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HomeMy WebLinkAboutNCG551311_2023 Lab Data Compliance Inspection_20231023Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 October 09, 2023 One Time Client Private Small Jobs Huntersville, NC 28078 RE: Project: Power Sampling Event Pace Project No.: 92690165 Dear One Client: Enclosed are the analytical results for sample(s) received by the laboratory on September 25, 2023. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services -Asheville • Pace Analytical Services - Charlotte • Pace Analytical Services - Eden • Pace Analytical Services - Raleigh If you have any questions concerning this report, please feel free to contact me. Sincerely, pely ��4--Wd- Ashari Taylor -Watson ashari.taylor-watson@pacelabs.com 704-977-0939 Project Manager Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 1 of 19 Project: Power Sampling Event Pace Project No.: 92690165 Pace Analytical Services Raleigh 4915 Waters Edge Dr. #120, Raleigh, NC 27606 North Carolina Wastewater Certification #: 67 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification #: 37738 CERTIFICATIONS North Carolina Drinking Water Certification #: 37731 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 North Carolina Wastewater Certification #: 633 Virginia/VELAP Certification #: 460025 REPORT OF LABORATORY ANALYSIS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 2 of 19 SAMPLE ANALYTE COUNT Project: Power Sampling Event Pace Project No.: 92690165 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92690165001 5719 Poragon Circle, Durham NC SM 2540D-2015 DAW 1 PASI-E SM 521OB-2016 LRB 1 PASI-E Colilert-18 HGH 1 PASI-R TKN+NO3+NO2 Calculation KDF1 1 PASI-A EPA 350.1 Rev 2.0 1993 NCF 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.0 1993 EGC 1 PASI-A EPA 365.1 Rev 2.0 1993 Zip 1 PASI-A PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte PASI-E = Pace Analytical Services - Eden PASI-R = Pace Analytical Services - Raleigh REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 ANALYTICAL RESULTS Project: Power Sampling Event Pace Project No.: 92690165 Sample: 5719 Poragon Circle, Lab ID: 92690165001 Collected: 09/25/23 09:55 Received: 09/25/23 13:15 Matrix: Water Durham NC Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540D Total Suspended Solids Analytical Method: SM 254OD-2015 Pace Analytical Services - Eden Total Suspended Solids 13.7 mg/L 2.8 1 09/28/23 15:14 5210B BOD, 5 day EDN Analytical Method: SM 521OB-2016 Preparation Method: SM 521 OB-2016 Pace Analytical Services - Eden BOD, 5 day ND mg/L 2.0 1 09/27/23 09:18 10/02/23 11:18 Field Data Raleigh Analytical Method: Pace Analytical Services - Charlotte Performed by Pace 1 09/28/23 19:15 Collected By TC 1 09/28/23 19:15 Collected Date 09/25/23 1 09/28/23 19:15 Collected Time 09:55 1 09/28/23 19:15 pH 7.2 Std. Units 1 09/28/23 19:15 Temperature 19.7 deg C 1 09/28/23 19:15 Chlorine, Total Residual 9 MG/L mg/L 1 09/28/23 19:15 7782-50-5 Colilert-18 Fecal Coliform RAL Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Raleigh Fecal Coliforms 11.0 MPN/100ml- 1.0 1 09/25/23 14:50 09/26/23 11:40 Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services - Asheville Total Nitrogen 3.4 mg/L 0.040 1 10/06/23 08:49 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia 0.55 mg/L 0.10 1 10/03/23 06:48 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Kjeldahl, Total 2.1 mg/L 0.50 1 10/05/23 14:20 10/06/23 04:17 7727-37-9 353.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, NO2 plus NO3 1.3 mg/L 0.040 1 10/05/23 11:57 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services - Asheville Phosphorus 0.56 mg/L 0.050 1 10/03/2318:00 10/05/2311:02 7723-14-0 Date: 10/09/2023 05:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 4 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Power Sampling Event Pace Project No.: 92690165 QC Batch: 802681 Analysis Method: SM 2540D-2015 QC Batch Method: SM 254OD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92690165001 METHOD BLANK: 4157554 Matrix: Water Associated Lab Samples: 92690165001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Suspended Solids mg/L ND 2.5 09/28/23 15:00 LABORATORY CONTROL SAMPLE: 4157555 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Suspended Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 4157556 92690222001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 176 193 9 SAMPLE DUPLICATE: 4157557 92690101003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 174 184 6 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Power Sampling Event Pace Project No.: 92690165 QC Batch: 802280 Analysis Method: SM 521 OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210B BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92690165001 METHOD BLANK: 4155777 Matrix: Water Associated Lab Samples: 92690165001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers BOD, 5 day mg/L ND 2.0 10/02/23 09:35 LABORATORY CONTROL SAMPLE: 4155778 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 172 87 84.6-115 SAMPLE DUPLICATE: 4155780 92689887002 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 97.5 120 20 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 6 of 19 QUALITY CONTROL DATA Project: Power Sampling Event Pace Project No.: 92690165 QC Batch: 803063 Analysis Method: Colilert-18 QC Batch Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform RAL Laboratory: Pace Analytical Services - Raleigh Associated Lab Samples: 92690165001 SAMPLE DUPLICATE: 4159410 Parameter Units Fecal Coliforms MPN/100mL 92689775002 Dup Result Result RPD Qualifiers 2420 2420 0 El Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 7 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Power Sampling Event Pace Project No.: 92690165 QC Batch: 803656 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92690165001 METHOD BLANK: 4162303 Matrix: Water Associated Lab Samples: 92690165001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 10/03/23 06:32 LABORATORY CONTROL SAMPLE: 4162304 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 4.9 97 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4162305 4162306 MS MSD 92689771002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.0 5.1 99 99 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4162307 4162308 MS MSD 92689773001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 3.9 5 5 8.8 8.7 97 97 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Power Sampling Event Pace Project No.: 92690165 QC Batch: 804042 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92690165001 METHOD BLANK: 4164105 Matrix: Water Associated Lab Samples: 92690165001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 10/06/23 04:01 LABORATORY CONTROL SAMPLE: 4164106 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.2 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4164107 4164108 MS MSD 92689775001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 13.1 10 10 22.7 22.5 96 94 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4164109 4164110 MS MSD 92689775002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 5.9 10 10 15.6 15.6 97 97 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Power Sampling Event Pace Project No.: 92690165 QC Batch: 804326 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92690165001 METHOD BLANK: 4165456 Matrix: Water Associated Lab Samples: 92690165001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg/L ND 0.040 10/05/23 11:55 LABORATORY CONTROL SAMPLE: 4165457 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 100 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4165458 4165459 MS MSD 92690165001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 1.3 2.5 2.5 3.7 3.7 96 98 90-110 1 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA Project: Power Sampling Event Pace Project No.: 92690165 QC Batch: 803558 Analysis Method: EPA 365.1 Rev 2.0 1993 QC Batch Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92690165001 METHOD BLANK: 4161810 Matrix: Water Associated Lab Samples: 92690165001 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/L ND 0.050 10/05/2310:58 LABORATORY CONTROL SAMPLE: 4161811 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/L 2.5 2.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4161812 4161813 MS MSD 92690198001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.064 2.5 2.5 2.6 2.6 101 100 90-110 1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 4161814 4161815 MS MSD 92690198002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Phosphorus mg/L 0.18 2.5 2.5 2.7 2.6 99 97 90-110 2 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALIFIERS Project: Power Sampling Event Pace Project No.: 92690165 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI -The NELAC Institute. ANALYTE QUALIFIERS El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 10/09/2023 05:12 PM without the written consent of Pace Analytical Services, LLC. Page 12 of 19 Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Pace Project No.: Power Sampling Event 92690165 Analytical Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch 92690165001 5719 Poragon Circle, Durham NC SM 254OD-2015 802681 92690165001 5719 Poragon Circle, Durham NC SM 521OB-2016 802280 SM 521OB-2016 802908 92690165001 5719 Poragon Circle, Durham NC 92690165001 5719 Poragon Circle, Durham NC Colilert-18 803063 Colilert-18 803064 92690165001 5719 Poragon Circle, Durham NC TKN+NO3+NO2 804591 Calculation 92690165001 5719 Poragon Circle, Durham NC EPA 350.1 Rev 2.0 1993 803656 92690165001 5719 Poragon Circle, Durham NC EPA 351.2 Rev 2.0 1993 804042 EPA 351.2 Rev 2.0 1993 804549 92690165001 5719 Poragon Circle, Durham NC EPA 353.2 Rev 2.0 1993 804326 92690165001 5719 Poragon Circle, Durham NC EPA 365.1 Rev 2.0 1993 803558 EPA 365.1 Rev 2.0 1993 804008 Date: 10/09/2023 05:12 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 13 of 19 DC# Title; ENV-FRM-HUN9-0083 011 Sample Condition Upon Receipt ace, A��s��= Effective Date; 05M212022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Fluntersville ❑ Raleigh❑ Mechanicsville❑ Atianta❑ Kernersville❑ ••SampleClient Name: ��� WO 92690165 raject #: rI Courier: LJ Fed Ex El UP5 El U5P5 J Client 2590168 ❑ Commercial ❑Pace �f ❑Other: Custody Seal Present? ElYes ? No Seals Intact? ❑ Yes XO'No Packing Material: El Bubble Wrap ❑Bubble Bags El Other Thermometer: n �'One ❑ IR Gun ID. v 1 Type of lce: et ❑ alue -----��� Correction Factor:�//�'�j Cooler Temp: ` Add/Subtract (°C) V Cooler Temp Corrected ("./& USDA Regulated Sall ( water sample) Did samples originat in a Arantine zone within the United States: CA, NY, or SC trher_k mansl? nYes No Date/initials Person Examining Contents: Biological Tis e Frozen?'' / ❑ Yes El ❑ N/A l ❑ NQne Temp should be above freezing to 5°C El Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a foreign source (IntiNto lonaily, includi nx Hawaii and Puerto Rico)? El yes Comments/Discrepancy: Chain of Custody Present? OYes 0 No N/A 1. Samples Arrived within Hold Time? es ❑ No ❑ WA 2, Short Hold Time Analysis (02 hr.)? Yes ❑ No ❑ N/A 3. Rush Turn Around Tlme Requested? ❑ Yes ❑ WA 4. Sufficient Volume? es ❑ No ❑ WA 5. Correct Containers Used? -Pace Containers Used? Y Yes ❑No [:]No ❑WA ❑N/A S. Containers Intact? Yes ❑ No ❑ WA 7. Dissolved analysis: Samples Field Filtered? El %j ❑No N/A 8. Sample Labels Match COC7 -Includes Date/Time/ID/Analysis Matrix: es ❑ No ❑ N/A 9. Headspace In VOA Vials (>5-6mm)? ❑Yes ❑ No /A ID. p BlankPresent7 FBlank CustodySeals Present? ❑Yes ❑Yes ❑No El N/A /A 11. COMMENTS/SAMPLE DISCREPANCY %07r(CATION/RESOLUTION Person contacted; Project Manager SCURF Review: Project Manager SRF Review: Lot ID of split containers: Date/Time: Date; Date: Field Data Required? LJYesI-lerNo I® ni ialrrMV In - AOA1A Dann 1 of') Page 14 of 19 DC#_Title: ENV-FRM-HUN1-0083 v01_Sample Condition Upon Receipt �ce JWkPiCi E�7G5 Effective Date: 05112/2022 *Check mark top half of box If pH and/or dechlorination is verified and project # within the acceptance range for preservation samples. Exceptions: VOA, Collform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottles ***Check all unpreserved Nitrates for chlorine WO#:92690165 PM: RTW Due Date: 10/09/23 CLIENT: 92-ONE TIME m _ z ch C, u v J E In N V a m z a u o J E o In rn a Co z v G u a J E a O N a oa a c r IL Y -' a m u i = u J E n N In rf a m M m u -1 E rrl.11 a m o z v ' E U" N r4 d m u ry ^ O z u J E N V a m a �i ❑ ❑a ? } iD 3 = z v m Q c v = rl +s a V n u d - e-I 2 rI lv a z Z r D m` E N M l7 a v a Q v raj 2 �, " a.-1 f%f ,4 t7 a ry S o. 2 E Ln N N rn l7 a -r Y Z 2 z y E Le) N R cn c9 o Z u p 'J a 2 n+ lh 4 d .- m 0 IIn m p J of a l9 > ¢ Pl n. e a 0 � o Q 7 01 L4 > z 8 a m a p E a o Z d 0 ri ¢ p of N M o a Z '° a 7 .-�. v CL �i M aC > 1 ? u Yn a a; - E In N F a �, 1 -� u 1i, a v in E a N F ii w �., 2 v /0 d E In rV G a m z c � J E o ri 7 a 12 A .5 o - V! a rry > z n E Q E o 7 M a 1 2 3 a s N N\N 7 N L� N\N s \ �S\\ N 10\d N\\� IL 11 ].2 N\N\� \—L L pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot N Note: WheneverthereisadiscrepanryattectingNortnt.arounacompnancesamplrs,dLUpyU4LHl]1UIIIIV4111UC] IKLUuerrululaas�nrloN�,.�..�lul,.al�l,�,.�=ti, Out of hold, incorrect preservative, out of temp, incorrect containers. nijolkrcIv In. rzor,4d pn— ? Page 15 of 19 ry4' 4 4 r+ f„ ul c Q a' 7 _ Y ~ A o A A M1 6 p I i � p a r� c 1 ! cc ,Jp Z 8a. 71 N 9 r O m i t I 3 C31ss 1 M g .�1 HIf IIIlUl41tl - 01 — BUD 5-day Fecal Coli _ ^— T55 K n R c r. Total Nitrogen u S; � (h (' Total Phosphorus r d _ a Fi a R l Lab UnOtif n c � : S - U r9 3i e� ^ � ' n El G Ten o RL G� IL 7 a n w g=_ n _ Pres 6onnornmnfolman�idenUflCd fpff E Page 16 of 19 a v q N o 9 m O N m (i fl �l A /✓ obi = p d m m A L O 3 A a ti A c a m R � 3 g 4 � A v O n p m v o 3 y_ E° f��{' IZ R p R R SO ]C ar f� 3 v O fl n - ft i5 z a 3 a c n O w_ `t 4 o 3 C m' a 3 s a o n r N o $ a 0 � — ro V = r„3 A O � — Ammonia BOD 5-day pm Fecal CollJd TSS� 77 3 3 3 g Total Nitrogen O 9 Total Phosphorus a ti o � c — 3 a c `n ^ A o p v n � X 2 ' n n L m � o N_ 2 a W 6 3 c ..•\ n 1 Lab Use Only ; z z v - ' a d o y'o y c ? o i [H f �$aR R + m c ° Q C" to 0 Q o 03 CD e i V Er it 77 2 O u Page 17 of 19 - preservation nao-conformance identlfied for — sample. W DC# Title: ENV-FRM-HUN1-0083 v01_Sample Condition Upon Receipt ace atiR:Y1fL 5'.Fi�_S Effective Date: 0511212022 Laboratory receiving samples: Asheville ❑ Eden❑ Greenwood ❑ Hunters`viNlle ❑ Raleigh❑ Mechanicsville❑ Atlanta❑ Kernersville❑ /( ct #: Courier: u reu ❑ Commercial ❑ Pace Custody Seal Present? ❑ Yes 0. LJ Other: Seals Intact? ❑Yes )ZNo ❑ Bubble Bags L I'+lone El Other Packing Material: El Bubble Wrap g / Thermometer: ❑ iR Gun ID: Type of Ice: et ❑ Blue ection Factor: 0 Cooler Temp: �WAdrd/subtract ('Q Cooler Temp Corrected (' ): USDA Regulated Soil ( N/A, water sample) Did samples originat in a arantine zone within the United States: CA, NY, or SC (check mapsl? ❑Yes No Chain of Custody Present? Samples Arrived within Hold Time? Short Hold Time Analysis (<72 hr,)? Rush Turn Around Time Requested? Sufficient Volume? Correct Containers Used? -Pace Containers Used? Containers Intact? Dissolved analysis: 5amples Field Filtered? Sample Labels Match COC? -Includes Date[flme/ID/Analysis Matrix: Headspace in VOA Vials (>5-6mm)? Trip Blank Present? Trip Blank Custody Seals Present? COMMENTS/SAMPLE DISCREPANCY ,_ ' &O --WATION/RESOLUTION Person contacted: Project Manager SCURF Review: Project Manager SRF Review: Yes ❑ No ] N/A I. es ❑ No ❑ N/A 2. Yes ❑ No ❑ N/A 3. ] Yes 01<0 ❑ N/A 4. s ❑ No ❑ N/A 5. Y ❑ No ❑ N/A 6. OYes ❑ No ❑ N/A Yes ❑ No ❑ N/A 7. ❑ Ye ❑ No N/A 8. kes ❑ No ❑ N/A 9, Date/Initials Person Examining Contents:'" Biological Tis e Frozen?� ❑ Yes ❑ N/❑ N/A ❑ None Temp should be above freezing to 6°C ❑ Samples out of temp criteria. Samples on ice, cooling process has begun Did samples originate from a Foreign source (inter tionally, including Hawaii and Puerto Rico)? ❑ Yes No Comme nts/Discrepancy: ❑ Yes ❑ No /A 10. ❑ Yes ❑ No f N/A 11. ❑ Yes ❑ No N/A Lot ID of split containers: Date/Time: Date: Date: Field Data Required? LIYes,A�fNo Page 18 of 19 p�no 1 of 7 hllalkrnv In. rQr_1A �ce DC#_Title: ENV-FRM-HUN1-0083 v01 Sample Condition Upon Receipt Effective Date. 05/12/2022 *Check mark top half of box if pH and/or dechlorination is verified and Project # within the acceptance range for preservation samples. Exceptions: VOA, Coliform, 70C, Oil and Grease, DRO/8015 (water) DOC, LLHg **Bottom half of box is to list number of bottles ***Cheek all unpreserved Nitrates for chlorine xs m uQJ Z �d1 o� m CL E ri 7 a m Z > E N 7 a m Z �> ri JE O 7 a m Z U N a `a H 7 a m N 2 a E VI a m v 2 Z E N Z a m Z a Q N E N n.. m N A 2 O Z E cN-1 m a. m Q i6 N -0N L` E LL L9 3 ^ Z � W a c E < a rl Lo a N = a E Q s rl 0 a V Z j a 4 c 7 4 o M 0 a v 2 n O E ai d) N 0 a t4 = Q. d o N of 4n m Q a U Q Z U z ¢o o a P) Q n Q Z O > x M W o>>❑❑ Q ? m > F- M C9 Q Z ai a D O > 7 d1 0 Q ? O DR > > 61 e7 Q Z a Lon Q E LA O1 L9 Z �+ Y ro a > ae I- m I Q ? u ro v E F `na I Q ? V a E ry F a V 0 co N u E N a m U 7 0- c nQ a Q 0 a Q Z N m o , "•m - E N v�i Q '> W > t d o. Qa E T 61 W ❑ 1 N, 2 3 5 6 7 8 9 10 11 12 pH Adjustment Log for Preserved Samples Sample ID Type of Preservative pH upon receipt Date preservation adjusted Time preservation adjusted Amount of Preservative added Lot # Note: Whenever there is a discrepancy attectingNortPLarwinacompuancesamples,acopy oTtnISTormwiuueseniEumervurrnk-droimavrNM�-U[,ncauUnUInLeti.e. Out of hold, incorrect preservative, out of temp, incorrect containers. Page 19 of 19 niinl+rav in. 9OF1d [Dona ? r,f 9