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HomeMy WebLinkAboutNCG551408_2023 Effluent Sampling Report_20240117ENVIRONMENTAL - WATER SUPPLY - WASTEWATER - GEOTHERMAL CONNER CONSULTING, LLC 12284 WINDY RIDGE ROAD, CHAPEL HILL, NORTH CAROLINA 27517 PHONE: (919) 260.7301 .............................................................................. .............................................................................. January 17, 2024 Mr. Elijah Lawrence NCG551408 8923 Walnut Grove Church Road Hurdle Mills, North Carolina 27541 Re: Effluent Sampling Residence 8923 Walnut Grove Church Road Hurdle Mills, Orange County Dear Mr. Lawrence: On November 30, 2023, Conner Consulting collected effluent samples as required on your septic system permit at 8923 Walnut Grove Church Road. The results (attached) are as follows: Flow Estimate Total Residual Chlorine: Ammonia BOD TSS Fecal Coliform TKN Nitrate/Nitrite Total Nitrogen Phosphorus <200 gallons per day 1.9 ppm @ 13:10 57 ppm 31 mg/L 7.1 mg/L >2400 cfa 120 ppm <0.041 ppm 120 ppm 5.2 ppm My recommendation is to add chlorine tablets more frequently. My field laboratory certification is #5149. Please call with questions and comments. Sincerely yours, Chad Leinbach Conner Consulting, LLC Field Laboratory Certification #5149 ti eurofins � Environment Testing I ANALYTICAL REPORT C PREPARED FOR Attn: Chad Leinbach Conner Consulting 1284 WINDY RIDGE RD C CHAPEL HILL, North Carolina 27517 Generated 12/8/2023 1 :24:24 PM JOB DESCRIPTION 8923 Walnut Grove Church Rd. JOB NUMBER 752-14159-1 This report may not be reproduced except in full, and with written approval from the laboratory. The results relate only to the samples tested. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. L The test results in this report relate only to the samples as received by the laboratory and will meet all requirements of the methodology, with any exceptions noted. This report shall not be reproduced except in full, without the express written approval of the laboratory. All questions should be directed to the Eurofins Environment Testing Southeast, LLC Project Manager. Generated 12/8/2023 1:24:24 PM Authorized for release by Amanda Gaines, Project Manager amanda.gaines@et.eurofinsus.com (919)677-1669 Eurofins Savannah is a laboratory within Eurofins Environment Testing Southeast, LLC, a company within Eurofins Environment Testing Group of Companies Page 2 of 21 12/8/2023 Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Table of Contents Laboratory Job ID: 752-14159-1 e Cover Page .............................................. 1 Table of Contents ......................................... 3 Definitions/Glossary....................................... 4 L Case Narrative ........................................... 5 Detection Summary ........................................ 6 Client Sample Results ...................................... 7 QC Sample Results ........................................ 8 QC Association Summary ................................... 11 Lab Chronicle ............................................ 13 C Certification Summary ...................................... 14 Method Summary ......................................... 15 Sample Summary ......................................... 16 Chain of Custody .......................................... 17 Receipt Checklists ......................................... 20 Eurofins Raleigh Page 3 of 21 12/8/2023 Definitions/Glossary Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Qualifiers General Chemistry Qualifier Qualifier Description LCS and/or LCSD is outside acceptance limits, low biased. '1 LCS/LCSD RPD exceeds control limits. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. c Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) oil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive / Present PQL Practical Quantitation Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count F Job ID: 752-14159-1 Eurofins Raleigh Page 4 of 21 12/8/2023 Case Narrative Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Job ID: 752-14159-1 Job ID: 752-14159-1 Laboratory: Eurofins Raleigh i Narrative Job Narrative 752-14159-1 Analytical test results meet all requirements of the associated regulatory program listed on the Accreditation/Certification Summary Page unless otherwise noted under the individual analysis. Data qualifiers are applied to indicate exceptions. Noncompliant quality control (QC) is further explained in narrative comments. Matrix QC may not be reported if insufficient sample or site -specific QC samples were not submitted. In these situations, to E: demonstrate precision and accuracy at a batch level, a LCS/LCSD may be performed, unless otherwise specified in the method. Surrogate and/or isotope dilution analyte recoveries (if applicable) which are outside of the QC window are confirmed unless attributed to a dilution or otherwise noted in the narrative. Regulated compliance samples (e.g. SDWA, NPDES) must comply with the associated agency requirements/permits. Receipt The sample was received on 11/30/2023 2:40 PM. Unless otherwise noted below, the sample arrived in good condition, and, where required, properly preserved and on ice. The temperature of the cooler at receipt time was 5.7°C General Chemistry E Method 353.2: The RPD of the laboratory control sample (LCS) and laboratory control sample duplicate (LCSD) for analytical batch 752-5384 recovered outside control limits for the following analytes: Nitrate Nitrite as N. Method SM5210B_Calc: The glucose-glutamic acid standard (LCS) recovered outside the recovery limits specified in the method in batch 752-5434. The method holding time had expired, therefore the analysis was not repeated. The data was qualified and reported. No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Biology No additional analytical or quality issues were noted, other than those described above or in the Definitions/ Glossary page. Eurofins Raleigh Page 5 of 21 12/8/20 g3 Detection Summary Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Client Sample ID: Eff.- 8923 Walnut Grove Church Rd. Analyte Result Qualifier Ammonia 57 Nitrogen, Kjeldahl 120 Phosphorus 5.2 Total Suspended Solids 7.1 Biochemical Oxygen Demand 31 *- Nitrogen, Total 120 Coliform, Fecal >2400 This Detection Summary does not include radiochemical test results. Job ID: 752-14159-1 Lab Sample ID: 752-14159-1 RL MDL Unit Dil Fac D Method Prep Type 2.6 1.0 mg/L 51.43 350.1 Total/NA 10 5.0 mg/L 50 351.2 Total/NA 0.50 0.21 mg/L 5 365.4-1974 Total/NA 3.8 3.8 mg/L 1 SM 2540D Total/NA 2.0 2.0 mg/L 1 SM 5210B Total/NA 0.25 0.25 mg/L 1 Total Nitrogen Total/NA 1.0 1.0 MPN/100ml- 1 Coliform Total/NA Eurofins Raleigh Page 6 of 21 12/8/2023 Client Sample Results Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. F Job ID: 752-14159-1 Client Sample ID: Eff.- 8923 Walnut Grove Church Rd. Lab Sample ID: 752-14159-1 Date Collected: 11/30/23 13:00 Matrix: Water Date Received: 11/30/23 14:40 General Chemistry Analyte Result Qualifier Ammonia (EPA 350.1) 57 Nitrogen, Kjeldahl (EPA 351.2) 120 Nitrate Nitrite as N (EPA 353.2) <0.041 *1 Phosphorus (EPA 365.4-1974) 5.2 Total Suspended Solids (SM 7.1 2540D) Biochemical Oxygen Demand (SM 31- 5210B) Nitrogen, Total (EPA Total 120 Nitrogen) Method: IDEXX Coliform - Coliforms, Fecal Analyte Result Qualifier Coliform, Fecal >2400 RL MDL Unit D Prepared Analyzed Dil Fac 2.6 1.0 mg/L 12/05/2314:42 51.43 10 5.0 mg/L 12/04/2311:21 12/05/2310:44 50 0.10 0.041 mg/L 12/04/2311:55 Y 1 0.50 0.21 mg/L 12/04/23 11:21 12/05/23 08:15 5 3.8 3.8 mg/L 12/05/23 09:53 1 2.0 2.0 mg/L 12/01/2315:24 1 C 0.25 0.25 mg/L 12/05/2313:05 1 RL 1.0 MDL Unit D Prepared 1.0 MPN/100ml- Analyzed Dil Fac 11/30/23 16:05 1 Page 7 of 21 Eurofins Raleigh 12/8/2023 QC Sample Results Client: Conner Consulting Job ID: 752-14159-1 Project/Site: 8923 Walnut Grove Church Rd. Method: 350.1 - Nitrogen, Ammonia Lab Sample ID: MB 752-5432/10 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 5432 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Ammonia <0.020 0.050 0.020 mg/L 12/05/2311:18 1 FLab Sample ID: MB 752-5432/40 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 5432 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Ammonia <0.020 0.050 0.020 mg/L 12/05/2313:28 1 Lab Sample ID: LCS 752-5432/11 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 5432 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Ammonia 1.02 1.00 mg/L 99 90 -110 Lab Sample ID: LCS 752-5432141 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 5432 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Ammonia 1.02 0.980 mg/L 96 90 - 110 Method: 351.2 - Nitrogen, Total Kjeldahl Lab Sample ID: MB 680-811350/13-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 811582 Prep Batch: 811350 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Nitrogen, Kjeldahl <0.10 0.20 0.10 mg/L 12/04/23 11:21 12/05/23 09:33 1 Lab Sample ID: LCS 680-811350/14-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 811582 Prep Batch: 811350 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Nitrogen, Kjeldahl 2.00 2.06 mg/L 103 75 - 125 Method: 353.2 - Nitrogen, Nitrate -Nitrite Lab Sample ID: MB 752-5384132 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 5384 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Nitrate Nitrite as N <0.041 0.10 0.041 mg/L 12/04/23 11:24 1 Page 8 of 21 Eurofins Raleigh 12/8/2023 QC Sample Results Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Method: 353.2 - Nitrogen, Nitrate -Nitrite (Continued) FLab Sample ID: MB 752-5384/64 Matrix: Water Analysis Batch: 5384 MB MB Analyte Result Qualifier Nitrate Nitrite as N <0.041 Lab Sample ID: LCS 752-5384/33 Matrix: Water Analysis Batch: 5384 Spike Added �Analyte Nitrate Nitrite as N 1.25 Lab Sample ID: LCS 752-5384/65 Matrix: Water Analysis Batch: 5384 Spike Analyte Added Nitrate Nitrite as N 1.25 Lab Sample ID: LCSD 752-5384/89 Matrix: Water Analysis Batch: 5384 Spike Analyte Added Nitrate Nitrite as N 1.25 Method: 365.4-1974 - Phosphorus, Total F Job ID: 752-14159-1 Client Sample ID: Method Blank Prep Type: Total/NA RL MDL Unit L D Prepared Analyzed Dil Fac 0.10 0.041 mg/L 12/04/2312:35 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS %Rec Result Qualifier Unit D °/Rec Limits 1.22 mg/L 98 90 - 11 o Client Sample ID: Lab Control Sample Prep Type: Total/NA LCS LCS %Rec Result Qualifier Unit D %Rec Limits 1.19 mg/L 95 90 -110 Client Sample ID: Lab Control Sample Dup Prep Type: Total/NA LCSD LCSD %Rec RPD Result Qualifier Unit D %Rec Limits RPD Limit 1.34 '1 mg/L 107 90 - 110 12 10 Lab Sample ID: MB 680-811350/13-A Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 811583 Prep Batch: 811350 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Phosphorus <0.041 0.10 0.041 mg/L 12/04/23 11:21 12/05/23 07:11 1 Lab Sample ID: LCS 680-811350/14-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 811583 Prep Batch: 811350 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Phosphorus 2.00 1.91 mg/L 95 90 -110 Method: SM 2540D - Solids, Total Suspended (TSS) Lab Sample ID: MB 752-539211 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 5392 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Suspended Solids <2.5 2.5 2.5 mg/L 12/05/23 09:53 1 Eurofins Raleigh Page 9 of 21 12/8/2023 QC Sample Results Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Method: SM 2540D - Solids, Total Suspended (TSS) (Continued) Lab Sample ID: LCS 752-5392/2 Matrix: Water Analysis Batch: 5392 Spike LCS LCS Analyte Added Result Qualifier Unit Total Suspended Solids 100 92.0 mg/L Method: SM 5210B - BOD, 5-Day Lab Sample ID: SCB 752-5434/2 Matrix: Water Analysis Batch: 5434 Analyte Biochemical Oxygen Demand Lab Sample ID: USB 752-5434/1 Matrix: Water Analysis Batch: 5434 Analyte Biochemical Oxygen Demand Lab Sample ID: LCS 752-5434/3 Matrix: Water Analysis Batch: 5434 Analyte Biochemical Oxygen Demand SCB SCB Result Qualifier RL MDL Unit 0.856 0.0000020 0.0000020 mg/L USB USB Result Qualifier RL MDL Unit 0.190 0.0000020 0.0000020 mg/L Spike LCS LCS Added Result Qualifier Unit 198 157 `- mg/L F Job ID: 752-14159-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec L D %Rec Limits 92 80 - 120 Y Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 12/01 /23 14:50 1 Client Sample ID: Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 12/01 /23 14:48 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA %Rec D %Rec Limits 79 85-115 Page 10 of 21 Eurofins Raleigh 12/8/2023 QC Association Summary Client: Conner Consulting Job ID: 752-14159-1 Project/Site: 8923 Walnut Grove Church Rd. General Chemistry Analysis Batch: 5384 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water 353.2 MB 752-5384/32 Method Blank Total/NA Water 353.2 MB 752-5384/64 Method Blank Total/NA Water 353.2 LCS 752-5384/33 Lab Control Sample Total/NA Water 353.2 LCS 752-5384/65 Lab Control Sample Total/NA Water 353.2 LCSD 752-5384/89 Lab Control Sample Dup Total/NA Water 353.2 Analysis Batch: 5392 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water SM 2540D MB 752-5392/1 Method Blank Total/NA Water SM 2540D LCS 752-5392/2 Lab Control Sample Total/NA Water SM 2540D Analysis Batch: 5432 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water 350.1 MB 752-5432/10 Method Blank Total/NA Water 350.1 MB 752-5432/40 Method Blank Total/NA Water 350.1 LCS 752-5432/11 Lab Control Sample Total/NA Water 350.1 LCS 752-5432/41 Lab Control Sample Total/NA Water 350.1 Analysis Batch: 5434 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water SM 5210B SCB 752-5434/2 Method Blank Total/NA Water SM 5210B USB 752-5434/1 Method Blank Total/NA Water SM 5210B LCS 752-5434/3 Lab Control Sample Total/NA Water SM 5210B Prep Batch: 811350 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water Digestion MB 680-811350/13-A Method Blank Total/NA Water Digestion LCS 680-811350/14-A Lab Control Sample Total/NA Water Digestion Analysis Batch: 811387 CLab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water Total Nitrogen Analysis Batch: 811582 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water 351.2 811350 MB 680-811350113-A Method Blank Total/NA Water 351.2 811350 LCS 680-811350/14-A Lab Control Sample Total/NA Water 351.2 811350 Analysis Batch: 811583 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Total/NA Water 365.4-1974 811350 MB 680-811350/13-A Method Blank Total/NA Water 365.4-1974 811350 LCS 680-811350/14-A Lab Control Sample Total/NA Water 365.4-1974 811350 Eurofins Raleigh Page 11 of 21 12/8/2023 QC Association Summary Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Biology Analysis Batch: 5355 Lab Sample ID Client Sample ID 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Prep Type Matrix Total/NA Water F Job ID: 752-14159-1 Method Prep Batch Coliform L 0 Page 12 of 21 Eurofins Raleigh 12/8/2023 Lab Chronicle Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Job ID: 752-14159-1 Client Sample ID: Eff.- 8923 Walnut Grove Church Rd. Lab Sample ID: 752-14159-1 Date Collected: 11/30/23 13:00 Matrix: Water Date Received: 11/30/23 14:40 Prep Type Batch Type Batch Method Run Dilution Factor Batch Number Analyst Lab Prepared or Analyzed Total/NA Analysis 350.1 51.43 5432 ME EET ESC 12/05/23 14:42 Total/NA Prep Digestion 811350 SM EET SAV 12/04/23 11:21 Total/NA Analysis 351.2 50 811582 AS EET SAV 12/05/23 10:44 Total/NA Analysis 353.2 1 5384 ME EET ESC 12/04/23 11:55 Total/NA Prep Digestion 811350 SM EET SAV 12/04/23 11:21 Total/NA Analysis 365.4-1974 5 811583 AS EET SAV 12/05/23 08:15 Total/NA Analysis SM 2540D 1 5392 CB EET ESC 12/05/23 09:53 Total/NA Analysis SM 5210B 1 5434 JC EET ESC 12/01/23 15:24 Total/NA Analysis Total Nitrogen 1 811387 TJW EET SAV 12/05/23 13:05 Total/NA Analysis Coliform 1 5355 CB EET ESC 11/30/23 16:05 - 12/01/23 10:19' This procedure uses a method stipulated length of time for the process. Both start and end times are displayed. Laboratory References: EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL (919)677-1669 EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 E Eurofins Raleigh Page 13 of 21 12/8/2023 Accreditation/Certification Summary Client: Conner Consulting Job ID: 752-14159-1 Project/Site: 8923 Walnut Grove Church Rd. Laboratory: Eurofins Raleigh The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WW/SW) State 591 12-31-23 Laboratory: Eurofins Savannah Unless otherwise noted, all analytes for this laboratory were covered under each accreditation/certification below. Authority Program Identification Number Expiration Date North Carolina (WW/SW) State 269 12-31-23 The following analytes are included in this report, but the laboratory is not certified by the governing authority. This list may include analytes for which the agency does not offer certification. Analysis Method Prep Method Matrix Analyte Total Nitrogen Water Nitrogen, Total 10 Eurofins Raleigh Page 14 of 21 12/8/2023 Method Summary Client: Conner Consulting Job ID: 752-14159-1 Project/Site: 8923 Walnut Grove Church Rd. Method Method Description Protocol Laboratory 350.1 Nitrogen, Ammonia EPA EET ESC 351.2 Nitrogen, Total Kjeldahl EPA EET SAV 353.2 Nitrogen, Nitrate -Nitrite EPA EET ESC 365.4-1974 Phosphorus, Total EPA EET SAV SM 2540D Solids, Total Suspended (TSS) SM EET ESC SM 5210B BOD, 5-Day SM EET ESC Total Nitrogen Nitrogen, Total EPA EET SAV Coliform Coliforms, Fecal IDEXX EET ESC Digestion Digestion, Hot Block EPA EET SAV Protocol References: EPA = US Environmental Protection Agency IDEXX = IDEXX Laboratories SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: EET ESC = Eurofins Raleigh, 102-A Woodwinds Industrial Court, Cary, NC 27511, TEL (919)677-1669 EET SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Raleigh Page 15 of 21 12/8/2023 Sample Summary Client: Conner Consulting Project/Site: 8923 Walnut Grove Church Rd. Lab Sample ID Client Sample ID Matrix 752-14159-1 Eff.- 8923 Walnut Grove Church Rd. Water Collected Received 11 /30/23 13:00 11 /30/23 14:40 Job ID: 752-14159-1 Page 16 of 21 Eurofins Raleigh 12/8/20 g3 T O C.1 43 U O C r C p Y V m o e�g°m fps m my (N�mN U� R ) `�q N� V �ZpC+.UfG uyF } �Y N a may. C` U ti Eg r C ¢ Z Up ¢ b0 E �0¢0 z Iq a1 az`Nz¢wwDIN w � m Q c E E_ o m y % fv P Q , � K Pm4 a U h & R < c c c a a o a 0 0 a 2 c� U U U o a is T u to pi o v � a � o x � r Lfnj l ViT o ro o a si ID 7- Page 17 of 21 12/8/2023 Eurofins Raleigh 102-A Woodwinds Industrial Court tiff eurofins Cary NC27511 Chaim of Custody Record Environment Testing Phone: 919-677-1669 Sampler Lab PM: Caller Tracking No(s): COG No: Client Information Sub Contract Lab Gaines, Amanda 752-1942.1 Client Contact Phone: E-Mail; State of Origin: Page: .Shipping/Receiving amanda.gaines@et.eurofinsus.com North Carolina Page 1 of 1 Company: Accreditations Required (See note): Job #: Eurofins Environment Testing Southeast, State North Carolina (WWlSW) 752-14159-1 Address. Due Date Requested: preservation Codes: 5102 LaRoche Avenue, 12/11/2023 Analysis Requested A HCL M Hexane N None B N30H City: TAT Requested (days): ��� t Savannah - M i` O ASNa02 C ZnAcehLe P Na204S D Nitric Acid Q Na2S03 Zip: State,ZE : GA, 31404 �}t� �� - fs� z, E NaHSO4 R Na252o3 F McOW PO #: Phone: 912-354 7858{Tel} 912-352-0165(Fax) f Y` , 9 r E`� t; ; �� S H2SO4 G Amchlor T TSP Dodecahydrate H Ascorbic Acid Email: WO#: w of }- U Acetone I ICs V MCAA 6' m lei K EDTAr W pH 4-5 Project Name: Project #: n ar 2 Z Y Trizma L EDA Eff. 8923 Walnut Grove Church Rd 75201353 iL f Z other (specify) Sit-: SSOW#:E'•.. m R m u` Other' o n [ I I I Sample Matrix Type Sample (C=comp, o.w..—a of Imo? N p ?1 Sample Identification Client ID Lab ID Sample Date Time G= rab) ST-Te.u...MMr 'w' E 2 p Special InstructionslNote: )) 9t- }}i3 1 Cf �i. ii 4:} ��Sri � is yyf �:� 1, �iR ., .-�� � a) a�4'i�<h.,�...�L.L. ==,f., _. , „ s,-, l.E2r. 5,���;: .. fi iSS ��/,��� l 0�.,. ? �� Eff 8923 Walnut Grove Church Rd {752-14159-1) 11/30/23 13:00 Water X X X Eastern t fit: 2 1 Ni „ }rzzi// ft 44�. �aEh� Note: Since laboratory aocreditations are subject to change, Eurofins Environment Testing Southeast, LLC places the ownership of method, analyte & accreditation compliance upon our subcontract laboratories. This sample shipment is forwarded underchain-of-custody. If the laboratory does not currently maintain accreditation in the State of Origin listed above for analysishestslmabix being analyzed, the samples must be shipped back to the Eurofins Environment Testing Southeast, LLC laboratory or other Instructions will be provided. Any changes to accreditation status should be brought to Eurofins Environment Testing Southeast, LLC attention immedlately. I£ all requested accreditations are current to dale, return the Signed Chain of Custody attesting to said compliance to Eurofins Environment Testing Southeast, LLC. Possible Hazard identification Sample Disposal (A fee may be assessed if samples are retained longer than 1 month) Unconfirmed = Return To Client © Disposal By Lab © Archive For Months Deliverable Requested: 1 11, III 1V Other (specify) Primary Deliverable Rank: 2 Special Instructions= Requirements: Empty Kit Relinquished by: Date: Time: Method of Shipment: Relinquished by. Daterif e: I2 Company ReOeive Da 'me: I Company t 3 Relinquished by Daterrime: Company Received by. DateMme: ..-y Company Relinquished by DateMme: Company Received by. DateMme: Company Custody Seals Intact Custody Seal No. Cooler Temperature{s) °C and Other Remarks: c� A Yes , No Page 18 of 21 vcr• 015108/2(�?P/8/2023 Eurofins Raleigh 102-A Woodwinds Industrial Court Phone: NC 27511 Phone: 9 „ 677 1669 Chain of Custody Record tiff eurofins Environment Felting Sampler Lab PM: Carrier TracJ ing No(s): COC No: Client Information Sub Contract Lab Bechtold, Chad 752-1937.2 Client Contact Phone: E-Mail: State of Origin: Page: Shipping/Receiving Chad.Bechto)d@et.eurofinsus,com North Carolina Page 2 of 2 Company: Accreditation Required (See note): Job P. Eurofins Environment Testing Southeast, State North Carolina (WW/SW) 752-14145-1 Address: Rue Date Requested: Preservation Codes: 5102 LaRoche Avenue, 12/13/2023 Anal ysisRequested A HCL M Hexane 9 NaOH N None City: TAT Requested (days): Savannah t ': , �t` o As C� lvao2 D Nitric Acid P Na204S 0 Na2SO3 State, Zip: GA, 31404 i ` 'm. E NaHsOa R Na25203 G Amchlor S H2SO4 Phone: PO#: 912-354-7858(Tel) 912-352-0165(Fax) o p t� aF rn Y�,ii; H Ascorbic Acid T TSP D�ecahydrate I ice i Di Water V MCPA Email: WO#: ,F m _tm4; L EK EDTA W pH 4-5ts) DA Y Ttixma Project Name: Project #. Duke Sparks 75202352 t z other (specify) 511e: WOW*� 'r?�; A y Y {6i � other P Sample MatrixType m p;: Sample (C comp, a.w..moll, m4: Sample Identification Client 1D Lab ID) Sample Date Time G= rab aT• b�w,Anglr xt(i W Special Instructions/Note: '. }gt .. � '�i�. Z t' �, . '1111�4 . OPT 1 (6-7) (752-14145-1) 11/29/23 14:00 Solid East m DPT-2 5-6 752-14145-2 11129/23 14:50 Solid Eastem ESSED-1 (752-14145-3) 11129/23 13:00 Solid is Eastern SW-1 {752-141454) 11/29123 11:45 Eestem Water SW-2 (752-14145-5) 11/29123 12:30 Water m C-N (0-2) (752-14145-6) 11/29/23 11 OS Solid X m C-S (0-2) (752-14145-7) 11/29/23 11 10rrt Solid X Trip Blank (752-14145-8) 11/29123 11:05 Water Eastern' 3 Note: Since laboratory accreditation are subject to change, Eurofins Environment Testing Southeast, LLC places the ownership of method, analyta & axreditation compliance upon our subcontract laboratories. This sample shipment is forwarded under chain -of -custody. if tho laboratory does not currently maintain accreditation in the State of Origin listed above for ana€ysisitestslmatdx being analyzed, the samples must be shipped back to the Eurofins Environment Testing Southeast, LLC laboratory or other instructions will be provided. Any changes to accreditation status should be brought to Eurofins Enviranment Testing Southeast, LLC attention immediately. If all requested accreditation are current to date, realm the signed Chain of Custody attesting to said compliance to Eurofins Environment Testing Southeast, LLC. Possible Hazard lderWrica#ion Sample Disposal ( q fee may be assessed if samples are retained longer than 1 month) Unconfirmed © Retum To Client = Disposal ?2 Lab Archive For Months Deliverable Requested. I, 11, Ill IV Other (specify) Primary Deliverable Rank: 2 Special Instructions/QC Requirements: Empty Kit Relinquished by' Date: Time: Method of Shipment: Relinquished by: DIM e: Company Received Date e: Company Relinquished by: Date/Time: Company Received by: Date/rii ee, Company J *t z Relinquished by: DateTme: Company Received by oate7rme: Company Custody Seals Intact: Custody Seal No. Cooler Temperatures)'C and Other Remarks: , -I G Yes e No e Page 19 of 21 ver"'I"' :19t2/8/2023 Login Sample Receipt Checklist Client: Conner Consulting Login Number: 14159 List Number: 1 Creator: Hyatt, Samantha Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey True meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. True Job Number: 752-14159-1 List Source: Eurofins Raleigh L m Eurofins Raleigh Page 20 of 21 12/8/2023 Login Sample Receipt Checklist Client: Conner Consulting Job Number: 752-14159-1 Login Number: 14159 List Number: 2 Creator: Harley, Tynisha Question List Source: Eurofins Savannah List Creation: 12/01/23 01:12 PM Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True m HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Raleigh Page 21 of 21 12/8/2023