NCG030669_2023 DMR_20230425

NCDEQ Division of Energy,Mineral and Land Resources
Stormwater Discharge Monitoring Report(DMR) Form for NCG030000
Metal Fabrication
Click here for instructions
Complete,sign,scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report(DMR) Upload form within
30 days of receiving sampling results. Mail the original,signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCGO3 0669 Person Collecting Samples: Robert Hensley
Facility Name: AFS MFG LLC Laboratory Name: Pace Analytical
Facility County: ROWAN Laboratory Cert. No.: DW#37706,WW#12, DW#37712,WW#40
Discharge during this period:0 Yes ©No (if no,skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances?DYes ❑No
If so,which Tier(I, II,or Ill)?
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR Eyes ❑No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities—Benchmarks in(Red)
Parameter Parameter Outfall 1 B Outfall 2 Outfall Outfall Outfall
Code
N/A Receiving Stream Class C C
N/A Date Sample Collected MM/DD/YYYY 03/25/2023 03/25/2023
46529 24-Hour Rainfall in inches 0.28" 0.28"
C0530 TSS in mg/L(100 or 50*) <2.5 mg/L <2.5 mg/L
00400 pH in standard units(6.0-9.0 FW, 7.22 7.39
6.8-8.5 SW)
01119 Copper,total recoverable in mg/L <0.0050 mg/Lmg/L
(0.010 FW,0.0058 SW) <0.0050
01051 Lead,total recoverable in mg/L <0.0050 mg/L <0.0050 mg/L
(0.075 FW,0.22 SW)
01094 Zinc,total recoverable in mg/L(0.126 <0.0100 mg/L <0.0100 mg/L
FW,0.095 SW)
Chemical Oxygen Demand(COD)in
00340 mg/L(120) <25.0 mg/L <25.0 mg/L
00552 Non-Polar Oil&Grease in mg/L(15) <4.9 mg/L <4.8 mg/L
* Outfalls to Outstanding Resource Waters(ORW),High Quality Waters(HQW),Trout Waters(Tr)and Primary Nursery Areas(PNA)
have a benchmark TSS limit of 50 mg/L.All other water classifications have a benchmark of 100 mg/L
FW(Freshwater)SW(Saltwater)
Notes(optional):
"I certify by my signature below,under penalty of law,that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted.Based on my
inquiry of the person or persons who manage the system,or those persons directly responsible for gathering the information,the information
submitted is,to the best of my knowledge and belief,true,accurate,and complete.I am aware that there are significant penalties for submitting
false information,including the possibility of fines and imprisonment for knowing violations."
-40 ti) i5 ) z 3
u P ittee or Delegated Authorized Individual Date
(LC'n . i'LL&dy Q Acyur, ► ti1-3 . co 1oW
Email Address Phone Number

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pac.Iabs.com
[phone]
March 30, 2023
Robert Hensley
Agility Fuel Systems
1010 Corporate Center Drive
Salisbury, NC 28146
RE: Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
Dear Robert Hensley:
Enclosed are the analytical results for sample(s)received by the laboratory on March 28, 2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNUNELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
•Pace Analytical Services-Asheville
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
/4 W.4- REPORT OF LABORATORY ANALYSIS
jilt - .
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without the written consent of Pace Analytical Services,LLC. Page 1 of 11

Pace Analytical Services,LLC
a 9800
aceAna/yt vcal Hunte s Ile,NC128078
www.pacelabs.com [phone]
CERTIFICATIONS
Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 Virginia/VELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
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without the written consent of Pace Analytical Services,LLC, Page 2 of 11

Pace Analytical Services,LLC
Kincey Ave. 100
ace Analytical a 9800Huntersv le,NC1te 28078
www.pacslabs.com [phone]
SAMPLE ANALYTE COUNT
Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92659223001 OUTFALL 1B GRAB SM 2540D-2015 JMH1 1 PASI-A
92659223002 OUTFALL 2 GRAB SM 2540D-2015 JMH1 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
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Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersviile,NC 28078
www.pacafabs.com [phone]
ANALYTICAL RESULTS
Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
Sample: OUTFALL 1 B GRAB Lab ID: 92659223001 Collected: 03/25/23 11:30 Received: 03/28/23 15:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 03/29/23 10:44
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:03/30/2023 05:21 PM without the written consent of Pace Analytical Services,LLC. Page 4 0f 11

Pace Analytical Services,LLC
0
aceAnalytical 9800Huntersv vle,Kincey Ave.NC Suite 178
www.pacelab9.eorn [phone]
ANALYTICAL RESULTS
Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
Sample: OUTFALL 2 GRAB Lab ID: 92659223002 Collected: 03/25/23 12:20 Received: 03/28/23 15:00 Matrix:Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids Analytical Method:SM 2540D-2015
Pace Analytical Services-Asheville
Total Suspended Solids ND mg/L 2.5 1 03/29/23 10:44
REPORT OF LABORATORY ANALYSIS
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Date:03/30/2023 05:21 PM without the written consent of Pace Analytical Services.LLC. Page 5 of 11

Pace Analytical Services,LLC
aceAnalytical® 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.cam [phone]
QUALITY CONTROL DATA
Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
QC Batch: 764530 Analysis Method: SM 2540D-2015
QC Batch Method: SM 2540D-2015 Analysis Description: 2540D Total Suspended Solids
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92659223001,92659223002
METHOD BLANK: 3969944 Matrix: Water
Associated Lab Samples: 92659223001,92659223002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Suspended Solids mg/L ND 2.5 03/29/23 10:43
LABORATORY CONTROL SAMPLE: 3969945
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Suspended Solids mg/L 250 240 96 90-110
SAMPLE DUPLICATE: 3970016
92658936001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 362 364 1
SAMPLE DUPLICATE: 3970017
92659144001 Dup
Parameter Units Result Result RPD Qualifiers
Total Suspended Solids mg/L 169 183 8
Results presented on this page are In the units Indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date:03/30/2023 05:21 PM without the written consent of Pace Analytical Services,LLC, Page 6 of 11

Pace Analytical Services,LLC
o 9800 Kincey Ave, Suite 100
aceAnalytical Huntersville,NC 28078
www.pecetabs.com [phone]
QUALIFIERS
Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration.
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration,
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TNI-The NELAC Institute.
REPORT OF LABORATORY ANALYSIS
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Date:03/30/2023 05:21 PM without the written consent of Pace Analytical Services.LLC. Page 7 of 11

Pace Analytical Services,LLC
('9
icai® 9800 Kinsey Ave. Suite 100
Huntersville,NC 28078
www.pacelabs.tom [phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORMWATER 1ST QUARTER TSS
Pace Project No.: 92659223
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92659223001 OUTFALL 1 B GRAB SM 2540D-2015 764530
92659223002 OUTFALL 2 GRAB SM 2540D-2015 764530
REPORT OF LABORATORY ANALYSIS
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Date:03/30/2023 05:21 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 11

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Page 11 of 11

Pace Analytical Services,LLC
'' 9800 Kincey Ave. Suite 100
ace Analytical Huntersville,NC 28078
www.pacalabs.com
[phone]
April 11, 2023
Robert Hensley
Agility Fuel Systems
1010 Corporate Center Drive
Salisbury, NC 28146
RE: Project: STORMWATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
Dear Robert Hensley:
Enclosed are the analytical results for sample(s)received by the laboratory on March 28,2023. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual,where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services-Asheville
• Pace Analytical Services-Charlotte
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Tyriek Hooks
[e-mail]
[phone]
Project Manager
Enclosures
cc: Kulema McKoy,Hexagon Agility
_ '�\��- REPORT OF LABORATORY ANALYSIS
y' This report shall not be reproduced,except in full,
• without the written consent of Pace Analytical Services,LLC. Page 1 of 13

Pace Analytical Services,LLC
aceAnalytical^ 9800 Kincey Ave. Suite 100
Huntersville,NC 28078
wwx.pacclabs.ccrn
( [phone]
CERTIFICATIONS
Project: STORMWATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
Pace Analytical Services Charlotte
South Carolina Laboratory ID:99006 South Carolina Certification#:99006001
9800 Kincey Ave.Ste 100,Huntersville,NC 28078 South Carolina Drinking Water Cert.#:99006003
North Carolina Drinking Water Certification#:37706 Florida/NELAP Certification#:E87627
North Carolina Field Services Certification#:5342 Kentucky UST Certification#:84
North Carolina Wastewater Certification#: 12 Louisiana DoH Drinking Water#:LA029
South Carolina Laboratory ID:99006 VirginiaNELAP Certification#:460221
Pace Analytical Services Asheville
2225 Riverside Drive,Asheville,NC 28804 South Carolina Laboratory ID:99030
Florida/NELAP Certification#:E87648 South Carolina Certification#:99030001
North Carolina Drinking Water Certification#:37712 VirginiaNELAP Certification#:460222
North Carolina Wastewater Certification#:40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 2 of 13

Pace Analytical Services,LLC
a
9800 KinceyAve. Suite 100
ceAnalytica! Huntersville.NC 28078
www.patelabs.cam [phone]
SAMPLE ANALYTE COUNT
Project: STORMWATER 1ST QUARTER FORAGI
Pace Project No.: 92659236
Analytes
Lab ID Sample ID Method Analysts Reported Laboratory
92659236001 OUTFALL 1 B GRAB EPA 1664B REL 1 PASI-C
EPA 200.7 Rev 4.4 1994 DBB1 3 PASI-A
SM 5220D-2011 JMH1 1 PASI-A
92659236002 OUTFALL 2 GRAB EPA 1664B REL 1 PASI-C
EPA 200.7 Rev 4.4 1994 DBB1 3 PASI-A
SM 5220D-2011 JMH1 1 PASI-A
PASI-A=Pace Analytical Services-Asheville
PASI-C=Pace Analytical Services-Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
without the written consent of Pace Analytical Services,LLC. Page 3 of 13

Pace Analytical Services,LLC
'*ace Analytical 9800 KlnceyAve. Suite'IOC)Huntersvitle,NC 28078
•
wwar.pacelabs.cam [phone]
ANALYTICAL RESULTS
Project: STORMWATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
Sample: OUTFALL 1B GRAB Lab ID: 92659236001 Collected: 03/25/23 11:30 Received: 03/28/23 15:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua!
1664 SGT-HEM,TPH Analytical Method:EPA 1664B
Pace Analytical Services-Charlotte
Total Petroleum Hydrocarbons ND mg/L 4.9 1 03/31/23 09:49
200.7 MET ICP Analytical Method:EPA 200.7 Rev 4.4 1994 Preparation Method: EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper ND ug/L 5.0 1 04/04/23 10:05 04/05/23 17:29 7440-50-8
Lead ND ug/L 5.0 1 04/04/23 10:05 04/05/23 17:29 7439-92-1
Zinc ND ug/L 10.0 1 04/04/23 10:05 04/05/23 17:29 7440-66-6
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand ND mg/L 25.0 1 03/30/23 10:52 03/30/23 16:42
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/11/2023 05:22 PM without the written consent of Pace Analytical Services,LLC. Page 4 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
rfaceAnalytical Huntersvine,NC 28078
www.pacelabs.com [phone]
ANALYTICAL RESULTS
Project: STORM WATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
Sample: OUTFALL 2 GRAB Lab ID: 92659236002 Collected: 03/25/23 12:20 Received: 03/28/23 15:00 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qua!
1664 SGT-HEM,TPH Analytical Method: EPA 16648
Pace Analytical Services-Charlotte
Total Petroleum Hydrocarbons ND mglL 4.8 1 03/31/23 09:49
200.7 MET ICP Analytical Method: EPA 200.7 Rev 4.4 1994 Preparation Method:EPA 200.7 Rev 4.4 1994
Pace Analytical Services-Asheville
Copper ND ug/L 5.0 1 04/04/23 10:05 04/05/23 17:32 7440-50-8
Lead ND ug/L 5.0 1 04/04/23 10:05 04/05/23 17:32 7439-92-1
Zinc ND ug/L 10.0 1 04/04/23 10:05 04/05/23 17:32 7440-66-6
5220D COD Analytical Method:SM 5220D-2011 Preparation Method:SM 5220D-2011
Pace Analytical Services-Asheville
Chemical Oxygen Demand ND mg/L 25.0 1 03/30/23 10:52 03/30/23 16:43
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full.
Date:04/11/2023 05:22 PM without the written consent of Pace Analytical Services,LLC. Page 5 of 13

Pace Analytical Services,LLC
9800 Kincey Ave. Suite 100
GaceAnalytical Huntersville,NC 28078
www,pacolabs. ara [phone]
QUALITY CONTROL DATA
Project: STORM WATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
QC Batch: 765035 Analysis Method: EPA 1664E
QC Batch Method: EPA 16648 Analysis Description: 1664 SGT-HEM,TPH
Laboratory: Pace Analytical Services-Charlotte
Associated Lab Samples: 92659236001,92659236002
METHOD BLANK: 3972568 Matrix: Water
Associated Lab Samples: 92659236001,92659236002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Total Petroleum Hydrocarbons mg/L ND 5.0 03/31/23 09:49
LABORATORY CONTROL SAMPLE: 3972569
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mg/L 20 18.0 90 64-132
MATRIX SPIKE SAMPLE: 3972570
92659110002 Spike MS MS %Rec
Parameter Units Result Conc. Result %Rec Limits Qualifiers
Total Petroleum Hydrocarbons mglL ND 20 20.5 94 64-132
SAMPLE DUPLICATE: 3972571
92659396002 Dup
Parameter Units Result Result RPD Qualifiers
Total Petroleum Hydrocarbons mg/L ND ND
Results presented on this page are in the units indicated by the"Units"column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/11/2023 05:22 PM without the written consent of Pace Analytical Services,LLC. Page 6 of 13

Pace Analytical Services,LLC
c 9800 Kincey Ave. Suite 100
6aceAnalytical Huntersville,NC 28078
wwv.pacelabs.cam [phone]
I
QUALITY CONTROL DATA
Project: STORMWATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
QC Batch: 765678 Analysis Method: EPA 200.7 Rev 4.4 1994
QC Batch Method: EPA 200.7 Rev 4.4 1994 Analysis Description: 200.7 MET
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92659236001,92659236002
METHOD BLANK: 3975543 Matrix: Water
Associated Lab Samples: 92659236001,92659236002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Copper ug/L ND 5.0 04/05/23 16:01
Lead ug/L ND 5.0 04/05/23 16:01
Zinc ug/L ND 10.0 04/05/23 16:01
LABORATORY CONTROL SAMPLE: 3975544
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Copper ug/L 500 527 105 85-115
Lead ug/L 500 541 108 85-115
Zinc ug/L 500 547 109 85-115
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3975545 3975546
MS MSD
92657942002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper ug/L ND 500 500 505 509 100 101 70-130 1
Lead ug/L ND 500 500 486 485 97 97 70-130 0
Zinc ug/L 52.1 500 500 562 557 102 101 70-130 1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3975547 3975548
MS MSD
92658520003 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Copper ug/L ND 500 500 530 525 102 101 70-130 1
Lead uglL ND 500 500 486 478 97 96 70-130 2
Zinc ug1L 871 500 500 1400 1390 106 103 70-130 1
Results presented on this page are In the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/11/2023 05:22 PM without the written consent of Pace Analytical Services,LLC. Page 7 of 13

Pace Analytical Services,LLC
9800 KlnceyAve. Suite 100
6'aceAnalytical Huntersvilre,NC 28078
www.pacolabs.com [phone]
QUALITY CONTROL DATA
Project: STORM WATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
QC Batch: 764857 Analysis Method: SM 5220D-2011
QC Batch Method: SM 5220D-2011 Analysis Description: 5220D COD
Laboratory: Pace Analytical Services-Asheville
Associated Lab Samples: 92659236001,92659236002
METHOD BLANK: 3971486 Matrix: Water
Associated Lab Samples: 92659236001,92659236002
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Chemical Oxygen Demand mg/L ND 25.0 03/30/23 16:41
LABORATORY CONTROL SAMPLE: 3971487
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Chemical Oxygen Demand mg/L 750 746 99 90-110
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3971488 3971489
MS MSD
92658861002 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 238 100 100 351 351 112 112 90-110 0 M1
MATRIX SPIKE&MATRIX SPIKE DUPLICATE: 3971490 3971491
MS MSD
92658906001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Cone. Result Result %Rec %Rec Limits RPD Qual
Chemical Oxygen Demand mglL 161 100 100 287 287 126 126 90-110 0 M1
Results presented on this page are In the units indicated by the"Units"column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/11/2023 05:22 PM without the written consent of Pace Analytical Services,LLC. Page 8 of 13

Pace Analytical Services,LLC
Kincey Ave. Suite 100
"aceAnalyi 9800 cal Huntersville,NC 28078
www.pacelabs.com
( [phone]
QUALIFIERS
Project: STORM WATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
DEFINITIONS
DF-Dilution Factor,if reported,represents the factor applied to the reported data due to dilution of the sample aliquot.
ND-Not Detected at or above adjusted reporting limit.
TNTC-Too Numerous To Count
J-Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL-Practical Quantitation Limit.
RL-Reporting Limit-The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S-Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270.The result for each analyte is
a combined concentration,
Consistent with EPA guidelines,unrounded data are displayed and have been used to calculate%recovery and RPD values.
LCS(D)-Laboratory Control Sample(Duplicate)
MS(D)-Matrix Spike(Duplicate)
DUP-Sample Duplicate
RPD-Relative Percent Difference
NC-Not Calculable.
SG-Silica Gel-Clean-Up
U-Indicates the compound was analyzed for,but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting.Therefore,calculated parameters that are typically reported as
"Total"may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited.Contact your Pace PM for the current list of accredited analytes.
TM-The NELAC Institute.
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample(LCS)recovery.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04111/2023 05:22 PM without the written consent of Pace Analytical Services,LLC. Page 9 of 13

Pace Analytical Services,LLC
c 9800 Kincey Ave. Suite 100
race Analytical Huntersville,NC 28078
wwW,pacalabs.com
[phone]
t
I
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: STORM WATER 1ST QUARTER FOR AGI
Pace Project No.: 92659236
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92659236001 OUTFALL 1 B GRAB EPA 1664E 765035
92659236002 OUTFALL 2 GRAB EPA 1664E 765035
92659236001 OUTFALL 1 B GRAB EPA 200.7 Rev 4.4 1994 765678 EPA 200.7 Rev 4.4 1994 765868
92659236002 OUTFALL 2 GRAB EPA 200.7 Rev 4.4 1994 765678 EPA 200.7 Rev 4.4 1994 765868
92659236001 OUTFALL 1B GRAB SM 5220D-2011 764857 SM 5220D-2011 764987
92659236002 OUTFALL 2 GRAB SM 5220D-2011 764857 SM 5220D-2011 764987
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced,except in full,
Date:04/11/2023 05:22 PM without the written consent of Pace Analytical Services,LLC. Page 10 of 13

. DC-#,:Tfttet::ENV.FRM HUN:1•0003 YQg:_,Sampi.0::ContiiE oil;' Upon' locelpt•
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.: - ., ----- kot;io of s'piks,ptalners:
ct.IENtot xt ckr o itioc turia,N .
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.. hate_ ime; •
Project;litlanager SCURF Reviews tD.'ate; •
Project Manager.SRFReview:: . Dake;
Page 11 of 13
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