadmium <0.0500 mg/L 0.0500 1 01/16/23 17:41 TJS L658925 TCLP Chromium <0.100 mg/L 0.100 1 01/16/23 17:41 TJS L658925 TCLP Lead <0.100 mg/L 0.100 1 01/16/23 17:41 TJS L658925 TCLP Selenium <0.500 mg/L 0.500 1 01/16/23 17.41 TJS L658925 TCLP Silver <0.0500 mg/L 0.0500 1 01/16/23 17:41 TJS L658925 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit H Beyond holding time Page 6 of 20 Waypoint(D ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseviile , NC 28115 Report Number :23-009-0011 Lab No : 97038 Sample ID : Class A Analytical Method: 7470A Prep Method: 7470A Test TCLP Mercury Analytical Method: 8081B Prep Method: 3510C Test TCLP Endrin TCLP gamma-BHC TCLP Methoxychlor TCLP Toxaphene TCLP Chlordane TCLP Heptachlor Epoxide TCLP Heptachlor Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Analytical Method: 8151A Prep Method: 8151A Test Results 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lytica I.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 REPORT OFANALYSIS Matrix: Sludge Sampled: 1/9/2023 8:27 Prep Batch(es): L660377 01/25/23 10:56 Units MQL DF Date / Time By Analytical Analyzed Batch <0.0200 mg/L 0.0200 1 01/25/23 15:44 JTR L660548 Prep Batch(es): L659760 01/20/23 16:20 Results Units MQL DF Date / Time By Analytical Analyzed Batch <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 <0.03000 mg/L 0.03000 10 01/20/23 23:34 NFP L659894 <0.02000 mg/L 0.02000 10 01/20/23 23:34 NFP L659894 <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 . <0.004000 mg/L 0.004000 10 01/20/23 23:34 NFP L659894 75.83 Limits: 36-116% 10 01/20/23 23:34 NFP L659894 58.50 Limits: 25-123% 10 01/20/23 23:34 NFP L659894 Prep Batch(es): L659539 01/19/23 17:20 Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 01/20/23 20:26 NFP L659908 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0,0020 1 01/20/23 20:26 NFP L659908 Surrogate: DCAA 58.40 Limits: 20-120% 1 01/20/23 20:26 NFP L659908 Qualifiers/ OF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 7 of 20 (D Waypoint, ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number : 23-009-0011 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana"cal.com REPORT OFANALYSIS Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 Lab No: 97038 Matrix: Sludge Sample ID : Class A Sampled: 1/9/2023 8:27 Analytical Method: 8260D Prep Batch(es): V29271 01/27/23 09:00 Prep Method: 5030E Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 01/27/23 17:14 MSA V29272 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Chloroform <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP 1,1-Dichloroethene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Methyl Ethyl Ketone (MEK) 0.209 mg/L 0.0500 10 01/27/23 17:14 MSA V29272 TCLP Tetrachloroethene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 01/27/23 17:14 MSA V29272 Surrogate:4-Bromofluorobenzene 105 Limits:80-124% 10 01/27/23 17:14 MSA V29272 Surrogate: Dibromofluoromethane 102 Limits: 75-129% 10 01/27/23 17:14 MSA V29272 Surrogate: Toluene -dB 110 Limits: 77-123% 10 01/27/23 17:14 MSA V29272 Analytical Method: 8270C Prep Batch(es): L659728 01/20/23 14:30 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP 3&4 Methyiphenol <0.200 mg/L 0.200 2 01/21/23 02:09 VBW L659895 TCLP 2,4-Dinitrotoluene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP Hexachlorobenzene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 8 of 20 Waypoint.0 ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number :23-009-0011 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalocal.com REPORT OPANALYSIS Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 Lab No : 97038 Matrix: Sludge Sample ID : Class Sampled: 1/9/2023 8:27 Analytical Method: 8270C Prep Batch(es): L659728 01/20/23 14:30 Prep Method: 3510C Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP Hexachlorobutadiene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP HexachlDroethane <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP Nitrobenzene <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP Pentachloropheno[ <0.200 mg/L 0.200 2 01/21/23 02:09 VBW L659895 TCLP Pyridine <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP 2,4,5-Trichlorophenol <0.100 mg/L 0.100 2 01/21/23 02:09 VBW L659895 TCLP 2,4,6-Trichlorophenol <0.100 mg/L 0.100 2 01/21/23 02.09 VBW L659895 Surrogate: TCLP 2,4,6-Tribromophenol 50.1 Limits: 42-102% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP 2-Fluorobiphenyl 43.7 Limits: 24-86% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP 2-Fluoropheno[ 16.7 Limits: 13-37% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP 4-Terphenyl-d14 57.2 Limits: 30-122% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP Nitrobenzene-d5 43.9 Limits: 25-78% 2 01/21/23 02:09 VBW L659895 Surrogate: TCLP Phenol-416 11.0 Limits: 9-27% 2 01/21/23 02:09 VBW L659895 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Page 9 of 20 Waypoint(D ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information : Mooreseville, NC 28115 Report Number :23-009-0011 Lab No : 97039 Sample ID : Class 449 Springbrook Rd, Charlotte, MC 28217 Main 704.529.6364 www.waypointanalytical.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 REPORT OPANRLYSIS Matrix: Solids Sampled: 1/9/2023 8:47 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Fecal Coliform MPN/g <2.5 MPN/g - dry 2.5 1 01/09/23 12:03 SMW 9221E-2011 Moisture 20.9 % 1 0111712316:06 FMM SW-DRYWT Ammonia Nitrogen 3120 mg/Kg AR 1 350.1 PH 6.5 H S.U. 1 01/23/23 14:00 SAR 9045D Total Solids 7%1 H % 0.010 1 01/17/23 16:06 FMM 2540G-2011 Total Kjeldahl Nitrogen 53100 mg/Kg - dry 1260 20 01/16/23 11.53 ANH 4500NORGD-2011 Phosphorus 16900 mg/Kg - dry 31.6 5 01/16/23 20:15 TJS 6010D Aluminum 15000 mg/Kg - dry 31.6 5 01/16/23 20:15 TJS 6010D Arsenic 3.59 mg/Kg - dry 0.632 1 01/14/23 03:08 TJS 60101) Cadmium 0.582 mg/Kg - dry 0.126 1 01/14/23 03:08 TJS 6010D Calcium 13100 mg/Kg - dry 316 5 01/16/23 20:15 TJS 6010D Copper 176 mg/Kg - dry 0.632 1 01/14/23 03:08 TJS 6010D Lead 8.77 mg/Kg - dry 0.379 1 01/14/23 03:08 TJS 60101) Magnesium 2530 mg/Kg - dry 6.32 1 01/14/23 03:08 TJS 6010D Mercury (Total) <0.196 mg/Kg - dry 0,196 1 01/19/23 16:12 JTR 7471A Molybdenum 12.8 mg/Kg - dry 0.316 1 01/14/23 03:08 TJS 6010D Nickel 10.2 mg/Kg - dry 0.316 1 01/14/23 03:08 TJS 6010D Potassium 2970 mg/Kg - dry 63.2 5 01/17/23 14:04 TJS 6010D Selenium 2.81 mg/Kg - dry 0.632 1 01/14/23 03:08 TJS 6010D Sodium 795 mg/Kg - dry 31.6 1 01/14/23 03:08 TJS 6010D Zinc 370 mg/Kg - dry 1.58 1 01/14/23 03:08 TJS 6010D Qualifiers/ DF Definitions Dilution Factor H Beyond holding time MQL Method Quantitation Limit Page 10 of 20 Waypoint,(2) ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number . 23-009-0011 Lab No : 97079 Sample ID : Class SAR 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalyUcal.com Original Report Date : 02/03/2023 Revised Report Date: 02/14/2023 Received : 01/09/2023 REPORT OFANALYSM Matrix: Solids Sampled: 1/9/2023 8:47 Test Results Units MQL DF Date I Time By Analytical Analyzed Method Calcium (saturated paste) 14.4 meq/L 0.005 1 01/17/23 14:16 SWL Saturate Paste Magnesium (saturated paste) 11.0 meq/L 0.008 1 01/17/23 14:16 SWL Saturate Paste Sodium (saturated paste) 7.59 meq/L 0.004 1 01/17/23 14:16 SWL Saturate Paste Sodium Absorption Ratio 2.13 1 01/17/23 14:16 SWL Saturate Paste Moisture 3.51 1 01/23/2316:46 FMM SW-DRYWF Qualifiers/ DF Dilution Factor H Beyond holding time Definitions Page 11 of 20 ACCESS ANAL n CAL, INC. ANALYTICAL REPORT CLIENT Waypoint Analytical, LLC (Charlotte) 449 Springbrook Road Charlotte NC 28217 ATTENTION Terri W Cole PROJECT ID 23-009-0011 LABORATORY REPORT NUMBER 2301B68 DATE January 17, 2023 Primary Data Review By Secondary Data Review By Ashley Amick Chris Pafford Project Manager, Access Analytical Project Manager, AES aamick@axs-inc.com PLEASE NOTE: - Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. - AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-E87582, NELAP certified laboratory # E87582 - AHIA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. - Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SCNCIGA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 12 of 20 Page 1 of 6 . . � % $ \ f (D o ; (L O / k JLn N . a m�/o ƒ k/k'r � � v 0 sl 2 t. em _gym 7 � JE am /- # E _ C', V E 2 t k g R Q § , $ A u 3 m «tMZn � ° k CL . M \ Ln \ g # 7 3 / { . � \ S \ � � . R �•� � � 7 e U 0 0 : i m" - _§ k � � / k ¢ / \ 2 k f 2 k t k 9 § _7 $ n a � o $ 2 2 3 n\ e 2 , / ` §AM k CO k M $CL■ \ 2 \ o 2/ 7/ 7 Or R Analytical Environmental Services, Inc Date: 17-7an-23 Client: Waypoint Analytical, LLC (Charlotte) Client Sample ID: 97039 Lab Order 23011368 Tag Number: Class A Project Name. 23-009-0011 Collection Date: 1/9/2023 8:47:00 AM Lab ID: 2301B68-001A Matrix: Solid Analyses Reporting Y Result Qua MDL Limit Units BatchlD DF Date Analyzed Analyst Nitrogen, Ammonia (as iv) Extractable E350.1 MOD (E350.1) Nitrogen, Ammonia (As N) Extractable 3120 104 212 tnglKg-dry 349327 20 01/17/2023 11:23 TL PERCENT MOISTURE D2216 Percent Moisture 8.35 0 0 wto/o R506077 1 01/13/2023 00:00 .1'W Qualifiers: ' Value exceeds maximum contaminant level BRL Not Detected at NIDL H Holding times for preparation or analysis exceeded N Analyte not NELAC certified B Amlyte detected in the associated method blank E Estimated value above quantitation range S Spike Recovery outside limits due to matrix > Greater than Result value d Estimated value detected below Repotting Limit Less than Result value Page 14 of 20 Page 3 of 6 C 2 c 2 d 7 fV 0 0 d ` a a m H 71 Q1 U 0 0 Ld 0 V o u C � p 3 R C y N aL 7 .y U U ,y U N v v 7 a L L @ C m C m `m v fl o n a E@ c w v d ~ v w F' � c Q/ v E `v `v E E v a 0 N 00 F U 0 u u r-I erf T-I r-I � ri 2 U i Yh "a ] J ❑u ❑ u u u 0 a)0 o n v •CQ L N d N 0 0 C C ❑❑ V .0 U 30 o d = U Q N v y p 0 R E E v ate+ 3* 0 ® :. •; o o _Dccc i��. cM o p o M1• � d } � C R M1• N �_-I 13 ry M1 v u v m m M1. (.. U U rL 'oy i M1. v M1• u 0 u M1• ea a d c u @ O V y p y Q .�+ 0 V c d t C C y O }' C U1 d m y E 0 u C p w'C+ o L 0 y , C1 U aV. C Q at+ CL 3 h R N C w C 41 C 0 a) C CGNl C 7 N u u 7l N O Q = y 17 V1 Ol h g. p 0 V ` Y c ? m E t y o E M w h y a o a N w ac E a 0 N p 6 v^ S U U O Q 7 0 0 z Y ID I v � C ca V V � Q y C p N m sy J bl N N d c 0 a V u N o a w aEi c z O �+ E c a a a r m di � a C E Y L N 2 N �G E 4 y cpi •C m a L > C @ V U 7 U ci N N N N N N N N co N N 0 C M O M N N C O O 0 I ro 0 0 a (71 06 (71 O O O 6 a � O N M �O VOA H ra N W zz � c a' v� Q � O O N n O O 4"' w N pC� G C� .0 A �1 o � o iPC xr do n +- a_ a on rn A pa U C � � e ao w o0 o6 o6 b cls v F� N v Y Ln Fi m z Q � A � � W Q W z � � z d � v A w Q e3 U] N r7. � co O 0) a E 6 N � v w 22 U � U W T _ z P4 a Y a, a X J W q Q v°i v ¢l Z End of Report Page 17 of 20 Page 6 of 6 ANALYTICAL Waypoint.0 449 Springbrook Rd, Charlotte, NC 29217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 23-009.0011 Shipping Method 0 Fed Ex 0 US Postal # Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer 1D: IRT15 3.3C Shipping container/cooler uncompromised? # Yes 0 No Number of coolers/boxes received I ' Custody seals intact on shipping container/cooler? 0 Yes 0 No # Not Present Custody seals intact on sample bottles? 0 Yes 0 No # Not Present Chain of Custody (COC) present? (0) Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COG properly completed * Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? # Yes O No Sufficient sample volume for indicated test(s)? * Yes 0 No All samples received within holding time? # Yes 0 No Cooler temperature in compliance? # Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. # Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes 0 No # N/A Trip Blanks received with VOAs 0 Yes 0 No 0 N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No # NIA F_ Nigh concentration container (48 hr) 7 Nigh concentration pre -weighed (methanol -14 d) F Low concentration EnCore samplers (48 hr) F_ Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes # No Comments: Signature:[Angel) Norvell Date & Time: 01/09/2023 14:18:50 Page 18 of 20 L: L z n _n Oz z � L U M z m 0 0 L: O O 0 m _ c? L C 1i � c cr n n v� m - n: L r! z IE L m �a aLJL C7 z m 0 a L n E L' z O L �o N y 0 y L:'. Ci mn, N L m �y 0 ALL 40 a 0 C L 03 8 0 0 m G) q r L i L"J C w 9 c n N m �c oc 0 .n. 5 a mom a c � 3 m M mm 3] .Z 0 wp MR. -0e m m v z30 c - m 1 y�r�t m n EDNA m o�a� mo x R m m ER �m > m z 0 R z z M y A Fd m D A x CA v z 0 en(Amm w w O w x C m c m 7 E mzan p a W m ; m m m m 0 Qm vv m � m zm G L"" G nm i 3 C Q Oyc to; c 3 Z pe 0 c W m"��� p Z N O ^���,,,���,,, �p M v.o 1 �dN a � r A° o_ n w @ �"rc� o ❑ m a x d K 00(c _ N ra m (D m y LJ a 2 m m W 'AXt p d<o aM�0. c 0N� M a❑ L 9" " s O aK O CD R � CI m CL 7 p m 0 o a n O AM .�i 3 = D N II° 3 I� I r Z Gf IQ m N 0 z z m r p�ro.�rn.ro a cs ' s c ID 0- y �s7.w o rL 0 m O 3 d y n C., m0 a y 10 C ZD G 9 y z �l -. y c C U)m o e C c F� Up (13 P r i- to X C m N O ocn�ov�cn 4 ❑ w A R fa Z rmi D . CD {nEi c) aa�yzm.o� � C 1 Z 3M m mwG)(n �y a 0 n J 0 fn m a n Page 19 of 20 -L! L z 0 a L z m M L L o z m 0 O L n 0 m rn w---- Q L a z n n L 4 N 1 0 n n 2 L L z 0 m n Q G 0 L !A N 7 0 T Li Z A r-• 9 sw n i O s p ' V• � a A e o �r �i I q f 0 S w D V r- m � o ym n 0 z m v *30 0�m ,J wta m x d ,... ow 0=0 I CI- E ^ C N 07 yom s n m pm D ,v m c , m mao.� m RI, m m � m m Q mw N n = 0 mm rn 01 z q 0 O o mayor m z 1 K m rn p N m a m N N yz_� Z `C Q1 9 �VJ z ZN L m MM nxs�m L � rn 0 v�CL H '0 L 3 a a' (D rAl D � m u x w a z 0 D { w m 0 C o°..' m rn m S m o n o o r �. a. 0 o O z b y) r z z z a a 1 I 1_ z GI 0 m d Z z m r = 0 Q raoo CL yro z � a 9 S m W� a cr o A� • r0 a M 4r rCrimp �z git Ca a� • � J r, x N 'C AN C O O G o A x a 0 m C cm 2 o � 4 a can. eo v M r rt C m y O 50 X MC70 •D;u F-oro °2o0 wn ��maa'Pa" m Onln�,z a ° g ? ,M r � 0 CSC m , Q W �> rn m 9Wn m w N a I\ w �tAA 'r Page 20 of 20 Waypoeint ANALYTICAL 2/3/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseviile, IBC, 28115 Ref: Analytical Testing Lab Report Number: 23-026-0009 Client Project Description: Class A Dear Whitney Munroe: 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 1/26/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, (OAVL�) W '0- — A:P CEUl- Terri W Cole Laboratory Project Manager ,Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 6 Waypoint, ANALYTICAL 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytica I.com Certification Summary Laboratory ID: VI/P CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12131 /2023 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Page t of 1 00016123-026-0009 Page 2 of 6 s Waypoint, ANALYTICAL Report Number: 23-026-0009 Client Project Description: Class A Lab No Client Sample ID 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529:6364 www.waypiaintana"cal.com Sample Summary Table Matrix Date Collected Date Received 98388 Class A Solids 01/26/2023 08:15 01/26/2023 11:21 Page 3 of 6 Waypoint(2) ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number : 23-026-0009 Lab No : 98388 Sample ID : Class A 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana lytical.corn REPORT OFANALYSIS Report Date : 02/03/2023 Received : 01/26/2023 .0 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 1/26/2023 8:15 Test Results Units MQI_ DF Date / Time By Analytical Analyzed Method Moisture 4.27 % Nitrate+Nitrite-N <10.4 mg/Kg - dry Qualifiers/ DF Dilution Factor Definitions 1 01/26/2317:35 AMB SW-DRYWT 10.4 10 01/27/23 17:42 9056A MQL Method Quantitation Limit Page 4 of 6 Waypoint..(D ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number:01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 23-026-0009 Shipping Method 0 Fed Ex 0 US Postal * Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IIRT153.5C Shipping container/cooler uncompromised? * Yes 0 No Numberof coolers/boxes received Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? 0 Yes 0 No COC agrees with sample label(s)? 0 Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? Yes 0 No . Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No NIA Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No N/A F_ High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr) F_ High concentration pre -weighed (methanol -14 d) F_. Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes (* No Comments: Signature: ngelo Norveli Date &Time: 01/26/2023 12:01:01 Page 5 of 6 5PGGG n n u 7 76 m al n cLLCc m Z x w 0* a L m A 7 m L L t- a za d 00 T L i= wr N 0 CLa a 0 M ip m L co m A 0 X G) r Q a m 0 s 3 vc mcr S' o m C/3 m m FL ar am -o z md.=° to w n b V r m �y mm y A .Z,E z 0 z 0 �q mi Am m a �mo� r SE mM x 0 m m Mm z O LA m -'l C', 'o b m c w � 01 M A a@ @ m m mmQ N m m A d Om , m o m m' z Z L L O AT fn am � W Z q ID M 7 0 S0 rn z o CD m ^' ro 0 O w us L7. :0 wLi G C fC tma m .x 1-n c m a p X Q cis ED r=N L COD a CN ND�. N �� p_o L, Q \3 Of � N c m m m D `a z a z x A m 0 - 0 0 ID m o 0 a o y ^ Z +�D � IV 0 .. � c m�Z � ivs. s s msn�/ 4 (' 0 �. "Z n A r • 1 7m0 70 � m w m C7- lmfi < :E -v Z .Z m cn - ;aD OaQ- m;--1 O O > B caa E � � Q a a m �. 2 fa7 � a m TT� J III III ���IIII➢ Page 6 of 6 (D Way point ANALYTICAL 4/20/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 23-093-0009 Client Project Description: Class A Dear Whitney Munroe: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointa nalyticat-corn Waypoint Analytical, LLC (Charlotte) received sample(s) on 4/3/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 20 s ANALYTICAL Waypoint 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program Lab ID Expiration Date North Carolina State Program 37735 07/31/2023 North Carolina State Program 402 12/31/2023 South Carolina State Program 99012 07/31/2023 South Carolina State Program 99012 12/31/2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/29/2024 Arkansas State Program 88-0650 02/07/2024 California Skate Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 11/14/2025 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2023 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 11/14/2025 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2024 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2023 Page 1 of 1 00016/23-093-0009 Page 2 of 20 Waypoin(bt�. ANALYTICAL Report Number: 23-093-0009 Client Project Description: Class A 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Sample Summary Table Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 92759 Class A Sludge 04/03/2023 08:30 04/03/2023 11:53 92759 (lass A Sludge 04/03/2023 08:30 04/03/2023 11:53 SW-1311 WP MTN 92759 Class A Sludge 04/03/2023 08:30 04/03/2023 11:53 80818 WP MTN 92759 Class A Sludge 04/03/2023 08:30 04/03/2023 11:53 8151A WP MTN 92759 Class A Sludge 04/03/2023 08:30 04/03/2023 11:53 8270C WP MTN 92759 Class A Sludge 04/03/2023 08:30 04/03/2023 11:53 6010D WP MTN 92759 C1assA Sludge 04/03/2023 08:30 04/03/2023 11:53 7470A WP MTN 92760 Class A Solids 04/03/2023 08:30 04/03/2023 11:53 92760 Class A Solids 04/03/2023 08:30 04/03/2023 11:53 350.1 AES 92760 Class A Solids 04/03/2023 08:30 04/03/2023 11:53 7471A WP MTN 92760 Class A Solids 04/03/2023 08:30 04/03/2023 11:53 6010D WP MTN 92760 Class A Solids 04/03/2023 08:30 04/03/2023 11:53 4500NORGD-2011 WP MTN 92787 Class A Solids 04/03/2023 08:30 04/03/2023 11:53 92787 Class A Solids 04/03/2023 08:30 04/03/2023 11:53 Saturate Paste WP MTN AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 20 Waypoint(D ANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A Lab Report Number. 23-093-0009 Date: 4/18/2023 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanilytical.com Ammonia subcontracted to Analytical Environmental Services. CASE NARRATIVE Fecal Coliform MPN Method 9221E-2011 QC Batch No: V31576 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Separatory Funnel Extraction 8081 Method 3510C Sample 92759 (Class A) QC Batch No: 1-675547/1-675547 The weightivolume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction 8270 Method 3510C Sample 92759 (Class A) QC Batch No: 1-675406/1-675406 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis Method 6010D Sample 93829 Analyte: Aluminum QC Batch No: 1-675666/1-674801 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 93829 Analyte: Potassium QC Batch No: 1-675666/1-674801 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Solids Total Mercury Analysis - CVAA Method 7471A Sample 95708 (SB-6) Analyte: Mercury QC Batch No: L676255/1-676023 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270D Sample 92759 (Class A) QC Batch No: 1-675553/1-675406 Surrogate recovery(s) was flagged as outside QC limits due to high levels of target and/or non -target analytes. Batch QC samples (method blank and laboratory control samples) all showed surrogates within QC limits. Page 4 of 20 Waypoint(D ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com SAR =[Na]/SQRT{([Ca]+[Mg] )12} Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. SAR =[2.69 ]!SQRT{( [2.89]+[3.49] )12} SAR = [ 2.69 j I SQRT { ( [6.38] )12 } SAR =[2.69]/SQRT {3.19} SAR =1.51 PAN Equation = 0.3 * (TKN --Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (67800-3760) + 0.5 * (3760) + 10 PAN = 21087 Page 5 of 20 Waypoeinto ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 449 5pringbrook Rd, Charlotte, NC 28217 Main 704:529.6364 www.waypointanalytical.com Report Number :23-093-0009 REPORT OFA/VALYSIS Lab No : 92759 Sample ID . Class Report Date : 04/20/2023 Received : 04/03/2023 Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 4/3/2023 8:30 Test Results Units MQL DF Date / Time Analyzed By Analytical Method TCLP Herbicide Extraction Leachate 1 04/10/23 13.00 ALM SW-1311 TCLP Metals Extraction Leachate 1 04/10/23 13:00 ALM SW-1311 TCLP Pesticide Extraction Leachate 1 04/10/23 13:00 ALM SW-1311 TCLP SVOC Extraction Leachate 1 04/10/23 13:00 ALM SW-1311 TCLP VOC ZHE Extraction Leachate 1 04/04/23 13:00 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L675452 04/11/23 13:52 Prep Method: 3015A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 04/11/23 18:43 JTR L675662 TCLP Barium <0.250 mg/L 0.250 1 04/11/23 18:43 JTR L675662 TCLP Cadmium <0.0500 mg/L 0.0500 1 04/11/23 18:43 JTR L675662 TCLP Chromium <0.100 mg/L 0.100 1 04/11/23 18:43 JTR L675662 TCLP Lead <0.100 mg/L 0.100 1 (14111123 18:43 JTR L675662 TCLP Selenium <0.500 mg/L 0.500 1 04/12/23 16:25 TJS L675662 TCLP Silver <0.0500 mg/L 0.0500 1 04/11/23 18:43 JTR L675662 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 6 of 20 Waypoin tu 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WVVTP Project Class A Whitney Munroe Report Date : 04/20/2023 369 Johnson Dairy Rd. Information : Received : 04/03/2023 Mooreseviile, NC 28115 �ML04 Report Number :23-093-0009 REPORTflFANALYSIS Terri W ColeLaboratory Project Manager Lab No : 92759 Matrix: Sludge Sample ID : Class A Sampled: 4/3/2023 8:30 Analytical Method: 7470A Prep Batch(es): L675539 04/12/23 07:55 Prep Method: 7470A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Mercury <0.0200 mg/L 0.0200 1 04/12/23 13:27 FDS L675724 Analytical Method: 8081E Prep Batch(es): L675547 04/11/23 17:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Endrin <0.004000 mg/L 0.004000 10 04/13/23 08:12 VIC L675962 TCLP gamma-BHC <0.004000 mg/L 0.004000 10 04/13/23 08.12 VIC L675962 TCLP Methoxychlor <0.004000 mg/L 0.004000 10 04/13/23 08:12 VIC L675962 TCLP Toxaphene <0.03000 mg/L 0.03000 10 04/13/23 08:12 VIC L675962 TCLP Chlordane <0.02000 mg/L 0.02000 10 04/13/23 08:12 VIC L675962 TCLP Heptachlor Epoxide <0.004000 mg/L 0.004000 10 04/13/23 08:12 VIC L675962 TCLP Heptachlor <0.004000 mg/L 0,004000 10 04/13/23 08:12 VIC L675962 Surrogate: Decachlorobiphenyl 65.90 Limits: 36-116% 10 04/13/23 08:12 L675962 Surrogate: Tetrachloro-m-xylerie 48.55 Limits: 25-123% 10 04/13/23 08:12 L675962 Analytical Method: 8151A Prep Batch(es): L675557 04/11/23 19:00 Prep Method: 8151A Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 04/13/23 22:13 VIC L676257 TCLP 2,4,5TP(Si [vex) <0.0020 mg/L 0.0020 1 04/13/23 22:13 VIC L676257 Surrogate: DCAA 70.80 Limits: 20-120% 1 04/13/23 22:13 L676257 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 7 of 20 Waypoin(l)tx. ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number : 23-093-0009 449 Springbrook Rd, Charlotte, NC 28217 Main 704S29.6364 www.waypointana"cal.com REPORT OFANALY"S Report Date : 04/20/2023 Received : 04/03/2023 60 W4 Terri W Cale Laboratory Project Manager Lab No: 92759 Matrix: Sludge Sample ID : ClassA Sampled: 4/3/2023 8:30 Analytical Method: 8260D Prep Batch(es): V31878 04/10/23 14:00 Prep Method: 5030B Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 04/11/23 12:04 MSA V31879 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 TCLP Chloroform <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 TCLP 1,1-Dichloroethene <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 TCLP Methyl Ethyl Ketone (M6K) <0.0500 mg/L 0.0500 10 04/11/23 12:04 MSA V31879 TCLP Tetrachloroethene <0.0050 mg/L 0.0050 10 04/11/23 12.04 MSA V31879 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 04/11/23 12:04 MSA V31879 Surrogate:4-Bromofluorobenzene 105 Limits: 80-124% 10 04/11/23 12:04 MSA V31879 Surrogate: Dibromofluoromethane 98.4 Limits: 75-129% 10 04/11/23 12:04 MSA V31879 Surrogate: Toluene-d8 96.0 Limits: 77-123% 10 04/11/23 12:04 MSA V31879 Analytical Method: 8270C Prep Batch(es): L675406 04/11/23 11:00 Prep Method: 3510C Test Results Units I4MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 TCLP 3&4 Methylphenol <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 TCLP 2,4-Dinitrotoluene <0.0620 mg/L 0.0620 5 (14111/23 20:30 VBW L675553 TCLP Hexachlorobenzene <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions I..I Beyond holding time MQL Method Quantitation Limit Page 8 of 20 Waypoint ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number : 23-093-0009 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalocal.com REPORT OFANALYSTS Report Date ; 04/20/2023 Received : 04/03/2023 iML04 Terri W Cole Laboratory Project Manager Lab No : 92759 Sample ID : Class Matrix: Sludge Sampled: 4/3/2023 8:30 Analytical Method: 8270C Prep Batch(es): L675406 04/11/23 11:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobutadiene <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 TCLP Hexachloroethane <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 TCLP Nitrobenzene <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 TCLP Pentachlorophenol <0.125 mg/L 0.125 5 04/11/23 20:30 VBW L675553 TCLP Pyridine <0.125 mg/L 0.125 5 04/11/23 20:30 VBW L675553 TCLP 2,4,5-Trichlorophenol <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 TCLP 2,4,6-Trichlorophenol <0.0620 mg/L 0.0620 5 04/11/23 20:30 VBW L675553 Surrogate: TCLP 2,4,6-Tribromaphenol 41.4 * Limits: 42-102% 5 04/11/23 20:30 VBW L675553 Surrogate: TCLP 2-Fluorobiphenyl 40.6 Limits: 24-86% 5 04/11/23 20:30 VBW L675553 Surrogate: TCLP 2-Fiuorophenol 18.1 Limits: 13-37% 5 04/11/23 20:30 VBW L675553 Surrogate: TCLP 4-Terphenyl-d14 41.1 Limits: 30-122% 5 04/11/23 20:30 VBW L675553 Surrogate: TCLP Nitrobenzene-d5 40.5 Limits: 25-78% 5 04/11/23 20:30 VBW L675553 Surrogate: TCLP Phenol-& 12.5 Limits: 9-27% 5 04/11/23 20:30 VBW L675553 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 9 of 20 Waypointo. ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 449 Springbrook Rd, Charlotte, MC. 28217 Main 704.529.6364 www.waypointanalytical.com Report Number : 23-093-0009 REPORT OFANAL YSIS Lab No : 92760 Sample ID : Class Report Date: 04/20/2023 Received : 04/03/2023 60 W4 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 4/3/2023 8:30 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Fecal Coliform MPNJg 2.0 MPN/g - dry 2.0 1 04/03/23 12:17 SMW 9221E-2011 Moisture 1.98 % 1 04/03/2316:45 ALN SW-DRYWT Ammonia Nitrogen 3760 mg/Kg AR 1 350.1 Nitrate+Nitrite-N <10.2 mg/Kg - dry 10.2 10 04/03/23 18:21 9056A pH 6.18 H S.U. 1 04/03/23 15:36 EKF 9045D Total Solids 96.1 % 0.010 1 04/04/23 15:18 PEB 2544G-2011 Total Kjeldahl Nitrogen 69200 mg/Kg - dry 5990 20 04/10/23 14:57 ANH 4500NORGD-2011 Phosphorus 17800 mg/Kg - dry 51.0 10 04/11/23 23:43 JTR 6010D Aluminum 9470 mg/Kg - dry 51.0 10 04/11/23 23:43 JTR 6010D Arsenic 2.44 mg/Kg - dry 0.510 1 04/11/23 03:27 3TR 6010D Cadmium 0.647 mg/Kg - dry 0.102 1 04/11/23 03:27 JTR 6010D Copper 204 mg/Kg - dry 0.510 1 04/11/23 03:27 JTR 6010D Lead 6.88 mg/Kg - dry 0.306 1 04/11/23 03:27 JTR 6010D Mercury (Total) 0.209 mg/Kg - dry 0.165 1 04/14/23 11:45 FDS 7471A Molybdenum 13.3 mg/Kg - dry 0.255 1 04/11/23 03:27 JTR 6010D Nickel 10.5 mg/Kg - dry 0.255 1 04/11/23 03:27 JTR 6010D Potassium 3490 mg/Kg - dry 102 10 04/11/23 23:43 JTR 6010D Selenium 4.66 mg/Kg - dry 0.510 1 04/11/23 03:27 .JTR 6010D Zinc 445 mg/Kg - dry 1.28 1 04/11/23 03:27 JTR 6010D Qualifiers/ * outside QC Limit DF Dilution Factor Definitions H Beyond holding time MQL Method Quantitation Limit Page 10 of 20 0 Waypoint 449 Springbrpok Rd, Charlptte, NC 28217 Main 704.529.6-164 ANALYTICAL www.waypointanatocal.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 04/20/2023 369 Johnson Dairy Rd. Information : Received : 04/03/2023 Mooreseville , NC 28115 Report Number :23-093-0004 REPORTOFA/VALYSI Terri W ColeS Laboratory Project Manager Lab No ; 92787 Matrix: Solids Sample ID : Class Sampled: 4/3/2023 8:30 Test Results Units MOIL DF Date I Time By Analytical Analyzed Method Calcium (saturated paste) 2.89 meq/L 0.005 1 04/17/23 15:49 SWL Saturate Paste Magnesium (saturated paste) 3.49 meq/L 0.008 1 04/17/23 15:49 SWL Saturate Paste Sodium (saturated paste) 2.69 meq/L 0.004 1 04/17/23 15:49 SWL Saturate Paste Sodium Absorption Ratio 1.51 1 04/17/23 15:49 SWL Saturate Paste Moisture 4.00 % 1 04/04/2315:18 PEi3 SW-DRYWT Qualifiers/ * Outside QC Limit Definitions DF Dilution Factor Page 11 of 20 ACCESS ANAMICAL, INC. ANALYTICAL REPORT CLIENT Way -point Analytical, LLC (Charlotte) 449 Springbrook Road Charlotte NC 28217 ATTENTION Terri W Cole PROJECT ID 23-093-0009 LABORATORY REPORT NUMBER 2304486 DATE April 11, 2023 Primary Data Review By Secondary Data Review By Chris Pafford Project Manager, AES PLEASE NOTE: Ashley Amick Project Manager, Access Analytical - Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA 30340. AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA certified lab # FL-ES7582, NELAP certified laboratory # E87582 AIHA-LAP,LLC Laboratory ID:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SCINCIGA areas. All questions regarding this report should be directed Page 12 of 20 Page 1 of 6 R 0 CN +III G L: u b 2E c u9 2 S IL qto m �� 2 c> m 'r x x o a Q � c A � k � � � 2 $ � k � \ � .' � 9 < ƒ 2 « t a G & � k�k� 2e j § � � & � \ �� ■ § @ : � k 01 �k t� � � k k k d \ Q # § 1 \ \ k k k © @ 2 C 9 7\ N 161 (0 / / Analytical Environmental Services, Inc Date: 11-Apr-23 Client: Waypoint Analytical, LLC (Charlotte) Client Sample ID: 92760 Lab Order 2304486 Tag Number: Class A Project Name 23-093-0009 Collection Date: 4/3/2023 9:30:00 AM Lab ID: 2304496-OOIA Matrix: Solid Analyses Result Qual MDL Reportinbat&A dzlyzBitchID DF Analyst Limit Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1) Nitrogen, Armonia (AsN) Extractable 3760 238 403 -glKg-dry 354206 40 04/10/2023 15:11 TL PERCENT MOISTURE D2216 Percent Moisture 3.72 0 0 wt% R513160 1 04/09/2023 06:00 JW Qualifiers: . Value exceeds maximum contaminant Ievel RRL Not Detected at MDL H Holding times for preparation or analysis exceeded N Analyte not NELAC certifwd B Analyte detected in the associated method blank E Estimated value above quantitation range S Spike Recovery outside limits due to matrix > Greater than Result value J Estimated value detected below Reporting Limit < Less than Result value Page 14 of 20 Page 3 of 6 tD Do Rr d' Q M N d E z a d `o w Q O] s O a O U V C c v u ❑ Ln LQ a a h a Ln � ❑ a V X �ii� ai ro AMA C LL a u u C 0 Y 0 U o6 E F a u � � Q Ul ~ o 'o E m 6 4 ar m v Y i O tt N L ElT 0 a aj as C Y C a d a V 0 a ro i a u ba b V Q 0 •. i, ® • • • •: i. • M4 7 a u w aj � ro c ro C m j n c-1 i u � n. c a E m � 0r � ro c y a c n. u �`• u a t, a E Y O G GO a tic i a C O ej c M1. U a C Q m sa u p E T) Q c Y a s i C h Q c y Y v m m ro u .Luo o O CO a % ,ocn Q i N u d a4 uw a as m o T y T C a Y c 'y a C m M ate+ f. o 0 o a E ro to m E E m w N c N a 7• o T v am. a aa+ u' o cis a N m m a a o o w c E a a a E c m c m p E a F vLA U u F U N 0 0 0 0 a a 3 4 m c. a m M N l0 a a) 0 p U u o 0 ni � d u m m L Q Q h � � r Ln C a `m `a E Uo u° Uo C* •7 ui lD I-� ap 61 O 4 N N] ui �i Q Ll U ❑ ❑ b u c a 0 O > ro a u a °± s ; _ Q a C C C � C ❑ ❑ O '0 c a D C 2 a g O a y U � _ u u C O N a a 0 E m o. o. ro C C m m • ® C 0 • .: ... i 0 ,, 0 POCCO • ®! 3 (E) q M a y M T 16 = C � m a�-s a n. a U 0i c c u n• a M1 N. U U O v p +10+ u0i ,cu a u a c ro C +„ ou C E a s fl0 Q 0 U a u u c a Q G. s . m c E m Q E E u y m E n n n c a 0 c n o Y a aj c C a �a d Y m — u & .0 u aroi > v E m a V a c a 0 a a3 •E y v u m c N = m h uu a L fl. vi u, c a E a a a 0 0. o o E m Y a w Y Ls a o �o m a? 3 m 2 z 0 z N O 9 co U 2 2 N N 3 41 a E ID 0 Q U m m Qr Q Co Q >. c Q � C U� E `n o E N a 0 `C U H U LD r� CO 6i O � N fri a Li Ld r, ,-1 r e c-I N N N N N N N N m N co 4' N La M c w O (V w 0 u1 r-1 a M rd W 4 CD 0 P] a 4 O 0 0 00 0 U) 0 z O h 0 m O 00 N ON N Lfi ON mte.� G r� CO O a) CD a b s T m O x E N •a q � ,u o m T y W Z n End of Report Page 17 of 20 Page 6 of 6 Waypoint.(D ANALYTICAL 449 5pringbrook Rd, Charlotte, NC 28217 Main 7p4.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number:01206 Customer Name: Town of Mooresville/RR WWTP Report Number: 23-093.0009 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier C) Other: Thermometer ID: IRT15 2.7C Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received 1' Custody seals intact on shipping container/cooler? 0 Yes 0 No Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? Yes 0 No COC agrees with sample label(s)? Yes 0 No COG properly completed Yes 0 No Samples in proper containers? 0 Yes 0 No Sample containers intact? 0 Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? 0 Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 N/A Water - VOA vials free of headspace 0 Yes O No N/A Trip Blanks received with VOAs 0 Yes 0 No 0 NIA Soil VOA method 5035 — compliance criteria met Yes 0 No 0 N/A High concentration container (48 hr) High concentration pre -weighed (methanol -14 d) F Low concentration EnCore samplers (48 hr) [_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes (# No Comments: Signature: ngelo Norvell Date & Time: 04/03/2023 12:02:04 Page 18 of 20 tzULzc am m x c) v 4LLtcfn� M 0. t7 O L rn � MCI n" 0LLfi: 00 czQ, v . Cy9 Cf m �i 711 t7 „ L L a 22 ^1 t7 z L z t- N C-) � L rt �I -I gal i r n L� m _ o m mLLM CL n� L_ n c u , aLC:'Cl �z o Lr �o n v N i L L: I- — > zz m A z w C r- an � r N � o L L z in A n m m L a m b v I r� �c C, 53 m� as r Ile.5r cm to as an 3 m. 01_ 2. Tam ol3l wes IIWRR WWTP 44t}3-2023 class A 12:01:12 0 m m D M.9 C5fm g tA m m a mt� . �. tOp rait t= � so 03 = � °n c°i a Zy sus = = 13 { m - N G a 01 x a n to a W H O iF m o T m.m0 eD t0 C O 0 > O v a � m iR n 0� m a� `p c b� 4- •a S V r M > z O Y a� ; T C) a �y n7 'o -ata'a y o_` e o L/ m n y y h 0 z > O 10 O m m `G fo ° c /� L * �# � v �� O Z z (D m Q ... � n m 0 m x. imv F prz. m -" 0 Ja 62 9 Om 2 c�. a mn Y1 Z 2 Z t`°i,➢tmllm� F d Z i'ri m -4 �-� r � e O 1 t7 s ,G)(n �. _t Q J 0 P U' m .9 Q m Page 19 of 20 jL L 2 Z z 0 p l Ci U 2' 0 --C L L rC a cf. M A O L d , M n f U U 0 A Z X li n C L zc1n 0 � n m If � i m G L ~ I 02 it L z G1 W ro m . it x n L co 0 rA F t" 4 L L X 0a CL • o n n L" L M 2 m G01 -n n y L L > Z Z m n T w L 1- N to i- N C1 TG L`0 a nm L� n n L C C: �91� D a a � � m 0 0 a MM� I to - ry m ti o . , !'Z' it - CA m y , m maw a q x-%� n a m N �+ yTin 0 m 2 C A 9L L A * -i cn cr rp 2 vr. � 7 a n � Rr DCJ M c -ms a a R 5m c � 0 .0 via g C-2 g m L fA' L a� m13 a 3 4 ^ 0 'K ID m Z N w xr m _ ..CL _ .... IEI�� a1XOB3-0UQB � OM a i CZass A 12:01:12 a a i0 O O [1 EL t ,OOi NO m w A r �x=A ci 3 r) 4ar� A N 7- Yin A yNp � 9 8 CAR O C tC 0 - p m pa. co, - tn 0 O Z b m �a,mon 3 b 7 o zw A m H m m i p .0 m z c C n D •o Z o y �v A. to 'tl eo A M VN i CY i v Page 20 of 20 (2) Waypoint ANALYTICAL 7/26/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number. 23-191-0004 Client Project Description: Class A Dear Whitney Munroe: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.corn Waypoint Analytical, LLC (Charlotte) received sample(s) on 7/10/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 23 Waypointo ANALYTICAL 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6264 www.waypointana"cal.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State North Carolina North Carolina South Carolina South Carolina Program Lab ID Expiration Date State Program 37735 07/31/2023 State Program 402 12/31/2023 State Program 99012 07/31/2023 State Program 99012 12/31 /2022 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/29/2024 Arkansas State Program 88-0650 02/07/2024 California State Program 2904 06/30/2024 Florida State Program - NELAP E871157 06/30/2024 Georgia State Program C044 11/14/2025 Georgia State Program 04015 06/30/2024 Illinois State Program - NELAP 200078 10/10/2023 Kentucky State Program 80215 06/30/2024 Kentucky State Program KY90047 12/31/2023 Louisiana State Program - NELAP LA037 12/31/2023 Louisiana State Program - NELAP 04015 06/30/2024 Mississippi State Program MS 11/14/2025 North Carolina State Program 47701 07/31/2023 North Carolina State Program 415 12/31/2023 Pennsylvania State Program - NELAP 68-03195 05/31/2024 South Carolina State Program 84002 06/30/2023 Tennessee State Program 02027 11/14/2025 Texas State Program - NELAP T104704180 09/30/2023 Virginia State Program 00106 06/30/2024 Virginia State Program - NELAP 460181 09/14/2023 Page t of 1 00016/23-191-0004 Page 2 of 23 • Waypoint- 449 5pringbrpnk Rd, Charlotte, 28217 Main 7U4.S 29.fi364 ANALYTICAL www.waypointanalytical,com Sample Summary Table Report Number; 23-191-0004 Client project Description: Class A Lab No Client Sample ID Matrix Date Collected Date Received Method Lab 10 89102 Class A Sludge 07/10/2023 08:30 07/10/2023 11:58 89102 Class A Sludge 07/10/2023 08:30 07/10/2023 11:58 6010D WP MTN 89102 Class A Sludge 07/10/2023 08:30 07/10/2023 11:58 SW-1311 WP MTN 89102 Class A Sludge 07/10/2023 08:30 07/10/2023 11:58 808113 WP MTN 89102 Class A Sludge 07/10/2023 08:30 07/10/2023 11:58 8151A WP MTN 89102 Class A Sludge 07/10/2023 08:30 07/10/2023 11:58 8270C WP MTN 89102 Class A Sludge 07/10/2023 08:30 07/10/2023 11:58 7470A WP MTN 89103 Class A Solids 07/10/2023 08:30 07/10/2023 11:58 89103 Class A Solids 07/10/2023 08:30 07/10/2023 11:58 350.1 AES 89103 Class Solids 07/10/2023 08:30 07/10/2023 11:58 6010D WP MTN 89103 Class Solids 07/10/2023 08:30 07/10/2023 11:58 4500NORGD-2011 WP MTN 89124 Class A SAR Solids 07/10/2023 08:30 07/10/2023 11:58 AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 23 Waypoint(2) ANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A Lab Report Number: 23-191-0004 Date: 8101 /2023 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE This is a revised report and supersedes the original laboratory report dated 7/26/23. The SAR calculation has been added to the case narrative. Report Comments Ammonia subcontracted to Analytical Environmental Services. SAR =[2.15]ISQRT {(3.3)/2) SAR =[Na]/SQRT {([Ca]+[Mg])12) SAR = [ 2.15 ] / SQRT { ( [1.98] + [1.32] )12 } SAR =[2.15]/SQRT {(3.3)12} SAR =[2.15]ISQRT {1.65} SAR =1.68 Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (50,000) + 0.6 * 2030.4 PAN=15,000 + 1,015.2 PAN=16,000 Fecal Coliform MAN Method 9221E-2011 Sample 89103 (Class A) QC Batch No: V35141 Duplicate result: 0 MPN/100mL SeparatoryFunnel Extraction 8081 Method 3510C Sample 99102 (Class A) QC Batch No: L693154IL693154 The weight/volume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Separatory Funnel Extraction 8270 Method 3510C Sample 89102 (Class A) QC Batch No: L6933411L693341 The weightivolume extracted was reduced during the extraction procedure due to the nature of the sample. Reporting limits are factored for the sample size reduction. Metals Analysis Method 601 OD Page 4 of 23 Waypoint(b ANALYTICAL 449 Springbrook Rd, Charlotte, NC 29217 Main 704.529.6364 www.waypointanalytical.coni Sample 98815 (ST23JUL01-03-001) Analyte: Aluminum QC Batch No: 1-69302611-692550 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98815 (ST23JUL01-03-001) Analyte: Calcium QC Batch No: L6930261L692550 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98815 (ST23JUL01-03-001) Analyte: Potassium QC Batch No: 1-693026/1-692550 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98815 (ST23JUL01-03-001) Analyte: Magnesium QC Batch No: L6930261L692550 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 98815 (ST23JUL01-03-001) Analyte: Zinc QC Batch No: L693026/1-692550 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Aluminum QC Batch No: V35277N35161 LRB/LLC failed high. Result 1 Ox concentration. Result not affected. Sample 89053 Analyte: Aluminum QC Batch No: V352771V35161 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Aluminum QC Batch No: V353451V35161 LLC failed high. Result 10x concentration. Result not affected. Sample 89053 Analyte: Aluminum QC Batch No: V35345N35161 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89053 Analyte: Aluminum QC Batch No: V35345N35161 Page 5 of 23 (D Waypoint ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 89053 Analyte: Arsenic QC Batch No: V35224N35161 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 89053 Analyte: Calcium QC Batch No: V35224lV35161 LRB/LCC failed high. Result 1 Ox concentration. Result not affected. Sample 89053 Analyte; Cadmium QC Batch No: V35224N35161 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 89053 Analyte: Copper QC Batch No: V352771V35161 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Sample 89053 Analyte: Potassium QC Batch No: V35277N35161 The matrix spike, matrix spike duplicate and the post digestion spike were all outside of the quality control acceptance ranges. Matrix interference is suspected Sample 89053 Analyte; Potassium QC Batch No: V35345N35161 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 89053 Analyte: Potassium QC Batch No: V35345N35161 Matrix spikelmatrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Sample 89053 Analyte: Magnesium QC Batch No: V35224N35161 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Sample 89053 Analyte: Molybdenum QC Batch No: V35224N35161 Page 6 of 23 Waypoint(D ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 89053 Analyte: Sodium QC Batch No: V35224N35161 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 89053 Analyte: Nickel QC Batch No: V35224N35161 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Sample 89053 Analyte: Lead QC Batch No: V35224N35161 The matrix spike, matrix spike duplicate and the dilution test were all outside of the quality control acceptance ranges. Matrix interference is suspected. Sample 89053 Analyte: Selenium QC Batch No: V35224N35161 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Analyte: Zinc QC Batch No: V35345N35161 LLC failed high. Result 1 Ox concentration. Result not affected. Semivolatile organic Compounds - GC/MS (TCLP) Method 8270D Sample 89102 (Class A) QC Batch No. L693601IL693341 The sample was diluted due to the nature of the sample matrix. Reporting limits have been adjusted accordingly. Anions by ion Chromatography Method 9056A Sample 89103 (Class A) QC Batch No: V35582N35578 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable. LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Page 7 of 23 Waypoint. ANALYTICAL 01205 Town of Mooresville/RR W4NTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalocal.com Report Number .23-191-0004 REPORT OFANALYS3'S Lab No : 89102 Sample ID : Class A Report Date : 08/01/2023 Received : 07/10/2023 Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 7/10/2023 8:30 Test Results Units MQL DF Date I Time Analyzed By Analytical Method TCLP Herbicide Extraction Leachate 1 07/13/23 13:00 ALM SW-1311 TCLP Metals Extraction Leachate 1 07/13/23 13:00 ALM SW-1311 TCLP Pesticide Extraction Leachate 1 07/13/23 13:00 ALM SW-1311 TCLP SVOC Extraction Leachate 1 07/13/23 13:00 ALM SW-1311 TCLP VOC ZHE Extraction Leachate 1 07/11/23 08:00 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): L692793 07/14/23 11:28 Prep Method: 3015A Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP Arsenic <0.250 mg/L 0.250 1 07/14/23 16:53 BKN L693021 TCLP Barium <0.250 mg1L 0.250 1 07/14/23 16:53 BKN L693021 TCLP Cadmium <0.0500 mglL 0.0500 1 07/14/23 16:53 BKN L693021 TCLP Chromium <0.100 mg/L 0.100 1 07/14/23 16:53 BKN L693021 TCLP Lead <0.100 mg/L 0.100 1 07/14/23 16:53 BKN L693021 TCLP Selenium <0.500 mg/L 0.500 1 07/14/23 16:53 BKN L693021 TCLP Silver <0.0500 mg/L 0.0500 1 07/14/23 16:53 BKN L693021 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 8 of 23 Waypoint.(b ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 Report Number : 23-191-0004 Lab No : 89102 Sample ID : Class 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana"cal.com REPORT OFANALYSIS Report Date : 08/01/2023 Received : 07/10/2023 4 Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 7/10/2023 8:30 Analytical Method: 7470A Prep Batch(es): L692975 07/17/23 08:03 Prep Method: 7470A Test Results Units MQL DF Date I Time By Analytical Analyzed Batch TCLP Mercury Analytical Method: 8081B Prep Method: 3510C Test TCLP Endrin TCLP gamma-BHC TCLP Methoxychlor TCLP Toxaphene TCLP Chlordane TCLP Heptachlor Epoxide TCLP Heptachlor Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Analytical Method: 8151A Prep Method: 8151A Test <0.0200 mg/L 0.0200 1 07/17/23 13:20 FDS L693136 Prep Batch(es): L693154 07/17/23 14:40 Results Units MQL DF Date 1 Time By Analytical Analyzed Batch <0.004000 mg/L 0.004000 10 07/17/23 22:44 VIC L693452 <0.004000 mg/L 0.004000 10 07/17/23 22:44 VIC L693452 <0.004000 mg/L 0.004000 10 07/17/23 22:44 VIC L693452 <0.03000 mg/L 0.03000 10 07/17/23 22:44 VIC L693452 <0.02000 mg/L O.02000 10 07/17/23 22:44 VIC L693452 <0.004000 mg/L 0.004000 10 07/17/23 22:44 VIC L693452 <0.004000 mg/L 0.004000 10 07/17/23 22:44 VIC L693452 63.35 Limits: 36-116% 10 07/17/23 22:44 L693452 43.55 Limits: 25-123% 10 07/17/23 22:44 L693452 Prep Batch(es): L692922 07/14/23 16:20 Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg/L 0.0200 1 07/18/23 22:37 VIC L693666 TCLP 2,4,5 TP(5ilvex) <0.0020 mg/L 0.0020 1 07/18/23 22:37 VIC L693666 Surrogate: DCAA 49.60 Limits: 20-120% 1 07/18/23 22:37 L693666 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 9 of 23 Wayoint,p.(D ANALYTICAL 01205 Town of Mooresville/RR WWrP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville , NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Report Number :23-191-0004 REPORrOFAMALYSIS Lab No: $9102 Sample ID : Class A Report Date : 08/01/2023 Received : 07/10/2023 +> U)4 Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 7/10/2023 8:30 Analytical Method: 8260D Prep Batch(es): V35392 07/14/23 09:00 Prep Method: 5030B Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 07/14/23 20:58 MSA V35394 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP Chloroform <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP 1,2-Dichloroethane <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP 1,i-Dichloroethene <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP Methyl Ethyl Ketone (MEK) 0,307 mg/L 0.0500 10 07/14/23 20:58 MSA V35394 TCLP Tetrachloroethene <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 07/14/23 20:58 MSA V35394 Surrogate:4-Bromofluorobenzene 99.4 Limits: 80-124% 10 07/14/23 20:58 MSA V35394 Surrogate: Dibromofluoromethane 101 Limits: 75-129% 10 07/14/23 20:58 MSA V35394 Surrogate: Toluene-d8 98.0 Limits: 77-123% 10 07/14/23 20:58 MSA V35394 Analytical Method: 8270C Prep Batch(es): L693341 07/18/23 11:00 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylphenol <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 TCLP 3&4 Methylphenol <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 TCLP 2,4-Dinitrotoluene <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 TCLP Hexachlorobenzene <0.0620 mg/L 0A620 5 07/19/23 15:29 VBW L693601 Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 10 of 23 Waypointo ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 449 5pringbrook Rd, Charlotte, NC.28217 [Main 704.529.6364 www.waypointana "cal.corn Report Number .23-191-0004 REPORT OF ANALYSIS Lab No : 89102 Sample ID : Class Report Date : 08/01/2023 Received : 07/10/2023 629U)4 Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 7/10/2023 8:30 Analytical Method: 8270C Prep Method: 3510C Test Results Prep Batch(es): Units L693341 07/18/23 11:00 MQL DF Date I Time By Analyzed Analytical Batch TCLP Hexachlorobutadiene <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 TCLP Hexachloroethane <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 TCLP Nitrobenzene <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 TCLP Pentach[orophenol <0.125 mg/L 0.125 5 07/19/23 15:29 VBW L693601 TCLP Pyridine <0.125 mg/L 0.125 5 07/19/23 15:29 VBW L693601 TCLP 2,4,5-Trichlorophenol <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 TCLP 2,4,6-Trichlorophenol <0.0620 mg/L 0.0620 5 07/19/23 15:29 VBW L693601 Surrogate: TCLP 2,4,6-Tribromophenol 70.2 Limits: 42-102% 5 07/19/23 15:29 VBW L693601 Surrogate: TCLP 2-Fluorobiphenyl 60.3 Limits: 24-86% 5 07/19/23 15:29 VBW L693601 Surrogate: TCLP 2-Fluorophenol 23.7 Limits: 13-37% 5 07/19/23 15:29 VBW L693601 Surrogate: TCLP 4-Terphenyl-d14 66.4 Limits: 30-122% 5 07/19/23 15:29 VBW L693601 Surrogate: TCLP Nitrobenzene-d5 60.3 Limits: 25-78% 5 07/19/23 15:29 VBW L693601 Surrogate: TCLP Phenol-d6 18.7 Limits: 9-27% 5 07/19/23 15:29 VBW L693601 Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit H Beyond holding time Q RPD >40% dual column results Page 11 of 23 (D Waypoint ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number :23-191-0004 Lab No : 89103 Sample ID : Class 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6164 www.waypointana"cal.com REPORT OFANALYSIS Report Date : 08/01/2023 Received : 07/10/2023 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 7/10/2023 8:30 Test Results Units MQL DF Date / Time Analyzed By Analytical Method Fecal Coliform MPN/g <2.0 MPN/9 - dry 2.0 1 07/10/23 12:35 SMW 9221E-2011 Plant Available Nitrogen 16700 mg/Kg - dry 10.5 10 07/17/23 13:50 CALCULATION Moisture 4.33 1 07/11/2314:40 PEB SW-DRYWT Ammonia Nitrogen 2000 mg/Kg AR 1 07/19/23 13:42 TWC 350.1 Nitrate+Nitrite-N 31.8 mg/Kg - dry 10.5 10 07/21/23 13:35 9056A pH 6.34 H S.U. 1 07/15/23 14:30 EKF 9045D Total Solids 95S % 0.010 1 07/11/23 14:40 PEB 254OG-2011 Total Kjeldahl Nitrogen 54400 mg/Kg - dry 4420 20 07/17/23 13:50 ANH 4500MORGD-2011 Phosphorus 18300 mg/Kg - dry 52.3 10 07/17/23 21:57 JTR 6010D Aluminum 20500 mg/Kg - dry 26.1 5 07/12/23 19:32 JKC 6010D Arsenic 2.68 mg/Kg - dry 0.522 1 07/18/23 16:13 JKC 6010D Cadmium 0.477 mg/Kg - dry 0.105 1 07/11/23 22:37 JKC 6010D Calcium 18000 mg/Kg - dry 26.1 5 07/12/23 19:32 JKC 6010D Copper 236 mg/Kg - dry 0.261 1 07/12/23 19:36 JKC 6010D Lead 9.09 mg/Kg - dry 0.313 1 07/11/23 22:37 JKC 6010D Magnesium 2580 mg/Kg - dry 5.23 1 07/11/23 22:37 JKC 6010D Mercury (Total) 0.247 mg/Kg - dry 0.0314 1 07/12/23 1920 JKC 7471E Molybdenum 8.50 mg/Kg - dry 0.522 1 07/11/23 22:37 JKC 6010D Nickel 21.4 mg/Kg - dry 0.261 1 07/11/23 22:37 JKC 6010D Potassium 2870 mg/Kg - dry 131 5 07/12/23 19:32 JKC 6010D Selenium 3.40 mg/Kg - dry 0.522 1 07/11/23 22:37 JKC 6010D Sodium 848 mg/Kg - dry 52.3 1 07/11/23 22:37 JKC 6010D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit Q RPD >40% dual column results Page 12 of 23 (D Waypoint, ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information : Mooreseville , NC 28115 Report Number : 23-191-0004 Lab No : 89103 Sample ID : Class A Test Zinc 449 Springbrook Rd, Charlotte, NG 28217 Main 704.529.6364 www.waypointanalytical.com REPORT OFANAL PSIS Results Units MQL 499 mg/Kg - dry 0.522 Report Date : 08/01/2023 Received : 07/10/2023 60 L -04 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 7/10/2023 8:30 DF Date I Time By Analytical Analyzed Method 1 07/18/23 16:13 JKC 6010D Qualifiers/ DF Dilution Factor H Beyond holding time Definitions MQL Method Quantitation Limit o Q RPD >40 /a dual column results Page 13 of 23 i Waypoint, 449 5pringbraok Rd, Charlotte, NC 28217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe Report Date : 08/01/2023 369 Johnson Dairy Rd. Information : Received : 07/10/2023 Mooreseville, NC 28115 Report Number : 23-191-0004 REPORT OFANAL PSIS Terri W ColeLaboratory Project Manager Lab No: 89124 Matrix: Solids Sample ID : Class A SAR Sampled: 7/10/2023 8:30 Test Results Units MQL DF Date I Time By Analytical Analyzed Method Calcium (saturated paste) 1.98 meq/L 0.050 1 07/20/23 11:32 JKC Saturate Paste Magnesium (saturated paste) 1.32 meq/L 0.083 1 07/20/23 11:32 JKC Saturate Paste Sodium (saturated paste) 2.15 meq/L 0.043 1 07/20/23 11:32 JKC Saturate Paste Sodium Absorption Ratio 1.68 1 07/20/23 11:32 JKC Saturate Paste Moisture 4.42 1 07/11/2314:40 PEB SW-DRYWf' Qualifiers/ DF Dilution Factor Definitions H Beyond holding time Page 14 of 23 Access ANALYKAL, INC. ANALYTICAL REPORT CLIENT Waypoint Analytical 449 Springbrook Road Charlotte NC 28217 ATTENTION Terri W Cole PROJECT ID 23-191-0004 LABORATORY REPORT NUMBER 2307751 DATE July 20, 2023 Primary Data Review By Secondary Data Review By Chris Pafford Project Manager, AES PLEASE NOTE: Ashlcy Amick Project Manager, Access Analytical aamick@axs-inc.com Unless otherwise noted, all analysis on this report performed at Analytical Environmental Services Inc. (AES Inc), 3080 Presidential Drive, Atlanta, GA30340. - AES is SCDHEC certified laboratory # 98016, NCDENR certified lab # 562, GA eertiiied lab # FL-E87582, NELAP certified laboratory # E87582 AIHA-LAP,LLC Laboratory 1113:100671 for Industrial Hygiene samples (Organics, Metals, PCM Asbestos, Gravimetric), Environmental Lead (Paint, Soil, Dust Wipes, Air), and Environmental Microbiology (Fungal) Direct Examination. Local support services for this project are provided by Access Analytical, Inc. Access Analytical is a representative of AES serving client in the SC/NC/GA areas. All questions regarding this report should be directed to your local Access Analytical representative at 803.781.4243 or toll fee at 883.315.4243 Page 1 of 6 Page 15 of 23 E A ■ » � �• � ƒ<� cn k u 2� ■ �� i g 8 ƒ L) . � � � �■ t2 6 \ «tag .4CE, CL � k .k :e .� : / rn rn � � $ � k k © . , C. � 2 � � 0 m 2 £ a Im & ƒ . � t � z (0 / & 2 j 0 / \ a Analytical Environmental Services, Inc Date: 20-Jul-23 Client: Waypoint Analytical Client Sample 1D: 89103 Lab Order 2307751 Tag Number: Class A Project Name: 23-19I-0004 Collection Date: 7/10/2023 8:30:00 AM Lab W- 2307751-001A Matrix: Soil Analyses Reporting Y Result QuaI MDL Limit Units BatchID DF Date Analyzed Analyst Nitrogen, Ammonia (as N) Extractable E350.1 MOD (E350.1) Nitrogen,Amraonia (As N) Extractable 2000 62.7 106 mg/tcg-dry 359577 10 07/19/2023 13:42 TL PERCENT MOISTURE D2216 Percent Moistm-e 7.68 0 0 wt! R521036 1 07/12/2023 00:00 JW Qualifiers: • Value exceeds maximum contaminant feud E Estimated value above quantitation range BRI. Not Detected at MDL S Spike Recovery outside limits due to matrix H Holding tunes for preparation or analysis exceeded > Greater than Result value N Aualyte not NELAC certified J Estimated value detected below Reporting Limit B Analyte detected in the associated method blank a Less than Result value Page 3 of 6 Page 17 of 23 N i 1 1 C O 'O O U N 41 u m � � Q a E m a c N v y � y L u (Um Ela ,aL m m a u c � o Y a N � ❑ b to C C E o y O v 1 la n` c 0 0 ♦i ., C. .. :� V O � v y a � c m m a ai m M in C" O '7� m v' C u c m n• m u '0 O NL) C i n• V a?d 3 + C v y o E M1 v OG.o V O u N O=D rw r ��•• 8� v a C y M1• �' G.0 hu } U c a ac� m - 'u O 0 c c •r, o- c h N y a y 0 E a a u h � 5 v f9 ro 0 0 y _ a E 0 E m m E d F- Q o U O U1 Q1 7 j � m W a C Q E � F v 00 v `m U U u u u U 0 c O o rn O r � E E CJ L `i Ln m `m v E u° u0 u° r6 -i L6 1D I� W 6 O e4 n1 to � vl 2 e 2 i 1 I ❑ ❑ ❑ Li u ❑ ❑ 0 u C d O O O c C O c ❑� V o p N O c 'a CV u 0) y 0 d a m v a E m o a a 0 E E y = m m V� :)Oo o c o 400 ® ® c ., 0 C. r• M1 N N � a L � m C � m W 0 a y m u n• L v y n• r. a cOi E c _ m W sn U u O .° c 'O N v a p e v$ 0 Y �'• V i u c E N t L C R L +' c m O V O +L+ E O O N a m u m N O N a O� +' 3 E a E a aj m a E r. N r E N W n •c v = CO c m C y } clj a IV Y 0 W c u 7 m N m c a E o E: O O Q C m Q u N K d i a u .2Q N m c °u N m Y E? m a� m CL E y > 0 m y Q, E s m a 7 +� _ m v t. D a m }a o R m 3 L V U B Q }j c7 C G7 C U Q m N 3 CO C. E 0CD g U CL R C, T O� c O lc� 7�; m W .�c E y m r U 5 [6 h W OZ O r4 N NI 7 L'i 46 h ' .-I +i r-i N N N N N N N M O cn N W 0 co N �l LL O n Oe ^ Q cn o n er e o en N r m +� en YK�II N N Ali �.-1 N U] N eM.3 kn 4 O z z z z c'V Lo CD ti z W z LYi z Z �+ m (V A 114 V] Q? rj c 10 Aq] w W in p per], � �j P7 r M M N N N N N N N N b q o 0 0 0 a 0 0 m 0 0 0 x en a v b E 00 F4 i� i�a 91. a a a ao no co p M PC � x � � M 3 ON M 3 M 3 M g D\ m � -•+ au c e c o o M E N A O y4-4 'o O '� r7 �✓ , � � fi rn U y N N 0 (u rA v y 1�f1 G v eY�I w is o o a y ea > N y > N ri vl� W 093 K UJ eG o a a e Y7 0 �1 on 0 Ei a d �F4i d a o ea M o O O e z" � z" coo z oot z .y •,U�+ H [y W T U �i N y Fi NCA o LL�y CY Ci V V � U Y u � 'o ..Cd W M p i a N U A QPC C a, CL> CD �a3 M CA ¢ z �m�6.1 ¢ z 5 d End of Report Page 6 of 6 Page 20 of 23 `�9 Springbraak Rd, Charlotte, 282 Waypoint(b64 Main 7p4.S.5 29.6354 ANALYTICAL www.waypointanalocal.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of Mooresville/RR WWTP Report Number: 23-191-0004 Shipping Method 0 Fed Ex 0 US Postal # Lab 0 UPS 0 Client 0 Courier 0 Other: Thermometer ID: IRT15 3AC Shipping container/cooler uncompromised? Yes 0 No Number of coolers/boxes received I ' Custody seals intact on shipping container/cooler? 0 Yes 0 No # Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? Yes 0 No COC agrees with sample Iabel(s)? Yes 0 No COC properly completed 0 Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? # Yes 0 No Sufficient sample volume for indicated test(s)? 0 Yes 0 No All samples received within holding time? 0 Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes (DNo Water -- Sample containers properly preserved 0 Yes 0 No 0 NIA Water - VOA vials free of heads pace 0 Yes C) No 0 NIA Trip Blanks received with VOAs 0 Yes 0 No NIA Soil VOA method 5035 — compliance criteria met 0 Yes 0 No 0 N/A F High concentration container (48 hr) F_ High concentration pre -weighed (methanol -14 d) F Low concentration EnCore samplers (48 hr) [_ Low cone pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? 0 Yes (* No Comments: Signature: n elo Norvell Date & Time: 07/10/2023 12:05:04 Page 21 of 23 ( c F, .z C z O D Gra N n c : CCLc CAFE 0 � _ n L O n m n , FLU i a z a C02 � 4 0 m 31 n CL0RE n z w a fith p rn rA IE � F E Y!0 _. _ 1 06 r iE C wn 0 w m r e 01 nn .. °a 0 � L Q M G Z M w n l to Yam' 00 m a H L) L a 1 zz no Ira O �= v+ N r N CD °❑L0 = z ID Ix 0 m h G G) z D i` S my m� 1 m m GI g w C a CL 0 CD a S to 3 A � o o�!?" H. a� I.�: A EO 4 ° 0 '° a `C pa, z S n• ro S f Ol x 3 Z V, Z. p� pia b 000 D 'N o e°o z I 2 vol- C1 =I W 0:9 Q M m III a Iv • N _� 4 • OW J ll V 0� G �- x sa r m N M m a ra CL tli H m O. A Ox .w O m 0 t9 p to4 d y �° pzm` a ° a Z oma� wO = O C maNm m z Ym ocn rn ° n.� _ O z �z�g�o_ ° C�� 11 m ° c obi m� Z y ... D n � m I' C. to . M .o �. 7 N rzi�ro� °� ❑ m �w m v 0 0 r S1 y F 7 a ram, z� ii�.`nec m OAS �wwaTv �rryri � m ra Q.. y o rL ♦ / m N N m W / m 4c -13 n m -35 -00 g o a f MY I M O a;mu a m MIN m no ,Zn DO 147m m-+rncyb M = l Z a m?3 rn w Im a J _\ w n c 0 (I I 0 r, Page 22 of 23 Q,z° m W�c mmmrnI C 7p D. ID m a CZj. n' a an .y (AN � m_ C1 a Cb .S W F m VOr-w n n a D CL w a m . 3e C' co`� _ m in ¢ SA� - �z�C mm Z�. o a 3 7 ill 1 � � G 40 ig _� � MI W Q m i w a( y• ib n m a �. �a� _ �'g O a 3tl 0 C (a nn m a W � o O w n$ �m � o ca ! Q 0 v� Cmg Tc Lc�o �m "gym W m '< z m C D r"b-.3 OZ�o = m 4 7 CD '+� - CL z n -u + a m� ca rn © a3 .. 0 ; a m na m� m m5., o so_ m n a�.. v m W 1 om� mm_ CJ V m �� m I a 0-4m d Cf am R. ro m a m m 9 1 z D �owm O s m 0 p V ip ours a L)Zn m a I1°5c G Q 2.FE. 3N ono w m 4 ° oC.a1 S ;� zM m m w rmt� z In q O z J ', NJ mm- p u g m & n25�' 4 Cl 4 @ 0 cm l° Eat o C3 p- d g 3 =. Q 0 OO �s m o .� m .. f c a ! — 4 m m •'• v IsCA CL 7r d ON iN m /��6 pNp z 4 _ ;1 3 a m (z) I M ` z yy !1 • e ,Wj R Mm lO a m z • o I C m m � n n� > d s1 ,� a ro$ k N h d =V 3 Z Z 0) m .. .E > a Lpo >�• P� m A l"F z N. 0 �'O W D -0 � U1 -0 a O_m O�. n m •� CIj �a yb� a r Z a CC)•• qa0z m lit So 0 0 �? m 14 v Page 23 of 23 Waypoint(D ANALYTICAL 10/30/2023 Town of Mooresville/RR WWTP Whitney Munroe 369 Johnson Dairy Rd. Mooreseville, NC, 28115 Ref: Analytical Testing Lab Report Number: 23-282-0003 Client Project Description: Class A Dear Whitney Munroe: 449 5pringbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Waypoint Analytical, LLC (Charlotte) received sample(s) on 10/9/2023 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) unless otherwise indicated. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 60) L Terri W Cole Laboratory Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 15 (D Waypoint. ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Certification Summary Laboratory ID: WP CNC: Waypoint Analytical Carolina, Inc. (C), Charlotte, NC State Program North Carolina State Program North Carolina State Program South Carolina State Program South Carolina State Program Lab ID Expiration Date 37735 07131 /2024 402 12/31 /2023 99012 07/31 /2024 99012 12/31 /2023 Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Alabama State Program Arkansas State Program California State Program Florida State Program - NELAP Georgia State Program Georgia State Program Illinois State Program - NELAP Kentucky State Program Kentucky State Program Louisiana State Program - NELAP Louisiana State Program - NELAP Mississippi State Program North Carolina State Program North Carolina State Program Pennsylvania State Program - NELAP South Carolina State Program Tennessee State Program Texas State Program - NELAP Virginia State Program Virginia State Program - NELAP Lab ID Expiration Date 40750 02/29/2024 88-0650 02/07/2024 2904 06/30/2024 E871157 06/30/2024 C044 11 /14/2025 04015 06/30/2024 200078 10/31 /2024 80215 06/30/2024 KY90047 12/31 /2023 LA037 12131 /2023 04015 06/30/2024 M S 11 /14/2025 47701 07/31 /2024 415 12/31 /2023 68-03195 05/31 /2024 84002 06/30/2024 02027 11 /14/2025 T104704180 09/30/2024 00106 06/30/2024 460181 09/14/2024 Page 1 of 1 Page 2 of 15 00016/23-282-0003 • Waynoint. 449 Springbrook Rd, Charlotte, NC 2$217 Main 704.529.6364 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 23-282-0003 Client Project Description: Class A Lab No Client Sample ID Matrix Date Collected Date Received Method Lab ID 97127 Class A Sludge 10/09/2023 09:35 10/09/2023 11:47 97127 Class A Sludge 10/09/2023 09;35 10/09/2023 11:47 SW-1311 WP MTN 97127 Class A Sludge 10/09/2023 09:35 10/09/2023 11:47 8151A WP MTN 97128 Class A Solids 10/09/2023 09:35 10/09/2023 11:47 97128 Class A Solids 10/09/2023 09:35 10/09/2023 11:47 350.1 AES 97128 Class A Solids 10/09/2023 09:35 10/09/2023 11:47 6010D WP MTN 97128 Class Solids 10/09/2023 09:35 10/09/2023 11:47 4500NORGD-2011 WP MTN 97157 Class A Solids 10/09/2023 09:35 10/09/2023 11:47 AES: Analytical Environmental Services, Inc., Atlanta, GA WP MTN - Memphis, TN: Waypoint Analytical - TN, Memphis, TN Page 3 of 15 Waypoint(D ANALYTICAL Client: Town of Mooresville/RR WWTP Project: Class A Lab Report Number: 23-282-0003 Date: 10/26/2023 Report Comments SAR = [ Na ] / SQRT { ([Ca] + [Mg] )12 } SAR = [ 5.04 ] 1 SQRT { ( [4.68] + [2.80] )12 } SAR =[5.04]1SQRT {3.74} SAR = 2.61 449 5pringbrook Rd, Charlotte, NC 29217 Main 704.529.6364 www.waypointanalytical.com CASE NARRATIVE Concentrations for Na, Ca, and Mg are expressed in milliequivalents per liter, and SQRT designates taking the square root of the operand in parentheses. PAN Equation = 0.3 * (TKN — Ammonia) + 0.5 * (Ammonia) + Nitrate -Nitrite PAN = 0.3 * (64200-2390) + 0.5 * (2390) + 26.6 Pan = 18543 + 1182 Pan = 19725 Block Digestion and FIA Method 4500NORGD-2011 Analyte: Total Kjeldahl Nitrogen QC Batch No: L711880 Matrix spike recovery is outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Fecal Coliform MPN Method 9221E-2011 Sample 97128 (Class A) QC Batch No: V38856 Duplicate result: 0 MPN / 100ml Metals Analysis Method 601OD Sample 96220 Analyte: Aluminum QC Batch No: L711152/L710685 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 96220 Analyte: Potassium QC Batch No: L7115291L710685 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 96220 Analyte: Phosphorus QC Batch No: L7111521L710685 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 15 Waypoint(b ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanaiytical.com Sample 97194 Analyte: Copper QC Batch No: V39135IV38827 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97128 (Class A) Analyte: Molybdenum QC Batch No: V38938N38827 LLC failed high. Result 10x cocnentration. Result not affected. Analyte: Lead QC Batch No: V39174N38827 LLC failed high. Result 10x concentration. Result not affected. Sample 97194 Analyte: Selenium QC Batch No: V39174N38827 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97128 (Class A) Analyte: Potassium QC Batch No: V39195N39007 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 97128 (Class A) Analyte: Zinc QC Batch No: V39195N39007 Matrix spikeimatrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Total Aqueous Mercury Analysis - CVAA (TCLP) Method 7470A Sample 97349 Analyte: Mercury QC Batch No: V38928N38903 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Sample 97349 Analyte: Mercury QC Batch No: V38928N38903 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Semivolatile Organic Compounds - GC/MS (TCLP) Method 8270E Sample 97127 (Class A) QC Batch No: V390331V39031 Page 5 of 15 (D Waypaint,4 ANALYTICAL 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointanalytical.com Surrogate(s) were flagged for recoveries in the associated project sample. During the extraction step, the extraction technician noted that a significant emulsion formed. Batch QC samples (Method Blank and Laboratory Control Samples) all showed surrogate recoveries within QC limits, indicating that the biased recoveries were due to the sample matrix. Analyte: Pyridine QC Batch No: V39033N39031 Relative Percent Difference (RPD) for the duplicate analysis was outside of the allowable QC limits. Anions by Ion Chromatography Method 9056A Sample 97128 (Class A) QC Batch No: V39321N39309 Matrix spike/matrix spike duplicate recoveries are outside of control limits. Acceptable LCS recovery indicates the system was in control, but the reported result could be affected by matrix interference. Page 6 of 15 Waypointo AN ALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number . 23-292-0003 Lab No: 97127 Sample ID : Class A 449 Springbrook Rd, Charlotte, IBC 28217 Main 704.529.6364 www.waypointanalytical.com REPORT OFANALYSIS Report Date : 10/30/2023 Received : 10/09/2023 66 .. Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 10/9/2023 9:35 Test Results Units MQL DF Date / Time Analyzed By Analytical Method TCLP Herbicide Extraction Leachate 1 10/16/23 13:00 ALM SW-1311 TCLP Metals Extraction Leachate 1 10/10/23 15:40 LFR SW-1311 TCLP Pesticide Extraction Leachate 1 10/10/23 15:40 LFR SW-1311 TCLP SVOC Extraction Leachate 1 10/10/23 15:40 LFR $W-1311 TCLP VOC ZHE Extraction Leachate 1 10/11/23 13:30 TBL SW-1311 (ZHE) Analytical Method: 6010D Prep Batch(es): V38917 10/11/23 14:10 Prep Method: SW-3010A Test Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP Arsenic <0.050 mg/L 0.050 1 10/12/23 01:20 BMP V38940 TCLP Barium 0.068 mg/L 0.050 1 10/17/23 03.20 JKC V39132 TCLP Cadmium <0.0150 mg/L 0.0150 1 10/12/23 01:20 BMP V38940 TCLP Chromium <0.025 mg/L 0.025 1 10/12/23 01:20 BMP V38940 TCLP Lead <0.030 mg/L 0.030 1 10/12/23 01:20 BMP V38940 TCLP Selenium <0.100 mg/L 0.100 1 10/17/23 03:20 JKC V39132 TCLP Silver <0.025 mg/L 0.025 1 10/12/23 01:20 BMP V38940 Qualifiers/ Outside QC Limit Definitions H Beyond holding time DF Dilution Factor MQL Method Quantitation Limit Page 7 of 15 Waypoint,(D ANALYTICAL 01205 Town of Mooresville/RR WNVTP Project Class A Whitney Munroe 369 Johnson Dairy Rd, Information Mooreseville , NC 28115 Report Number :23-282-0003 Lab No : 97127 Sample ID : Class A Analytical Method: 7470A Prep Method: 7470A Test TCLP Mercury Analytical Method: 8081B Prep Method: 3510C Test TCLP Endrin TCLP gamma-BHC TCLP Methoxychlor TCLP Toxaphene TCLP Chlordane TCLP Heptachlor Epoxide TCLP Heptachlor Surrogate: Decachlorobiphenyl Surrogate: Tetrachloro-m-xylene Analytical Method: 8151A Prep Method: 8151A Test 449 Spr€ngbrook Rd, Charlotte, NC 28217 Main 704.529.6364 www.waypointana"cal.com REPOR T OF A NA L YSIS Prep Batch(es): V38903 10/11/23 13:40 Report Date : 10/30/2023 Received : 10/09/2023 Terri W Cole Laboratory Project Manager Matrix: Sludge Sampled: 10/9/2023 9:35 Results Units MQL DF Date / Time By Analytical Analyzed Batch <0.0002 mg/L 0.0002 1 10/11/2317:09 BMP V38928 Prep Batch(es): V39013 10/13/23 10:20 Results Units MQL DF Date I Time By Analytical Analyzed Batch <0.05000 N9/L 0.05000 1 10/16/23 15:45 TJW` V39122 <0.05000 pg/L 0.05000 1 10/16/23 15:45 TJW V39122 <0.1000 ug/L 0.1000 1 10/16/23 15:45 TJW V39122 <1.000 pg/L 1.000 1 10/16/2315:45 TJW V39122 <0.5000 Ng/L 0.5000 1 10/16/2315:45 TJW V39122 <0.1000 Ng/L 0.1000 1 10/16/23 15:45 TJW V39122 <0.05000 lig/L 0.05000 1 10/16/23 15:45 TJW V39122 35.20 Limits:13-186% 1 10/16/2315:45 TJW V39122 40.30 Umits:40-134% 1 10/16/2315:45 TJW V39122 Prep Batch(es): L711470 10/17/23 16:40 Results Units MQL DF Date 1 Time By Analytical Analyzed Batch TCLP 2,4-D <0.0200 mg1L 0.0200 1 10/18/23 21:09 VIC L711908 TCLP 2,4,5-TP (Silvex) <0.0020 mg/L 0.0020 1 10/18/23 21:09 VIC L711908 Surrogate: DCAA 62.60 Limits: 20-120% 1 10/18/23 21:09 L711908 Qualifiers/ Outside QC Limit DF Dilution Factor Definitions H Beyond holding time y g MQL Method Quantitation Limit Page 8 of 15 Waypoint-(D ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number : 23-282-0003 449 Springbrook Rd, Charlotte, NC 23217 Main 704.529.6364 www.waypointana"cal.com REPORT OFANAL PSIS Report Date : 10/30/2023 Received : 10/09/2023 om'W4 Terri W Cole Laboratory Project Manager Lab No : 97127 Sample ID : Class A Matrix: Sludge Sampled: 10/9/2023 9:35 Analytical Method: 8260D Prep Batch(es): V39156 10/16/23 14:00 Prep Method: 5030E Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Benzene <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP Carbon Tetrachloride <0.0200 mg/L 0.0200 10 10/17/23 11:45 MSA V39157 TCLP Chlorobenzene <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP Chloroform <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP 1,4-Dichlorobenzene <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP 1,2-Dichloroethane 0.0544 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP 1,1-Dichloroethene <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP Methyl Ethyl Ketone (MEK) 0.136 mg/L 0.0500 10 10/17/23 11:45 MSA V39157 TCLP Tetrachloroethene <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP Trichloroethene <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 TCLP Vinyl Chloride <0.0050 mg/L 0.0050 10 10/17/23 11:45 MSA V39157 Surrogate:4-Bromofluorobenzene 90.8 Limits:80-124% 10 10/17/23 11:45 MSA V39157 Surrogate: Dibromofluoromethane 99.2 Limits: 75-129%9 10 10/17/23 11:45 MSA V39157 Surrogate: Toluene-d8 98.6 Limits: 77-123% 10 10/17/23 11:45 MSA V39157 Analytical Method: 8270E Prep Batch(es): V39031 10/12/23 09:56 Prep Method; 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP 2-Methylpheno[ <0.010 mg/L 0.010 1 10/13/23 15:11 AMP V39033 TCLP 3&4 Methylphenol <0.010 mg/L 0.010 1 10/13/23 15:11 AMP V39033 TCLP 2,4-Din[troto[uene <0.010 mg/L 0.010 1 10/13/23 15:11 AMP V39033 TCLP Hexachlarobenzene <0.020 mg/L 0.020 1 10/13/23 15.11 AMP V39033 Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions H Beyond holding time Y 9 MQL Method Quantitation Limit Page 9 of 15 Waypointo, . ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number : 23-282-0003 449 Springbrook Rd, Charlotte, NC 28217 Main 704:529.6A 4 www.waypointanalocal.com REPORT OFANALYSIS Report Date : 10/30/2023 Received : 10/09/2023 60 UJ '- -P Terri W Cole Laboratory Project Manager Lab No : 97127 Matrix: Sludge Sample ID :Class A Sampled: 10/9/2023 9:35 Analytical Method: 8270E Prep Batch(es): V39031 10/12/23 09:56 Prep Method: 3510C Test Results Units MQL DF Date / Time By Analytical Analyzed Batch TCLP Hexachlorobutadiene <0.020 mg/L 0.020 1 10/13/23 15:11 AMP V39033 TCLP Hexachloroethane <0.010 mg/L 0.010 1 10/13/23 15:11 AMP V39033 TCLP Nitrobenzene <0.010 mg/L 0.010 1 10/13/23 15:11 AMP V39033 TCLP Pentachlorophenol <0.050 mg/L 0.050 1 10/13/23 15.11 AMP V39033 TCLP Pyridine <0.010 mg/L 0.010 1 10/13/23 15:11 AMP V39033 TCLP 2,4,5-Trichlorophenol <0.020 mg/L 0.020 1 10/13/23 15:11 AMP V39033 TCLP 2,4,6-T6chlorophenol <0.020 mg/L 0.020 1 10/13/23 15:11 AMP V39033 Surrogate: TCLP Phenol-d5 19.0 Limits: 11-100% 1 10/13/23 15:11 AMP 8270E Surrogate: TCLP 2,4,6-Tribromophenol 52.0 Limits: 43-140% 1 10/13/23 15:11 AMP V39033 Surrogate: TCLP 2-Fluorobiphenyi 40.0 * Limits: 44-119% 1 10/13/23 15:11 AMP V39033 Surrogate: TCLP 2-Fluoropheno[ 26.0 Limits: 20-119% 1 10/13/23 15:11 AMP V39033 Surrogate: TCLP 4-Terphenyl-d14 46.0 Limits: 44-120% 1' 10/13/23 15:11 AMP V39033 Surrogate: TCLP Nitrobenzene-d5 34.0 * Limits: 44-120% 1 10/13/23 15:11 AMP V39033 Surrogate: TCLP Phenol-d5 18.0 Limits: 11-100% 4 10/12/23 22:19 AMP 8270E Surrogate: TCLP 2,4,6-Tribromophenol 49.0 Limits: 43-140% 4 10/12/23 22:19 AMP V39033 Surrogate: TCLP 2-Fluorobiphenyl 36.0 * Limits: 44-119% 4 10/12/23 22:19 AMP V39033 Surrogate: TCLP 2-Fluoropheno] 23.0 Limits: 20-119% 4 10/12/23 22:19 AMP V39033 Surrogate: TCLP 4-Terpheny1-d14 44.0 * Limits: 44-120% 4 10/12/23 22:19 AMP V39033 Surrogate: TCLP Nitrobenzene-d5 32.0 * Limits: 44-120% 4 10/12/23 22:19 AMP V39033 Qualifiers/ * Outside QC Limit Definitions H Beyond holding time DF Dilution Factor MQL Method Quantitation Limit Page 10 of 15 Waypoint.(b ANALYTICAL 01205 Town of Mooresville/RR WWTP Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 449 Springbrook Rd, Charlotte, NC 28217 Main 704.529.6364 wum-waypo€ntanalytica l.com Report Number :23-282-0003 REPORT OFANALYSIS Lab No : 97128 Sample ID : Class Report Date : 10/30/2023 Received : 10/09/2023 6)*'W4 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 10/9/2023 9:35 Test Results Units MQL DF Date i Time Analyzed By Analytical Method Fecal Coliform MPN/g <2.1 MAN/g - dry 2.1 1 10/09/23 15:05 JMD 9221E-2011 Moisture 4.88 % 1 10/10/2317:40 CNC SW-DRYWT Ammonia Nitrogen 2390 mg/Kg AR 1 350.1 Nitrate+ Nitrite-N <26.6 mg/Kg - dry 26.6 14 10/20/23 12:17 9056A pH 11.3 H S.U. 1 10/11/23 11:52 EKF 9045D Total Solids 94.2 % 0.010 1 10/10/23 17:40 CNC 254OG-2011 Total Kjeldahl Nitrogen 64200 mg/Kg - dry 8240 20 10/19/23 14:07 ANH 4500NORGD-2011 Phosphorus 18700 mg/Kg - dry 26.3 5 10/17/23 16:06 BKN 6010D Aluminum 15000 mg/Kg - dry 26.3 5 10/17/23 02:31 JKC 6010D Arsenic 2.72 mg/Kg - dry 0.525 1 10/11/23 20:16 BMP 6010D Cadmium 0.646 mg/Kg - dry 0.105 1 10/11/23 20.16 BMP 6010D Copper 244 rng/Kg - dry 0.263 1 10/18/23 03:48 JKC 6010D Lead 8.39 mg/Kg - dry 0.315 1 10/11/23 20:16 BMP 6010D Mercury (Total) 0.266 mg/Kg - dry 0.0315. 1 10/12/23 16:37 BMP 7471B Molybdenum 13.1 mg/Kg - dry 0.525 1 10/11/23 20:16 BMP 6010D Nickel 12.0 mg/Kg - dry 0.262 1 10/17/23 18:56 JKC 6010D Potassium 2900 mg/Kg - dry 131 5 10/17/23 19:14 JKC 6010D Selenium 4.67 mg/Kg - dry 0.525 1 10/18/23 03:48 JKC 6010D Zinc 673 mg/Kg - dry 2.63 5 10/17/23 19:14 JKC 6010D Qualifiers/ Outside QC Limit DF Dilution Factor Definitions H Beyond holding time Y g MQL Method Quantization Limit Page 11 of 15 Waypoin(bt� ANALYTICAL 01205 Town of Mooresville/RR WWI"P Project Class A Whitney Munroe 369 Johnson Dairy Rd. Information Mooreseville, NC 28115 Report Number :23-282-0003 Lab No : 97157 Sample ID : Class A Test 449 Springbrook Rd, Charlotte, IBC 28217 Main 704.529.6364 www.waypointanalOca l.corn REPORT OFAAfALYSIS Results Units MQL Report Date : 10/30/2023 Received : 10/09/2023 Terri W Cole Laboratory Project Manager Matrix: Solids Sampled: 10/9/2023 9:35 DF Date / Time 8y Analytical Analyzed Method Calcium (saturated paste) 4.68 meq/L 0.050 1 10/18/23 18:19 JKC Saturate Paste Magnesium (saturated paste) 2.80 meq/L 0.083 1 10/18/23 18:19 JKC Saturate Paste Sodium (saturated paste) 5.04 meq/L 0.043 1 10/18/23 18:19 JKC Saturate Paste Sodium Absorption Ratio 2.61 1 10/18/23 18:19 JKC Saturate Paste Moisture 4.36 % 1 10110/2317:40 CNC SW-DRYWT Qualifiers/ * Outside QC Limit DF Dilution Factor Definitions Page 12 of 15 Waypoint.0 ANALYTICAL 449 Springbrook Rd, Charlotte, NC 29217 Main 704.529.6364 www.waypointanalytical.com Shipment Receipt Form Customer Number: 01205 Customer Name: Town of MooresviilelRR WWTP Report Number: 23-282-0003 Shipping Method 0 Fed Ex 0 US Postal 0 Lab 0 UPS 0 Client 0 Courier Shipping container/cooler uncompromised? 0 Yes 0 Other: Thermometer ID: 0 No IRT-15 1 AC Numberof coolers/boxes received F 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No Not Present Chain of Custody (COC) present? Yes 0 No COC agrees with sample label(s)? Yes 0 No COC properly completed Yes 0 No Samples in proper containers? Yes 0 No Sample containers intact? Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. 0 Yes Yes 0 No 0 No Water - Sample containers properly preserved 0 Yes 0 No 0 NIA Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No 0 NIA Soil VOA method 5035 — compliance criteria met Yes 0 No 0 NIA F- High concentration container (48 hr) F- High concentration pre -weighed (methanol -14 d) Special precautions or instructions included? F- Low concentration EnCore samplers (48 hr) F- Low conc pre -weighed vials (Sod Bis -14 d) 0 Yes * No Comments: Signature: Caitlyn Cummins Date & Time: 10/09/2023 13:02:23 Page 13 of is cjc, Ci zu z 20a n L �I m h c x v UL,C CA m L i? L R ID 0 H cn L L Q z n C o u n 3 c m cr n n m h ml O t7 m LLd� m Z M a 0 Z W o', Gl 7C � A i cz ct) a Z' ID 0 r� ❑ !3 V m m u1 V of n L 10 m 1 0 is L 0 (A ? �S r g; mLLX01 n � � cLLm n n �{ m � Z O L r c A C �LLr Z Znc 1p m L rl e N cl a =LLO a m v L �I n N (�d r l -J CL a m � m a Ee CL 51 `mc �o v sa � m 5 fa d m ID to W vO �o n� z 70 w � �R ti m mg 'mom O S mS cr g W v O ro'ga tr 21 cr Q � � c a a 3 m SO�LO�EL d1MM NaelpAsaim" Y) unnol MUO Page 14 of 15 n a v hm �m a N to m m -0 a V O a o��Dro� if h J1 C �1 0 0. 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