WQ0013263_2022 Residual Annual Report_20230323 (2)

Initial Review
Reviewer
Nathaniel.Thornburg
Is this submittal an application? (Excluding additional information.) *
Yes No
If not an application what is the submittal type?* Annual Report
Residual Annual Report
Additional Information
Other
Annual Report Year* 2022
Permit Number (IR) * WQ0013263
Applicant/Permittee Town of Boone
Email Notifications
Does this need review by the hydrogeologist? * Yes U No
Regional Office Winston-Salem
CO Reviewer
Admin Reviewer

Submittal Form
Project Contact Information
Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence.
Name* Mike Everett
Email Address*
[e-mail]
Project Information
.........................
Application/Document Type*
New (Fee Required)
Modification - Major (Fee Required)
Renewal with Major Modification (Fee
Required)
Annual Report
Additional Information
Other
Phone Number*
828-268-6270
Modification - Minor
Renewal
GW-59, NDMR, NDMLR, NDAR-1,
N DAR-2
Residual Annual Report
Change of Ownership
We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form.
https://edoes.deq.nc.gov/Forms/NonDischarge_Monitoring_Report
Permit Type:*
Wastewater Irrigation
High -Rate Infiltration
Other Wastewater
Reclaimed Water
Closed -Loop Recycle
Residuals
Single -Family Residence Wastewater
Other
Irrigation
Permit Number:*
WQ0013263
Has Current Existing permit number
Applicant/Permittee Address*
PO Box 192, Boone, NC 28607
Facility Name*
Town of Boone Class A Residuals Program
Please provide comments/notes on your current submittal below.
The original submission was only the cover letter.
At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg
at [e-mail].
Please attach all information required or requested for this submittal to be reviewed here.
(Application Form, Engineering Plans, Specifications, Calculations, Etc.)
20230202102959825.pdf
7.24MB
Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger
than upload limit.
* By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has
been received by the Non -Discharge Branch. Application fees must be submitted by check or money order and made payable to the
North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts
of the application in correct order (as specified by the application).
Mail payment to:
NCDEQ — Division of Water Resources
Attn: Non -Discharge Branch
1617 Mail Service Center
Raleigh, NC 27699-1617
Signature
04r&zW 0"'?*
Submission Date 3/23/2023

1/31/23
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Attached is the Town of Boone's 2022 Class A residuals program annual report.
Our system employs a thermal drier by a natural gas steam generator. Heat is transferred
to the residuals through a hollow rotor via a series of concentric disks in the drier. The
system is manufactured by Atlas-Stord, Inc. The enclosed report includes a technical
specifications section for your reference.
To assist your review, we have included summaries on production volume, the quantity
distributed, and information on each recipient.
We tested for quarterly for metals and fecal coliform . All of our test results were within
our permitted requirements.
We will promptly provide any additional records you may request to verify compliance
of this system with the regulations for Class A residuals distribution. If there is any need,
please contact me at [phone].
Sincerely,
Mike Everett
Chief Operator
cc: Rudy Broschinski, Wastewater Treatment Superintendent
Rick Miller, Director of Public Utilities
P.O. DRAWER 192 • BOONE, NORTH CAROLINA 28607

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ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 1/1/2022 To 3/31/2022
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 0
Alternative 2 []
I Alternative ; Elr
Alternative 4 El
Altemative 5
Alternative 6 EJ
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost Cj
Heat Diving 121i
Heat Treatment El
Thermophilie
Beta Ray 0
Gamma Ray LEJ
Pasteurization El
Class B:
Alternative 1 0
Alternative 2 El
If applicable to alternative
performed (Class B only indicate "Process to Significantly- Reduce Pathogens":
Lime Stabilization
Air Diving
Composting
Aerobic Digestion
Anaerobic Digestion El
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
um er o
Excee-
d ces
Frequency
of Analysis
Sample
Type
Analytical
Tech -
i
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
88
190
412
MPN/g
Quarterly
grab
9221-E
Salmonella bacteria
(in lieu of fecal
coliform
3 WN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction) 0
Alt. 2 (40-day bench) El
Alt. 3 (30-day bench) 0
1 Alt. 4 (Spec. 02 uptake) 11
Alt. 5 (14-Day Aerobic) El
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) R1
jAlt. 8 (Drying - Unstable) El
Alt. 9 (Injection) 0
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed Ill
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been. met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
{
Mike Everett Chief Operator
Preparer Name and Title (type or p ' t)
AJI�0-4 / , F�Xo1�
Signature of Preparer*
NA
Land Applier Name and Title (if applicable)(type or print)
1-31- �3
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 4/1/20222 To 6/30/2022
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 El
Alternative 2 0
Alternative 3 El e
Alternative 4 0
Alternative 5
AlternatiVe 6 El
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost 11
Heat Drying
Heat Treatment
Thermophilic
Beta Ray 0
Gamma Ray 0
Pasteurization
Class B:
Alternative l
Alternative 2
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization EJ
Air DryingEj
Composting El
lAerobic Digestion El
Anaerobic Digestion El
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number ot
Excee-
e ces
Frequency
of Analysis
y
Sample
Type
a ytica
Tech -
i gue
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
84
137
223
MPN/G
Quarterly
grab
9221 E
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weigut
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.1 (VS reduction) 0
Alt. 2 (40-day bench) El
Alt. 3 (30-day bench) 0
Alt. 4 (Spec. 02 uptake) El
Alt. 5 (14-Day Aerobic) 0
Alt. 6 (Alk. Stabilization El
Alt 7 (Drying - Stable) 21
Alt. 8 (Drying - Unstable) El
Alt. 9 (Injection) 0
Alt. 10 (Incorporation) Q
No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
a
Mike Everett Chief Operator
Preetp/arer NameandTitle (type or print)
//1a,r�noY , A, &'Of�k
Signature of Preparer*
NA
Land Applier Name and Title (if applicable)(type or print)
1 3/-oI3
Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number: WQ0013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 7/l/2022 To 9/30/2022
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 Cl:
Alternative 2 0
Alternative
Alternative 4 0
Alternative 5 21
Alternative 6 I
If applicable to alternative
performed (Class A only) indicate "Process to Further
Reduce Pathogens":
Compost El
Heat Diving Z
Heat Treatment 0
Thermophilic EJ
Beta Ray 0
Gamma Ray 0
Pasteurization i
Class B:
Alternative 1 El
Alternative ? �
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization D
Air Diving®
Composting 0
jAerobic Digestion EJ
Anaerobic Digestion 1
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Bences e-
Frequency
of Analysis
Sample
Type
Analytical
Tech -
i ue
MinimumGeo.
Mean
MaximumUnits
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
234
289
358
MPN/G
Quarterly
grab
9221 E
Salmonella bacteria
(in lieu of fecal
coliform
3 MPN per 4 grams
total solid (dry
weiLhjt
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction) 01
Alt. 2 (40-day bench) El
Alt. 3 (30-day bench) El
Alt. 4 (Spec. 02 uptake) El
Alt. 5 (14-Day Aerobic) El
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) 21
Alt. 8 (Drying - Unstable) El
Alt. 9 (Injection)
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator NA
Preeparer Name and Title(ype or print) Land Applier Name and Title (if applicable)(type or print)
&",2 a, &Le'D*
Signature of Preparer* Date Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (503 Rules)
Facility Name: Town of Boone WQ Permit Number: W00013263
WWTP Name: Town of Boone Jimmy Smith Wastewater Plant NPDES Number: NCO020621
Monitoring Period: From 10/12022 To 12/31/2022
Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 0
Alternative 2 0
Alternative 3 El
Alternative 4 El
AlteruatiN.e 5
Alternative 6 El
If applicable to alternative
performed (('lass A only-) indicate "Process to Further
Reduce Pathogens":
Compost
Heat Drying &I
Heat Treatment D
Thernlophilic El
Beta Ray l
Ganuna RayEl
Pasteurization El
Class B:
AlternatiVe 1 0
Alternative 2
If applicable to alternative
performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization
Air Dryings
Composting
Aerobic Digestion El
Anaerobic Digestion it
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Allowable Level Pathogen Density Number ot
Excee-
Frequency Sample Analytical
Tech -
Parameter in Sludge
in Minimum Geo. Mean axim Units e
Y T e
of Anal sis yp
2 x 10 to the
MPN
6th power
per gram of
Fecal Coliform
total solids
CFU
1000 mpn per gram
of total solid (dry
243
328
444
MPN/G
Quarterly
grab
9221 E
weight)
Salmonella bacteria
3 MPN per 4 grams
(in lieu of fecal
total solid (dry
colifonn
weiliLt
Veetnr Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Alt.l (VS reduction) Cj
Alt. 2 (40-day bench) L-]
Alt. 3 (30-day bench) -
Alt. 4 (Spec. 02 uptake)
Alt. 5 (14-Day Aerobic) [I
Alt. 6 (Alk. Stabilization
Alt 7 (Drying - Stable) RI
I Alt. 8 (Drying - Unstable) ?-
Alt. 9 (Injection) El
Alt. 10 (Incorporation) 0
No vector attraction reduction alternatives were performed
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Mike Everett Chief Operator
P,Nree�parer Nam and Title (type or rint)
III, And l A, 1"-�u
Signature of Preparer*
NA
Land Applier Name and Title (if applicable)(type or print)
/-31--cl3
Date
Signature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 503 (12/2006)

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Omer Log q fl�- L� W—bj\\

Town of Boone Wastewater Treatment Plant
2022 Class Residuals Production
Run
Gallons
Digester
Total
No.
Run Date
Processed
% Solids
Dry Tons Notes
s
1
1-/3/2022
131,061
2.61
14.30
2
1/10/2022
166,998
2.30
16.00
3
1/18/2022
84,556
2.51
8.85
4
1/ 24/ 2022
312,857
2.21
28.83
5
1/31/2022
160,656
2.28
15.27
6
2/7/2022
209,276
2.35
20.50
7
2/142022
283,262
2.35
27.76
8
2/21/2022
251,554
2.31
24.23
9
2/28/2022
217,731
2.35
21.37
10
3 / 7/ 2022
333,996
2.23
31.05
11
3/14/2022
179,682
2.19
16.41
12
3/21/2022
158,542
2.22
14.68
13
3/28/2022
219,846
2.09
19.16
14
4/4/2022
247,326
2.16
22.28
15
4/11/2022
177,568
2.20
16.29
16
4/25/2022
190,251
2.30
18.25
17
5/2/2022
183,909
2.10
16.10
18
5/ 10/ 2022
179,682
2.31
17.31
19
5/16/2022
143,745
2.13
12.77
20
5/23/2022
154,315
2.20
14.16
21
5/31/2022
158,543
2.18
14.41
22
6/ 13/ 2022
97,239
2.70
10.95
23
6/21/2022
236,756
2.35
23.20
24
7/ 5/ 2022
23,253
2.33
2.26
25
7/ 11 / 2022
156,429
2.64
17.22
26
7/25/2022
88,784
2.52
9.33
27
8/1/2022
84,556
2.57
9.06
28
8/8/2022
150,087
2.99
18.71
29
8/ 22/ 2022
135,290
2.99
16.87
30
8/29/2022
200,821
3.04
25.46
31
9/12/2022
243,099
2.77
28.08
32
9/19/2022
150,087
2.86
17.90
33
9/26/2022
126,834
2.76
14.60
34
10/3/2022
137,404
2.86
16.39
35
10/10/2022
145,860
2.84
17.27
36
10/17/2022
270,579
2.84
32.04

37
10/24/2022
131,062
3.04
16.61
38
10/31/2022
169,112
2.72
19.18 r
39
11 /7/2022
93,012
2.63
10.20
40
11/14/2022
198,707
2.65
21.96
41
11 /21 /2022
118,378
2.88
14.22
42
11 /28/2022
52,847
2.89
6.37
43
12/5/2022
705,048
2.91
24.88
44
12/12/2022
101,467
2.90
12.27
45
12/19/2022
143,745
2.81
16.84
46
12/28/2022
179,681
2.66
19.93
Totals
7,785,493
811.78
A
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High Coup y 6-1-0 Mosall6ds
.Produced by the Town of Boone
P.O. Drawer 192, Boone, NC 28607
High country 6-1-0 (HC 610) is a high organic content fertilizer manufactured by the Town of Boone
Wastewater Treatment Facility. This product produces superior results on lawns, flower beds and
shrubs providing nutrients at the rates indicated below:
Guaranteed Analysis
Total Nitrogen
...................... ...................
Water Insoluble Nitrogen .....................
o/
. ...................
Available Phosphoric Acid
3.5%
..........................................
Soluble Potash
1%
.....................
Iron.................................................................................
o
1%
Recommended Application
Rates
Lawn -Sod Establishment: Apply HC 610 at rate of 30 Ibs per 1DDD sq feet.
Turf Maintenance: 'Apply HC 610 at a rate of 10-15 Ibs per 100D.sq feet.
Plant Bed Establishment: Apply HC 610 at a rate of 2 Ibs per 100 sq feet into soil..
Planting Bed Maintenance: Apply HC 610 at a rate of 2 Ibs per 100 sq feet in Spring/Fall
Warnings: HC 61D- is environmentally safe when used as directed, but can become a hazard if
mismanaged. This product should not be used bn Solis intended for food crop production.
Cover HC 610 with a tarp or plastic during transportation. Store HC 610 in a dry area away from wells
or surface water where it could be washed into streams; keep product away from children`s play
areas.
Limited Warranty and Disclaimer: The Town of Boone warrants that HC 610 meets the specifications
stated above, and that the heavy metal content is less than or equal to the limitations specified in the
EPA and NC Dept of Environmental and Natural Resources sludge quality criteria for land application.
If HC 610 fails to meet its specification, the buyer's sole remedy shall be the recovery of the purchase
price. Under no circumstances shall the Town of Boone be liable for any other 'damages, including
direct, indirect, consequential or special damages.
The undersigned Buyer agrees to abide by the following Restrictions:
HC 610 shall not be applied to land except in accordance with the instructions contained herein.
HC 610 shall not be applied to any site that is flooded, frozen, or snow-covered.
HC 610 shall not be applied within 1D0 feet of any water supply, stream, river, or lake.
Adequate measures shall be provided to prevent surface
surface waters. runoff from carrying this product into any
Buyer Signature Date
Name (Print): Quantity:
Ibs/tons
Street/Route: Intended Use:.
City/State/Zip: Amount Collected:
Telephone: Loaded By:

aceAnalXical
www.pacelabs.com
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Project: Town of Boone - Biosolids
Pace Project No.: 92582582
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 2
Report Date: 02/02/2022
Date Received: 01/13/2022
Sample: Biosolids
Lab ID: 92582582001 Collected: 01/13/22 08:00 Matrix:
Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Method
Parameters
Results
Units
Report Limit
Analyzed
Qualifiers
EPA 601 OD
Aluminum
12700
mg/kg
10.9
01/20/22 20:50
EPA 601 OD
Arsenic
3.8
mg/kg
3.3
01/20/22 20:50
EPA 601 OD
Cadmium
1.5
mg/kg
1.1
01/20/22 20:50
EPA 601 OD
Calcium
24100
mg/kg
109
01/20/22 20:50
EPA 601 OD
Copper
494
mg/kg
4.4
01/20/22 20:50
EPA 601 OD
Lead
28.2
mg/kg
2.7
01/20/22 20:50
EPA 601 OD
Magnesium
2880
mg/kg
5.4
01/20/22 20:50
EPA 601 OD
Molybdenum
4.5
mg/kg
4.4
01/20/22 20:50
EPA 601 OD
Nickel
15.7
mg/kg
2.2
01/20/22 20:50
EPA 601 OD
Potassium
3410
mg/kg
21.8
01/20/22 20:50
EPA 601 OD
Selenium
ND
mg/kg
4.4
01/20/22 20:50
EPA 601 OD
Silver
3.1
mg/kg
1.1
01/20/22 20:50
EPA 601 OD
Sodium
1160
mg/kg
109
01/20/22 20:50
EPA 601 OD
Zinc
1040
mg/kg
2.2
01/20/22 20:50
EPA 7471B
Mercury
0.37
mg/kg
0.26
01/21/2212:23
EPA 601 OD
Sodium Adsorption Ratio
2.0
meq/L
01/26/22 16:44
N2
SM 2540G-2011
Total Solids
90.1
%
0.10
01/14/22 16:38
SW-846
Percent Moisture
9.9
%
0.10
01/14/22 16:30
N2
EPA 9045D
pH at 25 Degrees C „
6.0
Std. Units
0.10
01 /17/22 15:45
H3
None
Plant Available Nitrogen
2610
mg/kg
02/02/22 15:31
N2
EPA 365.1 Rev 2.0 1993
Phosphorus
12600
mg/kg
277
01 /24/22 22:25
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
Page 1 of 15

accAnalytical "'
www.pacelabs.com
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
Pace Analytical Services Peachtree Corners
110 Technology Pkwy, Peachtree Corners, GA 30092
Florida DOH Certification #: E8.7315
Georgia DW Inorganics Certification #: 812
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Certification #: 381
South Carolina Certification #: 98011001
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 2
Page 2 of 15

9610 C 9513d
TEMP in G
Received an
Ice
(YIN)
q
ITEM
o
m
r
D
b o,
go
co
Q
-D
i3
ol
C.)
o
ED
0o
cl
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o
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o
q
Lt
c.
a,
T
ED
M.y err
cL
o
z
z
to
MATRIX, CODE valid codes to lest)
C
G)
&AMPLE TYPE (o--GRAB c=comp)
IS
m
rri
z
V
I
T COLLECTION
OF CONTAINERS
UnpreseTvad
H2SO4
HNO3
'0
HCI
NaOH
Na2S203
....... ...
Methanol
jV,
Other
5`7
31;,11
NH3-N (EPA 350,1), TKN (EPA
1351.2), N034402 (EPA353.2)
Plant Avallable.Kilro an (PAN)
lit
calcutatijon
x
Total Phosphorus (EPA 365. 1)
x
Percent Total Solids (SM 2540G)
Aluminum, Arsenic, Cadmium,
Calalum Copper, Lead, Magnesium,
x
Molybdenum, :NI&,et, Potassium,
Selenium, SodJum,2jnC.(EPA 150101
Sodium Absorption Rate ISAR)
x
calculation
Mercury (EPA7471Bj
PH (EPA 90.45D)
z
Residual Chlorine {YIN)
tr
>
=r
w
Er Z
6 9
''0
0
rn
Mr- 0
F
,0-
0 >
Ri
1<
>
fU
CD
CL
Ut
CD
0
3
(",I)

Table of Contents
con-testo
A Pace AnaVlcalO Laboratory
39 Spruce Street' East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
February 2, 2022
Stephanie Knott
Pace Analytical Services - NC
1377 South Park Dr.
Kemersville, NC 27284
Project Location: Town of Boone-Biosolids
Client Job Number:
Project Number: 92582582
Laboratory Work Order Number: 22A0729
Enclosed are results of analyses for samples as received by the laboratory on January 14, 2022. If you have any questions
concerning this report, please feel free to contact me.
Sincerely,
i
Raymond J. McCarthy
Project Manager
Page 1 of 12

Table of Contents
Table of Contents
Sample Summary
Case Narrative
Sample Results
22AO729-01
Sample Preparation Information
QC Data
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
B299215
B299644
B300021
Flag/Qualifier Summary
Certifications
Chain of Custody/Sample Receipt
r 3
4
5
5
6
7
7
7
7
7
8
9
10
g
Page 2 of 12

Table of Contents
con -test&
A Pace Analytical- Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Pace Analytical Services - NC
1377 South Park Dr. REPORT DATE: 2/$/2022
Kernersville, NC 27284 PURCHASE ORDER NUMBER:
ATTN: Stephanie Knott
PROJECT NUMBER: 92582582
ANALYTICAL SUMMARY
WORK ORDER NUMBER: 22AO729
The results of analyses perfonned on the following samples submitted to CON -TEST, a Pace Analytical Laboratory, are found in this report.
PROJECT LOCATION: Town of Boone-Biosolids
FIELD SAMPLE # LAB ID: MATRIX SAMPLE DESCRIPTION TEST SUB LAB
Biosolids 22AO729-01 Soil NECi N07-0003
Modified
SM 2540G
SM19-23 4500-N Org
B,C-NH3 C Modified
SM21-23 4500 NH3 C
Modified
0
I
Vf
pn­
Page 3 of 12

con-test'9
A Face Anatytical'a Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Cax,M3I -14*1*Tlil%a7MIM,1u/:11 1
All reported results are within defined laboratory quality control objectives unless listed below or otherwise qualified in this report.
REVISED REPORT - 1/27/2022 - Total nitrogen added per clients request.
The results of analyses reported only relate to{samples submitted to Con -Test, a Pace Analytical Laboratory, for testing.
I certif}/that the analyses listed above, unless specifically listed as subcontracted, if any, were performed under my direction according to the approved methodologies listed
in this document, and that based upon my inquiry of those individuals immediately responsible for obtaining the information, the material contained in this report is, to the
best of my knowledge and belief, accurate and complete.
J
Lisa A. Worthington v
Technical Representative
Table of Contents
Page 4 of 12

con -test@
A Pace Analytical" Laboratory
Table of Contents
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Project Location: Town of Boone-Biosolids Sample Description: Work Order: 22AO729
Date Received: 1/14/2022 1
Field Sample #: Biosolids Sampled: 1/13/2022 08:00
Samole ID: 22AO729-01
Samole Matrix: Soil
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total)
Date
Date/'Time
Analyte
Results
RL
DL Units
Dilution Flag/Qual
Method
Prepared
Analyzed
Analyst
% Solids
66.6
% Wt
I
SM 2540G
1/15/22
1/17/22 12:49
JMW
Ammonia as N
1200
42
25 mg/Kg dry
1
SM21-23 4M0 NH3 C
1/19/22
1/20/22 9:10
FAT
Modified
Nitrate/Nitrite as N
ND
2.5
mg/Kg
1
NECi N07-0003
1/31/22
1/31/22 16:00
IS
Modified
Total Kjeldahl Nitrogen
7900
30
2.1 mg/Kg dry
1
SM19-23 4500-N Org
1/25/22
1/26/22 13:41
EC
B,C-NH3 C Modified
Total Nitrogen
7900
10
mg/Kg
1
SM19-23 4500-N Org
2/2/22
2/2/22 11:00
LL
B,C-NH3 C Modified
t
Page 5 of 12

Table of Contents
con -test&
A Face AnalyticatO laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
Sample Extraction Data
1
NEC! N07-0003 Modified
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
22AO729-01 [Biosolids]
B300021
1.00
50.0
01/31/22
Prep Method: % Solids Analytical Method: SM 254OG
Lab Number [Field ID]
Batch
Date
22AO729-01[13iosolids]
B299021
01/15/22
Prep Method: SM4500 N Org B C Analytical Method: SM19-23 4500-N Org B,C-NH3 C Modified
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
22AO729-01 [Biosolids]
B299644
5.04
100
01/25/22
SM19-23 4500-N Org B,C-NH3 C Modified
Lab Number [Field ID]
Batch
Initial [g]
Date
22AO729-01 [Biosolids]
B300233
5.00
02/02/22
Prep Method: SM 4500-NH3 C Analytical Method: SM21-23 4500 NH3 C Modified
Lab Number [Field ID]
Batch
Initial [g]
Final [mL]
Date
22AO729-01 [Biosolids]
B299215
1.08
100
01/19/22
0
I
Page 6 of 12

Table of Contents
con-test'
A Face AnalyficalO Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
QUALITY CONTROL
i
Conventional Chemistry Parameters by EPA/APHA/SW-846 Methods (Total) - Quality Control
Reporting Spike Source %REC RPD
Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes
Batch B299215 - SM 4500-NH3 C
Blank (B299215-BLKI)
Prepared: O1/19/22 Analyzed: O1/20/22
Ammonia as N
ND 30 mg/Kg wet
LCS (B299215-BSI)
Prepared: O1/19/22 Analyzed: O1/20/22
Ammonia as N
480 30 mg/Kg wet
500 95.2 86.2-I10
LCS Dup (B299215-BSDI)
Prepared: O1/19/22 Analyzed: O1/20/22
Ammonia as N
480 30 mg/Kg wet
500 95.2 86.2-110
0.00 10
Duplicate (B299215-DUPI)
Source: 22A0729-01
Prepared: O1/19/22 Analyzed: O1/20/22
Ammonia as N
1200 42 mg/Kg dry
1200
2.68 26.7
Matrix Spike (B299215-MSI)
Source: 22A0729-01
Prepared: O1/19/22 Analyzed: O1/20/22
Ammonia as N
1400 41 mg/Kg dry
276 1200 75.3 56.2-136
Batch B299644 - SM4500 N Org B C
Blank (B299644-BLK1)
Prepared: 01/25/22 Analyzed: O1/26/22
Total Kjeldahl Nitrogen
ND 1.0 mg/Kg wet
LCS (B299644-BSI)
Prepared: O1/25/22 Analyzed: 01/26/22
Total Kjeldahl Nitrogen
19 1.0 mg/Kg wet
20.0 95.8 86.9-114
Batch B300021-NECi N07-0003 Modified
Blank (B300021-BLKI)
Prepared & Analyzed: 01/31/22
Nitrate/Nitrite as N
ND 2.5 mg/Kg
LCS (B300021-BS1)
Prepared & Analyzed: 01/31/22
Nitrate/Nitrite as N
130 2.5 mg/Kg ,
125 105 90-110
LCS Dup (B300021-BSDI)
Prepared & Analyzed: 01/31/22
Nitrate/Nitrite as N
130 2.5 mg/Kg
125 104 90-110
0.879 20
Duplicate (B300021-DUPI)
Source: 22A0729-01
Prepared & Analyzed: O1/31/22
Nitrate/Nitrite as N
ND v 2.5 mg/Kg
ND
NC 20
Matrix Spike (B300021-MSI)
Source: 22A0729-01
Prepared &Analyzed: 01/31/22
Nitrate/Nitrite as N
120 2.5 mg/Kg
124 ND 98.2 90-110
n
I
tn^
Page 7 of 12

Table of Contents
con -testa
A Pace Analytr`catO Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
FLAG/QUALIFIER SUMMARY
l
*
QC result is outside of established limits.
t
Wide recovery limits established for difficult compound.
$
Wide RPD limits established for difficult compound.
#
Data exceeded client recommended or regulatory level
ND
Not Detected
RL
Reporting Limit is at the level of quantitation (LOQ)
DL
Detection Limit is the lower limit of detection determined by the MDL study
MCL
Maximum Contaminant Level
Percent recoveries and relative percent differences (RPDs) are determined by the software using values in the
calculation which have not been rounded.
No results have been blank subtracted unless specified in the case narrative section.
0
I
11�f 15
Page 8 of 12

con -test&
A Face AnalyticatIO Laboratory
39 Spruce Street * East Longmeadow, MA 01028 * FAX [phone] * TEL. [phone]
CERTIFICATIONS
Certified Analyses included in this Report
Analyte Certifications
SM21-23 4500 NH3 CModified in Soil
Ammonia as N NC
Con -Test, a Pace Environmental Laboratory, operates under the following certifications and accreditations:
Code
Description
Number
Expires
AIHA
AIHA-LAP, LLC - ISO17025:2017
100033
03/1/2024
MA
Massachusetts DEP
M-MA100
06/30/2022
CT
Connecticut Department of Publilc Health
PH-0165
12/31/2022
NY
New York State Department of Health
10899 NELAP
04/l/2022
NH-S
New Hampshire Environmental Lab
2516 NELAP
02/5/2022
RI
Rhode Island Department of Health
LAO00373
12/30/2022
NC
North Carolina Div. of Water Quality
652
12/31/2022
NJ
New Jersey DEP
MA007 NELAP
06/30/2022
FL
Florida Department of Health
E871027 NELAP
06/30/2022
VT
Vermont Department of Health Lead Laboratory
LL720741
07/30/2022
ME
State of Maine
MA00100
06/9/2023 '.
VA
Commonwealth of Virginia
460217
12/14/2022
NH-P
New Hampshire Environmental Lab
2557 NELAP
09/6/2022
VT-DW
Vermont Department of Health Drinking Water
VT-255716
06/12/2022
NC-DW
North Carolina Department of Health
25703
07/31/2022
PA
Commonwealth of Pennsylvania DEP
68-05812
06/30/2022
MI
Dept. of Env, Great Lakes, and Energy
9100
09/6/2022
e
Table of Contents
Page 9 of 12

Table of Contents
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Page 10 of 12

Table of Contents
FROM
Kernersville, NC US
MANAGE DELIVERY
Travel History
TIME ZONE
Local Scan Time
Friday, January 14,
2022
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TRACK ANOTHER SHIPMENT
775748453462
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TO
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Delivered
Package delivered to recipient address - release authorized
On FedEx vehicle for delivery
At local FedEx facility
At destination sort facility
Departed FedEx hub
Arrived at FedEx hub
Picked up
Shipment information sent to FedEx
U

I Have Not Confirmed Sample Container
Numbers With Lab Staff Before Relinquishing
L-,A EK:)Fsa-r-oFk'r
Over Samples
Login Sample Receipt Checklist - (Rejection Criteria
Listing - Using Acceptance Policy) Any False
Statement will be brought to the attention of the Client - State True or False
Client
Received By t_�1--_
Date 11,E-(fa Time ►"�� �t
How were the samples In Cooler _T
No Cooler On Ice ..7 No Ice
received? Direct from Sampling
Ambient Melted ice
Were samples within By Gun # Actual Temp -
Temperature? 2-6'C By Blank #
Actual Temp -
Was Custody Seal Intact? _ Il_ (
Were Samples Tampered with?
Was COC Relinquished ? 'T
Does Chain Agree With Samples? i
Are there broken/leaking/loose caps on any samples? �-
Is COC in ink/ Legible? 1
Were samples received within holding time? -T
Did COC include all Client j
Analysis —T Sampler Name —['
pertinent information? Project
ID's i Collection Dates/Times i
Are Sample labels filled out and legible? 1
Are there Lab to Filters?
Who was notified?
Are there Rushes?
Who was notified?
Are there Short Holds?
Who was notified?
Is there enough Volume?
Is there Headspace where applicable?
MS/MSD? j—
Proper Media/Containers Used?
Is splitting samples required? T-
Were trip blanks received?
On COC?
Do all samples have the proper pH?
Acid tA:4 _ Base 1
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- y= Yh
WHO
comments:

Pace Analytical Services, LLC
aeeAnalytical 1 South Park Drive
t�Kernrnersville, NC 27284
www.pacolabs.cem [phone]
Page 1 of 2
Laboratory Report
Karen Reece Report Date: 05/11/2022
Town of Boone WWTP Date Received: 04/21/2022
PO Drawer 192
Boone, NC 28607
Project: Boone - Biosolids
Pace Project No.: 92600495
Sample: Biosolids
Lab ID:
92600495001 Collected: 04/21/22 07:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Method
Parameters
Results
Units
Report Limit
Analyzed
Qualifiers
EPA 601 OD
Aluminum
15000
mg/kg
50.6
04/25/22 17:57
EPA 601 OD
Arsenic
ND
mg/kg
2.5
04/25/22 00:33
EPA 601 OD
Cadmium
1.1
mg/kg
0.10
04/25/22 00:33
EPA 601 OD
Calcium
21100
mg/kg
126
04/25/22 17:57
EPA 601 OD
Copper
419
mg/kg
5.1
04/25/22 00:33
EPA 6010D
Lead
15.7
mg/kg
1.0
04/25/22 00:33
EPA 601 OD
Magnesium
2330
mg/kg
10.1
04/25/22 00:33
EPA 601 OD
Molybdenum
ND
mg/kg
5.1
04/25/22 00:33
EPA 6010D
Nickel
13.5
mg/kg
0.51
04/25/22 00:33
EPA 601 OD
Potassium
3110
mg/kg
506
04/25/22 00:33
EPA 601 OD
Selenium
6.6
mg/kg
1.0
04/25/22 00:33
EPA 601 OD
Sodium
959
mg/kg
506
04/25/22 00:33
EPA 601 OD
Zinc
755
mg/kg
1.0
04/25/22 00:33
EPA 601 OD
Sodium Adsorption Ratio
1.7
meq/L
05/11/22 08:37
N2
EPA 7471 B
Mercury
0.099
mg/kg
0.055
05/02/22 13:28
SM 2540G-2011
Total Solids
91.6
%
0.10
04/22/22 17:21
SW-846
Percent Moisture
8.4
%
0.10
04/22/22 17:13
N2
EPA 9045D
pH at 25 Degrees C
6.5
Std. Units
0.10
04/26/22 09:53
H3
None
Plant Available Nitrogen
12700
mg/kg
05/06/22 16:05
N2
TKN+NO3+NO2
Nitrogen
41600
mg/kg
40.0
05/06/2215:33
Calculation
EPA 350.1 Rev 2.0 1993
Nitrogen, Ammonia
1180
mg/kg
18.0
04/28/22 09:35
Mod.
EPA 351,2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
41600
mg/kg
2100
05/06/22 06:24
M1, R1
EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND
mg/kg
4.4
04/22/22 23:25
M1
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
ND
mg/kg
4A
04/22/22 23:25
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrite
ND
mg/kg
4.4
04/22/22 23:25
M1
EPA 365.1 Rev 2.0 1993
Phosphorus
17800
mg/kg
273
04/29/22 15:51
M1
ANALYTE QUALIFIERS
A
/ H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELACITNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
R1 RPD value was outside control limits.
Page 1 of 5

aceAnalytieal'
www.pecolobs.com
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification M 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water#: LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 2
Page 2 of 5

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r
✓ ' Document dame: Document Revised: November 1.5, 2021
.,
Sample Condition Upon Receipt (SCUR) Page1 of 2
'r3C8 �c7tr�(iC3 Document No.: Issuing Authority:
F-CAR-CS-033-Rev.09 Pace Carolinas Quality Office
Laboratory receiving samples: I
Asheville ❑ Eden Greenwood ❑ Huntersville ❑ Raleigh[] Mechanicsville❑ Atlanta. Kernersville
Clientlac,
A " Ji Project #:
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial [ace ❑Other:
Custody Seal Present? ❑Yes [1]fijo Seals Intact? Eyes ❑No
Packing Material: []Bubble wrap qr, bole Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: / ❑Yes ❑No [},KIA
IR Gun ID: Type of ice: []Blue ❑Plane
Correction Factor:
Cooler Temp: Add/Subtract ("C) Temp should be above freezing to 6°C
[]Samples out oftemp criteria. Samples on ice, cooling process
Cooler Temp Corrected ("C}: has begun
USDA Regulated Soil ([] N/A, water sample)
Did samples origina a in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (intern- Tonally,
IMPS M rl-.i. _ - ­_ -I, rev
Comments/ Discrepancy:
Chain of Custody Present?
tyrres
ONO
QNJA
1,
Samples Arrived within Hold Time?
es
ON.
©N/A
2.
Short Hold Time Analysis (<72 hr.)?
ED4
El No
QN/A
3.
Rush Turn Around Time Requested?
Qyes
01,46
QN%A
4,
Sufficient Volume?
C44
[IN.
[]N/A
5.
Correct Containers Used?
-Pace Containers Used?
jgres
QYes
QNo
[]No
QN/A
QN/A
6.
Containers Intact?
0;4's
QNo
[]N/A
7.
Dissolved analysis: Samples Field Filtered?
[]Yes
[]No
t/A
S.
Sample Labels Match COC?
-includes Date/Time/ID/Analysis Matrix:
ClWe'3
QNo
❑€ IA
9.
He3dspace in VOA Vials (>5-6mm)?
[]Yes
El No
j�/A
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
[]Yes
[]Yes
[]No
QPIo
//A
N/A
11.
COMMENTSISAMPL£ DISCREPANCY Field Data Required? []Yes Qifo
Lot ID of split containers:
'CLIENT NOTIFICATION/ RE50LUTIO N
A
Person contacted: Date/'rime:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Page 4 of 5

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V t 1� J Lj ci,r.a
PreSa"VJ'Ne, GL'OF taMp, incorrec- comimers.
Page 5 of 5

aceAnalytical e
www.pacelabs.com
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Project: Town of Boone-Biosolids
Pace Project No.: 92617304
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 2
Report Date: 08/31 /2022
Date Received: 07/28/2022
Sample: Biosolids Lab ID: 92617304001 Collected: 07/28/22 08:00 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 601 OD
Aluminum
18200
mg/kg
52.5
08/23/22 18:40
EPA 601 OD
Arsenic
3.1
mg/kg
2.6
08/23/22 18:36
EPA 601 OD
Cadmium
1.1
mg/kg
0.11
08/10/22 03:37
EPA 601 OD
Calcium
19800
mg/kg
131
08/23/22 18:40
EPA 601 OD
Copper
442
mg/kg
5.3
08/10/22 03:37
EPA 601 OD
Lead
17.2
mg/kg
1.1
08/10/22 03:37
EPA 601 OD
Magnesium
2420
mg/kg
10.5
08/10/22 03:37
EPA 601 OD
Molybdenum
5.5
mg/kg
5.3
08/10/22 03:37
EPA 601 OD
Nickel
15.2
mg/kg
0.53
08/10/22 03:37
EPA 601 OD
Potassium
2810
mg/kg
525
08/23/22 18:36
EPA 601 OD
Selenium
8.5
mg/kg
1 A
08/10/22 03:37
EPA 601 OD
Sodium
1030
mg/kg
525
08/10/22 03:37
EPA 601 OD
Zinc
831
mg/kg
1.1
08/10/22 03:37
EPA 601 OD
Sodium Adsorption Ratio
1.9
meq/L
08/31/22 08:20
N2
EPA 7471 B
Mercury
0.42
mg/kg
0.051
08/05/22 13:21
D3
SM 254OG-2011
Total Solids
89.8
%
0.10
07/29/22 16:27
SW-846
Percent Moisture
10.2
%
0.10
07/29/22 16:21
N2
EPA 9045D
pH at 25 Degrees C
6.2
Std. Units
0.10
08/10/22 12:56
H3
None
Plant Available Nitrogen
16900
mg/kg
08/04/22 18:54
N2
TKN+NO3+NO2
Nitrogen
55500
mg/kg
40.0
08/04/2218:58
Calculation
EPA 350.1 Rev 2.0 1993
Nitrogen, Ammonia
1390
mg/kg
22.3
08/03/22 13:58
Mod.
EPA 351.2 Rev 2.0 1993
Nitrogen, Kjeldahl, Total
55500
mg/kg
2650
08/04/22 04:51
EPA 353.2 Rev 2.0 1993
Nitrogen, NO2 plus NO3
ND
mg/kg
4.4
07/29/22 23:33
M1
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrate
ND
mg/kg
4.4
07/29/22 23:33
EPA 353.2 Rev 2.0 1993
Nitrogen, Nitrite
ND
mg/kg
4.4
07/29/22 23:33
EPA 365.1 Rev 2.0 1993
Phosphorus
15600
mg/kg
321
08/02/22 19:45
M1
ANALYTE QUALIFIERS
A
/ D3 Sample was diluted due to the presence of high levels of non -target analytes or other matrix interference.
H3 Sample was received or analysis requested beyond the recognized method
holding time.
M1 Matrix
spike recovery exceeded QC limits.
Batch accepted based on
laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but
other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
Page 1 of 5

aceAnalytiealo
www.pacelabsxam
Reviewed by: A�(
Stephanie Knott
704-977-0981
[e-mail]
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water* LA029
VirginiaNELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 2
Page 2 of 5

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Page 3 of 5

DC#^Title ENV-FRM-HUNT-0034 v01 Tech Spec Sample Condition
476ce- Upon Receipt
Effective Date: 06J1212022
—uVI. ul y I. C.S.•CI Vi°l6 Za i 7..If i1C5.
Asheville ❑ Eden ❑ Greenwood ❑ Huntersville ❑ RaleighMechanicsville[] Atlanta❑ Kernersv11 e`
Client Name TCM t)..S
{c� i Project ":
Courier: ❑ ed Ex ❑UPS ❑LISPS ❑Client
Commercial wPace ❑Other:
Carrier Tracking Number:
Custody Seal Present? byes Seals Intact? ❑Yes ❑into
Packing Material: ❑Bubble Wrap ubbie Baas ❑Itlon-. ❑ Other
Thermometer: ❑ IR Gun ID: L: Type of Ice: LAi4t ❑ slue
Cooler Temp ('C )a Correction Factor: Add / Subtract (-C)
Corrected Cooler Tamp ('C); �_\ v
USDA Regulated Soil i ❑ N/A, water sample)
Did samples or= mate in a quarantine zone within the United States: CA, NY, or SC.(check maps)?
[]Yes EVO
E
Date/Initials Person Examining Contents: na
Biological Tissue Fro -en?
❑Yes []No jA
❑ None
Tamp should be above freezing to 6°C
❑samples out of temp criteria. Samples on ice, cooling process
has begun
Did samples: criginat2 from a foreign source (internationally.
rr5:� v.yEi dilu i JerLo nice'! LJYes L-two
Comments/Dlscrepancy{
Chain of Custody Present?
l as
QNo
CIN/A
2.
Samples Arrived within Hold Time?
Q4
Ordo
CN/A
2.
Short Hold Time Analysis (<72 hr.)?
0yes
Pr+o
[]N/A
3.
Rush Turn Around Time Requestad?
❑yes
(Vjo
©N/A
4
Sufficient Volume?
❑Nu
QN/A
`E
# 5.
Correct Containers Used?
Pace Containers Used?
,Vrfas
L�t-9/'fes
ICY '-s
[]No
❑Na
MN/A
©N/A
6.
Containers Intact?
54
❑No
❑fi/A
7.
Dissolved analysis: Samples Field Filtered?
[lye,
ONO
r
g
Sample Labels Match CDC?
-Includes Date/TEme/lD/Analysis Matrix:_a�_
Headsoace in VOA Vials (s5-6mm)?
EXre
Elyes
❑No
ONo
❑NJA
i N A
9.
10,
Trip Blank Present?
Trip Blank Custody Seals Present?
0N1AtTENTG/1;AMP1 F nv;ri2.,:narury
©Yes
❑Yes
v
QFJa
❑tio
I 4A
GXIA
IL
Temp Log: Temp must be maintained
at <6 C during login, record temp
every 20 minutes.
'Time opened: � I • Temp:
T.
put in cooler
Time: Temp; °
Person Contacted;
Project Manager SCURF Review:
Project Manager SRF Review:
Qualtrax Document ID: 70677
CLIENT NOTIFICATI
Lot 10 of
ontainers:
r°eIo uaca ttequired? Uses "No
Date/Time:
Date:
Date:
Page 1 of 2
Page 4 of 5

r'7
DC #_ii a: Ilj�_F ,!_f� ;"41-Q 3 vu1 e h —qp?c San,,pje Condition
Pon Reced,nt
E�acf,lve Data: C6 12 ,^3
'Ch e:k fr. 2 1 t,oC ha!I Cs' t_oX i Y a"a,•rGi d�: icr;na:,Cn P ��,
is V_,. tad and L'It�in t ? a.�C''t3c C2Lr?"i—� f i
5—
�r45�:"t3`.EOn
Cif
"nctt^m hai` Cf box is to list nurn'rer of Lotties
'"Check all unpreserred Nitrates for chicrine
i
C
y
_
_
G.
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G
<=
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C ste preserradon sd i
Time pr erra.;on
I A;itcunCl
adjusted
A
ill
_ _'_,._, b �, ", „t;�_ i.;-Iptas, a „ ct or t^is fsr^i w it �, sa.^.cto t^.e Et ri C3:aiira C•_r*," C,
Out of held, incorrect presarva ;va,,Out of tamp, incorrect cantainersJ
Quaitra < Document ID: 70677 Page 2 of 2
Page 5 of 5

acaAnalytical
www.pacelabsxam
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Project: Town of Boone - Biosolids
Pace Project No.: 92629738
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 1 of 2
Repoli Date: 10/24/2022
Date Received: 10/06/2022
Sample: Biosolids Lab ID: 92629738001 Collected: 10/06/22 08:30 Matrix: Solid
Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions.
Method Parameters Results Units Report Limit Analyzed Qualifiers
EPA 6010D
EPA 601,OD
EPA 60100
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 6010D
EPA 7471B
SM 2540G-2011
SW-846
EPA 9045D
None
TKN+NO3+NO2
Calculation
EPA 350.1 Rev 2.0 1993
Mod.
EPA 351.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 353.2 Rev 2.0 1993
EPA 365.1 Rev 2.0 1993
Aluminum
18500
mg/kg
106
10/11/2221:28
Arsenic
ND
mg/kg
2.6
10/11/2221:25
Cadmium
1.2
mg/kg
0.11
10/10/22 21:20
Calcium
19500
mg/kg
264
10/11/2221:28
Copper
448
mg/kg
5.3
10/10/22 21:20
Lead
16.8
mg/kg
1.1
10/11/2221:25
Magnesium
2380
mg/kg
10.6
10/10/22 21:20
Molybdenum
5.9
mg/kg
5.3
10/10/22 21:20
Nickel
14.7
mg/kg
0.53
10/10/22 21:20
Potassium
2800
mg/kg
528
10/10/22 21:20
Selenium
5.9
mg/kg
1.1
10/10/22 21:20
Sodium
921
mg/kg
528
10/10/22 21:20
Zinc
840
mg/kg
1.1
10/10/22 21:20
Sodium Adsorption Ratio
1.7
meq/L
10/24/22 11:36
Mercury
0.38
mg/kg
0.028
10/17/2214:28
Total Solids
91.0
%
0.10
10/10/22 14:52
Percent Moisture
9.0
%
0.10
10/10/22 14:37
pH at 25 Degrees C
6.4
Std. Units
0.10
10/13/22 16:52
Plant Available Nitrogen
16100
mg/kg
10/19/22 14:29
Nitrogen
52400
mg/kg
40.0
10/17/2218:18
Nitrogen, Ammonia
1720
mg/kg
31.1
10/12/22 15:56
Nitrogen, Kjeldahl, Total
52400
mg/kg
2390
10/12/22 05:36
Nitrogen, NO2 plus NO3
ND
mg/kg
4.3
10/07/22 23:45
Nitrogen, Nitrate
ND
mg/kg
4.3
10/07/22 23:45
Nitrogen, Nitrite
ND
mg/kg
4.3
10/07/22 23:45
Phosphorus
15200
mg/kg
250
10/19/2218:51
ANALYTE QUALIFIERS
/ H3 Sample was received or analysis requested beyond the recognized method holding time.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
N2 The lab does not hold NELAC/TNI accreditation for this parameter but other accreditations/certifications may apply. A
complete list of accreditations/certifications is available upon request.
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
N2
N2
H3
N2
M1
M1
M1
Page 1 of 5

lacieAnalytical@
www.pacelabs.cam
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99006001
South Carolina Drinking Water Cent. * 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DcH Drinking Water#: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Page 2 of 2
Page 2 of 5

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Page 3 of 5

QC Title: ENV-FRPxt-Hid,`J-0084 v01 Tech Spec. Sample Condition
Upon Receipt
ETective Gate: 05:1Z.?C2
Laboratory receivin; samples:
Asheville ❑ Edon ❑ Green A4000' ❑ Hl:r,ter,`,11te
, ❑ R,(eiahPr?ech_nicsviile`_l Atlansa❑ Kerners°.rifle
P -act
rci
rc. - [lj?iitii3ri'72:
Courser: ❑Fed Ex ❑!UPS ❑Us?s ❑Client
❑ Ccmmer_iaE �c,�
e ❑ether.
Carrier Tracking Number
Custody Seat Present?
as
q �
Seats Intact? Oyes
❑Np
Packing (vlaterial'
❑EuL'Lle v,,raa
❑Euttie Sags ra
F7 othar
Tnermometar: ❑ IR Gun 10:
Type of ice:
* ❑flue
Cooler Temp (aC ), —4—=-- Correction Factor: Add / Subtract (-c) 10
Corrected Cooler Tamp (`C ):
USDA Regulated Sail (❑ N/A, water sample)
Dili sample or= inate m a quarantine zone within the United Statas: CA, NY, or SC (check maps)?
❑Yes &
Date/Initials Person Examining Ccntents'
Biological Tissue �Fr�o%-en?
Dyes ❑hid [�R/A
❑ mone
Tamp should be above fro zing to 6-C
Osampla_ out of tamp crit_;ia. Samples cn ice, coolingprocass
has begun
Did samples oe'g nate from a foreign s,,,,tr,
rnc:u,irgHa:+ysii and Pi
( Commen.
Chain of Custody Present?
—/
l�b,tres
ONO
i]N/A
Z,
Samples Arrlved •within Hold'Eme?
{ Yes
i_lcao
{iptr'A
2.
Snort Hold Time Analysis (<72 hr.)?
WYzs
❑Mo
MN/A
Rush Turn Around TimeRe,uested?
EYe,jo
CIN<•A
Suf*icEent:Volume?
I3 s
17No
©N/A
(5.
Correct, Containers Used?
-Pace Containers Used?as^lo
[�es
FIN.
©N/A
16.
Containers intact?
es
❑ila
❑rl,tA
17.
Cissclver: aral+ysis: Samples Field Filtered?
{`rts
ON-
(1Q
+ $.
Sample Labels tviatch COC?
-Includes Date/r�me/ID/Analysis Matrix:
Headscace in VOA Vials (>5-6rnm)?
[y las
QYes
ONo
(—fNa
MN/A
Aj I(A
9.
iC.
Trip Blank Present?
Trio Blank Custociv Seals Present?
Oyas
❑yes
(❑Na
CINa
(�JK"
14E,A
11.
CONVAENTS/SAMPLE DISCREPANCY
Temp Log; Temp must he maintained
at <G C during login, record temp
every 20 minutes.
Time opened Temp;
Time: utinIc
cooler
Time: Temp:
e
/ Person Contacted: _
Project Manager SCURF Review:
Lot1D of
LI:I ENT NOTIFICATION/112SO LUTION
Date/Tlme:
Date:
Project Manager SRF Review:
Date:
QUaltrax Document ID: 70677
Page 1 of 2
Page 4 of 5

i _. COc:u^1 �tt i13m 2:
Bottle Identification Form (31F)
Cccuman: hlo.:
F-CAR-CS-043-Rev.Ci
*Check- mark top half of box if pH and/or dechlorina'ion is Project
verified and within the accept.anca range for preservation
samples.
Excapticns: VC", CoNor,m, T:: -, C1ii a-7d Gr?asa, CR O/ SC S ( G'L r) CCC, L' uy
*'Bottom half of box is to list number of bottles
Cc .gin I v �:ita e 2:,,„
Fa,= " cf 1 ^
is ufn; but rrJ:
_e Ca'li€n35 ri,aa ini G_:
u
U
`
C
4'.
.
IT:
fit
G
Y
0
C7
¢.
l}
<
m
<
<
<
<
G
>
>
C
>
>
vi
vs
c
d
>
-
G
pH Adjustment Loa for Preserved Samples
Sample iD
Type of Preservative
pH upon receipt
Oat 2 preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
tot'#
dlot2: wh2geverther2
is a discr2aanod-aff-ti—
NI—th ('ar.�Gnz.-
. --�.� - _..._ ..,.. ••,•. �,. ..�,� ,u. eAua von r�tt Ge2IIltaiton Grsica {L2.
Qutof hall, incorrect preservative, out of temp, incorrect containers.
Page 5 of 5

aceAnalytical
www.pacelabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
Laboratory Report
Karen Reece
Town of Boone WWTP
PO Drawer 192
Boone, NC 28607
Project: Boone - TCLP Biosolids
Pace Project No.: 92600489
Page 1 of 2
Report Date: 05/05/2022
Date Received: 04/21/2022
Sample: Biosolids TCLP Lab ID: 92600489001 Collected: 04/21/22 07:30 Matrix:
Results reported on a "dry weight' basis and are adjusted for percent moisture, sample size and any dilutions.
Method Parameters Results Units Report Limit
EPA 8081 B
EPA 8081 B
EPA 8081 B
EPA 8081 B
EPA 8081 B
EPA 8081 B
EPA 8081 B
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 601 OD
EPA 7470A
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8270E
EPA 8260D
EPA 8?60D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 8260D
EPA 9045D
EPA 1030
gamma-BHC (Lindane)
Chlordane (Technical)
Endrin
Heptachlor
Heptachlor epoxide
Methoxychlor
Toxaphene
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Mercury
1,4-Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylp henol (o-C reso I)
3&4-Methylphenol (m&p Cresol)
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Benzene
2-Butahone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,4-Dichlorobenzene
1,2-Dichloroethane
1,1-Dichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloride
pH at 25 Degrees C
Ignitability
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
mg/L
ND
mg/L
ND
mg/L
ND
mg/L
ND
mg/L
ND
mg/L
ND
mg/L
ND
mg/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
ND
ug/L
6.5
Std. Units
NO
mm/sec
0.50
3.0
0.50
0.50
0.50
1000
3.0
0.050
0.25
0.0050
0.050
0.025
0.10
0.025
0.00020
50.0
50.0
50.0
50.0
50.0
50.0
50.0
50.0
100
50.0
50.0
50.0
100
200
100
100
100
100
100
100
100
100
100
0.10
2
Solid
Analyzed
04/29/22 14:51
04/29/22 14:51
04/29/22 14:51
04/29/22 14:51
04/29/22 14:51
04/29/22 14:51
04/29/22 14:51
04/27/22 11:29
04/27/22 11:29
04/27/22 11:29
04/27/22 11:29
04/27/22 11:29
04/27/22 11:29
04/27/22 11:29
05/02/22 15:16
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 16:49
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/27/22 19:45
04/26/22 09:52
04/25/22 12:00
Qualifiers
R1
R1
H3
Page 1 of 28

aceAnalytical
amxr pacalabs.com
Pace Analytical Services, LLC
1377 South Park Drive
Kernersville, NC 27284
[phone]
ANALYTE QUALIFIERS
H3 Sample was received or analysis requested beyond the recognized method holding time.
R1 RPD value was outside control limits.
Reviewed by:
Stephanie Knott
704-977-0981
[e-mail]
Pace Analytical Gulf Coast
7979 Innovation Park Drive, Baton Rouge, LA 70820
Arkansas Certification #: 88-0655
DoD ELAP Certification #: L18-597
Florida Certification #: E87854
Illinois Certification #: 004585
Kansas Certification #: E-10354
Louisiana/LELAP Certification #: 01955
North Carolina Certification #: 618
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Laboratory ID: 99006
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
North Dakota Certification #: R-195
Oklahoma Certification #: 2019-101
South Carolina Certification #: 73006001
Texas Certification #: T104704178-19-11
USDA Soil Permit # P330-19-00209
Virginia Certification #: 460215
Washington Certification #: C929
South Carolina Certification #: 99006001
South Carolina Drinking Water Cert. #: 99006003
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Louisiana DoH Drinking Water #: LA029
Virginia/VELAP Certification #: 460221
South Carolina Laboratory ID: 99030
South Carolina Certification #: 99030001
Virginia/VELAP Certification #: 460222
Page 2 of 2
Page 2 of 28

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® Document Name: Revised. November 15, 2021
/� Sample Condition Upon Receipt (SCUR) Pa e 1 of 2
SC@A(evl/t1C8I Document No.: Issuing Authority,
F-CAR-CS-033-Rev.08 Pace Carolinas Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑ Raleigh❑ Mechanicsville Atlanta❑ Kernersville
?r^. r�7r. Clie ame:
V Project if:
Courier: ❑Fed Ex ❑UPS ❑USPS ❑Client
❑ Commercial a ❑Other:
Custody Seal Present? ❑Yes Seals Intact? [Dyes ❑No
Packing Material: ❑Bubble Wrap ble Bags ❑None ❑ Other Biological Tissue Frozen?
Thermometer: et ❑Blue ❑None Dyes ❑No /A
❑ �, IR Gun ID: Type of Ice:
Correction Factor:
Cooler Temp: , Add/Subtract ("C) 0 Z Temp should be above freezing to 6°C
❑Samples out of temp criteria. Samples on ice, cooling process
Cooler Temp Corrected (°C): has begun
USDA Regulated Soil (❑ N/A, water sample)
Did samples originapo in a quarantine zone within the United States: CA, NY, or SC (check maps)? Did samples originate from a foreign source (internal nally,
Comments/Discrepancy:
Chain of Custody Present?
04.
[]No
[]N/A
1.
Samples Arrived within Hold Time?
es
[]No
❑N/A
2.
Short Hold Time Analysis (<72 hr.)?
Oyes
@ o
❑N/A
3.
Rush Turn Around Time Requested?
[]Yes
o
❑N/A
4.
Sufficient Volume?
EKes
ONO
❑N/A
5.
Correct Containers Used?
-Pace Containers Used?
62fes
Ofes
❑No
QNo
❑N/A
❑N/A
6.
Containers Intact?
LtejYes
ONo
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
❑Yes
®No
/A
8. I
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
Ves
[]No
❑N/A
9.
Headspace in VOA Vials (>5-6mm)?
Dyes
[]No
[2i/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
❑No
❑No
/A
A
11.
COMMENTS/SAMPLE DISCREPANCY Field Data Required? ❑Yes ❑No
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION +
Person contacted: Date/Time:
Project Manager SCURF Review: Date:
Project Manager SRF Review: Date:
Page 4 of 28

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Page 5 of 28

aceAnalytical
LELAP CERTIFICATE NUMBER: 01955
DOD -FLAP ACCREDITATION NUMBER: 74960
j
• •. Innovation Park Dr.
Baton Rouge, 70820
• /.. 1.
Report Date 04/26/2022
Report k222042303
111111111111111 �1111 1111111111
Project 92600489 Boone-TCLP Biosolids
Samples Collected 4/21/22
Deliver To Additional Recipients
Stephanie Knott NONE
Pace Analytical Kernersville
1377 South Park Drive
Kernersville, NC 27824
704-977-0981
Is
"01 17025
Pane R of 98
Pace Gulf Coast Report#: 222042303 Page 1 of 9

Report#: 222042303
Project ID: 92600489 Boone-TCLP Biosotids Report Date: 04/26/2022
Laboratory Endorsement
pie analysis was performed in accordance with approved methodologies provided by the Environmental Protection Agency or other recognized
icies. The samples and their corresponding extracts will be maintained for a period of 30 days unless otherwise arranged. Following this
rtion period the samples will be disposed in accordance with Pace Gulf Coast's Standard Operating Procedures.
Common Abbreviations that may be Utilized in this Report
NO Indicates the result was Not Detected at the specified reporting limit
NO Indicates the sample did not ignite when preliminary test performed for EPA Method 1030
DO • Indicates the result was Diluted Out
MI Indicates the result was subject to Matrix Interference
TNTC Indicates the result was Too Numerous To Count
SUBC Indicates the analysis was Sub -Contracted
FLO Indicates the analysis was performed in the Field
DL Detection Limit
LOD Limit of Detection
LOQ Limit of Quantitation
RE Re -analysis
CF HPLC or GC Confirmation
00:01 Reported as a time equivalent to 12:00 AM
Reporting Flags that may be Utilized in this Report
j or I Indicates the result is between the MDL and LOQ
J DOD flag on analyte in the parent sample for MS/MSD outside acceptance criteria
U Indicates the compound was analyzed for but not detected
B or V Indicates the analyte was detected in the associated Method Blank
Q Indicates a non -compliant QC Result (See Q Flag Application Report)
Indicates a non -compliant or not applicable QC recovery or RPD — see narrative
E Organics - The result is estimated because it exceeded the instrument calibration range
E Metals - % diference for the serial dilution is > 10%
L Reporting Limits adjusted to meet risk -based limit.
p RPD between primary and confirmation result is greater than 40
DL Diluted analysis — when appended to Client Sample ID
Sample receipt at Pace Gulf Coast is documented through the attached chain of custody. In accordance with NELAC, this report shall be
reproduced only, in full and with the written permission of Pace Gulf Coast. The results contained within this report relate only to the samples
reported. The documented results are presented within this report.
This report pertains only to the samples listed in the Report Sample Summary and should be retained as a permanent record thereof. The results
contained within this report are intended for the use of the client. Any unauthorized use of the information contained in this report is prohibited.
I certify that this data package is in compliance w(fh The NELAC Institute (TNI) Standard 2009 and terms and conditions of the contract and
Statement of Work both technically and for completeness, for other than the conditions in the case narrative. Release of the data contained in this
hardcopy data package and in the computer readable data submitted has been authorized by the Quality Assurance Manager or his/her designee,
as verified by the following signature.
Estimated uncertainty of measurement is available upon request. This report is in compliance with the DOD QSM as specified in the contract if
applicable.
Authorized Signature
od 22204
Pace Gulf Coast Rep
Pace Gulf Coast Report#:
2zzu42303 Page 2 of 9

Report#: 222042303
Analytkat"
Project ID: 92600489 Boone-TCLP Biosolids Report Date: 04/26/2022
Certifications
Certification
Certification Number
DOD FLAP
74960
Alabama
01955
Arkansas
88-0655
Colorado
01955
Delaware
01955
Florida
E87854
Georgia
01955
Hawaii
01955
Idaho
01955
Illinois
200048
Indiana
01955
Kansas
E-10354
Kentucky
95
Louisiana
01955
Maryland
01955
Massachusetts
01955
Michigan
01955
Mississippi
01955
Missouri
01955
Montana
N/A
Nebraska
01955
New Mexico
01955
North Carolina
618
North Dakota
R-195
Oklahoma
9403
South Carolina
73006001
South Dakota
01955
Tennessee
01955
Texas
T104704178
Vermont
01955
Virginia
460215
Washington
C929
USDA Soil Permit
P330-16-00234
Rup R of 98
Pace Gulf Coast Report#: 222042303 Page 3 of 9

Report#: 222042303
Project ID: 92600489 Boone-TCLP Biosolids Report Date: 04/26/2022
Case Narrative
Client: Pace Analytical Services Report: 222042303
Pace Analytical Gulf Coast received and analyzed the sample(s) listed
on the Report Sample Summary page of this report. Receipt of the sample(s) is documented
by the attached chain of custody. This applies only to the sample(s) listed in this report.
No sample integrity or quality control exceptions were identified unless noted below.
No anomalies were found for the analyzed sample(s).
Raaa q of 2
Pace Gulf Coast Report#: 222042303 Page 4 of 9

,!.2AWAral`
Report#: 222042303
Project ID: 92600489 Boone-TCLP Biosolids Report Date: 04/26/2022
Sample Summary
Lab ID Client ID Matrix Collect Date Receive Date
22204230301 BIOSOLIDS TCLP
Solid 4/21/22 07:30 4/22/22 09:30
Pane l of 2R
Pace Gulf Coast Report#: 222042303 Page 5 of 9

Report#: 222042303
Project ID: 92600489 Boone-TCLP Biosotids
Detect Summary
No analytes were detected for analyses performed by Pace Gulf Coast.
Report Date: 04/26/2022
Pala 11 of 9R
Pace Gulf Coast Report#: 222042303 Page 6 of 9

Report#: 222042303
Project ID: 92600489 Boone-TCLP Biosotids Report Date: 04/26/2022
Sample Results
BIOSOLIDS TCLP Collect Date 04/21/2022 07:30 Lab ID 22204230301
Receive Date 04/22/2022 09:30 Matrix Solid
1030
Prep Date Prep Batch Prep Method Dilution Run Date Run Batch Analyst %Moisture
NA NA NA 1 04/25/2212:00 739338 JGD 12.45
CAS# Parameter
000000-01-7 Ignitable
Result
DL
LOCI
Reg Limit
Units
NO
2
2
2
mm/sec
Dana 19 of 9R_
Pace Gulf Coast Report#: 222042303 Page 7 of 9

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NA><YTICAi_ ENVIRONMENTAL SERVICES, INC.
April 29, 2022
Stephanie Knott
Pace Analytical
1377 South Park Dr
Kernsville NC 27284
RE: 92600489
Dear Stephanie Knott: Order No: 2204P 17
Analytical Environmental Services, Inc. received I samples on 4/22/2022 8:49:00 AM
for the analyses presented in following report.
"No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in the
report or QC Summary. Additionally, all results for the associated Quality Control samples were within EPA
and/or AES established limits.
AES' certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/21-06/30/22.
=North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31/22.
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/22.
These results relate only to the items tested as received. This report may only be reproduced in full and with
written permission from the laboratory.
If yqu have, any questions regarding these test results, please feel free to call.
Sincerely,
4' ao
Paris Masoudi
Project Manager
;1,80 11),340 1`�,i, °!T(r. ,;��'i7 �a>:: 770.4 �,7.,R188 > -Cell 1rcr:800-972A889
Page 15 of 28
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Analytical Environmental Services, Inc
Date: 29-Apr-22
Client:
Pace Analytical
Client Sample ID:
BIOSOLIDS TCLP
Project Name
92600489
Collection Date:
4/21/2022 7:30:00 AM
Lab ID:
2204P17-001
Matrix:
Solid
Reporting Ulluno
Units BatchID n Date Analyzed Analyst
Analyses Result Limit Qual
HERBICIDES, TCLP SW1311/8151A
2,4,5-TP (Silvex) BRL 0.20
2,4-D BRL 0.20
Surr: DCAA 77.8 50.1-120
Qualifiers: * Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyte not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
(SW35100
mg/L 335157
mg/L 335157
%REC 335157
1 04/28/202213:43 KH
1 04/28/202213:43 KH
1 04/28/202213:43 KH
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
t Less than Result value
I Estimated value detected below Reporting Limit
Page 17 of 28
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Page 20 of 28
Pan.- A of Fi

ANALYTICAL ENVIRONMENTAL SERVICES, INC.
AES
May 05, 2022
Stephanie Knott
Pace Analytical
1377 South Park Dr
Kernsville NC 27284
RE: 92600489
Dear Stephanie Knott: Order No: 2204T46
Analytical Environmental Services, Inc. received 1 samples on 4/27/2022 9:17:00 AM
for the analyses presented in following report.
"No problems were encountered during the analyses except as noted in the Case Narrative or by qualifiers in
the report or QC Summary. Additionally, all results for the associated Quality Control samples were within
EPA and/or AES established limits.
AES' certifications are as follows:
-NELAP/Florida State Laboratory ID E87582 for analysis of Non -Potable Water, Solid & Chemical Materials,
Air & Emissions for Organics, and Drinking Water Microbiology & Metals, effective 07/01/21-06/30/22.
-North Carolina Certification number 562 for analysis of Surface Water, Groundwater, Effluent, effective until
12/31 /22,
-South Carolina Environmental Laboratory Certification number 98016003 effective until 6/30/22.
These results relate only to the items tested as received. This report may only be reproduced in full and with
written permission from the laboratory.
If you have any questions regarding these test results, please feel free to call.
Sincerely,
vas K aoam-k,
Paris Masoudi
Project Manager
i4)«(i �'r.>-irlrt7ii, 1 i)rie<• atl.tnla; Cn,n�;ia �Oli (1 <'� ol: 17(l.-1 `1.bI %'f ° rax: 710.457.8IS; a Toll Fro: 800.972.4889
Page21 of28
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Analytical Environmental Services, Inc
Date: 5-May-22
Client:
Pace Analytical
Client Sample ID:
BIOSOLIDS TCLP
Project Name:
92600489
Collection Date:
4/21/2022 7:30:00 AM
Lab ID:
2204T46-001
Matrix:
Solid
Reporting Dilution Date Analyzed Analyst
Analyses Result Limit Qual Units BatchID Factor
Sulfide, Reactive SW846-7.3
Sulfide, Reactive
Cyanide, Reactive SW846-7.3
Cyanide, Reactive
Qualifiers: . Value exceeds maximum contaminant level
BRL Below reporting limit
H Holding times for preparation or analysis exceeded
N Analyle not NELAC certified
B Analyte detected in the associated method blank
> Greater than Result value
(SW7.3.4.2)
BRL 100 mg/Kg 335376 1 04/28/202212:00 AD
(SW7.3.3.2)
1.49 0.962 ing/Kg 335702 1 05/04/2022 00:00 AD
E Estimated (value above quantitation range)
S Spike Recovery outside limits due to matrix
Narr See case narrative
F Analyzed in the lab which is a deviation from the method
Less than Result value
J Estimated value detected below Reporting Limit page 23 of 28
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End of Report
Page 28 of 28
P.M. A of R

CLIENT:
ADDRESS
CITY:
STATE:
|D#
WATER QUALITY LAB & OPERATIONS, INC.
P.D.BOX 1107
BANNER ELK, NC 28004
/828>808'0277
TOWN OF BOONEVVV0[P LOGIN TIME:
P.O.BOX 102 SAMPLER:
BOONE RECEIVED DATE:
NC ZIP28007
NCOO2O021
2O- an'22
A AY
TOTAL SOLIDS
91.0
%
SLUDGE
REPORTED BY: NC CERTIFIED LAB # 544

WATER QUALITY SERVICES, INC.
P.O. 'BOX 1102, BANNER ELK, NC 28604
[phone]
fax (828) 898,6255
CHAIN OF CUSTODY
TYPE SAMPLE: WASTEWATER
LOCATION: CLASS /� 5-roP�AGF- PRESERVATION CODE
FACILITY ID #: NC_ C) o,n Hai 1 - H2SO4, 2 - HNO3, 3 - HCL,
.5AMPLER NAME; owl p _1 4 - NAOH, 5 - NONE, 6 - COOL ICE
;OMPOSITE SAMPLE; START TIME: 7 - NA2S203, 8 - OTHER
-- ; STOP TIME;
)AMPLE NAME:
4]
��1-y �Y ODUMU11 Ur preservatives prior to sample
containers leaving the lab, unless otherwise noted.
CL2-D-CL2= Chlorine check and dechlorin:ation verification.
RESERVATION:
) COOL 4C : BOD, RESIDUE, CONDUCTIVITY, MBAS, COLOR, ALKALINITY, CR, VI, TURBIDITY
I COOL 4C, PH<2 H2SO4: NH3, NO2-NO3, TKN, O&G, TOC, COD, HARDNESS, PHENOLS, TOT PHOS,
) COOL 4C, PH<2 HNO3 :.METALS except CR, VI
) NONE : CHLORIDE, PH, FLUORIDE SAMPLE DEVIATION:
THER:
COOL 4C, NA2S203 : COLIFORM BACTERIA
NOTIFICATION:

WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 192 SAMPLER:
CITY: BOONE RECEIVED DATE:
STATE: NC ZIP 28607 REPORTED DATE:
ID#: NC0020621
MIKE EVERETT
28-Apr-22
25-May-22
ANALYSIS
LSID #
ANALYSIS
MQL's
UNITS
SAMPLE
ANALYSIS
INT
RESULTS
LOCATION
COMPLETED
TOTAL SOLIDS
1
90.2
%
SLUDGE
FECAL COLIFORM
213
MPN/g
SLUDGE
29-Apr-22
PI
TOTAL SOLIDS
2
91.3
%
SLUDGE
FECAL COLIFORM
84
MPN/g
SLUDGE
29-Apr-22
PI
TOTAL SOLIDS
3
91.5
%
SLUDGE
FECAL COLIFORM
130
MPN/g
SLUDGE
29-Apr-22
PI
TOTAL SOLIDS
4
90.8
%
SLUDGE
FECAL COLIFORM
140
MPN/g
SLUDGE
29-Apr-22
PI
TOTAL SOLIDS
5
91.7
%
SLUDGE
FECAL COLIFORM
223
MPN/g
SLUDGE
29-Apr-22
PI
TOTAL SOLIDS
6
92.4
%
SLUDGE
FECAL COLIFORM
188
MPN/g
SLUDGE
29-A-22
pr
PI
TOTAL SOLIDS
7
92.0
%
SLUDGE
FECAL COLIFORM
170
MPN/g
SLUDGE
29-Apr-22
PI
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

WATER QUALITY SERVICES, INC.
P.O. 'BOX 1102, BANNER ELK, NC 28604
[phone]
fax [phone]
CHAIN OF CUSTODY
TYPE SAMPLE: WASTEWATER
LOCATION: CLASS /h STDPIAG �R *PRESERVATION CODE
FACILITY ID #; L O Q� dal 1 - H2SO4, 2 - HNO3, 3 - HCL,
.5AMPLER NAME: pw� DC4 - NAOH, 5 - NONE, 6 - COOL ICE
�-----���� =----- ;OMPOSITE SAMPLE; START TIME:7 - NA2S203, 8 -OTHER
—______ ; STOP TIME:
)AMPLE NAME:
*- Laboratory preservation is ensured by addition of pi
containers leaving the lab, unless otherwise noted.
Cl 2-D-CL2= Chlorine check and dechlorinration verification:
-f
RESERVATION:
I COOL 4C,: BOD, RESIDUE, CONDUCTIVITY, MBAS, COLOR, ALKALINITY, CR, VI, TURBIDITY
I COOL 4C, PH<2 H2SO4: NH3, NO2-NO3, TKN, O&G, TOC, COD, HARDNESS, PHENOLS, TOT PROS.
I COOL 4C, PH<2 HNO3 : METALS except CR, VI
) NONE : CHLORIDE, PH, FLUORIDE SAMPLE DEVIATION:
)-HER:
i/COOL 4C, NA2S203 : COLIFORM BACTERIA
NOTIFICATION:

WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 192
CITY: BOONE RECEIVED DATE:
STATE: NC ZIP 28607 REPORTED DATE:
ID#: NCO020621
11-Aug-22
12-Sep-22
ANALYSIS
LSID #
ANALYSIS
MQL's
UNITS
SAMPLE
ANALYSIS
INT
RESULTS
LOCATION
COMPLETED
TOTAL SOLIDS
1
91.1
%
SLUDGE
FECAL COLIFORM
333
MPN/g
SLUDGE
12-Aug-22
PI
TOTAL SOLIDS
2
91.4
%
SLUDGE
FECAL COLIFORM
358
MPN/g
SLUDGE
12-Aug-22
PI
TOTAL SOLIDS
3
92.5
%
SLUDGE
FECAL COLIFORM
302
MPN/g
SLUDGE
12-Aug-22
PI
TOTAL SOLIDS
4
92.1
%
SLUDGE
FECAL COLIFORM
234
MPN/g
SLUDGE
12-Aug-22
PI
TOTAL SOLIDS
5
93.1
%
SLUDGE
FECAL COLIFORM
260
MPN/g
SLUDGE
12-Aug-22
PI
TOTAL SOLIDS
6
92.8
%
SLUDGE
FECAL COLIFORM
273
MPN/g
SLUDGE
12-Aug-22
PI
TOTAL SOLIDS
7
92.2
%
SLUDGE
FECAL COLIFORM
254
MPN/g
SLUDGE
12-Aug-22
PI
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

WATER QUALITY SERVICES, INC.
P.O. 'BOX 1102, BANNER ELK, NC 28604
[phone]
fax (828) 898�.6255
CHAIN OF CUSTODY
TYPE SAMPLE: WASTEWATER * PRESERVATION CODE
LOCATION: Cl,r1S5 -n 5TOPIMG AR 1 - H2SO4, 2 - HNO3, 3 - HCL,
FACILITY ID #: NC, d o,n ('al
SAMPLER NAME; 4 - NAOH, 5 -NONE, 6 - COOL ICE
TOwt� p% I�p,3�} I` 7 - NA2S203, 8 - OTHER
;OMPOSITE SAMPLE; START TIME: ; STOP TIME:
"'-'J �*�"`-+�Gi NIGJGIV4LIVCS EJIIOf IO Sarnp�e
containers leaving the lab, unless otherwise noted.
Cl 2-D-CL2= Chlorine check and dechlorin:ation verification.'
)2ESERVATION:
I COOL 4C : BOD, RESIDUE, CONDUCTIVITY, MBAS, COLOR, ALKALINITY, CR, VI, TURBIDITY
I COOL 4C, PH<2 H2SO4: NH3, NO2-NO3, TKN, O&G, TOC, COD, HARDNESS, PHENOLS, TOT PHOS.
I COOL 4C, PH<2 HNO3 : METALS except CR, VI
j NONE: CHLORIDE, PH, FLUORIDE SAMPLE DEVIATION:
FHER:
COOL 4C, NA2S203 : COLIFORM BACTERIA
NOTIFICATION:

WATER QUALITY LAB & OPERATIONS, INC.
P.O. BOX 1167
BANNER ELK, NC 28604
[phone]
CLIENT: TOWN OF BOONE WWTP
ADDRESS: P.O. BOX 192
CITY: BOONE RECEIVED DATE: 13-Oct-22
STATE: NC ZIP 28607 REPORTED DATE: 22-Nov-22
ID#: NCO020621
ANALYSIS
LSID #
ANALYSIS
MQL's
UNITS
SAMPLE
ANALYSIS
INT
RESULTS
LOCATION
COMPLETED
TOTAL SOLIDS
1
92.0
%
SLUDGE
FECAL COLIFORM
444
MPN/g
SLUDGE
14-Oct-22
PI
TOTAL SOLIDS
2
91.1
%
SLUDGE
FECAL COLIFORM
323
MPN/g
SLUDGE
14-Oct-22
PI
TOTAL SOLIDS
3
92.2
%
SLUDGE
FECAL COLIFORM
243
MPN/g
SLUDGE
14-Oct-22
PI
TOTAL SOLIDS
4
92.3
%
SLUDGE
FECAL COLIFORM
388
MPN/g
SLUDGE
14-Oct-22
PI
TOTAL SOLIDS
5
92.8
%
SLUDGE
FECAL COLIFORM
420
MPN/g
SLUDGE
14-Oct-22
PI
TOTAL SOLIDS
6
91.8
%
SLUDGE
FECAL COLIFORM
368
MPN/g
SLUDGE
14-Oct-22
PI
TOTAL SOLIDS
7
91.6
%
SLUDGE
FECAL COLIFORM
354
MPN/g
SLUDGE
14-Oct-22
PI
REPORTED BY: NC CERTIFIED LAB # 544
PAUL ISENHOUR, SUPERVISOR

WATER QUALITY SERVICES, INC.
P-O.'BOX 1102, BANNER ELK, NC 28604
[phone]
fax [phone]
CHAIN OF CUSTODY
TYPE SAMPLE: WASTEWATER
1,OCATION: CUSS -8 51'ORAGJ , 1 P RESERVATION
TIHN COD
FACILITY ID - HCL,
#: �_ 0 O�n dal
.5AMPLER NAME: —OWt� Q F Ro,3ij 4 - NAOH, 5 - NONE, 6 - COOL ICE
;OMPOSITE SAMPLE; START TIME: STOP TIME: 7 - NA2S203, 8 - OTHER
;�
)AMPLE NAME:
"- Laboratory preservation is ensured by addition of pi
containers leaving the lab, unless otherwise noted.
Cl 2-D-CL2= Chlorine check and dechlorin:ation verification:
-f
OJ NJwI to SdII1PIe
)ZESERVATION:
COOL 4C : BOD, RESIDUE, CONDUCTIVITY, MBAS, COLOR, ALKALINITY, CR, VI, TURBIDITY
COOL 4C, PH<2 H2SO4: NH3, NO2-NO3, TKN, O&G, TOC, COD, HARDNESS, PHENOLS, TOT PHOS.
I COOL 4C, PH<2 HNO3 : METALS except CR, VI
) NONE : CHLORIDE, PH, FLUORIDE SAMPLE DEVIATION:
FHER:
COOL 4C, NA2S203 : COLIFORM BACTERIA