NC0004987_Appendix B_Receptor Survey Update_20150908

Receptor Information
• Updated Receptor Survey Report
• NCDENR Well Water Sampling Results
• NCDENR Water Supply Well Tracking
Spreadsheet
• Background Water Supply Well
Analytical Results

Updated Receptor Survey Report
Marshall Steam Station Ash Basin
NCDENR Records Review
HDR reviewed the NCDENR Department of Environmental Health (DEH) Public Water Supply
Section's (PWSS) Public Water Supply Water Sources Geographic Information System (GIS)
point data set (pwsws.shp) obtained from the NC OneMap GeoSpatial Portal
(http://data.nconemap.com/geoportal/catalog/main/home.page) to identify public water supply
sources within a 0.5-mile radius of the Marshall ash basin compliance boundary.
On July 20, 2015, HDR reviewed the NCDENR DWR Source Water Assessment Program
(SWAP) online database for public water supply sources to identify any wells located within a
0.5-mile radius of the ash basin compliance boundary, confirm the location of wells included in
the Public Water Supply Water Sources GIS point data set, and identify any wellhead protection
areas located within a 0.5-mile radius of the compliance boundary. The NCDENR SWAP
database provides detailed assessments of all public drinking water intakes and wellhead
protection areas in North Carolina. The website address is:
(http://swap.ncwater.org/website/swap/viewer.htm.).
On July 20, 2015, Mr. Brian Booth with HDR contacted Mr. Sean McGuire, GIS Specialist with
the NCDENR PWSS, by telephone. Mr. McGuire stated that as of July 20, 2015, the data
contained in the Public Water Supply Water Sources GIS point data set obtained from the NC
OneMap GeoSpatial Portal was current through November 18, 2009. The most current GIS data
set of public water supply locations available from North Carolina state agencies was acquired
and reviewed by HDR on July 20, 2015. The current data matches the previous data obtained
from the NC OneMap GeoSpatial Portal. This new data set is current through June 2015. The
most current data is available by request. The GIS point data for the public water supply wells
includes, but is not limited to information such as public water supply (PWS) system
identification numbers, ownership information, PWS source type, well depth, and well yield. Mr.
McGuire indicated the Public Water Supply Water Sources GIS point data set and the SWAP
online database was in the process of being updated.
Three public water supply wells were identified in the Public Water Supply Water Sources GIS
point data set or on the NCDENR SWAP online database within a 0.5-mile radius of the
Marshall ash basin compliance boundary.
No wellhead protection areas were identified on the NCDENR SWAP online database within a
0.5-mile radius of the Marshall ash basin compliance boundary.

Catawba County Records Review
On July 27, 2015, Mr. Coleman Marchin with HDR contacted Mr. Mike Cash, with the Catawba
County Public Health Department to inquire about the location and details (if available) for
registered water supply wells located in Catawba County within a 0.5-mile radius of the ash
basin compliance boundary. On July 29, 2015, Mr. Mike Cash with Catawba County Public
Health Department contacted Mr. Coleman Marchin with HDR to confirm there are no records of
any changes to private or public water supply wells located within a 0.5-mile radius of the ash
basin compliance boundary. In addition, Mr. Marchin also contacted Mr. Jonathan Greer with
the Catawba County Utilities and Engineering Department to verify any changes to the
municipal water supply system within 0.5-miles of the Marshall ash basin compliance boundary.
According to Mr. Greer, no new installations or changes to the municipal water supply system in
the vicinity of the Marshall ash basin were noted.
Public Water Supplier Records Review
HDR contacted the City of Hickory to inquire about municipal water supply to properties located
in their service area within a 0.5-mile radius of the ash basin compliance boundary. On July 28,
2015, Mr. Coleman Marchin with HDR spoke with Ms. Tracy Church of the City of Hickory
Planning and Development Department, regarding the extent of the municipal water service.
Ms. Church confirmed that the City of Hickory provides municipal water service to the MSS site
and properties located to the west along Sherrills Ford Road and north of the site along Island
Point Road; however the major recipients of public water in the vicinity of the MSS are located in
recently constructed homes and subdivisions.
Water Supply Well Survey Questionnaires
Six questionnaire responses were received by HDR after October 31, 2014. Of the six
responses, only one previously unidentified water supply well was verified by the owner's
response. The remaining responses indicated that the subject property was on municipal water
provided by the City of Hickory or there was no well present on the property.

NCDENR Well Water Sampling Results

Marshall Steam Station Receptor Survey Vendor Data
Sample ID
OrderlD
Well ID
Sample Date
Laboratory
Reported Date
2015005737
J15020155
weIIMR-4
2/5/2015
Shealy
3/10/2015
2015005738
J15020155
weIIMR-9
2/5/2015
Shealy
3/10/2015
2015005739
J15020155
weIIMR-12
2/5/2015
Shealy
3/10/2015
2015005740
J15020155
weIIMR-14
2/5/2015
Shealy
3/10/2015
2015005741
J15020155
weIIMR-17
2/5/2015
Shealy
3/10/2015
2015005742
J15020155
weIIMR-18
2/5/2015
Shealy
3/10/2015
2015005743
J15020155
weIIMR-20
2/5/2015
Shealy
3/10/2015
2015005744
J15020155
weIIMR-21
2/5/2015
Shealy
3/10/2015
2015006724
J15020411
weIIMR23
2/12/2015
R&C
3/16/2015
2015007834
J15020411
1R23 - State wE
2/12/2015
State
3/24/2015
2015006725
J15020411
weIIMR26
2/12/2015
R&C
3/16/2015
2015007835
J15020411
IR26 - State w
2/12/2015
State
3/24/2015
Test
Parameter
AnalyticalWethod
Limits
Source
units
MRX
MRrSO
MR112
MR114
MR117
MR118
MR20
MR21
WRr23
WRr23
MR26
MRr26
Anions
Chloride
EPA 300.0
250
2L
mg/L
55
1.3
2.3
2.3
1.4
3.3
3.3
4
< 5
25
2.68
3.4
Anions
Sulfate
EPA 300.0
250
2L
mg/L
< 1
< 1
< 1
< 1
< 1
1.6
1.3
< 1
< 1
< 2
1.12
< 2
ICP Metals
Aluminum (AI)
EPA 200.7
mg/L
< 0.04
< 0.04
< 0.2
< 0.04
< 0.04
< 0.2
< 0.2
< 0.2
< 0.05
< 0.05
< 0.05
< 0.05
ICP Metals
Barium (Ba)
EPA 200.7
0.7
2L
mg/L
0.37
0.018
0.034
0.049
0.012
< 0.025
0.014
0.082
0.11
0.13
0.056
0.057
ICP Metals
Boron (B)
EPA 200.7
0.7
2L
mg/L
< 0.025
< 0.025
< 0.13
< 0.025
< 0.025
< 0.13
< 0.13
< 0.13
< 0.1
< 0.05
< 0.1
< 0.05
ICP Metals
Calcium (Ca)
EPA 200.7
mg/L
41
7.3
6.5
9.1
9.6
12
28
2.7
20
23
7.7
8.1
ICP Metals
Chromium (Cr)
EPA 200.7
0.01
2L
mg/L
< 0.005
< 0.005
<M.025
< 0.005
< 0.005
<M.025
<M.025
<M.025
0.001
< 0.01
0.001
< 0.01
ICP Metals
Copper (Cu)
EPA 200.7
1
2L
mg/L
< 0.001
0.051
0.36
0.02
0.0055
0.084
0.13
0.013
0.022
0.018
0.009
0.0084
ICP Metals
Iron (Fe)
EPA 200.7
0.3
2L
mg/L
1.2
0.18
0.33
0.21
0.24
0.5
1.1
0.19
< 0.05
< 0.05
< 0.05
< 0.05
ICP Metals
Magnesium (Mg)
EPA 200.7
mg/L
12
1.3
1.5
2.3
2.5
3
5.4
1.5
5.4
6.2
2.7
3
ICP Metals
Manganese (Mn)
EPA 200.7
0.05
2L
mg/L
0.03
< 0.005
0.053
< 0.005
< 0.005
< 0.025
< 0.025
0.034
< 0.005
< 0.01
< 0.005
< 0.01
ICP Metals
Nickel (Ni)
EPA 200.7
0.1
2L
mg/L
< 0.005
< 0.005
< 0.025
< 0.005
< 0.005
< 0.025
< 0.025
< 0.025
< 0.005
< 0.002
< 0.005
< 0.002
ICP Metals
Potassium (K)
EPA 200.7
mg/L
5
0.77
2.2
1.9
1.9
2.7
3
1.7
3
3.8
2
2.4
ICP Metals
Sodium (Na)
EPA 200.7
mg/L
19
6.5
10
6.4
5
13
14
2.5
16
18
6.8
7.1
ICP Metals
Strontium (Sr)
EPA 200.7
mg/L
0.58
0.081
0.099
0.077
0.16
0.24
0.17
< 0.05
0.27
0.28
0.17
0.16
ICP Metals
Zinc (Zn)
EPA 200.7
1
2L
mg/L
< 0.01
0.15
0.06
0.016
< 0.01
< 0.05
< 0.05
< 0.05
0.082
0.059
0.007
< 0.01
IMS Metals
Antimony (Sb)
EPA 200.8
1
(IMAC)
ug/L
< 1
< 1
< 1
< 1
< 1
«
< 1
< 1
< 1
«0
< 1
<M0
IMS Metals
Arsenic (As)
EPA 200.8
10
2L
ug/L
< 1
< 1
< 5
< 1
< 1
< 5
< 5
< 5
< 5
< 2
< 5
< 2
IMS Metals
Beryllium (Be)
EPA 200.8
4
(IMAC)
ug/L
< 0.4
< 0.4
< 2
< 0.4
< 0.4
< 2
< 2
< 2
< 1
<3
< 1
<Q,
IMS Metals
Cadmium (Cd)
EPA 200.8
2
2L
ug/L
0.12
< 0.1
< 0.1
< 0.1
< 0.1
< 0.5
< 0.1
< 0.5
< 0.1
< 0.5
< 0.1
< 0.5
IMS Metals
Cobalt (Co)
EPA 200.8
1
(IMAC)
ug/L
«
«
<125
«
«
<125
<125
<125
< 1
«0
< 1
«0
IMS Metals
Lead (Pb)
EPA 200.8
15
2L
ug/L
< 1
22
2.4
< 1
< 1
< 5
12
< 1
< 2
< 2
< 2
< 2
IMS Metals
Molybdenum (Mo)
EPA 200.8
ug/L
< 10
< 10
< 10
< 10
< 10
< 50
< 10
< 50
< 5
< 10
< 5
< 10
IMS Metals
Selenium (Se)
EPA 200.8
20
2L
ug/L
< 1
< 1
< 5
< 1
< 1
< 5
< 5
< 5
< 5
< 5
< 5
< 5
IMS Metals
Thallium (TI) Low Level
EPA 200.8
0.2
(IMAC)
ug/L
<M.5
<M.5
<M.5
<®.5
<M.5
<12.5
<3.5
<®.5
< 0.1
<l
< 0.1
IMS Metals
Vanadium (V) Low Level
EPA 200.8
0.3
(IMAC)
ug/L
«
5.8
«5
«
«
<125
<125
<[25
3
<35
3
<125
Wet Lab
Mercury (Hg)
EPA 245.1
1
2L
ug/L
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.2
< 0.2
< 0.2
< 0.2
Wet Lab
TDS
SM2540C
500
2L
mg/L
200
88
93
67
45
88
100
49
< 25
155
80
76
Wet Lab
TSS
SM2540D
mg/L
4.7
<1
<1
<1
<1
<1
<1
<1
<1
<6.2
<1
<6.2
Vendor Work
Alkalinity
(Vendor)
mg/L
86
29
34
37
38
43
71
< 10
52.9
54
< 5
Vendor Work
Bicarbonate Alkalinity
(Vendor)
mg/L
86
29
34
37
38
43
70
< 10
52.9
54
36.3
Vendor Work
Carbonate Alkalinity
(Vendor)
mg/L
< 10
< 10
< 10
< 10
< 10
< 10
< 10
< 10
0
< 1
0
Vendor Work
Hexavalent Chromium
(Vendor)
mg/L
< 0.02
< 0.02
< 0.02
< 0.02
< 0.02
< 0.02
< 0.02
< 0.02
< 0.01
< 0.05
< 0.01
Vendor Work
Conductivity
(Vendor)
umhos/cn
387
76
83
88
84
116
177
44
232
92.6
Vendor Work
Dissolved Oxygen
(Vendor)
mg/L
4.82
8.76
9.81
8.35
8.68
7.77
8.27
8.92
5.6
5.9
Vendor Work
pH
(Vendor)
su
7.09
6.73
6.75
6.7
7.13
7.18
7.81
6.11
6.1
6.5
6.2
Vendor Work
Temperature
(Vendor)
° C
14.1
14.4
12
10.3
10
11.2
11.1
14.5
18
18
17.2
Vendor Work
Turbidity
(Vendor)
NTU
2.5
< 1
< 1
< 1
< 1
< 1
< 1
< 1
< 1
< 1
< 1
Notes:
2L exceedance (highlighting added by HDR)
IMAC exceedance (highlighting added by HDR)
< n indicates results below laboratory reporting limit
Source: NCDENR 2015
38
38
<1
< 0.05
6.5
2.2
<1
Page 1

2015008294
J15020598
2015008295
J15020598
wellMR8
2015008296
J15020598
2015008297
J15020598
2015008787
J15020664
2015005988
J15030078
2015006017
J15030083
wellMR1
3/3/2015
Prism
4/20/2015
2015006018
J15030083
wellMR2-PlantwellMR2-Offic
3/3/2015
Prism
4/20/2015
2015006019
J15030083
3/3/2015
Prism
4/20/2015
2015006020
J15030083
wellMR25
3/3/2015
Prism
4/20/2015
2015013041
J15050027
MR-10
4/30/2015
Pace
5/18/2015
2015013043
J15050027
MR-22
4/30/2015
Pace
5/18/2015
2015013044
J15050027
MR-44
4/30/2015
Pace
5/18/2015
2015013045
J15050027
MR-11
4/30/2015
Pace
5/18/2015
2015013046
J15050027
MR-29
4/30/2015
Pace
5/18/2015
2015013047
J15050027
MR-28
4/30/2015
Pace
5/18/2015
2015015940
J15050647
MR33
5/21/2015
Pace
6/16/2015
2015015941
J15050647
MR35
5/21/2015
Pace
6/16/2015
wellMR6
wellMR16
wellMR30
wellMR32
wellMR13
2/18/2015
2/18/2015
2/18/2015
2/18/2015
2/23/2015
3/3/2015
Meritech
Meritech
Meritech
Meritech
R&C
R&AL
3/30/2015
3/30/2015
3/30/2015
3/30/2015
3/30/2015
4/13/2015
MRCS
MRS
MRC�16
MRSO
MRS2
MRC13
MRII
MRr2irlant
MRr2roffice
MRr25
MRC310
MRr22
MRA4
MRC11
MR29
MR128
MR33
MR35
4
2
7
1
5.72
1.9
7.2
< 1
1.2
7.8
2.4
2.3
1.6
1.3
1.5
14.3
2.9
1.4
<5
<5
16
5
<1
<10
11
4
<1
<1
<2
<2
<2
2
<2
2.4
<2
5
<0.05
<0.05
<0.05
<0.05
1.8
<0.05
<0.05
0.091
<0.05
<0.05
0.0246
<0.01
<0.01
<0.01
<0.01
<0.01
<0.01
0.0211
0.0529
0.0127
0.0868
0.0305
0.13
0.0114
0.013
0.13
0.031
0.047
0.0388
0.0793
0.033
0.0485
0.037
0.0445
0.0267
0.018
< 0.05
< 0.05
< 0.05
< 0.05
< 0.1
< 0.1
< 0.5
< 0.5
< 0.5
< 0.5
< 0.005
< 0.005
0.0051
< 0.005
< 0.005
< 0.005
< 0.005
< 0.005
9.98
7.81
19.9
13
15
3.46
5.2
22
5.4
10
5.13
< 0.04
9.06
< 0.04
< 0.04
< 0.04
4.51
< 0.04
< 0.002
< 0.002
< 0.002
0.00322
0.002
< 0.01
< 0.001
0.0021
0.0045
< 0.001
0.00099
0.00091
0.0012
0.00087
0.0029
0.001
0.001
< 0.0005
0.0568
0.0134
< 0.002
< 0.002
0.043
0.00953
< 0.005
0.0051
< 0.005
< 0.005
0.0033
0.0336
0.0085
0.0135
0.0119
0.0363
0.0113
0.0064
< 0.025
< 0.025
0.969
0.027
3.1
< 0.05
< 0.05
3.7
0.082
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
0.0654
2.42
1.67
4.08
2.23
1.8
1.09
1.4
3.8
1.8
3
0.804
1.2
2.13
0.584
0.915
2.5
0.831
3.27
< 0.002
< 0.002
0.131
< 0.002
0.13
< 0.01
< 0.005
0.05
< 0.005
< 0.005
0.0017
0.0038
0.00096
0.00072
0.0032
0.0044
< 0.0005
0.0235
< 0.0005
< 0.0005
< 0.0005
0.00061
< 0.005
< 0.01
< 0.002
< 0.002
< 0.002
< 0.002
< 0.0005
0.00055
< 0.0005
< 0.0005
0.00069
0.0011
< 0.0005
< 0.0005
2.13
1.57
2.49
1.74
3.5
1.52
1.3
3.4
2
2.3
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
< 0.05
9.28
7.25
4.89
9.26
5.4
3.82
10
7.8
5.6
12
5.43
< 0.05
8.34
< 0.05
< 0.05
8.06
5.08
7.18
0.309
0.05
0.103
0.163
0.11
0.106
0.028
0.26
0.1
0.11
0.059
0.0341
0.196
0.0782
0.106
0.162
0.0467
0.095
0.0336
0.0211
< 0.005
0.0501
0.118
< 0.01
0.34
0.2
0.72
0.039
< 0.005
< 0.005
< 0.005
0.0069
< 0.005
< 0.005
< 0.005
< 0.005
< 0.5
< 0.5
< 0.5
< 0.5
< 1
«
< 1
< 1
< 1
< 1
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
<2
<2
<2
<2
<5
<10
<1
<1
<1
<1
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 1
< 1
< 1
< 1
< 1
< 1
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
<0.15
<0.15
<0.15
<0.15
<0.1
<1
<1
<1
<1
<1
<0.08
<0.08
<0.08
<0.08
<0.08
<0.08
<0.08
<0.08
< 1
< 1
< 1
< 1
2
«r
< 1
< 1
< 1
< 1
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
0.65
0.78
< 0.5
< 0.5
8
< 5
< 1
4.1
32
< 1
0.7
2.4
0.33
0.43
0.28
1.2
0.44
1.4
< 2
2.8
< 2
< 2
< 5
< 10
< 2
< 2
< 2
< 2
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
1.3
<2
<2
<2
<2
<5
<10
<1
<1
<1
<1
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<0.5
<®.5
<CV.5
<®.5
<M.5
0.1
<Cl
< ZL
<a
< ZL
del
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
1.29
2.65
0.36
2.24
8
1.97
<CS
<CS
5.5
<C5
1.5
<CR
5.1
1
2.9
1.9
1.7
2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
119
95
125
68
106
56
58
130
68
150
65
55
93
71
59
< 25
57
96
< 2.5
< 2.5
< 2.5
< 2.5
105
< 5
< 3.1
< 3.1
< 3.3
< 3.3
< 2.5
< 2.5
< 2.6
< 2.5
< 5
< 2.5
< 2.5
< 2.5
38
36
53
49
32.3
19
17
87
31
53
< 5
< 5
< 5
< 5
< 5
< 5
< 5
54.5
32.3
19
17
87
31
53
<5
<5
<5
<5
<5
<5
<5
54.5
0
<1
<5
<5
<5
<5
<5
<5
<5
<5
<5
<5
<5
<5
< 0.005
< 0.005
< 0.005
< 0.005
< 0.01
< 0.02
< 0.01
< 0.01
< 0.01
< 0.01
0.00043
0.00056
0.00054
0.00052
0.0015
0.000064
0.0009
< 0.00003
135
106
196
191
117
63.6
63
149
60
104
64.2
62.4
103.4
86.9
45.7
130.4
61.7
143.3
8.39
7.98
4.77
5.41
6.6
4.44
13
5.5
6.9
7.7
7.6
8.2
6.6
7.7
7.6
6.6
7.9
1.8
5.98
6.33
7.12
6.36
6
7.36
6.4
7
6.2
5.8
6.0
5.7
6.2
6.5
6.3
6.2
6.2
7.3
12.3
12.7
15
15.6
18.8
10.7
7.4
15.6
14.6
12.9
16.5
16.2
16.9
17.6
16.4
16.6
18.1
16.5
< 1
< 1
4.9
< 1
28
<1
<1
3.9
<1
<1
<1
<1
3.2
<1
<1
<1
<1
<1
Page 2

2015015942
2015015943
2015016130
2015016131
2015016135
2015016726
2015016727
J15050647
J15050648
J15050681
J15050681
J15050682
J15050792
J15050792
MR37
MR21R
MR38
MR36
MR14R
MR43
MR45
5/21/2015
5/21/2015
5/22/2015
5/22/2015
5/22/2015
5/28/2015
5/28/2015
Pace
Pace
Pace
Pace
Pace
Pace
Pace
6/16/2015
6/16/2015
6/16/2015
6/16/2015
6/16/2015
6/16/2015
6/16/2015
MR37
MR21R
MR38
MR36
MR14R
MR43
MR45
5.3
4.1
1.5
2.7
2.3
1.6
6.2
<2
<2
<2
11.7
<2
<2
<2
<0.01
0.0251
<0.01
<0.01
<0.01
<0.01
0.0215
0.0323
0.0746
0.0917
< 0.0003
0.0495
0.043
0.127
< 0.005
< 0.005
< 0.005
< 0.005
< 0.005
< 0.005
< 0.005
< 0.04
< 0.04
< 0.04
< 0.04
9.68
5.01
3.53
0.0028
< 0.0005
0.0017
< 0.0005
0.00082
0.0048
0.001
0.0065
0.0041
0.0169
< 0.001
0.001
0.0149
0.0337
< 0.05
< 0.05
< 0.05
0.105
< 0.05
< 0.05
< 0.05
0.791
1.23
1.06
< 0.01
1.83
2.27
1.02
0.0041
0.0179
0.0053
0.00054
0.0015
0.0019
0.012
< 0.0005
0.00066
0.00051
< 0.0005
< 0.0005
0.0012
0.00097
< 0.05
< 0.05
< 0.05
0.155
1.94
< 0.05
2.36
< 0.05
< 0.05
< 0.05
33.5
5.85
5.72
4.6
0.0219
0.0097
0.036
< 0.0005
0.0853
0.0763
0.0374
< 0.005
< 0.005
< 0.005
< 0.005
< 0.005
0.0055
0.0422
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.2
< 0.2
0.21
< 0.2
< 0.2
< 0.2
< 0.2
< 0.08
< 0.08
< 0.08
< 0.08
< 0.08
< 0.08
< 0.08
< 0.5
0.75
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
0.24
0.2
0.54
< 0.1
0.13
1
0.44
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.5
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< 0.1
< M
< a
<[R
<a
1.1
3.9
<ML
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 0.2
< 25
26
< 25
75
38
90
65
< 2.5
< 5
< 2.5
< 2.5
< 2.5
< 2.5
< 2.5
8.3
<5
<5
46.6
33
<5
9.2
8.3
<5
<5
46.6
33
<5
9.2
<5
<5
<5
<5
<5
<5
<5
0.0027
0.00015
0.0013
< 0.00003
0.00065
0.0024
0.00073
44.8
42.2
48.8
136.3
89.6
79.1
61.3
8.7
8.1
6.8
0.01
5.7
7.3
7
6.1
5.4
5.8
8.7
6
6.1
5.6
17.9
16.7
16.3
16.2
17.5
16.9
17
<1
<1
<1
1.2
<1
1.2
<1
Page 3

Marshall Steam Station Water Supply Well Tracking Spreadsheet
Property Address
8623 Island Point Road Sherrills Ford, NC 28673
County
Catawba
Public Water
Supply ID
Public or Private
Private
DWR
Mailing
Post Cud Response
Well
Owner
ID
MR3
DWR Letter
Sent (Date)
12/17/2014
DWR Letter
Received
(Date)
12/19/2014
Post Card
Received
(Date)
Sample
(Y/N)
Lab
Preference
(Y/N)
Lab Selected by
Well Owner
Lab Assigned by DWR
coral
8665 bland Point Road Sh,, � 11, Ford, NC 28673
Private
MR6
919/2014
1172015
YES
NO
N/A
ental
Mcritech
8643 Nk d Point Road Sherrill, Ford, NC 28671
Private
MR7
19/2014
I116/2015
YES
NO
VAI
Mentech
X316 She rri11, Ford Road Shcuills Fold. NC"_8673
Catawba
Private
MR8
12, 17/2014
12'222014
1/�P_015
YES
YFS
Meritech
NSA
2971 Steam Plant Road Sherrills Ford, NC 28673
Catawba
Private
MR9
12/17,2014
12/20/2014
1 /5/2015
YES
NO
N/A
Shealy Environmental
8270 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MRIO
12/17/2014
12/24/2014
1/5/2015
YES
YES
Pace Analytical
N/A
8238 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MRl 1
12/17/2014
12/19/2014
12/30/2014
YES
YES
Pace Analytical
N/A
8220 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MR12
12/17/2014
12/19/2014
12/30/2014
YES
NO
N/A
Shealy Environmental
3.
-a
Catawba
Catawba
Private
Private
-` 3
MR15
MR19
12/17/2014
12/17/2014
12"9/2014
12/19/2014
6/2015
S
.S
YES
NO
NO
N/A
N/A
N/A
N/A
N/A
Research & Analytical
Shealy Environmental
Meritech
Shealy Environmental
Shealy Environmental
8632 Island Point Road Sherrills Ford, NC 28673
8294 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Catawba
14
T
1/5/2015
�E
YES
NO
NO
N/A
N/A
Shealy Environmental
Shealy Environmental
9 ' 'erri 'stord Road Slient sfof , -673
Catawba
- iva e
M
'912014
1/5/2015
YES
YES
Pace Analytical
N/A
8204 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MR23
12/17/2014
12/19/2014
12'23/2014
YES
NO
N/A
Rogers & Callco tt
8416 Sherrills Ford Road Shen ills Ford, NC 28673
Catawba
Private
MR24
12/17/2014
12/19/2014
12/22/2014
NO
NO
NiA
XI7^_ She rills Ford R. d Sherrills Ford, NC"_8673
Carnvbn
Privnte
MR'_5
12-''17.2014
1219i2014
12'23i 2014
YFS
NO
N/A
Prism
8566 Island Pulrt Rm 1 Sherrills Fa i NC _8673
Catawba
Private
MR26
12'17i'_014
12/19,'014
1' 3112014
YES
NO
N/A
Ro_eis & C'allcon
90571sland Point Road Sherrills Ford, NC 28673
Catawba _
Private
MR27
12/17/2014
12/19/2014
12/29/2014
YES
NO
N/A
Rogers & Callcott
8455 F NC 150 Highway Ter, cl 1, NC 28682
Catawha
NC0118736
Public
MR28
12/17/2014
1120,2014
1/5/2015
YES
YRS
Pacc Analvtical
NrA
8790 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MR29
12/17/2014
N/A
3/31/2015
YES
YES
Pace Analytical
N A
8320 F NC 150 Highway Terrell, NC 28682
Catawba
NC0118676
Public
MR30
12/17/2014
12/19/2015
1/13/2015
YES
NO
N/A
Mcritech
8353 S
8457 Sherrills Ford Road Sherrills Ford, NC 28673
IL
Catawba
Private
NM2
N/A
N/A
N/A
YES
NO
N/A
Rogers .& Callcott
Rogers & Callcott
8104 island Point Road Sherrills Ford, NC 28673
Catawba
Private
MR33
5/4/2015
5/7/2015
5/12/2015
YES
N/A
N/A
Pace Analytical
8511 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MR35
5/4/2015
5/5/2015
5/15/2015
YES
N/A
N/A
Pace Analytical
8550 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MR36
5/4/2015
5/11/2015
5/14/2015
YES
N/A
N/A
Pace Analytical
8084 Island Point Road Sherrills Ford, NC 28673
Catawba
Private
NM7
- /2015
5/8/2015
5/18/2015.
N/A
Pace Analytical
Private
MR39
5/4/2015
5/8/2015
NlA
Pace Analytical
8576 East NC Highway 150 Terrell, North Carolina 28682
Catawba
8303 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Private
MR40
5/4/2015
8411 East NC Highway 150 Terrell, North Carolina 28682
.
8140 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
Catawba
Private
Priva[e
MR41
MR43
5/4/2015
5/4/2015
5/7/2015
5/9/2015
5/13/20I5
YES
N/A
§Wr N/A
N/A
Pace Analytical
Pace Analytical
8833 Greenwood Road Terrell, North Carolina 28682
Catawba
MR44
N/A
N/A
N/A
Pace Analytical
8704 Sherrills Ford Road Sherrills Ford, NC 28673
Catawba
MR45
5/4/
N/A
N/A
Pace Analytical
Notes:
mittee to laboratory for sampling
-'ampling complete -waiting on results or HRC
nd Sent to Homeowner for Initial sampling. May
"attempts
h letters. Nositevisit Noresponse.
Page 1

NCDENR Water Supply Well Tracking Spreadsheet

Turbidity
Units
NTU
MRL
1
MDL
0.5
Method
EPA 180.1
Date
MRBKG-14
ND
06/01/2015
MRBKG-18
ND
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10
0.5
0.5
0.3
0.2
5
0.08
40
0.5
0.5
1
50
0.1
2.98
0.147
0.113
0.0807
0.0673
1.11
0.0245
16
0.169
0.126
0.214
13.7
0.0459
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
ND
ND
ND
24.9
ND
12.7
ND
1680
0.85
ND
3.2
ND
0.46
ND
ND
ND
44.0
ND
ND
ND
7510
1.9
ND
1.9
ND
0.18

Units
MRL
MDL
Method
Date
06/01/2015 MRBKG-14
MRBKG-18
Chromium,
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
Hexavalent
Mercury
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10
0.5
0.5
0.5
50
0.5
50
0.5
0.1
1
5
0.03
0.2
3.17
0.238
0.0942
0.162
11.74
0.202
16.3
0.132
0.0154
0.28
2.41
0.01
0.0216
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 218.7
EPA 245.1
808
10.7
ND
ND
1110
ND
6620
12.2
ND
ND
10.1
ND
ND
2430
ND
ND
ND
1940
ND
6440
119
ND
1.8
ND
1.7
ND
Sulfate
mg/L
2
1
EPA 300.0
ND
ND

iaiKwInny,
Carbonate
(CaCO3)
Units
mg/L
MRL
5
MDL
1
Method
SM 2320B
Date
06/01/2015 MRBKG-14 ND
MRBKG-18 ND
Alkalinity, Total Alkalinity,Bicarbo Total Dissolved Total Suspended
as CaCO3
nate (CaCO3)
Solids
Solids
Chloride
mg/L
mg/L
mg/L
mg/L
mg/L
5
5
2.5
2.5
1
1
1
2.5
2.5
0.5
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 4500-CI-E
7.4
7.4
ND
ND
3.5
33.5
33.5
51.0
ND
2.0

Turbidity
Units
NTU
MRL
1
MDL
0.5
Method
EPA 180.1
Date
05/28/2015 MRBKG-2
ND
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Calcium
Chromium
Cobalt
Copper
Iron
Lead
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
10
0.5
0.5
0.3
0.2
5
0.08
40
0.5
0.5
1
50
0.1
2.98
0.147
0.113
0.0807
0.0673
1.11
0.0245
16
0.169
0.126
0.214
13.7
0.0459
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
ND
ND
ND
13.8
ND
ND
ND
16000
ND
ND
1.9
57.5
0.16

Chromium,
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Sodium
Strontium
Thallium
Vanadium
Zinc
Hexavalent
Mercury
Units
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
MRL
10
0.5
0.5
0.5
50
0.5
50
0.5
0.1
1
5
0.03
0.2
MDL
3.17
0.238
0.0942
0.162
11.74
0.202
16.3
0.132
0.0154
0.28
2.41
0.01
0.0216
Method
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 218.7
EPA 245.1
Date
05/28/2015 M RBKG-2
5890
43.3
2.9
ND
3360
0.72
7180
89.6
ND
1.0
16.9
ND
ND
Sulfate
mg/L
2
1
EPA 300.0
13.3

iaiKwInny,
Carbonate
(CaCO3)
Units
mg/L
MRL
5
MDL
1
Method
SM 2320B
Date
05/28/2015 MRBKG-2 ND
Alkalinity, Total Alkalinity,Bicarbo Total Dissolved Total Suspended
as CaCO3
nate (CaCO3)
Solids
Solids
Chloride
mg/L
mg/L
mg/L
mg/L
mg/L
5
5
2.5
2.5
1
1
1
2.5
2.5
0.5
SM 2320B
SM 2320B
SM 2540C
SM 2540D
SM 4500-CI-E
55.8
55.8
105
ND
4.5

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, INC 28078
[phone]
June 10, 2015
Bruce Parris
NCDENR-Div. of Water Resources
610 East Center Ave
Suite 301
Mooresville, NC 28115
RE: Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Dear Bruce Parris:
Enclosed are the analytical results for sample(s) received by the laboratory on June 02, 2015. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TN standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Kevin Herring
[e-mail]
HORIZON Database Administrator
Enclosures
e pccft 2�' O
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 1 of 32

lacmnalyfica(
www.pacelabs.com
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Minnesota Certification IDs
1700 Elm Street SE Suite 200, Minneapolis, MN 55414
A21-A Certification #: 2926.01
Alaska Certification #: UST-078
Alaska Certification #MN00064
Alabama Certification #40770
Arizona Certification #: AZ-0014
Arkansas Certification #: 88-0680
California Certification #: 01155CA
Colorado Certification #Pace
Connecticut Certification #: PH-0256
EPA Region 8 Certification #: 8TMS-L
Florida/NELAP Certification #: E87605
Guam Certification #:14-008r
Georgia Certification #: 959
Georgia EPD #: Pace
Idaho Certification #: MN00064
Hawaii Certification #MN00064
Illinois Certification #: 200011
Indiana Certification#C-MN-01
Iowa Certification #: 368
Kansas Certification #: E-10167
Kentucky Dept of Envi. Protection - DW #90062
Kentucky Dept of Envi. Protection - WW #:90062
Louisiana DEQ Certification #: 3086
Louisiana DHH #: LA140001
Maine Certification #: 2013011
Maryland Certification #: 322
Michigan DEPH Certification #: 9909
Ormond Beach Certification IDs
8 East Tower Circle, Ormond Beach, FL 32174
Alabama Certification #: 41320
Connecticut Certification #: PH-0216
Delaware Certification: FL NELAC Reciprocity
Florida Certification #: E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Illinois Certification #: 200068
Indiana Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: FL NELAC Reciprocity
Louisiana Environmental Certificate #: 05007
Maryland Certification: #346
Massachusetts Certification #: M-FL1264
Michigan Certification #: 9911
Mississippi Certification: FL NELAC Reciprocity
Missouri Certification #: 236
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
CERTIFICATIONS
Minnesota Certification #: 027-053-137
Mississippi Certification #: Pace
Montana Certification #: MT0092
Nevada Certification #: MN_00064
Nebraska Certification #: Pace
New Jersey Certification #: MN-002
New York Certification #: 11647
North Carolina Certification #: 530
North Carolina State Public Health #: 27700
North Dakota Certification #: R-036
Ohio EPA#: 4150
Ohio VAP Certification #: CL101
Oklahoma Certification #: 9507
Oregon Certification #: MN200001
Oregon Certification #: MN300001
Pennsylvania Certification #: 68-00563
Puerto Rico Certification
Saipan (CNMI) #:MP0003
South Carolina #:74003001
Texas Certification #: T104704192
Tennessee Certification #: 02818
Utah Certification #: MN000642013-4
Virginia DGS Certification #: 251
Virginia/VELAP Certification #: Pace
Washington Certification #: C486
West Virginia Certification #: 382
West Virginia DHHR #:9952C
Wisconsin Certification #: 999407970
Montana Certification #: Cert 0074
Nebraska Certification: NE-OS-28-14
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification #: 2958
New Jersey Certification #: FL765
New York Certification #: 11608
North Carolina Environmental Certificate #: 667
Pennsylvania Certification #: 68-00547
Puerto Rico Certification #: FLO1264
South Carolina Certification: #96042001
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
US Virgin Islands Certification: FL NELAC Reciprocity
Virginia Environmental Certification #: 460165
Washington Certification #: C955
West Virginia Certification #: 9962C
Wisconsin Certification #: 399079670
Wyoming (EPA Region 8): FL NELAC Reciprocity
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
West Virginia Certification #: 356
Virginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
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SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
MARSHALL BACKGROUND WSW SAMPLI
92252271
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92252271001
MRBKG-14
EPA 200.8
TT3
24
PASI-M
EPA 245.1
LMW
1
PASI-M
EPA 180.1
JTJ
1
PASI-A
SM 2320B
MILS
3
PASI-A
SM 2540C
MDW
1
PASI-A
SM 2540D
MDW
1
PASI-A
EPA 218.7
TK1
1
PASI-O
EPA 300.0
AES2
1
PASI-A
SM 4500-CI-E
SER
1
PASI-A
92252271002
MRBKG-18
EPA 200.8
TT3
24
PASI-M
EPA 245.1
LMW
1
PASI-M
EPA 180.1
JTJ
1
PASI-A
SM 2320B
MLS
3
PASI-A
SM 2540C
MDW
1
PASI-A
SM 2540D
MDW
1
PASI-A
EPA 218.7
TK1
1
PASI-O
EPA 300.0
AES2
1
PASI-A
SM 4500-CI-E
SER
1
PASI-A
REPORT OF LABORATORY ANALYSIS
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SUMMARY OF DETECTION
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Lab Sample ID Client Sample ID
Method Parameters
Result Units Report Limit Analyzed
92252271001
MRBKG-14
EPA 200.8
Barium
24.9
ug/L
0.30
06/05/15 18:58
EPA 200.8
Boron
12.7
ug/L
5.0
06/05/15 18:58
EPA 200.8
Calcium
1680
ug/L
40.0
06/05/15 18:58
EPA 200.8
Chromium
0.85
ug/L
0.50
06/05/15 18:58
EPA 200.8
Copper
3.2
ug/L
1.0
06/05/15 18:58
EPA 200.8
Lead
0.46
ug/L
0.10
06/05/15 18:58
EPA 200.8
Magnesium
808
ug/L
10.0
06/05/15 18:58
EPA 200.8
Manganese
10.7
ug/L
0.50
06/05/15 18:58
EPA 200.8
Potassium
1110
ug/L
50.0
06/05/15 18:58
EPA 200.8
Sodium
6620
ug/L
50.0
06/05/15 18:58
EPA 200.8
Strontium
12.2
ug/L
0.50
06/05/15 18:58
EPA 200.8
Zinc
10.1
ug/L
5.0
06/05/15 18:58
SM 2320B
Alkalinity, Bicarbonate (CaCO3)
7.4
mg/L
5.0
06/08/15 20:05
SM 2320B
Alkalinity, Total as CaCO3
7.4
mg/L
5.0
06/08/15 20:05
SM 4500-CI-E
Chloride
3.5
mg/L
1.0
06/06/15 06:33
92252271002
MRBKG-18
EPA 200.8
Barium
44.0
ug/L
0.30
06/05/15 19:01
EPA 200.8
Calcium
7510
ug/L
40.0
06/05/15 19:01
EPA 200.8
Chromium
1.9
ug/L
0.50
06/05/15 19:01
EPA 200.8
Copper
1.9
ug/L
1.0
06/05/15 19:01
EPA 200.8
Lead
0.18
ug/L
0.10
06/05/15 19:01
EPA 200.8
Magnesium
2430
ug/L
10.0
06/05/15 19:01
EPA 200.8
Potassium
1940
ug/L
50.0
06/05/15 19:01
EPA 200.8
Sodium
6440
ug/L
50.0
06/05/15 19:01
EPA 200.8
Strontium
119
ug/L
0.50
06/05/15 19:01
EPA 200.8
Vanadium
1.8
ug/L
1.0
06/05/15 19:01
SM 2320B
Alkalinity, Bicarbonate (CaCO3)
33.5
mg/L
5.0
06/08/15 20:16
SM 2320B
Alkalinity, Total as CaCO3
33.5
mg/L
5.0
06/08/15 20:16
SM 2540C
Total Dissolved Solids
51.0
mg/L
25.0
06/07/15 19:08
EPA 218.7
Chromium, Hexavalent
1.7
ug/L
0.60
06/09/15 16:29
SM 4500-CI-E
Chloride
2.0
mg/L
1.0
06/06/15 06:36
REPORT OF LABORATORY ANALYSIS
Qualifiers
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: EPA 200.8
Description: 200.8 MET ICPMS
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for EPA 200.8. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 200.8 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Internal Standards:
All internal standards were within QC limits with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: MPRP/54918
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92251898001,92252245001
M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
• MS (Lab ID: 1984403)
• Calcium
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: EPA 245.1
Description: 245.1 Mercury
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for EPA 245.1. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Sample Preparation:
The samples were prepared in accordance with EPA 245.1 with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: EPA 180.1
Description: 180.1 Turbidity
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for EPA 180.1. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: SM 2320B
Description: 2320E Alkalinity
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for SM 2320B. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
QC Batch: WET/37952
A matrix spike and/or matrix spike duplicate (MS/MSD) were performed on the following sample(s): 92251906010,92252474001
M1: Matrix spike recovery exceeded QC limits.
• MS (Lab ID: 1478322)
• Alkalinity, Total as CaCO3
• MSD (Lab ID: 1478321)
• Alkalinity, Total as CaCO3
• MSD (Lab ID: 1478323)
• Alkalinity, Total as CaCO3
Additional Comments:
Batch accepted based on laboratory control sample (LCS) recovery.
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: SM 2540C
Description: 2540C Total Dissolved Solids
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for SM 2540C. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: SM 2540D
Description: 2540D Total Suspended Solids
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for SM 2540D. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Duplicate Sample:
All duplicate sample results were within method acceptance criteria with any exceptions noted below.
QC Batch: WET/37946
D6: The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
• DUP (Lab ID: 1477819)
• Total Suspended Solids
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: EPA 218.7
Description: Hexavalent Chromium by IC
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for EPA 218.7. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: EPA 300.0
Description: 300.0 IC Anions 28 Days
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for EPA 300.0. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
REPORT OF LABORATORY ANALYSIS
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PROJECT NARRATIVE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Method: SM 4500-CI-E
Description: 4500 Chloride
Client: NCDENR-Division of Water Resources
Date: June 10, 2015
General Information:
2 samples were analyzed for SM 4500-CI-E. All samples were received in acceptable condition with any exceptions noted below.
Hold Time:
The samples were analyzed within the method required hold times with any exceptions noted below.
Initial Calibrations (including MS Tune as applicable):
All criteria were within method requirements with any exceptions noted below.
Continuing Calibration:
All criteria were within method requirements with any exceptions noted below.
Method Blank:
All analytes were below the report limit in the method blank, where applicable, with any exceptions noted below.
Laboratory Control Spike:
All laboratory control spike compounds were within QC limits with any exceptions noted below.
Matrix Spikes:
All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.
Additional Comments:
This data package has been reviewed for quality and completeness and is approved for release.
REPORT OF LABORATORY ANALYSIS
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ANALYTICAL RESULTS
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Sample: MRBKG-14 Lab ID: 92252271001 Collected: 06/01/15 12:10 Received: 06/02/15 08:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Aluminum
ND
ug/L
10.0
1
06/04/1516:06
06/05/1518:58
7429-90-5
Antimony
ND
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7440-36-0
Arsenic
ND
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7440-38-2
Barium
24.9
ug/L
0.30
1
06/04/1516:06
06/05/1518:58
7440-39-3
Beryllium
ND
ug/L
0.20
1
06/04/1516:06
06/05/1518:58
7440-41-7
Boron
12.7
ug/L
5.0
1
06/04/1516:06
06/05/1518:58
7440-42-8
Cadmium
ND
ug/L
0.080
1
06/04/1516:06
06/05/1518:58
7440-43-9
Calcium
1680
ug/L
40.0
1
06/04/1516:06
06/05/1518:58
7440-70-2
Chromium
0.85
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7440-47-3
Cobalt
ND
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7440-48-4
Copper
3.2
ug/L
1.0
1
06/04/1516:06
06/05/1518:58
7440-50-8
Iron
ND
ug/L
50.0
1
06/04/1516:06
06/05/1518:58
7439-89-6
Lead
0.46
ug/L
0.10
1
06/04/1516:06
06/05/1518:58
7439-92-1
Magnesium
808
ug/L
10.0
1
06/04/1516:06
06/05/1518:58
7439-95-4
Manganese
10.7
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7439-96-5
Molybdenum
ND
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7439-98-7
Nickel
ND
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7440-02-0
Potassium
1110
ug/L
50.0
1
06/04/1516:06
06/05/1518:58
7440-09-7
Selenium
ND
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7782-49-2
Sodium
6620
ug/L
50.0
1
06/04/1516:06
06/05/1518:58
7440-23-5
Strontium
12.2
ug/L
0.50
1
06/04/1516:06
06/05/1518:58
7440-24-6
Thallium
ND
ug/L
0.10
1
06/04/1516:06
06/05/1518:58
7440-28-0
Vanadium
ND
ug/L
1.0
1
06/04/1516:06
06/05/1518:58
7440-62-2
Zinc
10.1
ug/L
5.0
1
06/04/1516:06
06/05/1518:58
7440-66-6
245.1 Mercury
Analytical Method:
EPA 245.1
Preparation Method: EPA 245.1
Mercury
ND
ug/L
0.20
1
06/06/1514:02
06/07/1518:44
7439-97-6
180.1 Turbidity
Analytical Method:
EPA 180.1
Turbidity
ND
NTU
1.0
1
06/03/1510:30
2320B Alkalinity
Analytical Method:
SM 2320B
Alkalinity, Bicarbonate (CaCO3)
7.4
mg/L
5.0
1
06/08/15 20:05
Alkalinity, Carbonate (CaCO3)
ND
mg/L
5.0
1
06/08/15 20:05
Alkalinity, Total as CaCO3
7.4
mg/L
5.0
1
06/08/15 20:05
2540C Total Dissolved Solids
Analytical Method:
SM 2540C
Total Dissolved Solids
ND
mg/L
25.0
1
06/07/15 19:07
2540D Total Suspended Solids
Analytical Method:
SM 2540D
Total Suspended Solids
ND
mg/L
2.5
1
06/07/15 20:27
Hexavalent Chromium by IC
Analytical Method:
EPA 218.7
Chromium, Hexavalent
ND
ug/L
0.60
20
06/09/15 16:16
18540-29-9
Date: 06/10/2015 11:53 AM
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services, Inc..
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ANALYTICAL RESULTS
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Sample: MRBKG-14 Lab ID: 92252271001 Collected: 06/01/15 12:10 Received: 06/02/15 08:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate ND mg/L 2.0 1 06/05/15 20:08 14808-79-8
4500 Chloride Analytical Method: SM 4500-CI-E
Chloride 3.5 mg/L 1.0 1 06/06/15 06:33 16887-00-6
Date: 06/10/2015 11:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 15 of 32

aceAnaiXical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Sample: MRBKG-18 Lab ID: 92252271002 Collected: 06/01/15 12:56 Received: 06/02/15 08:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
200.8 MET ICPMS Analytical Method: EPA 200.8 Preparation Method: EPA 200.8
Aluminum
ND
ug/L
10.0
1
06/04/1516:06
06/05/1519:01
7429-90-5
Antimony
ND
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7440-36-0
Arsenic
ND
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7440-38-2
Barium
44.0
ug/L
0.30
1
06/04/1516:06
06/05/1519:01
7440-39-3
Beryllium
ND
ug/L
0.20
1
06/04/1516:06
06/05/1519:01
7440-41-7
Boron
ND
ug/L
5.0
1
06/04/1516:06
06/05/1519:01
7440-42-8
Cadmium
ND
ug/L
0.080
1
06/04/1516:06
06/05/1519:01
7440-43-9
Calcium
7510
ug/L
40.0
1
06/04/1516:06
06/05/1519:01
7440-70-2
Chromium
1.9
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7440-47-3
Cobalt
ND
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7440-48-4
Copper
1.9
ug/L
1.0
1
06/04/1516:06
06/05/1519:01
7440-50-8
Iron
ND
ug/L
50.0
1
06/04/1516:06
06/05/1519:01
7439-89-6
Lead
0.18
ug/L
0.10
1
06/04/1516:06
06/05/1519:01
7439-92-1
Magnesium
2430
ug/L
10.0
1
06/04/1516:06
06/05/1519:01
7439-95-4
Manganese
ND
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7439-96-5
Molybdenum
ND
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7439-98-7
Nickel
ND
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7440-02-0
Potassium
1940
ug/L
50.0
1
06/04/1516:06
06/05/1519:01
7440-09-7
Selenium
ND
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7782-49-2
Sodium
6440
ug/L
50.0
1
06/04/1516:06
06/05/1519:01
7440-23-5
Strontium
119
ug/L
0.50
1
06/04/1516:06
06/05/1519:01
7440-24-6
Thallium
ND
ug/L
0.10
1
06/04/1516:06
06/05/1519:01
7440-28-0
Vanadium
1.8
ug/L
1.0
1
06/04/1516:06
06/05/1519:01
7440-62-2
Zinc
ND
ug/L
5.0
1
06/04/1516:06
06/05/1519:01
7440-66-6
245.1 Mercury
Analytical Method:
EPA 245.1
Preparation Method: EPA 245.1
Mercury
ND
ug/L
0.20
1
06/06/1514:02
06/07/1518:46
7439-97-6
180.1 Turbidity
Analytical Method:
EPA 180.1
Turbidity
ND
NTU
1.0
1
06/03/1510:30
2320B Alkalinity
Analytical Method:
SM 2320B
Alkalinity, Bicarbonate (CaCO3)
33.5
mg/L
5.0
1
06/08/15 20:16
Alkalinity, Carbonate (CaCO3)
ND
mg/L
5.0
1
06/08/15 20:16
Alkalinity, Total as CaCO3
33.5
mg/L
5.0
1
06/08/15 20:16
2540C Total Dissolved Solids
Analytical Method:
SM 2540C
Total Dissolved Solids
51.0
mg/L
25.0
1
06/07/15 19:08
2540D Total Suspended Solids
Analytical Method:
SM 2540D
Total Suspended Solids
ND
mg/L
2.5
1
06/07/15 20:28
Hexavalent Chromium by IC
Analytical Method:
EPA 218.7
Chromium, Hexavalent
1.7
ug/L
0.60
20
06/09/15 16:29
18540-29-9
Date: 06/10/2015 11:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 16 of 32

aceAnaiXical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
ANALYTICAL RESULTS
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Sample: MRBKG-18 Lab ID: 92252271002 Collected: 06/01/15 12:56 Received: 06/02/15 08:45 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
300.0 IC Anions 28 Days Analytical Method: EPA 300.0
Sulfate ND mg/L 2.0 1 06/05/15 21:16 14808-79-8
4500 Chloride Analytical Method: SM 4500-CI-E
Chloride 2.0 mg/L 1.0 1 06/06/15 06:36 16887-00-6
Date: 06/10/2015 11:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 17 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: MERP/13764
Analysis Method: EPA 245.1
QC Batch Method: EPA 245.1
Analysis Description: 245.1 Mercury
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1984468
Matrix: Water
Associated Lab Samples: 92252271001, 92252271002
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Mercury
ug/L
ND 0.20
06/07/1518:07
LABORATORY CONTROL SAMPLE:
1984469
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rec Limits Qualifiers
Mercury
ug/L
5 5.0
101 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1984470 1984471
MS MSD
92251874003
Spike Spike MS
MSD MS MSD
% Rec
Parameter
Units Result
Conc. Conc. Result
Result % Rec % Rec
Limits RPD Qual
Mercury
ug/L ND
5 5 5.2
5.2 105 104
70-130 1
MATRIX SPIKE SAMPLE:
1984472
10308075004 Spike
MS MS
% Rec
Parameter
Units
Result Conc.
Result % Rec
Limits Qualifiers
Mercury
ug/L
ND 5
5.4 107
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc.. Page 18 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: MPRP/54918 Analysis Method: EPA 200.8
QC Batch Method: EPA 200.8 Analysis Description: 200.8 MET
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1984399
Associated Lab Samples: 92252271001, 92252271002
Parameter
Units
Aluminum
ug/L
Antimony
ug/L
Arsenic
ug/L
Barium
ug/L
Beryllium
ug/L
Boron
ug/L
Cadmium
ug/L
Calcium
ug/L
Chromium
ug/L
Cobalt
ug/L
Copper
ug/L
Iron
ug/L
Lead
ug/L
Magnesium
ug/L
Manganese
ug/L
Molybdenum
ug/L
Nickel
ug/L
Potassium
ug/L
Selenium
ug/L
Sodium
ug/L
Strontium
ug/L
Thallium
ug/L
Vanadium
ug/L
Zinc
ug/L
Matrix: Water
Blank
Result
Reporting
Limit
Analyzed
ND
10.0
06/05/1518:01
ND
0.50
06/05/1518:01
ND
0.50
06/05/1518:01
ND
0.30
06/05/1518:01
ND
0.20
06/05/1518:01
ND
5.0
06/05/1518:01
ND
0.080
06/05/1518:01
ND
40.0
06/05/1518:01
ND
0.50
06/05/1518:01
ND
0.50
06/05/1518:01
ND
1.0
06/05/1518:01
ND
50.0
06/05/1518:01
ND
0.10
06/05/1518:01
ND
10.0
06/05/1518:01
ND
0.50
06/05/1518:01
ND
0.50
06/05/1518:01
ND
0.50
06/05/1518:01
ND
50.0
06/05/1518:01
ND
0.50
06/05/1518:01
ND
50.0
06/05/1518:01
ND
0.50
06/05/1518:01
ND
0.10
06/05/1518:01
ND
1.0
06/05/1518:01
ND
5.0
06/05/1518:01
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1984400
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Aluminum
ug/L
80
86.2
108
85-115
Antimony
ug/L
80
80.8
101
85-115
Arsenic
ug/L
80
80.7
101
85-115
Barium
ug/L
80
81.5
102
85-115
Beryllium
ug/L
80
83.1
104
85-115
Boron
ug/L
80
84.0
105
85-115
Cadmium
ug/L
80
82.9
104
85-115
Calcium
ug/L
1000
1090
109
85-115
Chromium
ug/L
80
86.5
108
85-115
Cobalt
ug/L
80
85.6
107
85-115
Copper
ug/L
80
82.9
104
85-115
Iron
ug/L
1000
1090
109
85-115
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc..
Page 19 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
LABORATORY CONTROL SAMPLE:
Parameter
1984400
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Lead
ug/L
80
86.5
108
85-115
Magnesium
ug/L
1000
1060
106
85-115
Manganese
ug/L
80
86.6
108
85-115
Molybdenum
ug/L
80
84.1
105
85-115
Nickel
ug/L
80
87.5
109
85-115
Potassium
ug/L
1000
1030
103
85-115
Selenium
ug/L
80
80.2
100
85-115
Sodium
ug/L
1000
1050
105
85-115
Strontium
ug/L
80
81.9
102
85-115
Thallium
ug/L
80
86.7
108
85-115
Vanadium
ug/L
80
84.3
105
85-115
Zinc
ug/L
80
85.2
107
85-115
Qualifiers
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1984401
MS
92251898001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1984402
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Aluminum
ug/L
ND
80
80
88.6
86.7
108
105
70-130
2
Antimony
ug/L
ND
80
80
80.3
78.9
100
99
70-130
2
Arsenic
ug/L
ND
80
80
78.7
77.4
98
97
70-130
2
Barium
ug/L
8.5
80
80
89.3
88.9
101
100
70-130
0
Beryllium
ug/L
ND
80
80
81.2
80.2
102
100
70-130
1
Boron
ug/L
ND
80
80
86.9
86.0
106
105
70-130
1
Cadmium
ug/L
ND
80
80
82.8
82.9
103
104
70-130
0
Calcium
ug/L
6720
1000
1000
7650
7520
93
79
70-130
2
Chromium
ug/L
ND
80
80
89.3
89.0
111
111
70-130
0
Cobalt
ug/L
ND
80
80
85.1
85.4
106
107
70-130
0
Copper
ug/L
7.0
80
80
93.2
94.4
108
109
70-130
1
Iron
ug/L
4600
1000
1000
5690
5660
108
106
70-130
0
Lead
ug/L
0.70
80
80
88.0
88.5
109
110
70-130
1
Magnesium
ug/L
3430
1000
1000
4470
4420
104
100
70-130
1
Manganese
ug/L
28.9
80
80
117
117
110
110
70-130
0
Molybdenum
ug/L
ND
80
80
85.4
85.5
107
107
70-130
0
Nickel
ug/L
ND
80
80
88.6
88.6
110
110
70-130
0
Potassium
ug/L
951
1000
1000
2000
1970
105
102
70-130
1
Selenium
ug/L
ND
80
80
78.9
76.0
99
95
70-130
4
Sodium
ug/L
5850
1000
1000
6970
6870
112
101
70-130
2
Strontium
ug/L
71.8
80
80
153
152
101
100
70-130
1
Thallium
ug/L
ND
80
80
86.1
86.2
108
108
70-130
0
Vanadium
ug/L
1.8
80
80
88.4
87.3
108
107
70-130
1
Zinc
ug/L
66.2
80
80
149
148
103
102
70-130
1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc..
Page 20 of 32

aceAnaiXical
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Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
MATRIX SPIKE SAMPLE:
1984403
92252245001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
Aluminum
ug/L
13.4
80
102
111
70-130
Antimony
ug/L
ND
80
80.7
101
70-130
Arsenic
ug/L
ND
80
79.0
99
70-130
Barium
ug/L
12.4
80
93.9
102
70-130
Beryllium
ug/L
ND
80
83.4
104
70-130
Boron
ug/L
ND
80
89.1
107
70-130
Cadmium
ug/L
ND
80
82.9
104
70-130
Calcium
ug/L
13700
1000
15300
159
70-130 M1
Chromium
ug/L
0.69
80
89.4
111
70-130
Cobalt
ug/L
ND
80
84.3
105
70-130
Copper
ug/L
3.0
80
88.7
107
70-130
Iron
ug/L
ND
1000
1140
112
70-130
Lead
ug/L
0.36
80
87.4
109
70-130
Magnesium
ug/L
3690
1000
4880
118
70-130
Manganese
ug/L
11.2
80
100
111
70-130
Molybdenum
ug/L
0.96
80
86.3
107
70-130
Nickel
ug/L
ND
80
87.9
109
70-130
Potassium
ug/L
2010
1000
3140
113
70-130
Selenium
ug/L
ND
80
77.9
97
70-130
Sodium
ug/L
7220
1000
8450
124
70-130
Strontium
ug/L
66.9
80
151
105
70-130
Thallium
ug/L
ND
80
85.5
107
70-130
Vanadium
ug/L
8.4
80
95.0
108
70-130
Zinc
ug/L
1540
80
1640
122
70-130
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc..
Page 21 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: WET/37841
Analysis Method:
EPA 180.1
QC Batch Method: EPA 180.1
Analysis Description:
180.1 Turbidity
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1473524
Matrix:
Water
Associated Lab Samples: 92252271001, 92252271002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Turbidity
NTU
ND
1.0 06/03/1510:30
LABORATORY CONTROL SAMPLE:
1473525
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Turbidity
NTU
10
9.5
95
90-110
SAMPLE DUPLICATE: 1473526
92252271001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Turbidity
NTU
ND
ND
SAMPLE DUPLICATE: 1473527
92252487001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
Turbidity
NTU
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc.. Page 22 of 32

Pace Analytical Services, Inc
aceAnalXical ® 9800 Kiney Ave. Suite 100
Huntersville, NC 28078078
www.pacelabs.com [phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: WET/37952 Analysis Method: SM 2320B
QC Batch Method: SM 2320B Analysis Description: 2320E Alkalinity
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1478318
Matrix:
Water
Associated Lab Samples: 92252271001, 92252271002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Alkalinity, Carbonate (CaCO3)
mg/L
ND
5.0
06/08/15 17:50
Alkalinity, Total as CaCO3
mg/L
ND
5.0
06/08/15 17:50
Alkalinity, Bicarbonate (CaCO3)
mg/L
ND
5.0
06/08/15 17:50
LABORATORY CONTROL SAMPLE:
1478319
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Alkalinity, Total as CaCO3 mg/L 50 47.4 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478320 1478321
MS MSD
92251906010 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 39.6 50 50 86.5 84.1 94 89 90-110 3 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1478322 1478323
MS MSD
92252474001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Alkalinity, Total as CaCO3 mg/L 192 50 50 218 220 53 58 90-110 1 M1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc..
Page 23 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: WET/37947
Analysis Method: SM 2540C
QC Batch Method: SM 2540C
Analysis Description: 2540C Total Dissolved Solids
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1477820
Matrix: Water
Associated Lab Samples: 92252271001, 92252271002
Blank Reporting
Parameter
Units
Result Limit Analyzed Qualifiers
Total Dissolved Solids
mg/L
ND 25.0 06/07/15 19:07
LABORATORY CONTROL SAMPLE:
1477821
Spike LCS LCS % Rec
Parameter
Units
Conc. Result % Rec Limits Qualifiers
Total Dissolved Solids
mg/L
250 244 98 90-110
SAMPLE DUPLICATE: 1477822
92252271001 Dup
Parameter
Units
Result Result RPD Qualifiers
Total Dissolved Solids
mg/L
ND ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc.. Page 24 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: WET/37946
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1477816
Matrix:
Water
Associated Lab Samples: 92252271001, 92252271002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
ND
2.5 06/07/15 20:19
LABORATORY CONTROL SAMPLE:
1477817
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Total Suspended Solids
mg/L
250
248
99 90-110
SAMPLE DUPLICATE: 1477818
92252373001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
204
196 4
SAMPLE DUPLICATE: 1477819
92252327001
Dup
Parameter
Units
Result
Result
RPD Qualifiers
Total Suspended Solids
mg/L
60.0
64.3 7 D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc.. Page 25 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: WETA/47098 Analysis Method: EPA 218.7
QC Batch Method: EPA 218.7 Analysis Description: Chromium, Hexavalent IC
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1235670 Matrix: Water
Associated Lab Samples:
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chromium, Hexavalent ug/L ND 0.030 06/09/15 14:32
LABORATORY CONTROL SAMPLE: 1235671
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chromium, Hexavalent ug/L .075 0.079 105 85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1235672 1235673
MS MSD
92252051001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chromium, Hexavalent ug/L 1.1 1.5 1.5 3.2 3.1 141 134 85-115 3 M6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc..
Page 26 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: WETA/23162
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1475158
Matrix: Water
Associated Lab Samples: 92252271001, 92252271002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Sulfate mg/L
ND 2.0
06/05/1519:41
LABORATORY CONTROL SAMPLE: 1475159
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Sulfate mg/L
20 20.0
100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1475160 1475161
MS MSD
92252271001
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Sulfate mg/L ND
20 20 20.3
20.3 102 102 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1475162
MS
92252055001 Spike
Parameter Units Result Conc.
Sulfate mg/L 12000J 20
ug/L
1475163
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
20 33.1 33.2 106 106 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc..
Qual
Page 27 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
QC Batch: WETA/23156
Analysis Method: SM 4500-CI-E
QC Batch Method: SM 4500-CI-E
Analysis Description: 4500 Chloride
Associated Lab Samples: 92252271001, 92252271002
METHOD BLANK: 1474750
Matrix: Water
Associated Lab Samples: 92252271001, 92252271002
Blank Reporting
Parameter Units
Result Limit
Analyzed Qualifiers
Chloride mg/L
ND 1.0
06/06/15 06:21
LABORATORY CONTROL SAMPLE: 1474751
Spike LCS
LCS % Rec
Parameter Units
Conc. Result
% Rec Limits Qualifiers
Chloride mg/L
20 19.8
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1474752 1474753
MS MSD
92251458004
Spike Spike MS
MSD MS MSD % Rec
Parameter Units Result
Conc. Conc. Result
Result % Rec % Rec Limits RPD Qual
Chloride mg/L 10.5
20 20 29.4
29.4 95 95 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1474754 1474755
MS MSD
92252271002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chloride mg/L 2.0 20 20 20.8 20.8 94 94 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc..
Page 28 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALIFIERS
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether, Styrene, and Vinyl chloride.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TN -The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-M Pace Analytical Services - Minneapolis
PASI-O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 06/10/2015 11:53 AM without the written consent of Pace Analytical Services, Inc.. Page 29 of 32

aceAnaiXical
www.pacelabs.com
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: MARSHALL BACKGROUND WSW SAMPLI
Pace Project No.: 92252271
Lab ID Sample ID QC Batch Method QC Batch Analytical Method
92252271001
MRBKG-14
EPA 200.8
MPRP/54918
EPA 200.8
92252271002
MRBKG-18
EPA 200.8
MPRP/54918
EPA 200.8
92252271001
MRBKG-14
EPA 245.1
MERP/13764
EPA 245.1
92252271002
MRBKG-18
EPA 245.1
MERP/13764
EPA 245.1
92252271001
MRBKG-14
EPA 180.1
WET/37841
92252271002
MRBKG-18
EPA 180.1
WET/37841
92252271001
MRBKG-14
SM 2320E
WET/37952
92252271002
MRBKG-18
SM 2320E
WET/37952
92252271001
MRBKG-14
SM 2540C
WET/37947
92252271002
MRBKG-18
SM 2540C
WET/37947
92252271001
MRBKG-14
SM 2540D
WET/37946
92252271002
MRBKG-18
SM 2540D
WET/37946
92252271001
MRBKG-14
EPA218.7
WETA/47098
92252271002
MRBKG-18
EPA 218.7
WETA/47098
92252271001
MRBKG-14
EPA 300.0
WETA/23162
92252271002
MRBKG-18
EPA 300.0
WETA/23162
92252271001
MRBKG-14
SM 4500-CI-E
WETA/23156
92252271002
MRBKG-18
SM 4500-CI-E
WETA/23156
Date: 06/10/2015 11:53 AM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Analytical
Batch
ICPM/24672
ICPM/24672
MERC/16040
MERC/16040
Page 30 of 32

�-XeAnalytlxf'
r
tocument Name:
le Condition Upon Recei
Document Number:
F-CHR-CS-003-rev.16
uocument Revised: May 1B, -LU'l0
Page 1 of 2*
Issuing Authority:
Pace Huntersville Qualitv Office
Client name: 1 0 Page 2 of 2 is for Internal Use Only
Courier: ❑ Fed Ex ❑ UPO USPS❑ Client❑ Commercial Pace Other
Custody Seal on Cooler/Box Present: ❑ yes ❑ 4o Seals intact: ❑ yes ❑ no
Packing Material: ❑ Bubble VDp ❑ Bubble Bags (] None ❑ Other
Thermometer Used: IR Gun T1401 Type of Ice; Wet Blue None Samples on ice, cooling process has begun
Tema Correction Factor T1401 No Correction
f
Corrected Cooler Temp.: •C
Biological Tissue is Frozen: Yes No N/A
Date a itiat of rson examining
eo'a n s
'
Temp should be above freezing to i6°C
Comments:
Chain�of Custody Present:
-' 'Ye. []No
❑NIA
1.
Chain of Custody Filled Out:
�es ONO
❑NIA
2,
Chain of Custody Relinquished:
PlYes ❑No
❑NIA
3.
Sampler Name & Signature on COC:
12 es ONO
❑WA
4,
Samples Arrived within Hold Time:
OYas ❑No
❑NIA
5.
Short Hold Time Analysis (a72hr):
C1.Y s 16A❑NIA
6.
Rush Turn Around Time Requested;
Dyes EXo
❑NIA
7.
Sufficient Volume:
Plas ONO
❑NIA
8.
Correct Containers Used:
I
2Ye8 ONO
❑NIA
9.
-Pace Containers Used:
FZYes ONO
❑N!A
Containers Intact:
Yes ONO
❑NIA
10.
Filtered volume received for Dissolved tests
❑Yes ONO
❑NIA
11.
Sample Labels match COC:
QY;� ONO
❑NIA
12.
-Includes date/time/ID/Analysis Matrix:
All containers needing preservation have been chec&ed.
❑Y�es''�❑No
t❑/Yes
❑N!A
13.
All containers needing preservation are found to be in
ONO
El N/A
compliance with EPA recommendation.
exceptions: VOA, coliform, TOC, O&G, WI-DRO (water)
CIYes ONO
Samples checked for dechlorination:
❑Yes ONO
EI NX
14.
Headspace in VOA Vials(>6mm):
Dyes ONO
❑IVIK
15.
Trip Blank Present:
❑Yes ONO
0N1A
16.
Trip Biank Custody Seals Present
❑Yes ONO
❑NIA
Pace Trip Blank Lot # (if purchased):
Client Notification/ Resolution:
Person Contacted: Daterrime:
Comments/ Resolution:
SCURF Review: Date: (I � ►/IS I
SRF Review: Date: !� 7�
Note: Whenever there is a discrepancy affecting North Carolina compliance
samples, a copy of this form will be sent to the North Carolina DEHNR
Certification Office ( i.e out of hold, incorrect preservative, out of temp,
incorrect containers)
Field Data Required? Y 1 N
w04:92252271
11111111111111111111111
Page 31 of 32

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Page 32 of 32

Background Water Supply Well Analytical Results